#------------------------------------------------------------------------------
#$Date: 2016-03-21 03:15:31 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178427 $
#$URL: svn://www.crystallography.net/cod/cif/4/02/48/4024851.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4024851
loop_
_publ_author_name
'Hai-Bo Yang'
'Brian H. Northrop'
'Yao-Rong Zheng'
'Koushik Ghosh'
'Peter J. Stang'
_publ_section_title
;
Facile Self-Assembly of Neutral Dendritic Metallocycles via
Oxygen-to-Platinum Coordination
;
_journal_name_full               'Journal of Organic Chemistry'
_journal_page_first              7067
_journal_page_last               7074
_journal_paper_doi               10.1021/jo9013589
_journal_volume                  74
_journal_year                    2009
_chemical_formula_sum            'C109 H162 O11 P8 Pt4'
_chemical_formula_weight         2676.51
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 99.9300(12)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   15.5715(3)
_cell_length_b                   14.5131(4)
_cell_length_c                   25.4337(4)
_cell_measurement_reflns_used    42429
_cell_measurement_temperature    150(1)
_cell_measurement_theta_max      27.485
_cell_measurement_theta_min      1.018
_cell_volume                     5661.7(2)
_computing_cell_refinement       DENZO-SMN
_computing_data_collection       'Nonius COLLECT'
_computing_data_reduction        DENZO-SMN
_computing_molecular_graphics    'WinGX, Ortep3'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    SIR97
_diffrn_ambient_temperature      150(1)
_diffrn_measured_fraction_theta_full 0.989
_diffrn_measured_fraction_theta_max 0.989
_diffrn_measurement_device_type  'Nonius KappaCCD Diffractometer'
_diffrn_measurement_method       'Phi and Omega scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0714
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_limit_l_min       -33
_diffrn_reflns_number            22371
_diffrn_reflns_theta_full        27.54
_diffrn_reflns_theta_max         27.54
_diffrn_reflns_theta_min         1.33
_exptl_absorpt_coefficient_mu    5.094
_exptl_absorpt_correction_T_max  0.4290
_exptl_absorpt_correction_T_min  0.3297
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'DENZO-SMN (Otwinowski & Minor, 1997)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.570
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             2672
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.20
_refine_diff_density_max         2.618
_refine_diff_density_min         -1.586
_refine_diff_density_rms         0.175
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.157(9)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.035
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1135
_refine_ls_number_reflns         22371
_refine_ls_number_restraints     4
_refine_ls_restrained_S_all      1.036
_refine_ls_R_factor_all          0.0753
_refine_ls_R_factor_gt           0.0531
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0375P)²+40.1701P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1051
_refine_ls_wR_factor_ref         0.1162
_reflns_number_gt                18422
_reflns_number_total             22371
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            jo9013589_si_002.cif
_cod_data_source_block           pjs234
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan' changed
to 'multi-scan' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P21
_cod_database_code               4024851
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.56280(3) 0.76674(3) 0.405934(18) 0.02199(11) Uani 1 1 d . . .
Pt2 Pt 0.99668(3) 0.88371(4) 0.293322(18) 0.02447(12) Uani 1 1 d . . .
Pt3 Pt 0.92430(3) 0.43303(4) 0.089744(18) 0.02348(12) Uani 1 1 d . . .
Pt4 Pt 0.49047(3) 0.31455(3) 0.206441(18) 0.02128(11) Uani 1 1 d . . .
P1 P 0.5178(3) 0.8015(3) 0.31770(15) 0.0406(9) Uani 1 1 d . . .
P2 P 0.6242(2) 0.7281(3) 0.49190(14) 0.0278(8) Uani 1 1 d . . .
P3 P 0.8944(2) 0.9368(3) 0.22359(14) 0.0332(8) Uani 1 1 d . . .
P4 P 1.0899(2) 0.8205(4) 0.36346(14) 0.0424(10) Uani 1 1 d . . .
P5 P 0.8790(2) 0.4646(3) 0.00119(15) 0.0297(8) Uani 1 1 d . . .
P6 P 0.9632(2) 0.4080(3) 0.17959(13) 0.0342(9) Uani 1 1 d . . .
P7 P 0.39762(19) 0.3807(3) 0.13697(13) 0.0300(8) Uani 1 1 d . . .
P8 P 0.5925(2) 0.2612(3) 0.27593(13) 0.0293(8) Uani 1 1 d . . .
O1 O 1.0497(5) 0.8041(7) 0.2372(4) 0.032(2) Uani 1 1 d . . .
O2 O 1.1679(6) 0.8950(9) 0.2431(4) 0.042(3) Uani 1 1 d . . .
O3 O 1.3301(5) 0.7679(8) 0.1074(3) 0.032(2) Uani 1 1 d . . .
O4 O 0.9935(5) 0.5585(7) 0.1058(3) 0.027(2) Uani 1 1 d . . .
O5 O 1.0988(5) 0.5168(8) 0.0600(4) 0.035(2) Uani 1 1 d . . .
O6 O 0.4395(5) 0.3905(7) 0.2648(3) 0.0241(19) Uani 1 1 d . . .
O7 O 0.3142(5) 0.3105(8) 0.2533(4) 0.036(2) Uani 1 1 d . . .
O8 O 0.1615(5) 0.4301(7) 0.3962(3) 0.029(2) Uani 1 1 d . . .
O9 O 0.4930(5) 0.6404(6) 0.3905(3) 0.0231(19) Uani 1 1 d . . .
O10 O 0.3950(5) 0.6793(7) 0.4420(3) 0.027(2) Uani 1 1 d . . .
C1 C 0.6236(6) 0.8861(9) 0.4168(4) 0.019(2) Uani 1 1 d . . .
C2 C 0.5862(7) 0.9614(10) 0.4411(5) 0.028(3) Uani 1 1 d . . .
H2 H 0.5291 0.9545 0.4491 0.034 Uiso 1 1 calc R . .
C3 C 0.6290(7) 1.0435(9) 0.4534(5) 0.023(3) Uani 1 1 d . . .
H3 H 0.6015 1.0903 0.4707 0.028 Uiso 1 1 calc R . .
C4 C 0.7121(7) 1.0601(9) 0.4413(5) 0.023(3) Uani 1 1 d . . .
C5 C 0.7580(8) 1.1473(11) 0.4538(5) 0.031(3) Uani 1 1 d . . .
H5 H 0.7314 1.1940 0.4717 0.037 Uiso 1 1 calc R . .
C6 C 0.8356(8) 1.1631(11) 0.4409(5) 0.031(3) Uani 1 1 d . . .
H6 H 0.8653 1.2190 0.4516 0.037 Uiso 1 1 calc R . .
C7 C 0.8762(8) 1.0945(10) 0.4100(5) 0.028(3) Uani 1 1 d . . .
C8 C 0.9536(8) 1.1136(10) 0.3910(5) 0.029(3) Uani 1 1 d . . .
H8 H 0.9824 1.1705 0.4000 0.035 Uiso 1 1 calc R . .
C9 C 0.9886(8) 1.0527(10) 0.3597(6) 0.032(3) Uani 1 1 d . . .
H9 H 1.0406 1.0684 0.3470 0.039 Uiso 1 1 calc R . .
C10 C 0.9481(7) 0.9655(9) 0.3458(5) 0.023(3) Uani 1 1 d . . .
C11 C 0.8718(7) 0.9471(9) 0.3649(4) 0.023(3) Uani 1 1 d . . .
H11 H 0.8440 0.8893 0.3566 0.028 Uiso 1 1 calc R . .
C12 C 0.8333(7) 1.0103(9) 0.3960(4) 0.019(3) Uani 1 1 d . . .
C13 C 0.7512(7) 0.9907(9) 0.4129(5) 0.021(3) Uani 1 1 d . . .
C14 C 0.7058(7) 0.9053(9) 0.4043(4) 0.024(3) Uani 1 1 d . . .
H14 H 0.7339 0.8570 0.3886 0.028 Uiso 1 1 calc R . .
C15 C 1.1203(7) 0.8300(11) 0.2241(5) 0.028(3) Uani 1 1 d . . .
C16 C 1.1475(7) 0.7749(11) 0.1794(4) 0.024(3) Uani 1 1 d . . .
C17 C 1.0951(7) 0.7029(10) 0.1549(5) 0.026(3) Uani 1 1 d . . .
H17 H 1.0414 0.6890 0.1661 0.031 Uiso 1 1 calc R . .
C18 C 1.1218(7) 0.6521(9) 0.1145(5) 0.020(3) Uani 1 1 d . . .
C19 C 1.1994(7) 0.6738(10) 0.0965(5) 0.024(3) Uani 1 1 d . . .
H19 H 1.2155 0.6402 0.0676 0.028 Uiso 1 1 calc R . .
C20 C 1.2522(7) 0.7426(11) 0.1200(5) 0.030(3) Uani 1 1 d . . .
C21 C 1.2271(7) 0.7951(10) 0.1623(5) 0.028(3) Uani 1 1 d . . .
H21 H 1.2636 0.8430 0.1789 0.034 Uiso 1 1 calc R . .
C22 C 1.3618(7) 0.7172(11) 0.0672(5) 0.030(3) Uani 1 1 d . . .
H22A H 1.3291 0.7348 0.0317 0.036 Uiso 1 1 calc R . .
H22B H 1.3530 0.6505 0.0724 0.036 Uiso 1 1 calc R . .
C23 C 1.4579(7) 0.7369(10) 0.0696(5) 0.026(3) Uani 1 1 d . . .
C24 C 1.4956(9) 0.7192(14) 0.0272(6) 0.053(5) Uani 1 1 d . . .
H24 H 1.4615 0.6980 -0.0052 0.064 Uiso 1 1 calc R . .
C25 C 1.5859(9) 0.7319(14) 0.0307(6) 0.052(5) Uani 1 1 d . . .
H25 H 1.6113 0.7220 -0.0002 0.063 Uiso 1 1 calc R . .
C26 C 1.6376(9) 0.7577(15) 0.0764(7) 0.051(5) Uani 1 1 d . . .
H26 H 1.6980 0.7691 0.0777 0.061 Uiso 1 1 calc R . .
C27 C 1.6009(11) 0.7667(16) 0.1198(7) 0.073(6) Uani 1 1 d . . .
H27 H 1.6368 0.7787 0.1532 0.087 Uiso 1 1 calc R . .
C28 C 1.5084(9) 0.7587(14) 0.1171(6) 0.056(5) Uani 1 1 d . . .
H28 H 1.4828 0.7684 0.1480 0.067 Uiso 1 1 calc R . .
C29 C 1.0678(7) 0.5687(10) 0.0901(5) 0.021(3) Uani 1 1 d . . .
C30 C 0.8589(7) 0.3095(10) 0.0782(4) 0.024(2) Uiso 1 1 d . . .
C31 C 0.8995(7) 0.2371(10) 0.0551(4) 0.026(3) Uani 1 1 d . . .
H31 H 0.9557 0.2463 0.0463 0.032 Uiso 1 1 calc R . .
C32 C 0.8588(8) 0.1528(11) 0.0451(5) 0.027(3) Uani 1 1 d . . .
H32 H 0.8863 0.1045 0.0290 0.033 Uiso 1 1 calc R . .
C33 C 0.7745(8) 0.1392(10) 0.0593(5) 0.024(3) Uani 1 1 d . . .
C34 C 0.7307(9) 0.0545(10) 0.0471(6) 0.034(3) Uani 1 1 d . . .
H34 H 0.7571 0.0078 0.0291 0.041 Uiso 1 1 calc R . .
C35 C 0.6520(7) 0.0392(9) 0.0608(5) 0.024(3) Uani 1 1 d . . .
H35 H 0.6226 -0.0170 0.0504 0.029 Uiso 1 1 calc R . .
C36 C 0.6114(8) 0.1051(10) 0.0904(5) 0.024(3) Uani 1 1 d . . .
C37 C 0.5347(8) 0.0843(10) 0.1086(6) 0.031(3) Uani 1 1 d . . .
H37 H 0.5062 0.0270 0.0999 0.037 Uiso 1 1 calc R . .
C38 C 0.4997(8) 0.1491(11) 0.1399(5) 0.028(3) Uani 1 1 d . . .
H38 H 0.4462 0.1353 0.1514 0.034 Uiso 1 1 calc R . .
C39 C 0.5411(7) 0.2344(9) 0.1553(5) 0.024(3) Uani 1 1 d . . .
C40 C 0.6140(6) 0.2540(10) 0.1339(4) 0.020(3) Uani 1 1 d . . .
H40 H 0.6399 0.3130 0.1408 0.024 Uiso 1 1 calc R . .
C41 C 0.6531(6) 0.1924(9) 0.1025(5) 0.020(3) Uani 1 1 d . . .
C42 C 0.7358(7) 0.2109(10) 0.0853(5) 0.023(3) Uani 1 1 d . . .
C43 C 0.7807(7) 0.2960(10) 0.0939(5) 0.026(3) Uani 1 1 d . . .
H43 H 0.7556 0.3446 0.1111 0.031 Uiso 1 1 calc R . .
C44 C 0.3645(7) 0.3691(10) 0.2766(5) 0.024(3) Uani 1 1 d . . .
C45 C 0.3405(6) 0.4263(9) 0.3227(4) 0.018(2) Uani 1 1 d . . .
C46 C 0.2640(6) 0.4042(9) 0.3404(4) 0.019(3) Uani 1 1 d . . .
H46 H 0.2286 0.3548 0.3248 0.023 Uiso 1 1 calc R . .
C47 C 0.2400(7) 0.4555(9) 0.3814(5) 0.022(3) Uani 1 1 d . . .
C48 C 0.2938(7) 0.5279(9) 0.4053(5) 0.020(3) Uani 1 1 d . . .
H48 H 0.2774 0.5629 0.4336 0.024 Uiso 1 1 calc R . .
C49 C 0.3708(7) 0.5471(10) 0.3869(5) 0.028(3) Uani 1 1 d . . .
C50 C 0.3939(7) 0.4955(9) 0.3454(4) 0.020(3) Uani 1 1 d . . .
H50 H 0.4466 0.5084 0.3329 0.024 Uiso 1 1 calc R . .
C51 C 0.1311(7) 0.4800(10) 0.4371(5) 0.024(3) Uani 1 1 d . . .
H51A H 0.1406 0.5468 0.4326 0.029 Uiso 1 1 calc R . .
H51B H 0.1639 0.4611 0.4724 0.029 Uiso 1 1 calc R . .
C52 C 0.0355(8) 0.4614(11) 0.4348(5) 0.029(3) Uani 1 1 d . . .
C53 C -0.0079(8) 0.4984(14) 0.4727(5) 0.045(4) Uani 1 1 d . . .
H53 H 0.0244 0.5312 0.5019 0.055 Uiso 1 1 calc R . .
C54 C -0.0966(9) 0.4895(13) 0.4697(6) 0.045(4) Uani 1 1 d . . .
H54 H -0.1247 0.5166 0.4961 0.054 Uiso 1 1 calc R . .
C55 C -0.1430(9) 0.4424(17) 0.4293(7) 0.059(6) Uani 1 1 d . . .
H55 H -0.2046 0.4386 0.4260 0.070 Uiso 1 1 calc R . .
C56 C -0.1005(9) 0.3984(15) 0.3917(8) 0.084(8) Uani 1 1 d . . .
H56 H -0.1319 0.3596 0.3650 0.101 Uiso 1 1 calc R . .
C57 C -0.0133(9) 0.4126(14) 0.3944(7) 0.069(6) Uani 1 1 d . . .
H57 H 0.0146 0.3877 0.3671 0.083 Uiso 1 1 calc R . .
C58 C 0.4223(7) 0.6281(9) 0.4088(5) 0.024(3) Uani 1 1 d . . .
C59 C 0.4955(13) 0.9188(14) 0.3010(7) 0.082(5) Uiso 1 1 d . . .
H59A H 0.4489 0.9400 0.3201 0.099 Uiso 1 1 calc R . .
H59B H 0.5484 0.9552 0.3147 0.099 Uiso 1 1 calc R . .
C60 C 0.4674(12) 0.9411(14) 0.2410(7) 0.084(5) Uiso 1 1 d . . .
H60A H 0.4608 1.0079 0.2363 0.126 Uiso 1 1 calc R . .
H60B H 0.4117 0.9108 0.2275 0.126 Uiso 1 1 calc R . .
H60C H 0.5119 0.9188 0.2211 0.126 Uiso 1 1 calc R . .
C61 C 0.4368(11) 0.7271(11) 0.2792(5) 0.059(5) Uani 1 1 d . . .
H61A H 0.4328 0.7394 0.2406 0.071 Uiso 1 1 calc R . .
H61B H 0.4528 0.6616 0.2860 0.071 Uiso 1 1 calc R . .
C62 C 0.3514(12) 0.7474(14) 0.2965(7) 0.082(6) Uani 1 1 d . . .
H62A H 0.3059 0.7080 0.2766 0.123 Uiso 1 1 calc R . .
H62B H 0.3361 0.8122 0.2892 0.123 Uiso 1 1 calc R . .
H62C H 0.3563 0.7353 0.3348 0.123 Uiso 1 1 calc R . .
C63 C 0.6113(14) 0.7873(15) 0.2815(7) 0.088(7) Uani 1 1 d . . .
H63A H 0.5911 0.8001 0.2431 0.106 Uiso 1 1 calc R . .
H63B H 0.6567 0.8333 0.2951 0.106 Uiso 1 1 calc R . .
C64 C 0.650(2) 0.695(2) 0.2870(10) 0.144(13) Uani 1 1 d . . .
H64A H 0.6992 0.6926 0.2675 0.216 Uiso 1 1 calc R . .
H64B H 0.6063 0.6494 0.2724 0.216 Uiso 1 1 calc R . .
H64C H 0.6711 0.6822 0.3249 0.216 Uiso 1 1 calc R . .
C65 C 0.7429(9) 0.7379(12) 0.5034(6) 0.048(4) Uani 1 1 d . . .
H65A H 0.7646 0.7031 0.4748 0.057 Uiso 1 1 calc R . .
H65B H 0.7579 0.8035 0.4992 0.057 Uiso 1 1 calc R . .
C66 C 0.7927(9) 0.7044(10) 0.5571(6) 0.056(4) Uani 1 1 d . . .
H66A H 0.8555 0.7116 0.5578 0.083 Uiso 1 1 calc R . .
H66B H 0.7794 0.6393 0.5619 0.083 Uiso 1 1 calc R . .
H66C H 0.7752 0.7408 0.5859 0.083 Uiso 1 1 calc R . .
C67 C 0.5912(8) 0.7979(11) 0.5442(5) 0.034(3) Uani 1 1 d . . .
H67A H 0.6152 0.7702 0.5792 0.041 Uiso 1 1 calc R . .
H67B H 0.6170 0.8601 0.5431 0.041 Uiso 1 1 calc R . .
C68 C 0.4926(8) 0.8075(12) 0.5398(5) 0.039(3) Uani 1 1 d . . .
H68A H 0.4796 0.8465 0.5689 0.059 Uiso 1 1 calc R . .
H68B H 0.4666 0.7465 0.5422 0.059 Uiso 1 1 calc R . .
H68C H 0.4682 0.8358 0.5054 0.059 Uiso 1 1 calc R . .
C69 C 0.6034(9) 0.6095(12) 0.5103(6) 0.042(4) Uani 1 1 d . . .
H69A H 0.6296 0.5993 0.5482 0.050 Uiso 1 1 calc R . .
H69B H 0.5397 0.5999 0.5067 0.050 Uiso 1 1 calc R . .
C70 C 0.6407(8) 0.5390(8) 0.4756(5) 0.041(3) Uani 1 1 d . . .
H70A H 0.6289 0.4766 0.4872 0.061 Uiso 1 1 calc R . .
H70B H 0.7039 0.5480 0.4791 0.061 Uiso 1 1 calc R . .
H70C H 0.6134 0.5473 0.4382 0.061 Uiso 1 1 calc R . .
C71 C 0.9176(12) 1.0463(16) 0.1951(8) 0.070(6) Uani 1 1 d . . .
H71A H 0.8677 1.0638 0.1672 0.084 Uiso 1 1 calc R . .
H71B H 0.9237 1.0941 0.2233 0.084 Uiso 1 1 calc R . .
C72 C 1.0002(10) 1.0442(14) 0.1707(7) 0.058(5) Uani 1 1 d . . .
H72A H 1.0105 1.1053 0.1566 0.087 Uiso 1 1 calc R . .
H72B H 0.9936 0.9989 0.1417 0.087 Uiso 1 1 calc R . .
H72C H 1.0499 1.0270 0.1981 0.087 Uiso 1 1 calc R . .
C73 C 0.7859(10) 0.9461(15) 0.2394(6) 0.058(5) Uani 1 1 d . . .
H73A H 0.7685 0.8847 0.2509 0.070 Uiso 1 1 calc R . .
H73B H 0.7884 0.9882 0.2702 0.070 Uiso 1 1 calc R . .
C74 C 0.7136(11) 0.9807(17) 0.1943(7) 0.079(7) Uani 1 1 d . . .
H74A H 0.6582 0.9841 0.2075 0.119 Uiso 1 1 calc R . .
H74B H 0.7078 0.9380 0.1640 0.119 Uiso 1 1 calc R . .
H74C H 0.7290 1.0420 0.1827 0.119 Uiso 1 1 calc R . .
C75 C 0.8782(10) 0.8551(12) 0.1669(6) 0.046(4) Uani 1 1 d . . .
H75A H 0.8330 0.8800 0.1383 0.055 Uiso 1 1 calc R . .
H75B H 0.9332 0.8502 0.1525 0.055 Uiso 1 1 calc R . .
C76 C 0.8511(11) 0.7597(14) 0.1819(7) 0.067(6) Uani 1 1 d . . .
H76A H 0.8428 0.7200 0.1503 0.101 Uiso 1 1 calc R . .
H76B H 0.7963 0.7638 0.1959 0.101 Uiso 1 1 calc R . .
H76C H 0.8965 0.7336 0.2093 0.101 Uiso 1 1 calc R . .
C77 C 1.1440(9) 0.7176(12) 0.3477(7) 0.054(4) Uani 1 1 d . . .
H77A H 1.1850 0.7344 0.3235 0.065 Uiso 1 1 calc R . .
H77B H 1.1790 0.6936 0.3810 0.065 Uiso 1 1 calc R . .
C78 C 1.0854(17) 0.6398(16) 0.3215(9) 0.120(10) Uani 1 1 d . . .
H78A H 1.1216 0.5879 0.3139 0.179 Uiso 1 1 calc R . .
H78B H 1.0506 0.6620 0.2881 0.179 Uiso 1 1 calc R . .
H78C H 1.0465 0.6197 0.3457 0.179 Uiso 1 1 calc R . .
C79 C 1.1785(14) 0.8954(15) 0.3868(9) 0.113(10) Uani 1 1 d . . .
H79A H 1.2033 0.9144 0.3552 0.135 Uiso 1 1 calc R . .
H79B H 1.1533 0.9515 0.4003 0.135 Uiso 1 1 calc R . .
C80 C 1.2562(19) 0.866(3) 0.4301(12) 0.161(13) Uiso 1 1 d . . .
H80A H 1.2991 0.9161 0.4361 0.241 Uiso 1 1 calc R . .
H80B H 1.2836 0.8108 0.4182 0.241 Uiso 1 1 calc R . .
H80C H 1.2352 0.8526 0.4635 0.241 Uiso 1 1 calc R . .
C81 C 1.0485(15) 0.808(2) 0.4263(8) 0.125(12) Uani 1 1 d . . .
H81A H 1.0955 0.7833 0.4541 0.150 Uiso 1 1 calc R . .
H81B H 1.0312 0.8688 0.4383 0.150 Uiso 1 1 calc R . .
C82 C 0.977(2) 0.748(2) 0.4208(12) 0.155(13) Uiso 1 1 d . . .
H82A H 0.9560 0.7439 0.4549 0.233 Uiso 1 1 calc R . .
H82B H 0.9945 0.6870 0.4103 0.233 Uiso 1 1 calc R . .
H82C H 0.9304 0.7721 0.3934 0.233 Uiso 1 1 calc R . .
C83 C 0.9232(8) 0.3887(12) -0.0451(5) 0.039(3) Uani 1 1 d . . .
H83A H 0.8977 0.3266 -0.0430 0.047 Uiso 1 1 calc R . .
H83B H 0.9039 0.4118 -0.0818 0.047 Uiso 1 1 calc R . .
C84 C 1.0201(9) 0.3796(15) -0.0357(6) 0.054(5) Uani 1 1 d . . .
H84A H 1.0373 0.3380 -0.0624 0.081 Uiso 1 1 calc R . .
H84B H 1.0403 0.3547 0.0001 0.081 Uiso 1 1 calc R . .
H84C H 1.0465 0.4403 -0.0387 0.081 Uiso 1 1 calc R . .
C85 C 0.9037(9) 0.5829(12) -0.0163(6) 0.037(4) Uani 1 1 d . . .
H85A H 0.8833 0.6255 0.0094 0.045 Uiso 1 1 calc R . .
H85B H 0.9678 0.5898 -0.0123 0.045 Uiso 1 1 calc R . .
C86 C 0.8610(12) 0.6128(12) -0.0751(6) 0.077(5) Uani 1 1 d . . .
H86A H 0.8774 0.6765 -0.0814 0.115 Uiso 1 1 calc R . .
H86B H 0.7974 0.6082 -0.0792 0.115 Uiso 1 1 calc R . .
H86C H 0.8818 0.5720 -0.1009 0.115 Uiso 1 1 calc R . .
C87 C 0.7613(8) 0.4515(14) -0.0216(7) 0.053(4) Uani 1 1 d . . .
H87A H 0.7475 0.4649 -0.0604 0.063 Uiso 1 1 calc R . .
H87B H 0.7446 0.3867 -0.0163 0.063 Uiso 1 1 calc R . .
C88 C 0.7099(13) 0.5120(18) 0.0064(9) 0.111(8) Uani 1 1 d . . .
H88A H 0.6477 0.5014 -0.0066 0.167 Uiso 1 1 calc R . .
H88B H 0.7243 0.5763 0.0000 0.167 Uiso 1 1 calc R . .
H88C H 0.7232 0.4991 0.0448 0.167 Uiso 1 1 calc R . .
C89 C 1.0818(13) 0.4115(15) 0.2009(7) 0.094(8) Uani 1 1 d . . .
H89A H 1.1042 0.4732 0.1937 0.113 Uiso 1 1 calc R . .
H89B H 1.0966 0.3996 0.2397 0.113 Uiso 1 1 calc R . .
C90 C 1.1258(12) 0.3349(15) 0.1689(9) 0.094(6) Uani 1 1 d . . .
H90A H 1.1893 0.3378 0.1793 0.141 Uiso 1 1 calc R . .
H90B H 1.1097 0.3462 0.1304 0.141 Uiso 1 1 calc R . .
H90C H 1.1052 0.2737 0.1773 0.141 Uiso 1 1 calc R . .
C91 C 0.9247(17) 0.5033(11) 0.2167(7) 0.098(8) Uani 1 1 d . . .
H91A H 0.9457 0.4943 0.2553 0.118 Uiso 1 1 calc R . .
H91B H 0.9494 0.5619 0.2060 0.118 Uiso 1 1 calc R . .
C92 C 0.8242(13) 0.5099(15) 0.2062(10) 0.094(8) Uani 1 1 d . . .
H92A H 0.8060 0.5611 0.2269 0.142 Uiso 1 1 calc R . .
H92B H 0.7996 0.4522 0.2171 0.142 Uiso 1 1 calc R . .
H92C H 0.8034 0.5205 0.1681 0.142 Uiso 1 1 calc R . .
C93 C 0.9300(10) 0.3012(11) 0.2066(6) 0.060(4) Uiso 1 1 d . . .
H93A H 0.8655 0.2986 0.2001 0.072 Uiso 1 1 calc R . .
H93B H 0.9510 0.2494 0.1869 0.072 Uiso 1 1 calc R . .
C94 C 0.9635(13) 0.2863(15) 0.2676(8) 0.097(6) Uiso 1 1 d . . .
H94A H 0.9427 0.2268 0.2786 0.146 Uiso 1 1 calc R . .
H94B H 0.9415 0.3358 0.2879 0.146 Uiso 1 1 calc R . .
H94C H 1.0274 0.2870 0.2747 0.146 Uiso 1 1 calc R . .
C95 C 0.4548(9) 0.4308(13) 0.0865(6) 0.056(4) Uani 1 1 d . . .
H95A H 0.4735 0.3802 0.0650 0.067 Uiso 1 1 calc R . .
H95B H 0.4132 0.4697 0.0623 0.067 Uiso 1 1 calc R . .
C96 C 0.5359(10) 0.4900(11) 0.1092(7) 0.064(5) Uani 1 1 d . . .
H96A H 0.5619 0.5145 0.0797 0.096 Uiso 1 1 calc R . .
H96B H 0.5787 0.4517 0.1322 0.096 Uiso 1 1 calc R . .
H96C H 0.5181 0.5411 0.1301 0.096 Uiso 1 1 calc R . .
C97 C 0.3298(8) 0.4732(11) 0.1551(5) 0.035(3) Uani 1 1 d . . .
H97A H 0.2933 0.4969 0.1222 0.042 Uiso 1 1 calc R . .
H97B H 0.2900 0.4471 0.1778 0.042 Uiso 1 1 calc R . .
C98 C 0.3788(10) 0.5548(11) 0.1850(6) 0.050(4) Uani 1 1 d . . .
H98A H 0.3367 0.6010 0.1926 0.076 Uiso 1 1 calc R . .
H98B H 0.4175 0.5824 0.1628 0.076 Uiso 1 1 calc R . .
H98C H 0.4134 0.5331 0.2186 0.076 Uiso 1 1 calc R . .
C99 C 0.3189(10) 0.2996(13) 0.1002(6) 0.056(5) Uani 1 1 d . . .
H99A H 0.3511 0.2470 0.0882 0.067 Uiso 1 1 calc R . .
H99B H 0.2813 0.2754 0.1246 0.067 Uiso 1 1 calc R . .
C100 C 0.2614(10) 0.3420(11) 0.0518(6) 0.061(5) Uani 1 1 d . . .
H10A H 0.2215 0.2951 0.0338 0.091 Uiso 1 1 calc R . .
H10B H 0.2980 0.3654 0.0270 0.091 Uiso 1 1 calc R . .
H10C H 0.2277 0.3929 0.0634 0.091 Uiso 1 1 calc R . .
C101 C 0.6980(9) 0.2271(14) 0.2587(6) 0.054(5) Uani 1 1 d . . .
H10D H 0.6875 0.1796 0.2304 0.065 Uiso 1 1 calc R . .
H10E H 0.7238 0.2814 0.2436 0.065 Uiso 1 1 calc R . .
C102 C 0.7634(11) 0.1901(16) 0.3045(7) 0.072(6) Uani 1 1 d . . .
H10F H 0.8176 0.1745 0.2918 0.108 Uiso 1 1 calc R . .
H10G H 0.7397 0.1348 0.3188 0.108 Uiso 1 1 calc R . .
H10H H 0.7754 0.2369 0.3325 0.108 Uiso 1 1 calc R . .
C103 C 0.6160(11) 0.3437(13) 0.3296(6) 0.049(5) Uani 1 1 d . . .
H10I H 0.5624 0.3557 0.3445 0.059 Uiso 1 1 calc R . .
H10J H 0.6603 0.3178 0.3584 0.059 Uiso 1 1 calc R . .
C104 C 0.6499(13) 0.4351(18) 0.3099(8) 0.078(6) Uani 1 1 d . . .
H10K H 0.6622 0.4785 0.3398 0.117 Uiso 1 1 calc R . .
H10L H 0.6056 0.4613 0.2819 0.117 Uiso 1 1 calc R . .
H10M H 0.7034 0.4234 0.2956 0.117 Uiso 1 1 calc R . .
C105 C 0.5639(10) 0.1580(13) 0.3089(6) 0.043(4) Uani 1 1 d . . .
H10N H 0.5604 0.1053 0.2840 0.052 Uiso 1 1 calc R . .
H10O H 0.6099 0.1444 0.3400 0.052 Uiso 1 1 calc R . .
C106 C 0.4740(10) 0.1700(14) 0.3283(6) 0.056(5) Uani 1 1 d . . .
H10P H 0.4602 0.1135 0.3463 0.083 Uiso 1 1 calc R . .
H10Q H 0.4282 0.1820 0.2975 0.083 Uiso 1 1 calc R . .
H10R H 0.4776 0.2219 0.3533 0.083 Uiso 1 1 calc R . .
O11 O 1.1397(16) 0.1622(18) 0.2783(10) 0.205(10) Uiso 1 1 d D . .
C107 C 1.275(2) 0.077(2) 0.3158(12) 0.196(15) Uiso 1 1 d D . .
H10S H 1.2537 0.0832 0.3498 0.295 Uiso 1 1 calc R . .
H10T H 1.3311 0.1089 0.3184 0.295 Uiso 1 1 calc R . .
H10U H 1.2819 0.0121 0.3078 0.295 Uiso 1 1 calc R . .
C108 C 1.2097(19) 0.121(2) 0.2718(11) 0.161(12) Uiso 1 1 d D . .
C109 C 1.2494(14) 0.1069(17) 0.2164(8) 0.097(7) Uiso 1 1 d D . .
H10V H 1.2078 0.1309 0.1862 0.146 Uiso 1 1 calc R . .
H10W H 1.2594 0.0412 0.2109 0.146 Uiso 1 1 calc R . .
H10$ H 1.3047 0.1404 0.2192 0.146 Uiso 1 1 calc R . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Pt1 O9 177.0(4) . . ?
C1 Pt1 P1 90.1(3) . . ?
O9 Pt1 P1 87.1(3) . . ?
C1 Pt1 P2 88.3(3) . . ?
O9 Pt1 P2 94.6(2) . . ?
P1 Pt1 P2 173.06(14) . . ?
C10 Pt2 O1 177.4(5) . . ?
C10 Pt2 P4 88.8(3) . . ?
O1 Pt2 P4 92.2(3) . . ?
C10 Pt2 P3 91.4(3) . . ?
O1 Pt2 P3 87.8(3) . . ?
P4 Pt2 P3 174.91(17) . . ?
C30 Pt3 O4 177.1(4) . . ?
C30 Pt3 P5 88.5(3) . . ?
O4 Pt3 P5 94.5(3) . . ?
C30 Pt3 P6 92.5(3) . . ?
O4 Pt3 P6 84.6(3) . . ?
P5 Pt3 P6 176.32(14) . . ?
C39 Pt4 O6 175.5(5) . . ?
C39 Pt4 P7 90.5(4) . . ?
O6 Pt4 P7 93.4(2) . . ?
C39 Pt4 P8 90.4(4) . . ?
O6 Pt4 P8 85.9(2) . . ?
P7 Pt4 P8 174.15(15) . . ?
C59 P1 C61 110.7(8) . . ?
C59 P1 C63 97.2(9) . . ?
C61 P1 C63 101.3(8) . . ?
C59 P1 Pt1 117.4(6) . . ?
C61 P1 Pt1 117.6(5) . . ?
C63 P1 Pt1 109.1(6) . . ?
C67 P2 C65 104.3(7) . . ?
C67 P2 C69 104.7(7) . . ?
C65 P2 C69 104.6(7) . . ?
C67 P2 Pt1 115.9(5) . . ?
C65 P2 Pt1 112.1(5) . . ?
C69 P2 Pt1 114.2(5) . . ?
C71 P3 C73 106.3(9) . . ?
C71 P3 C75 105.1(9) . . ?
C73 P3 C75 102.3(8) . . ?
C71 P3 Pt2 116.3(7) . . ?
C73 P3 Pt2 113.7(5) . . ?
C75 P3 Pt2 111.7(6) . . ?
C79 P4 C77 102.6(8) . . ?
C79 P4 C81 98.1(13) . . ?
C77 P4 C81 111.1(10) . . ?
C79 P4 Pt2 111.5(7) . . ?
C77 P4 Pt2 114.7(6) . . ?
C81 P4 Pt2 116.7(6) . . ?
C85 P5 C83 106.9(7) . . ?
C85 P5 C87 105.2(8) . . ?
C83 P5 C87 101.5(7) . . ?
C85 P5 Pt3 112.6(5) . . ?
C83 P5 Pt3 115.2(5) . . ?
C87 P5 Pt3 114.4(6) . . ?
C93 P6 C91 108.2(8) . . ?
C93 P6 C89 104.5(8) . . ?
C91 P6 C89 103.3(11) . . ?
C93 P6 Pt3 118.2(5) . . ?
C91 P6 Pt3 109.9(7) . . ?
C89 P6 Pt3 111.7(5) . . ?
C97 P7 C95 105.0(7) . . ?
C97 P7 C99 103.7(7) . . ?
C95 P7 C99 105.0(8) . . ?
C97 P7 Pt4 115.5(4) . . ?
C95 P7 Pt4 112.8(5) . . ?
C99 P7 Pt4 113.7(6) . . ?
C103 P8 C105 103.4(8) . . ?
C103 P8 C101 106.6(8) . . ?
C105 P8 C101 101.0(8) . . ?
C103 P8 Pt4 112.4(6) . . ?
C105 P8 Pt4 116.3(5) . . ?
C101 P8 Pt4 115.8(5) . . ?
C15 O1 Pt2 118.5(9) . . ?
C20 O3 C22 117.8(11) . . ?
C29 O4 Pt3 119.4(8) . . ?
C44 O6 Pt4 120.2(8) . . ?
C47 O8 C51 119.1(10) . . ?
C58 O9 Pt1 119.7(8) . . ?
C14 C1 C2 113.8(11) . . ?
C14 C1 Pt1 125.4(9) . . ?
C2 C1 Pt1 120.7(7) . . ?
C3 C2 C1 122.9(10) . . ?
C2 C3 C4 121.9(12) . . ?
C3 C4 C13 118.6(12) . . ?
C3 C4 C5 122.4(12) . . ?
C13 C4 C5 118.9(11) . . ?
C6 C5 C4 121.9(13) . . ?
C5 C6 C7 120.5(14) . . ?
C8 C7 C12 118.8(13) . . ?
C8 C7 C6 121.6(13) . . ?
C12 C7 C6 119.4(11) . . ?
C9 C8 C7 121.9(13) . . ?
C8 C9 C10 120.9(12) . . ?
C11 C10 C9 116.9(12) . . ?
C11 C10 Pt2 123.9(10) . . ?
C9 C10 Pt2 118.8(9) . . ?
C10 C11 C12 122.9(12) . . ?
C7 C12 C11 118.5(11) . . ?
C7 C12 C13 120.0(11) . . ?
C11 C12 C13 121.5(12) . . ?
C14 C13 C4 116.5(10) . . ?
C14 C13 C12 124.5(11) . . ?
C4 C13 C12 119.1(11) . . ?
C1 C14 C13 126.0(11) . . ?
O2 C15 O1 127.7(12) . . ?
O2 C15 C16 117.9(11) . . ?
O1 C15 C16 114.4(11) . . ?
C17 C16 C21 119.5(12) . . ?
C17 C16 C15 120.7(10) . . ?
C21 C16 C15 119.8(12) . . ?
C18 C17 C16 120.0(11) . . ?
C17 C18 C19 120.6(11) . . ?
C17 C18 C29 120.3(10) . . ?
C19 C18 C29 119.1(11) . . ?
C20 C19 C18 120.6(12) . . ?
O3 C20 C19 126.2(13) . . ?
O3 C20 C21 113.9(12) . . ?
C19 C20 C21 119.9(11) . . ?
C16 C21 C20 119.3(12) . . ?
O3 C22 C23 109.8(11) . . ?
C24 C23 C28 119.6(12) . . ?
C24 C23 C22 119.9(12) . . ?
C28 C23 C22 119.7(11) . . ?
C23 C24 C25 119.7(14) . . ?
C26 C25 C24 122.2(14) . . ?
C27 C26 C25 117.6(14) . . ?
C26 C27 C28 121.6(16) . . ?
C23 C28 C27 118.8(14) . . ?
O5 C29 O4 126.0(12) . . ?
O5 C29 C18 119.1(10) . . ?
O4 C29 C18 114.8(11) . . ?
C43 C30 C31 120.3(13) . . ?
C43 C30 Pt3 122.0(10) . . ?
C31 C30 Pt3 117.6(8) . . ?
C32 C31 C30 121.0(11) . . ?
C31 C32 C33 119.1(13) . . ?
C34 C33 C42 120.8(12) . . ?
C34 C33 C32 119.5(13) . . ?
C42 C33 C32 119.7(13) . . ?
C35 C34 C33 120.8(13) . . ?
C34 C35 C36 121.9(12) . . ?
C37 C36 C41 120.4(12) . . ?
C37 C36 C35 120.9(12) . . ?
C41 C36 C35 118.6(11) . . ?
C36 C37 C38 119.0(13) . . ?
C37 C38 C39 122.7(11) . . ?
C40 C39 C38 116.0(12) . . ?
C40 C39 Pt4 125.6(10) . . ?
C38 C39 Pt4 118.3(9) . . ?
C39 C40 C41 124.3(12) . . ?
C40 C41 C36 117.4(11) . . ?
C40 C41 C42 123.1(11) . . ?
C36 C41 C42 119.4(11) . . ?
C43 C42 C33 118.2(11) . . ?
C43 C42 C41 123.6(11) . . ?
C33 C42 C41 118.2(12) . . ?
C30 C43 C42 121.5(12) . . ?
O7 C44 O6 125.3(12) . . ?
O7 C44 C45 121.3(10) . . ?
O6 C44 C45 113.4(11) . . ?
C50 C45 C46 121.9(11) . . ?
C50 C45 C44 120.6(10) . . ?
C46 C45 C44 117.5(11) . . ?
C45 C46 C47 118.7(11) . . ?
C46 C47 O8 115.3(11) . . ?
C46 C47 C48 120.5(11) . . ?
O8 C47 C48 124.2(10) . . ?
C49 C48 C47 119.0(12) . . ?
C48 C49 C50 119.9(12) . . ?
C48 C49 C58 118.5(12) . . ?
C50 C49 C58 121.4(11) . . ?
C45 C50 C49 119.9(10) . . ?
O8 C51 C52 109.5(10) . . ?
C57 C52 C53 116.9(12) . . ?
C57 C52 C51 122.7(12) . . ?
C53 C52 C51 120.3(12) . . ?
C54 C53 C52 122.2(14) . . ?
C55 C54 C53 119.7(15) . . ?
C54 C55 C56 120.0(13) . . ?
C57 C56 C55 118.5(15) . . ?
C56 C57 C52 122.4(15) . . ?
O10 C58 O9 125.1(12) . . ?
O10 C58 C49 120.1(11) . . ?
O9 C58 C49 114.8(11) . . ?
C60 C59 P1 116.6(14) . . ?
C62 C61 P1 107.1(12) . . ?
C64 C63 P1 113.5(15) . . ?
C66 C65 P2 117.5(11) . . ?
C68 C67 P2 113.9(9) . . ?
C70 C69 P2 112.3(10) . . ?
C72 C71 P3 112.7(15) . . ?
C74 C73 P3 116.6(11) . . ?
C76 C75 P3 113.3(12) . . ?
C78 C77 P4 116.4(14) . . ?
C80 C79 P4 122(2) . . ?
C82 C81 P4 112(2) . . ?
C84 C83 P5 115.6(10) . . ?
C86 C85 P5 114.4(11) . . ?
C88 C87 P5 112.6(14) . . ?
C90 C89 P6 109.2(13) . . ?
C92 C91 P6 111.7(13) . . ?
C94 C93 P6 115.3(13) . . ?
C96 C95 P7 114.9(11) . . ?
C98 C97 P7 115.8(9) . . ?
C100 C99 P7 113.7(14) . . ?
C102 C101 P8 115.0(11) . . ?
C104 C103 P8 111.1(11) . . ?
C106 C105 P8 111.0(12) . . ?
O11 C108 C107 125(3) . . ?
O11 C108 C109 128(3) . . ?
C107 C108 C109 106(2) . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C1 1.971(12) . ?
Pt1 O9 2.133(8) . ?
Pt1 P1 2.289(4) . ?
Pt1 P2 2.299(4) . ?
Pt2 C10 2.028(12) . ?
Pt2 O1 2.111(9) . ?
Pt2 P4 2.288(4) . ?
Pt2 P3 2.302(3) . ?
Pt3 C30 2.058(14) . ?
Pt3 O4 2.119(9) . ?
Pt3 P5 2.287(4) . ?
Pt3 P6 2.290(3) . ?
Pt4 C39 2.004(12) . ?
Pt4 O6 2.110(8) . ?
Pt4 P7 2.292(3) . ?
Pt4 P8 2.298(3) . ?
P1 C59 1.77(2) . ?
P1 C61 1.814(14) . ?
P1 C63 1.864(19) . ?
P2 C67 1.815(14) . ?
P2 C65 1.826(14) . ?
P2 C69 1.828(16) . ?
P3 C71 1.81(2) . ?
P3 C73 1.809(16) . ?
P3 C75 1.850(16) . ?
P4 C79 1.78(2) . ?
P4 C77 1.793(17) . ?
P4 C81 1.83(2) . ?
P5 C85 1.830(17) . ?
P5 C83 1.831(16) . ?
P5 C87 1.835(13) . ?
P6 C93 1.808(16) . ?
P6 C91 1.831(17) . ?
P6 C89 1.83(2) . ?
P7 C97 1.816(14) . ?
P7 C95 1.833(14) . ?
P7 C99 1.835(16) . ?
P8 C103 1.806(17) . ?
P8 C105 1.809(17) . ?
P8 C101 1.839(14) . ?
O1 C15 1.260(15) . ?
O2 C15 1.245(17) . ?
O3 C20 1.357(14) . ?
O3 C22 1.416(16) . ?
O4 C29 1.297(13) . ?
O5 C29 1.230(16) . ?
O6 C44 1.293(13) . ?
O7 C44 1.237(16) . ?
O8 C47 1.390(13) . ?
O8 C51 1.414(14) . ?
O9 C58 1.280(13) . ?
O10 C58 1.254(15) . ?
C1 C14 1.399(14) . ?
C1 C2 1.429(17) . ?
C2 C3 1.374(18) . ?
C3 C4 1.402(16) . ?
C4 C13 1.434(18) . ?
C4 C5 1.461(19) . ?
C5 C6 1.325(17) . ?
C6 C7 1.477(19) . ?
C7 C8 1.401(17) . ?
C7 C12 1.409(19) . ?
C8 C9 1.363(19) . ?
C9 C10 1.431(19) . ?
C10 C11 1.385(16) . ?
C11 C12 1.411(17) . ?
C12 C13 1.446(15) . ?
C13 C14 1.425(17) . ?
C15 C16 1.509(18) . ?
C16 C17 1.402(19) . ?
C16 C21 1.412(16) . ?
C17 C18 1.386(18) . ?
C18 C19 1.401(15) . ?
C18 C29 1.541(17) . ?
C19 C20 1.364(19) . ?
C20 C21 1.428(19) . ?
C22 C23 1.515(16) . ?
C23 C24 1.339(19) . ?
C23 C28 1.360(19) . ?
C24 C25 1.404(18) . ?
C25 C26 1.35(2) . ?
C26 C27 1.33(2) . ?
C27 C28 1.44(2) . ?
C30 C43 1.360(15) . ?
C30 C31 1.405(18) . ?
C31 C32 1.38(2) . ?
C32 C33 1.435(16) . ?
C33 C34 1.41(2) . ?
C33 C42 1.420(18) . ?
C34 C35 1.349(18) . ?
C35 C36 1.432(18) . ?
C36 C37 1.387(17) . ?
C36 C41 1.431(17) . ?
C37 C38 1.40(2) . ?
C38 C39 1.419(19) . ?
C39 C40 1.371(15) . ?
C40 C41 1.406(17) . ?
C41 C42 1.456(16) . ?
C42 C43 1.416(19) . ?
C44 C45 1.535(17) . ?
C45 C50 1.367(17) . ?
C45 C46 1.381(14) . ?
C46 C47 1.383(16) . ?
C47 C48 1.414(17) . ?
C48 C49 1.390(16) . ?
C49 C50 1.390(18) . ?
C49 C58 1.476(19) . ?
C51 C52 1.504(16) . ?
C52 C57 1.37(2) . ?
C52 C53 1.378(19) . ?
C53 C54 1.375(18) . ?
C54 C55 1.34(2) . ?
C55 C56 1.41(2) . ?
C56 C57 1.364(19) . ?
C59 C60 1.55(2) . ?
C61 C62 1.50(2) . ?
C63 C64 1.46(3) . ?
C65 C66 1.529(18) . ?
C67 C68 1.528(17) . ?
C69 C70 1.53(2) . ?
C71 C72 1.52(2) . ?
C73 C74 1.55(2) . ?
C75 C76 1.52(3) . ?
C77 C78 1.53(3) . ?
C79 C80 1.55(3) . ?
C81 C82 1.40(4) . ?
C83 C84 1.493(18) . ?
C85 C86 1.59(2) . ?
C87 C88 1.46(3) . ?
C89 C90 1.60(3) . ?
C91 C92 1.54(3) . ?
C93 C94 1.56(2) . ?
C95 C96 1.55(2) . ?
C97 C98 1.54(2) . ?
C99 C100 1.52(2) . ?
C101 C102 1.51(2) . ?
C103 C104 1.54(3) . ?
C105 C106 1.57(2) . ?
O11 C108 1.281(17) . ?
C107 C108 1.511(18) . ?
C108 C109 1.645(17) . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1 Pt1 P1 C59 -33.4(8) . . . . ?
O9 Pt1 P1 C59 145.6(8) . . . . ?
P2 Pt1 P1 C59 -109.9(14) . . . . ?
C1 Pt1 P1 C61 -169.5(7) . . . . ?
O9 Pt1 P1 C61 9.5(7) . . . . ?
P2 Pt1 P1 C61 114.0(13) . . . . ?
C1 Pt1 P1 C63 75.8(8) . . . . ?
O9 Pt1 P1 C63 -105.1(7) . . . . ?
P2 Pt1 P1 C63 -0.6(15) . . . . ?
C1 Pt1 P2 C67 64.3(6) . . . . ?
O9 Pt1 P2 C67 -115.1(6) . . . . ?
P1 Pt1 P2 C67 140.8(12) . . . . ?
C1 Pt1 P2 C65 -55.2(7) . . . . ?
O9 Pt1 P2 C65 125.4(6) . . . . ?
P1 Pt1 P2 C65 21.3(14) . . . . ?
C1 Pt1 P2 C69 -173.9(6) . . . . ?
O9 Pt1 P2 C69 6.7(6) . . . . ?
P1 Pt1 P2 C69 -97.4(13) . . . . ?
C10 Pt2 P3 C71 81.1(9) . . . . ?
O1 Pt2 P3 C71 -96.4(8) . . . . ?
P4 Pt2 P3 C71 173.8(17) . . . . ?
C10 Pt2 P3 C73 -43.0(9) . . . . ?
O1 Pt2 P3 C73 139.5(8) . . . . ?
P4 Pt2 P3 C73 50(2) . . . . ?
C10 Pt2 P3 C75 -158.3(7) . . . . ?
O1 Pt2 P3 C75 24.3(6) . . . . ?
P4 Pt2 P3 C75 -65.6(18) . . . . ?
C10 Pt2 P4 C79 -76.6(10) . . . . ?
O1 Pt2 P4 C79 100.9(9) . . . . ?
P3 Pt2 P4 C79 -169.4(18) . . . . ?
C10 Pt2 P4 C77 167.3(7) . . . . ?
O1 Pt2 P4 C77 -15.1(7) . . . . ?
P3 Pt2 P4 C77 74.5(18) . . . . ?
C10 Pt2 P4 C81 34.9(13) . . . . ?
O1 Pt2 P4 C81 -147.5(12) . . . . ?
P3 Pt2 P4 C81 -58(2) . . . . ?
C30 Pt3 P5 C85 171.4(6) . . . . ?
O4 Pt3 P5 C85 -8.5(6) . . . . ?
P6 Pt3 P5 C85 66(2) . . . . ?
C30 Pt3 P5 C83 -65.7(6) . . . . ?
O4 Pt3 P5 C83 114.4(5) . . . . ?
P6 Pt3 P5 C83 -171(2) . . . . ?
C30 Pt3 P5 C87 51.4(8) . . . . ?
O4 Pt3 P5 C87 -128.5(7) . . . . ?
P6 Pt3 P5 C87 -54(2) . . . . ?
C30 Pt3 P6 C93 1.2(7) . . . . ?
O4 Pt3 P6 C93 -178.7(6) . . . . ?
P5 Pt3 P6 C93 106(2) . . . . ?
C30 Pt3 P6 C91 -123.5(8) . . . . ?
O4 Pt3 P6 C91 56.6(8) . . . . ?
P5 Pt3 P6 C91 -18(2) . . . . ?
C30 Pt3 P6 C89 122.5(9) . . . . ?
O4 Pt3 P6 C89 -57.4(8) . . . . ?
P5 Pt3 P6 C89 -132(2) . . . . ?
C39 Pt4 P7 C97 -176.4(6) . . . . ?
O6 Pt4 P7 C97 5.8(6) . . . . ?
P8 Pt4 P7 C97 -77.8(13) . . . . ?
C39 Pt4 P7 C95 -55.6(8) . . . . ?
O6 Pt4 P7 C95 126.6(7) . . . . ?
P8 Pt4 P7 C95 43.0(15) . . . . ?
C39 Pt4 P7 C99 63.8(7) . . . . ?
O6 Pt4 P7 C99 -114.0(7) . . . . ?
P8 Pt4 P7 C99 162.5(13) . . . . ?
C39 Pt4 P8 C103 152.8(7) . . . . ?
O6 Pt4 P8 C103 -29.9(7) . . . . ?
P7 Pt4 P8 C103 54.1(14) . . . . ?
C39 Pt4 P8 C105 -88.4(7) . . . . ?
O6 Pt4 P8 C105 89.0(7) . . . . ?
P7 Pt4 P8 C105 173.0(13) . . . . ?
C39 Pt4 P8 C101 29.9(8) . . . . ?
O6 Pt4 P8 C101 -152.7(8) . . . . ?
P7 Pt4 P8 C101 -68.7(15) . . . . ?
C10 Pt2 O1 C15 32(9) . . . . ?
P4 Pt2 O1 C15 -79.8(10) . . . . ?
P3 Pt2 O1 C15 105.3(9) . . . . ?
C30 Pt3 O4 C29 106(8) . . . . ?
P5 Pt3 O4 C29 -75.0(8) . . . . ?
P6 Pt3 O4 C29 108.6(8) . . . . ?
C39 Pt4 O6 C44 -75(5) . . . . ?
P7 Pt4 O6 C44 74.8(9) . . . . ?
P8 Pt4 O6 C44 -111.0(9) . . . . ?
C1 Pt1 O9 C58 -89(7) . . . . ?
P1 Pt1 O9 C58 -108.6(9) . . . . ?
P2 Pt1 O9 C58 78.2(9) . . . . ?
O9 Pt1 C1 C14 -100(7) . . . . ?
P1 Pt1 C1 C14 -80.8(10) . . . . ?
P2 Pt1 C1 C14 92.5(10) . . . . ?
O9 Pt1 C1 C2 82(7) . . . . ?
P1 Pt1 C1 C2 101.8(9) . . . . ?
P2 Pt1 C1 C2 -84.9(9) . . . . ?
C14 C1 C2 C3 -3.1(18) . . . . ?
Pt1 C1 C2 C3 174.6(10) . . . . ?
C1 C2 C3 C4 2(2) . . . . ?
C2 C3 C4 C13 3.1(19) . . . . ?
C2 C3 C4 C5 179.4(13) . . . . ?
C3 C4 C5 C6 -178.2(13) . . . . ?
C13 C4 C5 C6 -2(2) . . . . ?
C4 C5 C6 C7 4(2) . . . . ?
C5 C6 C7 C8 173.0(14) . . . . ?
C5 C6 C7 C12 -2(2) . . . . ?
C12 C7 C8 C9 -1(2) . . . . ?
C6 C7 C8 C9 -176.0(13) . . . . ?
C7 C8 C9 C10 -1(2) . . . . ?
C8 C9 C10 C11 0.9(19) . . . . ?
C8 C9 C10 Pt2 173.9(10) . . . . ?
O1 Pt2 C10 C11 149(8) . . . . ?
P4 Pt2 C10 C11 -99.0(10) . . . . ?
P3 Pt2 C10 C11 75.9(10) . . . . ?
O1 Pt2 C10 C9 -23(9) . . . . ?
P4 Pt2 C10 C9 88.6(9) . . . . ?
P3 Pt2 C10 C9 -96.5(9) . . . . ?
C9 C10 C11 C12 0.8(17) . . . . ?
Pt2 C10 C11 C12 -171.8(9) . . . . ?
C8 C7 C12 C11 2.2(18) . . . . ?
C6 C7 C12 C11 177.8(11) . . . . ?
C8 C7 C12 C13 -176.9(12) . . . . ?
C6 C7 C12 C13 -1.3(18) . . . . ?
C10 C11 C12 C7 -2.3(18) . . . . ?
C10 C11 C12 C13 176.8(11) . . . . ?
C3 C4 C13 C14 -6.7(18) . . . . ?
C5 C4 C13 C14 176.8(12) . . . . ?
C3 C4 C13 C12 174.6(11) . . . . ?
C5 C4 C13 C12 -1.9(18) . . . . ?
C7 C12 C13 C14 -175.2(12) . . . . ?
C11 C12 C13 C14 5.7(18) . . . . ?
C7 C12 C13 C4 3.4(17) . . . . ?
C11 C12 C13 C4 -175.7(11) . . . . ?
C2 C1 C14 C13 -1.1(18) . . . . ?
Pt1 C1 C14 C13 -178.7(9) . . . . ?
C4 C13 C14 C1 5.9(19) . . . . ?
C12 C13 C14 C1 -175.4(11) . . . . ?
Pt2 O1 C15 O2 5.7(19) . . . . ?
Pt2 O1 C15 C16 -173.4(8) . . . . ?
O2 C15 C16 C17 -177.7(12) . . . . ?
O1 C15 C16 C17 1.5(18) . . . . ?
O2 C15 C16 C21 3.2(19) . . . . ?
O1 C15 C16 C21 -177.6(12) . . . . ?
C21 C16 C17 C18 0.1(19) . . . . ?
C15 C16 C17 C18 -179.0(12) . . . . ?
C16 C17 C18 C19 -2.0(19) . . . . ?
C16 C17 C18 C29 175.8(11) . . . . ?
C17 C18 C19 C20 2.9(19) . . . . ?
C29 C18 C19 C20 -174.9(11) . . . . ?
C22 O3 C20 C19 -2(2) . . . . ?
C22 O3 C20 C21 177.7(11) . . . . ?
C18 C19 C20 O3 177.6(12) . . . . ?
C18 C19 C20 C21 -1.8(19) . . . . ?
C17 C16 C21 C20 0.9(19) . . . . ?
C15 C16 C21 C20 -179.9(12) . . . . ?
O3 C20 C21 C16 -179.6(11) . . . . ?
C19 C20 C21 C16 -0.1(19) . . . . ?
C20 O3 C22 C23 -164.2(11) . . . . ?
O3 C22 C23 C24 -160.6(15) . . . . ?
O3 C22 C23 C28 30(2) . . . . ?
C28 C23 C24 C25 -6(3) . . . . ?
C22 C23 C24 C25 -176.0(16) . . . . ?
C23 C24 C25 C26 3(3) . . . . ?
C24 C25 C26 C27 3(3) . . . . ?
C25 C26 C27 C28 -6(3) . . . . ?
C24 C23 C28 C27 3(3) . . . . ?
C22 C23 C28 C27 173.0(17) . . . . ?
C26 C27 C28 C23 3(3) . . . . ?
Pt3 O4 C29 O5 10.2(17) . . . . ?
Pt3 O4 C29 C18 -166.8(8) . . . . ?
C17 C18 C29 O5 -169.5(12) . . . . ?
C19 C18 C29 O5 8.4(18) . . . . ?
C17 C18 C29 O4 7.7(17) . . . . ?
C19 C18 C29 O4 -174.4(11) . . . . ?
O4 Pt3 C30 C43 76(8) . . . . ?
P5 Pt3 C30 C43 -103.1(10) . . . . ?
P6 Pt3 C30 C43 73.3(10) . . . . ?
O4 Pt3 C30 C31 -102(8) . . . . ?
P5 Pt3 C30 C31 79.3(9) . . . . ?
P6 Pt3 C30 C31 -104.2(9) . . . . ?
C43 C30 C31 C32 3.8(19) . . . . ?
Pt3 C30 C31 C32 -178.6(9) . . . . ?
C30 C31 C32 C33 -0.9(19) . . . . ?
C31 C32 C33 C34 177.3(12) . . . . ?
C31 C32 C33 C42 -2.5(18) . . . . ?
C42 C33 C34 C35 -1(2) . . . . ?
C32 C33 C34 C35 178.9(12) . . . . ?
C33 C34 C35 C36 -3(2) . . . . ?
C34 C35 C36 C37 -173.5(13) . . . . ?
C34 C35 C36 C41 5(2) . . . . ?
C41 C36 C37 C38 -1(2) . . . . ?
C35 C36 C37 C38 176.6(12) . . . . ?
C36 C37 C38 C39 -2(2) . . . . ?
C37 C38 C39 C40 5.4(19) . . . . ?
C37 C38 C39 Pt4 -173.7(10) . . . . ?
O6 Pt4 C39 C40 -116(5) . . . . ?
P7 Pt4 C39 C40 94.1(11) . . . . ?
P8 Pt4 C39 C40 -80.1(11) . . . . ?
O6 Pt4 C39 C38 63(5) . . . . ?
P7 Pt4 C39 C38 -87.0(10) . . . . ?
P8 Pt4 C39 C38 98.8(10) . . . . ?
C38 C39 C40 C41 -5.7(18) . . . . ?
Pt4 C39 C40 C41 173.2(9) . . . . ?
C39 C40 C41 C36 2.6(18) . . . . ?
C39 C40 C41 C42 -173.0(11) . . . . ?
C37 C36 C41 C40 1.2(18) . . . . ?
C35 C36 C41 C40 -176.9(11) . . . . ?
C37 C36 C41 C42 177.0(12) . . . . ?
C35 C36 C41 C42 -1.2(18) . . . . ?
C34 C33 C42 C43 -176.8(12) . . . . ?
C32 C33 C42 C43 3.1(18) . . . . ?
C34 C33 C42 C41 4.5(18) . . . . ?
C32 C33 C42 C41 -175.7(11) . . . . ?
C40 C41 C42 C43 -6.4(19) . . . . ?
C36 C41 C42 C43 178.1(11) . . . . ?
C40 C41 C42 C33 172.3(11) . . . . ?
C36 C41 C42 C33 -3.2(17) . . . . ?
C31 C30 C43 C42 -3.2(19) . . . . ?
Pt3 C30 C43 C42 179.3(9) . . . . ?
C33 C42 C43 C30 -0.2(18) . . . . ?
C41 C42 C43 C30 178.5(11) . . . . ?
Pt4 O6 C44 O7 -6.0(18) . . . . ?
Pt4 O6 C44 C45 175.5(7) . . . . ?
O7 C44 C45 C50 -175.1(12) . . . . ?
O6 C44 C45 C50 3.4(17) . . . . ?
O7 C44 C45 C46 5.6(18) . . . . ?
O6 C44 C45 C46 -175.9(11) . . . . ?
C50 C45 C46 C47 1.7(17) . . . . ?
C44 C45 C46 C47 -179.0(11) . . . . ?
C45 C46 C47 O8 178.8(10) . . . . ?
C45 C46 C47 C48 -1.2(17) . . . . ?
C51 O8 C47 C46 -178.8(11) . . . . ?
C51 O8 C47 C48 1.2(18) . . . . ?
C46 C47 C48 C49 0.3(18) . . . . ?
O8 C47 C48 C49 -179.7(11) . . . . ?
C47 C48 C49 C50 0.2(18) . . . . ?
C47 C48 C49 C58 174.6(11) . . . . ?
C46 C45 C50 C49 -1.2(18) . . . . ?
C44 C45 C50 C49 179.5(11) . . . . ?
C48 C49 C50 C45 0.2(18) . . . . ?
C58 C49 C50 C45 -173.9(11) . . . . ?
C47 O8 C51 C52 162.5(11) . . . . ?
O8 C51 C52 C57 -7(2) . . . . ?
O8 C51 C52 C53 176.4(14) . . . . ?
C57 C52 C53 C54 -2(3) . . . . ?
C51 C52 C53 C54 174.6(15) . . . . ?
C52 C53 C54 C55 1(3) . . . . ?
C53 C54 C55 C56 3(3) . . . . ?
C54 C55 C56 C57 -6(4) . . . . ?
C55 C56 C57 C52 6(4) . . . . ?
C53 C52 C57 C56 -2(3) . . . . ?
C51 C52 C57 C56 -178.0(19) . . . . ?
Pt1 O9 C58 O10 -10.5(17) . . . . ?
Pt1 O9 C58 C49 168.3(8) . . . . ?
C48 C49 C58 O10 -2.2(18) . . . . ?
C50 C49 C58 O10 172.1(11) . . . . ?
C48 C49 C58 O9 179.0(11) . . . . ?
C50 C49 C58 O9 -6.8(17) . . . . ?
C61 P1 C59 C60 -42.5(17) . . . . ?
C63 P1 C59 C60 62.6(15) . . . . ?
Pt1 P1 C59 C60 178.5(11) . . . . ?
C59 P1 C61 C62 -65.5(12) . . . . ?
C63 P1 C61 C62 -167.9(12) . . . . ?
Pt1 P1 C61 C62 73.3(12) . . . . ?
C59 P1 C63 C64 179(2) . . . . ?
C61 P1 C63 C64 -68(2) . . . . ?
Pt1 P1 C63 C64 56(2) . . . . ?
C67 P2 C65 C66 60.3(14) . . . . ?
C69 P2 C65 C66 -49.4(14) . . . . ?
Pt1 P2 C65 C66 -173.6(10) . . . . ?
C65 P2 C67 C68 174.7(11) . . . . ?
C69 P2 C67 C68 -75.7(12) . . . . ?
Pt1 P2 C67 C68 51.0(12) . . . . ?
C67 P2 C69 C70 -170.9(9) . . . . ?
C65 P2 C69 C70 -61.5(11) . . . . ?
Pt1 P2 C69 C70 61.4(10) . . . . ?
C73 P3 C71 C72 -169.9(14) . . . . ?
C75 P3 C71 C72 -61.9(16) . . . . ?
Pt2 P3 C71 C72 62.3(16) . . . . ?
C71 P3 C73 C74 51.0(19) . . . . ?
C75 P3 C73 C74 -59.0(18) . . . . ?
Pt2 P3 C73 C74 -179.6(14) . . . . ?
C71 P3 C75 C76 -175.6(12) . . . . ?
C73 P3 C75 C76 -64.6(13) . . . . ?
Pt2 P3 C75 C76 57.4(12) . . . . ?
C79 P4 C77 C78 -175.0(16) . . . . ?
C81 P4 C77 C78 81.1(18) . . . . ?
Pt2 P4 C77 C78 -53.9(16) . . . . ?
C77 P4 C79 C80 -50(2) . . . . ?
C81 P4 C79 C80 63(2) . . . . ?
Pt2 P4 C79 C80 -173.6(19) . . . . ?
C79 P4 C81 C82 -179(2) . . . . ?
C77 P4 C81 C82 -72(2) . . . . ?
Pt2 P4 C81 C82 62(2) . . . . ?
C85 P5 C83 C84 72.9(14) . . . . ?
C87 P5 C83 C84 -177.2(13) . . . . ?
Pt3 P5 C83 C84 -53.1(14) . . . . ?
C83 P5 C85 C86 61.4(12) . . . . ?
C87 P5 C85 C86 -46.0(12) . . . . ?
Pt3 P5 C85 C86 -171.1(9) . . . . ?
C85 P5 C87 C88 -63.9(16) . . . . ?
C83 P5 C87 C88 -175.2(15) . . . . ?
Pt3 P5 C87 C88 60.2(16) . . . . ?
C93 P6 C89 C90 70.2(12) . . . . ?
C91 P6 C89 C90 -176.7(12) . . . . ?
Pt3 P6 C89 C90 -58.7(12) . . . . ?
C93 P6 C91 C92 -67.1(16) . . . . ?
C89 P6 C91 C92 -177.4(14) . . . . ?
Pt3 P6 C91 C92 63.3(15) . . . . ?
C91 P6 C93 C94 -57.9(16) . . . . ?
C89 P6 C93 C94 51.7(15) . . . . ?
Pt3 P6 C93 C94 176.5(11) . . . . ?
C97 P7 C95 C96 80.7(12) . . . . ?
C99 P7 C95 C96 -170.2(11) . . . . ?
Pt4 P7 C95 C96 -45.9(13) . . . . ?
C95 P7 C97 C98 -67.5(12) . . . . ?
C99 P7 C97 C98 -177.5(11) . . . . ?
Pt4 P7 C97 C98 57.4(12) . . . . ?
C97 P7 C99 C100 57.7(14) . . . . ?
C95 P7 C99 C100 -52.3(14) . . . . ?
Pt4 P7 C99 C100 -176.1(10) . . . . ?
C103 P8 C101 C102 55.6(17) . . . . ?
C105 P8 C101 C102 -52.1(17) . . . . ?
Pt4 P8 C101 C102 -178.5(13) . . . . ?
C105 P8 C103 C104 175.0(13) . . . . ?
C101 P8 C103 C104 69.0(14) . . . . ?
Pt4 P8 C103 C104 -58.8(14) . . . . ?
C103 P8 C105 C106 69.4(13) . . . . ?
C101 P8 C105 C106 179.7(12) . . . . ?
Pt4 P8 C105 C106 -54.2(13) . . . . ?
