#------------------------------------------------------------------------------
#$Date: 2016-03-21 01:21:50 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178377 $
#$URL: svn://www.crystallography.net/cod/cif/4/00/16/4001616.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4001616
loop_
_publ_author_name
'Phelan, W. Adam'
'Menard, Melissa C.'
'Kangas, Michael J.'
'McCandless, Gregory T.'
'Drake, Brenton L.'
'Chan, Julia Y.'
_publ_section_title
;
 Adventures in Crystal Growth: Synthesis and Characterization of Single
 Crystals of Complex Intermetallic Compounds
;
_journal_issue                   3
_journal_name_full               'Chemistry of Materials'
_journal_page_first              409
_journal_paper_doi               10.1021/cm2019873
_journal_volume                  24
_journal_year                    2012
_chemical_formula_sum            'Ga9 Pd3 Yb1.97'
_chemical_formula_weight         1287.14
_space_group_IT_number           63
_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_audit_update_record
;
2011-11-21 # Formatted by publCIF
;
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   13.166(4)
_cell_length_b                   7.605(2)
_cell_length_c                   9.496(3)
_cell_measurement_reflns_used    816
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      30.034
_cell_measurement_theta_min      2.546
_cell_volume                     950.8(5)
_computing_cell_refinement       'HKL SCALEPACK (Otwinowski & Minor, 1997)'
_computing_data_collection       'COLLECT (Nonius, 2000)'
_computing_data_reduction
'HKL DENZO and SCALEPACK (Otwinowski & Minor, 1997)'
_computing_molecular_graphics    'CrystalMaker for Windows'
_computing_publication_material
'SHELXL97 (Sheldrick, 2008) and publCIF (Westrip, 2010)'
_computing_structure_refinement  'SHELXL97 (Sheldrick, 2008)'
_computing_structure_solution    'SIR97 (Altomare et al., 1999)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Nonius KappaCCD'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0926
_diffrn_reflns_av_sigmaI/netI    0.0520
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            4499
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         30.23
_diffrn_reflns_theta_min         3.09
_exptl_absorpt_coefficient_mu    49.612
_exptl_absorpt_correction_T_max  0.1905
_exptl_absorpt_correction_T_min  0.1905
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'HKL SCALEPACK (Otwinowski & Minor, 1997)'
_exptl_crystal_density_diffrn    8.992
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             2219
_exptl_crystal_size_max          0.05
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.05
_refine_diff_density_max         2.527
_refine_diff_density_min         -2.979
_refine_diff_density_rms         0.479
_refine_ls_extinction_coef       0.00136(9)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.893
_refine_ls_matrix_type           full
_refine_ls_number_parameters     71
_refine_ls_number_reflns         776
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.893
_refine_ls_R_factor_all          0.0754
_refine_ls_R_factor_gt           0.0297
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0419P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0731
_refine_ls_wR_factor_ref         0.0984
_reflns_number_gt                271
_reflns_number_total             776
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cm2019873_si_002.cif
_cod_data_source_block           mb9OrthorhombicCmcm
_cod_original_cell_volume        950.8(4)
_cod_database_code               4001616
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'x, -y, -z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'x+1/2, -y+1/2, -z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z-1/2'
'-x, y, z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'-x+1/2, y+1/2, z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Yb1 Yb 0.33315(10) 0.33323(10) 0.2500 0.0080(3) Uani 0.6666(19) 2 d SP
Pd1 Pd 0.33299(9) 0.0000 0.0000 0.0082(3) Uani 1 2 d S
Pd2 Pd 0.0000 0.0000 0.0000 0.0074(5) Uani 1 4 d S
Ga1 Ga 0.16665(9) 0.16653(10) 0.07629(12) 0.0100(3) Uani 1 1 d .
Ga2 Ga 0.0000 0.33409(17) 0.5761(2) 0.0096(5) Uani 1 2 d S
Ga3 Ga 0.1048(4) 0.4357(6) 0.2500 0.0165(19) Uani 0.391(4) 2 d SP
Ga4 Ga 0.0000 0.1254(8) 0.2500 0.014(3) Uani 0.346(7) 4 d SP
Yb2 Yb 0.0000 0.33335(18) 0.2500 0.0067(6) Uani 0.641(3) 4 d SP
Ga5 Ga 0.4375(4) 0.4376(6) 0.2500 0.0069(18) Uani 0.305(4) 2 d SP
Ga6 Ga 0.2293(4) 0.4330(7) 0.2500 0.010(2) Uani 0.322(5) 2 d SP
Ga7 Ga 0.3326(4) 0.1257(5) 0.2500 0.0052(15) Uani 0.310(4) 2 d SP
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Yb Yb -0.3850 5.5486 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ga Ga 0.2307 1.6083 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ga6 Yb1 Ga7 118.8(3) . .
Ga6 Yb1 Ga5 121.0(2) . .
Ga7 Yb1 Ga5 120.3(3) . .
Ga6 Yb1 Ga1 64.49(15) . 10_556
Ga7 Yb1 Ga1 65.00(17) . 10_556
Ga5 Yb1 Ga1 146.92(3) . 10_556
Ga6 Yb1 Ga1 64.49(15) . .
Ga7 Yb1 Ga1 65.00(17) . .
Ga5 Yb1 Ga1 146.92(3) . .
Ga1 Yb1 Ga1 66.16(5) 10_556 .
Ga6 Yb1 Ga1 66.05(15) . 8
Ga7 Yb1 Ga1 146.95(2) . 8
Ga5 Yb1 Ga1 65.16(13) . 8
Ga1 Yb1 Ga1 93.13(4) 10_556 8
Ga1 Yb1 Ga1 130.54(4) . 8
Ga6 Yb1 Ga1 66.05(15) . 15
Ga7 Yb1 Ga1 146.95(2) . 15
Ga5 Yb1 Ga1 65.16(13) . 15
Ga1 Yb1 Ga1 130.54(4) 10_556 15
Ga1 Yb1 Ga1 93.13(4) . 15
Ga1 Yb1 Ga1 66.11(5) 8 15
Ga6 Yb1 Ga2 146.94(4) . 13_556
Ga7 Yb1 Ga2 65.35(17) . 13_556
Ga5 Yb1 Ga2 65.30(13) . 13_556
Ga1 Yb1 Ga2 92.99(3) 10_556 13_556
Ga1 Yb1 Ga2 130.35(4) . 13_556
Ga1 Yb1 Ga2 93.10(4) 8 13_556
Ga1 Yb1 Ga2 130.46(5) 15 13_556
Ga6 Yb1 Ga2 146.94(4) . 6_554
Ga7 Yb1 Ga2 65.35(17) . 6_554
Ga5 Yb1 Ga2 65.30(13) . 6_554
Ga1 Yb1 Ga2 130.35(4) 10_556 6_554
Ga1 Yb1 Ga2 92.99(3) . 6_554
Ga1 Yb1 Ga2 130.46(5) 8 6_554
Ga1 Yb1 Ga2 93.10(4) 15 6_554
Ga2 Yb1 Ga2 66.09(7) 13_556 6_554
Ga6 Yb1 Ga1 90.03(3) . 6
Ga7 Yb1 Ga1 90.03(2) . 6
Ga5 Yb1 Ga1 89.94(3) . 6
Ga1 Yb1 Ga1 56.98(4) 10_556 6
Ga1 Yb1 Ga1 123.14(4) . 6
Ga1 Yb1 Ga1 56.91(3) 8 6
Ga1 Yb1 Ga1 123.02(3) 15 6
Ga2 Yb1 Ga1 56.93(4) 13_556 6
Ga2 Yb1 Ga1 123.02(5) 6_554 6
Ga6 Yb1 Ga1 90.03(3) . 13
Ga7 Yb1 Ga1 90.03(2) . 13
Ga5 Yb1 Ga1 89.94(3) . 13
Ga1 Yb1 Ga1 123.14(4) 10_556 13
Ga1 Yb1 Ga1 56.98(4) . 13
Ga1 Yb1 Ga1 123.02(3) 8 13
Ga1 Yb1 Ga1 56.91(3) 15 13
Ga2 Yb1 Ga1 123.02(5) 13_556 13
Ga2 Yb1 Ga1 56.93(4) 6_554 13
Ga1 Yb1 Ga1 179.88(6) 6 13
Ga6 Yb1 Ga3 14.5(2) . .
Ga7 Yb1 Ga3 104.3(2) . .
Ga5 Yb1 Ga3 135.45(18) . .
Ga1 Yb1 Ga3 53.36(7) 10_556 .
Ga1 Yb1 Ga3 53.36(7) . .
Ga1 Yb1 Ga3 77.91(8) 8 .
Ga1 Yb1 Ga3 77.91(8) 15 .
Ga2 Yb1 Ga3 143.86(5) 13_556 .
Ga2 Yb1 Ga3 143.86(5) 6_554 .
Ga1 Yb1 Ga3 90.04(3) 6 .
Ga1 Yb1 Ga3 90.04(3) 13 .
Ga3 Pd1 Ga3 142.7(2) 15_545 13
Ga3 Pd1 Ga7 37.93(12) 15_545 .
Ga3 Pd1 Ga7 142.18(14) 13 .
Ga3 Pd1 Ga7 142.18(14) 15_545 3
Ga3 Pd1 Ga7 37.93(12) 13 3
Ga7 Pd1 Ga7 179.8(3) . 3
Ga3 Pd1 Ga6 179.55(18) 15_545 13
Ga3 Pd1 Ga6 37.32(11) 13 13
Ga7 Pd1 Ga6 141.67(17) . 13
Ga7 Pd1 Ga6 38.22(14) 3 13
Ga3 Pd1 Ga6 37.32(11) 15_545 15_545
Ga3 Pd1 Ga6 179.55(18) 13 15_545
Ga7 Pd1 Ga6 38.22(14) . 15_545
Ga7 Pd1 Ga6 141.67(17) 3 15_545
Ga6 Pd1 Ga6 142.7(2) 13 15_545
Ga3 Pd1 Ga1 115.45(11) 15_545 3
Ga3 Pd1 Ga1 95.90(11) 13 3
Ga7 Pd1 Ga1 115.70(12) . 3
Ga7 Pd1 Ga1 64.10(13) 3 3
Ga6 Pd1 Ga1 64.81(12) 13 3
Ga6 Pd1 Ga1 83.86(13) 15_545 3
Ga3 Pd1 Ga1 95.90(11) 15_545 .
Ga3 Pd1 Ga1 115.45(11) 13 .
Ga7 Pd1 Ga1 64.11(13) . .
Ga7 Pd1 Ga1 115.70(12) 3 .
Ga6 Pd1 Ga1 83.86(13) 13 .
Ga6 Pd1 Ga1 64.81(12) 15_545 .
Ga1 Pd1 Ga1 67.35(5) 3 .
Ga3 Pd1 Ga2 64.54(12) 15_545 6_554
Ga3 Pd1 Ga2 84.03(11) 13 6_554
Ga7 Pd1 Ga2 64.43(13) . 6_554
Ga7 Pd1 Ga2 115.77(12) 3 6_554
Ga6 Pd1 Ga2 115.19(12) 13 6_554
Ga6 Pd1 Ga2 96.20(13) 15_545 6_554
Ga1 Pd1 Ga2 179.80(5) 3 6_554
Ga1 Pd1 Ga2 112.85(3) . 6_554
Ga3 Pd1 Ga2 84.03(11) 15_545 14_546
Ga3 Pd1 Ga2 64.54(12) 13 14_546
Ga7 Pd1 Ga2 115.76(12) . 14_546
Ga7 Pd1 Ga2 64.44(13) 3 14_546
Ga6 Pd1 Ga2 96.20(13) 13 14_546
Ga6 Pd1 Ga2 115.19(12) 15_545 14_546
Ga1 Pd1 Ga2 112.85(3) 3 14_546
Ga1 Pd1 Ga2 179.80(5) . 14_546
Ga2 Pd1 Ga2 66.95(6) 6_554 14_546
Ga3 Pd1 Ga1 115.98(10) 15_545 13
Ga3 Pd1 Ga1 63.94(10) 13 13
Ga7 Pd1 Ga1 84.01(8) . 13
Ga7 Pd1 Ga1 95.99(8) 3 13
Ga6 Pd1 Ga1 63.57(12) 13 13
Ga6 Pd1 Ga1 116.50(12) 15_545 13
Ga1 Pd1 Ga1 112.87(4) 3 13
Ga1 Pd1 Ga1 67.32(4) . 13
Ga2 Pd1 Ga1 67.27(4) 6_554 13
Ga2 Pd1 Ga1 112.55(5) 14_546 13
Ga3 Pd1 Ga1 63.94(10) 15_545 15_545
Ga3 Pd1 Ga1 115.98(10) 13 15_545
Ga7 Pd1 Ga1 95.99(8) . 15_545
Ga7 Pd1 Ga1 84.01(8) 3 15_545
Ga6 Pd1 Ga1 116.50(12) 13 15_545
Ga6 Pd1 Ga1 63.57(12) 15_545 15_545
Ga1 Pd1 Ga1 67.32(4) 3 15_545
Ga1 Pd1 Ga1 112.87(4) . 15_545
Ga2 Pd1 Ga1 112.55(5) 6_554 15_545
Ga2 Pd1 Ga1 67.27(4) 14_546 15_545
Ga1 Pd1 Ga1 179.80(7) 13 15_545
Ga5 Pd2 Ga5 180.0 15_545 7_455
Ga5 Pd2 Ga5 142.4(2) 15_545 13
Ga5 Pd2 Ga5 37.6(2) 7_455 13
Ga5 Pd2 Ga5 37.6(2) 15_545 5_445
Ga5 Pd2 Ga5 142.4(2) 7_455 5_445
Ga5 Pd2 Ga5 180.0(3) 13 5_445
Ga5 Pd2 Ga4 142.40(14) 15_545 9
Ga5 Pd2 Ga4 37.60(14) 7_455 9
Ga5 Pd2 Ga4 37.60(14) 13 9
Ga5 Pd2 Ga4 142.40(14) 5_445 9
Ga5 Pd2 Ga4 37.60(14) 15_545 .
Ga5 Pd2 Ga4 142.40(14) 7_455 .
Ga5 Pd2 Ga4 142.40(14) 13 .
Ga5 Pd2 Ga4 37.60(14) 5_445 .
Ga4 Pd2 Ga4 180.0 9 .
Ga5 Pd2 Ga1 64.27(10) 15_545 .
Ga5 Pd2 Ga1 115.73(10) 7_455 .
Ga5 Pd2 Ga1 84.15(10) 13 .
Ga5 Pd2 Ga1 95.85(10) 5_445 .
Ga4 Pd2 Ga1 115.74(6) 9 .
Ga4 Pd2 Ga1 64.26(6) . .
Ga5 Pd2 Ga1 115.73(10) 15_545 9
Ga5 Pd2 Ga1 64.27(10) 7_455 9
Ga5 Pd2 Ga1 95.85(11) 13 9
Ga5 Pd2 Ga1 84.15(11) 5_445 9
Ga4 Pd2 Ga1 64.26(6) 9 9
Ga4 Pd2 Ga1 115.74(6) . 9
Ga1 Pd2 Ga1 180.0 . 9
Ga5 Pd2 Ga1 95.85(11) 15_545 11
Ga5 Pd2 Ga1 84.15(11) 7_455 11
Ga5 Pd2 Ga1 115.73(10) 13 11
Ga5 Pd2 Ga1 64.27(10) 5_445 11
Ga4 Pd2 Ga1 115.74(6) 9 11
Ga4 Pd2 Ga1 64.26(6) . 11
Ga1 Pd2 Ga1 112.75(5) . 11
Ga1 Pd2 Ga1 67.25(5) 9 11
Ga5 Pd2 Ga1 84.15(11) 15_545 3
Ga5 Pd2 Ga1 95.85(11) 7_455 3
Ga5 Pd2 Ga1 64.27(10) 13 3
Ga5 Pd2 Ga1 115.73(10) 5_445 3
Ga4 Pd2 Ga1 64.26(6) 9 3
Ga4 Pd2 Ga1 115.74(6) . 3
Ga1 Pd2 Ga1 67.25(5) . 3
Ga1 Pd2 Ga1 112.75(5) 9 3
Ga1 Pd2 Ga1 180.00(3) 11 3
Ga5 Pd2 Ga2 115.63(11) 15_545 10_556
Ga5 Pd2 Ga2 64.37(11) 7_455 10_556
Ga5 Pd2 Ga2 64.37(11) 13 10_556
Ga5 Pd2 Ga2 115.63(11) 5_445 10_556
Ga4 Pd2 Ga2 96.01(14) 9 10_556
Ga4 Pd2 Ga2 83.99(14) . 10_556
Ga1 Pd2 Ga2 67.23(3) . 10_556
Ga1 Pd2 Ga2 112.77(3) 9 10_556
Ga1 Pd2 Ga2 67.23(3) 11 10_556
Ga1 Pd2 Ga2 112.77(3) 3 10_556
Ga5 Pd2 Ga2 64.37(11) 15_545 2_554
Ga5 Pd2 Ga2 115.63(11) 7_455 2_554
Ga5 Pd2 Ga2 115.63(11) 13 2_554
Ga5 Pd2 Ga2 64.37(11) 5_445 2_554
Ga4 Pd2 Ga2 83.99(14) 9 2_554
Ga4 Pd2 Ga2 96.01(14) . 2_554
Ga1 Pd2 Ga2 112.77(3) . 2_554
Ga1 Pd2 Ga2 67.23(3) 9 2_554
Ga1 Pd2 Ga2 112.77(3) 11 2_554
Ga1 Pd2 Ga2 67.23(3) 3 2_554
Ga2 Pd2 Ga2 180.00(8) 10_556 2_554
Pd1 Ga1 Pd2 112.70(4) . .
Pd1 Ga1 Pd1 112.68(4) . 13
Pd2 Ga1 Pd1 112.84(5) . 13
Pd1 Ga1 Ga6 105.74(13) . .
Pd2 Ga1 Ga6 140.50(12) . .
Pd1 Ga1 Ga6 56.88(9) 13 .
Pd1 Ga1 Ga3 140.27(12) . .
Pd2 Ga1 Ga3 106.03(12) . .
Pd1 Ga1 Ga3 56.63(7) 13 .
Ga6 Ga1 Ga3 34.72(12) . .
Pd1 Ga1 Ga7 56.67(8) . .
Pd2 Ga1 Ga7 140.43(8) . .
Pd1 Ga1 Ga7 105.74(9) 13 .
Ga6 Ga1 Ga7 58.96(15) . .
Ga3 Ga1 Ga7 87.68(12) . .
Pd1 Ga1 Ga5 105.91(11) . 15_545
Pd2 Ga1 Ga5 56.50(7) . 15_545
Pd1 Ga1 Ga5 140.44(11) 13 15_545
Ga6 Ga1 Ga5 104.83(10) . 15_545
Ga3 Ga1 Ga5 87.95(12) . 15_545
Ga7 Ga1 Ga5 88.00(11) . 15_545
Pd1 Ga1 Ga4 140.43(12) . .
Pd2 Ga1 Ga4 56.53(7) . .
Pd1 Ga1 Ga4 105.92(14) 13 .
Ga6 Ga1 Ga4 87.89(14) . .
Ga3 Ga1 Ga4 59.43(16) . .
Ga7 Ga1 Ga4 105.05(8) . .
Ga5 Ga1 Ga4 34.72(15) 15_545 .
Pd1 Ga1 Ga6 56.40(8) . 15_545
Pd2 Ga1 Ga6 105.43(13) . 15_545
Pd1 Ga1 Ga6 140.82(13) 13 15_545
Ga6 Ga1 Ga6 88.11(5) . 15_545
Ga3 Ga1 Ga6 105.36(11) . 15_545
Ga7 Ga1 Ga6 35.24(14) . 15_545
Ga5 Ga1 Ga6 59.23(13) 15_545 15_545
Ga4 Ga1 Ga6 87.99(13) . 15_545
Pd1 Ga1 Ga1 56.33(3) . 3
Pd2 Ga1 Ga1 56.38(2) . 3
Pd1 Ga1 Ga1 134.28(7) 13 3
Ga6 Ga1 Ga1 160.21(13) . 3
Ga3 Ga1 Ga1 160.61(11) . 3
Ga7 Ga1 Ga1 101.50(8) . 3
Ga5 Ga1 Ga1 75.49(8) 15_545 3
Ga4 Ga1 Ga1 101.43(12) . 3
Ga6 Ga1 Ga1 74.96(9) 15_545 3
Pd1 Ga1 Ga1 56.44(4) . 13
Pd2 Ga1 Ga1 134.29(7) . 13
Pd1 Ga1 Ga1 56.24(3) 13 13
Ga6 Ga1 Ga1 75.58(9) . 13
Ga3 Ga1 Ga1 101.32(10) . 13
Ga7 Ga1 Ga1 75.52(9) . 13
Ga5 Ga1 Ga1 160.60(12) 15_545 13
Ga4 Ga1 Ga1 160.44(14) . 13
Ga6 Ga1 Ga1 101.62(12) 15_545 13
Ga1 Ga1 Ga1 97.53(6) 3 13
Pd1 Ga1 Ga2 134.32(4) . 10_556
Pd2 Ga1 Ga2 56.50(4) . 10_556
Pd1 Ga1 Ga2 56.34(4) 13 10_556
Ga6 Ga1 Ga2 101.63(12) . 10_556
Ga3 Ga1 Ga2 75.54(9) . 10_556
Ga7 Ga1 Ga2 160.29(9) . 10_556
Ga5 Ga1 Ga2 101.42(11) 15_545 10_556
Ga4 Ga1 Ga2 75.45(8) . 10_556
Ga6 Ga1 Ga2 160.29(13) 15_545 10_556
Ga1 Ga1 Ga2 97.62(4) 3 10_556
Ga1 Ga1 Ga2 97.41(4) 13 10_556
Pd1 Ga2 Pd1 113.05(6) 6 14_456
Pd1 Ga2 Pd2 112.67(4) 6 2
Pd1 Ga2 Pd2 112.67(4) 14_456 2
Pd1 Ga2 Ga5 140.20(10) 6 7_456
Pd1 Ga2 Ga5 105.82(10) 14_456 7_456
Pd2 Ga2 Ga5 56.34(7) 2 7_456
Pd1 Ga2 Ga5 105.82(10) 6 13_556
Pd1 Ga2 Ga5 140.20(10) 14_456 13_556
Pd2 Ga2 Ga5 56.34(7) 2 13_556
Ga5 Ga2 Ga5 34.6(2) 7_456 13_556
Pd1 Ga2 Ga7 56.44(7) 6 13_556
Pd1 Ga2 Ga7 140.71(10) 14_456 13_556
Pd2 Ga2 Ga7 105.62(10) 2 13_556
Ga5 Ga2 Ga7 87.90(11) 7_456 13_556
Ga5 Ga2 Ga7 59.38(13) 13_556 13_556
Pd1 Ga2 Ga7 140.71(10) 6 7_456
Pd1 Ga2 Ga7 56.44(7) 14_456 7_456
Pd2 Ga2 Ga7 105.62(10) 2 7_456
Ga5 Ga2 Ga7 59.38(13) 7_456 7_456
Ga5 Ga2 Ga7 87.90(11) 13_556 7_456
Ga7 Ga2 Ga7 105.38(15) 13_556 7_456
Pd1 Ga2 Ga3 56.37(8) 6 3_566
Pd1 Ga2 Ga3 106.03(11) 14_456 3_566
Pd2 Ga2 Ga3 140.34(10) 2 3_566
Ga5 Ga2 Ga3 105.29(11) 7_456 3_566
Ga5 Ga2 Ga3 88.17(12) 13_556 3_566
Ga7 Ga2 Ga3 34.91(12) 13_556 3_566
Ga7 Ga2 Ga3 88.35(13) 7_456 3_566
Pd1 Ga2 Ga3 106.03(11) 6 9_566
Pd1 Ga2 Ga3 56.37(8) 14_456 9_566
Pd2 Ga2 Ga3 140.34(10) 2 9_566
Ga5 Ga2 Ga3 88.17(12) 7_456 9_566
Ga5 Ga2 Ga3 105.29(11) 13_556 9_566
Ga7 Ga2 Ga3 88.35(13) 13_556 9_566
Ga7 Ga2 Ga3 34.91(12) 7_456 9_566
Ga3 Ga2 Ga3 59.7(2) 3_566 9_566
Pd1 Ga2 Ga2 56.52(3) 6 9_566
Pd1 Ga2 Ga2 56.52(3) 14_456 9_566
Pd2 Ga2 Ga2 134.32(11) 2 9_566
Ga5 Ga2 Ga2 160.65(11) 7_456 9_566
Ga5 Ga2 Ga2 160.65(11) 13_556 9_566
Ga7 Ga2 Ga2 101.57(9) 13_556 9_566
Ga7 Ga2 Ga2 101.57(9) 7_456 9_566
Ga3 Ga2 Ga2 75.42(9) 3_566 9_566
Ga3 Ga2 Ga2 75.42(9) 9_566 9_566
Pd1 Ga2 Ga1 134.39(7) 6 4
Pd1 Ga2 Ga1 56.39(3) 14_456 4
Pd2 Ga2 Ga1 56.28(3) 2 4
Ga5 Ga2 Ga1 75.33(8) 7_456 4
Ga5 Ga2 Ga1 101.14(10) 13_556 4
Ga7 Ga2 Ga1 160.20(10) 13_556 4
Ga7 Ga2 Ga1 75.29(9) 7_456 4
Ga3 Ga2 Ga1 160.71(11) 3_566 4
Ga3 Ga2 Ga1 101.34(10) 9_566 4
Ga2 Ga2 Ga1 97.60(6) 9_566 4
Pd1 Ga2 Ga1 56.39(3) 6 10_556
Pd1 Ga2 Ga1 134.39(7) 14_456 10_556
Pd2 Ga2 Ga1 56.28(3) 2 10_556
Ga5 Ga2 Ga1 101.14(10) 7_456 10_556
Ga5 Ga2 Ga1 75.33(8) 13_556 10_556
Ga7 Ga2 Ga1 75.29(9) 13_556 10_556
Ga7 Ga2 Ga1 160.20(10) 7_456 10_556
Ga3 Ga2 Ga1 101.34(10) 3_566 10_556
Ga3 Ga2 Ga1 160.71(11) 9_566 10_556
Ga2 Ga2 Ga1 97.60(6) 9_566 10_556
Ga1 Ga2 Ga1 97.38(5) 4 10_556
Yb2 Ga3 Ga6 149.9(4) . .
Yb2 Ga3 Ga7 149.1(4) . 15
Ga6 Ga3 Ga7 61.0(3) . 15
Yb2 Ga3 Pd1 111.88(11) . 6
Ga6 Ga3 Pd1 71.48(13) . 6
Ga7 Ga3 Pd1 71.07(10) 15 6
Yb2 Ga3 Pd1 111.88(11) . 13
Ga6 Ga3 Pd1 71.48(13) . 13
Ga7 Ga3 Pd1 71.07(10) 15 13
Pd1 Ga3 Pd1 136.2(2) 6 13
Yb2 Ga3 Ga4 30.26(10) . .
Ga6 Ga3 Ga4 119.6(3) . .
Ga7 Ga3 Ga4 179.4(3) 15 .
Pd1 Ga3 Ga4 109.06(10) 6 .
Pd1 Ga3 Ga4 109.06(10) 13 .
Yb2 Ga3 Ga1 83.81(15) . 10_556
Ga6 Ga3 Ga1 72.2(2) . 10_556
Ga7 Ga3 Ga1 120.0(2) 15 10_556
Pd1 Ga3 Ga1 59.43(6) 6 10_556
Pd1 Ga3 Ga1 127.14(18) 13 10_556
Ga4 Ga3 Ga1 60.48(10) . 10_556
Yb2 Ga3 Ga1 83.81(15) . .
Ga6 Ga3 Ga1 72.2(2) . .
Ga7 Ga3 Ga1 120.0(2) 15 .
Pd1 Ga3 Ga1 127.14(18) 6 .
Pd1 Ga3 Ga1 59.43(6) 13 .
Ga4 Ga3 Ga1 60.48(10) . .
Ga1 Ga3 Ga1 73.65(12) 10_556 .
Yb2 Ga3 Ga3 29.42(17) . 11
Ga6 Ga3 Ga3 179.3(3) . 11
Ga7 Ga3 Ga3 119.7(2) 15 11
Pd1 Ga3 Ga3 108.66(11) 6 11
Pd1 Ga3 Ga3 108.66(11) 13 11
Ga4 Ga3 Ga3 59.68(12) . 11
Ga1 Ga3 Ga3 107.20(11) 10_556 11
Ga1 Ga3 Ga3 107.20(11) . 11
Yb2 Ga3 Ga2 82.92(18) . 9_566
Ga6 Ga3 Ga2 120.4(3) . 9_566
Ga7 Ga3 Ga2 72.4(2) 15 9_566
Pd1 Ga3 Ga2 59.08(7) 6 9_566
Pd1 Ga3 Ga2 126.22(16) 13 9_566
Ga4 Ga3 Ga2 107.07(16) . 9_566
Ga1 Ga3 Ga2 105.05(5) 10_556 9_566
Ga1 Ga3 Ga2 166.7(2) . 9_566
Ga3 Ga3 Ga2 60.17(10) 11 9_566
Yb2 Ga3 Ga2 82.92(18) . 2_564
Ga6 Ga3 Ga2 120.4(3) . 2_564
Ga7 Ga3 Ga2 72.4(2) 15 2_564
Pd1 Ga3 Ga2 126.22(16) 6 2_564
Pd1 Ga3 Ga2 59.08(7) 13 2_564
Ga4 Ga3 Ga2 107.07(16) . 2_564
Ga1 Ga3 Ga2 166.7(2) 10_556 2_564
Ga1 Ga3 Ga2 105.05(5) . 2_564
Ga3 Ga3 Ga2 60.17(10) 11 2_564
Ga2 Ga3 Ga2 73.06(13) 9_566 2_564
Yb2 Ga3 Yb1 136.0(2) . .
Ga6 Ga3 Yb1 13.8(2) . .
Ga7 Ga3 Yb1 74.9(2) 15 .
Pd1 Ga3 Yb1 74.82(12) 6 .
Pd1 Ga3 Yb1 74.82(12) 13 .
Ga4 Ga3 Yb1 105.79(16) . .
Ga1 Ga3 Yb1 61.77(10) 10_556 .
Ga1 Ga3 Yb1 61.77(10) . .
Ga3 Ga3 Yb1 165.47(8) 11 .
Ga2 Ga3 Yb1 129.79(13) 9_566 .
Ga2 Ga3 Yb1 129.79(13) 2_564 .
Yb2 Ga4 Ga5 150.1(2) . 5_445
Yb2 Ga4 Ga5 150.1(2) . 15_545
Ga5 Ga4 Ga5 59.9(4) 5_445 15_545
Yb2 Ga4 Pd2 111.89(13) . .
Ga5 Ga4 Pd2 71.15(14) 5_445 .
Ga5 Ga4 Pd2 71.15(14) 15_545 .
Yb2 Ga4 Pd2 111.89(13) . 2
Ga5 Ga4 Pd2 71.15(14) 5_445 2
Ga5 Ga4 Pd2 71.15(14) 15_545 2
Pd2 Ga4 Pd2 136.2(3) . 2
Yb2 Ga4 Ga3 30.32(12) . 11
Ga5 Ga4 Ga3 119.7(2) 5_445 11
Ga5 Ga4 Ga3 179.6(2) 15_545 11
Pd2 Ga4 Ga3 108.77(10) . 11
Pd2 Ga4 Ga3 108.77(10) 2 11
Yb2 Ga4 Ga3 30.32(12) . .
Ga5 Ga4 Ga3 179.6(2) 5_445 .
Ga5 Ga4 Ga3 119.7(2) 15_545 .
Pd2 Ga4 Ga3 108.77(10) . .
Pd2 Ga4 Ga3 108.77(10) 2 .
Ga3 Ga4 Ga3 60.6(2) 11 .
Yb2 Ga4 Ga1 83.50(13) . .
Ga5 Ga4 Ga1 119.6(2) 5_445 .
Ga5 Ga4 Ga1 72.64(13) 15_545 .
Pd2 Ga4 Ga1 59.21(3) . .
Pd2 Ga4 Ga1 126.60(7) 2 .
Ga3 Ga4 Ga1 107.7(2) 11 .
Ga3 Ga4 Ga1 60.09(11) . .
Yb2 Ga4 Ga1 83.50(13) . 10_556
Ga5 Ga4 Ga1 119.6(2) 5_445 10_556
Ga5 Ga4 Ga1 72.64(13) 15_545 10_556
Pd2 Ga4 Ga1 126.60(7) . 10_556
Pd2 Ga4 Ga1 59.21(3) 2 10_556
Ga3 Ga4 Ga1 107.7(2) 11 10_556
Ga3 Ga4 Ga1 60.09(11) . 10_556
Ga1 Ga4 Ga1 73.32(6) . 10_556
Yb2 Ga4 Ga1 83.50(13) . 11
Ga5 Ga4 Ga1 72.64(13) 5_445 11
Ga5 Ga4 Ga1 119.6(2) 15_545 11
Pd2 Ga4 Ga1 59.21(3) . 11
Pd2 Ga4 Ga1 126.60(7) 2 11
Ga3 Ga4 Ga1 60.09(11) 11 11
Ga3 Ga4 Ga1 107.7(2) . 11
Ga1 Ga4 Ga1 105.15(6) . 11
Ga1 Ga4 Ga1 167.0(3) 10_556 11
Yb2 Ga4 Ga1 83.50(13) . 4
Ga5 Ga4 Ga1 72.64(13) 5_445 4
Ga5 Ga4 Ga1 119.6(2) 15_545 4
Pd2 Ga4 Ga1 126.60(7) . 4
Pd2 Ga4 Ga1 59.21(3) 2 4
Ga3 Ga4 Ga1 60.09(11) 11 4
Ga3 Ga4 Ga1 107.7(2) . 4
Ga1 Ga4 Ga1 167.0(3) . 4
Ga1 Ga4 Ga1 105.15(6) 10_556 4
Ga1 Ga4 Ga1 73.32(6) 11 4
Yb2 Ga4 Yb1 135.33(8) . 5_445
Ga5 Ga4 Yb1 14.72(16) 5_445 5_445
Ga5 Ga4 Yb1 74.6(3) 15_545 5_445
Pd2 Ga4 Yb1 74.63(11) . 5_445
Pd2 Ga4 Yb1 74.63(11) 2 5_445
Ga3 Ga4 Yb1 105.01(11) 11 5_445
Ga3 Ga4 Yb1 165.65(18) . 5_445
Ga1 Ga4 Yb1 129.70(16) . 5_445
Ga1 Ga4 Yb1 129.70(16) 10_556 5_445
Ga1 Ga4 Yb1 61.46(6) 11 5_445
Ga1 Ga4 Yb1 61.46(6) 4 5_445
Ga4 Yb2 Ga3 119.42(17) . 11
Ga4 Yb2 Ga3 119.42(17) . .
Ga3 Yb2 Ga3 121.2(3) 11 .
Ga4 Yb2 Ga2 146.86(4) . 9_566
Ga3 Yb2 Ga2 65.71(13) 11 9_566
Ga3 Yb2 Ga2 65.71(13) . 9_566
Ga4 Yb2 Ga2 146.86(4) . 2_564
Ga3 Yb2 Ga2 65.71(13) 11 2_564
Ga3 Yb2 Ga2 65.71(13) . 2_564
Ga2 Yb2 Ga2 66.28(8) 9_566 2_564
Ga4 Yb2 Ga1 65.19(3) . .
Ga3 Yb2 Ga1 146.94(2) 11 .
Ga3 Yb2 Ga1 64.79(13) . .
Ga2 Yb2 Ga1 130.51(3) 9_566 .
Ga2 Yb2 Ga1 93.04(3) 2_564 .
Ga4 Yb2 Ga1 65.19(3) . 11
Ga3 Yb2 Ga1 64.79(13) 11 11
Ga3 Yb2 Ga1 146.94(2) . 11
Ga2 Yb2 Ga1 130.51(3) 9_566 11
Ga2 Yb2 Ga1 93.04(3) 2_564 11
Ga1 Yb2 Ga1 93.03(5) . 11
Ga4 Yb2 Ga1 65.19(3) . 10_556
Ga3 Yb2 Ga1 146.94(2) 11 10_556
Ga3 Yb2 Ga1 64.79(13) . 10_556
Ga2 Yb2 Ga1 93.04(3) 9_566 10_556
Ga2 Yb2 Ga1 130.51(3) 2_564 10_556
Ga1 Yb2 Ga1 66.12(5) . 10_556
Ga1 Yb2 Ga1 130.39(6) 11 10_556
Ga4 Yb2 Ga1 65.19(3) . 4
Ga3 Yb2 Ga1 64.79(13) 11 4
Ga3 Yb2 Ga1 146.94(2) . 4
Ga2 Yb2 Ga1 93.04(3) 9_566 4
Ga2 Yb2 Ga1 130.51(3) 2_564 4
Ga1 Yb2 Ga1 130.39(6) . 4
Ga1 Yb2 Ga1 66.12(5) 11 4
Ga1 Yb2 Ga1 93.03(5) 10_556 4
Ga4 Yb2 Ga2 90.10(3) . 10_556
Ga3 Yb2 Ga2 89.949(17) 11 10_556
Ga3 Yb2 Ga2 89.949(17) . 10_556
Ga2 Yb2 Ga2 123.04(5) 9_566 10_556
Ga2 Yb2 Ga2 56.75(5) 2_564 10_556
Ga1 Yb2 Ga2 56.99(3) . 10_556
Ga1 Yb2 Ga2 56.99(3) 11 10_556
Ga1 Yb2 Ga2 123.11(3) 10_556 10_556
Ga1 Yb2 Ga2 123.11(3) 4 10_556
Ga4 Yb2 Ga2 90.10(3) . .
Ga3 Yb2 Ga2 89.949(17) 11 .
Ga3 Yb2 Ga2 89.949(17) . .
Ga2 Yb2 Ga2 56.75(5) 9_566 .
Ga2 Yb2 Ga2 123.04(5) 2_564 .
Ga1 Yb2 Ga2 123.11(3) . .
Ga1 Yb2 Ga2 123.11(3) 11 .
Ga1 Yb2 Ga2 56.99(3) 10_556 .
Ga1 Yb2 Ga2 56.99(3) 4 .
Ga2 Yb2 Ga2 179.79(7) 10_556 .
Ga4 Yb2 Ga6 104.09(11) . .
Ga3 Yb2 Ga6 136.48(18) 11 .
Ga3 Yb2 Ga6 15.3(2) . .
Ga2 Yb2 Ga6 78.23(9) 9_566 .
Ga2 Yb2 Ga6 78.23(9) 2_564 .
Ga1 Yb2 Ga6 53.02(8) . .
Ga1 Yb2 Ga6 143.69(5) 11 .
Ga1 Yb2 Ga6 53.02(8) 10_556 .
Ga1 Yb2 Ga6 143.69(5) 4 .
Ga2 Yb2 Ga6 89.975(8) 10_556 .
Ga2 Yb2 Ga6 89.975(8) . .
Yb1 Ga5 Ga5 149.98(16) . 11_655
Yb1 Ga5 Ga4 150.0(3) . 5
Ga5 Ga5 Ga4 60.1(2) 11_655 5
Yb1 Ga5 Pd2 111.81(10) . 6
Ga5 Ga5 Pd2 71.22(10) 11_655 6
Ga4 Ga5 Pd2 71.24(11) 5 6
Yb1 Ga5 Pd2 111.81(10) . 5
Ga5 Ga5 Pd2 71.22(10) 11_655 5
Ga4 Ga5 Pd2 71.24(11) 5 5
Pd2 Ga5 Pd2 136.4(2) 6 5
Yb1 Ga5 Ga6 29.29(14) . .
Ga5 Ga5 Ga6 179.27(17) 11_655 .
Ga4 Ga5 Ga6 120.7(3) 5 .
Pd2 Ga5 Ga6 108.92(10) 6 .
Pd2 Ga5 Ga6 108.92(10) 5 .
Yb1 Ga5 Ga7 29.78(15) . .
Ga5 Ga5 Ga7 120.20(15) 11_655 .
Ga4 Ga5 Ga7 179.7(3) 5 .
Pd2 Ga5 Ga7 108.80(10) 6 .
Pd2 Ga5 Ga7 108.80(10) 5 .
Ga6 Ga5 Ga7 59.1(2) . .
Yb1 Ga5 Ga1 83.43(16) . 8
Ga5 Ga5 Ga1 119.75(10) 11_655 8
Ga4 Ga5 Ga1 72.64(15) 5 8
Pd2 Ga5 Ga1 59.23(6) 6 8
Pd2 Ga5 Ga1 126.66(16) 5 8
Ga6 Ga5 Ga1 60.78(13) . 8
Ga7 Ga5 Ga1 107.16(17) . 8
Yb1 Ga5 Ga1 83.43(16) . 15
Ga5 Ga5 Ga1 119.75(10) 11_655 15
Ga4 Ga5 Ga1 72.64(15) 5 15
Pd2 Ga5 Ga1 126.66(16) 6 15
Pd2 Ga5 Ga1 59.23(6) 5 15
Ga6 Ga5 Ga1 60.78(13) . 15
Ga7 Ga5 Ga1 107.16(17) . 15
Ga1 Ga5 Ga1 73.32(12) 8 15
Yb1 Ga5 Ga2 83.35(16) . 6_554
Ga5 Ga5 Ga2 72.72(10) 11_655 6_554
Ga4 Ga5 Ga2 119.9(2) 5 6_554
Pd2 Ga5 Ga2 126.60(16) 6 6_554
Pd2 Ga5 Ga2 59.29(6) 5 6_554
Ga6 Ga5 Ga2 106.72(19) . 6_554
Ga7 Ga5 Ga2 60.32(12) . 6_554
Ga1 Ga5 Ga2 166.8(2) 8 6_554
Ga1 Ga5 Ga2 105.16(5) 15 6_554
Yb1 Ga5 Ga2 83.35(16) . 13_556
Ga5 Ga5 Ga2 72.72(10) 11_655 13_556
Ga4 Ga5 Ga2 119.9(2) 5 13_556
Pd2 Ga5 Ga2 59.29(6) 6 13_556
Pd2 Ga5 Ga2 126.60(16) 5 13_556
Ga6 Ga5 Ga2 106.72(19) . 13_556
Ga7 Ga5 Ga2 60.32(12) . 13_556
Ga1 Ga5 Ga2 105.16(5) 8 13_556
Ga1 Ga5 Ga2 166.8(2) 15 13_556
Ga2 Ga5 Ga2 73.19(13) 6_554 13_556
Yb1 Ga5 Yb2 135.3(2) . 5
Ga5 Ga5 Yb2 74.71(9) 11_655 5
Ga4 Ga5 Yb2 14.66(13) 5 5
Pd2 Ga5 Yb2 74.70(10) 6 5
Pd2 Ga5 Yb2 74.70(10) 5 5
Ga6 Ga5 Yb2 106.02(19) . 5
Ga7 Ga5 Yb2 165.1(2) . 5
Ga1 Ga5 Yb2 61.51(9) 8 5
Ga1 Ga5 Yb2 61.51(9) 15 5
Ga2 Ga5 Yb2 129.87(13) 6_554 5
Ga2 Ga5 Yb2 129.87(13) 13_556 5
Yb1 Ga6 Ga3 151.7(5) . .
Yb1 Ga6 Ga7 148.1(4) . 15
Ga3 Ga6 Ga7 60.2(3) . 15
Yb1 Ga6 Pd1 112.10(13) . 13
Ga3 Ga6 Pd1 71.19(14) . 13
Ga7 Ga6 Pd1 70.78(13) 15 13
Yb1 Ga6 Pd1 112.10(13) . 6
Ga3 Ga6 Pd1 71.19(14) . 6
Ga7 Ga6 Pd1 70.78(13) 15 6
Pd1 Ga6 Pd1 135.7(3) 13 6
Yb1 Ga6 Ga7 30.77(18) . .
Ga3 Ga6 Ga7 120.9(3) . .
Ga7 Ga6 Ga7 178.9(3) 15 .
Pd1 Ga6 Ga7 109.44(12) 13 .
Pd1 Ga6 Ga7 109.44(12) 6 .
Yb1 Ga6 Ga1 84.5(2) . 10_556
Ga3 Ga6 Ga1 73.0(2) . 10_556
Ga7 Ga6 Ga1 120.0(2) 15 10_556
Pd1 Ga6 Ga1 127.48(19) 13 10_556
Pd1 Ga6 Ga1 59.54(6) 6 10_556
Ga7 Ga6 Ga1 60.81(12) . 10_556
Yb1 Ga6 Ga1 84.5(2) . .
Ga3 Ga6 Ga1 73.0(2) . .
Ga7 Ga6 Ga1 120.0(2) 15 .
Pd1 Ga6 Ga1 59.54(6) 13 .
Pd1 Ga6 Ga1 127.48(19) 6 .
Ga7 Ga6 Ga1 60.81(12) . .
Ga1 Ga6 Ga1 74.03(14) 10_556 .
Yb1 Ga6 Ga5 29.75(14) . .
Ga3 Ga6 Ga5 178.6(4) . .
Ga7 Ga6 Ga5 118.4(3) 15 .
Pd1 Ga6 Ga5 108.50(12) 13 .
Pd1 Ga6 Ga5 108.50(12) 6 .
Ga7 Ga6 Ga5 60.5(2) . .
Ga1 Ga6 Ga5 108.1(2) 10_556 .
Ga1 Ga6 Ga5 108.1(2) . .
Yb1 Ga6 Ga1 83.06(18) . 8
Ga3 Ga6 Ga1 119.0(3) . 8
Ga7 Ga6 Ga1 71.4(2) 15 8
Pd1 Ga6 Ga1 125.41(19) 13 8
Pd1 Ga6 Ga1 58.79(7) 6 8
Ga7 Ga6 Ga1 107.7(2) . 8
Ga1 Ga6 Ga1 105.26(6) 10_556 8
Ga1 Ga6 Ga1 167.6(2) . 8
Ga5 Ga6 Ga1 59.99(12) . 8
Yb1 Ga6 Ga1 83.06(18) . 15
Ga3 Ga6 Ga1 119.0(3) . 15
Ga7 Ga6 Ga1 71.4(2) 15 15
Pd1 Ga6 Ga1 58.79(7) 13 15
Pd1 Ga6 Ga1 125.41(19) 6 15
Ga7 Ga6 Ga1 107.7(2) . 15
Ga1 Ga6 Ga1 167.6(2) 10_556 15
Ga1 Ga6 Ga1 105.26(6) . 15
Ga5 Ga6 Ga1 59.99(12) . 15
Ga1 Ga6 Ga1 72.66(13) 8 15
Yb1 Ga6 Yb2 136.9(3) . .
Ga3 Ga6 Yb2 14.8(2) . .
Ga7 Ga6 Yb2 75.0(3) 15 .
Pd1 Ga6 Yb2 74.82(12) 13 .
Pd1 Ga6 Yb2 74.82(12) 6 .
Ga7 Ga6 Yb2 106.11(18) . .
Ga1 Ga6 Yb2 61.84(10) 10_556 .
Ga1 Ga6 Yb2 61.84(10) . .
Ga5 Ga6 Yb2 166.6(3) . .
Ga1 Ga6 Yb2 129.24(16) 8 .
Ga1 Ga6 Yb2 129.24(16) 15 .
Yb1 Ga7 Ga3 150.1(4) . 15_545
Yb1 Ga7 Ga6 151.2(4) . 15_545
Ga3 Ga7 Ga6 58.8(2) 15_545 15_545
Yb1 Ga7 Pd1 111.93(8) . .
Ga3 Ga7 Pd1 71.01(10) 15_545 .
Ga6 Ga7 Pd1 71.00(9) 15_545 .
Yb1 Ga7 Pd1 111.93(8) . 10_556
Ga3 Ga7 Pd1 71.01(10) 15_545 10_556
Ga6 Ga7 Pd1 71.00(9) 15_545 10_556
Pd1 Ga7 Pd1 136.13(16) . 10_556
Yb1 Ga7 Ga6 30.46(17) . .
Ga3 Ga7 Ga6 179.5(3) 15_545 .
Ga6 Ga7 Ga6 120.7(3) 15_545 .
Pd1 Ga7 Ga6 108.89(11) . .
Pd1 Ga7 Ga6 108.89(11) 10_556 .
Yb1 Ga7 Ga5 29.95(14) . .
Ga3 Ga7 Ga5 120.1(4) 15_545 .
Ga6 Ga7 Ga5 178.9(4) 15_545 .
Pd1 Ga7 Ga5 108.78(10) . .
Pd1 Ga7 Ga5 108.78(10) 10_556 .
Ga6 Ga7 Ga5 60.41(16) . .
Yb1 Ga7 Ga1 83.73(19) . 10_556
Ga3 Ga7 Ga1 119.4(2) 15_545 10_556
Ga6 Ga7 Ga1 73.3(2) 15_545 10_556
Pd1 Ga7 Ga1 126.79(19) . 10_556
Pd1 Ga7 Ga1 59.22(7) 10_556 10_556
Ga6 Ga7 Ga1 60.24(13) . 10_556
Ga5 Ga7 Ga1 107.55(15) . 10_556
Yb1 Ga7 Ga1 83.73(19) . .
Ga3 Ga7 Ga1 119.4(2) 15_545 .
Ga6 Ga7 Ga1 73.3(2) 15_545 .
Pd1 Ga7 Ga1 59.22(7) . .
Pd1 Ga7 Ga1 126.79(19) 10_556 .
Ga6 Ga7 Ga1 60.24(13) . .
Ga5 Ga7 Ga1 107.55(15) . .
Ga1 Ga7 Ga1 73.55(15) 10_556 .
Yb1 Ga7 Ga2 83.47(17) . 13_556
Ga3 Ga7 Ga2 72.7(2) 15_545 13_556
Ga6 Ga7 Ga2 118.9(2) 15_545 13_556
Pd1 Ga7 Ga2 126.3(2) . 13_556
Pd1 Ga7 Ga2 59.13(8) 10_556 13_556
Ga6 Ga7 Ga2 107.75(14) . 13_556
Ga5 Ga7 Ga2 60.30(12) . 13_556
Ga1 Ga7 Ga2 105.16(4) 10_556 13_556
Ga1 Ga7 Ga2 167.19(16) . 13_556
Yb1 Ga7 Ga2 83.47(17) . 6_554
Ga3 Ga7 Ga2 72.7(2) 15_545 6_554
Ga6 Ga7 Ga2 118.9(2) 15_545 6_554
Pd1 Ga7 Ga2 59.13(8) . 6_554
Pd1 Ga7 Ga2 126.3(2) 10_556 6_554
Ga6 Ga7 Ga2 107.75(14) . 6_554
Ga5 Ga7 Ga2 60.30(12) . 6_554
Ga1 Ga7 Ga2 167.19(16) 10_556 6_554
Ga1 Ga7 Ga2 105.16(4) . 6_554
Ga2 Ga7 Ga2 73.17(14) 13_556 6_554
Yb1 Ga7 Yb1 135.8(3) . 15_545
Ga3 Ga7 Yb1 74.1(2) 15_545 15_545
Ga6 Ga7 Yb1 15.4(2) 15_545 15_545
Pd1 Ga7 Yb1 74.61(9) . 15_545
Pd1 Ga7 Yb1 74.61(9) 10_556 15_545
Ga6 Ga7 Yb1 105.3(2) . 15_545
Ga5 Ga7 Yb1 165.7(2) . 15_545
Ga1 Ga7 Yb1 61.64(10) 10_556 15_545
Ga1 Ga7 Yb1 61.64(10) . 15_545
Ga2 Ga7 Yb1 129.48(11) 13_556 15_545
Ga2 Ga7 Yb1 129.48(11) 6_554 15_545
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Yb1 Ga6 1.564(6) .
Yb1 Ga7 1.578(4) .
Yb1 Ga5 1.586(5) .
Yb1 Ga1 3.0221(15) 10_556
Yb1 Ga1 3.0222(15) .
Yb1 Ga1 3.0243(13) 8
Yb1 Ga1 3.0243(13) 15
Yb1 Ga2 3.0285(17) 13_556
Yb1 Ga2 3.0285(17) 6_554
Yb1 Ga1 3.0986(14) 6
Yb1 Ga1 3.0986(14) 13
Yb1 Ga3 3.105(5) .
Pd1 Ga3 2.558(2) 15_545
Pd1 Ga3 2.558(2) 13
Pd1 Ga7 2.5593(15) .
Pd1 Ga7 2.5593(15) 3
Pd1 Ga6 2.563(2) 13
Pd1 Ga6 2.563(2) 15_545
Pd1 Ga1 2.6316(16) 3
Pd1 Ga1 2.6316(16) .
Pd1 Ga2 2.6360(14) 6_554
Pd1 Ga2 2.6360(14) 14_546
Pd1 Ga1 2.6375(10) 13
Pd1 Ga1 2.6375(10) 15_545
Pd2 Ga5 2.5571(19) 15_545
Pd2 Ga5 2.5571(19) 7_455
Pd2 Ga5 2.5571(19) 13
Pd2 Ga5 2.5571(19) 5_445
Pd2 Ga4 2.558(2) 9
Pd2 Ga4 2.558(2) .
Pd2 Ga1 2.6349(12) .
Pd2 Ga1 2.6349(12) 9
Pd2 Ga1 2.6349(12) 11
Pd2 Ga1 2.6349(12) 3
Pd2 Ga2 2.6416(15) 10_556
Pd2 Ga2 2.6416(15) 2_554
Ga1 Pd1 2.6375(10) 13
Ga1 Ga6 2.740(4) .
Ga1 Ga3 2.752(4) .
Ga1 Ga7 2.755(5) .
Ga1 Ga5 2.763(4) 15_545
Ga1 Ga4 2.7627(15) .
Ga1 Ga6 2.784(4) 15_545
Ga1 Ga1 2.9182(19) 3
Ga1 Ga1 2.920(2) 13
Ga1 Ga2 2.9209(14) 10_556
Ga2 Pd1 2.6361(14) 6
Ga2 Pd1 2.6361(14) 14_456
Ga2 Pd2 2.6416(15) 2
Ga2 Ga5 2.770(4) 7_456
Ga2 Ga5 2.770(4) 13_556
Ga2 Ga7 2.771(5) 13_556
Ga2 Ga7 2.771(5) 7_456
Ga2 Ga3 2.774(4) 3_566
Ga2 Ga3 2.774(4) 9_566
Ga2 Ga2 2.908(3) 9_566
Ga2 Ga1 2.9210(14) 4
Ga2 Ga1 2.9210(14) 10_556
Ga3 Yb2 1.584(5) .
Ga3 Ga6 1.639(5) .
Ga3 Ga7 1.663(6) 15
Ga3 Pd1 2.558(2) 6
Ga3 Pd1 2.558(2) 13
Ga3 Ga4 2.734(7) .
Ga3 Ga1 2.752(4) 10_556
Ga3 Ga3 2.760(10) 11
Ga3 Ga2 2.774(4) 9_566
Ga3 Ga2 2.774(4) 2_564
Ga4 Yb2 1.581(6) .
Ga4 Ga5 1.649(7) 5_445
Ga4 Ga5 1.649(7) 15_545
Ga4 Pd2 2.558(2) 2
Ga4 Ga3 2.734(7) 11
Ga4 Ga1 2.7627(15) 10_556
Ga4 Ga1 2.7627(15) 11
Ga4 Ga1 2.7627(15) 4
Ga4 Yb1 3.125(5) 5_445
Yb2 Ga3 1.584(5) 11
Yb2 Ga2 3.021(2) 9_566
Yb2 Ga2 3.021(2) 2_564
Yb2 Ga1 3.0240(14) 11
Yb2 Ga1 3.0240(14) 10_556
Yb2 Ga1 3.0240(14) 4
Yb2 Ga2 3.097(2) 10_556
Yb2 Ga6 3.112(5) .
Ga5 Ga5 1.646(10) 11_655
Ga5 Ga4 1.649(7) 5
Ga5 Pd2 2.5571(19) 6
Ga5 Pd2 2.5571(19) 5
Ga5 Ga6 2.741(7) .
Ga5 Ga7 2.744(7) .
Ga5 Ga1 2.763(4) 8
Ga5 Ga1 2.763(4) 15
Ga5 Ga2 2.770(4) 6_554
Ga5 Ga2 2.770(4) 13_556
Ga5 Yb2 3.120(5) 5
Ga6 Ga7 1.677(7) 15
Ga6 Pd1 2.563(2) 13
Ga6 Pd1 2.563(2) 6
Ga6 Ga7 2.704(8) .
Ga6 Ga1 2.740(4) 10_556
Ga6 Ga1 2.784(4) 8
Ga6 Ga1 2.784(4) 15
Ga7 Ga3 1.663(6) 15_545
Ga7 Ga6 1.677(7) 15_545
Ga7 Pd1 2.5593(15) 10_556
Ga7 Ga1 2.755(5) 10_556
Ga7 Ga2 2.771(5) 13_556
Ga7 Ga2 2.771(5) 6_554
Ga7 Yb1 3.116(5) 15_545
