#------------------------------------------------------------------------------
#$Date: 2016-03-21 01:21:50 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178377 $
#$URL: svn://www.crystallography.net/cod/cif/4/00/18/4001854.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4001854
loop_
_publ_author_name
'Zeilinger, Michael'
'Kurylyshyn, Iryna M.'
'Häussermann, Ulrich'
'Fässler, Thomas F.'
_publ_section_title
;
 Revision of the Li--Si Phase Diagram: Discovery and Single-Crystal X-ray
 Structure Determination of the High-Temperature Phase Li4.11Si
;
_journal_issue                   22
_journal_name_full               'Chemistry of Materials'
_journal_page_first              4623
_journal_paper_doi               10.1021/cm4029885
_journal_volume                  25
_journal_year                    2013
_chemical_formula_analytical     'Li4.106 Si'
_chemical_formula_moiety         'Li4.106 Si'
_chemical_formula_sum            'Li4.106 Si'
_chemical_formula_weight         56.59
_chemical_melting_point          '891 K, peritectic decomposition'
_chemical_name_common            'Lithium Silicide'
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           63
_symmetry_cell_setting           orthorhombic
_symmetry_Int_Tables_number      63
_symmetry_space_group_name_Hall  '-C 2c 2'
_symmetry_space_group_name_H-M   'C m c m'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            16
_cell_length_a                   4.5246(2)
_cell_length_b                   21.9437(10)
_cell_length_c                   13.2001(6)
_cell_measurement_reflns_used    9834
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      50.0916
_cell_measurement_theta_min      2.4138
_cell_volume                     1310.59(10)
_citation_year                   2013
_computing_cell_refinement
'SAINT Version 7.56a, Bruker AXS Inc., Madison, Wisconsin, USA, 2008. '
_computing_data_collection
;APEX suite of crystallographic software. APEX 2 Version 2008.4,
 Bruker AXS Inc., Madison, Wisconsin, USA, 2008.
;
_computing_data_reduction
'SAINT Version 7.56a, Bruker AXS Inc., Madison, Wisconsin, USA, 2008. '
_computing_molecular_graphics    'Diamond 3 (Crystal Impact 2011)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      100(2)
_diffrn_detector                 'CCD plate'
_diffrn_detector_area_resol_mean 16
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'phi- and omega-rotation'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0197
_diffrn_reflns_av_sigmaI/netI    0.0074
_diffrn_reflns_limit_h_max       9
_diffrn_reflns_limit_h_min       -9
_diffrn_reflns_limit_k_max       43
_diffrn_reflns_limit_k_min       -43
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -26
_diffrn_reflns_number            53893
_diffrn_reflns_theta_full        45.29
_diffrn_reflns_theta_max         45.29
_diffrn_reflns_theta_min         1.86
_exptl_absorpt_coefficient_mu    0.390
_exptl_absorpt_correction_T_max  0.7499
_exptl_absorpt_correction_T_min  0.5676
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS, Bruker, 2008b'
_exptl_crystal_colour            'metallic silver'
_exptl_crystal_density_diffrn    1.147
_exptl_crystal_density_meas      ?
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             421
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.28
_refine_diff_density_max         0.348
_refine_diff_density_min         -0.305
_refine_diff_density_rms         0.039
_refine_ls_extinction_coef       -
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.087
_refine_ls_matrix_type           full
_refine_ls_number_parameters     81
_refine_ls_number_reflns         3052
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.087
_refine_ls_R_factor_all          0.0171
_refine_ls_R_factor_gt           0.0120
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0137P)²+0.0415P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0274
_refine_ls_wR_factor_ref         0.0294
_reflns_number_gt                2596
_reflns_number_total             3052
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            cm4029885_si_002.cif
_cod_data_source_block           Li4.11Si_100K
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_crystal_density_meas' value 'not measured' was changed to '?'
- the value is perceived as not measured.

Automatic conversion script
Id: cif_fix_values 3008 2015-01-20 13:52:24Z robertas 
;
_cod_database_code               4001854
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, z+1/2'
'-x, y, -z+1/2'
'x, -y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z'
'-x, -y, -z'
'x, y, -z-1/2'
'x, -y, z-1/2'
'-x, y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, y+1/2, -z-1/2'
'x+1/2, -y+1/2, z-1/2'
'-x+1/2, y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_group
Si1 Si 0.0000 0.256155(4) 0.2500 0.00789(2) Uani 1 4 d S .
Si2 Si 0.5000 0.454324(4) 0.2500 0.00681(2) Uani 1 4 d S .
Si3 Si 0.5000 0.105366(3) 0.067645(5) 0.00775(2) Uani 1 2 d S .
Li1 Li 0.5000 0.03270(3) 0.2500 0.01340(11) Uani 1 4 d S .
Li2 Li 0.5000 0.32951(3) 0.2500 0.01271(11) Uani 1 4 d S .
Li3 Li 0.0000 0.39263(3) 0.2500 0.01648(13) Uani 1 4 d S .
Li4A Li 0.5000 0.14744(7) 0.2500 0.0435(7) Uani 0.575(3) 4 d SP 1
Li5A Li 0.0000 0.17392(4) 0.08488(13) 0.0142(2) Uani 0.848(7) 2 d SP 1
Li4B Li 0.2084(3) 0.13867(5) 0.2500 0.0181(3) Uani 0.425(3) 2 d SP 2
Li5B Li 0.0000 0.1641(3) 0.1246(9) 0.0180(16) Uani 0.152(7) 2 d SP 2
Li6 Li 0.0000 0.04654(2) 0.12217(4) 0.01309(8) Uani 1 2 d S .
Li7 Li 0.0000 0.31629(3) 0.07895(4) 0.01535(8) Uani 1 2 d S .
Li8 Li 0.0000 0.47119(3) 0.09071(4) 0.01814(9) Uani 1 2 d S .
Li9 Li 0.5000 0.23121(3) 0.13577(4) 0.01796(9) Uani 1 2 d S .
Li10 Li 0.5000 0.40459(2) 0.06398(4) 0.01402(8) Uani 1 2 d S .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Li5B Si1 Li5B 78.6(6) . 10_556
Li5B Si1 Li7 81.0(3) . .
Li5B Si1 Li7 159.6(3) 10_556 .
Li5B Si1 Li7 159.6(3) . 10_556
Li5B Si1 Li7 81.0(3) 10_556 10_556
Li7 Si1 Li7 119.40(3) . 10_556
Li7 Si1 Li4B 118.284(14) . .
Li7 Si1 Li4B 118.285(14) 10_556 .
Li7 Si1 Li4B 118.285(14) . 3
Li7 Si1 Li4B 118.284(14) 10_556 3
Li5B Si1 Li9 60.19(10) . 1_455
Li5B Si1 Li9 101.06(16) 10_556 1_455
Li7 Si1 Li9 68.293(15) . 1_455
Li7 Si1 Li9 124.680(10) 10_556 1_455
Li4B Si1 Li9 95.44(3) . 1_455
Li4B Si1 Li9 62.25(3) 3 1_455
Li5B Si1 Li9 101.06(16) . 10_556
Li5B Si1 Li9 60.19(10) 10_556 10_556
Li7 Si1 Li9 124.681(9) . 10_556
Li7 Si1 Li9 68.294(14) 10_556 10_556
Li4B Si1 Li9 62.25(3) . 10_556
Li4B Si1 Li9 95.44(3) 3 10_556
Li9 Si1 Li9 157.24(2) 1_455 10_556
Li5B Si1 Li9 101.06(16) . 10_456
Li5B Si1 Li9 60.19(10) 10_556 10_456
Li7 Si1 Li9 124.681(9) . 10_456
Li7 Si1 Li9 68.294(15) 10_556 10_456
Li4B Si1 Li9 95.44(3) . 10_456
Li4B Si1 Li9 62.25(3) 3 10_456
Li9 Si1 Li9 65.87(2) 1_455 10_456
Li9 Si1 Li9 109.322(19) 10_556 10_456
Li5B Si1 Li9 60.19(10) . .
Li5B Si1 Li9 101.06(16) 10_556 .
Li7 Si1 Li9 68.294(14) . .
Li7 Si1 Li9 124.681(9) 10_556 .
Li4B Si1 Li9 62.25(3) . .
Li4B Si1 Li9 95.44(3) 3 .
Li9 Si1 Li9 109.322(19) 1_455 .
Li9 Si1 Li9 65.87(2) 10_556 .
Li9 Si1 Li9 157.24(2) 10_456 .
Li5B Si1 Li2 116.65(12) . .
Li5B Si1 Li2 116.65(12) 10_556 .
Li7 Si1 Li2 72.991(9) . .
Li7 Si1 Li2 72.991(9) 10_556 .
Li4B Si1 Li2 105.34(3) . .
Li4B Si1 Li2 145.53(3) 3 .
Li9 Si1 Li2 141.176(14) 1_455 .
Li9 Si1 Li2 56.617(14) 10_556 .
Li9 Si1 Li2 141.176(14) 10_456 .
Li9 Si1 Li2 56.617(14) . .
Li5B Si1 Li2 116.65(12) . 1_455
Li5B Si1 Li2 116.65(12) 10_556 1_455
Li7 Si1 Li2 72.991(9) . 1_455
Li7 Si1 Li2 72.989(9) 10_556 1_455
Li4B Si1 Li2 145.53(3) . 1_455
Li4B Si1 Li2 105.34(3) 3 1_455
Li9 Si1 Li2 56.619(14) 1_455 1_455
Li9 Si1 Li2 141.174(14) 10_556 1_455
Li9 Si1 Li2 56.617(14) 10_456 1_455
Li9 Si1 Li2 141.176(14) . 1_455
Li2 Si1 Li2 109.13(2) . 1_455
Li6 Si2 Li6 79.64(2) 14_556 5
Li6 Si2 Li3 113.225(10) 14_556 1_655
Li6 Si2 Li3 113.227(10) 5 1_655
Li6 Si2 Li3 113.226(10) 14_556 .
Li6 Si2 Li3 113.226(10) 5 .
Li3 Si2 Li3 118.21(3) 1_655 .
Li6 Si2 Li10 153.785(17) 14_556 .
Li6 Si2 Li10 74.142(16) 5 .
Li3 Si2 Li10 77.964(8) 1_655 .
Li3 Si2 Li10 77.963(8) . .
Li6 Si2 Li10 74.142(16) 14_556 10_556
Li6 Si2 Li10 153.785(17) 5 10_556
Li3 Si2 Li10 77.962(8) 1_655 10_556
Li3 Si2 Li10 77.963(8) . 10_556
Li10 Si2 Li10 132.07(2) . 10_556
Li6 Si2 Li2 140.178(12) 14_556 .
Li6 Si2 Li2 140.178(12) 5 .
Li3 Si2 Li2 59.105(13) 1_655 .
Li3 Si2 Li2 59.105(13) . .
Li10 Si2 Li2 66.037(12) . .
Li10 Si2 Li2 66.037(12) 10_556 .
Li6 Si2 Li1 62.300(10) 14_556 5
Li6 Si2 Li1 62.302(10) 5 5
Li3 Si2 Li1 68.139(17) 1_655 5
Li3 Si2 Li1 173.651(18) . 5
Li10 Si2 Li1 104.231(9) . 5
Li10 Si2 Li1 104.229(8) 10_556 5
Li2 Si2 Li1 127.244(12) . 5
Li6 Si2 Li1 62.300(10) 14_556 5_455
Li6 Si2 Li1 62.302(10) 5 5_455
Li3 Si2 Li1 173.651(18) 1_655 5_455
Li3 Si2 Li1 68.139(17) . 5_455
Li10 Si2 Li1 104.231(9) . 5_455
Li10 Si2 Li1 104.229(8) 10_556 5_455
Li2 Si2 Li1 127.244(12) . 5_455
Li1 Si2 Li1 105.51(2) 5 5_455
Li6 Si2 Li8 58.382(11) 14_556 10_656
Li6 Si2 Li8 109.969(12) 5 10_656
Li3 Si2 Li8 55.735(12) 1_655 10_656
Li3 Si2 Li8 133.249(10) . 10_656
Li10 Si2 Li8 131.760(9) . 10_656
Li10 Si2 Li8 55.293(10) 10_556 10_656
Li2 Si2 Li8 96.832(10) . 10_656
Li1 Si2 Li8 49.385(10) 5 10_656
Li1 Si2 Li8 120.461(12) 5_455 10_656
Li6 Si2 Li8 109.969(12) 14_556 1_655
Li6 Si2 Li8 58.382(11) 5 1_655
Li3 Si2 Li8 55.737(12) 1_655 1_655
Li3 Si2 Li8 133.249(10) . 1_655
Li10 Si2 Li8 55.293(10) . 1_655
Li10 Si2 Li8 131.760(9) 10_556 1_655
Li2 Si2 Li8 96.832(10) . 1_655
Li1 Si2 Li8 49.387(11) 5 1_655
Li1 Si2 Li8 120.463(12) 5_455 1_655
Li8 Si2 Li8 85.057(16) 10_656 1_655
Li6 Si2 Li8 58.382(12) 14_556 10_556
Li6 Si2 Li8 109.969(12) 5 10_556
Li3 Si2 Li8 133.248(10) 1_655 10_556
Li3 Si2 Li8 55.736(12) . 10_556
Li10 Si2 Li8 131.760(9) . 10_556
Li10 Si2 Li8 55.293(10) 10_556 10_556
Li2 Si2 Li8 96.832(10) . 10_556
Li1 Si2 Li8 120.461(12) 5 10_556
Li1 Si2 Li8 49.385(10) 5_455 10_556
Li8 Si2 Li8 93.318(16) 10_656 10_556
Li8 Si2 Li8 166.34(2) 1_655 10_556
Li4A Si3 Li7 117.40(4) . 13
Li4A Si3 Li8 162.20(3) . 13
Li7 Si3 Li8 80.41(2) 13 13
Li4A Si3 Li6 85.55(2) . 1_655
Li7 Si3 Li6 121.090(10) 13 1_655
Li8 Si3 Li6 84.744(14) 13 1_655
Li4A Si3 Li6 85.55(2) . .
Li7 Si3 Li6 121.090(10) 13 .
Li8 Si3 Li6 84.743(14) 13 .
Li6 Si3 Li6 113.688(17) 1_655 .
Li4A Si3 Li5B 64.6(2) . 1_655
Li7 Si3 Li5B 83.8(3) 13 1_655
Li8 Si3 Li5B 120.94(15) 13 1_655
Li6 Si3 Li5B 56.92(15) 1_655 1_655
Li6 Si3 Li5B 148.4(3) . 1_655
Li4A Si3 Li5B 64.6(2) . .
Li7 Si3 Li5B 83.8(3) 13 .
Li8 Si3 Li5B 120.94(15) 13 .
Li6 Si3 Li5B 148.4(3) 1_655 .
Li6 Si3 Li5B 56.92(15) . .
Li5B Si3 Li5B 113.20(15) 1_655 .
Li4A Si3 Li5A 74.01(4) . .
Li7 Si3 Li5A 72.30(4) 13 .
Li8 Si3 Li5A 114.25(3) 13 .
Li6 Si3 Li5A 159.40(4) 1_655 .
Li6 Si3 Li5A 63.04(2) . .
Li5B Si3 Li5A 114.04(7) 1_655 .
Li4A Si3 Li5A 74.01(4) . 1_655
Li7 Si3 Li5A 72.29(4) 13 1_655
Li8 Si3 Li5A 114.25(3) 13 1_655
Li6 Si3 Li5A 63.04(2) 1_655 1_655
Li6 Si3 Li5A 159.40(4) . 1_655
Li5B Si3 Li5A 114.03(7) . 1_655
Li5A Si3 Li5A 112.16(3) . 1_655
Li7 Si3 Li4B 117.56(2) 13 .
Li8 Si3 Li4B 145.25(3) 13 .
Li6 Si3 Li4B 106.62(3) 1_655 .
Li6 Si3 Li4B 60.55(3) . .
Li5B Si3 Li4B 91.7(2) 1_655 .
Li5A Si3 Li4B 53.27(4) . .
Li5A Si3 Li4B 99.95(4) 1_655 .
Li7 Si3 Li4B 117.56(2) 13 3_655
Li8 Si3 Li4B 145.25(3) 13 3_655
Li6 Si3 Li4B 60.55(3) 1_655 3_655
Li6 Si3 Li4B 106.62(3) . 3_655
Li5B Si3 Li4B 91.7(2) . 3_655
Li5A Si3 Li4B 99.95(4) . 3_655
Li5A Si3 Li4B 53.27(4) 1_655 3_655
Li4B Si3 Li4B 55.35(5) . 3_655
Li4A Si3 Li10 126.470(10) . 13
Li7 Si3 Li10 66.216(13) 13 13
Li8 Si3 Li10 58.584(10) 13 13
Li6 Si3 Li10 141.935(15) 1_655 13
Li6 Si3 Li10 57.539(14) . 13
Li5B Si3 Li10 149.9(3) 1_655 13
Li5B Si3 Li10 62.92(18) . 13
Li5A Si3 Li10 55.71(3) . 13
Li5A Si3 Li10 138.50(4) 1_655 13
Li4B Si3 Li10 99.61(3) . 13
Li4B Si3 Li10 154.37(3) 3_655 13
Li8 Li1 Li8 114.60(4) 5_545 14_546
Li8 Li1 Li4A 122.700(19) 5_545 .
Li8 Li1 Li4A 122.700(19) 14_546 .
Li8 Li1 Li4B 118.028(17) 5_545 3_655
Li8 Li1 Li4B 118.025(17) 14_546 3_655
Li4A Li1 Li4B 29.57(3) . 3_655
Li8 Li1 Li4B 118.026(17) 5_545 .
Li8 Li1 Li4B 118.026(17) 14_546 .
Li4A Li1 Li4B 29.57(3) . .
Li4B Li1 Li4B 59.14(6) 3_655 .
Li8 Li1 Li6 123.919(15) 5_545 10_656
Li8 Li1 Li6 63.742(12) 14_546 10_656
Li4A Li1 Li6 83.858(17) . 10_656
Li4B Li1 Li6 60.90(3) 3_655 10_656
Li4B Li1 Li6 107.47(3) . 10_656
Li8 Li1 Li6 63.742(12) 5_545 1_655
Li8 Li1 Li6 123.919(15) 14_546 1_655
Li4A Li1 Li6 83.858(17) . 1_655
Li4B Li1 Li6 60.90(3) 3_655 1_655
Li4B Li1 Li6 107.47(3) . 1_655
Li6 Li1 Li6 72.945(18) 10_656 1_655
Li8 Li1 Li6 123.919(15) 5_545 10_556
Li8 Li1 Li6 63.742(12) 14_546 10_556
Li4A Li1 Li6 83.858(17) . 10_556
Li4B Li1 Li6 107.47(3) 3_655 10_556
Li4B Li1 Li6 60.90(3) . 10_556
Li6 Li1 Li6 105.688(18) 10_656 10_556
Li6 Li1 Li6 167.72(3) 1_655 10_556
Li8 Li1 Li6 63.740(12) 5_545 .
Li8 Li1 Li6 123.919(15) 14_546 .
Li4A Li1 Li6 83.860(17) . .
Li4B Li1 Li6 107.47(3) 3_655 .
Li4B Li1 Li6 60.90(3) . .
Li6 Li1 Li6 167.72(3) 10_656 .
Li6 Li1 Li6 105.688(18) 1_655 .
Li6 Li1 Li6 72.945(18) 10_556 .
Li8 Li1 Si2 70.917(15) 5_545 5_445
Li8 Li1 Si2 70.915(15) 14_546 5_445
Li4A Li1 Si2 127.243(12) . 5_445
Li4B Li1 Si2 156.81(4) 3_655 5_445
Li4B Li1 Si2 97.67(3) . 5_445
Li6 Li1 Si2 134.36(2) 10_656 5_445
Li6 Li1 Si2 134.37(2) 1_655 5_445
Li6 Li1 Si2 55.269(10) 10_556 5_445
Li6 Li1 Si2 55.269(10) . 5_445
Li8 Li1 Si2 70.917(15) 5_545 5_545
Li8 Li1 Si2 70.915(15) 14_546 5_545
Li4A Li1 Si2 127.243(12) . 5_545
Li4B Li1 Si2 97.67(3) 3_655 5_545
Li4B Li1 Si2 156.81(4) . 5_545
Li6 Li1 Si2 55.269(10) 10_656 5_545
Li6 Li1 Si2 55.270(10) 1_655 5_545
Li6 Li1 Si2 134.36(2) 10_556 5_545
Li6 Li1 Si2 134.36(2) . 5_545
Si2 Li1 Si2 105.51(2) 5_445 5_545
Li8 Li1 Si3 179.18(3) 5_545 10_556
Li8 Li1 Si3 66.221(14) 14_546 10_556
Li4A Li1 Si3 56.479(12) . 10_556
Li4B Li1 Si3 61.293(16) 3_655 10_556
Li4B Li1 Si3 61.294(16) . 10_556
Li6 Li1 Si3 56.313(10) 10_656 10_556
Li6 Li1 Si3 115.880(18) 1_655 10_556
Li6 Li1 Si3 56.313(10) 10_556 10_556
Li6 Li1 Si3 115.881(18) . 10_556
Si2 Li1 Si3 109.524(2) 5_445 10_556
Si2 Li1 Si3 109.524(2) 5_545 10_556
Li9 Li2 Li9 69.91(3) 10_556 .
Li9 Li2 Li3 115.339(13) 10_556 .
Li9 Li2 Li3 115.339(13) . .
Li9 Li2 Li3 115.338(13) 10_556 1_655
Li9 Li2 Li3 115.340(13) . 1_655
Li3 Li2 Li3 117.05(4) . 1_655
Li9 Li2 Si2 145.046(16) 10_556 .
Li9 Li2 Si2 145.046(16) . .
Li3 Li2 Si2 58.523(18) . .
Li3 Li2 Si2 58.522(18) 1_655 .
Li9 Li2 Si1 61.629(13) 10_556 .
Li9 Li2 Si1 61.629(13) . .
Li3 Li2 Si1 66.912(13) . .
Li3 Li2 Si1 176.04(3) 1_655 .
Si2 Li2 Si1 125.434(12) . .
Li9 Li2 Si1 61.628(13) 10_556 1_655
Li9 Li2 Si1 61.629(13) . 1_655
Li3 Li2 Si1 176.04(3) . 1_655
Li3 Li2 Si1 66.912(13) 1_655 1_655
Si2 Li2 Si1 125.435(12) . 1_655
Si1 Li2 Si1 109.13(2) . 1_655
Li9 Li2 Li10 88.905(17) 10_556 10_556
Li9 Li2 Li10 158.81(3) . 10_556
Li3 Li2 Li10 73.087(14) . 10_556
Li3 Li2 Li10 73.085(14) 1_655 10_556
Si2 Li2 Li10 56.140(15) . 10_556
Si1 Li2 Li10 108.846(5) . 10_556
Si1 Li2 Li10 108.845(5) 1_655 10_556
Li9 Li2 Li10 158.81(3) 10_556 .
Li9 Li2 Li10 88.905(17) . .
Li3 Li2 Li10 73.087(14) . .
Li3 Li2 Li10 73.087(14) 1_655 .
Si2 Li2 Li10 56.140(15) . .
Si1 Li2 Li10 108.846(5) . .
Si1 Li2 Li10 108.847(5) 1_655 .
Li10 Li2 Li10 112.28(3) 10_556 .
Li9 Li2 Li7 109.20(2) 10_556 .
Li9 Li2 Li7 61.497(15) . .
Li3 Li2 Li7 56.363(11) . .
Li3 Li2 Li7 130.421(16) 1_655 .
Si2 Li2 Li7 95.189(16) . .
Si1 Li2 Li7 51.188(9) . .
Si1 Li2 Li7 121.460(18) 1_655 .
Li10 Li2 Li7 129.391(16) 10_556 .
Li10 Li2 Li7 57.736(11) . .
Li9 Li2 Li7 61.498(15) 10_556 10_656
Li9 Li2 Li7 109.21(2) . 10_656
Li3 Li2 Li7 130.419(16) . 10_656
Li3 Li2 Li7 56.361(11) 1_655 10_656
Si2 Li2 Li7 95.188(16) . 10_656
Si1 Li2 Li7 121.460(18) . 10_656
Si1 Li2 Li7 51.188(9) 1_655 10_656
Li10 Li2 Li7 57.735(11) 10_556 10_656
Li10 Li2 Li7 129.390(16) . 10_656
Li7 Li2 Li7 169.62(3) . 10_656
Li9 Li2 Li7 61.498(15) 10_556 10_556
Li9 Li2 Li7 109.21(2) . 10_556
Li3 Li2 Li7 56.362(11) . 10_556
Li3 Li2 Li7 130.418(16) 1_655 10_556
Si2 Li2 Li7 95.188(16) . 10_556
Si1 Li2 Li7 51.189(9) . 10_556
Si1 Li2 Li7 121.459(18) 1_655 10_556
Li10 Li2 Li7 57.735(11) 10_556 10_556
Li10 Li2 Li7 129.390(16) . 10_556
Li7 Li2 Li7 89.422(14) . 10_556
Li7 Li2 Li7 89.641(14) 10_656 10_556
Si2 Li3 Si2 118.21(3) . 1_455
Si2 Li3 Li2 179.42(3) . 1_455
Si2 Li3 Li2 62.372(13) 1_455 1_455
Si2 Li3 Li2 62.372(13) . .
Si2 Li3 Li2 179.42(3) 1_455 .
Li2 Li3 Li2 117.05(4) 1_455 .
Si2 Li3 Li8 71.002(13) . 10_556
Si2 Li3 Li8 71.000(13) 1_455 10_556
Li2 Li3 Li8 109.330(9) 1_455 10_556
Li2 Li3 Li8 109.332(8) . 10_556
Si2 Li3 Li8 71.002(13) . .
Si2 Li3 Li8 71.002(13) 1_455 .
Li2 Li3 Li8 109.332(9) 1_455 .
Li2 Li3 Li8 109.332(9) . .
Li8 Li3 Li8 101.31(3) 10_556 .
Si2 Li3 Li7 107.816(5) . 10_556
Si2 Li3 Li7 107.816(5) 1_455 10_556
Li2 Li3 Li7 71.872(14) 1_455 10_556
Li2 Li3 Li7 71.872(14) . 10_556
Li8 Li3 Li7 75.919(16) 10_556 10_556
Li8 Li3 Li7 177.23(3) . 10_556
Si2 Li3 Li7 107.816(5) . .
Si2 Li3 Li7 107.818(5) 1_455 .
Li2 Li3 Li7 71.873(14) 1_455 .
Li2 Li3 Li7 71.872(14) . .
Li8 Li3 Li7 177.23(3) 10_556 .
Li8 Li3 Li7 75.921(16) . .
Li7 Li3 Li7 106.85(3) 10_556 .
Si2 Li3 Si1 120.895(13) . .
Si2 Li3 Si1 120.897(13) 1_455 .
Li2 Li3 Si1 58.524(18) 1_455 .
Li2 Li3 Si1 58.523(18) . .
Li8 Li3 Si1 129.345(16) 10_556 .
Li8 Li3 Si1 129.345(16) . .
Li7 Li3 Si1 53.426(15) 10_556 .
Li7 Li3 Si1 53.424(15) . .
Si2 Li3 Li1 59.105(13) . 5_455
Si2 Li3 Li1 59.103(13) 1_455 5_455
Li2 Li3 Li1 121.476(18) 1_455 5_455
Li2 Li3 Li1 121.477(18) . 5_455
Li8 Li3 Li1 50.654(16) 10_556 5_455
Li8 Li3 Li1 50.656(16) . 5_455
Li7 Li3 Li1 126.573(15) 10_556 5_455
Li7 Li3 Li1 126.577(15) . 5_455
Si1 Li3 Li1 180.0 . 5_455
Si2 Li3 Li10 51.692(8) . 10_556
Si2 Li3 Li10 122.644(16) 1_455 10_556
Li2 Li3 Li10 128.098(15) 1_455 10_556
Li2 Li3 Li10 57.642(10) . 10_556
Li8 Li3 Li10 51.927(10) 10_556 10_556
Li8 Li3 Li10 121.15(2) . 10_556
Li7 Li3 Li10 57.172(11) 10_556 10_556
Li7 Li3 Li10 129.455(16) . 10_556
Si1 Li3 Li10 94.493(15) . 10_556
Li1 Li3 Li10 85.506(15) 5_455 10_556
Si2 Li3 Li10 122.645(16) . 1_455
Si2 Li3 Li10 51.694(8) 1_455 1_455
Li2 Li3 Li10 57.643(10) 1_455 1_455
Li2 Li3 Li10 128.098(15) . 1_455
Li8 Li3 Li10 121.15(2) 10_556 1_455
Li8 Li3 Li10 51.927(10) . 1_455
Li7 Li3 Li10 129.456(16) 10_556 1_455
Li7 Li3 Li10 57.173(11) . 1_455
Si1 Li3 Li10 94.493(15) . 1_455
Li1 Li3 Li10 85.508(15) 5_455 1_455
Li10 Li3 Li10 171.01(3) 10_556 1_455
Li9 Li4A Li9 78.72(5) . 10_556
Li9 Li4A Li1 140.64(3) . .
Li9 Li4A Li1 140.64(3) 10_556 .
Li9 Li4A Si3 150.34(6) . 10_556
Li9 Li4A Si3 71.624(16) 10_556 10_556
Li1 Li4A Si3 69.02(3) . 10_556
Li9 Li4A Si3 71.623(16) . .
Li9 Li4A Si3 150.34(6) 10_556 .
Li1 Li4A Si3 69.02(3) . .
Si3 Li4A Si3 138.03(7) 10_556 .
Li9 Li4A Li5A 55.02(2) . .
Li9 Li4A Li5A 106.98(4) 10_556 .
Li1 Li4A Li5A 100.48(3) . .
Si3 Li4A Li5A 134.60(3) 10_556 .
Si3 Li4A Li5A 55.120(17) . .
Li9 Li4A Li5A 106.98(4) . 10_656
Li9 Li4A Li5A 55.02(2) 10_556 10_656
Li1 Li4A Li5A 100.48(3) . 10_656
Si3 Li4A Li5A 55.120(17) 10_556 10_656
Si3 Li4A Li5A 134.60(3) . 10_656
Li5A Li4A Li5A 159.04(6) . 10_656
Li9 Li4A Li5A 55.02(2) . 1_655
Li9 Li4A Li5A 106.98(4) 10_556 1_655
Li1 Li4A Li5A 100.48(3) . 1_655
Si3 Li4A Li5A 134.60(3) 10_556 1_655
Si3 Li4A Li5A 55.120(17) . 1_655
Li5A Li4A Li5A 90.17(5) . 1_655
Li5A Li4A Li5A 86.04(4) 10_656 1_655
Li9 Li4A Li5A 106.98(4) . 10_556
Li9 Li4A Li5A 55.02(2) 10_556 10_556
Li1 Li4A Li5A 100.48(3) . 10_556
Si3 Li4A Li5A 55.120(17) 10_556 10_556
Si3 Li4A Li5A 134.60(3) . 10_556
Li5A Li4A Li5A 86.04(4) . 10_556
Li5A Li4A Li5A 90.17(5) 10_656 10_556
Li5A Li4A Li5A 159.04(6) 1_655 10_556
Li10 Li5A Li9 119.92(3) 13 .
Li10 Li5A Li9 119.92(3) 13 1_455
Li9 Li5A Li9 115.57(3) . 1_455
Li10 Li5A Si3 64.754(16) 13 1_455
Li9 Li5A Si3 169.25(8) . 1_455
Li9 Li5A Si3 65.060(12) 1_455 1_455
Li10 Li5A Si3 64.754(16) 13 .
Li9 Li5A Si3 65.060(12) . .
Li9 Li5A Si3 169.25(8) 1_455 .
Si3 Li5A Si3 112.16(3) 1_455 .
Li10 Li5A Si1 178.38(7) 13 .
Li9 Li5A Si1 60.44(2) . .
Li9 Li5A Si1 60.44(2) 1_455 .
Si3 Li5A Si1 114.59(4) 1_455 .
Si3 Li5A Si1 114.59(4) . .
Li10 Li5A Li6 58.75(2) 13 .
Li9 Li5A Li6 114.80(4) . .
Li9 Li5A Li6 114.80(4) 1_455 .
Si3 Li5A Li6 58.065(18) 1_455 .
Si3 Li5A Li6 58.066(18) . .
Si1 Li5A Li6 119.63(7) . .
Li10 Li5A Li7 129.81(7) 13 .
Li9 Li5A Li7 62.372(19) . .
Li9 Li5A Li7 62.372(19) 1_455 .
Si3 Li5A Li7 123.33(2) 1_455 .
Si3 Li5A Li7 123.33(2) . .
Si1 Li5A Li7 51.814(15) . .
Li6 Li5A Li7 171.45(7) . .
Li10 Li5A Li7 61.76(3) 13 13_455
Li9 Li5A Li7 138.69(6) . 13_455
Li9 Li5A Li7 62.02(2) 1_455 13_455
Si3 Li5A Li7 51.818(17) 1_455 13_455
Si3 Li5A Li7 125.36(4) . 13_455
Si1 Li5A Li7 119.16(2) . 13_455
Li6 Li5A Li7 100.78(2) . 13_455
Li7 Li5A Li7 85.08(4) . 13_455
Li10 Li5A Li7 61.76(3) 13 13
Li9 Li5A Li7 62.02(2) . 13
Li9 Li5A Li7 138.69(6) 1_455 13
Si3 Li5A Li7 125.36(4) 1_455 13
Si3 Li5A Li7 51.818(17) . 13
Si1 Li5A Li7 119.16(2) . 13
Li6 Li5A Li7 100.78(2) . 13
Li7 Li5A Li7 85.08(4) . 13
Li7 Li5A Li7 92.30(5) 13_455 13
Li10 Li5A Li4A 113.15(3) 13 .
Li9 Li5A Li4A 46.76(3) . .
Li9 Li5A Li4A 120.88(6) 1_455 .
Si3 Li5A Li4A 122.97(6) 1_455 .
Si3 Li5A Li4A 50.87(2) . .
Si1 Li5A Li4A 65.83(4) . .
Li6 Li5A Li4A 72.69(4) . .
Li7 Li5A Li4A 101.48(3) . .
Li7 Li5A Li4A 173.44(4) 13_455 .
Li7 Li5A Li4A 88.401(8) 13 .
Li10 Li5A Li4A 113.15(3) 13 1_455
Li9 Li5A Li4A 120.88(6) . 1_455
Li9 Li5A Li4A 46.77(3) 1_455 1_455
Si3 Li5A Li4A 50.87(2) 1_455 1_455
Si3 Li5A Li4A 122.97(6) . 1_455
Si1 Li5A Li4A 65.83(4) . 1_455
Li6 Li5A Li4A 72.69(4) . 1_455
Li7 Li5A Li4A 101.48(3) . 1_455
Li7 Li5A Li4A 88.401(8) 13_455 1_455
Li7 Li5A Li4A 173.44(4) 13 1_455
Li4A Li5A Li4A 90.17(5) . 1_455
Li4B Li4B Li5B 61.63(19) 3 10_556
Li4B Li4B Li5B 61.63(18) 3 .
Li5B Li4B Li5B 113.0(3) 10_556 .
Li4B Li4B Li4B 180.0 3 3_655
Li5B Li4B Li4B 118.37(19) 10_556 3_655
Li5B Li4B Li4B 118.37(19) . 3_655
Li4B Li4B Li1 119.57(3) 3 .
Li5B Li4B Li1 118.60(11) 10_556 .
Li5B Li4B Li1 118.60(11) . .
Li4B Li4B Li1 60.43(3) 3_655 .
Li4B Li4B Si1 69.91(3) 3 .
Li5B Li4B Si1 64.72(11) 10_556 .
Li5B Li4B Si1 64.72(11) . .
Li4B Li4B Si1 110.09(3) 3_655 .
Li1 Li4B Si1 170.52(6) . .
Li4B Li4B Li6 70.30(3) 3 10_556
Li5B Li4B Li6 62.60(12) 10_556 10_556
Li5B Li4B Li6 123.08(19) . 10_556
Li4B Li4B Li6 109.70(3) 3_655 10_556
Li1 Li4B Li6 62.47(2) . 10_556
Si1 Li4B Li6 124.26(4) . 10_556
Li4B Li4B Li6 70.30(3) 3 .
Li5B Li4B Li6 123.08(19) 10_556 .
Li5B Li4B Li6 62.60(12) . .
Li4B Li4B Li6 109.70(3) 3_655 .
Li1 Li4B Li6 62.47(2) . .
Si1 Li4B Li6 124.26(4) . .
Li6 Li4B Li6 74.21(4) 10_556 .
Li4B Li4B Si3 117.67(3) 3 10_556
Li5B Li4B Si3 65.56(15) 10_556 10_556
Li5B Li4B Si3 178.33(12) . 10_556
Li4B Li4B Si3 62.32(3) 3_655 10_556
Li1 Li4B Si3 63.07(2) . 10_556
Si1 Li4B Si3 113.65(3) . 10_556
Li6 Li4B Si3 57.277(14) 10_556 10_556
Li6 Li4B Si3 118.81(4) . 10_556
Li4B Li4B Si3 117.68(3) 3 .
Li5B Li4B Si3 178.33(12) 10_556 .
Li5B Li4B Si3 65.56(15) . .
Li4B Li4B Si3 62.33(3) 3_655 .
Li1 Li4B Si3 63.07(2) . .
Si1 Li4B Si3 113.65(3) . .
Li6 Li4B Si3 118.81(4) 10_556 .
Li6 Li4B Si3 57.277(14) . .
Si3 Li4B Si3 115.86(5) 10_556 .
Li4B Li4B Li9 117.55(3) 3 .
Li5B Li4B Li9 117.43(14) 10_556 .
Li5B Li4B Li9 65.11(18) . .
Li4B Li4B Li9 62.45(3) 3_655 .
Li1 Li4B Li9 113.01(4) . .
Si1 Li4B Li9 59.36(2) . .
Li6 Li4B Li9 171.61(5) 10_556 .
Li6 Li4B Li9 110.583(16) . .
Si3 Li4B Li9 114.60(5) 10_556 .
Si3 Li4B Li9 61.34(2) . .
Li4B Li4B Li9 117.55(3) 3 10_556
Li5B Li4B Li9 65.11(18) 10_556 10_556
Li5B Li4B Li9 117.42(14) . 10_556
Li4B Li4B Li9 62.45(3) 3_655 10_556
Li1 Li4B Li9 113.01(4) . 10_556
Si1 Li4B Li9 59.36(2) . 10_556
Li6 Li4B Li9 110.583(16) 10_556 10_556
Li6 Li4B Li9 171.61(5) . 10_556
Si3 Li4B Li9 61.34(2) 10_556 10_556
Si3 Li4B Li9 114.60(5) . 10_556
Li9 Li4B Li9 63.82(4) . 10_556
Li4B Li5B Li4B 56.7(4) . 3
Li4B Li5B Li6 74.3(3) . .
Li4B Li5B Li6 74.3(3) 3 .
Li4B Li5B Si1 71.9(3) . .
Li4B Li5B Si1 71.9(3) 3 .
Li6 Li5B Si1 141.4(5) . .
Li4B Li5B Li9 73.15(12) . .
Li4B Li5B Li9 120.4(4) 3 .
Li6 Li5B Li9 123.06(13) . .
Si1 Li5B Li9 62.87(8) . .
Li4B Li5B Li9 120.4(4) . 1_455
Li4B Li5B Li9 73.15(12) 3 1_455
Li6 Li5B Li9 123.06(13) . 1_455
Si1 Li5B Li9 62.87(8) . 1_455
Li9 Li5B Li9 113.59(19) . 1_455
Li4B Li5B Si3 119.6(4) . 1_455
Li4B Li5B Si3 72.62(14) 3 1_455
Li6 Li5B Si3 61.39(9) . 1_455
Si1 Li5B Si3 122.93(13) . 1_455
Li9 Li5B Si3 166.6(6) . 1_455
Li9 Li5B Si3 64.89(4) 1_455 1_455
Li4B Li5B Si3 72.62(14) . .
Li4B Li5B Si3 119.6(4) 3 .
Li6 Li5B Si3 61.39(9) . .
Si1 Li5B Si3 122.93(13) . .
Li9 Li5B Si3 64.89(4) . .
Li9 Li5B Si3 166.6(6) 1_455 .
Si3 Li5B Si3 113.20(15) 1_455 .
Li4B Li5B Li10 124.61(19) . 13
Li4B Li5B Li10 124.61(19) 3 13
Li6 Li5B Li10 58.10(10) . 13
Si1 Li5B Li10 160.5(5) . 13
Li9 Li5B Li10 109.2(3) . 13
Li9 Li5B Li10 109.2(3) 1_455 13
Si3 Li5B Li10 61.08(13) 1_455 13
Si3 Li5B Li10 61.08(13) . 13
Li4B Li5B Li5B 33.50(15) . 10_556
Li4B Li5B Li5B 33.50(15) 3 10_556
Li6 Li5B Li5B 90.7(3) . 10_556
Si1 Li5B Li5B 50.7(3) . 10_556
Li9 Li5B Li5B 86.9(3) . 10_556
Li9 Li5B Li5B 86.9(3) 1_455 10_556
Si3 Li5B Li5B 106.1(3) 1_455 10_556
Si3 Li5B Li5B 106.1(3) . 10_556
Li10 Li5B Li5B 148.8(2) 13 10_556
Li4B Li5B Li7 115.12(16) . .
Li4B Li5B Li7 115.12(16) 3 .
Li6 Li5B Li7 169.0(5) . .
Si1 Li5B Li7 49.55(11) . .
Li9 Li5B Li7 58.22(13) . .
Li9 Li5B Li7 58.22(13) 1_455 .
Si3 Li5B Li7 114.7(3) 1_455 .
Si3 Li5B Li7 114.7(3) . .
Li10 Li5B Li7 110.9(4) 13 .
Li5B Li5B Li7 100.24(19) 10_556 .
Li4B Li5B Li7 166.2(3) . 13_455
Li4B Li5B Li7 111.32(6) 3 13_455
Li6 Li5B Li7 96.44(17) . 13_455
Si1 Li5B Li7 112.8(2) . 13_455
Li9 Li5B Li7 120.6(4) . 13_455
Li9 Li5B Li7 55.95(16) 1_455 13_455
Si3 Li5B Li7 46.64(14) 1_455 13_455
Si3 Li5B Li7 112.4(3) . 13_455
Li10 Li5B Li7 54.09(17) 13 13_455
Li5B Li5B Li7 139.40(12) 10_556 13_455
Li7 Li5B Li7 75.2(2) . 13_455
Li5B Li6 Si2 139.5(3) . 5_445
Li5B Li6 Li10 67.1(3) . 13
Si2 Li6 Li10 153.40(2) 5_445 13
Li5B Li6 Si3 61.69(9) . 1_455
Si2 Li6 Si3 122.510(9) 5_445 1_455
Li10 Li6 Si3 64.203(11) 13 1_455
Li5B Li6 Si3 61.69(9) . .
Si2 Li6 Si3 122.510(9) 5_445 .
Li10 Li6 Si3 64.203(11) 13 .
Si3 Li6 Si3 113.687(17) 1_455 .
Li5B Li6 Li4B 43.1(2) . .
Si2 Li6 Li4B 99.71(2) 5_445 .
Li10 Li6 Li4B 105.30(2) 13 .
Si3 Li6 Li4B 95.60(3) 1_455 .
Si3 Li6 Li4B 62.17(3) . .
Li5B Li6 Li4B 43.1(2) . 3
Si2 Li6 Li4B 99.71(2) 5_445 3
Li10 Li6 Li4B 105.30(2) 13 3
Si3 Li6 Li4B 62.17(3) 1_455 3
Si3 Li6 Li4B 95.60(3) . 3
Li4B Li6 Li4B 39.40(6) . 3
Li5B Li6 Li8 125.84(5) . 5_445
Si2 Li6 Li8 69.243(15) 5_445 5_445
Li10 Li6 Li8 95.688(19) 13 5_445
Si3 Li6 Li8 64.608(10) 1_455 5_445
Si3 Li6 Li8 155.28(3) . 5_445
Li4B Li6 Li8 141.22(3) . 5_445
Li4B Li6 Li8 103.95(3) 3 5_445
Li5B Li6 Li8 125.84(5) . 5_545
Si2 Li6 Li8 69.243(15) 5_445 5_545
Li10 Li6 Li8 95.688(19) 13 5_545
Si3 Li6 Li8 155.28(3) 1_455 5_545
Si3 Li6 Li8 64.608(11) . 5_545
Li4B Li6 Li8 103.95(3) . 5_545
Li4B Li6 Li8 141.22(3) 3 5_545
Li8 Li6 Li8 106.00(2) 5_445 5_545
Li5B Li6 Li5A 10.7(2) . .
Si2 Li6 Li5A 150.16(4) 5_445 .
Li10 Li6 Li5A 56.44(4) 13 .
Si3 Li6 Li5A 58.892(11) 1_455 .
Si3 Li6 Li5A 58.892(11) . .
Li4B Li6 Li5A 52.61(4) . .
Li4B Li6 Li5A 52.61(4) 3 .
Li8 Li6 Li5A 123.328(17) 5_445 .
Li8 Li6 Li5A 123.328(17) 5_545 .
Li5B Li6 Li1 95.71(16) . .
Si2 Li6 Li1 62.428(15) 5_445 .
Li10 Li6 Li1 125.987(11) 13 .
Si3 Li6 Li1 151.24(2) 1_455 .
Si3 Li6 Li1 62.755(10) . .
Li4B Li6 Li1 56.63(3) . .
Li4B Li6 Li1 89.28(3) 3 .
Li8 Li6 Li1 131.39(2) 5_445 .
Li8 Li6 Li1 52.282(15) 5_545 .
Li5A Li6 Li1 102.03(3) . .
Li5B Li6 Li1 95.71(16) . 1_455
Si2 Li6 Li1 62.428(15) 5_445 1_455
Li10 Li6 Li1 125.988(11) 13 1_455
Si3 Li6 Li1 62.755(10) 1_455 1_455
Si3 Li6 Li1 151.24(2) . 1_455
Li4B Li6 Li1 89.28(3) . 1_455
Li4B Li6 Li1 56.63(3) 3 1_455
Li8 Li6 Li1 52.282(15) 5_445 1_455
Li8 Li6 Li1 131.39(2) 5_545 1_455
Li5A Li6 Li1 102.03(3) . 1_455
Li1 Li6 Li1 105.687(18) . 1_455
Si3 Li7 Si1 168.68(3) 13 .
Si3 Li7 Li3 101.80(2) 13 .
Si1 Li7 Li3 66.877(17) . .
Si3 Li7 Li10 61.276(13) 13 .
Si1 Li7 Li10 112.620(16) . .
Li3 Li7 Li10 70.509(17) . .
Si3 Li7 Li10 61.276(13) 13 1_455
Si1 Li7 Li10 112.620(16) . 1_455
Li3 Li7 Li10 70.509(17) . 1_455
Li10 Li7 Li10 98.54(2) . 1_455
Si3 Li7 Li9 61.811(17) 13 13
Si1 Li7 Li9 129.51(2) . 13
Li3 Li7 Li9 163.61(3) . 13
Li10 Li7 Li9 99.319(17) . 13
Li10 Li7 Li9 99.319(17) 1_455 13
Si3 Li7 Li9 126.496(14) 13 1_455
Si1 Li7 Li9 58.331(13) . 1_455
Li3 Li7 Li9 99.699(18) . 1_455
Li10 Li7 Li9 169.40(2) . 1_455
Li10 Li7 Li9 81.394(12) 1_455 1_455
Li9 Li7 Li9 91.129(18) 13 1_455
Si3 Li7 Li9 126.496(14) 13 .
Si1 Li7 Li9 58.330(13) . .
Li3 Li7 Li9 99.699(18) . .
Li10 Li7 Li9 81.394(12) . .
Li10 Li7 Li9 169.40(2) 1_455 .
Li9 Li7 Li9 91.129(18) 13 .
Li9 Li7 Li9 96.71(2) 1_455 .
Si3 Li7 Li5A 133.06(4) 13 .
Si1 Li7 Li5A 58.26(3) . .
Li3 Li7 Li5A 125.14(4) . .
Li10 Li7 Li5A 130.584(13) . .
Li10 Li7 Li5A 130.584(13) 1_455 .
Li9 Li7 Li5A 71.25(4) 13 .
Li9 Li7 Li5A 51.491(15) 1_455 .
Li9 Li7 Li5A 51.491(15) . .
Si3 Li7 Li5A 55.89(3) 13 13_455
Si1 Li7 Li5A 129.03(3) . 13_455
Li3 Li7 Li5A 120.85(2) . 13_455
Li10 Li7 Li5A 117.16(3) . 13_455
Li10 Li7 Li5A 50.462(16) 1_455 13_455
Li9 Li7 Li5A 51.438(19) 13 13_455
Li9 Li7 Li5A 70.98(3) 1_455 13_455
Li9 Li7 Li5A 138.76(3) . 13_455
Li5A Li7 Li5A 94.92(4) . 13_455
Si3 Li7 Li5A 55.89(3) 13 13
Si1 Li7 Li5A 129.03(3) . 13
Li3 Li7 Li5A 120.85(2) . 13
Li10 Li7 Li5A 50.462(16) . 13
Li10 Li7 Li5A 117.16(3) 1_455 13
Li9 Li7 Li5A 51.438(19) 13 13
Li9 Li7 Li5A 138.76(3) 1_455 13
Li9 Li7 Li5A 70.98(3) . 13
Li5A Li7 Li5A 94.92(4) . 13
Li5A Li7 Li5A 92.30(5) 13_455 13
Si3 Li7 Li2 117.765(17) 13 .
Si1 Li7 Li2 55.821(12) . .
Li3 Li7 Li2 51.766(13) . .
Li10 Li7 Li2 56.883(14) . .
Li10 Li7 Li2 121.47(2) 1_455 .
Li9 Li7 Li2 133.750(10) 13 .
Li9 Li7 Li2 114.09(2) 1_455 .
Li9 Li7 Li2 49.815(15) . .
Li5A Li7 Li2 94.17(3) . .
Li5A Li7 Li2 170.80(3) 13_455 .
Li5A Li7 Li2 88.31(2) 13 .
Li1 Li8 Si3 173.91(3) 5_455 13
Li1 Li8 Li8 119.47(3) 5_455 9_565
Si3 Li8 Li8 66.62(2) 13 9_565
Li1 Li8 Li10 113.575(18) 5_455 1_455
Si3 Li8 Li10 64.007(14) 13 1_455
Li8 Li8 Li10 97.84(2) 9_565 1_455
Li1 Li8 Li10 113.575(18) 5_455 .
Si3 Li8 Li10 64.007(14) 13 .
Li8 Li8 Li10 97.84(2) 9_565 .
Li10 Li8 Li10 112.79(3) 1_455 .
Li1 Li8 Li3 72.04(2) 5_455 .
Si3 Li8 Li3 101.87(2) 13 .
Li8 Li8 Li3 168.49(4) 9_565 .
Li10 Li8 Li3 76.074(18) 1_455 .
Li10 Li8 Li3 76.074(18) . .
Li1 Li8 Li6 63.978(16) 5_455 5
Si3 Li8 Li6 118.682(16) 13 5
Li8 Li8 Li6 81.78(2) 9_565 5
Li10 Li8 Li6 176.59(2) 1_455 5
Li10 Li8 Li6 70.607(12) . 5
Li3 Li8 Li6 104.874(19) . 5
Li1 Li8 Li6 63.978(16) 5_455 5_455
Si3 Li8 Li6 118.682(16) 13 5_455
Li8 Li8 Li6 81.78(2) 9_565 5_455
Li10 Li8 Li6 70.607(12) 1_455 5_455
Li10 Li8 Li6 176.59(2) . 5_455
Li3 Li8 Li6 104.874(19) . 5_455
Li6 Li8 Li6 105.99(2) 5 5_455
Li1 Li8 Si3 63.204(19) 5_455 5_455
Si3 Li8 Si3 122.88(2) 13 5_455
Li8 Li8 Si3 56.26(2) 9_565 5_455
Li10 Li8 Si3 121.454(14) 1_455 5_455
Li10 Li8 Si3 121.454(14) . 5_455
Li3 Li8 Si3 135.25(2) . 5_455
Li6 Li8 Si3 55.560(12) 5 5_455
Li6 Li8 Si3 55.560(12) 5_455 5_455
Li1 Li8 Si2 59.698(13) 5_455 .
Si3 Li8 Si2 116.896(13) 13 .
Li8 Li8 Si2 130.790(12) 9_565 .
Li10 Li8 Si2 129.01(2) 1_455 .
Li10 Li8 Si2 54.413(12) . .
Li3 Li8 Si2 53.261(10) . .
Li6 Li8 Si2 52.377(11) 5 .
Li6 Li8 Si2 123.45(2) 5_455 .
Si3 Li8 Si2 100.828(13) 5_455 .
Li1 Li8 Si2 59.696(13) 5_455 1_455
Si3 Li8 Si2 116.897(13) 13 1_455
Li8 Li8 Si2 130.790(12) 9_565 1_455
Li10 Li8 Si2 54.414(12) 1_455 1_455
Li10 Li8 Si2 129.01(2) . 1_455
Li3 Li8 Si2 53.262(10) . 1_455
Li6 Li8 Si2 123.44(2) 5 1_455
Li6 Li8 Si2 52.376(11) 5_455 1_455
Si3 Li8 Si2 100.826(13) 5_455 1_455
Si2 Li8 Si2 93.317(16) . 1_455
Li1 Li8 Li7 125.31(3) 5_455 .
Si3 Li8 Li7 48.597(13) 13 .
Li8 Li8 Li7 115.22(3) 9_565 .
Li10 Li8 Li7 57.086(13) 1_455 .
Li10 Li8 Li7 57.086(13) . .
Li3 Li8 Li7 53.270(18) . .
Li6 Li8 Li7 126.143(12) 5 .
Li6 Li8 Li7 126.143(12) 5_455 .
Si3 Li8 Li7 171.48(2) 5_455 .
Si2 Li8 Li7 84.951(13) . .
Si2 Li8 Li7 84.953(13) 1_455 .
Li4A Li9 Li2 105.69(3) . .
Li4A Li9 Li5A 78.22(4) . 1_655
Li2 Li9 Li5A 121.956(18) . 1_655
Li4A Li9 Li5A 78.22(4) . .
Li2 Li9 Li5A 121.957(18) . .
Li5A Li9 Li5A 115.57(3) 1_655 .
Li4A Li9 Li5B 67.2(3) . .
Li2 Li9 Li5B 118.54(11) . .
Li5A Li9 Li5B 115.98(7) 1_655 .
Li5A Li9 Li5B 12.1(2) . .
Li4A Li9 Li5B 67.2(3) . 1_655
Li2 Li9 Li5B 118.54(11) . 1_655
Li5A Li9 Li5B 12.1(2) 1_655 1_655
Li5A Li9 Li5B 115.98(7) . 1_655
Li5B Li9 Li5B 113.59(19) . 1_655
Li4A Li9 Si1 78.918(19) . .
Li2 Li9 Si1 61.754(10) . .
Li5A Li9 Si1 156.86(5) 1_655 .
Li5A Li9 Si1 62.56(2) . .
Li5B Li9 Si1 56.94(13) . .
Li5B Li9 Si1 145.0(3) 1_655 .
Li4A Li9 Si1 78.92(2) . 1_655
Li2 Li9 Si1 61.754(11) . 1_655
Li5A Li9 Si1 62.56(2) 1_655 1_655
Li5A Li9 Si1 156.86(5) . 1_655
Li5B Li9 Si1 145.0(3) . 1_655
Li5B Li9 Si1 56.95(13) 1_655 1_655
Si1 Li9 Si1 109.321(19) . 1_655
Li4A Li9 Li4B 27.67(3) . .
Li2 Li9 Li4B 106.30(2) . .
Li5A Li9 Li4B 100.92(4) 1_655 .
Li5A Li9 Li4B 53.62(5) . .
Li5B Li9 Li4B 41.7(3) . .
Li5B Li9 Li4B 91.6(2) 1_655 .
Si1 Li9 Li4B 58.39(2) . .
Si1 Li9 Li4B 103.32(3) 1_655 .
Li4A Li9 Li4B 27.67(3) . 3_655
Li2 Li9 Li4B 106.30(2) . 3_655
Li5A Li9 Li4B 53.62(5) 1_655 3_655
Li5A Li9 Li4B 100.92(4) . 3_655
Li5B Li9 Li4B 91.6(2) . 3_655
Li5B Li9 Li4B 41.7(3) 1_655 3_655
Si1 Li9 Li4B 103.32(3) . 3_655
Si1 Li9 Li4B 58.39(2) 1_655 3_655
Li4B Li9 Li4B 55.09(5) . 3_655
Li4A Li9 Si3 57.40(3) . .
Li2 Li9 Si3 163.08(3) . .
Li5A Li9 Si3 58.343(16) 1_655 .
Li5A Li9 Si3 58.342(16) . .
Li5B Li9 Si3 57.66(7) . .
Li5B Li9 Si3 57.66(7) 1_655 .
Si1 Li9 Si3 110.855(14) . .
Si1 Li9 Si3 110.855(14) 1_655 .
Li4B Li9 Si3 59.12(2) . .
Li4B Li9 Si3 59.12(2) 3_655 .
Li4A Li9 Li9 50.64(3) . 10_556
Li2 Li9 Li9 55.045(16) . 10_556
Li5A Li9 Li9 104.55(4) 1_655 10_556
Li5A Li9 Li9 104.55(4) . 10_556
Li5B Li9 Li9 93.1(3) . 10_556
Li5B Li9 Li9 93.1(3) 1_655 10_556
Si1 Li9 Li9 57.064(10) . 10_556
Si1 Li9 Li9 57.063(10) 1_655 10_556
Li4B Li9 Li9 58.092(18) . 10_556
Li4B Li9 Li9 58.091(18) 3_655 10_556
Si3 Li9 Li9 108.037(12) . 10_556
Li5A Li10 Li6 64.82(4) 13 13
Li5A Li10 Si2 162.72(4) 13 .
Li6 Li10 Si2 132.46(2) 13 .
Li5A Li10 Li8 116.894(19) 13 1_655
Li6 Li10 Li8 84.483(18) 13 1_655
Si2 Li10 Li8 70.294(16) . 1_655
Li5A Li10 Li8 116.894(19) 13 .
Li6 Li10 Li8 84.483(18) 13 .
Si2 Li10 Li8 70.294(16) . .
Li8 Li10 Li8 112.79(3) 1_655 .
Li5A Li10 Si3 59.535(17) 13 13
Li6 Li10 Si3 58.257(10) 13 13
Si2 Li10 Si3 125.874(10) . 13
Li8 Li10 Si3 141.13(2) 1_655 13
Li8 Li10 Si3 57.409(12) . 13
Li5A Li10 Si3 59.535(17) 13 13_655
Li6 Li10 Si3 58.257(10) 13 13_655
Si2 Li10 Si3 125.874(9) . 13_655
Li8 Li10 Si3 57.409(12) 1_655 13_655
Li8 Li10 Si3 141.13(2) . 13_655
Si3 Li10 Si3 104.514(17) 13 13_655
Li5A Li10 Li5B 10.07(18) 13 13
Li6 Li10 Li5B 54.8(2) 13 13
Si2 Li10 Li5B 172.8(2) . 13
Li8 Li10 Li5B 112.93(9) 1_655 13
Li8 Li10 Li5B 112.93(9) . 13
Si3 Li10 Li5B 56.00(7) 13 13
Si3 Li10 Li5B 56.00(6) 13_655 13
Li5A Li10 Li2 104.90(4) 13 .
Li6 Li10 Li2 169.72(3) 13 .
Si2 Li10 Li2 57.823(15) . .
Li8 Li10 Li2 101.064(18) 1_655 .
Li8 Li10 Li2 101.065(18) . .
Si3 Li10 Li2 117.502(13) 13 .
Si3 Li10 Li2 117.502(13) 13_655 .
Li5B Li10 Li2 115.0(2) 13 .
Li5A Li10 Li7 67.78(3) 13 1_655
Li6 Li10 Li7 108.677(16) 13 1_655
Si2 Li10 Li7 101.723(16) . 1_655
Li8 Li10 Li7 73.109(14) 1_655 1_655
Li8 Li10 Li7 166.36(2) . 1_655
Si3 Li10 Li7 126.15(2) 13 1_655
Si3 Li10 Li7 52.507(10) 13_655 1_655
Li5B Li10 Li7 73.77(13) 13 1_655
Li2 Li10 Li7 65.381(15) . 1_655
Li5A Li10 Li7 67.78(3) 13 .
Li6 Li10 Li7 108.678(16) 13 .
Si2 Li10 Li7 101.723(16) . .
Li8 Li10 Li7 166.36(2) 1_655 .
Li8 Li10 Li7 73.111(14) . .
Si3 Li10 Li7 52.508(10) 13 .
Si3 Li10 Li7 126.15(2) 13_655 .
Li5B Li10 Li7 73.77(13) 13 .
Li2 Li10 Li7 65.380(15) . .
Li7 Li10 Li7 98.55(2) 1_655 .
Li5A Li10 Li6 145.10(4) 13 5
Li6 Li10 Li6 80.28(2) 13 5
Si2 Li10 Li6 52.185(14) . 5
Li8 Li10 Li6 56.395(13) 1_655 5
Li8 Li10 Li6 56.395(13) . 5
Si3 Li10 Li6 102.683(14) 13 5
Si3 Li10 Li6 102.683(14) 13_655 5
Li5B Li10 Li6 135.0(2) 13 5
Li2 Li10 Li6 110.01(2) . 5
Li7 Li10 Li6 127.906(14) 1_655 5
Li7 Li10 Li6 127.907(14) . 5
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Si1 Li5B 2.612(5) .
Si1 Li5B 2.612(5) 10_556
Si1 Li7 2.6152(5) .
Si1 Li7 2.6153(5) 10_556
Si1 Li4B 2.7451(11) .
Si1 Li4B 2.7451(11) 3
Si1 Li9 2.7733(3) 1_455
Si1 Li9 2.7733(3) 10_556
Si1 Li9 2.7733(3) 10_456
Si1 Li9 2.7733(3) .
Si1 Li2 2.7766(4) .
Si1 Li2 2.7766(4) 1_455
Si2 Li6 2.6348(5) 14_556
Si2 Li6 2.6348(5) 5
Si2 Li3 2.6364(4) 1_655
Si2 Li3 2.6364(4) .
Si2 Li10 2.6870(5) .
Si2 Li10 2.6870(5) 10_556
Si2 Li2 2.7388(7) .
Si2 Li1 2.8419(4) 5
Si2 Li1 2.8419(4) 5_455
Si2 Li8 3.1106(4) 10_656
Si2 Li8 3.1106(4) 1_655
Si2 Li8 3.1106(4) 10_556
Si3 Li4A 2.5781(6) .
Si3 Li7 2.5884(5) 13
Si3 Li8 2.6817(5) 13
Si3 Li6 2.7023(3) 1_655
Si3 Li6 2.7023(3) .
Si3 Li5B 2.710(2) 1_655
Si3 Li5B 2.710(2) .
Si3 Li5A 2.7263(4) .
Si3 Li5A 2.7263(4) 1_655
Si3 Li4B 2.8406(7) .
Si3 Li4B 2.8406(7) 3_655
Si3 Li10 2.8609(3) 13
Li1 Li8 2.4987(7) 5_545
Li1 Li8 2.4987(7) 14_546
Li1 Li4A 2.5177(17) .
Li1 Li4B 2.6735(13) 3_655
Li1 Li4B 2.6735(13) .
Li1 Li6 2.8385(3) 10_656
Li1 Li6 2.8385(3) 1_655
Li1 Li6 2.8385(3) 10_556
Li1 Li6 2.8385(3) .
Li1 Si2 2.8418(4) 5_445
Li1 Si2 2.8418(4) 5_545
Li1 Si3 2.8873(4) 10_556
Li2 Li9 2.6319(8) 10_556
Li2 Li9 2.6319(8) .
Li2 Li3 2.6526(5) .
Li2 Li3 2.6527(5) 1_655
Li2 Si1 2.7766(4) 1_655
Li2 Li10 2.9569(7) 10_556
Li2 Li10 2.9569(7) .
Li2 Li7 3.2094(4) .
Li2 Li7 3.2094(4) 10_656
Li2 Li7 3.2094(4) 10_556
Li3 Si2 2.6364(4) 1_455
Li3 Li2 2.6526(5) 1_455
Li3 Li8 2.7189(8) 10_556
Li3 Li8 2.7189(8) .
Li3 Li7 2.8116(7) 10_556
Li3 Li7 2.8116(7) .
Li3 Li1 3.0736(10) 5_455
Li3 Li10 3.3490(4) 10_556
Li3 Li10 3.3490(4) 1_455
Li4A Li9 2.3776(14) .
Li4A Li9 2.3776(14) 10_556
Li4A Si3 2.5781(6) 10_556
Li4A Li5A 3.1947(13) .
Li4A Li5A 3.1948(13) 10_656
Li4A Li5A 3.1948(13) 1_655
Li4A Li5A 3.1948(13) 10_556
Li5A Li10 2.6133(11) 13
Li5A Li9 2.6739(5) .
Li5A Li9 2.6739(5) 1_455
Li5A Si3 2.7263(4) 1_455
Li5A Li6 2.8382(12) .
Li5A Li7 3.1250(11) .
Li5A Li7 3.1370(13) 13_455
Li5A Li7 3.1370(13) 13
Li5A Li4A 3.1948(13) 1_455
Li4B Li4B 1.886(3) 3
Li4B Li5B 1.984(12) 10_556
Li4B Li5B 1.984(12) .
Li4B Li4B 2.639(3) 3_655
Li4B Li6 2.7970(11) 10_556
Li4B Li6 2.7971(11) .
Li4B Si3 2.8406(7) 10_556
Li4B Li9 2.8527(13) .
Li4B Li9 2.8527(13) 10_556
Li5B Li4B 1.985(12) 3
Li5B Li6 2.579(6) .
Li5B Li9 2.704(3) .
Li5B Li9 2.704(3) 1_455
Li5B Si3 2.710(2) 1_455
Li5B Li10 2.910(8) 13
Li5B Li5B 3.31(2) 10_556
Li5B Li7 3.394(8) .
Li6 Si2 2.6347(5) 5_445
Li6 Li10 2.6811(7) 13
Li6 Si3 2.7023(3) 1_455
Li6 Li4B 2.7971(11) 3
Li6 Li8 2.8328(4) 5_445
Li6 Li8 2.8328(4) 5_545
Li6 Li1 2.8386(3) 1_455
Li7 Si3 2.5885(5) 13
Li7 Li10 2.9853(5) .
Li7 Li10 2.9853(5) 1_455
Li7 Li9 3.0198(8) 13
Li7 Li9 3.0275(6) 1_455
Li7 Li9 3.0275(6) .
Li7 Li5A 3.1370(13) 13_455
Li7 Li5A 3.1370(13) 13
Li8 Li1 2.4987(7) 5_455
Li8 Si3 2.6817(5) 13
Li8 Li8 2.7081(12) 9_565
Li8 Li10 2.7163(4) 1_455
Li8 Li10 2.7163(4) .
Li8 Li6 2.8328(5) 5
Li8 Li6 2.8328(4) 5_455
Li8 Si3 2.9600(6) 5_455
Li8 Si2 3.1107(4) 1_455
Li9 Li5A 2.6739(5) 1_655
Li9 Li5B 2.704(3) 1_655
Li9 Si1 2.7733(3) 1_655
Li9 Li4B 2.8528(13) 3_655
Li9 Li9 3.0157(12) 10_556
Li10 Li5A 2.6134(11) 13
Li10 Li6 2.6811(7) 13
Li10 Li8 2.7163(4) 1_655
Li10 Si3 2.8609(3) 13
Li10 Si3 2.8609(3) 13_655
Li10 Li5B 2.910(8) 13
Li10 Li7 2.9852(5) 1_655
Li10 Li6 3.2083(7) 5
