#------------------------------------------------------------------------------
#$Date: 2016-03-21 01:21:50 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178377 $
#$URL: svn://www.crystallography.net/cod/cif/4/00/21/4002191.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4002191
loop_
_publ_author_name
'Rai, Binod K.'
'Oswald, Iain W. H.'
'Wang, Jiakui K.'
'McCandless, Gregory T.'
'Chan, Julia Y.'
'Morosan, E.'
_publ_section_title
;
 Superconductivity in Single Crystals of Lu3T4Ge13--x(T= Co, Rh, Os) and
 Y3T4Ge13--x(T= Ir, Rh, Os)
;
_journal_issue                   7
_journal_name_full               'Chemistry of Materials'
_journal_page_first              2488
_journal_paper_doi               10.1021/cm504658h
_journal_volume                  27
_journal_year                    2015
_chemical_formula_sum            'Ge12.53 Lu3 Os4'
_chemical_formula_weight         2195.26
_space_group_crystal_system      cubic
_space_group_IT_number           223
_space_group_name_Hall           '-P 4n 2 3'
_space_group_name_H-M_alt        'P m -3 n'
_symmetry_space_group_name_Hall  '-P 4n 2 3'
_symmetry_space_group_name_H-M   'P m -3 n'
_audit_creation_method           SHELXL-2014
_audit_update_record
;
2014-10-31 # Formatted by publCIF

;
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   8.9390(10)
_cell_length_b                   8.9390(10)
_cell_length_c                   8.9390(10)
_cell_measurement_reflns_used    1560
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      30.40
_cell_measurement_theta_min      3.22
_cell_volume                     714.28(14)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    CrystalMaker
_computing_publication_material  'publCIF (Westrip, 2010)'
_computing_structure_refinement  'SHELXL-2014 (Sheldrick, 2014)'
_computing_structure_solution    'SHELXS Direct Methods (Sheldrick, 2013)'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 1.000
_diffrn_measurement_device_type  'Bruker Kappa D8 Quest CMOS'
_diffrn_measurement_method       'φ scan'
_diffrn_radiation_monochromator  'HELIOS optics'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0469
_diffrn_reflns_av_unetI/netI     0.0267
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 1.000
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -12
_diffrn_reflns_limit_l_max       11
_diffrn_reflns_limit_l_min       -8
_diffrn_reflns_number            2427
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 1.000
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         30.397
_diffrn_reflns_theta_min         3.223
_diffrn_source                   'I\mS microfocus tube'
_exptl_absorpt_coefficient_mu    81.781
_exptl_absorpt_correction_T_max  0.7461
_exptl_absorpt_correction_T_min  0.3616
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS(2014)
_exptl_crystal_colour            Silver
_exptl_crystal_density_diffrn    10.207
_exptl_crystal_description       Fragment
_exptl_crystal_F_000             1836
_exptl_crystal_size_max          0.24
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.10
_refine_diff_density_max         7.749
_refine_diff_density_min         -5.090
_refine_diff_density_rms         0.710
_refine_ls_extinction_coef       0.0054(4)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.257
_refine_ls_hydrogen_treatment    undef
_refine_ls_matrix_type           full
_refine_ls_number_constraints    0
_refine_ls_number_parameters     17
_refine_ls_number_reflns         220
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.257
_refine_ls_R_factor_all          0.0347
_refine_ls_R_factor_gt           0.0333
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0127P)²+76.7919P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0784
_refine_ls_wR_factor_ref         0.0789
_reflns_Friedel_coverage         0.000
_reflns_number_gt                209
_reflns_number_total             220
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            Lu3Os4Ge13_CIF.cif
_cod_data_source_block           shelx
_cod_depositor_comments
'Adding full bibliography for 4002190--4002195.cif.'
_cod_original_cell_volume        714.3(2)
_cod_database_code               4002191
#BEGIN Tags that were not found in dictionaries:
_publcif_datablock.id            {8b01e77d-dca6-4488-a19e-27c3c9fd1c63}
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelxl_version_number           2014-3
#END Tags that were not found in dictionaries
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'z, x, y'
'z, -x, -y'
'-z, -x, y'
'-z, x, -y'
'y, z, x'
'-y, z, -x'
'y, -z, -x'
'-y, -z, x'
'y+1/2, x+1/2, -z+1/2'
'-y+1/2, -x+1/2, -z+1/2'
'y+1/2, -x+1/2, z+1/2'
'-y+1/2, x+1/2, z+1/2'
'x+1/2, z+1/2, -y+1/2'
'-x+1/2, z+1/2, y+1/2'
'-x+1/2, -z+1/2, -y+1/2'
'x+1/2, -z+1/2, y+1/2'
'z+1/2, y+1/2, -x+1/2'
'z+1/2, -y+1/2, x+1/2'
'-z+1/2, y+1/2, x+1/2'
'-z+1/2, -y+1/2, -x+1/2'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-z, -x, -y'
'-z, x, y'
'z, x, -y'
'z, -x, y'
'-y, -z, -x'
'y, -z, x'
'-y, z, x'
'y, z, -x'
'-y-1/2, -x-1/2, z-1/2'
'y-1/2, x-1/2, z-1/2'
'-y-1/2, x-1/2, -z-1/2'
'y-1/2, -x-1/2, -z-1/2'
'-x-1/2, -z-1/2, y-1/2'
'x-1/2, -z-1/2, -y-1/2'
'x-1/2, z-1/2, y-1/2'
'-x-1/2, z-1/2, -y-1/2'
'-z-1/2, -y-1/2, x-1/2'
'-z-1/2, y-1/2, -x-1/2'
'z-1/2, -y-1/2, -x-1/2'
'z-1/2, y-1/2, x-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
Lu1 Lu 0.2500 0.5000 0.0000 0.0079(4) Uani 1 8 d S T P
Os1 Os 0.2500 0.2500 0.2500 0.0048(3) Uani 1 6 d S T P
Ge1 Ge 0.0000 0.0000 0.0000 0.032(6) Uani 0.54(4) 24 d S T P
Ge2A Ge 0.0000 0.3075(16) 0.1465(14) 0.0230(18) Uani 0.89(6) 2 d S T P
Ge2B Ge 0.0000 0.346(9) 0.179(7) 0.0230(18) Uani 0.11(6) 2 d S T P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Lu Lu -0.4720 5.8584 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Os Os -1.2165 7.6030 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Ge2B Lu1 Ge2B 94.7(10) 37_665 34_565
Ge2B Lu1 Ge2B 147(3) 37_665 14
Ge2B Lu1 Ge2B 94.7(10) 34_565 14
Ge2B Lu1 Ge2B 94.7(10) 37_665 9
Ge2B Lu1 Ge2B 147(3) 34_565 9
Ge2B Lu1 Ge2B 94.7(10) 14 9
Ge2B Lu1 Ge2B 106.9(7) 37_665 .
Ge2B Lu1 Ge2B 129.6(4) 34_565 .
Ge2B Lu1 Ge2B 45(3) 14 .
Ge2B Lu1 Ge2B 77(3) 9 .
Ge2B Lu1 Ge2B 129.6(4) 37_665 17
Ge2B Lu1 Ge2B 45(3) 34_565 17
Ge2B Lu1 Ge2B 77(3) 14 17
Ge2B Lu1 Ge2B 106.9(7) 9 17
Ge2B Lu1 Ge2B 121.9(6) . 17
Ge2B Lu1 Ge2B 45(3) 37_665 26
Ge2B Lu1 Ge2B 129.6(4) 34_565 26
Ge2B Lu1 Ge2B 106.9(7) 14 26
Ge2B Lu1 Ge2B 77(3) 9 26
Ge2B Lu1 Ge2B 63(3) . 26
Ge2B Lu1 Ge2B 174(4) 17 26
Ge2B Lu1 Ge2B 77(3) 37_665 18_554
Ge2B Lu1 Ge2B 45(3) 34_565 18_554
Ge2B Lu1 Ge2B 129.6(4) 14 18_554
Ge2B Lu1 Ge2B 106.9(7) 9 18_554
Ge2B Lu1 Ge2B 174(4) . 18_554
Ge2B Lu1 Ge2B 53(3) 17 18_554
Ge2B Lu1 Ge2B 121.9(6) 26 18_554
Ge2B Lu1 Ge2B 45(3) 37_665 25_565
Ge2B Lu1 Ge2B 77(3) 34_565 25_565
Ge2B Lu1 Ge2B 106.9(7) 14 25_565
Ge2B Lu1 Ge2B 129.6(4) 9 25_565
Ge2B Lu1 Ge2B 86.8(10) . 25_565
Ge2B Lu1 Ge2B 121.9(6) 17 25_565
Ge2B Lu1 Ge2B 53(3) 26 25_565
Ge2B Lu1 Ge2B 93.5(11) 18_554 25_565
Ge2B Lu1 Ge2B 129.6(4) 37_665 42_666
Ge2B Lu1 Ge2B 106.9(7) 34_565 42_666
Ge2B Lu1 Ge2B 77(3) 14 42_666
Ge2B Lu1 Ge2B 45(3) 9 42_666
Ge2B Lu1 Ge2B 93.5(11) . 42_666
Ge2B Lu1 Ge2B 63(3) 17 42_666
Ge2B Lu1 Ge2B 121.9(6) 26 42_666
Ge2B Lu1 Ge2B 86.8(10) 18_554 42_666
Ge2B Lu1 Ge2B 174(4) 25_565 42_666
Ge2B Lu1 Ge2B 106.9(7) 37_665 2_565
Ge2B Lu1 Ge2B 77(3) 34_565 2_565
Ge2B Lu1 Ge2B 45(3) 14 2_565
Ge2B Lu1 Ge2B 129.6(4) 9 2_565
Ge2B Lu1 Ge2B 53(3) . 2_565
Ge2B Lu1 Ge2B 93.5(11) 17 2_565
Ge2B Lu1 Ge2B 86.8(10) 26 2_565
Ge2B Lu1 Ge2B 121.9(6) 18_554 2_565
Ge2B Lu1 Ge2B 63(3) 25_565 2_565
Ge2B Lu1 Ge2B 121.9(6) 42_666 2_565
Ge2B Lu1 Ge2B 77(3) 37_665 41_665
Ge2B Lu1 Ge2B 106.9(7) 34_565 41_665
Ge2B Lu1 Ge2B 129.6(4) 14 41_665
Ge2B Lu1 Ge2B 45(3) 9 41_665
Ge2B Lu1 Ge2B 121.9(6) . 41_665
Ge2B Lu1 Ge2B 86.8(10) 17 41_665
Ge2B Lu1 Ge2B 93.5(11) 26 41_665
Ge2B Lu1 Ge2B 63(3) 18_554 41_665
Ge2B Lu1 Ge2B 121.9(6) 25_565 41_665
Ge2B Lu1 Ge2B 53(3) 42_666 41_665
Ge2B Lu1 Ge2B 174(4) 2_565 41_665
Ge2A Os1 Ge2A 136.0(5) . 45_666
Ge2A Os1 Ge2A 131.42(18) . 42_666
Ge2A Os1 Ge2A 85.8(6) 45_666 42_666
Ge2A Os1 Ge2A 85.8(6) . 9
Ge2A Os1 Ge2A 131.41(18) 45_666 9
Ge2A Os1 Ge2A 76.4(8) 42_666 9
Ge2A Os1 Ge2A 76.4(8) . 14
Ge2A Os1 Ge2A 85.8(6) 45_666 14
Ge2A Os1 Ge2A 85.8(6) 42_666 14
Ge2A Os1 Ge2A 136.0(5) 9 14
Ge2A Os1 Ge2A 85.8(6) . 5
Ge2A Os1 Ge2A 76.4(8) 45_666 5
Ge2A Os1 Ge2A 136.0(5) 42_666 5
Ge2A Os1 Ge2A 85.8(6) 9 5
Ge2A Os1 Ge2A 131.41(18) 14 5
Ge2A Os1 Ge2B 129.9(16) . 45_666
Ge2A Os1 Ge2B 10.4(18) 45_666 45_666
Ge2A Os1 Ge2B 95(2) 42_666 45_666
Ge2A Os1 Ge2B 129.3(9) 9 45_666
Ge2A Os1 Ge2B 91.6(17) 14 45_666
Ge2A Os1 Ge2B 66(3) 5 45_666
Ge2A Os1 Ge2B 129.3(9) . 42_666
Ge2A Os1 Ge2B 91.6(17) 45_666 42_666
Ge2A Os1 Ge2B 10.4(18) 42_666 42_666
Ge2A Os1 Ge2B 66(3) 9 42_666
Ge2A Os1 Ge2B 95(2) 14 42_666
Ge2A Os1 Ge2B 129.9(16) 5 42_666
Ge2B Os1 Ge2B 100(3) 45_666 42_666
Ge2A Os1 Ge2B 91.6(17) . 9
Ge2A Os1 Ge2B 129.3(9) 45_666 9
Ge2A Os1 Ge2B 66(3) 42_666 9
Ge2A Os1 Ge2B 10.4(18) 9 9
Ge2A Os1 Ge2B 129.9(16) 14 9
Ge2A Os1 Ge2B 95(2) 5 9
Ge2B Os1 Ge2B 129.7(15) 45_666 9
Ge2B Os1 Ge2B 56(4) 42_666 9
Ge2A Os1 Ge2B 95(2) . 5
Ge2A Os1 Ge2B 66(3) 45_666 5
Ge2A Os1 Ge2B 129.9(16) 42_666 5
Ge2A Os1 Ge2B 91.6(17) 9 5
Ge2A Os1 Ge2B 129.3(9) 14 5
Ge2A Os1 Ge2B 10.4(18) 5 5
Ge2B Os1 Ge2B 56(4) 45_666 5
Ge2B Os1 Ge2B 126(2) 42_666 5
Ge2B Os1 Ge2B 100(3) 9 5
Ge2A Os1 Ge2B 66(3) . 14
Ge2A Os1 Ge2B 95(2) 45_666 14
Ge2A Os1 Ge2B 91.6(17) 42_666 14
Ge2A Os1 Ge2B 129.9(16) 9 14
Ge2A Os1 Ge2B 10.4(18) 14 14
Ge2A Os1 Ge2B 129.3(9) 5 14
Ge2B Os1 Ge2B 100(3) 45_666 14
Ge2B Os1 Ge2B 100(3) 42_666 14
Ge2B Os1 Ge2B 126(2) 9 14
Ge2B Os1 Ge2B 129.7(15) 5 14
Ge2A Os1 Ge2B 10.4(18) . .
Ge2A Os1 Ge2B 129.9(16) 45_666 .
Ge2A Os1 Ge2B 129.3(9) 42_666 .
Ge2A Os1 Ge2B 95(2) 9 .
Ge2A Os1 Ge2B 66(3) 14 .
Ge2A Os1 Ge2B 91.6(17) 5 .
Ge2B Os1 Ge2B 126(2) 45_666 .
Ge2B Os1 Ge2B 129.7(15) 42_666 .
Ge2B Os1 Ge2B 100(3) 9 .
Ge2B Os1 Ge2B 100(3) 5 .
Ge2B Os1 Ge2B 56(4) 14 .
Os1 Ge2A Os1 129.3(2) . 28
Os1 Ge2A Ge2A 112.0(3) . 26
Os1 Ge2A Ge2A 112.0(3) 28 26
Os1 Ge2A Ge2B 57.0(15) . 14
Os1 Ge2A Ge2B 112.2(8) 28 14
Ge2A Ge2A Ge2B 125.2(8) 26 14
Os1 Ge2A Ge2B 112.2(8) . 13_455
Os1 Ge2A Ge2B 57.0(15) 28 13_455
Ge2A Ge2A Ge2B 125.2(8) 26 13_455
Ge2B Ge2A Ge2B 61(2) 14 13_455
Os1 Ge2A Ge2B 113.30(15) . 26
Os1 Ge2A Ge2B 113.30(15) 28 26
Ge2A Ge2A Ge2B 6.7(12) 26 26
Ge2B Ge2A Ge2B 119.9(15) 14 26
Ge2B Ge2A Ge2B 119.9(15) 13_455 26
Os1 Ge2A Lu1 67.85(7) . .
Os1 Ge2A Lu1 157.2(4) 28 .
Ge2A Ge2A Lu1 65.1(3) 26 .
Ge2B Ge2A Lu1 61.5(7) 14 .
Ge2B Ge2A Lu1 104.9(10) 13_455 .
Ge2B Ge2A Lu1 61.1(9) 26 .
Os1 Ge2A Lu1 157.2(4) . 25_565
Os1 Ge2A Lu1 67.85(7) 28 25_565
Ge2A Ge2A Lu1 65.1(3) 26 25_565
Ge2B Ge2A Lu1 104.9(10) 14 25_565
Ge2B Ge2A Lu1 61.5(7) 13_455 25_565
Ge2B Ge2A Lu1 61.1(9) 26 25_565
Lu1 Ge2A Lu1 91.87(14) . 25_565
Os1 Ge2A Lu1 66.26(19) . 5
Os1 Ge2A Lu1 66.26(19) 28 5
Ge2A Ge2A Lu1 170.8(3) 26 5
Ge2B Ge2A Lu1 62.1(10) 14 5
Ge2B Ge2A Lu1 62.1(10) 13_455 5
Ge2B Ge2A Lu1 177.4(10) 26 5
Lu1 Ge2A Lu1 120.3(4) . 5
Lu1 Ge2A Lu1 120.3(4) 25_565 5
Ge2B Ge2B Ge2B 72.8(18) 14 13_455
Ge2B Ge2B Os1 127(3) 14 28
Ge2B Ge2B Os1 62(2) 13_455 28
Ge2B Ge2B Os1 62(2) 14 .
Ge2B Ge2B Os1 127(3) 13_455 .
Os1 Ge2B Os1 129.1(18) 28 .
Ge2B Ge2B Ge2A 5.7(13) 14 14
Ge2B Ge2B Ge2A 76.2(19) 13_455 14
Os1 Ge2B Ge2A 127(3) 28 14
Os1 Ge2B Ge2A 56.9(11) . 14
Ge2B Ge2B Ge2A 76.2(19) 14 13_455
Ge2B Ge2B Ge2A 5.7(13) 13_455 13_455
Os1 Ge2B Ge2A 56.9(11) 28 13_455
Os1 Ge2B Ge2A 127(3) . 13_455
Ge2A Ge2B Ge2A 79(2) 14 13_455
Ge2B Ge2B Ge2B 53.6(9) 14 2_565
Ge2B Ge2B Ge2B 53.6(9) 13_455 2_565
Os1 Ge2B Ge2B 110.2(18) 28 2_565
Os1 Ge2B Ge2B 110.2(18) . 2_565
Ge2A Ge2B Ge2B 59.3(10) 14 2_565
Ge2A Ge2B Ge2B 59.3(10) 13_455 2_565
Ge2B Ge2B Ge2A 127.6(19) 14 26
Ge2B Ge2B Ge2A 127.6(19) 13_455 26
Os1 Ge2B Ge2A 102(2) 28 26
Os1 Ge2B Ge2A 102(2) . 26
Ge2A Ge2B Ge2A 129.2(9) 14 26
Ge2A Ge2B Ge2A 129.2(9) 13_455 26
Ge2B Ge2B Ge2A 96.7(12) 2_565 26
Ge2B Ge2B Lu1 69(3) 14 5
Ge2B Ge2B Lu1 69(3) 13_455 5
Os1 Ge2B Lu1 69.9(9) 28 5
Os1 Ge2B Lu1 69.9(9) . 5
Ge2A Ge2B Lu1 66.0(16) 14 5
Ge2A Ge2B Lu1 66.0(16) 13_455 5
Ge2B Ge2B Lu1 106.6(17) 2_565 5
Ge2A Ge2B Lu1 157(3) 26 5
Ge2B Ge2B Lu1 116.6(15) 14 25_565
Ge2B Ge2B Lu1 65.6(14) 13_455 25_565
Os1 Ge2B Lu1 68.4(3) 28 25_565
Os1 Ge2B Lu1 160.7(15) . 25_565
Ge2A Ge2B Lu1 122(3) 14 25_565
Ge2A Ge2B Lu1 66.9(9) 13_455 25_565
Ge2B Ge2B Lu1 63.3(16) 2_565 25_565
Ge2A Ge2B Lu1 62.3(10) 26 25_565
Lu1 Ge2B Lu1 128.8(15) 5 25_565
Ge2B Ge2B Lu1 65.6(14) 14 .
Ge2B Ge2B Lu1 116.6(15) 13_455 .
Os1 Ge2B Lu1 160.7(15) 28 .
Os1 Ge2B Lu1 68.4(3) . .
Ge2A Ge2B Lu1 66.9(9) 14 .
Ge2A Ge2B Lu1 122(3) 13_455 .
Ge2B Ge2B Lu1 63.3(16) 2_565 .
Ge2A Ge2B Lu1 62.3(10) 26 .
Lu1 Ge2B Lu1 128.8(15) 5 .
Lu1 Ge2B Lu1 93.2(9) 25_565 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Lu1 Ge2B 2.99(5) 37_665
Lu1 Ge2B 2.99(5) 34_565
Lu1 Ge2B 2.99(5) 14
Lu1 Ge2B 2.99(5) 9
Lu1 Ge2B 3.08(2) .
Lu1 Ge2B 3.08(2) 17
Lu1 Ge2B 3.08(2) 26
Lu1 Ge2B 3.08(2) 18_554
Lu1 Ge2B 3.08(2) 25_565
Lu1 Ge2B 3.08(2) 42_666
Lu1 Ge2B 3.08(2) 2_565
Lu1 Ge2B 3.08(2) 41_665
Os1 Ge2A 2.472(2) .
Os1 Ge2A 2.472(2) 45_666
Os1 Ge2A 2.472(2) 42_666
Os1 Ge2A 2.472(2) 9
Os1 Ge2A 2.472(2) 14
Os1 Ge2A 2.472(2) 5
Os1 Ge2B 2.475(18) 45_666
Os1 Ge2B 2.475(18) 42_666
Os1 Ge2B 2.475(18) 9
Os1 Ge2B 2.475(18) 5
Os1 Ge2B 2.475(18) 14
Os1 Ge2B 2.475(18) .
Ge2A Os1 2.472(2) 28
Ge2A Ge2A 2.62(2) 26
Ge2A Ge2B 2.70(9) 14
Ge2A Ge2B 2.70(9) 13_455
Ge2A Ge2B 2.93(8) 26
Ge2A Lu1 3.110(4) 25_565
Ge2A Lu1 3.201(10) 5
Ge2B Ge2B 2.33(15) 14
Ge2B Ge2B 2.33(15) 13_455
Ge2B Os1 2.475(18) 28
Ge2B Ge2A 2.70(9) 14
Ge2B Ge2A 2.70(9) 13_455
Ge2B Ge2B 2.76(16) 2_565
Ge2B Ge2A 2.93(8) 26
Ge2B Lu1 2.99(5) 5
Ge2B Lu1 3.08(2) 25_565
#BEGIN Loops that were not found in dictionaries:
loop_
_publcif_info_datablock.id
_publcif_info_datablock.publ_exptl
_publcif_info_datablock.publ_geom
_publcif_info_datablock.structure
{8b01e77d-dca6-4488-a19e-27c3c9fd1c63} y y y
#END Loops that were not found in dictionaries
