#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/00/07/4000747.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4000747
loop_
_publ_author_name
'Riyadi, Syarif'
'Giriyapura, Shivakumara'
'de Groot, Robert A.'
'Caretta, Antonio'
'van Loosdrecht, Paul H. M.'
'Palstra, Thomas T. M.'
'Blake, Graeme R.'
_publ_section_title
;
 Ferromagnetic Order from p-Electrons in Rubidium Oxide
;
_journal_issue                   6
_journal_name_full               'Chemistry of Materials'
_journal_page_first              1578
_journal_paper_doi               10.1021/cm103433r
_journal_volume                  23
_journal_year                    2011
_chemical_formula_sum            'O6.88 Rb4'
_chemical_formula_weight         451.95
_chemical_name_systematic        ' ?'
_space_group_IT_number           69
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-F 2 2'
_symmetry_space_group_name_H-M   'F m m m'
_audit_creation_date             2010-12-01T11:01
_audit_creation_method           'from EXP file using GSAS2CIF'
_audit_update_record
' 2010-12-01T11:01  Initial CIF as created by GSAS2CIF'
_cell_angle_alpha                90.0
_cell_angle_beta                 90.0
_cell_angle_gamma                90.0
_cell_formula_units_Z            1
_cell_length_a                   6.30280(29)
_cell_length_b                   6.25587(23)
_cell_length_c                   5.81797(7)
_cell_measurement_temperature    20
_cell_volume                     229.400(14)
_computing_structure_refinement  GSAS
_diffrn_ambient_temperature      20
_diffrn_radiation_polarisn_ratio 0.7
_diffrn_radiation_probe          x-ray
_diffrn_radiation_wavelength     1.54059
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  1.00000
_exptl_absorpt_process_details
;   GSAS Absorption/surface roughness correction: function number 4
 Flat plate transmission absorption correction
Terms =      0.0000         0.0000    
Correction is not refined.
;
_pd_block_id                     2010-12-01T11:01|RBO2-D_20K|graeme|D8
_pd_calc_method                  'Rietveld Refinement'
_pd_char_colour                  yellow
_pd_instr_location               ' ?'
_pd_meas_2theta_range_inc        0.005
_pd_meas_2theta_range_max        70.0
_pd_meas_2theta_range_min        10.01
_pd_meas_number_of_points        11999
_pd_phase_name                   RbO2_lowT
_pd_proc_2theta_range_inc        0.005
_pd_proc_2theta_range_max        71.3375
_pd_proc_2theta_range_min        11.3475
_pd_proc_info_datetime           2010-12-01T11:01:08
_pd_proc_info_excluded_regions   ' ?'
_pd_proc_ls_background_function
;   GSAS Background function number 1 with 12 terms.
 Shifted Chebyshev function of 1st kind
      1:    505.106     2:    6.02265     3:   -10.7949     4:    5.24962    
      5:    1.92834     6:    4.40346     7:   0.684686     8:   -2.09726    
      9:   0.559522    10:    2.20724    11:   -2.70845    12:   5.564340E-02
;
_pd_proc_ls_peak_cutoff          0.00100
_pd_proc_ls_profile_function
;
 CW Profile function number 4 with  18 terms
 Pseudovoigt profile coefficients as parameterized in
 P. Thompson, D.E. Cox & J.B. Hastings (1987). J. Appl. Cryst.,20,79-83.
 Asymmetry correction of L.W. Finger, D.E. Cox & A. P. Jephcoat (1994).
 J. Appl. Cryst.,27,892-900.
 Microstrain broadening by P.W. Stephens,  (1999). J. Appl. Cryst.,32,281-289.
 Peak tails are ignored  where the intensity is below 0.0010 times the peak
   Aniso. broadening axis   1.0   1.0   0.0
;
_pd_proc_ls_prof_R_factor        0.0101
_pd_proc_ls_prof_wR_expected     0.0431
_pd_proc_ls_prof_wR_factor       0.0143
_pd_proc_number_of_points        11999
_pd_spec_mounting                ' ?'
_refine_ls_goodness_of_fit_all   0.33
_refine_ls_matrix_type           full
_refine_ls_number_parameters     27
_refine_ls_number_restraints     1
_refine_ls_R_Fsqd_factor         0.03820
_refine_ls_shift/su_max          0.06
_refine_ls_shift/su_mean         0.01
_reflns_d_resolution_high        1.434
_reflns_d_resolution_low         3.530
_reflns_limit_h_max              4
_reflns_limit_h_min              0
_reflns_limit_k_max              4
_reflns_limit_k_min              0
_reflns_limit_l_max              4
_reflns_limit_l_min              0
_reflns_number_total             15
_cod_data_source_file            cm103433r_si_002.cif
_cod_data_source_block           RBO2-D_20K_publ
_cod_depositor_comments
;
The following automatic conversions were performed:

'_geom_bond_publ_flag' value 'N' changed to 'n' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29 (98
times).

'_geom_angle_publ_flag' value 'N' changed to 'n' according
to /home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary
named 'cif_core.dic' version 2.4.1 from 2010-06-29 (510 times).

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 

 Adding full bibliography for 4000747.cif.
;
_cod_original_cell_volume        229.400(6)
_cod_original_formula_sum        'O6.88 Rb4.00'
_cod_database_code               4000747
#BEGIN Tags that were not found in dictionaries:
_gsas_exptl_extinct_corr_t_min   1.00000
_gsas_exptl_extinct_corr_t_max   1.00000
#END Tags that were not found in dictionaries
loop_
_symmetry_equiv_pos_site_id
_symmetry_equiv_pos_as_xyz
1 +x,+y,+z
2 -x,+y,+z
3 +x,-y,+z
4 -x,-y,+z
-1 -x,-y,-z
-2 +x,-y,-z
-3 -x,+y,-z
-4 +x,+y,-z
101 +x,+y+1/2,+z+1/2
102 -x,+y+1/2,+z+1/2
103 +x,-y+1/2,+z+1/2
104 -x,-y+1/2,+z+1/2
-101 -x,-y+1/2,-z+1/2
-102 +x,-y+1/2,-z+1/2
-103 -x,+y+1/2,-z+1/2
-104 +x,+y+1/2,-z+1/2
201 +x+1/2,+y,+z+1/2
202 -x+1/2,+y,+z+1/2
203 +x+1/2,-y,+z+1/2
204 -x+1/2,-y,+z+1/2
-201 -x+1/2,-y,-z+1/2
-202 +x+1/2,-y,-z+1/2
-203 -x+1/2,+y,-z+1/2
-204 +x+1/2,+y,-z+1/2
301 +x+1/2,+y+1/2,+z
302 -x+1/2,+y+1/2,+z
303 +x+1/2,-y+1/2,+z
304 -x+1/2,-y+1/2,+z
-301 -x+1/2,-y+1/2,-z
-302 +x+1/2,-y+1/2,-z
-303 -x+1/2,+y+1/2,-z
-304 +x+1/2,+y+1/2,-z
loop_
_atom_site_type_symbol
_atom_site_label
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_thermal_displace_type
_atom_site_U_iso_or_equiv
_atom_site_symmetry_multiplicity
Rb Rb 0.0548(7) 0.0518(5) 0.0 0.25 Uiso 0.0117(7) 16
O Oa 0.3989(7) 0.5287(26) 0.5 0.43 Uiso 0.0194(12) 16
loop_
_atom_type_symbol
_atom_type_number_in_cell
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
Rb 4.0 -0.469 1.608 17.1784 1.78880 9.64350 17.3151 5.13990 0.27480 1.52920
164.934 3.48730 International_Tables_Vol_C
O 6.88 0.049 0.032 3.04850 13.2771 2.28680 5.70110 1.54630 0.32390 0.86700
32.9089 0.25080 International_Tables_Vol_C
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Rb Rb Rb 90.0 2_555 3_555 n
Rb Rb Rb 43.2(6) 2_555 4_555 n
Rb Rb Rb 90.0 2_555 101_544 n
Rb Rb Rb 90.0 2_555 101_545 n
Rb Rb Rb 90.0 2_555 101_554 n
Rb Rb Rb 90.0 2_555 101_555 n
Rb Rb Rb 80.81(11) 2_555 102_544 n
Rb Rb Rb 80.81(11) 2_555 102_545 n
Rb Rb Rb 80.81(11) 2_555 102_554 n
Rb Rb Rb 80.81(11) 2_555 102_555 n
Rb Rb Rb 90.0 2_555 103_544 n
Rb Rb Rb 90.0 2_555 103_545 n
Rb Rb Rb 90.0 2_555 103_554 n
Rb Rb Rb 90.0 2_555 103_555 n
Rb Rb Rb 81.75(11) 2_555 104_544 n
Rb Rb Rb 81.75(11) 2_555 104_545 n
Rb Rb Rb 79.76(12) 2_555 104_554 n
Rb Rb Rb 79.76(12) 2_555 104_555 n
Rb Rb Rb 42.7093(14) 2_555 201_454 n
Rb Rb Rb 42.7094(14) 2_555 201_455 n
Rb Rb Rb 137.2906(14) 2_555 201_554 n
Rb Rb Rb 137.2906(14) 2_555 201_555 n
Rb Rb Rb 37.13(6) 2_555 202_454 n
Rb Rb Rb 37.13(6) 2_555 202_455 n
Rb Rb Rb 46.8(6) 3_555 4_555 n
Rb Rb Rb 42.9229(11) 3_555 101_544 n
Rb Rb Rb 42.9229(11) 3_555 101_545 n
Rb Rb Rb 137.0771(11) 3_555 101_554 n
Rb Rb Rb 137.0771(11) 3_555 101_555 n
Rb Rb Rb 43.707(19) 3_555 102_544 n
Rb Rb Rb 43.707(19) 3_555 102_545 n
Rb Rb Rb 136.292(19) 3_555 102_554 n
Rb Rb Rb 136.292(19) 3_555 102_555 n
Rb Rb Rb 37.61(5) 3_555 103_544 n
Rb Rb Rb 37.61(5) 3_555 103_545 n
Rb Rb Rb 130.45(7) 3_555 103_554 n
Rb Rb Rb 130.45(7) 3_555 103_555 n
Rb Rb Rb 38.38(6) 3_555 104_544 n
Rb Rb Rb 38.38(6) 3_555 104_545 n
Rb Rb Rb 129.68(6) 3_555 104_554 n
Rb Rb Rb 129.68(6) 3_555 104_555 n
Rb Rb Rb 90.0 3_555 201_454 n
Rb Rb Rb 90.0 3_555 201_455 n
Rb Rb Rb 90.0 3_555 201_554 n
Rb Rb Rb 90.0 3_555 201_555 n
Rb Rb Rb 90.0 3_555 202_454 n
Rb Rb Rb 90.0 3_555 202_455 n
Rb Rb Rb 59.9(4) 4_555 101_544 n
Rb Rb Rb 59.9(4) 4_555 101_545 n
Rb Rb Rb 120.1(4) 4_555 101_554 n
Rb Rb Rb 120.1(4) 4_555 101_555 n
Rb Rb Rb 52.35(23) 4_555 102_544 n
Rb Rb Rb 52.35(23) 4_555 102_545 n
Rb Rb Rb 112.2(5) 4_555 102_554 n
Rb Rb Rb 112.2(5) 4_555 102_555 n
Rb Rb Rb 57.2(4) 4_555 103_544 n
Rb Rb Rb 57.2(4) 4_555 103_545 n
Rb Rb Rb 116.34(28) 4_555 103_554 n
Rb Rb Rb 116.34(28) 4_555 103_555 n
Rb Rb Rb 50.15(31) 4_555 104_544 n
Rb Rb Rb 50.15(31) 4_555 104_545 n
Rb Rb Rb 107.9(4) 4_555 104_554 n
Rb Rb Rb 107.9(4) 4_555 104_555 n
Rb Rb Rb 57.6(4) 4_555 201_454 n
Rb Rb Rb 57.6(4) 4_555 201_455 n
Rb Rb Rb 122.4(4) 4_555 201_554 n
Rb Rb Rb 122.4(4) 4_555 201_555 n
Rb Rb Rb 54.4(4) 4_555 202_454 n
Rb Rb Rb 54.4(4) 4_555 202_455 n
Rb Rb Rb 85.8458(22) 101_544 101_545 n
Rb Rb Rb 94.1542(22) 101_544 101_554 n
Rb Rb Rb 180.0 101_544 101_555 n
Rb Rb Rb 9.19(11) 101_544 102_544 n
Rb Rb Rb 85.8992(26) 101_544 102_545 n
Rb Rb Rb 94.1008(26) 101_544 102_554 n
Rb Rb Rb 170.81(11) 101_544 102_555 n
Rb Rb Rb 5.31(5) 101_544 103_544 n
Rb Rb Rb 80.54(5) 101_544 103_545 n
Rb Rb Rb 87.53(7) 101_544 103_554 n
Rb Rb Rb 173.38(7) 101_544 103_555 n
Rb Rb Rb 9.80(7) 101_544 104_544 n
Rb Rb Rb 80.64(5) 101_544 104_545 n
Rb Rb Rb 87.57(7) 101_544 104_554 n
Rb Rb Rb 167.82(8) 101_544 104_555 n
Rb Rb Rb 62.4891(10) 101_544 201_454 n
Rb Rb Rb 117.5109(10) 101_544 201_455 n
Rb Rb Rb 62.4891(10) 101_544 201_554 n
Rb Rb Rb 117.5109(10) 101_544 201_555 n
Rb Rb Rb 65.73(4) 101_544 202_454 n
Rb Rb Rb 114.27(4) 101_544 202_455 n
Rb Rb Rb 180.0 101_545 101_554 n
Rb Rb Rb 94.1542(22) 101_545 101_555 n
Rb Rb Rb 85.8992(26) 101_545 102_544 n
Rb Rb Rb 9.19(11) 101_545 102_545 n
Rb Rb Rb 170.81(11) 101_545 102_554 n
Rb Rb Rb 94.1008(26) 101_545 102_555 n
Rb Rb Rb 80.54(5) 101_545 103_544 n
Rb Rb Rb 5.31(5) 101_545 103_545 n
Rb Rb Rb 173.38(7) 101_545 103_554 n
Rb Rb Rb 87.53(7) 101_545 103_555 n
Rb Rb Rb 80.64(5) 101_545 104_544 n
Rb Rb Rb 9.80(7) 101_545 104_545 n
Rb Rb Rb 167.82(8) 101_545 104_554 n
Rb Rb Rb 87.57(7) 101_545 104_555 n
Rb Rb Rb 117.5109(10) 101_545 201_454 n
Rb Rb Rb 62.4891(10) 101_545 201_455 n
Rb Rb Rb 117.5109(10) 101_545 201_554 n
Rb Rb Rb 62.4891(10) 101_545 201_555 n
Rb Rb Rb 114.27(4) 101_545 202_454 n
Rb Rb Rb 65.73(4) 101_545 202_455 n
Rb Rb Rb 85.8458(22) 101_554 101_555 n
Rb Rb Rb 94.1008(26) 101_554 102_544 n
Rb Rb Rb 170.81(11) 101_554 102_545 n
Rb Rb Rb 9.19(11) 101_554 102_554 n
Rb Rb Rb 85.8992(26) 101_554 102_555 n
Rb Rb Rb 99.46(5) 101_554 103_544 n
Rb Rb Rb 174.69(5) 101_554 103_545 n
Rb Rb Rb 6.63(7) 101_554 103_554 n
Rb Rb Rb 92.47(7) 101_554 103_555 n
Rb Rb Rb 99.36(5) 101_554 104_544 n
Rb Rb Rb 170.20(7) 101_554 104_545 n
Rb Rb Rb 12.18(8) 101_554 104_554 n
Rb Rb Rb 92.43(7) 101_554 104_555 n
Rb Rb Rb 62.4891(10) 101_554 201_454 n
Rb Rb Rb 117.5109(10) 101_554 201_455 n
Rb Rb Rb 62.4891(10) 101_554 201_554 n
Rb Rb Rb 117.5109(10) 101_554 201_555 n
Rb Rb Rb 65.73(4) 101_554 202_454 n
Rb Rb Rb 114.27(4) 101_554 202_455 n
Rb Rb Rb 170.81(11) 101_555 102_544 n
Rb Rb Rb 94.1008(26) 101_555 102_545 n
Rb Rb Rb 85.8992(26) 101_555 102_554 n
Rb Rb Rb 9.19(11) 101_555 102_555 n
Rb Rb Rb 174.69(5) 101_555 103_544 n
Rb Rb Rb 99.46(5) 101_555 103_545 n
Rb Rb Rb 92.47(7) 101_555 103_554 n
Rb Rb Rb 6.63(7) 101_555 103_555 n
Rb Rb Rb 170.20(7) 101_555 104_544 n
Rb Rb Rb 99.36(5) 101_555 104_545 n
Rb Rb Rb 92.43(7) 101_555 104_554 n
Rb Rb Rb 12.18(8) 101_555 104_555 n
Rb Rb Rb 117.5109(10) 101_555 201_454 n
Rb Rb Rb 62.4891(10) 101_555 201_455 n
Rb Rb Rb 117.5109(10) 101_555 201_554 n
Rb Rb Rb 62.4891(10) 101_555 201_555 n
Rb Rb Rb 114.27(4) 101_555 202_454 n
Rb Rb Rb 65.73(4) 101_555 202_455 n
Rb Rb Rb 84.486(33) 102_544 102_545 n
Rb Rb Rb 92.59(4) 102_544 102_554 n
Rb Rb Rb 161.63(22) 102_544 102_555 n
Rb Rb Rb 10.60(8) 102_544 103_544 n
Rb Rb Rb 80.66(5) 102_544 103_545 n
Rb Rb Rb 87.56(7) 102_544 103_554 n
Rb Rb Rb 168.69(7) 102_544 103_555 n
Rb Rb Rb 5.33(5) 102_544 104_544 n
Rb Rb Rb 79.424(32) 102_544 104_545 n
Rb Rb Rb 85.97(5) 102_544 104_554 n
Rb Rb Rb 159.48(20) 102_544 104_555 n
Rb Rb Rb 55.02(9) 102_544 201_454 n
Rb Rb Rb 109.80(10) 102_544 201_455 n
Rb Rb Rb 70.20(10) 102_544 201_554 n
Rb Rb Rb 124.98(9) 102_544 201_555 n
Rb Rb Rb 57.79(6) 102_544 202_454 n
Rb Rb Rb 106.17(14) 102_544 202_455 n
Rb Rb Rb 161.63(22) 102_545 102_554 n
Rb Rb Rb 92.59(4) 102_545 102_555 n
Rb Rb Rb 80.66(5) 102_545 103_544 n
Rb Rb Rb 10.60(8) 102_545 103_545 n
Rb Rb Rb 168.69(7) 102_545 103_554 n
Rb Rb Rb 87.56(7) 102_545 103_555 n
Rb Rb Rb 79.424(32) 102_545 104_544 n
Rb Rb Rb 5.33(5) 102_545 104_545 n
Rb Rb Rb 159.48(20) 102_545 104_554 n
Rb Rb Rb 85.97(5) 102_545 104_555 n
Rb Rb Rb 109.80(10) 102_545 201_454 n
Rb Rb Rb 55.02(9) 102_545 201_455 n
Rb Rb Rb 124.98(9) 102_545 201_554 n
Rb Rb Rb 70.20(10) 102_545 201_555 n
Rb Rb Rb 106.17(14) 102_545 202_454 n
Rb Rb Rb 57.79(6) 102_545 202_455 n
Rb Rb Rb 84.486(33) 102_554 102_555 n
Rb Rb Rb 99.34(5) 102_554 103_544 n
Rb Rb Rb 169.40(8) 102_554 103_545 n
Rb Rb Rb 11.31(7) 102_554 103_554 n
Rb Rb Rb 92.44(7) 102_554 103_555 n
Rb Rb Rb 97.92(8) 102_554 104_544 n
Rb Rb Rb 161.78(20) 102_554 104_545 n
Rb Rb Rb 6.61(7) 102_554 104_554 n
Rb Rb Rb 90.77(10) 102_554 104_555 n
Rb Rb Rb 55.02(9) 102_554 201_454 n
Rb Rb Rb 109.80(10) 102_554 201_455 n
Rb Rb Rb 70.20(10) 102_554 201_554 n
Rb Rb Rb 124.98(9) 102_554 201_555 n
Rb Rb Rb 57.79(6) 102_554 202_454 n
Rb Rb Rb 106.17(14) 102_554 202_455 n
Rb Rb Rb 169.40(8) 102_555 103_544 n
Rb Rb Rb 99.34(5) 102_555 103_545 n
Rb Rb Rb 92.44(7) 102_555 103_554 n
Rb Rb Rb 11.31(7) 102_555 103_555 n
Rb Rb Rb 161.78(20) 102_555 104_544 n
Rb Rb Rb 97.92(8) 102_555 104_545 n
Rb Rb Rb 90.77(10) 102_555 104_554 n
Rb Rb Rb 6.61(7) 102_555 104_555 n
Rb Rb Rb 109.80(10) 102_555 201_454 n
Rb Rb Rb 55.02(9) 102_555 201_455 n
Rb Rb Rb 124.98(9) 102_555 201_554 n
Rb Rb Rb 70.20(10) 102_555 201_555 n
Rb Rb Rb 106.17(14) 102_555 202_454 n
Rb Rb Rb 57.79(6) 102_555 202_455 n
Rb Rb Rb 75.23(10) 103_544 103_545 n
Rb Rb Rb 92.839(27) 103_544 103_554 n
Rb Rb Rb 168.07(12) 103_544 103_555 n
Rb Rb Rb 8.25(11) 103_544 104_544 n
Rb Rb Rb 75.38(10) 103_544 104_545 n
Rb Rb Rb 92.793(26) 103_544 104_554 n
Rb Rb Rb 164.32(7) 103_544 104_555 n
Rb Rb Rb 65.545(28) 103_544 201_454 n
Rb Rb Rb 114.455(28) 103_544 201_455 n
Rb Rb Rb 65.545(28) 103_544 201_554 n
Rb Rb Rb 114.455(28) 103_544 201_555 n
Rb Rb Rb 68.383(22) 103_544 202_454 n
Rb Rb Rb 111.617(22) 103_544 202_455 n
Rb Rb Rb 168.07(12) 103_545 103_554 n
Rb Rb Rb 92.839(27) 103_545 103_555 n
Rb Rb Rb 75.38(10) 103_545 104_544 n
Rb Rb Rb 8.25(11) 103_545 104_545 n
Rb Rb Rb 164.32(7) 103_545 104_554 n
Rb Rb Rb 92.793(26) 103_545 104_555 n
Rb Rb Rb 114.455(28) 103_545 201_454 n
Rb Rb Rb 65.545(28) 103_545 201_455 n
Rb Rb Rb 114.455(28) 103_545 201_554 n
Rb Rb Rb 65.545(28) 103_545 201_555 n
Rb Rb Rb 111.617(22) 103_545 202_454 n
Rb Rb Rb 68.383(22) 103_545 202_455 n
Rb Rb Rb 99.10(15) 103_554 103_555 n
Rb Rb Rb 92.809(26) 103_554 104_544 n
Rb Rb Rb 165.53(7) 103_554 104_545 n
Rb Rb Rb 10.24(12) 103_554 104_554 n
Rb Rb Rb 98.95(15) 103_554 104_555 n
Rb Rb Rb 58.93(4) 103_554 201_454 n
Rb Rb Rb 121.07(4) 103_554 201_455 n
Rb Rb Rb 58.93(4) 103_554 201_554 n
Rb Rb Rb 121.07(4) 103_554 201_555 n
Rb Rb Rb 62.66(7) 103_554 202_454 n
Rb Rb Rb 117.34(7) 103_554 202_455 n
Rb Rb Rb 165.53(7) 103_555 104_544 n
Rb Rb Rb 92.809(26) 103_555 104_545 n
Rb Rb Rb 98.95(15) 103_555 104_554 n
Rb Rb Rb 10.24(12) 103_555 104_555 n
Rb Rb Rb 121.07(4) 103_555 201_454 n
Rb Rb Rb 58.93(4) 103_555 201_455 n
Rb Rb Rb 121.07(4) 103_555 201_554 n
Rb Rb Rb 58.93(4) 103_555 201_555 n
Rb Rb Rb 117.34(7) 103_555 202_454 n
Rb Rb Rb 62.66(7) 103_555 202_455 n
Rb Rb Rb 74.32(8) 104_544 104_545 n
Rb Rb Rb 91.302(25) 104_544 104_554 n
Rb Rb Rb 158.02(15) 104_544 104_555 n
Rb Rb Rb 59.00(11) 104_544 201_454 n
Rb Rb Rb 107.72(7) 104_544 201_455 n
Rb Rb Rb 72.28(7) 104_544 201_554 n
Rb Rb Rb 121.00(11) 104_544 201_555 n
Rb Rb Rb 61.38(8) 104_544 202_454 n
Rb Rb Rb 104.49(11) 104_544 202_455 n
Rb Rb Rb 158.02(15) 104_545 104_554 n
Rb Rb Rb 91.302(25) 104_545 104_555 n
Rb Rb Rb 107.72(7) 104_545 201_454 n
Rb Rb Rb 59.00(11) 104_545 201_455 n
Rb Rb Rb 121.00(11) 104_545 201_554 n
Rb Rb Rb 72.28(7) 104_545 201_555 n
Rb Rb Rb 104.49(11) 104_545 202_454 n
Rb Rb Rb 61.38(8) 104_545 202_455 n
Rb Rb Rb 96.98(18) 104_554 104_555 n
Rb Rb Rb 50.31(7) 104_554 201_454 n
Rb Rb Rb 112.16(13) 104_554 201_455 n
Rb Rb Rb 67.84(13) 104_554 201_554 n
Rb Rb Rb 129.69(7) 104_554 201_555 n
Rb Rb Rb 53.57(5) 104_554 202_454 n
Rb Rb Rb 108.07(17) 104_554 202_455 n
Rb Rb Rb 112.16(13) 104_555 201_454 n
Rb Rb Rb 50.31(7) 104_555 201_455 n
Rb Rb Rb 129.69(7) 104_555 201_554 n
Rb Rb Rb 67.84(13) 104_555 201_555 n
Rb Rb Rb 108.07(17) 104_555 202_454 n
Rb Rb Rb 53.57(5) 104_555 202_455 n
Rb Rb Rb 85.4187(27) 201_454 201_455 n
Rb Rb Rb 94.5813(27) 201_454 201_554 n
Rb Rb Rb 180.0 201_454 201_555 n
Rb Rb Rb 5.58(6) 201_454 202_454 n
Rb Rb Rb 79.84(6) 201_454 202_455 n
Rb Rb Rb 180.0 201_455 201_554 n
Rb Rb Rb 94.5813(27) 201_455 201_555 n
Rb Rb Rb 79.84(6) 201_455 202_454 n
Rb Rb Rb 5.58(6) 201_455 202_455 n
Rb Rb Rb 85.4187(27) 201_554 201_555 n
Rb Rb Rb 100.16(6) 201_554 202_454 n
Rb Rb Rb 174.42(6) 201_554 202_455 n
Rb Rb Rb 174.42(6) 201_555 202_454 n
Rb Rb Rb 100.16(6) 201_555 202_455 n
Rb Rb Rb 74.26(12) 202_454 202_455 n
Rb Oa Rb 0.92(11) 101_555 102_555 n
Rb Oa Rb 16.87(16) 101_555 103_555 n
Rb Oa Rb 13.79(22) 101_555 104_555 n
Rb Oa Rb 112.0(6) 101_555 201_555 n
Rb Oa Rb 102.9(5) 101_555 201_565 n
Rb Oa Rb 99.4(6) 101_555 202_555 n
Rb Oa Rb 91.3(4) 101_555 202_565 n
Rb Oa Rb 106.7(5) 101_555 203_565 n
Rb Oa Rb 92.5(4) 101_555 204_565 n
Rb Oa Rb 108.41(8) 101_555 301_555 n
Rb Oa Rb 108.41(8) 101_555 301_556 n
Rb Oa Rb 95.52(10) 101_555 302_555 n
Rb Oa Rb 95.52(10) 101_555 302_556 n
Rb Oa Rb 109.02(14) 101_555 303_555 n
Rb Oa Rb 109.02(14) 101_555 303_556 n
Rb Oa Rb 96.28(20) 101_555 304_555 n
Rb Oa Rb 96.28(20) 101_555 304_556 n
Rb Oa Oa 176.2(5) 101_555 2_655 n
Rb Oa Oa 93.8(5) 101_555 3_565 n
Rb Oa Oa 168.1(19) 101_555 4_665 n
Rb Oa Rb 15.95(14) 102_555 103_555 n
Rb Oa Rb 12.87(15) 102_555 104_555 n
Rb Oa Rb 111.1(5) 102_555 201_555 n
Rb Oa Rb 103.8(4) 102_555 201_565 n
Rb Oa Rb 98.5(5) 102_555 202_555 n
Rb Oa Rb 92.20(27) 102_555 202_565 n
Rb Oa Rb 107.6(4) 102_555 203_565 n
Rb Oa Rb 93.45(26) 102_555 204_565 n
Rb Oa Rb 108.48(8) 102_555 301_555 n
Rb Oa Rb 108.48(8) 102_555 301_556 n
Rb Oa Rb 95.57(11) 102_555 302_555 n
Rb Oa Rb 95.57(11) 102_555 302_556 n
Rb Oa Rb 108.88(13) 102_555 303_555 n
Rb Oa Rb 108.88(13) 102_555 303_556 n
Rb Oa Rb 96.13(18) 102_555 304_555 n
Rb Oa Rb 96.13(18) 102_555 304_556 n
Rb Oa Oa 177.11(35) 102_555 2_655 n
Rb Oa Oa 92.89(35) 102_555 3_565 n
Rb Oa Oa 167.2(18) 102_555 4_665 n
Rb Oa Rb 3.08(10) 103_555 104_555 n
Rb Oa Rb 95.2(6) 103_555 201_555 n
Rb Oa Rb 119.8(4) 103_555 201_565 n
Rb Oa Rb 82.5(5) 103_555 202_555 n
Rb Oa Rb 108.16(33) 103_555 202_565 n
Rb Oa Rb 123.6(4) 103_555 203_565 n
Rb Oa Rb 109.41(33) 103_555 204_565 n
Rb Oa Rb 108.79(15) 103_555 301_555 n
Rb Oa Rb 108.79(15) 103_555 301_556 n
Rb Oa Rb 96.22(20) 103_555 302_555 n
Rb Oa Rb 96.22(20) 103_555 302_556 n
Rb Oa Rb 105.73(25) 103_555 303_555 n
Rb Oa Rb 105.73(25) 103_555 303_556 n
Rb Oa Rb 93.30(27) 103_555 304_555 n
Rb Oa Rb 93.30(27) 103_555 304_556 n
Rb Oa Oa 166.9(4) 103_555 2_655 n
Rb Oa Oa 76.9(4) 103_555 3_565 n
Rb Oa Oa 151.2(19) 103_555 4_665 n
Rb Oa Rb 98.3(5) 104_555 201_555 n
Rb Oa Rb 116.69(33) 104_555 201_565 n
Rb Oa Rb 85.6(4) 104_555 202_555 n
Rb Oa Rb 105.08(26) 104_555 202_565 n
Rb Oa Rb 120.5(4) 104_555 203_565 n
Rb Oa Rb 106.32(26) 104_555 204_565 n
Rb Oa Rb 108.84(13) 104_555 301_555 n
Rb Oa Rb 108.84(13) 104_555 301_556 n
Rb Oa Rb 96.13(18) 104_555 302_555 n
Rb Oa Rb 96.13(18) 104_555 302_556 n
Rb Oa Rb 106.44(21) 104_555 303_555 n
Rb Oa Rb 106.44(21) 104_555 303_556 n
Rb Oa Rb 93.87(23) 104_555 304_555 n
Rb Oa Rb 93.87(23) 104_555 304_556 n
Rb Oa Oa 170.02(31) 104_555 2_655 n
Rb Oa Oa 80.02(31) 104_555 3_565 n
Rb Oa Oa 154.3(18) 104_555 4_665 n
Rb Oa Rb 145.05(18) 201_555 201_565 n
Rb Oa Rb 12.64(14) 201_555 202_555 n
Rb Oa Rb 156.67(23) 201_555 202_565 n
Rb Oa Rb 141.24(16) 201_555 203_565 n
Rb Oa Rb 155.42(25) 201_555 204_565 n
Rb Oa Rb 86.83(25) 201_555 301_555 n
Rb Oa Rb 86.83(25) 201_555 301_556 n
Rb Oa Rb 90.90(26) 201_555 302_555 n
Rb Oa Rb 90.90(26) 201_555 302_556 n
Rb Oa Rb 75.38(23) 201_555 303_555 n
Rb Oa Rb 75.38(23) 201_555 303_556 n
Rb Oa Rb 78.94(26) 201_555 304_555 n
Rb Oa Rb 78.94(26) 201_555 304_556 n
Rb Oa Oa 71.77(16) 201_555 2_655 n
Rb Oa Oa 18.23(16) 201_555 3_565 n
Rb Oa Oa 56.1(13) 201_555 4_665 n
Rb Oa Rb 157.70(12) 201_565 202_555 n
Rb Oa Rb 11.62(18) 201_565 202_565 n
Rb Oa Rb 3.81(4) 201_565 203_565 n
Rb Oa Rb 10.37(21) 201_565 204_565 n
Rb Oa Rb 82.13(31) 201_565 301_555 n
Rb Oa Rb 82.13(31) 201_565 301_556 n
Rb Oa Rb 85.6(4) 201_565 302_555 n
Rb Oa Rb 85.6(4) 201_565 302_556 n
Rb Oa Rb 93.67(31) 201_565 303_555 n
Rb Oa Rb 93.67(31) 201_565 303_556 n
Rb Oa Rb 97.71(33) 201_565 304_555 n
Rb Oa Rb 97.71(33) 201_565 304_556 n
Rb Oa Oa 73.28(8) 201_565 2_655 n
Rb Oa Oa 163.28(8) 201_565 3_565 n
Rb Oa Oa 89.0(15) 201_565 4_665 n
Rb Oa Rb 169.32(27) 202_555 202_565 n
Rb Oa Rb 153.89(10) 202_555 203_565 n
Rb Oa Rb 168.07(29) 202_555 204_565 n
Rb Oa Rb 90.90(26) 202_555 301_555 n
Rb Oa Rb 90.90(26) 202_555 301_556 n
Rb Oa Rb 92.26(30) 202_555 302_555 n
Rb Oa Rb 92.26(30) 202_555 302_556 n
Rb Oa Rb 78.95(26) 202_555 303_555 n
Rb Oa Rb 78.95(26) 202_555 303_556 n
Rb Oa Rb 79.72(30) 202_555 304_555 n
Rb Oa Rb 79.72(30) 202_555 304_556 n
Rb Oa Oa 84.41(17) 202_555 2_655 n
Rb Oa Oa 5.59(17) 202_555 3_565 n
Rb Oa Oa 68.7(13) 202_555 4_665 n
Rb Oa Rb 15.43(18) 202_565 203_565 n
Rb Oa Rb 1.248(31) 202_565 204_565 n
Rb Oa Rb 85.69(35) 202_565 301_555 n
Rb Oa Rb 85.69(35) 202_565 301_556 n
Rb Oa Rb 86.7(4) 202_565 302_555 n
Rb Oa Rb 86.7(4) 202_565 302_556 n
Rb Oa Rb 97.64(33) 202_565 303_555 n
Rb Oa Rb 97.64(33) 202_565 303_556 n
Rb Oa Rb 99.22(33) 202_565 304_555 n
Rb Oa Rb 99.22(33) 202_565 304_556 n
Rb Oa Oa 84.90(10) 202_565 2_655 n
Rb Oa Oa 174.90(10) 202_565 3_565 n
Rb Oa Oa 100.6(16) 202_565 4_665 n
Rb Oa Rb 14.18(21) 203_565 204_565 n
Rb Oa Rb 81.02(30) 203_565 301_555 n
Rb Oa Rb 81.02(30) 203_565 301_556 n
Rb Oa Rb 85.3(4) 203_565 302_555 n
Rb Oa Rb 85.3(4) 203_565 302_556 n
Rb Oa Rb 92.33(30) 203_565 303_555 n
Rb Oa Rb 92.33(30) 203_565 303_556 n
Rb Oa Rb 97.14(33) 203_565 304_555 n
Rb Oa Rb 97.14(33) 203_565 304_556 n
Rb Oa Oa 69.47(8) 203_565 2_655 n
Rb Oa Oa 159.47(8) 203_565 3_565 n
Rb Oa Oa 85.2(14) 203_565 4_665 n
Rb Oa Rb 85.3(4) 204_565 301_555 n
Rb Oa Rb 85.3(4) 204_565 301_556 n
Rb Oa Rb 86.6(4) 204_565 302_555 n
Rb Oa Rb 86.6(4) 204_565 302_556 n
Rb Oa Rb 97.23(34) 204_565 303_555 n
Rb Oa Rb 97.23(34) 204_565 303_556 n
Rb Oa Rb 99.07(34) 204_565 304_555 n
Rb Oa Rb 99.07(34) 204_565 304_556 n
Rb Oa Oa 83.65(13) 204_565 2_655 n
Rb Oa Oa 173.66(13) 204_565 3_565 n
Rb Oa Oa 99.4(16) 204_565 4_665 n
Rb Oa Rb 142.29(24) 301_555 301_556 n
Rb Oa Rb 12.92(16) 301_555 302_555 n
Rb Oa Rb 155.00(31) 301_555 302_556 n
Rb Oa Rb 12.00(12) 301_555 303_555 n
Rb Oa Rb 142.32(15) 301_555 303_556 n
Rb Oa Rb 17.92(8) 301_555 304_555 n
Rb Oa Rb 154.756(31) 301_555 304_556 n
Rb Oa Oa 71.36(9) 301_555 2_655 n
Rb Oa Oa 92.69(32) 301_555 3_565 n
Rb Oa Oa 72.84(19) 301_555 4_665 n
Rb Oa Rb 155.00(31) 301_556 302_555 n
Rb Oa Rb 12.92(16) 301_556 302_556 n
Rb Oa Rb 142.32(15) 301_556 303_555 n
Rb Oa Rb 12.00(12) 301_556 303_556 n
Rb Oa Rb 154.756(31) 301_556 304_555 n
Rb Oa Rb 17.92(8) 301_556 304_556 n
Rb Oa Oa 71.36(9) 301_556 2_655 n
Rb Oa Oa 92.69(32) 301_556 3_565 n
Rb Oa Oa 72.84(19) 301_556 4_665 n
Rb Oa Rb 167.2(5) 302_555 302_556 n
Rb Oa Rb 17.70(7) 302_555 303_555 n
Rb Oa Rb 154.906(32) 302_555 303_556 n
Rb Oa Rb 12.59(13) 302_555 304_555 n
Rb Oa Rb 166.67(19) 302_555 304_556 n
Rb Oa Oa 84.28(14) 302_555 2_655 n
Rb Oa Oa 92.83(33) 302_555 3_565 n
Rb Oa Oa 85.26(15) 302_555 4_665 n
Rb Oa Rb 154.906(32) 302_556 303_555 n
Rb Oa Rb 17.70(7) 302_556 303_556 n
Rb Oa Rb 166.67(19) 302_556 304_555 n
Rb Oa Rb 12.59(13) 302_556 304_556 n
Rb Oa Oa 84.28(14) 302_556 2_655 n
Rb Oa Oa 92.83(33) 302_556 3_565 n
Rb Oa Oa 85.26(15) 302_556 4_665 n
Rb Oa Rb 138.43(18) 303_555 303_556 n
Rb Oa Rb 12.77(16) 303_555 304_555 n
Rb Oa Rb 149.12(25) 303_555 304_556 n
Rb Oa Oa 71.59(10) 303_555 2_655 n
Rb Oa Oa 80.69(31) 303_555 3_565 n
Rb Oa Oa 69.64(14) 303_555 4_665 n
Rb Oa Rb 149.12(25) 303_556 304_555 n
Rb Oa Rb 12.77(16) 303_556 304_556 n
Rb Oa Oa 71.59(10) 303_556 2_655 n
Rb Oa Oa 80.69(31) 303_556 3_565 n
Rb Oa Oa 69.64(14) 303_556 4_665 n
Rb Oa Rb 157.4(5) 304_555 304_556 n
Rb Oa Oa 84.35(14) 304_555 2_655 n
Rb Oa Oa 80.23(32) 304_555 3_565 n
Rb Oa Oa 81.91(19) 304_555 4_665 n
Rb Oa Oa 84.35(14) 304_556 2_655 n
Rb Oa Oa 80.23(32) 304_556 3_565 n
Rb Oa Oa 81.91(19) 304_556 4_665 n
Oa Oa Oa 90.0 2_655 3_565 n
Oa Oa Oa 15.7(15) 2_655 4_665 n
Oa Oa Oa 74.3(15) 3_565 4_665 n
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Rb Rb 0.691(9) 2_555 n
Rb Rb 0.648(7) 3_555 n
Rb Rb 0.947(4) 4_555 n
Rb Rb 4.27155(9) 101_544 n
Rb Rb 4.27155(9) 101_545 n
Rb Rb 4.27155(9) 101_554 n
Rb Rb 4.27155(9) 101_555 n
Rb Rb 4.3271(14) 102_544 n
Rb Rb 4.3271(14) 102_545 n
Rb Rb 4.3271(14) 102_554 n
Rb Rb 4.3271(14) 102_555 n
Rb Rb 4.766(5) 103_544 n
Rb Rb 4.766(5) 103_545 n
Rb Rb 3.823(4) 103_554 n
Rb Rb 3.823(4) 103_555 n
Rb Rb 4.816(4) 104_544 n
Rb Rb 4.816(4) 104_545 n
Rb Rb 3.885(5) 104_554 n
Rb Rb 3.885(5) 104_555 n
Rb Rb 4.28877(11) 201_454 n
Rb Rb 4.28877(11) 201_455 n
Rb Rb 4.28877(11) 201_554 n
Rb Rb 4.28877(11) 201_555 n
Rb Rb 4.819(7) 202_454 n
Rb Rb 4.819(7) 202_455 n
Rb Rb 3.810(6) 202_554 n
Rb Rb 3.810(6) 202_555 n
Rb Rb 4.3374(10) 203_454 n
Rb Rb 4.3374(10) 203_455 n
Rb Rb 4.3374(10) 203_554 n
Rb Rb 4.3374(10) 203_555 n
Rb Rb 4.863(6) 204_454 n
Rb Rb 4.863(6) 204_455 n
Rb Rb 3.865(6) 204_554 n
Rb Rb 3.865(6) 204_555 n
Rb Rb 4.44019(13) 301_445 n
Rb Rb 4.44019(13) 301_455 n
Rb Rb 4.44019(13) 301_545 n
Rb Rb 4.44019(13) 301_555 n
Rb Rb 4.954(7) 302_445 n
Rb Rb 4.954(7) 302_455 n
Rb Rb 3.980(5) 302_545 n
Rb Rb 3.980(5) 302_555 n
Rb Rb 4.918(5) 303_445 n
Rb Rb 4.010(4) 303_455 n
Rb Rb 4.918(5) 303_545 n
Rb Rb 4.010(4) 303_555 n
Rb Rb 5.387(4) 304_445 n
Rb Rb 4.573(10) 304_455 n
Rb Rb 4.507(9) 304_545 n
Rb Rb 3.494(4) 304_555 n
Rb Oa 2.173(5) 101_544 n
Rb Oa 2.863(7) 102_544 n
Rb Oa 3.446(8) 102_644 n
Rb Oa 2.226(8) 103_554 n
Rb Oa 2.903(9) 104_554 n
Rb Oa 3.480(6) 104_654 n
Rb Oa 3.417(17) 201_444 n
Rb Oa 3.141(15) 201_454 n
Rb Oa 3.285(18) 202_544 n
Rb Oa 2.998(16) 202_554 n
Rb Oa 3.762(15) 203_454 n
Rb Oa 2.803(17) 203_464 n
Rb Oa 3.643(16) 204_554 n
Rb Oa 2.641(17) 204_564 n
Rb Oa 3.0739(22) 301_444 n
Rb Oa 3.0739(22) 301_445 n
Rb Oa 2.9272(15) 302_544 n
Rb Oa 2.9272(15) 302_545 n
Rb Oa 3.1114(19) 303_454 n
Rb Oa 3.1114(19) 303_455 n
Rb Oa 2.9666(23) 304_554 n
Rb Oa 2.9666(23) 304_555 n
Oa Rb 2.173(5) 101_555 n
Oa Rb 2.863(7) 102_555 n
Oa Rb 3.446(8) 102_655 n
Oa Rb 2.226(8) 103_555 n
Oa Rb 2.903(9) 104_555 n
Oa Rb 3.480(6) 104_655 n
Oa Rb 3.141(15) 201_555 n
Oa Rb 3.417(17) 201_565 n
Oa Rb 2.998(16) 202_555 n
Oa Rb 3.285(18) 202_565 n
Oa Rb 3.762(15) 203_555 n
Oa Rb 2.803(17) 203_565 n
Oa Rb 3.643(16) 204_555 n
Oa Rb 2.641(17) 204_565 n
Oa Rb 3.0739(22) 301_555 n
Oa Rb 3.0739(22) 301_556 n
Oa Rb 2.9272(15) 302_555 n
Oa Rb 2.9272(15) 302_556 n
Oa Rb 3.1114(19) 303_555 n
Oa Rb 3.1114(19) 303_556 n
Oa Rb 2.9666(23) 304_555 n
Oa Rb 2.9666(23) 304_556 n
Oa Oa 1.275(9) 2_655 n
Oa Oa 0.359(33) 3_565 n
Oa Oa 1.3241(16) 4_665 n
loop_
_pd_meas_counts_total
_pd_proc_ls_weight
_pd_proc_intensity_bkg_calc
_pd_calc_intensity_total
477.0 . . .
474.0 . . .
474.0 . . .
474.0 . . .
472.0 . . .
472.0 . . .
471.0 . . .
478.0 . . .
477.0 . . .
477.0 . . .
477.0 . . .
478.0 . . .
480.0 . . .
477.0 . . .
472.0 . . .
477.0 . . .
478.0 . . .
479.0 . . .
474.0 . . .
478.0 . . .
477.0 . . .
475.0 . . .
475.0 . . .
477.0 . . .
478.0 . . .
478.0 . . .
474.0 . . .
477.0 . . .
479.0 . . .
474.0 . . .
475.0 . . .
475.0 . . .
474.0 . . .
477.0 . . .
472.0 . . .
476.0 . . .
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473.0 . . .
476.0 . . .
478.0 . . .
478.0 . . .
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481.0 . . .
484.0 . . .
481.0 . . .
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479.0 . . .
477.0 . . .
477.0 . . .
476.0 . . .
479.0 . . .
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476.0 . . .
476.0 . . .
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476.0 . . .
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478.0 . . .
480.0 . . .
483.0 . . .
477.0 . . .
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480.0 . . .
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476.0 . . .
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481.0 . . .
475.0 . . .
475.0 . . .
474.0 . . .
478.0 . . .
478.0 . . .
473.0 . . .
475.0 . . .
475.0 . . .
478.0 . . .
474.0 . . .
473.0 . . .
475.0 . . .
475.0 . . .
475.0 . . .
476.0 . . .
476.0 . . .
475.0 . . .
476.0 . . .
479.0 . . .
481.0 . . .
481.0 . . .
477.0 . . .
477.0 . . .
480.0 . . .
479.0 . . .
479.0 . . .
478.0 . . .
481.0 . . .
478.0 . . .
479.0 . . .
483.0 . . .
480.0 . . .
476.0 . . .
476.0 . . .
475.0 . . .
477.0 . . .
478.0 . . .
472.0 . . .
478.0 . . .
480.0 . . .
478.0 . . .
477.0 . . .
480.0 . . .
485.0 . . .
480.0 . . .
478.0 . . .
479.0 . . .
479.0 . . .
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498.0 0.002008 504.70145 505.44363
499.0 0.002004 504.69482 505.43698
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505.0 0.001980 504.66171 505.40332
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505.0 0.001980 504.58170 505.32285
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504.0 0.001984 504.56161 505.30267
507.0 0.001972 504.55490 505.29608
507.0 0.001972 504.54816 505.28928
505.0 0.001980 504.54144 505.28262
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508.0 0.001969 504.52798 505.26917
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503.0 0.001988 504.51453 505.25583
500.0 0.002000 504.50778 505.24911
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505.0 0.001980 504.41287 505.15552
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503.0 0.001988 504.39240 505.13565
504.0 0.001984 504.38556 505.12894
504.0 0.001984 504.37872 505.12225
504.0 0.001984 504.37189 505.11563
510.0 0.001961 504.36505 505.10892
511.0 0.001957 504.35822 505.10223
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512.0 0.001953 504.33762 505.08234
512.0 0.001953 504.33075 505.07571
510.0 0.001961 504.32388 505.06912
505.0 0.001980 504.31702 505.06241
512.0 0.001953 504.31012 505.05582
511.0 0.001957 504.30325 505.04913
507.0 0.001972 504.29636 505.04248
512.0 0.001953 504.28946 505.03586
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513.0 0.001949 504.27563 505.02264
508.0 0.001969 504.26874 505.01602
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504.0 0.001984 504.25488 505.00275
510.0 0.001961 504.24799 504.99619
512.0 0.001953 504.24103 504.98956
511.0 0.001957 504.23410 504.98297
510.0 0.001961 504.22717 504.97629
509.0 0.001965 504.22021 504.96982
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506.0 0.001976 504.19937 504.94995
508.0 0.001969 504.19241 504.94336
506.0 0.001976 504.18542 504.93683
499.0 0.002004 504.17847 504.93021
504.0 0.001984 504.17148 504.92365
507.0 0.001972 504.16449 504.91705
511.0 0.001957 504.15750 504.91052
508.0 0.001969 504.15051 504.90396
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513.0 0.001949 504.13651 504.89087
511.0 0.001957 504.12952 504.88425
507.0 0.001972 504.12250 504.87775
510.0 0.001961 504.11548 504.87119
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517.0 0.001934 504.10144 504.85812
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504.0 0.001984 503.81656 504.60123
506.0 0.001976 503.80933 504.59488
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509.0 0.001965 503.73691 504.53256
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516.0 0.001938 503.71509 504.51404
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505.0 0.001980 503.68591 504.48953
504.0 0.001984 503.67862 504.48337
507.0 0.001972 503.67133 504.48752
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514.0 0.001946 503.62006 504.44519
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507.0 0.001972 503.58331 504.41531
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506.0 0.001976 503.53168 504.37411
507.0 0.001972 503.52429 504.36826
502.0 0.001992 503.51688 504.36252
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507.0 0.001972 503.49466 504.34512
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505.0 0.001980 503.31552 504.21191
502.0 0.001992 503.30801 504.20657
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504.0 0.001984 503.29297 504.19601
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502.0 0.001992 503.27789 504.18564
502.0 0.001992 503.27036 504.18045
502.0 0.001992 503.26282 504.17532
502.0 0.001992 503.25528 504.17014
498.0 0.002008 503.24771 504.16501
501.0 0.001996 503.24017 504.15994
503.0 0.001988 503.23260 504.15491
503.0 0.001988 503.22507 504.14987
501.0 0.001996 503.21750 504.14487
504.0 0.001984 503.20993 504.13989
503.0 0.001988 503.20236 504.13495
499.0 0.002004 503.19476 504.13000
499.0 0.002004 503.18719 504.12506
504.0 0.001984 503.17960 504.12024
505.0 0.001980 503.17203 504.11539
506.0 0.001976 503.16443 504.11057
501.0 0.001996 503.15683 504.10587
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510.0 0.001961 503.14163 504.09631
503.0 0.001988 503.13400 504.09164
501.0 0.001996 503.12640 504.08704
503.0 0.001988 503.11880 504.08237
504.0 0.001984 503.11118 504.07770
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499.0 0.002004 503.09592 504.06873
502.0 0.001992 503.08829 504.06421
503.0 0.001988 503.08066 504.05972
498.0 0.002008 503.07303 504.05533
503.0 0.001988 503.06537 504.05087
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502.0 0.001992 503.05008 504.04233
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498.0 0.002008 503.03476 504.03369
508.0 0.001969 503.02710 504.02954
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504.0 0.001984 502.90405 503.96802
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498.0 0.002008 502.84995 503.94482
504.0 0.001984 502.84219 503.94168
500.0 0.002000 502.83447 503.93863
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495.0 0.002020 502.81897 503.93271
499.0 0.002004 502.81119 503.92981
498.0 0.002008 502.80344 503.92703
497.0 0.002012 502.79568 503.92419
497.0 0.002012 502.78790 503.92154
501.0 0.001996 502.78015 503.91885
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503.0 0.001988 502.76459 503.91382
497.0 0.002012 502.75681 503.91129
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501.0 0.001996 502.74124 503.90665
505.0 0.001980 502.73346 503.90436
504.0 0.001984 502.72568 503.90216
503.0 0.001988 502.71786 503.89999
501.0 0.001996 502.71008 503.89798
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495.0 0.002020 502.69446 503.89410
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494.0 0.002024 502.38010 503.88834
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502.0 0.001992 502.22153 503.95355
501.0 0.001996 502.21359 503.95834
502.0 0.001992 502.20563 503.96329
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494.0 0.002024 501.96643 504.18729
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495.0 0.002020 501.77444 504.46915
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526.0 . . .
520.0 . . .
523.0 . . .
521.0 . . .
522.0 . . .
526.0 . . .
526.0 . . .
527.0 . . .
526.0 . . .
527.0 . . .
524.0 . . .
526.0 . . .
528.0 . . .
525.0 . . .
531.0 . . .
533.0 . . .
530.0 . . .
532.0 . . .
528.0 . . .
527.0 . . .
523.0 . . .
524.0 . . .
532.0 . . .
529.0 . . .
527.0 . . .
530.0 . . .
532.0 . . .
535.0 . . .
534.0 . . .
534.0 . . .
536.0 . . .
534.0 . . .
533.0 . . .
532.0 . . .
535.0 . . .
538.0 . . .
535.0 . . .
537.0 . . .
541.0 . . .
540.0 . . .
536.0 . . .
534.0 . . .
530.0 . . .
532.0 . . .
536.0 . . .
542.0 . . .
543.0 . . .
538.0 . . .
544.0 . . .
541.0 . . .
544.0 . . .
537.0 . . .
