#------------------------------------------------------------------------------
#$Date: 2020-01-28 01:19:45 +0200 (Tue, 28 Jan 2020) $
#$Revision: 247263 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/00/34/4003468.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4003468
loop_
_publ_author_name
'Solokha, Pavlo'
'Eremin, Roman A.'
'Leisegang, Tilmann'
'Proserpio, Davide M.'
'Akhmetshina, Tatiana'
'Gurskaya, Albina'
'Saccone, Adriana'
'De Negri, Serena'
_publ_section_title
;
 New Quasicrystal Approximant in the Sc--Pd System: From Topological Data
 Mining to the Bench
;
_journal_name_full               'Chemistry of Materials'
_journal_paper_doi               10.1021/acs.chemmater.9b03767
_journal_year                    2020
_chemical_formula_moiety         'Pd15.54 Sc37.40, 18(Sc)'
_chemical_formula_sum            'Pd15.54 Sc54.4'
_chemical_formula_weight         4113.76
_space_group_crystal_system      orthorhombic
_space_group_IT_number           71
_space_group_name_Hall           '-I 2 2'
_space_group_name_H-M_alt        'I m m m'
_audit_creation_method           SHELXL-2014/7
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_formula_units_Z            2
_cell_length_a                   14.252(3)
_cell_length_b                   14.372(3)
_cell_length_c                   14.776(3)
_cell_measurement_reflns_used    2017
_cell_measurement_temperature    295(2)
_cell_measurement_theta_max      31.751
_cell_measurement_theta_min      1.977
_cell_volume                     3026.6(11)
_computing_structure_refinement  'SHELXL-2014/7 (Sheldrick, 2014)'
_diffrn_ambient_temperature      295(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.978
_diffrn_measurement_device_type  'Bruker APEXII'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1067
_diffrn_reflns_av_unetI/netI     0.0534
_diffrn_reflns_Laue_measured_fraction_full 1.000
_diffrn_reflns_Laue_measured_fraction_max 0.978
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            35879
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.978
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         31.751
_diffrn_reflns_theta_min         1.977
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    10.094
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Bruker SADABS'
_exptl_crystal_colour            'metallic luster'
_exptl_crystal_density_diffrn    4.514
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       'irregularly shaped'
_exptl_crystal_F_000             3732
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.03
_exptl_transmission_factor_max   0.7463
_exptl_transmission_factor_min   0.6194
_refine_diff_density_max         1.319
_refine_diff_density_min         -1.502
_refine_diff_density_rms         0.311
_refine_ls_goodness_of_fit_ref   1.056
_refine_ls_matrix_type           full
_refine_ls_number_parameters     126
_refine_ls_number_reflns         2787
_refine_ls_number_restraints     25
_refine_ls_restrained_S_all      1.051
_refine_ls_R_factor_all          0.0672
_refine_ls_R_factor_gt           0.0374
_refine_ls_shift/su_max          0.033
_refine_ls_shift/su_mean         0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0256P)²+11.6967P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0689
_refine_ls_wR_factor_ref         0.0766
_reflns_Friedel_coverage         0.000
_reflns_number_gt                2017
_reflns_number_total             2787
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            cm9b03767_si_005.cif
_cod_data_source_block           shelx_CSD-1874074
_cod_original_cell_volume        3026.7(10)
_cod_original_formula_sum        'Pd15.54 Sc54.40'
_cod_database_code               4003468
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, -y, z'
'-x, y, -z'
'x, -y, -z'
'x+1/2, y+1/2, z+1/2'
'-x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, -z+1/2'
'-x, -y, -z'
'x, y, -z'
'x, -y, z'
'-x, y, z'
'-x+1/2, -y+1/2, -z+1/2'
'x+1/2, y+1/2, -z+1/2'
'x+1/2, -y+1/2, z+1/2'
'-x+1/2, y+1/2, z+1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pd1 Pd 0.0000 0.0000 0.0000 0.0095(2) Uani 1 8 d S T P A .
Pd2 Pd 0.33557(4) 0.20615(4) 0.0000 0.01300(13) Uani 1 2 d S T P A .
Pd3 Pd 0.0000 0.33396(4) 0.20949(4) 0.01288(12) Uani 1 2 d S T P A .
Pd4 Pd 0.20304(4) 0.0000 0.33180(4) 0.01283(12) Uani 1 2 d S T P A .
Pd5 Pd 0.5000 0.0000 0.16162(5) 0.01491(17) Uani 1 4 d S T P A .
Sc1 Sc 0.17875(9) 0.10949(9) 0.0000 0.0097(3) Uani 1 2 d S T P A .
Sc2 Sc 0.0000 0.0000 0.35401(12) 0.0100(4) Uani 1 4 d S T P A .
Sc3 Sc 0.38047(13) 0.0000 0.0000 0.0098(4) Uani 1 4 d S T P A .
Sc4 Sc 0.0000 0.18179(9) 0.10582(9) 0.0104(3) Uani 1 2 d S T P A .
Sc5 Sc 0.10997(9) 0.0000 0.16787(9) 0.0091(3) Uani 1 2 d S T P A .
Sc6 Sc 0.11689(6) 0.17771(6) 0.28750(6) 0.01035(19) Uani 1 1 d . . . . .
Sc7 Sc 0.0000 0.32428(10) 0.39604(9) 0.0123(3) Uani 1 2 d S T P A .
Sc8 Sc 0.0000 0.37977(14) 0.0000 0.0109(4) Uani 1 4 d S T P A .
Sc9A Sc 0.392(3) 0.376(2) 0.0000 0.016(7) Uani 0.43(3) 2 d S TU P A 1
Sc9B Sc 0.363(2) 0.3936(17) 0.0000 0.016(3) Uani 0.30(3) 2 d S TU P A 2
Sc9C Sc 0.412(5) 0.370(5) 0.0000 0.016(7) Uani 0.26(3) 2 d S TU P A 3
Sc10 Sc 0.18680(6) 0.30126(7) 0.11099(6) 0.01095(19) Uani 1 1 d . . . . .
Sc11 Sc 0.30213(7) 0.11464(6) 0.17807(6) 0.01044(18) Uani 1 1 d . . . . .
Sc12 Sc 0.39734(10) 0.0000 0.33106(10) 0.0170(3) Uani 1 2 d S T P A .
Sc13 Sc 0.1817(11) 0.5000 0.0000 0.0143(17) Uani 0.72(5) 4 d S TU . A .
Pd23 Pd 0.2257(17) 0.5000 0.0000 0.027(3) Uani 0.27(2) 4 d S TU . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Sc Sc 0.2519 0.3716 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Sc5 Pd1 Sc5 64.58(5) 9 10
Sc5 Pd1 Sc5 115.42(5) 9 2
Sc5 Pd1 Sc5 180.00(5) 10 2
Sc5 Pd1 Sc5 180.0 9 .
Sc5 Pd1 Sc5 115.42(5) 10 .
Sc5 Pd1 Sc5 64.58(5) 2 .
Sc5 Pd1 Sc1 117.03(2) 9 .
Sc5 Pd1 Sc1 62.97(2) 10 .
Sc5 Pd1 Sc1 117.03(2) 2 .
Sc5 Pd1 Sc1 62.97(2) . .
Sc5 Pd1 Sc1 62.97(2) 9 9
Sc5 Pd1 Sc1 117.03(2) 10 9
Sc5 Pd1 Sc1 62.97(2) 2 9
Sc5 Pd1 Sc1 117.03(2) . 9
Sc1 Pd1 Sc1 180.00(4) . 9
Sc5 Pd1 Sc1 117.03(2) 9 11
Sc5 Pd1 Sc1 62.97(2) 10 11
Sc5 Pd1 Sc1 117.03(2) 2 11
Sc5 Pd1 Sc1 62.97(2) . 11
Sc1 Pd1 Sc1 63.41(5) . 11
Sc1 Pd1 Sc1 116.59(5) 9 11
Sc5 Pd1 Sc1 62.97(2) 9 3
Sc5 Pd1 Sc1 117.03(2) 10 3
Sc5 Pd1 Sc1 62.97(2) 2 3
Sc5 Pd1 Sc1 117.03(2) . 3
Sc1 Pd1 Sc1 116.59(5) . 3
Sc1 Pd1 Sc1 63.41(5) 9 3
Sc1 Pd1 Sc1 180.00(5) 11 3
Sc5 Pd1 Sc4 115.73(2) 9 .
Sc5 Pd1 Sc4 115.73(2) 10 .
Sc5 Pd1 Sc4 64.27(2) 2 .
Sc5 Pd1 Sc4 64.27(2) . .
Sc1 Pd1 Sc4 63.20(2) . .
Sc1 Pd1 Sc4 116.80(2) 9 .
Sc1 Pd1 Sc4 116.80(2) 11 .
Sc1 Pd1 Sc4 63.20(2) 3 .
Sc5 Pd1 Sc4 64.27(2) 9 9
Sc5 Pd1 Sc4 64.27(2) 10 9
Sc5 Pd1 Sc4 115.73(2) 2 9
Sc5 Pd1 Sc4 115.73(2) . 9
Sc1 Pd1 Sc4 116.80(2) . 9
Sc1 Pd1 Sc4 63.20(2) 9 9
Sc1 Pd1 Sc4 63.20(2) 11 9
Sc1 Pd1 Sc4 116.80(2) 3 9
Sc4 Pd1 Sc4 180.0 . 9
Sc5 Pd1 Sc4 64.27(2) 9 10
Sc5 Pd1 Sc4 64.27(2) 10 10
Sc5 Pd1 Sc4 115.73(2) 2 10
Sc5 Pd1 Sc4 115.73(2) . 10
Sc1 Pd1 Sc4 63.20(2) . 10
Sc1 Pd1 Sc4 116.80(2) 9 10
Sc1 Pd1 Sc4 116.80(2) 11 10
Sc1 Pd1 Sc4 63.20(2) 3 10
Sc4 Pd1 Sc4 61.80(5) . 10
Sc4 Pd1 Sc4 118.20(5) 9 10
Sc5 Pd1 Sc4 115.73(2) 9 2
Sc5 Pd1 Sc4 115.73(2) 10 2
Sc5 Pd1 Sc4 64.27(2) 2 2
Sc5 Pd1 Sc4 64.27(2) . 2
Sc1 Pd1 Sc4 116.80(2) . 2
Sc1 Pd1 Sc4 63.20(2) 9 2
Sc1 Pd1 Sc4 63.20(2) 11 2
Sc1 Pd1 Sc4 116.80(2) 3 2
Sc4 Pd1 Sc4 118.20(5) . 2
Sc4 Pd1 Sc4 61.80(5) 9 2
Sc4 Pd1 Sc4 180.00(5) 10 2
Sc9A Pd2 Sc1 140.0(9) . .
Sc9C Pd2 Sc1 146.6(15) . .
Sc1 Pd2 Sc9B 130.2(6) . .
Sc9A Pd2 Sc7 83.6(7) . 13
Sc9C Pd2 Sc7 78.1(13) . 13
Sc1 Pd2 Sc7 128.35(4) . 13
Sc9B Pd2 Sc7 91.9(5) . 13
Sc9A Pd2 Sc7 83.6(7) . 6_554
Sc9C Pd2 Sc7 78.1(13) . 6_554
Sc1 Pd2 Sc7 128.35(4) . 6_554
Sc9B Pd2 Sc7 91.9(5) . 6_554
Sc7 Pd2 Sc7 65.59(5) 13 6_554
Sc9A Pd2 Sc11 117.99(3) . .
Sc9C Pd2 Sc11 117.89(7) . .
Sc1 Pd2 Sc11 68.36(2) . .
Sc9B Pd2 Sc11 117.38(7) . .
Sc7 Pd2 Sc11 65.53(3) 13 .
Sc7 Pd2 Sc11 122.84(4) 6_554 .
Sc9A Pd2 Sc11 117.98(3) . 10
Sc9C Pd2 Sc11 117.89(7) . 10
Sc1 Pd2 Sc11 68.36(2) . 10
Sc9B Pd2 Sc11 117.38(7) . 10
Sc7 Pd2 Sc11 122.84(4) 13 10
Sc7 Pd2 Sc11 65.53(3) 6_554 10
Sc11 Pd2 Sc11 124.00(4) . 10
Sc9A Pd2 Sc10 77.8(7) . .
Sc9C Pd2 Sc10 83.3(13) . .
Sc1 Pd2 Sc10 68.98(3) . .
Sc9B Pd2 Sc10 69.7(5) . .
Sc7 Pd2 Sc10 110.92(3) 13 .
Sc7 Pd2 Sc10 161.36(4) 6_554 .
Sc11 Pd2 Sc10 66.83(3) . .
Sc11 Pd2 Sc10 124.68(3) 10 .
Sc9A Pd2 Sc10 77.8(7) . 10
Sc9C Pd2 Sc10 83.3(13) . 10
Sc1 Pd2 Sc10 68.98(3) . 10
Sc9B Pd2 Sc10 69.7(5) . 10
Sc7 Pd2 Sc10 161.37(4) 13 10
Sc7 Pd2 Sc10 110.92(3) 6_554 10
Sc11 Pd2 Sc10 124.68(3) . 10
Sc11 Pd2 Sc10 66.83(3) 10 10
Sc10 Pd2 Sc10 66.05(4) . 10
Sc9A Pd2 Sc3 149.6(9) . .
Sc9C Pd2 Sc3 143.0(15) . .
Sc1 Pd2 Sc3 70.32(5) . .
Sc9B Pd2 Sc3 159.5(6) . .
Sc7 Pd2 Sc3 71.02(4) 13 .
Sc7 Pd2 Sc3 71.02(4) 6_554 .
Sc11 Pd2 Sc3 66.57(2) . .
Sc11 Pd2 Sc3 66.57(2) 10 .
Sc10 Pd2 Sc3 126.36(3) . .
Sc10 Pd2 Sc3 126.36(3) 10 .
Sc4 Pd3 Sc7 122.12(5) . .
Sc4 Pd3 Sc12 124.24(4) . 13
Sc7 Pd3 Sc12 104.54(4) . 13
Sc4 Pd3 Sc12 124.24(4) . 14_455
Sc7 Pd3 Sc12 104.54(4) . 14_455
Sc12 Pd3 Sc12 61.48(5) 13 14_455
Sc4 Pd3 Sc6 67.07(3) . .
Sc7 Pd3 Sc6 65.29(3) . .
Sc12 Pd3 Sc6 114.66(3) 13 .
Sc12 Pd3 Sc6 168.61(4) 14_455 .
Sc4 Pd3 Sc6 67.07(3) . 12
Sc7 Pd3 Sc6 65.29(3) . 12
Sc12 Pd3 Sc6 168.61(4) 13 12
Sc12 Pd3 Sc6 114.66(3) 14_455 12
Sc6 Pd3 Sc6 66.85(4) . 12
Sc4 Pd3 Pd5 176.42(4) . 13
Sc7 Pd3 Pd5 54.30(3) . 13
Sc12 Pd3 Pd5 58.60(3) 13 13
Sc12 Pd3 Pd5 58.60(3) 14_455 13
Sc6 Pd3 Pd5 110.04(3) . 13
Sc6 Pd3 Pd5 110.04(3) 12 13
Sc4 Pd3 Sc10 66.59(2) . 12
Sc7 Pd3 Sc10 117.76(2) . 12
Sc12 Pd3 Sc10 118.13(4) 13 12
Sc12 Pd3 Sc10 65.49(3) 14_455 12
Sc6 Pd3 Sc10 123.00(3) . 12
Sc6 Pd3 Sc10 65.76(3) 12 12
Pd5 Pd3 Sc10 114.54(2) 13 12
Sc4 Pd3 Sc10 66.59(2) . .
Sc7 Pd3 Sc10 117.76(2) . .
Sc12 Pd3 Sc10 65.49(3) 13 .
Sc12 Pd3 Sc10 118.13(4) 14_455 .
Sc6 Pd3 Sc10 65.76(3) . .
Sc6 Pd3 Sc10 123.00(3) 12 .
Pd5 Pd3 Sc10 114.54(2) 13 .
Sc10 Pd3 Sc10 120.25(4) 12 .
Sc4 Pd3 Sc8 67.00(5) . .
Sc7 Pd3 Sc8 170.88(5) . .
Sc12 Pd3 Sc8 67.78(4) 13 .
Sc12 Pd3 Sc8 67.78(4) 14_455 .
Sc6 Pd3 Sc8 121.82(3) . .
Sc6 Pd3 Sc8 121.82(3) 12 .
Pd5 Pd3 Sc8 116.58(4) 13 .
Sc10 Pd3 Sc8 64.42(2) 12 .
Sc10 Pd3 Sc8 64.42(2) . .
Sc4 Pd3 Sc11 117.67(2) . 13
Sc7 Pd3 Sc11 61.09(2) . 13
Sc12 Pd3 Sc11 59.37(3) 13 13
Sc12 Pd3 Sc11 110.47(3) 14_455 13
Sc6 Pd3 Sc11 60.78(3) . 13
Sc6 Pd3 Sc11 115.96(3) 12 13
Pd5 Pd3 Sc11 61.254(19) 13 13
Sc10 Pd3 Sc11 175.69(3) 12 13
Sc10 Pd3 Sc11 62.59(3) . 13
Sc8 Pd3 Sc11 116.01(2) . 13
Sc4 Pd3 Sc11 117.67(2) . 8_455
Sc7 Pd3 Sc11 61.09(2) . 8_455
Sc12 Pd3 Sc11 110.47(3) 13 8_455
Sc12 Pd3 Sc11 59.37(3) 14_455 8_455
Sc6 Pd3 Sc11 115.96(3) . 8_455
Sc6 Pd3 Sc11 60.78(3) 12 8_455
Pd5 Pd3 Sc11 61.254(19) 13 8_455
Sc10 Pd3 Sc11 62.59(3) 12 8_455
Sc10 Pd3 Sc11 175.69(3) . 8_455
Sc8 Pd3 Sc11 116.01(2) . 8_455
Sc11 Pd3 Sc11 114.38(4) 13 8_455
Pd23 Pd4 Sc5 173.5(5) 13 .
Pd23 Pd4 Sc12 68.0(5) 13 .
Sc5 Pd4 Sc12 118.48(5) . .
Pd23 Pd4 Sc6 111.59(16) 13 11
Sc5 Pd4 Sc6 66.41(2) . 11
Sc12 Pd4 Sc6 114.91(2) . 11
Pd23 Pd4 Sc6 111.59(16) 13 .
Sc5 Pd4 Sc6 66.41(2) . .
Sc12 Pd4 Sc6 114.91(2) . .
Sc6 Pd4 Sc6 122.84(4) 11 .
Pd23 Pd4 Sc2 105.8(5) 13 .
Sc5 Pd4 Sc2 67.77(5) . .
Sc12 Pd4 Sc2 173.75(5) . .
Sc6 Pd4 Sc2 66.79(2) 11 .
Sc6 Pd4 Sc2 66.79(2) . .
Pd23 Pd4 Sc13 11.2(2) 13 13
Sc5 Pd4 Sc13 175.2(3) . 13
Sc12 Pd4 Sc13 56.8(3) . 13
Sc6 Pd4 Sc13 114.87(7) 11 13
Sc6 Pd4 Sc13 114.87(7) . 13
Sc2 Pd4 Sc13 117.0(3) . 13
Pd23 Pd4 Sc9B 50.7(6) 13 13
Sc5 Pd4 Sc9B 124.2(4) . 13
Sc12 Pd4 Sc9B 108.2(5) . 13
Sc6 Pd4 Sc9B 119.3(5) 11 13
Sc6 Pd4 Sc9B 67.3(4) . 13
Sc2 Pd4 Sc9B 66.6(5) . 13
Sc13 Pd4 Sc9B 59.6(5) 13 13
Pd23 Pd4 Sc9B 50.7(6) 13 7_545
Sc5 Pd4 Sc9B 124.2(4) . 7_545
Sc12 Pd4 Sc9B 108.2(5) . 7_545
Sc6 Pd4 Sc9B 67.3(4) 11 7_545
Sc6 Pd4 Sc9B 119.3(5) . 7_545
Sc2 Pd4 Sc9B 66.6(5) . 7_545
Sc13 Pd4 Sc9B 59.6(5) 13 7_545
Sc9B Pd4 Sc9B 59.8(9) 13 7_545
Pd23 Pd4 Sc11 119.9(4) 13 .
Sc5 Pd4 Sc11 65.27(3) . .
Sc12 Pd4 Sc11 63.10(3) . .
Sc6 Pd4 Sc11 119.18(3) 11 .
Sc6 Pd4 Sc11 64.31(3) . .
Sc2 Pd4 Sc11 121.88(4) . .
Sc13 Pd4 Sc11 110.8(2) 13 .
Sc9B Pd4 Sc11 117.6(5) 13 .
Sc9B Pd4 Sc11 170.4(5) 7_545 .
Pd23 Pd4 Sc11 119.9(4) 13 11
Sc5 Pd4 Sc11 65.27(3) . 11
Sc12 Pd4 Sc11 63.10(3) . 11
Sc6 Pd4 Sc11 64.31(3) 11 11
Sc6 Pd4 Sc11 119.18(3) . 11
Sc2 Pd4 Sc11 121.88(4) . 11
Sc13 Pd4 Sc11 110.8(2) 13 11
Sc9B Pd4 Sc11 170.4(5) 13 11
Sc9B Pd4 Sc11 117.6(5) 7_545 11
Sc11 Pd4 Sc11 63.27(4) . 11
Pd23 Pd4 Sc9A 57.6(6) 13 13
Sc5 Pd4 Sc9A 117.2(5) . 13
Sc12 Pd4 Sc9A 114.0(6) . 13
Sc6 Pd4 Sc9A 117.7(5) 11 13
Sc6 Pd4 Sc9A 61.9(5) . 13
Sc2 Pd4 Sc9A 60.9(6) . 13
Sc13 Pd4 Sc9A 66.6(6) 13 13
Sc11 Pd4 Sc9A 116.1(4) . 13
Sc11 Pd4 Sc9A 177.1(6) 11 13
Sc7 Pd5 Sc7 142.71(7) 14_545 13
Sc7 Pd5 Sc12 106.02(3) 14_545 .
Sc7 Pd5 Sc12 106.02(3) 13 .
Sc7 Pd5 Sc12 106.02(3) 14_545 2_655
Sc7 Pd5 Sc12 106.02(3) 13 2_655
Sc12 Pd5 Sc12 60.61(6) . 2_655
Sc7 Pd5 Sc3 74.92(3) 14_545 9_655
Sc7 Pd5 Sc3 74.92(3) 13 9_655
Sc12 Pd5 Sc3 174.80(4) . 9_655
Sc12 Pd5 Sc3 114.20(4) 2_655 9_655
Sc7 Pd5 Sc3 74.92(3) 14_545 .
Sc7 Pd5 Sc3 74.92(3) 13 .
Sc12 Pd5 Sc3 114.19(4) . .
Sc12 Pd5 Sc3 174.80(4) 2_655 .
Sc3 Pd5 Sc3 71.01(6) 9_655 .
Sc7 Pd5 Pd3 160.05(4) 14_545 13
Sc7 Pd5 Pd3 57.23(3) 13 13
Sc12 Pd5 Pd3 57.42(2) . 13
Sc12 Pd5 Pd3 57.42(2) 2_655 13
Sc3 Pd5 Pd3 120.516(17) 9_655 13
Sc3 Pd5 Pd3 120.515(17) . 13
Sc7 Pd5 Pd3 57.23(3) 14_545 14_545
Sc7 Pd5 Pd3 160.05(4) 13 14_545
Sc12 Pd5 Pd3 57.42(2) . 14_545
Sc12 Pd5 Pd3 57.42(2) 2_655 14_545
Sc3 Pd5 Pd3 120.516(17) 9_655 14_545
Sc3 Pd5 Pd3 120.515(17) . 14_545
Pd3 Pd5 Pd3 102.82(3) 13 14_545
Sc7 Pd5 Sc11 120.026(19) 14_545 .
Sc7 Pd5 Sc11 63.067(19) 13 .
Sc12 Pd5 Sc11 60.10(3) . .
Sc12 Pd5 Sc11 111.74(4) 2_655 .
Sc3 Pd5 Sc11 124.09(4) 9_655 .
Sc3 Pd5 Sc11 63.92(3) . .
Pd3 Pd5 Sc11 63.928(19) 13 .
Pd3 Pd5 Sc11 110.30(2) 14_545 .
Sc7 Pd5 Sc11 120.026(19) 14_545 12_655
Sc7 Pd5 Sc11 63.067(19) 13 12_655
Sc12 Pd5 Sc11 111.74(4) . 12_655
Sc12 Pd5 Sc11 60.10(3) 2_655 12_655
Sc3 Pd5 Sc11 63.92(3) 9_655 12_655
Sc3 Pd5 Sc11 124.09(4) . 12_655
Pd3 Pd5 Sc11 63.927(19) 13 12_655
Pd3 Pd5 Sc11 110.30(2) 14_545 12_655
Sc11 Pd5 Sc11 118.87(4) . 12_655
Sc7 Pd5 Sc11 63.067(19) 14_545 11
Sc7 Pd5 Sc11 120.026(19) 13 11
Sc12 Pd5 Sc11 60.10(3) . 11
Sc12 Pd5 Sc11 111.74(4) 2_655 11
Sc3 Pd5 Sc11 124.09(4) 9_655 11
Sc3 Pd5 Sc11 63.92(3) . 11
Pd3 Pd5 Sc11 110.30(2) 13 11
Pd3 Pd5 Sc11 63.927(19) 14_545 11
Sc11 Pd5 Sc11 60.41(4) . 11
Sc11 Pd5 Sc11 171.49(4) 12_655 11
Sc7 Pd5 Sc11 63.067(19) 14_545 2_655
Sc7 Pd5 Sc11 120.026(19) 13 2_655
Sc12 Pd5 Sc11 111.74(4) . 2_655
Sc12 Pd5 Sc11 60.10(3) 2_655 2_655
Sc3 Pd5 Sc11 63.92(3) 9_655 2_655
Sc3 Pd5 Sc11 124.09(4) . 2_655
Pd3 Pd5 Sc11 110.30(2) 13 2_655
Pd3 Pd5 Sc11 63.927(19) 14_545 2_655
Sc11 Pd5 Sc11 171.49(4) . 2_655
Sc11 Pd5 Sc11 60.41(4) 12_655 2_655
Sc11 Pd5 Sc11 118.87(4) 11 2_655
Pd2 Sc1 Pd1 179.84(5) . .
Pd2 Sc1 Sc5 122.49(3) . 10
Pd1 Sc1 Sc5 57.56(3) . 10
Pd2 Sc1 Sc5 122.49(3) . .
Pd1 Sc1 Sc5 57.56(3) . .
Sc5 Sc1 Sc5 106.45(5) 10 .
Pd2 Sc1 Sc1 121.86(3) . 11
Pd1 Sc1 Sc1 58.30(3) . 11
Sc5 Sc1 Sc1 59.46(3) 10 11
Sc5 Sc1 Sc1 59.46(3) . 11
Pd2 Sc1 Sc4 120.69(5) . .
Pd1 Sc1 Sc4 59.18(3) . .
Sc5 Sc1 Sc4 107.92(5) 10 .
Sc5 Sc1 Sc4 61.07(3) . .
Sc1 Sc1 Sc4 109.17(3) 11 .
Pd2 Sc1 Sc4 120.69(5) . 10
Pd1 Sc1 Sc4 59.18(3) . 10
Sc5 Sc1 Sc4 61.07(3) 10 10
Sc5 Sc1 Sc4 107.93(5) . 10
Sc1 Sc1 Sc4 109.17(3) 11 10
Sc4 Sc1 Sc4 59.22(5) . 10
Pd2 Sc1 Sc11 61.05(3) . .
Pd1 Sc1 Sc11 119.00(3) . .
Sc5 Sc1 Sc11 148.59(5) 10 .
Sc5 Sc1 Sc11 61.44(3) . .
Sc1 Sc1 Sc11 91.34(3) 11 .
Sc4 Sc1 Sc11 91.65(3) . .
Sc4 Sc1 Sc11 148.23(5) 10 .
Pd2 Sc1 Sc11 61.05(3) . 10
Pd1 Sc1 Sc11 119.00(3) . 10
Sc5 Sc1 Sc11 61.44(3) 10 10
Sc5 Sc1 Sc11 148.59(5) . 10
Sc1 Sc1 Sc11 91.34(3) 11 10
Sc4 Sc1 Sc11 148.23(5) . 10
Sc4 Sc1 Sc11 91.65(3) 10 10
Sc11 Sc1 Sc11 112.44(5) . 10
Pd2 Sc1 Sc10 61.07(3) . 10
Pd1 Sc1 Sc10 118.80(4) . 10
Sc5 Sc1 Sc10 92.20(3) 10 10
Sc5 Sc1 Sc10 148.99(4) . 10
Sc1 Sc1 Sc10 149.18(2) 11 10
Sc4 Sc1 Sc10 89.96(4) . 10
Sc4 Sc1 Sc10 59.62(3) 10 10
Sc11 Sc1 Sc10 112.63(5) . 10
Sc11 Sc1 Sc10 62.31(3) 10 10
Pd2 Sc1 Sc10 61.07(3) . .
Pd1 Sc1 Sc10 118.80(4) . .
Sc5 Sc1 Sc10 148.99(4) 10 .
Sc5 Sc1 Sc10 92.20(3) . .
Sc1 Sc1 Sc10 149.18(2) 11 .
Sc4 Sc1 Sc10 59.62(3) . .
Sc4 Sc1 Sc10 89.96(4) 10 .
Sc11 Sc1 Sc10 62.31(3) . .
Sc11 Sc1 Sc10 112.63(5) 10 .
Sc10 Sc1 Sc10 61.46(4) 10 .
Pd2 Sc1 Sc3 60.56(4) . .
Pd1 Sc1 Sc3 119.60(5) . .
Sc5 Sc1 Sc3 91.93(4) 10 .
Sc5 Sc1 Sc3 91.93(4) . .
Sc1 Sc1 Sc3 61.30(3) 11 .
Sc4 Sc1 Sc3 149.75(3) . .
Sc4 Sc1 Sc3 149.75(3) 10 .
Sc11 Sc1 Sc3 61.57(3) . .
Sc11 Sc1 Sc3 61.57(3) 10 .
Sc10 Sc1 Sc3 112.40(4) 10 .
Sc10 Sc1 Sc3 112.40(4) . .
Pd4 Sc2 Pd4 167.06(8) 2 .
Pd4 Sc2 Sc9C 118.6(12) 2 13
Pd4 Sc2 Sc9C 71.2(12) . 13
Pd4 Sc2 Sc9C 71.2(12) 2 15_455
Pd4 Sc2 Sc9C 118.6(12) . 15_455
Sc9C Sc2 Sc9C 48(2) 13 15_455
Pd4 Sc2 Sc9C 118.6(12) 2 7_545
Pd4 Sc2 Sc9C 71.2(12) . 7_545
Sc9C Sc2 Sc9C 74(2) 13 7_545
Sc9C Sc2 Sc9C 92.6(17) 15_455 7_545
Pd4 Sc2 Sc9C 71.2(12) 2 5_445
Pd4 Sc2 Sc9C 118.6(12) . 5_445
Sc9C Sc2 Sc9C 92.6(17) 13 5_445
Sc9C Sc2 Sc9C 74(2) 15_455 5_445
Sc9C Sc2 Sc9C 48(2) 7_545 5_445
Pd4 Sc2 Sc5 113.21(6) 2 .
Pd4 Sc2 Sc5 53.85(3) . .
Sc9C Sc2 Sc5 113.6(9) 13 .
Sc9C Sc2 Sc5 143.1(10) 15_455 .
Sc9C Sc2 Sc5 113.6(9) 7_545 .
Sc9C Sc2 Sc5 143.1(10) 5_445 .
Pd4 Sc2 Sc5 53.85(3) 2 2
Pd4 Sc2 Sc5 113.21(6) . 2
Sc9C Sc2 Sc5 143.1(10) 13 2
Sc9C Sc2 Sc5 113.6(9) 15_455 2
Sc9C Sc2 Sc5 143.1(10) 7_545 2
Sc9C Sc2 Sc5 113.6(10) 5_445 2
Sc5 Sc2 Sc5 59.35(6) . 2
Pd4 Sc2 Sc9A 123.8(7) 2 13
Pd4 Sc2 Sc9A 66.2(6) . 13
Sc5 Sc2 Sc9A 110.4(4) . 13
Sc5 Sc2 Sc9A 145.7(5) 2 13
Pd4 Sc2 Sc9A 66.2(6) 2 15_455
Pd4 Sc2 Sc9A 123.8(7) . 15_455
Sc5 Sc2 Sc9A 145.7(5) . 15_455
Sc5 Sc2 Sc9A 110.4(4) 2 15_455
Sc9A Sc2 Sc9A 57.7(13) 13 15_455
Pd4 Sc2 Sc9A 66.2(6) 2 5_445
Pd4 Sc2 Sc9A 123.8(7) . 5_445
Sc5 Sc2 Sc9A 145.7(5) . 5_445
Sc5 Sc2 Sc9A 110.4(5) 2 5_445
Sc9A Sc2 Sc9A 95.0(7) 13 5_445
Sc9A Sc2 Sc9A 67.7(12) 15_455 5_445
Pd4 Sc2 Sc9A 123.8(7) 2 7_545
Pd4 Sc2 Sc9A 66.2(6) . 7_545
Sc5 Sc2 Sc9A 110.4(4) . 7_545
Sc5 Sc2 Sc9A 145.7(5) 2 7_545
Sc9A Sc2 Sc9A 67.7(12) 13 7_545
Sc9A Sc2 Sc9A 95.0(7) 15_455 7_545
Sc9A Sc2 Sc9A 57.7(13) 5_445 7_545
Pd5 Sc3 Pd5 108.99(6) 9_655 .
Pd5 Sc3 Pd2 97.041(16) 9_655 11
Pd5 Sc3 Pd2 97.041(16) . 11
Pd5 Sc3 Pd2 97.041(16) 9_655 .
Pd5 Sc3 Pd2 97.041(16) . .
Pd2 Sc3 Pd2 155.63(7) 11 .
Pd5 Sc3 Sc1 120.63(2) 9_655 11
Pd5 Sc3 Sc1 120.62(2) . 11
Pd2 Sc3 Sc1 49.12(3) 11 11
Pd2 Sc3 Sc1 106.51(6) . 11
Pd5 Sc3 Sc1 120.63(2) 9_655 .
Pd5 Sc3 Sc1 120.63(2) . .
Pd2 Sc3 Sc1 106.51(6) 11 .
Pd2 Sc3 Sc1 49.12(3) . .
Sc1 Sc3 Sc1 57.39(6) 11 .
Pd5 Sc3 Sc11 147.76(3) 9_655 .
Pd5 Sc3 Sc11 63.08(2) . .
Pd2 Sc3 Sc11 114.63(3) 11 .
Pd2 Sc3 Sc11 55.97(2) . .
Sc1 Sc3 Sc11 86.73(4) 11 .
Sc1 Sc3 Sc11 57.54(3) . .
Pd5 Sc3 Sc11 63.08(2) 9_655 4
Pd5 Sc3 Sc11 147.76(3) . 4
Pd2 Sc3 Sc11 55.97(2) 11 4
Pd2 Sc3 Sc11 114.63(3) . 4
Sc1 Sc3 Sc11 57.54(3) 11 4
Sc1 Sc3 Sc11 86.73(4) . 4
Sc11 Sc3 Sc11 140.44(7) . 4
Pd5 Sc3 Sc11 63.08(2) 9_655 10
Pd5 Sc3 Sc11 147.76(3) . 10
Pd2 Sc3 Sc11 114.63(3) 11 10
Pd2 Sc3 Sc11 55.97(2) . 10
Sc1 Sc3 Sc11 86.73(4) 11 10
Sc1 Sc3 Sc11 57.54(3) . 10
Sc11 Sc3 Sc11 105.79(5) . 10
Sc11 Sc3 Sc11 59.92(4) 4 10
Pd5 Sc3 Sc11 147.76(3) 9_655 11
Pd5 Sc3 Sc11 63.08(2) . 11
Pd2 Sc3 Sc11 55.97(2) 11 11
Pd2 Sc3 Sc11 114.63(3) . 11
Sc1 Sc3 Sc11 57.54(3) 11 11
Sc1 Sc3 Sc11 86.73(4) . 11
Sc11 Sc3 Sc11 59.92(4) . 11
Sc11 Sc3 Sc11 105.79(5) 4 11
Sc11 Sc3 Sc11 140.44(7) 10 11
Pd5 Sc3 Sc3 54.50(3) 9_655 9_655
Pd5 Sc3 Sc3 54.50(3) . 9_655
Pd2 Sc3 Sc3 102.19(4) 11 9_655
Pd2 Sc3 Sc3 102.19(4) . 9_655
Sc1 Sc3 Sc3 151.30(3) 11 9_655
Sc1 Sc3 Sc3 151.30(3) . 9_655
Sc11 Sc3 Sc3 109.78(3) . 9_655
Sc11 Sc3 Sc3 109.78(3) 4 9_655
Sc11 Sc3 Sc3 109.78(3) 10 9_655
Sc11 Sc3 Sc3 109.78(3) 11 9_655
Pd5 Sc3 Sc7 94.39(4) 9_655 13
Pd5 Sc3 Sc7 48.97(3) . 13
Pd2 Sc3 Sc7 145.99(4) 11 13
Pd2 Sc3 Sc7 51.82(2) . 13
Sc1 Sc3 Sc7 142.51(4) 11 13
Sc1 Sc3 Sc7 94.74(3) . 13
Sc11 Sc3 Sc7 55.96(2) . 13
Sc11 Sc3 Sc7 153.86(4) 4 13
Sc11 Sc3 Sc7 99.11(3) 10 13
Sc11 Sc3 Sc7 100.35(3) 11 13
Sc3 Sc3 Sc7 60.04(3) 9_655 13
Pd3 Sc4 Pd1 175.89(5) . .
Pd3 Sc4 Sc4 125.01(3) . 10
Pd1 Sc4 Sc4 59.10(3) . 10
Pd3 Sc4 Sc6 61.82(3) . 12
Pd1 Sc4 Sc6 114.85(4) . 12
Sc4 Sc4 Sc6 148.16(2) 10 12
Pd3 Sc4 Sc6 61.82(3) . .
Pd1 Sc4 Sc6 114.86(4) . .
Sc4 Sc4 Sc6 148.16(2) 10 .
Sc6 Sc4 Sc6 63.63(4) 12 .
Pd3 Sc4 Sc1 123.53(3) . .
Pd1 Sc4 Sc1 57.63(3) . .
Sc4 Sc4 Sc1 60.39(2) 10 .
Sc6 Sc4 Sc1 146.94(5) 12 .
Sc6 Sc4 Sc1 89.38(3) . .
Pd3 Sc4 Sc1 123.53(3) . 3
Pd1 Sc4 Sc1 57.63(3) . 3
Sc4 Sc4 Sc1 60.39(2) 10 3
Sc6 Sc4 Sc1 89.38(3) 12 3
Sc6 Sc4 Sc1 146.94(5) . 3
Sc1 Sc4 Sc1 107.23(5) . 3
Pd3 Sc4 Sc10 62.76(3) . 12
Pd1 Sc4 Sc10 118.51(3) . 12
Sc4 Sc4 Sc10 91.38(3) 10 12
Sc6 Sc4 Sc10 63.04(3) 12 12
Sc6 Sc4 Sc10 115.62(5) . 12
Sc1 Sc4 Sc10 150.02(5) . 12
Sc1 Sc4 Sc10 60.89(3) 3 12
Pd3 Sc4 Sc10 62.76(3) . .
Pd1 Sc4 Sc10 118.51(3) . .
Sc4 Sc4 Sc10 91.38(3) 10 .
Sc6 Sc4 Sc10 115.62(5) 12 .
Sc6 Sc4 Sc10 63.04(3) . .
Sc1 Sc4 Sc10 60.89(3) . .
Sc1 Sc4 Sc10 150.02(5) 3 .
Sc10 Sc4 Sc10 114.30(5) 12 .
Pd3 Sc4 Sc5 120.48(5) . 2
Pd1 Sc4 Sc5 56.18(3) . 2
Sc4 Sc4 Sc5 106.75(3) 10 2
Sc6 Sc4 Sc5 58.68(3) 12 2
Sc6 Sc4 Sc5 89.98(4) . 2
Sc1 Sc4 Sc5 105.62(5) . 2
Sc1 Sc4 Sc5 58.41(3) 3 2
Sc10 Sc4 Sc5 91.38(3) 12 2
Sc10 Sc4 Sc5 148.41(4) . 2
Pd3 Sc4 Sc5 120.48(5) . .
Pd1 Sc4 Sc5 56.18(3) . .
Sc4 Sc4 Sc5 106.75(3) 10 .
Sc6 Sc4 Sc5 89.98(4) 12 .
Sc6 Sc4 Sc5 58.68(3) . .
Sc1 Sc4 Sc5 58.41(3) . .
Sc1 Sc4 Sc5 105.63(5) 3 .
Sc10 Sc4 Sc5 148.41(4) 12 .
Sc10 Sc4 Sc5 91.38(3) . .
Sc5 Sc4 Sc5 59.02(5) 2 .
Pd3 Sc4 Sc8 63.80(4) . .
Pd1 Sc4 Sc8 120.31(5) . .
Sc4 Sc4 Sc8 61.21(3) 10 .
Sc6 Sc4 Sc8 115.17(4) 12 .
Sc6 Sc4 Sc8 115.17(4) . .
Sc1 Sc4 Sc8 92.86(4) . .
Sc1 Sc4 Sc8 92.86(4) 3 .
Sc10 Sc4 Sc8 62.40(3) 12 .
Sc10 Sc4 Sc8 62.40(3) . .
Sc5 Sc4 Sc8 149.14(3) 2 .
Sc5 Sc4 Sc8 149.14(3) . .
Pd4 Sc5 Pd1 176.42(5) . .
Pd4 Sc5 Sc1 123.40(5) . .
Pd1 Sc5 Sc1 59.47(3) . .
Pd4 Sc5 Sc1 123.40(5) . 11
Pd1 Sc5 Sc1 59.47(3) . 11
Sc1 Sc5 Sc1 61.08(5) . 11
Pd4 Sc5 Sc6 59.06(3) . 11
Pd1 Sc5 Sc6 119.85(3) . 11
Sc1 Sc5 Sc6 149.68(5) . 11
Sc1 Sc5 Sc6 91.60(3) 11 11
Pd4 Sc5 Sc6 59.06(3) . .
Pd1 Sc5 Sc6 119.85(3) . .
Sc1 Sc5 Sc6 91.60(3) . .
Sc1 Sc5 Sc6 149.68(5) 11 .
Sc6 Sc5 Sc6 110.55(5) 11 .
Pd4 Sc5 Sc5 118.71(3) . 2
Pd1 Sc5 Sc5 57.71(3) . 2
Sc1 Sc5 Sc5 108.45(3) . 2
Sc1 Sc5 Sc5 108.45(3) 11 2
Sc6 Sc5 Sc5 91.82(3) 11 2
Sc6 Sc5 Sc5 91.82(3) . 2
Pd4 Sc5 Sc2 58.38(4) . .
Pd1 Sc5 Sc2 118.03(5) . .
Sc1 Sc5 Sc2 148.50(3) . .
Sc1 Sc5 Sc2 148.50(3) 11 .
Sc6 Sc5 Sc2 61.41(3) 11 .
Sc6 Sc5 Sc2 61.41(3) . .
Sc5 Sc5 Sc2 60.32(3) 2 .
Pd4 Sc5 Sc4 119.30(3) . .
Pd1 Sc5 Sc4 59.55(3) . .
Sc1 Sc5 Sc4 60.52(3) . .
Sc1 Sc5 Sc4 110.02(5) 11 .
Sc6 Sc5 Sc4 148.70(5) 11 .
Sc6 Sc5 Sc4 60.31(3) . .
Sc5 Sc5 Sc4 60.49(2) 2 .
Sc2 Sc5 Sc4 90.37(4) . .
Pd4 Sc5 Sc4 119.30(3) . 2
Pd1 Sc5 Sc4 59.55(3) . 2
Sc1 Sc5 Sc4 110.02(5) . 2
Sc1 Sc5 Sc4 60.52(3) 11 2
Sc6 Sc5 Sc4 60.31(3) 11 2
Sc6 Sc5 Sc4 148.70(5) . 2
Sc5 Sc5 Sc4 60.49(2) 2 2
Sc2 Sc5 Sc4 90.37(4) . 2
Sc4 Sc5 Sc4 110.40(5) . 2
Pd4 Sc5 Sc11 63.10(3) . .
Pd1 Sc5 Sc11 119.80(4) . .
Sc1 Sc5 Sc11 60.34(3) . .
Sc1 Sc5 Sc11 91.63(5) 11 .
Sc6 Sc5 Sc11 111.67(5) 11 .
Sc6 Sc5 Sc11 61.50(3) . .
Sc5 Sc5 Sc11 148.86(2) 2 .
Sc2 Sc5 Sc11 112.51(4) . .
Sc4 Sc5 Sc11 90.71(3) . .
Sc4 Sc5 Sc11 149.10(4) 2 .
Pd4 Sc5 Sc11 63.10(3) . 11
Pd1 Sc5 Sc11 119.80(4) . 11
Sc1 Sc5 Sc11 91.63(5) . 11
Sc1 Sc5 Sc11 60.34(3) 11 11
Sc6 Sc5 Sc11 61.50(3) 11 11
Sc6 Sc5 Sc11 111.67(5) . 11
Sc5 Sc5 Sc11 148.86(2) 2 11
Sc2 Sc5 Sc11 112.51(4) . 11
Sc4 Sc5 Sc11 149.10(4) . 11
Sc4 Sc5 Sc11 90.71(3) 2 11
Sc11 Sc5 Sc11 61.99(4) . 11
Pd4 Sc6 Pd3 166.01(4) . .
Pd4 Sc6 Sc5 54.53(3) . .
Pd3 Sc6 Sc5 112.09(4) . .
Pd4 Sc6 Sc7 134.49(4) . .
Pd3 Sc6 Sc7 53.27(3) . .
Sc5 Sc6 Sc7 145.91(4) . .
Pd4 Sc6 Sc4 115.47(4) . .
Pd3 Sc6 Sc4 51.10(3) . .
Sc5 Sc6 Sc4 61.01(4) . .
Sc7 Sc6 Sc4 98.18(4) . .
Pd4 Sc6 Sc10 66.86(3) . 13
Pd3 Sc6 Sc10 126.31(4) . 13
Sc5 Sc6 Sc10 111.92(4) . 13
Sc7 Sc6 Sc10 99.34(4) . 13
Sc4 Sc6 Sc10 149.36(4) . 13
Pd4 Sc6 Sc2 56.66(2) . .
Pd3 Sc6 Sc2 114.99(3) . .
Sc5 Sc6 Sc2 60.18(4) . .
Sc7 Sc6 Sc2 95.89(4) . .
Sc4 Sc6 Sc2 90.07(4) . .
Sc10 Sc6 Sc2 112.80(4) 13 .
Pd4 Sc6 Sc11 61.35(3) . .
Pd3 Sc6 Sc11 117.93(4) . .
Sc5 Sc6 Sc11 60.65(3) . .
Sc7 Sc6 Sc11 151.89(4) . .
Sc4 Sc6 Sc11 90.62(3) . .
Sc10 Sc6 Sc11 62.89(3) 13 .
Sc2 Sc6 Sc11 110.81(4) . .
Pd4 Sc6 Sc9A 65.7(6) . 13
Pd3 Sc6 Sc9A 121.7(7) . 13
Sc5 Sc6 Sc9A 110.7(5) . 13
Sc7 Sc6 Sc9A 69.1(7) . 13
Sc4 Sc6 Sc9A 143.9(6) . 13
Sc10 Sc6 Sc9A 66.4(6) 13 13
Sc2 Sc6 Sc9A 59.5(5) . 13
Sc11 Sc6 Sc9A 116.8(7) . 13
Pd4 Sc6 Sc9C 69.5(12) . 13
Pd3 Sc6 Sc9C 117.2(12) . 13
Sc5 Sc6 Sc9C 112.0(11) . 13
Sc7 Sc6 Sc9C 65.0(12) . 13
Sc4 Sc6 Sc9C 139.6(12) . 13
Sc10 Sc6 Sc9C 71.0(12) 13 13
Sc2 Sc6 Sc9C 58.0(11) . 13
Sc11 Sc6 Sc9C 122.0(12) . 13
Pd4 Sc6 Sc11 128.55(4) . 13
Pd3 Sc6 Sc11 64.67(3) . 13
Sc5 Sc6 Sc11 149.05(4) . 13
Sc7 Sc6 Sc11 59.26(3) . 13
Sc4 Sc6 Sc11 107.70(4) . 13
Sc10 Sc6 Sc11 61.73(3) 13 13
Sc2 Sc6 Sc11 150.62(5) . 13
Sc11 Sc6 Sc11 92.64(3) . 13
Sc9A Sc6 Sc11 94.7(5) 13 13
Sc9C Sc6 Sc11 94.9(11) 13 13
Pd4 Sc6 Sc10 121.44(4) . .
Pd3 Sc6 Sc10 57.79(3) . .
Sc5 Sc6 Sc10 90.13(4) . .
Sc7 Sc6 Sc10 101.72(4) . .
Sc4 Sc6 Sc10 58.61(3) . .
Sc10 Sc6 Sc10 93.19(3) 13 .
Sc2 Sc6 Sc10 145.71(5) . .
Sc11 Sc6 Sc10 60.61(3) . .
Sc9A Sc6 Sc10 154.8(5) 13 .
Sc9C Sc6 Sc10 156.2(11) 13 .
Sc11 Sc6 Sc10 61.45(3) 13 .
Pd5 Sc7 Pd3 68.47(4) 13 .
Pd5 Sc7 Pd2 108.62(4) 13 13
Pd3 Sc7 Pd2 123.28(3) . 13
Pd5 Sc7 Pd2 108.62(4) 13 15_455
Pd3 Sc7 Pd2 123.28(3) . 15_455
Pd2 Sc7 Pd2 111.45(5) 13 15_455
Pd5 Sc7 Sc7 108.64(3) 13 10_556
Pd3 Sc7 Sc7 177.11(3) . 10_556
Pd2 Sc7 Sc7 57.20(2) 13 10_556
Pd2 Sc7 Sc7 57.20(2) 15_455 10_556
Pd5 Sc7 Sc6 118.31(5) 13 .
Pd3 Sc7 Sc6 61.44(3) . .
Pd2 Sc7 Sc6 74.56(3) 13 .
Pd2 Sc7 Sc6 127.87(5) 15_455 .
Sc7 Sc7 Sc6 120.84(3) 10_556 .
Pd5 Sc7 Sc6 118.31(5) 13 12
Pd3 Sc7 Sc6 61.44(3) . 12
Pd2 Sc7 Sc6 127.87(5) 13 12
Pd2 Sc7 Sc6 74.56(3) 15_455 12
Sc7 Sc7 Sc6 120.84(3) 10_556 12
Sc6 Sc7 Sc6 64.36(4) . 12
Pd5 Sc7 Sc11 67.96(3) 13 8_455
Pd3 Sc7 Sc11 68.82(3) . 8_455
Pd2 Sc7 Sc11 166.18(5) 13 8_455
Pd2 Sc7 Sc11 59.44(2) 15_455 8_455
Sc7 Sc7 Sc11 110.34(3) 10_556 8_455
Sc6 Sc7 Sc11 119.09(5) . 8_455
Sc6 Sc7 Sc11 62.14(3) 12 8_455
Pd5 Sc7 Sc11 67.96(3) 13 13
Pd3 Sc7 Sc11 68.82(3) . 13
Pd2 Sc7 Sc11 59.44(2) 13 13
Pd2 Sc7 Sc11 166.18(5) 15_455 13
Sc7 Sc7 Sc11 110.34(3) 10_556 13
Sc6 Sc7 Sc11 62.14(3) . 13
Sc6 Sc7 Sc11 119.09(5) 12 13
Sc11 Sc7 Sc11 127.08(6) 8_455 13
Pd5 Sc7 Sc3 56.12(3) 13 13
Pd3 Sc7 Sc3 114.35(4) . 13
Pd2 Sc7 Sc3 57.16(3) 13 13
Pd2 Sc7 Sc3 106.43(5) 15_455 13
Sc7 Sc7 Sc3 63.24(2) 10_556 13
Sc6 Sc7 Sc3 117.61(3) . 13
Sc6 Sc7 Sc3 174.42(5) 12 13
Sc11 Sc7 Sc3 113.41(5) 8_455 13
Sc11 Sc7 Sc3 60.21(3) 13 13
Pd5 Sc7 Sc3 56.12(3) 13 5_455
Pd3 Sc7 Sc3 114.35(4) . 5_455
Pd2 Sc7 Sc3 106.43(5) 13 5_455
Pd2 Sc7 Sc3 57.16(3) 15_455 5_455
Sc7 Sc7 Sc3 63.24(2) 10_556 5_455
Sc6 Sc7 Sc3 174.42(5) . 5_455
Sc6 Sc7 Sc3 117.61(3) 12 5_455
Sc11 Sc7 Sc3 60.21(3) 8_455 5_455
Sc11 Sc7 Sc3 113.41(5) 13 5_455
Sc3 Sc7 Sc3 59.91(6) 13 5_455
Pd5 Sc7 Sc9C 156.2(11) 13 15_455
Pd3 Sc7 Sc9C 119.3(5) . 15_455
Pd2 Sc7 Sc9C 86.3(10) 13 15_455
Pd2 Sc7 Sc9C 47.7(11) 15_455 15_455
Sc7 Sc7 Sc9C 63.3(5) 10_556 15_455
Sc6 Sc7 Sc9C 83.0(9) . 15_455
Sc6 Sc7 Sc9C 59.1(6) 12 15_455
Sc11 Sc7 Sc9C 93.1(11) 8_455 15_455
Sc11 Sc7 Sc9C 135.4(11) 13 15_455
Sc3 Sc7 Sc9C 125.8(5) 13 15_455
Sc3 Sc7 Sc9C 102.5(9) 5_455 15_455
Sc13 Sc8 Sc13 112.6(3) 9_565 .
Sc13 Sc8 Pd3 96.63(3) 9_565 .
Sc13 Sc8 Pd3 96.63(3) . .
Sc13 Sc8 Pd3 96.63(3) 9_565 10
Sc13 Sc8 Pd3 96.63(3) . 10
Pd3 Sc8 Pd3 155.98(7) . 10
Sc13 Sc8 Sc4 119.11(13) 9_565 10
Sc13 Sc8 Sc4 119.11(13) . 10
Pd3 Sc8 Sc4 106.78(6) . 10
Pd3 Sc8 Sc4 49.20(3) 10 10
Sc13 Sc8 Sc4 119.11(13) 9_565 .
Sc13 Sc8 Sc4 119.11(13) . .
Pd3 Sc8 Sc4 49.20(3) . .
Pd3 Sc8 Sc4 106.78(6) 10 .
Sc4 Sc8 Sc4 57.57(6) 10 .
Sc13 Sc8 Sc10 61.46(13) 9_565 3
Sc13 Sc8 Sc10 148.71(6) . 3
Pd3 Sc8 Sc10 114.33(3) . 3
Pd3 Sc8 Sc10 56.41(2) 10 3
Sc4 Sc8 Sc10 57.65(3) 10 3
Sc4 Sc8 Sc10 86.56(4) . 3
Sc13 Sc8 Sc10 61.46(13) 9_565 12
Sc13 Sc8 Sc10 148.71(6) . 12
Pd3 Sc8 Sc10 56.41(2) . 12
Pd3 Sc8 Sc10 114.33(3) 10 12
Sc4 Sc8 Sc10 86.56(4) 10 12
Sc4 Sc8 Sc10 57.65(3) . 12
Sc10 Sc8 Sc10 59.12(4) 3 12
Sc13 Sc8 Sc10 148.71(6) 9_565 10
Sc13 Sc8 Sc10 61.46(13) . 10
Pd3 Sc8 Sc10 114.33(3) . 10
Pd3 Sc8 Sc10 56.41(2) 10 10
Sc4 Sc8 Sc10 57.65(3) 10 10
Sc4 Sc8 Sc10 86.56(4) . 10
Sc10 Sc8 Sc10 106.42(5) 3 10
Sc10 Sc8 Sc10 140.31(7) 12 10
Sc13 Sc8 Sc10 148.71(6) 9_565 .
Sc13 Sc8 Sc10 61.46(13) . .
Pd3 Sc8 Sc10 56.41(2) . .
Pd3 Sc8 Sc10 114.33(3) 10 .
Sc4 Sc8 Sc10 86.57(4) 10 .
Sc4 Sc8 Sc10 57.65(3) . .
Sc10 Sc8 Sc10 140.31(7) 3 .
Sc10 Sc8 Sc10 106.42(5) 12 .
Sc10 Sc8 Sc10 59.12(4) 10 .
Sc13 Sc8 Sc12 94.39(12) 9_565 13
Sc13 Sc8 Sc12 49.78(5) . 13
Pd3 Sc8 Sc12 51.85(2) . 13
Pd3 Sc8 Sc12 146.22(4) 10 13
Sc4 Sc8 Sc12 143.71(4) 10 13
Sc4 Sc8 Sc12 95.32(3) . 13
Sc10 Sc8 Sc12 152.52(4) 3 13
Sc10 Sc8 Sc12 98.99(3) 12 13
Sc10 Sc8 Sc12 101.06(3) 10 13
Sc10 Sc8 Sc12 57.38(3) . 13
Sc13 Sc8 Sc12 49.78(5) 9_565 14_455
Sc13 Sc8 Sc12 94.39(12) . 14_455
Pd3 Sc8 Sc12 51.85(2) . 14_455
Pd3 Sc8 Sc12 146.22(4) 10 14_455
Sc4 Sc8 Sc12 143.71(4) 10 14_455
Sc4 Sc8 Sc12 95.32(3) . 14_455
Sc10 Sc8 Sc12 101.06(3) 3 14_455
Sc10 Sc8 Sc12 57.38(3) 12 14_455
Sc10 Sc8 Sc12 152.52(4) 10 14_455
Sc10 Sc8 Sc12 98.99(3) . 14_455
Sc12 Sc8 Sc12 51.46(5) 13 14_455
Pd2 Sc9A Pd23 108.8(12) . .
Pd2 Sc9A Sc9A 108.2(9) . 3_655
Pd23 Sc9A Sc9A 143.1(6) . 3_655
Pd2 Sc9A Sc2 132.9(7) . 13
Pd23 Sc9A Sc2 92.9(8) . 13
Sc9A Sc9A Sc2 61.1(7) 3_655 13
Pd2 Sc9A Sc2 132.9(7) . 5_554
Pd23 Sc9A Sc2 92.9(8) . 5_554
Sc9A Sc9A Sc2 61.1(7) 3_655 5_554
Sc2 Sc9A Sc2 85.0(7) 13 5_554
Pd2 Sc9A Sc6 76.2(5) . 6_554
Pd23 Sc9A Sc6 96.5(7) . 6_554
Sc9A Sc9A Sc6 92.2(7) 3_655 6_554
Sc2 Sc9A Sc6 143.8(9) 13 6_554
Sc2 Sc9A Sc6 59.77(17) 5_554 6_554
Pd2 Sc9A Sc6 76.2(5) . 13
Pd23 Sc9A Sc6 96.5(7) . 13
Sc9A Sc9A Sc6 92.2(7) 3_655 13
Sc2 Sc9A Sc6 59.77(17) 13 13
Sc2 Sc9A Sc6 143.8(9) 5_554 13
Sc6 Sc9A Sc6 152.0(10) 6_554 13
Pd2 Sc9A Pd4 112.3(8) . 13
Pd23 Sc9A Pd4 50.0(5) . 13
Sc9A Sc9A Pd4 113.9(6) 3_655 13
Sc2 Sc9A Pd4 52.9(3) 13 13
Sc2 Sc9A Pd4 113.6(9) 5_554 13
Sc6 Sc9A Pd4 146.4(12) 6_554 13
Sc6 Sc9A Pd4 52.4(2) 13 13
Pd2 Sc9A Pd4 112.3(8) . 6_554
Pd23 Sc9A Pd4 50.0(5) . 6_554
Sc9A Sc9A Pd4 113.9(6) 3_655 6_554
Sc2 Sc9A Pd4 113.6(9) 13 6_554
Sc2 Sc9A Pd4 52.9(3) 5_554 6_554
Sc6 Sc9A Pd4 52.4(2) 6_554 6_554
Sc6 Sc9A Pd4 146.4(12) 13 6_554
Pd4 Sc9A Pd4 96.1(10) 13 6_554
Pd2 Sc9A Sc13 102.6(11) . .
Pd23 Sc9A Sc13 6.21(19) . .
Sc9A Sc9A Sc13 149.3(5) 3_655 .
Sc2 Sc9A Sc13 97.5(8) 13 .
Sc2 Sc9A Sc13 97.5(8) 5_554 .
Sc6 Sc9A Sc13 95.1(7) 6_554 .
Sc6 Sc9A Sc13 95.1(7) 13 .
Pd4 Sc9A Sc13 51.7(5) 13 .
Pd4 Sc9A Sc13 51.7(5) 6_554 .
Pd2 Sc9A Sc10 56.7(5) . .
Pd23 Sc9A Sc10 61.3(7) . .
Sc9A Sc9A Sc10 146.1(5) 3_655 .
Sc2 Sc9A Sc10 104.9(4) 13 .
Sc2 Sc9A Sc10 152.4(12) 5_554 .
Sc6 Sc9A Sc10 110.3(8) 6_554 .
Sc6 Sc9A Sc10 56.1(3) 13 .
Pd4 Sc9A Sc10 58.7(5) 13 .
Pd4 Sc9A Sc10 100.0(10) 6_554 .
Sc13 Sc9A Sc10 56.1(6) . .
Pd2 Sc9A Sc10 56.7(5) . 10
Pd23 Sc9A Sc10 61.3(7) . 10
Sc9A Sc9A Sc10 146.1(5) 3_655 10
Sc2 Sc9A Sc10 152.4(12) 13 10
Sc2 Sc9A Sc10 104.9(4) 5_554 10
Sc6 Sc9A Sc10 56.1(3) 6_554 10
Sc6 Sc9A Sc10 110.3(8) 13 10
Pd4 Sc9A Sc10 100.0(10) 13 10
Pd4 Sc9A Sc10 58.7(5) 6_554 10
Sc13 Sc9A Sc10 56.1(6) . 10
Sc10 Sc9A Sc10 55.5(5) . 10
Pd23 Sc9B Pd2 119.6(12) . .
Pd23 Sc9B Sc13 7.4(2) . .
Pd2 Sc9B Sc13 112.2(10) . .
Pd23 Sc9B Sc9B 52.1(7) . 11_565
Pd2 Sc9B Sc9B 171.6(6) . 11_565
Sc13 Sc9B Sc9B 59.4(5) . 11_565
Pd23 Sc9B Pd4 56.7(4) . 13
Pd2 Sc9B Pd4 116.6(6) . 13
Sc13 Sc9B Pd4 58.7(4) . 13
Sc9B Sc9B Pd4 60.1(4) 11_565 13
Pd23 Sc9B Pd4 56.7(4) . 6_554
Pd2 Sc9B Pd4 116.6(6) . 6_554
Sc13 Sc9B Pd4 58.7(4) . 6_554
Sc9B Sc9B Pd4 60.1(4) 11_565 6_554
Pd4 Sc9B Pd4 108.2(7) 13 6_554
Pd23 Sc9B Sc10 69.2(7) . .
Pd2 Sc9B Sc10 59.3(5) . .
Sc13 Sc9B Sc10 63.0(5) . .
Sc9B Sc9B Sc10 113.8(4) 11_565 .
Pd4 Sc9B Sc10 63.9(4) 13 .
Pd4 Sc9B Sc10 111.7(8) 6_554 .
Pd23 Sc9B Sc10 69.2(7) . 10
Pd2 Sc9B Sc10 59.3(5) . 10
Sc13 Sc9B Sc10 63.0(5) . 10
Sc9B Sc9B Sc10 113.8(4) 11_565 10
Pd4 Sc9B Sc10 111.7(8) 13 10
Pd4 Sc9B Sc10 63.9(4) 6_554 10
Sc10 Sc9B Sc10 59.9(5) . 10
Pd23 Sc9B Sc2 100.5(7) . 13
Pd2 Sc9B Sc2 123.2(6) . 13
Sc13 Sc9B Sc2 105.9(6) . 13
Sc9B Sc9B Sc2 62.2(4) 11_565 13
Pd4 Sc9B Sc2 54.4(3) 13 13
Pd4 Sc9B Sc2 118.9(8) 6_554 13
Sc10 Sc9B Sc2 108.33(13) . 13
Sc10 Sc9B Sc2 166.1(7) 10 13
Pd23 Sc9B Sc2 100.5(7) . 5_554
Pd2 Sc9B Sc2 123.2(6) . 5_554
Sc13 Sc9B Sc2 105.9(6) . 5_554
Sc9B Sc9B Sc2 62.2(4) 11_565 5_554
Pd4 Sc9B Sc2 118.9(8) 13 5_554
Pd4 Sc9B Sc2 54.4(3) 6_554 5_554
Sc10 Sc9B Sc2 166.1(7) . 5_554
Sc10 Sc9B Sc2 108.33(13) 10 5_554
Sc2 Sc9B Sc2 82.1(7) 13 5_554
Pd23 Sc9B Sc6 104.9(5) . 6_554
Pd2 Sc9B Sc6 72.9(4) . 6_554
Sc13 Sc9B Sc6 103.3(5) . 6_554
Sc9B Sc9B Sc6 108.0(4) 11_565 6_554
Pd4 Sc9B Sc6 161.4(8) 13 6_554
Pd4 Sc9B Sc6 54.05(5) 6_554 6_554
Sc10 Sc9B Sc6 114.4(8) . 6_554
Sc10 Sc9B Sc6 57.8(3) 10 6_554
Sc2 Sc9B Sc6 135.7(9) 13 6_554
Sc2 Sc9B Sc6 58.1(2) 5_554 6_554
Pd23 Sc9B Sc6 104.9(5) . 13
Pd2 Sc9B Sc6 72.9(4) . 13
Sc13 Sc9B Sc6 103.3(5) . 13
Sc9B Sc9B Sc6 108.0(4) 11_565 13
Pd4 Sc9B Sc6 54.05(5) 13 13
Pd4 Sc9B Sc6 161.4(8) 6_554 13
Sc10 Sc9B Sc6 57.8(3) . 13
Sc10 Sc9B Sc6 114.4(8) 10 13
Sc2 Sc9B Sc6 58.1(2) 13 13
Sc2 Sc9B Sc6 135.7(9) 5_554 13
Sc6 Sc9B Sc6 142.6(8) 6_554 13
Sc9C Sc9C Pd2 114.8(15) 3_655 .
Sc9C Sc9C Sc2 66.2(12) 3_655 13
Pd2 Sc9C Sc2 135.5(9) . 13
Sc9C Sc9C Sc2 66.2(12) 3_655 5_554
Pd2 Sc9C Sc2 135.5(9) . 5_554
Sc2 Sc9C Sc2 87.4(17) 13 5_554
Sc9C Sc9C Sc6 97.2(12) 3_655 6_554
Pd2 Sc9C Sc6 75.9(11) . 6_554
Sc2 Sc9C Sc6 148(2) 13 6_554
Sc2 Sc9C Sc6 60.5(3) 5_554 6_554
Sc9C Sc9C Sc6 97.2(12) 3_655 13
Pd2 Sc9C Sc6 75.9(11) . 13
Sc2 Sc9C Sc6 60.5(3) 13 13
Sc2 Sc9C Sc6 148(2) 5_554 13
Sc6 Sc9C Sc6 152(2) 6_554 13
Sc9C Sc9C Pd23 144.8(12) 3_655 .
Pd2 Sc9C Pd23 100(2) . .
Sc2 Sc9C Pd23 89.0(15) 13 .
Sc2 Sc9C Pd23 89.0(15) 5_554 .
Sc6 Sc9C Pd23 91.1(12) 6_554 .
Sc6 Sc9C Pd23 91.1(12) 13 .
Sc9C Sc9C Sc7 68.4(11) 3_655 6_554
Pd2 Sc9C Sc7 54.2(11) . 6_554
Sc2 Sc9C Sc7 131(2) 13 6_554
Sc2 Sc9C Sc7 91.7(10) 5_554 6_554
Sc6 Sc9C Sc7 55.9(7) 6_554 6_554
Sc6 Sc9C Sc7 108.1(17) 13 6_554
Pd23 Sc9C Sc7 140.4(16) . 6_554
Sc9C Sc9C Sc7 68.4(11) 3_655 13
Pd2 Sc9C Sc7 54.2(11) . 13
Sc2 Sc9C Sc7 91.7(10) 13 13
Sc2 Sc9C Sc7 131(2) 5_554 13
Sc6 Sc9C Sc7 108.1(17) 6_554 13
Sc6 Sc9C Sc7 55.9(7) 13 13
Pd23 Sc9C Sc7 140.4(16) . 13
Sc7 Sc9C Sc7 53.3(10) 6_554 13
Pd2 Sc10 Pd3 159.87(4) . .
Pd2 Sc10 Sc4 109.43(4) . .
Pd3 Sc10 Sc4 50.65(3) . .
Pd2 Sc10 Sc6 71.41(3) . 13
Pd3 Sc10 Sc6 121.55(4) . 13
Sc4 Sc10 Sc6 143.11(4) . 13
Pd2 Sc10 Sc1 49.95(3) . .
Pd3 Sc10 Sc1 110.04(4) . .
Sc4 Sc10 Sc1 59.49(4) . .
Sc6 Sc10 Sc1 110.68(4) 13 .
Pd2 Sc10 Sc12 144.28(4) . 13
Pd3 Sc10 Sc12 54.14(3) . 13
Sc4 Sc10 Sc12 100.05(4) . 13
Sc6 Sc10 Sc12 96.77(4) 13 13
Sc1 Sc10 Sc12 152.38(5) . 13
Pd2 Sc10 Sc10 56.973(19) . 10
Pd3 Sc10 Sc10 118.30(2) . 10
Sc4 Sc10 Sc10 88.62(3) . 10
Sc6 Sc10 Sc10 118.06(2) 13 10
Sc1 Sc10 Sc10 59.27(2) . 10
Sc12 Sc10 Sc10 105.45(3) 13 10
Pd2 Sc10 Sc9B 51.1(4) . .
Pd3 Sc10 Sc9B 147.1(4) . .
Sc4 Sc10 Sc9B 148.3(3) . .
Sc6 Sc10 Sc9B 61.6(3) 13 .
Sc1 Sc10 Sc9B 96.8(4) . .
Sc12 Sc10 Sc9B 93.4(4) 13 .
Sc10 Sc10 Sc9B 60.0(3) 10 .
Pd2 Sc10 Sc13 97.94(19) . .
Pd3 Sc10 Sc13 94.8(2) . .
Sc4 Sc10 Sc13 116.1(3) . .
Sc6 Sc10 Sc13 99.9(2) 13 .
Sc1 Sc10 Sc13 119.30(4) . .
Sc12 Sc10 Sc13 49.75(13) 13 .
Sc10 Sc10 Sc13 60.145(18) 10 .
Sc9B Sc10 Sc13 54.4(5) . .
Pd2 Sc10 Sc11 56.16(3) . .
Pd3 Sc10 Sc11 114.46(4) . .
Sc4 Sc10 Sc11 89.15(4) . .
Sc6 Sc10 Sc11 59.90(3) 13 .
Sc1 Sc10 Sc11 58.19(3) . .
Sc12 Sc10 Sc11 145.96(4) 13 .
Sc10 Sc10 Sc11 107.49(2) 10 .
Sc9B Sc10 Sc11 95.6(4) . .
Sc13 Sc10 Sc11 150.0(3) . .
Pd2 Sc10 Sc6 113.45(4) . .
Pd3 Sc10 Sc6 56.45(3) . .
Sc4 Sc10 Sc6 58.35(3) . .
Sc6 Sc10 Sc6 86.81(3) 13 .
Sc1 Sc10 Sc6 86.05(3) . .
Sc12 Sc10 Sc6 98.90(4) 13 .
Sc10 Sc10 Sc6 142.02(2) 10 .
Sc9B Sc10 Sc6 147.3(3) . .
Sc13 Sc10 Sc6 148.33(17) . .
Sc11 Sc10 Sc6 58.45(3) . .
Pd2 Sc10 Sc8 116.72(3) . .
Pd3 Sc10 Sc8 59.17(2) . .
Sc4 Sc10 Sc8 59.95(4) . .
Sc6 Sc10 Sc8 154.49(5) 13 .
Sc1 Sc10 Sc8 90.62(4) . .
Sc12 Sc10 Sc8 62.03(4) 13 .
Sc10 Sc10 Sc8 60.439(18) 10 .
Sc9B Sc10 Sc8 103.3(4) . .
Sc13 Sc10 Sc8 56.1(3) . .
Sc11 Sc10 Sc8 145.43(5) . .
Sc6 Sc10 Sc8 109.26(4) . .
Pd2 Sc11 Sc12 143.72(5) . .
Pd2 Sc11 Pd4 160.36(4) . .
Sc12 Sc11 Pd4 52.59(3) . .
Pd2 Sc11 Sc7 55.03(3) . 13
Sc12 Sc11 Sc7 90.56(4) . 13
Pd4 Sc11 Sc7 143.13(4) . 13
Pd2 Sc11 Sc1 50.60(3) . .
Sc12 Sc11 Sc1 146.56(4) . .
Pd4 Sc11 Sc1 109.82(4) . .
Sc7 Sc11 Sc1 102.41(4) 13 .
Pd2 Sc11 Sc5 108.82(4) . .
Sc12 Sc11 Sc5 97.75(4) . .
Pd4 Sc11 Sc5 51.62(3) . .
Sc7 Sc11 Sc5 153.31(5) 13 .
Sc1 Sc11 Sc5 58.22(4) . .
Pd2 Sc11 Sc6 116.71(4) . .
Sc12 Sc11 Sc6 98.14(4) . .
Pd4 Sc11 Sc6 54.34(2) . .
Sc7 Sc11 Sc6 145.96(4) 13 .
Sc1 Sc11 Sc6 88.20(4) . .
Sc5 Sc11 Sc6 57.85(3) . .
Pd2 Sc11 Sc6 71.04(3) . 13
Sc12 Sc11 Sc6 102.62(4) . 13
Pd4 Sc11 Sc6 121.99(3) . 13
Sc7 Sc11 Sc6 58.60(3) 13 13
Sc1 Sc11 Sc6 110.48(4) . 13
Sc5 Sc11 Sc6 141.87(4) . 13
Sc6 Sc11 Sc6 87.36(3) . 13
Pd2 Sc11 Pd5 91.08(3) . .
Sc12 Sc11 Pd5 53.95(3) . .
Pd4 Sc11 Pd5 100.19(3) . .
Sc7 Sc11 Pd5 48.97(3) 13 .
Sc1 Sc11 Pd5 113.88(4) . .
Sc5 Sc11 Pd5 118.32(3) . .
Sc6 Sc11 Pd5 152.04(4) . .
Sc6 Sc11 Pd5 99.69(3) 13 .
Pd2 Sc11 Sc11 116.19(2) . 11
Sc12 Sc11 Sc11 58.00(2) . 11
Pd4 Sc11 Sc11 58.367(19) . 11
Sc7 Sc11 Sc11 106.18(3) 13 11
Sc1 Sc11 Sc11 88.66(3) . 11
Sc5 Sc11 Sc11 59.01(2) . 11
Sc6 Sc11 Sc11 106.32(2) . 11
Sc6 Sc11 Sc11 157.09(2) 13 11
Pd5 Sc11 Sc11 59.797(18) . 11
Pd2 Sc11 Sc10 57.01(3) . .
Sc12 Sc11 Sc10 150.11(4) . .
Pd4 Sc11 Sc10 114.82(3) . .
Sc7 Sc11 Sc10 96.61(4) 13 .
Sc1 Sc11 Sc10 59.50(3) . .
Sc5 Sc11 Sc10 88.74(3) . .
Sc6 Sc11 Sc10 60.94(3) . .
Sc6 Sc11 Sc10 58.37(3) 13 .
Pd5 Sc11 Sc10 144.68(4) . .
Sc11 Sc11 Sc10 144.41(2) 11 .
Pd2 Sc11 Sc3 57.46(2) . .
Sc12 Sc11 Sc3 99.65(4) . .
Pd4 Sc11 Sc3 117.83(3) . .
Sc7 Sc11 Sc3 63.83(4) 13 .
Sc1 Sc11 Sc3 60.88(4) . .
Sc5 Sc11 Sc3 89.71(4) . .
Sc6 Sc11 Sc3 144.79(5) . .
Sc6 Sc11 Sc3 117.69(4) 13 .
Pd5 Sc11 Sc3 53.00(3) . .
Sc11 Sc11 Sc3 60.040(19) 11 .
Sc10 Sc11 Sc3 109.58(3) . .
Sc13 Sc12 Pd4 65.5(3) 13 .
Sc13 Sc12 Pd3 113.64(13) 13 13
Pd4 Sc12 Pd3 120.79(3) . 13
Sc13 Sc12 Pd3 113.64(13) 13 14_545
Pd4 Sc12 Pd3 120.79(3) . 14_545
Pd3 Sc12 Pd3 112.95(5) 13 14_545
Sc13 Sc12 Pd5 174.0(3) 13 .
Pd4 Sc12 Pd5 120.53(5) . .
Pd3 Sc12 Pd5 63.98(3) 13 .
Pd3 Sc12 Pd5 63.98(3) 14_545 .
Sc13 Sc12 Sc12 114.3(3) 13 2_655
Pd4 Sc12 Sc12 179.77(3) . 2_655
Pd3 Sc12 Sc12 59.26(3) 13 2_655
Pd3 Sc12 Sc12 59.26(3) 14_545 2_655
Pd5 Sc12 Sc12 59.70(3) . 2_655
Sc13 Sc12 Pd23 10.80(10) 13 13
Pd4 Sc12 Pd23 54.7(4) . 13
Pd3 Sc12 Pd23 117.72(13) 13 13
Pd3 Sc12 Pd23 117.72(13) 14_545 13
Pd5 Sc12 Pd23 175.2(4) . 13
Sc12 Sc12 Pd23 125.1(4) 2_655 13
Sc13 Sc12 Sc11 118.9(2) 13 11
Pd4 Sc12 Sc11 64.30(3) . 11
Pd3 Sc12 Sc11 120.84(5) 13 11
Pd3 Sc12 Sc11 68.23(3) 14_545 11
Pd5 Sc12 Sc11 65.95(4) . 11
Sc12 Sc12 Sc11 115.88(3) 2_655 11
Pd23 Sc12 Sc11 110.1(3) 13 11
Sc13 Sc12 Sc11 118.9(2) 13 .
Pd4 Sc12 Sc11 64.30(3) . .
Pd3 Sc12 Sc11 68.23(3) 13 .
Pd3 Sc12 Sc11 120.84(5) 14_545 .
Pd5 Sc12 Sc11 65.95(4) . .
Sc12 Sc12 Sc11 115.88(3) 2_655 .
Pd23 Sc12 Sc11 110.1(3) 13 .
Sc11 Sc12 Sc11 64.00(5) 11 .
Sc13 Sc12 Sc10 66.65(8) 13 7_545
Pd4 Sc12 Sc10 68.03(3) . 7_545
Pd3 Sc12 Sc10 170.87(5) 13 7_545
Pd3 Sc12 Sc10 60.37(2) 14_545 7_545
Pd5 Sc12 Sc10 114.72(3) . 7_545
Sc12 Sc12 Sc10 111.91(3) 2_655 7_545
Pd23 Sc12 Sc10 64.38(7) 13 7_545
Sc11 Sc12 Sc10 63.89(3) 11 7_545
Sc11 Sc12 Sc10 120.12(5) . 7_545
Sc13 Sc12 Sc10 66.65(8) 13 13
Pd4 Sc12 Sc10 68.03(3) . 13
Pd3 Sc12 Sc10 60.37(2) 13 13
Pd3 Sc12 Sc10 170.87(5) 14_545 13
Pd5 Sc12 Sc10 114.72(3) . 13
Sc12 Sc12 Sc10 111.91(3) 2_655 13
Pd23 Sc12 Sc10 64.38(7) 13 13
Sc11 Sc12 Sc10 120.12(5) 11 13
Sc11 Sc12 Sc10 63.89(3) . 13
Sc10 Sc12 Sc10 125.43(6) 7_545 13
Sc13 Sc12 Sc8 60.2(2) 13 13
Pd4 Sc12 Sc8 115.55(4) . 13
Pd3 Sc12 Sc8 60.38(3) 13 13
Pd3 Sc12 Sc8 111.14(5) 14_545 13
Pd5 Sc12 Sc8 114.86(4) . 13
Sc12 Sc12 Sc8 64.27(3) 2_655 13
Pd23 Sc12 Sc8 69.1(3) 13 13
Sc11 Sc12 Sc8 178.74(5) 11 13
Sc11 Sc12 Sc8 117.15(4) . 13
Sc10 Sc12 Sc8 114.86(5) 7_545 13
Sc10 Sc12 Sc8 60.59(3) 13 13
Pd23 Sc13 Sc12 114.3(3) . 6_554
Pd23 Sc13 Sc12 114.3(3) . 13
Sc12 Sc13 Sc12 131.4(6) 6_554 13
Pd23 Sc13 Pd4 56.5(2) . 13
Sc12 Sc13 Pd4 170.8(5) 6_554 13
Sc12 Sc13 Pd4 57.75(6) 13 13
Pd23 Sc13 Pd4 56.5(2) . 6_554
Sc12 Sc13 Pd4 57.75(6) 6_554 6_554
Sc12 Sc13 Pd4 170.8(5) 13 6_554
Pd4 Sc13 Pd4 113.1(5) 13 6_554
Pd23 Sc13 Sc9B 30.6(5) . 11_565
Sc12 Sc13 Sc9B 110.7(2) 6_554 11_565
Sc12 Sc13 Sc9B 110.7(2) 13 11_565
Pd4 Sc13 Sc9B 61.7(3) 13 11_565
Pd4 Sc13 Sc9B 61.7(3) 6_554 11_565
Pd23 Sc13 Sc9B 30.6(5) . .
Sc12 Sc13 Sc9B 110.7(2) 6_554 .
Sc12 Sc13 Sc9B 110.7(2) 13 .
Pd4 Sc13 Sc9B 61.7(3) 13 .
Pd4 Sc13 Sc9B 61.7(3) 6_554 .
Sc9B Sc13 Sc9B 61.1(11) 11_565 .
Pd23 Sc13 Sc8 146.29(16) . 9_565
Sc12 Sc13 Sc8 70.0(3) 6_554 9_565
Sc12 Sc13 Sc8 70.0(3) 13 9_565
Pd4 Sc13 Sc8 117.30(14) 13 9_565
Pd4 Sc13 Sc8 117.30(14) 6_554 9_565
Sc9B Sc13 Sc8 115.7(5) 11_565 9_565
Sc9B Sc13 Sc8 176.9(6) . 9_565
Pd23 Sc13 Sc8 146.29(16) . .
Sc12 Sc13 Sc8 70.0(3) 6_554 .
Sc12 Sc13 Sc8 70.0(3) 13 .
Pd4 Sc13 Sc8 117.30(14) 13 .
Pd4 Sc13 Sc8 117.30(14) 6_554 .
Sc9B Sc13 Sc8 176.9(6) 11_565 .
Sc9B Sc13 Sc8 115.7(5) . .
Sc8 Sc13 Sc8 67.4(3) 9_565 .
Pd23 Sc13 Sc10 88.7(3) . .
Sc12 Sc13 Sc10 117.57(18) 6_554 .
Sc12 Sc13 Sc10 63.60(6) 13 .
Pd4 Sc13 Sc10 64.69(9) 13 .
Pd4 Sc13 Sc10 113.8(2) 6_554 .
Sc9B Sc13 Sc10 115.0(6) 11_565 .
Sc9B Sc13 Sc10 62.6(5) . .
Sc8 Sc13 Sc10 120.0(4) 9_565 .
Sc8 Sc13 Sc10 62.43(13) . .
Pd23 Sc13 Sc10 88.7(3) . 11_565
Sc12 Sc13 Sc10 117.57(18) 6_554 11_565
Sc12 Sc13 Sc10 63.60(6) 13 11_565
Pd4 Sc13 Sc10 64.69(9) 13 11_565
Pd4 Sc13 Sc10 113.8(2) 6_554 11_565
Sc9B Sc13 Sc10 62.6(5) 11_565 11_565
Sc9B Sc13 Sc10 115.0(6) . 11_565
Sc8 Sc13 Sc10 62.43(13) 9_565 11_565
Sc8 Sc13 Sc10 120.0(4) . 11_565
Sc10 Sc13 Sc10 120.23(4) . 11_565
Pd23 Sc13 Sc10 88.7(3) . 10
Sc12 Sc13 Sc10 63.60(6) 6_554 10
Sc12 Sc13 Sc10 117.57(18) 13 10
Pd4 Sc13 Sc10 113.8(2) 13 10
Pd4 Sc13 Sc10 64.69(9) 6_554 10
Sc9B Sc13 Sc10 115.0(6) 11_565 10
Sc9B Sc13 Sc10 62.6(5) . 10
Sc8 Sc13 Sc10 120.0(4) 9_565 10
Sc8 Sc13 Sc10 62.43(13) . 10
Sc10 Sc13 Sc10 59.71(4) . 10
Sc10 Sc13 Sc10 177.5(5) 11_565 10
Sc13 Pd23 Sc9B 142.1(7) . 11_565
Sc13 Pd23 Sc9B 142.1(7) . .
Sc9B Pd23 Sc9B 75.9(15) 11_565 .
Sc13 Pd23 Pd4 112.2(5) . 13
Sc9B Pd23 Pd4 72.6(5) 11_565 13
Sc9B Pd23 Pd4 72.6(5) . 13
Sc13 Pd23 Pd4 112.2(5) . 6_554
Sc9B Pd23 Pd4 72.6(5) 11_565 6_554
Sc9B Pd23 Pd4 72.6(5) . 6_554
Pd4 Pd23 Pd4 135.5(9) 13 6_554
Sc13 Pd23 Sc9A 143.1(6) . 11_565
Pd4 Pd23 Sc9A 72.4(5) 13 11_565
Pd4 Pd23 Sc9A 72.4(5) 6_554 11_565
Sc13 Pd23 Sc9A 143.1(6) . .
Pd4 Pd23 Sc9A 72.4(5) 13 .
Pd4 Pd23 Sc9A 72.4(5) 6_554 .
Sc9A Pd23 Sc9A 73.9(12) 11_565 .
Sc13 Pd23 Sc12 54.9(4) . 6_554
Sc9B Pd23 Sc12 117.0(3) 11_565 6_554
Sc9B Pd23 Sc12 117.0(3) . 6_554
Pd4 Pd23 Sc12 167.1(8) 13 6_554
Pd4 Pd23 Sc12 57.32(11) 6_554 6_554
Sc9A Pd23 Sc12 117.4(3) 11_565 6_554
Sc9A Pd23 Sc12 117.4(3) . 6_554
Sc13 Pd23 Sc12 54.9(4) . 13
Sc9B Pd23 Sc12 117.0(3) 11_565 13
Sc9B Pd23 Sc12 117.0(3) . 13
Pd4 Pd23 Sc12 57.32(11) 13 13
Pd4 Pd23 Sc12 167.1(8) 6_554 13
Sc9A Pd23 Sc12 117.4(3) 11_565 13
Sc9A Pd23 Sc12 117.4(3) . 13
Sc12 Pd23 Sc12 109.8(7) 6_554 13
Sc13 Pd23 Sc9C 144.8(12) . 11_565
Pd4 Pd23 Sc9C 72.0(5) 13 11_565
Pd4 Pd23 Sc9C 72.0(5) 6_554 11_565
Sc12 Pd23 Sc9C 118.0(5) 6_554 11_565
Sc12 Pd23 Sc9C 118.0(5) 13 11_565
Sc13 Pd23 Sc9C 144.8(12) . .
Pd4 Pd23 Sc9C 72.0(5) 13 .
Pd4 Pd23 Sc9C 72.0(5) 6_554 .
Sc12 Pd23 Sc9C 118.0(5) 6_554 .
Sc12 Pd23 Sc9C 118.0(5) 13 .
Sc9C Pd23 Sc9C 70(2) 11_565 .
Sc13 Pd23 Sc10 80.4(4) . .
Sc9B Pd23 Sc10 131.0(8) 11_565 .
Sc9B Pd23 Sc10 66.7(6) . .
Pd4 Pd23 Sc10 66.94(3) 13 .
Pd4 Pd23 Sc10 121.15(16) 6_554 .
Sc9A Pd23 Sc10 130.3(7) 11_565 .
Sc9A Pd23 Sc10 67.6(5) . .
Sc12 Pd23 Sc10 107.8(4) 6_554 .
Sc12 Pd23 Sc10 60.19(17) 13 .
Sc9C Pd23 Sc10 129.0(11) 11_565 .
Sc9C Pd23 Sc10 69.0(10) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pd1 Sc5 2.9341(14) 9
Pd1 Sc5 2.9341(14) 10
Pd1 Sc5 2.9341(14) 2
Pd1 Sc5 2.9342(14) .
Pd1 Sc1 2.9944(14) .
Pd1 Sc1 2.9945(14) 9
Pd1 Sc1 2.9945(14) 11
Pd1 Sc1 2.9945(14) 3
Pd1 Sc4 3.0448(14) .
Pd1 Sc4 3.0448(14) 9
Pd1 Sc4 3.0448(14) 10
Pd1 Sc4 3.0448(14) 2
Pd2 Sc9A 2.57(3) .
Pd2 Sc9C 2.59(7) .
Pd2 Sc1 2.6316(15) .
Pd2 Sc9B 2.72(3) .
Pd2 Sc7 2.8360(10) 13
Pd2 Sc7 2.8360(10) 6_554
Pd2 Sc11 2.9800(11) .
Pd2 Sc11 2.9800(11) 10
Pd2 Sc10 3.0090(11) .
Pd2 Sc10 3.0090(11) 10
Pd2 Sc3 3.0312(9) .
Pd3 Sc4 2.6702(15) .
Pd3 Sc7 2.7599(15) .
Pd3 Sc12 2.8627(10) 13
Pd3 Sc12 2.8627(10) 14_455
Pd3 Sc6 3.0244(11) .
Pd3 Sc6 3.0244(11) 12
Pd3 Pd5 3.0532(9) 13
Pd3 Sc10 3.0703(11) 12
Pd3 Sc10 3.0703(11) .
Pd3 Sc8 3.1648(9) .
Pd3 Sc11 3.3554(11) 13
Pd3 Sc11 3.3554(11) 8_455
Pd4 Pd23 2.685(9) 13
Pd4 Sc5 2.7615(15) .
Pd4 Sc12 2.7692(16) .
Pd4 Sc6 2.9085(11) 11
Pd4 Sc6 2.9085(11) .
Pd4 Sc2 2.9123(8) .
Pd4 Sc13 2.979(9) 13
Pd4 Sc9B 3.068(14) 13
Pd4 Sc9B 3.068(14) 7_545
Pd4 Sc11 3.1415(11) .
Pd4 Sc11 3.1415(11) 11
Pd4 Sc9A 3.34(3) 13
Pd5 Sc7 2.6654(15) 14_545
Pd5 Sc7 2.6654(15) 13
Pd5 Sc12 2.8998(17) .
Pd5 Sc12 2.8999(17) 2_655
Pd5 Sc3 2.9335(13) 9_655
Pd5 Sc3 2.9335(13) .
Pd5 Pd3 3.0532(9) 13
Pd5 Pd3 3.0532(9) 14_545
Pd5 Sc11 3.2751(11) .
Pd5 Sc11 3.2752(11) 12_655
Pd5 Sc11 3.2752(11) 11
Pd5 Sc11 3.2752(11) 2_655
Sc1 Sc5 3.0968(14) 10
Sc1 Sc5 3.0968(14) .
Sc1 Sc1 3.147(3) 11
Sc1 Sc4 3.1646(14) .
Sc1 Sc4 3.1646(14) 10
Sc1 Sc11 3.1655(13) .
Sc1 Sc11 3.1656(13) 10
Sc1 Sc10 3.2093(16) 10
Sc1 Sc10 3.2093(16) .
Sc1 Sc3 3.277(2) .
Sc2 Pd4 2.9123(8) 2
Sc2 Sc9C 3.12(5) 13
Sc2 Sc9C 3.12(5) 15_455
Sc2 Sc9C 3.12(5) 7_545
Sc2 Sc9C 3.12(5) 5_445
Sc2 Sc5 3.166(2) .
Sc2 Sc5 3.166(2) 2
Sc2 Sc9A 3.19(2) 13
Sc2 Sc9A 3.19(2) 15_455
Sc2 Sc9A 3.19(2) 5_445
Sc2 Sc9A 3.19(2) 7_545
Sc3 Pd5 2.9335(13) 9_655
Sc3 Pd2 3.0311(9) 11
Sc3 Sc1 3.277(2) 11
Sc3 Sc11 3.2991(12) .
Sc3 Sc11 3.2992(12) 4
Sc3 Sc11 3.2992(12) 10
Sc3 Sc11 3.2992(12) 11
Sc3 Sc3 3.407(4) 9_655
Sc3 Sc7 3.4118(15) 13
Sc4 Sc4 3.127(3) 10
Sc4 Sc6 3.1600(15) 12
Sc4 Sc6 3.1600(15) .
Sc4 Sc1 3.1646(14) 3
Sc4 Sc10 3.1689(13) 12
Sc4 Sc10 3.1690(13) .
Sc4 Sc5 3.1817(14) 2
Sc4 Sc5 3.1818(14) .
Sc4 Sc8 3.247(2) .
Sc5 Sc1 3.0968(14) 11
Sc5 Sc6 3.1076(13) 11
Sc5 Sc6 3.1077(13) .
Sc5 Sc5 3.135(3) 2
Sc5 Sc4 3.1818(14) 2
Sc5 Sc11 3.1996(16) .
Sc5 Sc11 3.1996(15) 11
Sc6 Sc7 3.1282(15) .
Sc6 Sc10 3.1889(14) 13
Sc6 Sc11 3.2258(14) .
Sc6 Sc9A 3.236(7) 13
Sc6 Sc9C 3.239(16) 13
Sc6 Sc11 3.2401(14) 13
Sc6 Sc10 3.3088(14) .
Sc7 Pd5 2.6653(15) 13
Sc7 Pd2 2.8359(10) 13
Sc7 Pd2 2.8359(10) 15_455
Sc7 Sc7 3.072(3) 10_556
Sc7 Sc6 3.1282(15) 12
Sc7 Sc11 3.1500(12) 8_455
Sc7 Sc11 3.1500(12) 13
Sc7 Sc3 3.4117(15) 13
Sc7 Sc3 3.4117(15) 5_455
Sc7 Sc9C 3.42(6) 15_455
Sc8 Sc13 3.113(13) 9_565
Sc8 Sc13 3.113(13) .
Sc8 Pd3 3.1648(9) 10
Sc8 Sc4 3.247(2) 10
Sc8 Sc10 3.3243(12) 3
Sc8 Sc10 3.3243(12) 12
Sc8 Sc10 3.3243(12) 10
Sc8 Sc10 3.3243(12) .
Sc8 Sc12 3.3701(17) 13
Sc8 Sc12 3.3701(17) 14_455
Sc9A Pd23 2.96(4) .
Sc9A Sc9A 3.08(7) 3_655
Sc9A Sc2 3.19(2) 13
Sc9A Sc2 3.19(2) 5_554
Sc9A Sc6 3.236(7) 6_554
Sc9A Sc6 3.236(7) 13
Sc9A Pd4 3.34(3) 13
Sc9A Pd4 3.34(3) 6_554
Sc9A Sc13 3.48(4) .
Sc9A Sc10 3.52(3) .
Sc9A Sc10 3.52(3) 10
Sc9B Pd23 2.49(3) .
Sc9B Sc13 3.01(3) .
Sc9B Sc9B 3.06(5) 11_565
Sc9B Pd4 3.068(14) 13
Sc9B Pd4 3.068(14) 6_554
Sc9B Sc10 3.28(3) .
Sc9B Sc10 3.28(3) 10
Sc9B Sc2 3.28(2) 13
Sc9B Sc2 3.28(2) 5_554
Sc9B Sc6 3.315(8) 6_554
Sc9B Sc6 3.315(8) 13
Sc9C Sc9C 2.52(14) 3_655
Sc9C Sc2 3.12(5) 13
Sc9C Sc2 3.12(5) 5_554
Sc9C Sc6 3.239(16) 6_554
Sc9C Sc6 3.239(16) 13
Sc9C Pd23 3.25(7) .
Sc9C Sc7 3.42(6) 6_554
Sc9C Sc7 3.42(6) 13
Sc10 Sc6 3.1889(14) 13
Sc10 Sc12 3.2140(13) 13
Sc10 Sc10 3.2801(19) 10
Sc10 Sc13 3.2945(11) .
Sc10 Sc11 3.2983(14) .
Sc11 Sc12 3.1091(16) .
Sc11 Sc7 3.1501(12) 13
Sc11 Sc6 3.2402(14) 13
Sc11 Sc11 3.295(2) 11
Sc12 Sc13 2.739(7) 13
Sc12 Pd3 2.8627(10) 13
Sc12 Pd3 2.8627(10) 14_545
Sc12 Sc12 2.926(3) 2_655
Sc12 Pd23 3.051(14) 13
Sc12 Sc11 3.1091(16) 11
Sc12 Sc10 3.2140(13) 7_545
Sc12 Sc10 3.2140(13) 13
Sc12 Sc8 3.3701(17) 13
Sc13 Pd23 0.627(9) .
Sc13 Sc12 2.739(7) 6_554
Sc13 Sc12 2.739(7) 13
Sc13 Pd4 2.979(9) 13
Sc13 Pd4 2.979(9) 6_554
Sc13 Sc9B 3.01(3) 11_565
Sc13 Sc8 3.113(13) 9_565
Sc13 Sc10 3.2945(11) 11_565
Sc13 Sc10 3.2945(11) 10
Pd23 Sc9B 2.49(3) 11_565
Pd23 Pd4 2.685(9) 13
Pd23 Pd4 2.685(9) 6_554
Pd23 Sc9A 2.96(4) 11_565
Pd23 Sc12 3.050(14) 6_554
Pd23 Sc12 3.050(14) 13
Pd23 Sc9C 3.25(7) 11_565
