#------------------------------------------------------------------------------
#$Date: 2016-03-21 03:15:31 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178427 $
#$URL: svn://www.crystallography.net/cod/cif/4/02/48/4024852.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4024852
loop_
_publ_author_name
'Hai-Bo Yang'
'Brian H. Northrop'
'Yao-Rong Zheng'
'Koushik Ghosh'
'Peter J. Stang'
_publ_section_title
;
Facile Self-Assembly of Neutral Dendritic Metallocycles via
Oxygen-to-Platinum Coordination
;
_journal_name_full               'Journal of Organic Chemistry'
_journal_page_first              7067
_journal_page_last               7074
_journal_paper_doi               10.1021/jo9013589
_journal_volume                  74
_journal_year                    2009
_chemical_formula_moiety         'C134 H180 O14 P8 Pt4,3(C3 H6 O)'
_chemical_formula_sum            'C143 H198 O17 P8 Pt4'
_chemical_formula_weight         3217.13
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                81.5975(8)
_cell_angle_beta                 81.9972(7)
_cell_angle_gamma                72.5629(8)
_cell_formula_units_Z            2
_cell_length_a                   15.6185(2)
_cell_length_b                   16.1923(2)
_cell_length_c                   29.9377(4)
_cell_measurement_reflns_used    185545
_cell_measurement_temperature    150(1)
_cell_measurement_theta_max      25.35
_cell_measurement_theta_min      1.018
_cell_volume                     7109.15(16)
_computing_cell_refinement       DENZO-SMN
_computing_data_collection       'Nonius COLLECT'
_computing_data_reduction        DENZO-SMN
_computing_molecular_graphics    'WinGX, Ortep3'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    SIR97
_diffrn_ambient_temperature      150(1)
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Nonius KappaCCD Diffractometer'
_diffrn_measurement_method       'Phi and Omega scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0546
_diffrn_reflns_av_sigmaI/netI    0.1023
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       36
_diffrn_reflns_limit_l_min       -33
_diffrn_reflns_number            40885
_diffrn_reflns_theta_full        25.35
_diffrn_reflns_theta_max         25.35
_diffrn_reflns_theta_min         1.43
_exptl_absorpt_coefficient_mu    4.074
_exptl_absorpt_correction_T_max  0.6195
_exptl_absorpt_correction_T_min  0.3950
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'DENZO-SMN (Otwinowski & Minor, 1997)'
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.503
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             3248
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.23
_exptl_crystal_size_min          0.13
_refine_diff_density_max         1.967
_refine_diff_density_min         -1.398
_refine_diff_density_rms         0.162
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.040
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1380
_refine_ls_number_reflns         25919
_refine_ls_number_restraints     25
_refine_ls_restrained_S_all      1.041
_refine_ls_R_factor_all          0.1530
_refine_ls_R_factor_gt           0.0788
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0438P)²+95.4995P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1488
_refine_ls_wR_factor_ref         0.1801
_reflns_number_gt                15194
_reflns_number_total             25919
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            jo9013589_si_003.cif
_cod_data_source_block           pjs235
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan' changed
to 'multi-scan' according to
'/home/saulius/struct/CIF-dictionaries/cif_core.dic' dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4024852
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.90228(4) 0.29486(3) 0.415893(16) 0.02968(15) Uani 0.90 1 d P A 1
Pt2 Pt 1.21231(7) 0.17164(6) 0.18630(3) 0.0407(3) Uani 0.90 1 d P A 1
Pt3 Pt 1.06628(5) 0.69928(3) 0.07367(2) 0.04324(19) Uani 0.90 1 d P A 1
Pt4 Pt 0.77504(5) 0.82201(4) 0.30649(2) 0.03936(19) Uani 0.90 1 d P A 1
Pt1A Pt 0.9450(4) 0.3034(3) 0.43008(18) 0.0363(12) Uiso 0.10 1 d P B 2
Pt3A Pt 1.1064(4) 0.7040(3) 0.08491(17) 0.0259(14) Uiso 0.10 1 d P C 2
Pt4A Pt 0.8023(5) 0.8232(5) 0.3178(2) 0.036(2) Uiso 0.10 1 d P D 2
Pt2A Pt 1.2285(7) 0.1811(6) 0.1936(3) 0.029(2) Uiso 0.10 1 d P E 2
P1 P 0.7889(3) 0.2728(3) 0.3823(2) 0.0867(16) Uani 1 1 d . A 1
P2 P 1.0200(3) 0.3113(2) 0.44686(12) 0.0541(10) Uani 1 1 d . A 1
P3 P 1.0944(3) 0.1478(3) 0.16019(15) 0.0801(14) Uani 1 1 d . A 1
P4 P 1.3344(3) 0.1964(3) 0.21310(13) 0.0701(12) Uani 1 1 d . A 1
P5 P 0.9366(3) 0.6699(3) 0.06331(15) 0.0770(14) Uani 1 1 d . A 1
P6 P 1.1926(3) 0.7280(3) 0.0896(2) 0.0936(17) Uani 1 1 d . A 1
P7 P 0.6656(3) 0.7920(3) 0.27486(13) 0.0636(11) Uani 1 1 d . A 1
P8 P 0.8983(3) 0.8378(3) 0.33483(14) 0.0688(12) Uani 1 1 d . A 1
O1 O 1.2196(5) 0.2643(5) 0.1287(3) 0.044(2) Uani 1 1 d . A 1
O2 O 1.3326(6) 0.1672(5) 0.0941(3) 0.058(3) Uani 1 1 d . A 1
O3 O 1.1420(7) 0.5709(5) 0.0622(3) 0.061(3) Uani 1 1 d . A 1
O4 O 1.2124(9) 0.6131(6) -0.0044(3) 0.101(5) Uani 1 1 d . A 1
O5 O 1.4294(6) 0.3229(5) -0.0484(3) 0.051(2) Uani 1 1 d . A 1
O6 O 1.5831(8) 0.0946(6) -0.1477(3) 0.075(3) Uani 1 1 d . A 1
O7 O 1.6146(8) 0.3620(8) -0.2355(3) 0.093(4) Uani 1 1 d . A 1
O8 O 0.7683(6) 0.7288(5) 0.3645(3) 0.054(2) Uani 1 1 d . A 1
O9 O 0.6576(7) 0.8300(6) 0.3992(3) 0.064(3) Uani 1 1 d . A 1
O10 O 0.8273(6) 0.4234(5) 0.4272(3) 0.047(2) Uani 1 1 d . A 1
O11 O 0.7634(7) 0.3851(6) 0.4951(3) 0.075(3) Uani 1 1 d . A 1
O12 O 0.5755(6) 0.6781(5) 0.5467(3) 0.059(3) Uani 1 1 d . A 1
O13 O 0.4430(7) 0.9159(6) 0.6420(4) 0.075(3) Uani 1 1 d . A 1
O14 O 0.4410(11) 0.6751(8) 0.7450(4) 0.112(5) Uani 1 1 d . A 1
C1 C 0.9788(8) 0.1733(7) 0.4056(3) 0.037(3) Uani 1 1 d . A 1
C2 C 0.9766(10) 0.1038(9) 0.4413(4) 0.061(4) Uani 1 1 d . A 1
H2 H 0.9357 0.1154 0.4678 0.073 Uiso 1 1 calc R A 1
C3 C 1.0323(11) 0.0216(8) 0.4377(4) 0.070(5) Uani 1 1 d . A 1
H3 H 1.0312 -0.0227 0.4622 0.084 Uiso 1 1 calc R A 1
C4 C 1.0909(10) 0.0015(8) 0.3985(4) 0.054(4) Uani 1 1 d . A 1
C5 C 1.1524(11) -0.0831(8) 0.3950(5) 0.075(5) Uani 1 1 d . A 1
H5 H 1.1515 -0.1274 0.4195 0.090 Uiso 1 1 calc R A 1
C6 C 1.2113(14) -0.1025(10) 0.3585(6) 0.110(8) Uani 1 1 d . A 1
H6 H 1.2533 -0.1588 0.3580 0.132 Uiso 1 1 calc R A 1
C7 C 1.2111(11) -0.0386(8) 0.3200(5) 0.073(5) Uani 1 1 d . A 1
C8 C 1.2692(14) -0.0580(9) 0.2805(6) 0.110(8) Uani 1 1 d . A 1
H8 H 1.3096 -0.1150 0.2798 0.132 Uiso 1 1 calc R A 1
C9 C 1.2707(11) 0.0009(9) 0.2429(5) 0.084(6) Uani 1 1 d . A 1
H9 H 1.3128 -0.0149 0.2173 0.101 Uiso 1 1 calc R A 1
C10 C 1.2083(9) 0.0866(8) 0.2423(4) 0.052(4) Uani 1 1 d . A 1
C11 C 1.1511(9) 0.1056(8) 0.2806(4) 0.044(3) Uani 1 1 d . A 1
H11 H 1.1090 0.1618 0.2807 0.052 Uiso 1 1 calc R A 1
C12 C 1.1512(9) 0.0460(8) 0.3202(4) 0.049(3) Uani 1 1 d . A 1
C13 C 1.0921(9) 0.0667(8) 0.3616(4) 0.045(3) Uani 1 1 d . A 1
C14 C 1.0337(8) 0.1528(7) 0.3672(4) 0.035(3) Uani 1 1 d . A 1
H14 H 1.0336 0.1975 0.3429 0.042 Uiso 1 1 calc R A 1
C15 C 1.2798(8) 0.2408(8) 0.0963(4) 0.039(3) Uani 1 1 d . A 1
C16 C 1.2891(8) 0.3116(7) 0.0579(4) 0.035(3) Uani 1 1 d . A 1
C17 C 1.3521(8) 0.2897(7) 0.0211(4) 0.037(3) Uani 1 1 d . A 1
H17 H 1.3874 0.2309 0.0197 0.045 Uiso 1 1 calc R A 1
C18 C 1.3641(9) 0.3529(7) -0.0137(4) 0.042(3) Uani 1 1 d . A 1
C19 C 1.3125(10) 0.4394(9) -0.0121(4) 0.059(4) Uani 1 1 d . A 1
H19 H 1.3205 0.4830 -0.0359 0.070 Uiso 1 1 calc R A 1
C20 C 1.2492(10) 0.4604(8) 0.0249(4) 0.053(4) Uani 1 1 d . A 1
C21 C 1.2372(9) 0.3982(8) 0.0599(4) 0.048(3) Uani 1 1 d . A 1
H21 H 1.1941 0.4139 0.0852 0.057 Uiso 1 1 calc R A 1
C22 C 1.1972(12) 0.5558(9) 0.0258(5) 0.074(5) Uani 1 1 d . A 1
C23 C 1.4363(9) 0.3787(7) -0.0889(4) 0.047(3) Uani 1 1 d . A 1
H23A H 1.4648 0.4232 -0.0840 0.057 Uiso 1 1 calc R A 1
H23B H 1.3757 0.4087 -0.0988 0.057 Uiso 1 1 calc R A 1
C24 C 1.4939(9) 0.3221(8) -0.1244(4) 0.050(3) Uani 1 1 d . A 1
C25 C 1.5112(10) 0.2329(8) -0.1171(4) 0.053(4) Uani 1 1 d . A 1
H25 H 1.4880 0.2061 -0.0896 0.064 Uiso 1 1 calc R A 1
C26 C 1.5633(11) 0.1821(9) -0.1506(5) 0.065(4) Uani 1 1 d . A 1
C27 C 1.6004(11) 0.2235(10) -0.1909(4) 0.066(4) Uani 1 1 d . A 1
H27 H 1.6387 0.1895 -0.2131 0.080 Uiso 1 1 calc R A 1
C28 C 1.5804(11) 0.3129(10) -0.1975(5) 0.065(4) Uani 1 1 d . A 1
C29 C 1.5285(10) 0.3628(9) -0.1641(4) 0.060(4) Uani 1 1 d . A 1
H29 H 1.5168 0.4243 -0.1682 0.071 Uiso 1 1 calc R A 1
C30 C 1.5714(10) 0.0490(8) -0.1037(5) 0.061(4) Uani 1 1 d . A 1
H30A H 1.5963 0.0736 -0.0818 0.074 Uiso 1 1 calc R A 1
H30B H 1.6069 -0.0128 -0.1045 0.074 Uiso 1 1 calc R A 1
C31 C 1.4742(11) 0.0527(9) -0.0866(5) 0.062(4) Uani 1 1 d . A 1
C32 C 1.4416(13) 0.0675(10) -0.0428(6) 0.079(5) Uani 1 1 d . A 1
H32 H 1.4806 0.0771 -0.0236 0.095 Uiso 1 1 calc R A 1
C33 C 1.3531(14) 0.0692(10) -0.0248(6) 0.079(5) Uani 1 1 d . A 1
H33 H 1.3324 0.0797 0.0058 0.094 Uiso 1 1 calc R A 1
C34 C 1.2959(13) 0.0548(12) -0.0537(8) 0.096(6) Uani 1 1 d . A 1
H34 H 1.2365 0.0525 -0.0426 0.115 Uiso 1 1 calc R A 1
C35 C 1.3284(14) 0.0441(11) -0.0992(7) 0.086(6) Uani 1 1 d . A 1
H35 H 1.2907 0.0360 -0.1194 0.104 Uiso 1 1 calc R A 1
C36 C 1.4152(13) 0.0454(10) -0.1142(6) 0.076(5) Uani 1 1 d . A 1
H36 H 1.4350 0.0410 -0.1455 0.091 Uiso 1 1 calc R A 1
C37 C 1.6782(12) 0.3133(11) -0.2664(6) 0.088(5) Uani 1 1 d . A 1
H37A H 1.6518 0.2749 -0.2795 0.106 Uiso 1 1 calc R A 1
H37B H 1.7315 0.2769 -0.2513 0.106 Uiso 1 1 calc R A 1
C38 C 1.7043(14) 0.3784(13) -0.3030(6) 0.089(6) Uani 1 1 d . A 1
C39 C 1.7258(13) 0.4475(12) -0.2929(6) 0.089(6) Uani 1 1 d . A 1
H39 H 1.7143 0.4650 -0.2632 0.107 Uiso 1 1 calc R A 1
C40 C 1.7667(14) 0.4922(14) -0.3298(9) 0.111(8) Uani 1 1 d . A 1
H40 H 1.7852 0.5403 -0.3242 0.133 Uiso 1 1 calc R A 1
C41 C 1.7807(14) 0.470(2) -0.3718(9) 0.144(14) Uani 1 1 d . A 1
H41 H 1.8066 0.5031 -0.3957 0.173 Uiso 1 1 calc R A 1
C42 C 1.7586(19) 0.4022(15) -0.3800(8) 0.120(10) Uani 1 1 d . A 1
H42 H 1.7691 0.3862 -0.4100 0.144 Uiso 1 1 calc R A 1
C43 C 1.7234(15) 0.3576(12) -0.3486(7) 0.105(7) Uani 1 1 d . A 1
H43 H 1.7092 0.3083 -0.3558 0.125 Uiso 1 1 calc R A 1
C44 C 0.9944(9) 0.8217(8) 0.0860(4) 0.050(3) Uani 1 1 d . A 1
C45 C 0.9864(10) 0.8892(8) 0.0485(5) 0.073(5) Uani 1 1 d . A 1
H45 H 1.0156 0.8752 0.0195 0.088 Uiso 1 1 calc R A 1
C46 C 0.9378(10) 0.9730(8) 0.0540(5) 0.070(5) Uani 1 1 d . A 1
H46 H 0.9339 1.0163 0.0287 0.084 Uiso 1 1 calc R A 1
C47 C 0.8930(8) 0.9969(7) 0.0965(4) 0.041(3) Uani 1 1 d . A 1
C48 C 0.8404(9) 1.0849(8) 0.1019(5) 0.058(4) Uani 1 1 d . A 1
H48 H 0.8364 1.1282 0.0765 0.069 Uiso 1 1 calc R A 1
C49 C 0.7965(9) 1.1069(8) 0.1425(4) 0.054(4) Uani 1 1 d . A 1
H49 H 0.7663 1.1663 0.1462 0.064 Uiso 1 1 calc R A 1
C50 C 0.7952(8) 1.0410(8) 0.1803(4) 0.041(3) Uani 1 1 d . A 1
C51 C 0.7438(9) 1.0622(8) 0.2222(4) 0.052(4) Uani 1 1 d . A 1
H51 H 0.7116 1.1212 0.2259 0.063 Uiso 1 1 calc R A 1
C52 C 0.7402(10) 0.9990(8) 0.2572(4) 0.054(4) Uani 1 1 d . A 1
H52 H 0.7048 1.0154 0.2847 0.065 Uiso 1 1 calc R A 1
C53 C 0.7862(9) 0.9115(7) 0.2546(4) 0.042(3) Uani 1 1 d . A 1
C54 C 0.8395(8) 0.8922(7) 0.2140(4) 0.044(3) Uani 1 1 d . A 1
H54 H 0.8739 0.8334 0.2117 0.053 Uiso 1 1 calc R A 1
C55 C 0.8461(8) 0.9528(7) 0.1766(4) 0.039(3) Uani 1 1 d . A 1
C56 C 0.8981(8) 0.9309(7) 0.1336(4) 0.043(3) Uani 1 1 d . A 1
C57 C 0.9507(8) 0.8454(7) 0.1265(4) 0.040(3) Uani 1 1 d . A 1
H57 H 0.9557 0.8018 0.1517 0.048 Uiso 1 1 calc R A 1
C58 C 0.7072(9) 0.7570(9) 0.3969(4) 0.048(3) Uani 1 1 d . A 1
C59 C 0.6990(8) 0.6849(7) 0.4357(4) 0.040(3) Uani 1 1 d . A 1
C60 C 0.6446(9) 0.7103(8) 0.4749(4) 0.045(3) Uani 1 1 d . A 1
H60 H 0.6152 0.7701 0.4778 0.054 Uiso 1 1 calc R A 1
C61 C 0.6339(9) 0.6457(8) 0.5104(4) 0.045(3) Uani 1 1 d . A 1
C62 C 0.6763(9) 0.5609(8) 0.5069(4) 0.050(4) Uani 1 1 d . A 1
H62 H 0.6682 0.5182 0.5312 0.061 Uiso 1 1 calc R A 1
C63 C 0.7324(9) 0.5354(8) 0.4676(4) 0.051(4) Uani 1 1 d . A 1
C64 C 0.7434(8) 0.5986(7) 0.4322(4) 0.042(3) Uani 1 1 d . A 1
H64 H 0.7818 0.5820 0.4056 0.050 Uiso 1 1 calc R A 1
C65 C 0.7771(9) 0.4396(8) 0.4640(4) 0.053(4) Uani 1 1 d . A 1
C66 C 0.5765(9) 0.6248(8) 0.5885(4) 0.050(3) Uani 1 1 d . A 1
H66A H 0.6395 0.5934 0.5945 0.060 Uiso 1 1 calc R A 1
H66B H 0.5441 0.5812 0.5875 0.060 Uiso 1 1 calc R A 1
C67 C 0.5307(8) 0.6824(8) 0.6258(4) 0.042(3) Uani 1 1 d . A 1
C68 C 0.5091(9) 0.7726(8) 0.6156(4) 0.049(3) Uani 1 1 d . A 1
H68 H 0.5242 0.7964 0.5857 0.058 Uiso 1 1 calc R A 1
C69 C 0.4670(9) 0.8277(8) 0.6477(5) 0.053(4) Uani 1 1 d . A 1
C70 C 0.4448(10) 0.7911(10) 0.6913(5) 0.068(4) Uani 1 1 d . A 1
H70 H 0.4152 0.8279 0.7142 0.081 Uiso 1 1 calc R A 1
C71 C 0.4660(11) 0.7004(10) 0.7016(4) 0.069(5) Uani 1 1 d . A 1
C72 C 0.5099(9) 0.6464(8) 0.6687(4) 0.052(4) Uani 1 1 d . A 1
H72 H 0.5256 0.5849 0.6758 0.063 Uiso 1 1 calc R A 1
C73 C 0.4546(11) 0.9555(9) 0.5964(5) 0.068(4) Uani 1 1 d . A 1
H73A H 0.4209 1.0181 0.5952 0.081 Uiso 1 1 calc R A 1
H73B H 0.4274 0.9288 0.5765 0.081 Uiso 1 1 calc R A 1
C74 C 0.5508(11) 0.9477(8) 0.5776(6) 0.063(4) Uani 1 1 d . A 1
C75 C 0.5787(11) 0.9314(9) 0.5333(5) 0.067(4) Uani 1 1 d . A 1
H75 H 0.5373 0.9226 0.5153 0.080 Uiso 1 1 calc R A 1
C76 C 0.6629(15) 0.9278(11) 0.5150(7) 0.093(6) Uani 1 1 d . A 1
H76 H 0.6816 0.9156 0.4845 0.111 Uiso 1 1 calc R A 1
C77 C 0.7237(14) 0.9425(12) 0.5418(9) 0.101(7) Uani 1 1 d . A 1
H77 H 0.7823 0.9439 0.5288 0.121 Uiso 1 1 calc R A 1
C78 C 0.6980(14) 0.9543(13) 0.5859(9) 0.104(7) Uani 1 1 d . A 1
H78 H 0.7406 0.9604 0.6041 0.125 Uiso 1 1 calc R A 1
C79 C 0.6107(14) 0.9579(10) 0.6057(7) 0.086(5) Uani 1 1 d . A 1
H79 H 0.5928 0.9669 0.6367 0.103 Uiso 1 1 calc R A 1
C80 C 0.4388(14) 0.5910(12) 0.7559(5) 0.088(6) Uani 1 1 d . A 1
H80A H 0.4988 0.5536 0.7637 0.106 Uiso 1 1 calc R A 1
H80B H 0.4230 0.5697 0.7297 0.106 Uiso 1 1 calc R A 1
C81 C 0.3671(15) 0.5865(10) 0.7972(5) 0.084(6) Uani 1 1 d . A 1
C82 C 0.3018(12) 0.5450(11) 0.7973(5) 0.076(5) Uani 1 1 d . A 1
H82 H 0.2990 0.5201 0.7709 0.091 Uiso 1 1 calc R A 1
C83 C 0.2410(13) 0.5386(14) 0.8343(7) 0.105(7) Uani 1 1 d . A 1
H83 H 0.1991 0.5064 0.8344 0.127 Uiso 1 1 calc R A 1
C84 C 0.2415(12) 0.5814(12) 0.8730(5) 0.083(6) Uani 1 1 d . A 1
H84 H 0.2001 0.5794 0.8993 0.099 Uiso 1 1 calc R A 1
C85 C 0.3043(15) 0.6248(12) 0.8698(7) 0.112(8) Uani 1 1 d . A 1
H85 H 0.3010 0.6594 0.8934 0.134 Uiso 1 1 calc R A 1
C86 C 0.3733(15) 0.6227(13) 0.8347(6) 0.104(6) Uani 1 1 d . A 1
H86 H 0.4220 0.6453 0.8367 0.124 Uiso 1 1 calc R A 1
C87 C 0.8294(15) 0.2447(16) 0.3226(6) 0.128(8) Uani 1 1 d . A 1
H87A H 0.8531 0.2923 0.3063 0.153 Uiso 1 1 calc R A 1
H87B H 0.8814 0.1917 0.3246 0.153 Uiso 1 1 calc R A 1
C88 C 0.7695(19) 0.2295(19) 0.2938(10) 0.184(12) Uiso 1 1 d . A 1
H88A H 0.8026 0.2152 0.2643 0.276 Uiso 1 1 calc R A 1
H88B H 0.7189 0.2821 0.2894 0.276 Uiso 1 1 calc R A 1
H88C H 0.7465 0.1809 0.3082 0.276 Uiso 1 1 calc R A 1
C89 C 0.7516(14) 0.1823(12) 0.4081(11) 0.160(13) Uani 1 1 d . A 1
H89A H 0.7049 0.1761 0.3907 0.191 Uiso 1 1 calc R A 1
H89B H 0.8029 0.1287 0.4068 0.191 Uiso 1 1 calc R A 1
C90 C 0.7118(18) 0.1907(16) 0.4588(7) 0.142(10) Uani 1 1 d . A 1
H90A H 0.6910 0.1397 0.4711 0.214 Uiso 1 1 calc R A 1
H90B H 0.6609 0.2436 0.4604 0.214 Uiso 1 1 calc R A 1
H90C H 0.7585 0.1940 0.4766 0.214 Uiso 1 1 calc R A 1
C91 C 0.6873(12) 0.3604(13) 0.3816(9) 0.129(9) Uani 1 1 d . A 1
H91A H 0.6395 0.3397 0.3725 0.154 Uiso 1 1 calc R A 1
H91B H 0.6683 0.3769 0.4128 0.154 Uiso 1 1 calc R A 1
C92 C 0.6947(15) 0.4399(14) 0.3505(9) 0.146(11) Uani 1 1 d . A 1
H92A H 0.6361 0.4843 0.3515 0.218 Uiso 1 1 calc R A 1
H92B H 0.7131 0.4245 0.3194 0.218 Uiso 1 1 calc R A 1
H92C H 0.7398 0.4628 0.3601 0.218 Uiso 1 1 calc R A 1
C93 C 1.1269(10) 0.2841(11) 0.4141(5) 0.078(5) Uani 1 1 d . A 1
H93A H 1.1405 0.2228 0.4080 0.093 Uiso 1 1 calc R A 1
H93B H 1.1204 0.3204 0.3845 0.093 Uiso 1 1 calc R A 1
C94 C 1.2103(11) 0.2936(11) 0.4333(7) 0.095(6) Uani 1 1 d . A 1
H94A H 1.2637 0.2756 0.4116 0.143 Uiso 1 1 calc R A 1
H94B H 1.2197 0.2567 0.4622 0.143 Uiso 1 1 calc R A 1
H94C H 1.2002 0.3545 0.4381 0.143 Uiso 1 1 calc R A 1
C95 C 1.0383(12) 0.2470(13) 0.5021(5) 0.086(5) Uani 1 1 d . A 1
H95A H 1.0604 0.1844 0.4978 0.103 Uiso 1 1 calc R A 1
H95B H 1.0854 0.2620 0.5155 0.103 Uiso 1 1 calc R A 1
C96 C 0.9530(13) 0.2628(14) 0.5348(6) 0.111(7) Uani 1 1 d . A 1
H96A H 0.9657 0.2268 0.5637 0.166 Uiso 1 1 calc R A 1
H96B H 0.9063 0.2473 0.5218 0.166 Uiso 1 1 calc R A 1
H96C H 0.9317 0.3244 0.5398 0.166 Uiso 1 1 calc R A 1
C97 C 1.0057(12) 0.4205(10) 0.4617(7) 0.093(6) Uani 1 1 d . A 1
H97A H 0.9489 0.4387 0.4817 0.111 Uiso 1 1 calc R A 1
H97B H 1.0562 0.4193 0.4787 0.111 Uiso 1 1 calc R A 1
C98 C 1.0029(13) 0.4868(11) 0.4196(7) 0.107(7) Uani 1 1 d . A 1
H98A H 0.9952 0.5444 0.4289 0.160 Uiso 1 1 calc R A 1
H98B H 0.9523 0.4890 0.4031 0.160 Uiso 1 1 calc R A 1
H98C H 1.0595 0.4696 0.4000 0.160 Uiso 1 1 calc R A 1
C99 C 1.110(2) 0.125(2) 0.1008(11) 0.199(14) Uiso 1 1 d . A 1
H99A H 1.0552 0.1129 0.0938 0.239 Uiso 1 1 calc R A 1
H99B H 1.1172 0.1772 0.0809 0.239 Uiso 1 1 calc R A 1
C100 C 1.176(2) 0.063(2) 0.0917(10) 0.188(13) Uiso 1 1 d . A 1
H10A H 1.1807 0.0563 0.0593 0.282 Uiso 1 1 calc R A 1
H10B H 1.1675 0.0094 0.1096 0.282 Uiso 1 1 calc R A 1
H10C H 1.2305 0.0731 0.0989 0.282 Uiso 1 1 calc R A 1
C101 C 1.036(2) 0.074(2) 0.1924(11) 0.203(14) Uiso 1 1 d D A 1
H10D H 1.0265 0.0824 0.2251 0.244 Uiso 1 1 calc R A 1
H10E H 0.9772 0.0824 0.1812 0.244 Uiso 1 1 calc R A 1
C102 C 1.102(3) -0.018(2) 0.1844(15) 0.31(2) Uiso 1 1 d D A 1
H10F H 1.0750 -0.0632 0.2007 0.459 Uiso 1 1 calc R A 1
H10G H 1.1596 -0.0249 0.1957 0.459 Uiso 1 1 calc R A 1
H10H H 1.1111 -0.0246 0.1519 0.459 Uiso 1 1 calc R A 1
C103 C 1.0029(19) 0.2495(18) 0.1554(10) 0.168(11) Uiso 1 1 d . A 1
H10I H 1.0260 0.2969 0.1383 0.202 Uiso 1 1 calc R A 1
H10J H 0.9548 0.2424 0.1393 0.202 Uiso 1 1 calc R A 1
C104 C 0.965(2) 0.272(2) 0.2050(11) 0.204(14) Uiso 1 1 d . A 1
H10K H 0.9165 0.3269 0.2038 0.305 Uiso 1 1 calc R A 1
H10L H 1.0134 0.2776 0.2208 0.305 Uiso 1 1 calc R A 1
H10M H 0.9410 0.2252 0.2214 0.305 Uiso 1 1 calc R A 1
C105 C 1.4407(10) 0.1169(12) 0.1879(6) 0.082(5) Uani 1 1 d . A 1
H10N H 1.4387 0.0569 0.1996 0.099 Uiso 1 1 calc R A 1
H10O H 1.4393 0.1233 0.1546 0.099 Uiso 1 1 calc R A 1
C106 C 1.5264(15) 0.1264(15) 0.1971(8) 0.132(8) Uiso 1 1 d . A 1
H10P H 1.5763 0.0827 0.1826 0.199 Uiso 1 1 calc R A 1
H10Q H 1.5301 0.1179 0.2300 0.199 Uiso 1 1 calc R A 1
H10R H 1.5304 0.1848 0.1850 0.199 Uiso 1 1 calc R A 1
C107 C 1.3505(12) 0.1709(13) 0.2710(6) 0.091(6) Uani 1 1 d . A 1
H10S H 1.3444 0.1118 0.2813 0.110 Uiso 1 1 calc R A 1
H10T H 1.4125 0.1703 0.2752 0.110 Uiso 1 1 calc R A 1
C108 C 1.2816(14) 0.2371(13) 0.3009(6) 0.109(7) Uani 1 1 d . A 1
H10U H 1.2929 0.2201 0.3328 0.164 Uiso 1 1 calc R A 1
H10V H 1.2202 0.2372 0.2973 0.164 Uiso 1 1 calc R A 1
H10W H 1.2885 0.2955 0.2914 0.164 Uiso 1 1 calc R A 1
C109 C 1.3539(12) 0.3000(10) 0.1939(6) 0.081(5) Uani 1 1 d . A 1
H10X H 1.4014 0.3075 0.2103 0.098 Uiso 1 1 calc R A 1
H10Y H 1.3747 0.3030 0.1611 0.098 Uiso 1 1 calc R A 1
C110 C 1.2672(14) 0.3716(14) 0.2024(7) 0.119(7) Uiso 1 1 d . A 1
H11A H 1.2777 0.4283 0.1920 0.179 Uiso 1 1 calc R A 1
H11B H 1.2471 0.3684 0.2349 0.179 Uiso 1 1 calc R A 1
H11C H 1.2207 0.3642 0.1857 0.179 Uiso 1 1 calc R A 1
C111 C 0.8969(16) 0.7012(16) 0.0057(7) 0.133(8) Uiso 1 1 d D A 1
H11D H 0.8505 0.6727 0.0024 0.159 Uiso 1 1 calc R A 1
H11E H 0.8709 0.7651 0.0001 0.159 Uiso 1 1 calc R A 1
C112 C 0.983(2) 0.669(2) -0.0282(11) 0.227(16) Uiso 1 1 d D A 1
H11F H 0.9668 0.6840 -0.0594 0.341 Uiso 1 1 calc R A 1
H11G H 1.0078 0.6058 -0.0221 0.341 Uiso 1 1 calc R A 1
H11H H 1.0285 0.6974 -0.0241 0.341 Uiso 1 1 calc R A 1
C113 C 0.9491(15) 0.5539(14) 0.0733(7) 0.118(7) Uiso 1 1 d . A 1
H11I H 0.8922 0.5428 0.0686 0.142 Uiso 1 1 calc R A 1
H11J H 0.9975 0.5231 0.0515 0.142 Uiso 1 1 calc R A 1
C114 C 0.9717(14) 0.5196(14) 0.1206(7) 0.118(7) Uiso 1 1 d . A 1
H11K H 0.9783 0.4569 0.1255 0.177 Uiso 1 1 calc R A 1
H11L H 0.9232 0.5494 0.1422 0.177 Uiso 1 1 calc R A 1
H11M H 1.0284 0.5300 0.1252 0.177 Uiso 1 1 calc R A 1
C115 C 0.8373(11) 0.7234(10) 0.0972(6) 0.078(5) Uani 1 1 d . A 1
H11N H 0.8508 0.7113 0.1293 0.094 Uiso 1 1 calc R A 1
H11O H 0.8257 0.7869 0.0887 0.094 Uiso 1 1 calc R A 1
C116 C 0.7484(12) 0.7003(13) 0.0948(7) 0.113(7) Uani 1 1 d . A 1
H11P H 0.7000 0.7344 0.1150 0.169 Uiso 1 1 calc R A 1
H11Q H 0.7572 0.6381 0.1044 0.169 Uiso 1 1 calc R A 1
H11R H 0.7321 0.7139 0.0636 0.169 Uiso 1 1 calc R A 1
C117 C 1.3002(12) 0.6437(11) 0.0878(7) 0.100(6) Uani 1 1 d . A 1
H11S H 1.3146 0.6238 0.0572 0.120 Uiso 1 1 calc R A 1
H11T H 1.3479 0.6691 0.0928 0.120 Uiso 1 1 calc R A 1
C118 C 1.3016(14) 0.5633(12) 0.1238(7) 0.112(7) Uani 1 1 d . A 1
H11U H 1.3608 0.5201 0.1206 0.168 Uiso 1 1 calc R A 1
H11V H 1.2548 0.5374 0.1190 0.168 Uiso 1 1 calc R A 1
H11W H 1.2900 0.5819 0.1543 0.168 Uiso 1 1 calc R A 1
C119 C 1.190(3) 0.767(3) 0.1354(13) 0.241(17) Uiso 1 1 d . A 1
H11X H 1.2521 0.7683 0.1382 0.290 Uiso 1 1 calc R A 1
H11Y H 1.1519 0.8280 0.1324 0.290 Uiso 1 1 calc R A 1
C120 C 1.1610(19) 0.7274(19) 0.1742(10) 0.176(12) Uiso 1 1 d . A 1
H12A H 1.1626 0.7591 0.1994 0.264 Uiso 1 1 calc R A 1
H12B H 1.1999 0.6675 0.1790 0.264 Uiso 1 1 calc R A 1
H12C H 1.0990 0.7266 0.1727 0.264 Uiso 1 1 calc R A 1
C121 C 1.2239(19) 0.8146(18) 0.0374(9) 0.162(11) Uiso 1 1 d . A 1
H12E H 1.2356 0.7886 0.0085 0.195 Uiso 1 1 calc R A 1
H12F H 1.1727 0.8682 0.0349 0.195 Uiso 1 1 calc R A 1
C122 C 1.292(3) 0.833(2) 0.0449(13) 0.245(18) Uiso 1 1 d . A 1
H12G H 1.3067 0.8746 0.0201 0.367 Uiso 1 1 calc R A 1
H12H H 1.3425 0.7798 0.0468 0.367 Uiso 1 1 calc R A 1
H12I H 1.2798 0.8587 0.0736 0.367 Uiso 1 1 calc R A 1
C123 C 0.7106(12) 0.7470(11) 0.2176(6) 0.094(6) Uani 1 1 d D A 1
H12J H 0.6614 0.7374 0.2034 0.112 Uiso 1 1 calc R A 1
H12K H 0.7370 0.7884 0.1967 0.112 Uiso 1 1 calc R A 1
C124 C 0.7848(13) 0.6586(12) 0.2280(7) 0.118(7) Uiso 1 1 d D A 1
H12L H 0.8100 0.6329 0.1997 0.178 Uiso 1 1 calc R A 1
H12M H 0.7577 0.6184 0.2487 0.178 Uiso 1 1 calc R A 1
H12N H 0.8328 0.6692 0.2422 0.178 Uiso 1 1 calc R A 1
C125 C 0.6222(12) 0.7084(11) 0.3083(6) 0.081(5) Uani 1 1 d . A 1
H12O H 0.6741 0.6580 0.3162 0.098 Uiso 1 1 calc R A 1
H12P H 0.5909 0.7310 0.3370 0.098 Uiso 1 1 calc R A 1
C126 C 0.5570(14) 0.6754(14) 0.2864(7) 0.121(7) Uiso 1 1 d . A 1
H12Q H 0.5375 0.6309 0.3077 0.182 Uiso 1 1 calc R A 1
H12R H 0.5876 0.6502 0.2586 0.182 Uiso 1 1 calc R A 1
H12S H 0.5042 0.7241 0.2791 0.182 Uiso 1 1 calc R A 1
C127 C 0.5735(13) 0.8798(11) 0.2568(6) 0.093(6) Uani 1 1 d . A 1
H12T H 0.5956 0.9235 0.2356 0.112 Uiso 1 1 calc R A 1
H12U H 0.5338 0.8584 0.2412 0.112 Uiso 1 1 calc R A 1
C128 C 0.5215(13) 0.9204(13) 0.2998(7) 0.104(6) Uiso 1 1 d . A 1
H12V H 0.4696 0.9691 0.2912 0.155 Uiso 1 1 calc R A 1
H12W H 0.5615 0.9415 0.3148 0.155 Uiso 1 1 calc R A 1
H12X H 0.5004 0.8763 0.3206 0.155 Uiso 1 1 calc R A 1
C129 C 0.9744(13) 0.7337(14) 0.3530(8) 0.121(8) Uani 1 1 d . A 1
H12Y H 1.0293 0.7424 0.3621 0.145 Uiso 1 1 calc R A 1
H12Z H 0.9450 0.7051 0.3797 0.145 Uiso 1 1 calc R A 1
C130 C 1.001(2) 0.674(2) 0.3141(10) 0.194(13) Uiso 1 1 d . A 1
H13A H 1.0422 0.6183 0.3244 0.291 Uiso 1 1 calc R A 1
H13B H 1.0304 0.7026 0.2878 0.291 Uiso 1 1 calc R A 1
H13C H 0.9464 0.6651 0.3055 0.291 Uiso 1 1 calc R A 1
C131 C 0.8712(16) 0.8811(15) 0.3902(7) 0.124(8) Uiso 1 1 d . A 1
H13D H 0.8566 0.8354 0.4131 0.149 Uiso 1 1 calc R A 1
H13E H 0.9263 0.8912 0.3983 0.149 Uiso 1 1 calc R A 1
C132 C 0.8028(18) 0.9556(17) 0.3941(9) 0.162(10) Uiso 1 1 d . A 1
H13F H 0.7946 0.9707 0.4252 0.242 Uiso 1 1 calc R A 1
H13G H 0.7471 0.9469 0.3868 0.242 Uiso 1 1 calc R A 1
H13H H 0.8175 1.0029 0.3730 0.242 Uiso 1 1 calc R A 1
C133 C 0.964(2) 0.904(2) 0.3002(12) 0.205(14) Uiso 1 1 d . A 1
H13I H 0.9425 0.9239 0.2698 0.245 Uiso 1 1 calc R A 1
H13J H 0.9618 0.9557 0.3151 0.245 Uiso 1 1 calc R A 1
C134 C 1.045(5) 0.851(5) 0.298(2) 0.52(5) Uiso 1 1 d . A 1
H13K H 1.0853 0.8788 0.2771 0.780 Uiso 1 1 calc R A 1
H13L H 1.0437 0.7980 0.2858 0.780 Uiso 1 1 calc R A 1
H13M H 1.0661 0.8361 0.3278 0.780 Uiso 1 1 calc R A 1
O15 O 0.5633(17) 0.2165(15) 0.0716(8) 0.237(11) Uiso 1 1 d D F 1
C135 C 0.4826(13) 0.3517(12) 0.1000(6) 0.105(6) Uiso 1 1 d D F 1
H13N H 0.4676 0.3159 0.1275 0.158 Uiso 1 1 calc R F 1
H13O H 0.4273 0.3837 0.0859 0.158 Uiso 1 1 calc R F 1
H13P H 0.5113 0.3931 0.1078 0.158 Uiso 1 1 calc R F 1
C136 C 0.5422(19) 0.2977(16) 0.0693(8) 0.178(12) Uiso 1 1 d D F 1
C137 C 0.5513(17) 0.3703(16) 0.0311(8) 0.159(10) Uiso 1 1 d D F 1
H13Q H 0.5920 0.3446 0.0056 0.238 Uiso 1 1 calc R F 1
H13R H 0.5759 0.4114 0.0425 0.238 Uiso 1 1 calc R F 1
H13S H 0.4919 0.4012 0.0209 0.238 Uiso 1 1 calc R F 1
O16 O 0.0660(17) 0.4006(16) 0.3017(8) 0.246(11) Uiso 1 1 d D G 1
C138 C 0.032(2) 0.506(2) 0.2393(10) 0.249(18) Uiso 1 1 d D G 1
H13T H 0.0975 0.4903 0.2310 0.374 Uiso 1 1 calc R G 1
H13U H 0.0109 0.5662 0.2469 0.374 Uiso 1 1 calc R G 1
H13V H 0.0019 0.5009 0.2137 0.374 Uiso 1 1 calc R G 1
C139 C 0.013(2) 0.4509(18) 0.2763(10) 0.97(13) Uiso 1 1 d D G 1
C140 C -0.088(2) 0.462(3) 0.2810(16) 0.40(3) Uiso 1 1 d D G 1
H14A H -0.1031 0.4215 0.3065 0.599 Uiso 1 1 calc R G 1
H14B H -0.1048 0.4492 0.2530 0.599 Uiso 1 1 calc R G 1
H14C H -0.1207 0.5218 0.2867 0.599 Uiso 1 1 calc R G 1
O17 O 0.4276(18) 0.7970(18) 0.4339(9) 0.286(14) Uiso 1 1 d D H 1
C141 C 0.4215(15) 0.7326(15) 0.3719(7) 0.137(8) Uiso 1 1 d D H 1
H14D H 0.4029 0.7935 0.3587 0.205 Uiso 1 1 calc R H 1
H14E H 0.3748 0.7048 0.3694 0.205 Uiso 1 1 calc R H 1
H14F H 0.4784 0.7018 0.3557 0.205 Uiso 1 1 calc R H 1
C142 C 0.4330(11) 0.7292(15) 0.4166(7) 0.122(8) Uiso 1 1 d D H 1
C143 C 0.459(2) 0.6323(16) 0.4338(10) 0.206(14) Uiso 1 1 d D H 1
H14G H 0.4655 0.6249 0.4663 0.310 Uiso 1 1 calc R H 1
H14H H 0.5163 0.6026 0.4175 0.310 Uiso 1 1 calc R H 1
H14I H 0.4118 0.6072 0.4287 0.310 Uiso 1 1 calc R H 1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
C1 Pt1 O10 177.5(4) . . ?
C1 Pt1 P2 87.5(3) . . ?
O10 Pt1 P2 90.0(3) . . ?
C1 Pt1 P1 89.7(4) . . ?
O10 Pt1 P1 92.8(3) . . ?
P2 Pt1 P1 176.86(16) . . ?
C10 Pt2 O1 177.4(5) . . ?
C10 Pt2 P3 93.3(4) . . ?
O1 Pt2 P3 89.1(3) . . ?
C10 Pt2 P4 86.9(4) . . ?
O1 Pt2 P4 90.8(2) . . ?
P3 Pt2 P4 179.84(16) . . ?
C44 Pt3 O3 178.8(4) . . ?
C44 Pt3 P6 88.9(4) . . ?
O3 Pt3 P6 90.5(3) . . ?
C44 Pt3 P5 90.0(4) . . ?
O3 Pt3 P5 90.5(3) . . ?
P6 Pt3 P5 175.77(19) . . ?
C53 Pt4 O8 176.4(5) . . ?
C53 Pt4 P7 90.5(4) . . ?
O8 Pt4 P7 93.0(3) . . ?
C53 Pt4 P8 90.5(4) . . ?
O8 Pt4 P8 86.1(3) . . ?
P7 Pt4 P8 172.95(16) . . ?
C89 P1 C91 103.3(10) . . ?
C89 P1 C87 102.8(13) . . ?
C91 P1 C87 109.1(12) . . ?
C89 P1 Pt1 114.5(8) . . ?
C91 P1 Pt1 115.5(7) . . ?
C87 P1 Pt1 110.7(7) . . ?
C93 P2 C97 104.7(8) . . ?
C93 P2 C95 105.3(8) . . ?
C97 P2 C95 100.7(9) . . ?
C93 P2 Pt1 116.4(5) . . ?
C97 P2 Pt1 115.2(6) . . ?
C95 P2 Pt1 112.8(6) . . ?
C101 P3 C103 101.5(14) . . ?
C101 P3 C99 106.9(15) . . ?
C103 P3 C99 98.7(14) . . ?
C101 P3 Pt2 120.8(11) . . ?
C103 P3 Pt2 109.5(9) . . ?
C99 P3 Pt2 116.2(11) . . ?
C107 P4 C109 108.8(9) . . ?
C107 P4 C105 99.8(8) . . ?
C109 P4 C105 102.6(8) . . ?
C107 P4 Pt2 119.9(7) . . ?
C109 P4 Pt2 116.0(6) . . ?
C105 P4 Pt2 107.0(6) . . ?
C115 P5 C113 107.6(9) . . ?
C115 P5 C111 100.4(9) . . ?
C113 P5 C111 103.5(10) . . ?
C115 P5 Pt3 115.8(5) . . ?
C113 P5 Pt3 111.1(7) . . ?
C111 P5 Pt3 117.1(8) . . ?
C119 P6 C117 102.4(16) . . ?
C119 P6 C121 107.2(17) . . ?
C117 P6 C121 98.8(10) . . ?
C119 P6 Pt3 119.1(15) . . ?
C117 P6 Pt3 120.1(7) . . ?
C121 P6 Pt3 106.9(8) . . ?
C127 P7 C125 108.7(9) . . ?
C127 P7 C123 98.7(8) . . ?
C125 P7 C123 104.2(8) . . ?
C127 P7 Pt4 118.5(6) . . ?
C125 P7 Pt4 113.4(5) . . ?
C123 P7 Pt4 111.4(6) . . ?
C129 P8 C133 108.5(14) . . ?
C129 P8 C131 97.4(10) . . ?
C133 P8 C131 105.0(14) . . ?
C129 P8 Pt4 111.6(7) . . ?
C133 P8 Pt4 118.6(11) . . ?
C131 P8 Pt4 113.4(8) . . ?
C15 O1 Pt2 117.8(7) . . ?
C22 O3 Pt3 120.8(8) . . ?
C18 O5 C23 119.1(9) . . ?
C26 O6 C30 117.3(11) . . ?
C37 O7 C28 115.7(12) . . ?
C58 O8 Pt4 115.0(7) . . ?
C65 O10 Pt1 121.1(8) . . ?
C61 O12 C66 118.8(9) . . ?
C69 O13 C73 116.0(11) . . ?
C71 O14 C80 117.9(12) . . ?
C14 C1 C2 117.6(11) . . ?
C14 C1 Pt1 123.9(8) . . ?
C2 C1 Pt1 118.5(8) . . ?
C3 C2 C1 121.0(11) . . ?
C3 C2 H2 119.5 . . ?
C1 C2 H2 119.5 . . ?
C2 C3 C4 121.1(11) . . ?
C2 C3 H3 119.5 . . ?
C4 C3 H3 119.5 . . ?
C3 C4 C13 119.8(11) . . ?
C3 C4 C5 121.8(11) . . ?
C13 C4 C5 118.3(11) . . ?
C6 C5 C4 122.6(12) . . ?
C6 C5 H5 118.7 . . ?
C4 C5 H5 118.7 . . ?
C5 C6 C7 119.9(13) . . ?
C5 C6 H6 120.0 . . ?
C7 C6 H6 120.0 . . ?
C8 C7 C12 117.3(12) . . ?
C8 C7 C6 121.4(13) . . ?
C12 C7 C6 121.3(12) . . ?
C9 C8 C7 123.3(13) . . ?
C9 C8 H8 118.4 . . ?
C7 C8 H8 118.4 . . ?
C8 C9 C10 119.8(12) . . ?
C8 C9 H9 120.1 . . ?
C10 C9 H9 120.1 . . ?
C11 C10 C9 117.1(12) . . ?
C11 C10 Pt2 124.2(9) . . ?
C9 C10 Pt2 118.7(9) . . ?
C10 C11 C12 123.4(12) . . ?
C10 C11 H11 118.3 . . ?
C12 C11 H11 118.3 . . ?
C7 C12 C11 119.0(11) . . ?
C7 C12 C13 117.3(11) . . ?
C11 C12 C13 123.7(11) . . ?
C4 C13 C14 117.2(10) . . ?
C4 C13 C12 120.3(11) . . ?
C14 C13 C12 122.5(10) . . ?
C1 C14 C13 123.2(10) . . ?
C1 C14 H14 118.4 . . ?
C13 C14 H14 118.4 . . ?
O2 C15 O1 125.9(11) . . ?
O2 C15 C16 118.0(10) . . ?
O1 C15 C16 116.1(10) . . ?
C17 C16 C21 119.7(10) . . ?
C17 C16 C15 119.0(10) . . ?
C21 C16 C15 121.3(10) . . ?
C16 C17 C18 120.4(10) . . ?
C16 C17 H17 119.8 . . ?
C18 C17 H17 119.8 . . ?
O5 C18 C17 114.9(10) . . ?
O5 C18 C19 124.8(10) . . ?
C17 C18 C19 120.4(11) . . ?
C20 C19 C18 118.7(12) . . ?
C20 C19 H19 120.7 . . ?
C18 C19 H19 120.7 . . ?
C21 C20 C19 121.5(12) . . ?
C21 C20 C22 122.0(11) . . ?
C19 C20 C22 116.5(11) . . ?
C20 C21 C16 119.4(11) . . ?
C20 C21 H21 120.3 . . ?
C16 C21 H21 120.3 . . ?
O4 C22 O3 124.8(13) . . ?
O4 C22 C20 122.0(12) . . ?
O3 C22 C20 112.9(11) . . ?
O5 C23 C24 106.9(9) . . ?
O5 C23 H23A 110.3 . . ?
C24 C23 H23A 110.3 . . ?
O5 C23 H23B 110.3 . . ?
C24 C23 H23B 110.3 . . ?
H23A C23 H23B 108.6 . . ?
C25 C24 C29 121.4(12) . . ?
C25 C24 C23 120.3(11) . . ?
C29 C24 C23 118.3(11) . . ?
C24 C25 C26 119.2(12) . . ?
C24 C25 H25 120.4 . . ?
C26 C25 H25 120.4 . . ?
O6 C26 C25 124.6(13) . . ?
O6 C26 C27 116.0(13) . . ?
C25 C26 C27 119.4(12) . . ?
C28 C27 C26 119.8(12) . . ?
C28 C27 H27 120.1 . . ?
C26 C27 H27 120.1 . . ?
C27 C28 C29 120.4(13) . . ?
C27 C28 O7 125.3(13) . . ?
C29 C28 O7 114.1(12) . . ?
C28 C29 C24 119.6(13) . . ?
C28 C29 H29 120.2 . . ?
C24 C29 H29 120.2 . . ?
O6 C30 C31 114.6(12) . . ?
O6 C30 H30A 108.6 . . ?
C31 C30 H30A 108.6 . . ?
O6 C30 H30B 108.6 . . ?
C31 C30 H30B 108.6 . . ?
H30A C30 H30B 107.6 . . ?
C36 C31 C32 117.3(17) . . ?
C36 C31 C30 122.1(16) . . ?
C32 C31 C30 120.5(15) . . ?
C31 C32 C33 122.9(17) . . ?
C31 C32 H32 118.6 . . ?
C33 C32 H32 118.6 . . ?
C32 C33 C34 118.0(18) . . ?
C32 C33 H33 121.0 . . ?
C34 C33 H33 121.0 . . ?
C35 C34 C33 118.6(18) . . ?
C35 C34 H34 120.7 . . ?
C33 C34 H34 120.7 . . ?
C36 C35 C34 119.6(17) . . ?
C36 C35 H35 120.2 . . ?
C34 C35 H35 120.2 . . ?
C31 C36 C35 123.3(17) . . ?
C31 C36 H36 118.4 . . ?
C35 C36 H36 118.4 . . ?
O7 C37 C38 106.1(15) . . ?
O7 C37 H37A 110.5 . . ?
C38 C37 H37A 110.5 . . ?
O7 C37 H37B 110.5 . . ?
C38 C37 H37B 110.5 . . ?
H37A C37 H37B 108.7 . . ?
C39 C38 C43 118.4(17) . . ?
C39 C38 C37 121.6(17) . . ?
C43 C38 C37 118.9(18) . . ?
C38 C39 C40 115.1(19) . . ?
C38 C39 H39 122.5 . . ?
C40 C39 H39 122.5 . . ?
C41 C40 C39 123(2) . . ?
C41 C40 H40 118.5 . . ?
C39 C40 H40 118.5 . . ?
C42 C41 C40 120(3) . . ?
C42 C41 H41 120.2 . . ?
C40 C41 H41 120.2 . . ?
C43 C42 C41 121(3) . . ?
C43 C42 H42 119.4 . . ?
C41 C42 H42 119.4 . . ?
C42 C43 C38 123(2) . . ?
C42 C43 H43 118.7 . . ?
C38 C43 H43 118.7 . . ?
C57 C44 C45 116.7(11) . . ?
C57 C44 Pt3 125.4(9) . . ?
C45 C44 Pt3 117.8(8) . . ?
C46 C45 C44 121.2(12) . . ?
C46 C45 H45 119.4 . . ?
C44 C45 H45 119.4 . . ?
C45 C46 C47 121.5(12) . . ?
C45 C46 H46 119.2 . . ?
C47 C46 H46 119.2 . . ?
C46 C47 C56 118.3(11) . . ?
C46 C47 C48 121.2(11) . . ?
C56 C47 C48 120.4(11) . . ?
C49 C48 C47 120.8(12) . . ?
C49 C48 H48 119.6 . . ?
C47 C48 H48 119.6 . . ?
C48 C49 C50 120.4(11) . . ?
C48 C49 H49 119.8 . . ?
C50 C49 H49 119.8 . . ?
C51 C50 C55 118.4(11) . . ?
C51 C50 C49 121.0(11) . . ?
C55 C50 C49 120.6(10) . . ?
C52 C51 C50 120.6(12) . . ?
C52 C51 H51 119.7 . . ?
C50 C51 H51 119.7 . . ?
C51 C52 C53 123.0(12) . . ?
C51 C52 H52 118.5 . . ?
C53 C52 H52 118.5 . . ?
C54 C53 C52 115.7(11) . . ?
C54 C53 Pt4 123.5(9) . . ?
C52 C53 Pt4 120.8(9) . . ?
C55 C54 C53 124.8(11) . . ?
C55 C54 H54 117.6 . . ?
C53 C54 H54 117.6 . . ?
C54 C55 C50 117.4(10) . . ?
C54 C55 C56 124.1(10) . . ?
C50 C55 C56 118.4(10) . . ?
C57 C56 C47 118.1(10) . . ?
C57 C56 C55 122.8(10) . . ?
C47 C56 C55 119.0(10) . . ?
C44 C57 C56 124.1(11) . . ?
C44 C57 H57 117.9 . . ?
C56 C57 H57 117.9 . . ?
O9 C58 O8 127.9(11) . . ?
O9 C58 C59 119.3(11) . . ?
O8 C58 C59 112.8(11) . . ?
C64 C59 C60 120.4(11) . . ?
C64 C59 C58 122.1(10) . . ?
C60 C59 C58 117.5(11) . . ?
C59 C60 C61 118.7(11) . . ?
C59 C60 H60 120.6 . . ?
C61 C60 H60 120.6 . . ?
C62 C61 O12 125.3(11) . . ?
C62 C61 C60 121.0(11) . . ?
O12 C61 C60 113.6(10) . . ?
C61 C62 C63 120.3(11) . . ?
C61 C62 H62 119.8 . . ?
C63 C62 H62 119.8 . . ?
C64 C63 C62 119.2(11) . . ?
C64 C63 C65 121.6(11) . . ?
C62 C63 C65 119.2(11) . . ?
C59 C64 C63 120.3(11) . . ?
C59 C64 H64 119.8 . . ?
C63 C64 H64 119.8 . . ?
O11 C65 O10 125.7(12) . . ?
O11 C65 C63 120.1(12) . . ?
O10 C65 C63 114.2(11) . . ?
O12 C66 C67 108.3(9) . . ?
O12 C66 H66A 110.0 . . ?
C67 C66 H66A 110.0 . . ?
O12 C66 H66B 110.0 . . ?
C67 C66 H66B 110.0 . . ?
H66A C66 H66B 108.4 . . ?
C72 C67 C68 120.2(11) . . ?
C72 C67 C66 120.6(11) . . ?
C68 C67 C66 119.2(10) . . ?
C69 C68 C67 121.8(12) . . ?
C69 C68 H68 119.1 . . ?
C67 C68 H68 119.1 . . ?
O13 C69 C68 127.2(13) . . ?
O13 C69 C70 114.7(12) . . ?
C68 C69 C70 118.1(12) . . ?
C69 C70 C71 120.3(13) . . ?
C69 C70 H70 119.8 . . ?
C71 C70 H70 119.8 . . ?
O14 C71 C72 126.4(14) . . ?
O14 C71 C70 113.4(13) . . ?
C72 C71 C70 120.2(12) . . ?
C67 C72 C71 119.4(12) . . ?
C67 C72 H72 120.3 . . ?
C71 C72 H72 120.3 . . ?
O13 C73 C74 115.0(13) . . ?
O13 C73 H73A 108.5 . . ?
C74 C73 H73A 108.5 . . ?
O13 C73 H73B 108.5 . . ?
C74 C73 H73B 108.5 . . ?
H73A C73 H73B 107.5 . . ?
C75 C74 C79 120.9(17) . . ?
C75 C74 C73 119.9(15) . . ?
C79 C74 C73 119.1(16) . . ?
C76 C75 C74 121.4(18) . . ?
C76 C75 H75 119.3 . . ?
C74 C75 H75 119.3 . . ?
C75 C76 C77 119(2) . . ?
C75 C76 H76 120.5 . . ?
C77 C76 H76 120.5 . . ?
C78 C77 C76 120(2) . . ?
C78 C77 H77 120.1 . . ?
C76 C77 H77 120.1 . . ?
C77 C78 C79 122(2) . . ?
C77 C78 H78 119.0 . . ?
C79 C78 H78 119.0 . . ?
C78 C79 C74 116.8(19) . . ?
C78 C79 H79 121.6 . . ?
C74 C79 H79 121.6 . . ?
O14 C80 C81 109.1(14) . . ?
O14 C80 H80A 109.9 . . ?
C81 C80 H80A 109.9 . . ?
O14 C80 H80B 109.9 . . ?
C81 C80 H80B 109.9 . . ?
H80A C80 H80B 108.3 . . ?
C86 C81 C82 120.5(17) . . ?
C86 C81 C80 117.3(18) . . ?
C82 C81 C80 122.1(14) . . ?
C83 C82 C81 121.9(17) . . ?
C83 C82 H82 119.1 . . ?
C81 C82 H82 119.1 . . ?
C82 C83 C84 118.9(19) . . ?
C82 C83 H83 120.6 . . ?
C84 C83 H83 120.6 . . ?
C85 C84 C83 116.2(16) . . ?
C85 C84 H84 121.9 . . ?
C83 C84 H84 121.9 . . ?
C84 C85 C86 125.2(19) . . ?
C84 C85 H85 117.4 . . ?
C86 C85 H85 117.4 . . ?
C81 C86 C85 116(2) . . ?
C81 C86 H86 121.8 . . ?
C85 C86 H86 121.8 . . ?
C88 C87 P1 121.3(19) . . ?
C88 C87 H87A 107.0 . . ?
P1 C87 H87A 107.0 . . ?
C88 C87 H87B 107.0 . . ?
P1 C87 H87B 107.0 . . ?
H87A C87 H87B 106.7 . . ?
C87 C88 H88A 109.5 . . ?
C87 C88 H88B 109.5 . . ?
H88A C88 H88B 109.5 . . ?
C87 C88 H88C 109.5 . . ?
H88A C88 H88C 109.5 . . ?
H88B C88 H88C 109.5 . . ?
C90 C89 P1 113.0(16) . . ?
C90 C89 H89A 109.0 . . ?
P1 C89 H89A 109.0 . . ?
C90 C89 H89B 109.0 . . ?
P1 C89 H89B 109.0 . . ?
H89A C89 H89B 107.8 . . ?
C89 C90 H90A 109.5 . . ?
C89 C90 H90B 109.5 . . ?
H90A C90 H90B 109.5 . . ?
C89 C90 H90C 109.5 . . ?
H90A C90 H90C 109.5 . . ?
H90B C90 H90C 109.5 . . ?
C92 C91 P1 114.5(16) . . ?
C92 C91 H91A 108.6 . . ?
P1 C91 H91A 108.6 . . ?
C92 C91 H91B 108.6 . . ?
P1 C91 H91B 108.6 . . ?
H91A C91 H91B 107.6 . . ?
C91 C92 H92A 109.5 . . ?
C91 C92 H92B 109.5 . . ?
H92A C92 H92B 109.5 . . ?
C91 C92 H92C 109.5 . . ?
H92A C92 H92C 109.5 . . ?
H92B C92 H92C 109.5 . . ?
C94 C93 P2 119.2(12) . . ?
C94 C93 H93A 107.5 . . ?
P2 C93 H93A 107.5 . . ?
C94 C93 H93B 107.5 . . ?
P2 C93 H93B 107.5 . . ?
H93A C93 H93B 107.0 . . ?
C93 C94 H94A 109.5 . . ?
C93 C94 H94B 109.5 . . ?
H94A C94 H94B 109.5 . . ?
C93 C94 H94C 109.5 . . ?
H94A C94 H94C 109.5 . . ?
H94B C94 H94C 109.5 . . ?
C96 C95 P2 112.3(12) . . ?
C96 C95 H95A 109.1 . . ?
P2 C95 H95A 109.1 . . ?
C96 C95 H95B 109.1 . . ?
P2 C95 H95B 109.1 . . ?
H95A C95 H95B 107.9 . . ?
C95 C96 H96A 109.5 . . ?
C95 C96 H96B 109.5 . . ?
H96A C96 H96B 109.5 . . ?
C95 C96 H96C 109.5 . . ?
H96A C96 H96C 109.5 . . ?
H96B C96 H96C 109.5 . . ?
C98 C97 P2 111.8(13) . . ?
C98 C97 H97A 109.3 . . ?
P2 C97 H97A 109.3 . . ?
C98 C97 H97B 109.3 . . ?
P2 C97 H97B 109.3 . . ?
H97A C97 H97B 107.9 . . ?
C97 C98 H98A 109.5 . . ?
C97 C98 H98B 109.5 . . ?
H98A C98 H98B 109.5 . . ?
C97 C98 H98C 109.5 . . ?
H98A C98 H98C 109.5 . . ?
H98B C98 H98C 109.5 . . ?
C100 C99 P3 115(3) . . ?
C100 C99 H99A 108.6 . . ?
P3 C99 H99A 108.6 . . ?
C100 C99 H99B 108.6 . . ?
P3 C99 H99B 108.6 . . ?
H99A C99 H99B 107.6 . . ?
C99 C100 H10A 109.5 . . ?
C99 C100 H10B 109.5 . . ?
H10A C100 H10B 109.5 . . ?
C99 C100 H10C 109.5 . . ?
H10A C100 H10C 109.5 . . ?
H10B C100 H10C 109.5 . . ?
C102 C101 P3 104(2) . . ?
C102 C101 H10D 111.0 . . ?
P3 C101 H10D 111.0 . . ?
C102 C101 H10E 111.0 . . ?
P3 C101 H10E 111.0 . . ?
H10D C101 H10E 109.0 . . ?
C101 C102 H10F 109.5 . . ?
C101 C102 H10G 109.5 . . ?
H10F C102 H10G 109.5 . . ?
C101 C102 H10H 109.5 . . ?
H10F C102 H10H 109.5 . . ?
H10G C102 H10H 109.5 . . ?
C104 C103 P3 107(2) . . ?
C104 C103 H10I 110.3 . . ?
P3 C103 H10I 110.3 . . ?
C104 C103 H10J 110.3 . . ?
P3 C103 H10J 110.3 . . ?
H10I C103 H10J 108.5 . . ?
C103 C104 H10K 109.5 . . ?
C103 C104 H10L 109.5 . . ?
H10K C104 H10L 109.5 . . ?
C103 C104 H10M 109.5 . . ?
H10K C104 H10M 109.5 . . ?
H10L C104 H10M 109.5 . . ?
C106 C105 P4 116.2(14) . . ?
C106 C105 H10N 108.2 . . ?
P4 C105 H10N 108.2 . . ?
C106 C105 H10O 108.2 . . ?
P4 C105 H10O 108.2 . . ?
H10N C105 H10O 107.4 . . ?
C105 C106 H10P 109.5 . . ?
C105 C106 H10Q 109.5 . . ?
H10P C106 H10Q 109.5 . . ?
C105 C106 H10R 109.5 . . ?
H10P C106 H10R 109.5 . . ?
H10Q C106 H10R 109.5 . . ?
C108 C107 P4 112.4(13) . . ?
C108 C107 H10S 109.1 . . ?
P4 C107 H10S 109.1 . . ?
C108 C107 H10T 109.1 . . ?
P4 C107 H10T 109.1 . . ?
H10S C107 H10T 107.9 . . ?
C107 C108 H10U 109.5 . . ?
C107 C108 H10V 109.5 . . ?
H10U C108 H10V 109.5 . . ?
C107 C108 H10W 109.5 . . ?
H10U C108 H10W 109.5 . . ?
H10V C108 H10W 109.5 . . ?
C110 C109 P4 109.3(13) . . ?
C110 C109 H10X 109.8 . . ?
P4 C109 H10X 109.8 . . ?
C110 C109 H10Y 109.8 . . ?
P4 C109 H10Y 109.8 . . ?
H10X C109 H10Y 108.3 . . ?
C109 C110 H11A 109.5 . . ?
C109 C110 H11B 109.5 . . ?
H11A C110 H11B 109.5 . . ?
C109 C110 H11C 109.5 . . ?
H11A C110 H11C 109.5 . . ?
H11B C110 H11C 109.5 . . ?
C112 C111 P5 105.3(18) . . ?
C112 C111 H11D 110.7 . . ?
P5 C111 H11D 110.7 . . ?
C112 C111 H11E 110.7 . . ?
P5 C111 H11E 110.7 . . ?
H11D C111 H11E 108.8 . . ?
C111 C112 H11F 109.5 . . ?
C111 C112 H11G 109.5 . . ?
H11F C112 H11G 109.5 . . ?
C111 C112 H11H 109.5 . . ?
H11F C112 H11H 109.5 . . ?
H11G C112 H11H 109.5 . . ?
C114 C113 P5 110.4(15) . . ?
C114 C113 H11I 109.6 . . ?
P5 C113 H11I 109.6 . . ?
C114 C113 H11J 109.6 . . ?
P5 C113 H11J 109.6 . . ?
H11I C113 H11J 108.1 . . ?
C113 C114 H11K 109.5 . . ?
C113 C114 H11L 109.5 . . ?
H11K C114 H11L 109.5 . . ?
C113 C114 H11M 109.5 . . ?
H11K C114 H11M 109.5 . . ?
H11L C114 H11M 109.5 . . ?
C116 C115 P5 118.5(11) . . ?
C116 C115 H11N 107.7 . . ?
P5 C115 H11N 107.7 . . ?
C116 C115 H11O 107.7 . . ?
P5 C115 H11O 107.7 . . ?
H11N C115 H11O 107.1 . . ?
C115 C116 H11P 109.5 . . ?
C115 C116 H11Q 109.5 . . ?
H11P C116 H11Q 109.5 . . ?
C115 C116 H11R 109.5 . . ?
H11P C116 H11R 109.5 . . ?
H11Q C116 H11R 109.5 . . ?
C118 C117 P6 113.6(13) . . ?
C118 C117 H11S 108.8 . . ?
P6 C117 H11S 108.8 . . ?
C118 C117 H11T 108.8 . . ?
P6 C117 H11T 108.8 . . ?
H11S C117 H11T 107.7 . . ?
C117 C118 H11U 109.5 . . ?
C117 C118 H11V 109.5 . . ?
H11U C118 H11V 109.5 . . ?
C117 C118 H11W 109.5 . . ?
H11U C118 H11W 109.5 . . ?
H11V C118 H11W 109.5 . . ?
C120 C119 P6 119(3) . . ?
C120 C119 H11X 107.6 . . ?
P6 C119 H11X 107.6 . . ?
C120 C119 H11Y 107.6 . . ?
P6 C119 H11Y 107.6 . . ?
H11X C119 H11Y 107.1 . . ?
C119 C120 H12A 109.5 . . ?
C119 C120 H12B 109.5 . . ?
H12A C120 H12B 109.5 . . ?
C119 C120 H12C 109.5 . . ?
H12A C120 H12C 109.5 . . ?
H12B C120 H12C 109.5 . . ?
C122 C121 P6 109(3) . . ?
C122 C121 H12E 109.8 . . ?
P6 C121 H12E 109.8 . . ?
C122 C121 H12F 109.8 . . ?
P6 C121 H12F 109.8 . . ?
H12E C121 H12F 108.3 . . ?
C121 C122 H12G 109.5 . . ?
C121 C122 H12H 109.5 . . ?
H12G C122 H12H 109.5 . . ?
C121 C122 H12I 109.5 . . ?
H12G C122 H12I 109.5 . . ?
H12H C122 H12I 109.5 . . ?
C124 C123 P7 106.3(13) . . ?
C124 C123 H12J 110.5 . . ?
P7 C123 H12J 110.5 . . ?
C124 C123 H12K 110.5 . . ?
P7 C123 H12K 110.5 . . ?
H12J C123 H12K 108.7 . . ?
C123 C124 H12L 109.5 . . ?
C123 C124 H12M 109.5 . . ?
H12L C124 H12M 109.5 . . ?
C123 C124 H12N 109.5 . . ?
H12L C124 H12N 109.5 . . ?
H12M C124 H12N 109.5 . . ?
C126 C125 P7 116.8(12) . . ?
C126 C125 H12O 108.1 . . ?
P7 C125 H12O 108.1 . . ?
C126 C125 H12P 108.1 . . ?
P7 C125 H12P 108.1 . . ?
H12O C125 H12P 107.3 . . ?
C125 C126 H12Q 109.5 . . ?
C125 C126 H12R 109.5 . . ?
H12Q C126 H12R 109.5 . . ?
C125 C126 H12S 109.5 . . ?
H12Q C126 H12S 109.5 . . ?
H12R C126 H12S 109.5 . . ?
C128 C127 P7 106.9(12) . . ?
C128 C127 H12T 110.3 . . ?
P7 C127 H12T 110.3 . . ?
C128 C127 H12U 110.3 . . ?
P7 C127 H12U 110.3 . . ?
H12T C127 H12U 108.6 . . ?
C127 C128 H12V 109.5 . . ?
C127 C128 H12W 109.5 . . ?
H12V C128 H12W 109.5 . . ?
C127 C128 H12X 109.5 . . ?
H12V C128 H12X 109.5 . . ?
H12W C128 H12X 109.5 . . ?
C130 C129 P8 110.3(16) . . ?
C130 C129 H12Y 109.6 . . ?
P8 C129 H12Y 109.6 . . ?
C130 C129 H12Z 109.6 . . ?
P8 C129 H12Z 109.6 . . ?
H12Y C129 H12Z 108.1 . . ?
C129 C130 H13A 109.5 . . ?
C129 C130 H13B 109.5 . . ?
H13A C130 H13B 109.5 . . ?
C129 C130 H13C 109.5 . . ?
H13A C130 H13C 109.5 . . ?
H13B C130 H13C 109.5 . . ?
C132 C131 P8 117.7(19) . . ?
C132 C131 H13D 107.9 . . ?
P8 C131 H13D 107.9 . . ?
C132 C131 H13E 107.9 . . ?
P8 C131 H13E 107.9 . . ?
H13D C131 H13E 107.2 . . ?
C131 C132 H13F 109.5 . . ?
C131 C132 H13G 109.5 . . ?
H13F C132 H13G 109.5 . . ?
C131 C132 H13H 109.5 . . ?
H13F C132 H13H 109.5 . . ?
H13G C132 H13H 109.5 . . ?
C134 C133 P8 103(4) . . ?
C134 C133 H13I 111.2 . . ?
P8 C133 H13I 111.2 . . ?
C134 C133 H13J 111.2 . . ?
P8 C133 H13J 111.2 . . ?
H13I C133 H13J 109.2 . . ?
C133 C134 H13K 109.5 . . ?
C133 C134 H13L 109.5 . . ?
H13K C134 H13L 109.5 . . ?
C133 C134 H13M 109.5 . . ?
H13K C134 H13M 109.5 . . ?
H13L C134 H13M 109.5 . . ?
C136 C135 H13N 109.5 . . ?
C136 C135 H13O 109.5 . . ?
H13N C135 H13O 109.5 . . ?
C136 C135 H13P 109.5 . . ?
H13N C135 H13P 109.5 . . ?
H13O C135 H13P 109.5 . . ?
O15 C136 C135 128(2) . . ?
O15 C136 C137 134(2) . . ?
C135 C136 C137 97.1(17) . . ?
C136 C137 H13Q 109.5 . . ?
C136 C137 H13R 109.5 . . ?
H13Q C137 H13R 109.5 . . ?
C136 C137 H13S 109.5 . . ?
H13Q C137 H13S 109.5 . . ?
H13R C137 H13S 109.5 . . ?
C139 C138 H13T 109.5 . . ?
C139 C138 H13U 109.5 . . ?
H13T C138 H13U 109.5 . . ?
C139 C138 H13V 109.5 . . ?
H13T C138 H13V 109.5 . . ?
H13U C138 H13V 109.5 . . ?
O16 C139 C138 127(3) . . ?
O16 C139 C140 125(3) . . ?
C138 C139 C140 108(2) . . ?
C139 C140 H14A 109.5 . . ?
C139 C140 H14B 109.5 . . ?
H14A C140 H14B 109.5 . . ?
C139 C140 H14C 109.5 . . ?
H14A C140 H14C 109.5 . . ?
H14B C140 H14C 109.5 . . ?
C142 C141 H14D 109.5 . . ?
C142 C141 H14E 109.5 . . ?
H14D C141 H14E 109.5 . . ?
C142 C141 H14F 109.5 . . ?
H14D C141 H14F 109.5 . . ?
H14E C141 H14F 109.5 . . ?
O17 C142 C141 121(2) . . ?
O17 C142 C143 134(2) . . ?
C141 C142 C143 104.9(19) . . ?
C142 C143 H14G 109.5 . . ?
C142 C143 H14H 109.5 . . ?
H14G C143 H14H 109.5 . . ?
C142 C143 H14I 109.5 . . ?
H14G C143 H14I 109.5 . . ?
H14H C143 H14I 109.5 . . ?
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 C1 2.016(11) . ?
Pt1 O10 2.110(7) . ?
Pt1 P2 2.270(4) . ?
Pt1 P1 2.292(4) . ?
Pt2 C10 2.015(13) . ?
Pt2 O1 2.129(7) . ?
Pt2 P3 2.251(5) . ?
Pt2 P4 2.328(4) . ?
Pt3 C44 2.022(12) . ?
Pt3 O3 2.112(8) . ?
Pt3 P6 2.283(5) . ?
Pt3 P5 2.285(5) . ?
Pt4 C53 1.991(11) . ?
Pt4 O8 2.140(7) . ?
Pt4 P7 2.266(4) . ?
Pt4 P8 2.304(5) . ?
P1 C89 1.77(2) . ?
P1 C91 1.784(18) . ?
P1 C87 1.886(19) . ?
P2 C93 1.780(17) . ?
P2 C97 1.827(14) . ?
P2 C95 1.830(15) . ?
P3 C101 1.80(3) . ?
P3 C103 1.83(3) . ?
P3 C99 1.84(3) . ?
P4 C107 1.758(17) . ?
P4 C109 1.792(16) . ?
P4 C105 1.906(16) . ?
P5 C115 1.789(16) . ?
P5 C113 1.81(2) . ?
P5 C111 1.86(2) . ?
P6 C119 1.58(4) . ?
P6 C117 1.820(17) . ?
P6 C121 2.05(3) . ?
P7 C127 1.774(17) . ?
P7 C125 1.805(16) . ?
P7 C123 1.920(16) . ?
P8 C129 1.806(18) . ?
P8 C133 1.82(3) . ?
P8 C131 1.84(2) . ?
O1 C15 1.268(13) . ?
O2 C15 1.234(13) . ?
O3 C22 1.296(15) . ?
O4 C22 1.249(16) . ?
O5 C18 1.384(13) . ?
O5 C23 1.413(13) . ?
O6 C26 1.349(15) . ?
O6 C30 1.430(16) . ?
O7 C37 1.396(18) . ?
O7 C28 1.428(16) . ?
O8 C58 1.294(14) . ?
O9 C58 1.210(14) . ?
O10 C65 1.273(14) . ?
O11 C65 1.230(14) . ?
O12 C61 1.375(13) . ?
O12 C66 1.410(13) . ?
O13 C69 1.356(15) . ?
O13 C73 1.432(16) . ?
O14 C71 1.344(15) . ?
O14 C80 1.363(18) . ?
C1 C14 1.354(14) . ?
C1 C2 1.438(16) . ?
C2 C3 1.365(17) . ?
C2 H2 0.9500 . ?
C3 C4 1.398(17) . ?
C3 H3 0.9500 . ?
C4 C13 1.416(16) . ?
C4 C5 1.427(17) . ?
C5 C6 1.336(19) . ?
C5 H5 0.9500 . ?
C6 C7 1.430(19) . ?
C6 H6 0.9500 . ?
C7 C8 1.401(18) . ?
C7 C12 1.408(17) . ?
C8 C9 1.37(2) . ?
C8 H8 0.9500 . ?
C9 C10 1.437(18) . ?
C9 H9 0.9500 . ?
C10 C11 1.363(15) . ?
C11 C12 1.414(15) . ?
C11 H11 0.9500 . ?
C12 C13 1.456(16) . ?
C13 C14 1.438(15) . ?
C14 H14 0.9500 . ?
C15 C16 1.525(15) . ?
C16 C17 1.382(14) . ?
C16 C21 1.399(15) . ?
C17 C18 1.385(15) . ?
C17 H17 0.9500 . ?
C18 C19 1.394(17) . ?
C19 C20 1.388(17) . ?
C19 H19 0.9500 . ?
C20 C21 1.378(16) . ?
C20 C22 1.516(18) . ?
C21 H21 0.9500 . ?
C23 C24 1.518(15) . ?
C23 H23A 0.9900 . ?
C23 H23B 0.9900 . ?
C24 C25 1.378(17) . ?
C24 C29 1.394(16) . ?
C25 C26 1.399(18) . ?
C25 H25 0.9500 . ?
C26 C27 1.428(19) . ?
C27 C28 1.376(19) . ?
C27 H27 0.9500 . ?
C28 C29 1.388(18) . ?
C29 H29 0.9500 . ?
C30 C31 1.52(2) . ?
C30 H30A 0.9900 . ?
C30 H30B 0.9900 . ?
C31 C36 1.36(2) . ?
C31 C32 1.37(2) . ?
C32 C33 1.41(2) . ?
C32 H32 0.9500 . ?
C33 C34 1.42(2) . ?
C33 H33 0.9500 . ?
C34 C35 1.40(2) . ?
C34 H34 0.9500 . ?
C35 C36 1.37(2) . ?
C35 H35 0.9500 . ?
C36 H36 0.9500 . ?
C37 C38 1.51(2) . ?
C37 H37A 0.9900 . ?
C37 H37B 0.9900 . ?
C38 C39 1.35(2) . ?
C38 C43 1.42(2) . ?
C39 C40 1.41(3) . ?
C39 H39 0.9500 . ?
C40 C41 1.33(3) . ?
C40 H40 0.9500 . ?
C41 C42 1.31(4) . ?
C41 H41 0.9500 . ?
C42 C43 1.26(3) . ?
C42 H42 0.9500 . ?
C43 H43 0.9500 . ?
C44 C57 1.354(15) . ?
C44 C45 1.438(17) . ?
C45 C46 1.363(17) . ?
C45 H45 0.9500 . ?
C46 C47 1.410(16) . ?
C46 H46 0.9500 . ?
C47 C56 1.419(15) . ?
C47 C48 1.435(16) . ?
C48 C49 1.352(17) . ?
C48 H48 0.9500 . ?
C49 C50 1.440(16) . ?
C49 H49 0.9500 . ?
C50 C51 1.421(16) . ?
C50 C55 1.423(15) . ?
C51 C52 1.361(16) . ?
C51 H51 0.9500 . ?
C52 C53 1.393(16) . ?
C52 H52 0.9500 . ?
C53 C54 1.392(16) . ?
C54 C55 1.392(15) . ?
C54 H54 0.9500 . ?
C55 C56 1.452(15) . ?
C56 C57 1.412(15) . ?
C57 H57 0.9500 . ?
C58 C59 1.543(16) . ?
C59 C64 1.374(15) . ?
C59 C60 1.386(15) . ?
C60 C61 1.407(16) . ?
C60 H60 0.9500 . ?
C61 C62 1.347(16) . ?
C62 C63 1.400(16) . ?
C62 H62 0.9500 . ?
C63 C64 1.391(16) . ?
C63 C65 1.510(17) . ?
C64 H64 0.9500 . ?
C66 C67 1.521(16) . ?
C66 H66A 0.9900 . ?
C66 H66B 0.9900 . ?
C67 C72 1.371(16) . ?
C67 C68 1.393(16) . ?
C68 C69 1.368(17) . ?
C68 H68 0.9500 . ?
C69 C70 1.397(19) . ?
C70 C71 1.40(2) . ?
C70 H70 0.9500 . ?
C71 C72 1.381(17) . ?
C72 H72 0.9500 . ?
C73 C74 1.50(2) . ?
C73 H73A 0.9900 . ?
C73 H73B 0.9900 . ?
C74 C75 1.37(2) . ?
C74 C79 1.40(2) . ?
C75 C76 1.34(2) . ?
C75 H75 0.9500 . ?
C76 C77 1.41(3) . ?
C76 H76 0.9500 . ?
C77 C78 1.35(3) . ?
C77 H77 0.9500 . ?
C78 C79 1.40(2) . ?
C78 H78 0.9500 . ?
C79 H79 0.9500 . ?
C80 C81 1.56(2) . ?
C80 H80A 0.9900 . ?
C80 H80B 0.9900 . ?
C81 C86 1.37(2) . ?
C81 C82 1.38(2) . ?
C82 C83 1.37(2) . ?
C82 H82 0.9500 . ?
C83 C84 1.44(3) . ?
C83 H83 0.9500 . ?
C84 C85 1.35(2) . ?
C84 H84 0.9500 . ?
C85 C86 1.39(2) . ?
C85 H85 0.9500 . ?
C86 H86 0.9500 . ?
C87 C88 1.45(3) . ?
C87 H87A 0.9900 . ?
C87 H87B 0.9900 . ?
C88 H88A 0.9800 . ?
C88 H88B 0.9800 . ?
C88 H88C 0.9800 . ?
C89 C90 1.57(3) . ?
C89 H89A 0.9900 . ?
C89 H89B 0.9900 . ?
C90 H90A 0.9800 . ?
C90 H90B 0.9800 . ?
C90 H90C 0.9800 . ?
C91 C92 1.50(3) . ?
C91 H91A 0.9900 . ?
C91 H91B 0.9900 . ?
C92 H92A 0.9800 . ?
C92 H92B 0.9800 . ?
C92 H92C 0.9800 . ?
C93 C94 1.551(19) . ?
C93 H93A 0.9900 . ?
C93 H93B 0.9900 . ?
C94 H94A 0.9800 . ?
C94 H94B 0.9800 . ?
C94 H94C 0.9800 . ?
C95 C96 1.52(2) . ?
C95 H95A 0.9900 . ?
C95 H95B 0.9900 . ?
C96 H96A 0.9800 . ?
C96 H96B 0.9800 . ?
C96 H96C 0.9800 . ?
C97 C98 1.53(2) . ?
C97 H97A 0.9900 . ?
C97 H97B 0.9900 . ?
C98 H98A 0.9800 . ?
C98 H98B 0.9800 . ?
C98 H98C 0.9800 . ?
C99 C100 1.23(4) . ?
C99 H99A 0.9900 . ?
C99 H99B 0.9900 . ?
C100 H10A 0.9800 . ?
C100 H10B 0.9800 . ?
C100 H10C 0.9800 . ?
C101 C102 1.568(19) . ?
C101 H10D 0.9900 . ?
C101 H10E 0.9900 . ?
C102 H10F 0.9800 . ?
C102 H10G 0.9800 . ?
C102 H10H 0.9800 . ?
C103 C104 1.57(3) . ?
C103 H10I 0.9900 . ?
C103 H10J 0.9900 . ?
C104 H10K 0.9800 . ?
C104 H10L 0.9800 . ?
C104 H10M 0.9800 . ?
C105 C106 1.46(2) . ?
C105 H10N 0.9900 . ?
C105 H10O 0.9900 . ?
C106 H10P 0.9800 . ?
C106 H10Q 0.9800 . ?
C106 H10R 0.9800 . ?
C107 C108 1.56(2) . ?
C107 H10S 0.9900 . ?
C107 H10T 0.9900 . ?
C108 H10U 0.9800 . ?
C108 H10V 0.9800 . ?
C108 H10W 0.9800 . ?
C109 C110 1.51(2) . ?
C109 H10X 0.9900 . ?
C109 H10Y 0.9900 . ?
C110 H11A 0.9800 . ?
C110 H11B 0.9800 . ?
C110 H11C 0.9800 . ?
C111 C112 1.570(18) . ?
C111 H11D 0.9900 . ?
C111 H11E 0.9900 . ?
C112 H11F 0.9800 . ?
C112 H11G 0.9800 . ?
C112 H11H 0.9800 . ?
C113 C114 1.49(3) . ?
C113 H11I 0.9900 . ?
C113 H11J 0.9900 . ?
C114 H11K 0.9800 . ?
C114 H11L 0.9800 . ?
C114 H11M 0.9800 . ?
C115 C116 1.55(2) . ?
C115 H11N 0.9900 . ?
C115 H11O 0.9900 . ?
C116 H11P 0.9800 . ?
C116 H11Q 0.9800 . ?
C116 H11R 0.9800 . ?
C117 C118 1.56(2) . ?
C117 H11S 0.9900 . ?
C117 H11T 0.9900 . ?
C118 H11U 0.9800 . ?
C118 H11V 0.9800 . ?
C118 H11W 0.9800 . ?
C119 C120 1.33(4) . ?
C119 H11X 0.9900 . ?
C119 H11Y 0.9900 . ?
C120 H12A 0.9800 . ?
C120 H12B 0.9800 . ?
C120 H12C 0.9800 . ?
C121 C122 1.24(4) . ?
C121 H12E 0.9900 . ?
C121 H12F 0.9900 . ?
C122 H12G 0.9800 . ?
C122 H12H 0.9800 . ?
C122 H12I 0.9800 . ?
C123 C124 1.570(16) . ?
C123 H12J 0.9900 . ?
C123 H12K 0.9900 . ?
C124 H12L 0.9800 . ?
C124 H12M 0.9800 . ?
C124 H12N 0.9800 . ?
C125 C126 1.54(2) . ?
C125 H12O 0.9900 . ?
C125 H12P 0.9900 . ?
C126 H12Q 0.9800 . ?
C126 H12R 0.9800 . ?
C126 H12S 0.9800 . ?
C127 C128 1.54(2) . ?
C127 H12T 0.9900 . ?
C127 H12U 0.9900 . ?
C128 H12V 0.9800 . ?
C128 H12W 0.9800 . ?
C128 H12X 0.9800 . ?
C129 C130 1.55(3) . ?
C129 H12Y 0.9900 . ?
C129 H12Z 0.9900 . ?
C130 H13A 0.9800 . ?
C130 H13B 0.9800 . ?
C130 H13C 0.9800 . ?
C131 C132 1.36(3) . ?
C131 H13D 0.9900 . ?
C131 H13E 0.9900 . ?
C132 H13F 0.9800 . ?
C132 H13G 0.9800 . ?
C132 H13H 0.9800 . ?
C133 C134 1.29(7) . ?
C133 H13I 0.9900 . ?
C133 H13J 0.9900 . ?
C134 H13K 0.9800 . ?
C134 H13L 0.9800 . ?
C134 H13M 0.9800 . ?
O15 C136 1.25(2) . ?
C135 C136 1.407(16) . ?
C135 H13N 0.9800 . ?
C135 H13O 0.9800 . ?
C135 H13P 0.9800 . ?
C136 C137 1.540(16) . ?
C137 H13Q 0.9800 . ?
C137 H13R 0.9800 . ?
C137 H13S 0.9800 . ?
O16 C139 1.23(3) . ?
C138 C139 1.38(2) . ?
C138 H13T 0.9800 . ?
C138 H13U 0.9800 . ?
C138 H13V 0.9800 . ?
C139 C140 1.52(2) . ?
C140 H14A 0.9800 . ?
C140 H14B 0.9800 . ?
C140 H14C 0.9800 . ?
O17 C142 1.26(2) . ?
C141 C142 1.363(19) . ?
C141 H14D 0.9800 . ?
C141 H14E 0.9800 . ?
C141 H14F 0.9800 . ?
C142 C143 1.53(2) . ?
C143 H14G 0.9800 . ?
C143 H14H 0.9800 . ?
C143 H14I 0.9800 . ?
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
C1 Pt1 P1 C89 57.2(11) . . . . ?
O10 Pt1 P1 C89 -123.4(11) . . . . ?
P2 Pt1 P1 C89 84(3) . . . . ?
C1 Pt1 P1 C91 177.0(10) . . . . ?
O10 Pt1 P1 C91 -3.6(10) . . . . ?
P2 Pt1 P1 C91 -156(3) . . . . ?
C1 Pt1 P1 C87 -58.3(9) . . . . ?
O10 Pt1 P1 C87 121.0(9) . . . . ?
P2 Pt1 P1 C87 -32(3) . . . . ?
C1 Pt1 P2 C93 51.0(7) . . . . ?
O10 Pt1 P2 C93 -128.4(7) . . . . ?
P1 Pt1 P2 C93 24(3) . . . . ?
C1 Pt1 P2 C97 174.2(8) . . . . ?
O10 Pt1 P2 C97 -5.2(8) . . . . ?
P1 Pt1 P2 C97 148(3) . . . . ?
C1 Pt1 P2 C95 -70.9(7) . . . . ?
O10 Pt1 P2 C95 109.8(7) . . . . ?
P1 Pt1 P2 C95 -98(3) . . . . ?
C10 Pt2 P3 C101 1.9(13) . . . . ?
O1 Pt2 P3 C101 -177.1(13) . . . . ?
P4 Pt2 P3 C101 148(100) . . . . ?
C10 Pt2 P3 C103 119.1(10) . . . . ?
O1 Pt2 P3 C103 -59.9(10) . . . . ?
P4 Pt2 P3 C103 -95(99) . . . . ?
C10 Pt2 P3 C99 -130.3(13) . . . . ?
O1 Pt2 P3 C99 50.7(12) . . . . ?
P4 Pt2 P3 C99 16(100) . . . . ?
C10 Pt2 P4 C107 -21.0(8) . . . . ?
O1 Pt2 P4 C107 158.0(8) . . . . ?
P3 Pt2 P4 C107 -167(100) . . . . ?
C10 Pt2 P4 C109 -154.9(7) . . . . ?
O1 Pt2 P4 C109 24.1(6) . . . . ?
P3 Pt2 P4 C109 59(99) . . . . ?
C10 Pt2 P4 C105 91.4(7) . . . . ?
O1 Pt2 P4 C105 -89.7(6) . . . . ?
P3 Pt2 P4 C105 -55(100) . . . . ?
C44 Pt3 P5 C115 -33.3(7) . . . . ?
O3 Pt3 P5 C115 145.6(7) . . . . ?
P6 Pt3 P5 C115 42(2) . . . . ?
C44 Pt3 P5 C113 -156.4(8) . . . . ?
O3 Pt3 P5 C113 22.6(8) . . . . ?
P6 Pt3 P5 C113 -82(2) . . . . ?
C44 Pt3 P5 C111 85.0(9) . . . . ?
O3 Pt3 P5 C111 -96.1(9) . . . . ?
P6 Pt3 P5 C111 160(2) . . . . ?
C44 Pt3 P6 C119 51.3(17) . . . . ?
O3 Pt3 P6 C119 -127.6(17) . . . . ?
P5 Pt3 P6 C119 -24(3) . . . . ?
C44 Pt3 P6 C117 178.7(8) . . . . ?
O3 Pt3 P6 C117 -0.3(8) . . . . ?
P5 Pt3 P6 C117 104(2) . . . . ?
C44 Pt3 P6 C121 -70.2(9) . . . . ?
O3 Pt3 P6 C121 110.8(9) . . . . ?
P5 Pt3 P6 C121 -145(2) . . . . ?
C53 Pt4 P7 C127 -50.5(8) . . . . ?
O8 Pt4 P7 C127 128.9(8) . . . . ?
P8 Pt4 P7 C127 -148.5(13) . . . . ?
C53 Pt4 P7 C125 -179.9(7) . . . . ?
O8 Pt4 P7 C125 -0.5(7) . . . . ?
P8 Pt4 P7 C125 82.1(13) . . . . ?
C53 Pt4 P7 C123 62.9(7) . . . . ?
O8 Pt4 P7 C123 -117.7(6) . . . . ?
P8 Pt4 P7 C123 -35.1(14) . . . . ?
C53 Pt4 P8 C129 -135.6(9) . . . . ?
O8 Pt4 P8 C129 45.4(9) . . . . ?
P7 Pt4 P8 C129 -37.6(15) . . . . ?
C53 Pt4 P8 C133 -8.4(14) . . . . ?
O8 Pt4 P8 C133 172.7(13) . . . . ?
P7 Pt4 P8 C133 89.7(18) . . . . ?
C53 Pt4 P8 C131 115.5(9) . . . . ?
O8 Pt4 P8 C131 -63.4(9) . . . . ?
P7 Pt4 P8 C131 -146.4(13) . . . . ?
C10 Pt2 O1 C15 102(9) . . . . ?
P3 Pt2 O1 C15 -101.5(9) . . . . ?
P4 Pt2 O1 C15 78.4(9) . . . . ?
C44 Pt3 O3 C22 -134(23) . . . . ?
P6 Pt3 O3 C22 -73.5(12) . . . . ?
P5 Pt3 O3 C22 110.6(12) . . . . ?
C53 Pt4 O8 C58 84(7) . . . . ?
P7 Pt4 O8 C58 -85.3(9) . . . . ?
P8 Pt4 O8 C58 101.7(9) . . . . ?
C1 Pt1 O10 C65 -105(8) . . . . ?
P2 Pt1 O10 C65 -90.2(10) . . . . ?
P1 Pt1 O10 C65 91.3(10) . . . . ?
O10 Pt1 C1 C14 -76(8) . . . . ?
P2 Pt1 C1 C14 -90.8(10) . . . . ?
P1 Pt1 C1 C14 87.7(10) . . . . ?
O10 Pt1 C1 C2 102(8) . . . . ?
P2 Pt1 C1 C2 88.1(10) . . . . ?
P1 Pt1 C1 C2 -93.3(10) . . . . ?
C14 C1 C2 C3 4(2) . . . . ?
Pt1 C1 C2 C3 -174.7(12) . . . . ?
C1 C2 C3 C4 -2(3) . . . . ?
C2 C3 C4 C13 -1(2) . . . . ?
C2 C3 C4 C5 177.2(16) . . . . ?
C3 C4 C5 C6 -177.4(19) . . . . ?
C13 C4 C5 C6 1(3) . . . . ?
C4 C5 C6 C7 -3(3) . . . . ?
C5 C6 C7 C8 -177(2) . . . . ?
C5 C6 C7 C12 2(3) . . . . ?
C12 C7 C8 C9 1(3) . . . . ?
C6 C7 C8 C9 179(2) . . . . ?
C7 C8 C9 C10 -2(3) . . . . ?
C8 C9 C10 C11 2(3) . . . . ?
C8 C9 C10 Pt2 -179.9(16) . . . . ?
O1 Pt2 C10 C11 75(10) . . . . ?
P3 Pt2 C10 C11 -81.7(12) . . . . ?
P4 Pt2 C10 C11 98.4(12) . . . . ?
O1 Pt2 C10 C9 -103(9) . . . . ?
P3 Pt2 C10 C9 99.8(13) . . . . ?
P4 Pt2 C10 C9 -80.1(13) . . . . ?
C9 C10 C11 C12 1(2) . . . . ?
Pt2 C10 C11 C12 -178.0(10) . . . . ?
C8 C7 C12 C11 1(2) . . . . ?
C6 C7 C12 C11 -177.4(17) . . . . ?
C8 C7 C12 C13 -178.7(16) . . . . ?
C6 C7 C12 C13 2(3) . . . . ?
C10 C11 C12 C7 -2(2) . . . . ?
C10 C11 C12 C13 178.1(13) . . . . ?
C3 C4 C13 C14 2(2) . . . . ?
C5 C4 C13 C14 -176.0(13) . . . . ?
C3 C4 C13 C12 -178.4(14) . . . . ?
C5 C4 C13 C12 3(2) . . . . ?
C7 C12 C13 C4 -5(2) . . . . ?
C11 C12 C13 C4 174.9(13) . . . . ?
C7 C12 C13 C14 174.5(14) . . . . ?
C11 C12 C13 C14 -6(2) . . . . ?
C2 C1 C14 C13 -2.9(19) . . . . ?
Pt1 C1 C14 C13 176.0(9) . . . . ?
C4 C13 C14 C1 -0.2(19) . . . . ?
C12 C13 C14 C1 -179.6(12) . . . . ?
Pt2 O1 C15 O2 3.6(17) . . . . ?
Pt2 O1 C15 C16 -174.0(7) . . . . ?
O2 C15 C16 C17 3.7(17) . . . . ?
O1 C15 C16 C17 -178.5(11) . . . . ?
O2 C15 C16 C21 -174.2(12) . . . . ?
O1 C15 C16 C21 3.6(17) . . . . ?
C21 C16 C17 C18 -0.1(18) . . . . ?
C15 C16 C17 C18 -178.0(11) . . . . ?
C23 O5 C18 C17 169.4(11) . . . . ?
C23 O5 C18 C19 -10.7(19) . . . . ?
C16 C17 C18 O5 179.7(11) . . . . ?
C16 C17 C18 C19 -0.2(19) . . . . ?
O5 C18 C19 C20 -179.9(13) . . . . ?
C17 C18 C19 C20 0(2) . . . . ?
C18 C19 C20 C21 1(2) . . . . ?
C18 C19 C20 C22 178.0(14) . . . . ?
C19 C20 C21 C16 -1(2) . . . . ?
C22 C20 C21 C16 -178.1(14) . . . . ?
C17 C16 C21 C20 0.6(19) . . . . ?
C15 C16 C21 C20 178.5(12) . . . . ?
Pt3 O3 C22 O4 2(2) . . . . ?
Pt3 O3 C22 C20 176.7(10) . . . . ?
C21 C20 C22 O4 175.0(16) . . . . ?
C19 C20 C22 O4 -2(2) . . . . ?
C21 C20 C22 O3 0(2) . . . . ?
C19 C20 C22 O3 -177.4(14) . . . . ?
C18 O5 C23 C24 -164.8(11) . . . . ?
O5 C23 C24 C25 14.4(18) . . . . ?
O5 C23 C24 C29 -165.3(12) . . . . ?
C29 C24 C25 C26 -1(2) . . . . ?
C23 C24 C25 C26 179.0(13) . . . . ?
C30 O6 C26 C25 -17(2) . . . . ?
C30 O6 C26 C27 161.5(13) . . . . ?
C24 C25 C26 O6 -178.6(14) . . . . ?
C24 C25 C26 C27 2(2) . . . . ?
O6 C26 C27 C28 177.2(15) . . . . ?
C25 C26 C27 C28 -4(2) . . . . ?
C26 C27 C28 C29 4(2) . . . . ?
C26 C27 C28 O7 178.4(15) . . . . ?
C37 O7 C28 C27 -5(2) . . . . ?
C37 O7 C28 C29 170.4(15) . . . . ?
C27 C28 C29 C24 -2(2) . . . . ?
O7 C28 C29 C24 -177.7(13) . . . . ?
C25 C24 C29 C28 1(2) . . . . ?
C23 C24 C29 C28 -179.1(14) . . . . ?
C26 O6 C30 C31 77.7(17) . . . . ?
O6 C30 C31 C36 40.7(18) . . . . ?
O6 C30 C31 C32 -136.3(14) . . . . ?
C36 C31 C32 C33 5(2) . . . . ?
C30 C31 C32 C33 -178.2(13) . . . . ?
C31 C32 C33 C34 0(2) . . . . ?
C32 C33 C34 C35 -3(2) . . . . ?
C33 C34 C35 C36 2(3) . . . . ?
C32 C31 C36 C35 -6(2) . . . . ?
C30 C31 C36 C35 176.6(15) . . . . ?
C34 C35 C36 C31 3(3) . . . . ?
C28 O7 C37 C38 -179.8(14) . . . . ?
O7 C37 C38 C39 48(2) . . . . ?
O7 C37 C38 C43 -144.5(18) . . . . ?
C43 C38 C39 C40 -1(3) . . . . ?
C37 C38 C39 C40 167.3(17) . . . . ?
C38 C39 C40 C41 2(3) . . . . ?
C39 C40 C41 C42 -2(4) . . . . ?
C40 C41 C42 C43 1(4) . . . . ?
C41 C42 C43 C38 1(4) . . . . ?
C39 C38 C43 C42 -1(3) . . . . ?
C37 C38 C43 C42 -169(2) . . . . ?
O3 Pt3 C44 C57 -32(24) . . . . ?
P6 Pt3 C44 C57 -92.2(12) . . . . ?
P5 Pt3 C44 C57 83.8(12) . . . . ?
O3 Pt3 C44 C45 150(22) . . . . ?
P6 Pt3 C44 C45 89.8(12) . . . . ?
P5 Pt3 C44 C45 -94.3(12) . . . . ?
C57 C44 C45 C46 1(2) . . . . ?
Pt3 C44 C45 C46 178.8(13) . . . . ?
C44 C45 C46 C47 0(3) . . . . ?
C45 C46 C47 C56 -1(2) . . . . ?
C45 C46 C47 C48 -178.8(15) . . . . ?
C46 C47 C48 C49 178.9(14) . . . . ?
C56 C47 C48 C49 1(2) . . . . ?
C47 C48 C49 C50 -6(2) . . . . ?
C48 C49 C50 C51 -175.3(14) . . . . ?
C48 C49 C50 C55 5(2) . . . . ?
C55 C50 C51 C52 -3(2) . . . . ?
C49 C50 C51 C52 177.6(13) . . . . ?
C50 C51 C52 C53 1(2) . . . . ?
C51 C52 C53 C54 2(2) . . . . ?
C51 C52 C53 Pt4 -178.2(11) . . . . ?
O8 Pt4 C53 C54 105(7) . . . . ?
P7 Pt4 C53 C54 -84.8(11) . . . . ?
P8 Pt4 C53 C54 88.3(11) . . . . ?
O8 Pt4 C53 C52 -74(7) . . . . ?
P7 Pt4 C53 C52 95.8(11) . . . . ?
P8 Pt4 C53 C52 -91.2(11) . . . . ?
C52 C53 C54 C55 -3(2) . . . . ?
Pt4 C53 C54 C55 177.6(10) . . . . ?
C53 C54 C55 C50 1(2) . . . . ?
C53 C54 C55 C56 -176.4(13) . . . . ?
C51 C50 C55 C54 2.4(18) . . . . ?
C49 C50 C55 C54 -178.2(12) . . . . ?
C51 C50 C55 C56 179.6(12) . . . . ?
C49 C50 C55 C56 -1.0(19) . . . . ?
C46 C47 C56 C57 2(2) . . . . ?
C48 C47 C56 C57 179.9(12) . . . . ?
C46 C47 C56 C55 -174.7(13) . . . . ?
C48 C47 C56 C55 3(2) . . . . ?
C54 C55 C56 C57 -3(2) . . . . ?
C50 C55 C56 C57 -179.9(12) . . . . ?
C54 C55 C56 C47 174.1(12) . . . . ?
C50 C55 C56 C47 -2.9(19) . . . . ?
C45 C44 C57 C56 1(2) . . . . ?
Pt3 C44 C57 C56 -177.4(10) . . . . ?
C47 C56 C57 C44 -2(2) . . . . ?
C55 C56 C57 C44 174.8(13) . . . . ?
Pt4 O8 C58 O9 -4.1(19) . . . . ?
Pt4 O8 C58 C59 174.3(8) . . . . ?
O9 C58 C59 C64 170.0(13) . . . . ?
O8 C58 C59 C64 -8.5(18) . . . . ?
O9 C58 C59 C60 -10.2(19) . . . . ?
O8 C58 C59 C60 171.3(12) . . . . ?
C64 C59 C60 C61 -1.9(19) . . . . ?
C58 C59 C60 C61 178.3(12) . . . . ?
C66 O12 C61 C62 18(2) . . . . ?
C66 O12 C61 C60 -163.9(12) . . . . ?
C59 C60 C61 C62 1(2) . . . . ?
C59 C60 C61 O12 -177.3(12) . . . . ?
O12 C61 C62 C63 178.2(13) . . . . ?
C60 C61 C62 C63 0(2) . . . . ?
C61 C62 C63 C64 0(2) . . . . ?
C61 C62 C63 C65 -178.3(13) . . . . ?
C60 C59 C64 C63 2(2) . . . . ?
C58 C59 C64 C63 -178.4(12) . . . . ?
C62 C63 C64 C59 -1(2) . . . . ?
C65 C63 C64 C59 177.3(13) . . . . ?
Pt1 O10 C65 O11 -3(2) . . . . ?
Pt1 O10 C65 C63 176.7(9) . . . . ?
C64 C63 C65 O11 -177.3(14) . . . . ?
C62 C63 C65 O11 1(2) . . . . ?
C64 C63 C65 O10 3(2) . . . . ?
C62 C63 C65 O10 -179.4(13) . . . . ?
C61 O12 C66 C67 162.0(11) . . . . ?
O12 C66 C67 C72 170.0(12) . . . . ?
O12 C66 C67 C68 -9.4(17) . . . . ?
C72 C67 C68 C69 0(2) . . . . ?
C66 C67 C68 C69 179.2(13) . . . . ?
C73 O13 C69 C68 7(2) . . . . ?
C73 O13 C69 C70 -172.5(13) . . . . ?
C67 C68 C69 O13 179.6(13) . . . . ?
C67 C68 C69 C70 -1(2) . . . . ?
O13 C69 C70 C71 -179.9(14) . . . . ?
C68 C69 C70 C71 0(2) . . . . ?
C80 O14 C71 C72 -16(3) . . . . ?
C80 O14 C71 C70 164.9(17) . . . . ?
C69 C70 C71 O14 179.6(15) . . . . ?
C69 C70 C71 C72 1(3) . . . . ?
C68 C67 C72 C71 1(2) . . . . ?
C66 C67 C72 C71 -178.1(14) . . . . ?
O14 C71 C72 C67 179.8(16) . . . . ?
C70 C71 C72 C67 -2(2) . . . . ?
C69 O13 C73 C74 -72.9(17) . . . . ?
O13 C73 C74 C75 140.1(13) . . . . ?
O13 C73 C74 C79 -40.5(18) . . . . ?
C79 C74 C75 C76 -2(2) . . . . ?
C73 C74 C75 C76 177.1(14) . . . . ?
C74 C75 C76 C77 -1(2) . . . . ?
C75 C76 C77 C78 4(3) . . . . ?
C76 C77 C78 C79 -4(3) . . . . ?
C77 C78 C79 C74 1(3) . . . . ?
C75 C74 C79 C78 2(2) . . . . ?
C73 C74 C79 C78 -176.9(15) . . . . ?
C71 O14 C80 C81 -151.9(16) . . . . ?
O14 C80 C81 C86 -52(2) . . . . ?
O14 C80 C81 C82 130.1(18) . . . . ?
C86 C81 C82 C83 0(3) . . . . ?
C80 C81 C82 C83 177.7(17) . . . . ?
C81 C82 C83 C84 4(3) . . . . ?
C82 C83 C84 C85 -1(3) . . . . ?
C83 C84 C85 C86 -8(3) . . . . ?
C82 C81 C86 C85 -8(3) . . . . ?
C80 C81 C86 C85 174.6(18) . . . . ?
C84 C85 C86 C81 12(3) . . . . ?
C89 P1 C87 C88 59(2) . . . . ?
C91 P1 C87 C88 -50(2) . . . . ?
Pt1 P1 C87 C88 -179(2) . . . . ?
C91 P1 C89 C90 -65(2) . . . . ?
C87 P1 C89 C90 -178.7(17) . . . . ?
Pt1 P1 C89 C90 61.2(18) . . . . ?
C89 P1 C91 C92 -164.1(18) . . . . ?
C87 P1 C91 C92 -55.3(19) . . . . ?
Pt1 P1 C91 C92 70(2) . . . . ?
C97 P2 C93 C94 51.6(14) . . . . ?
C95 P2 C93 C94 -54.1(14) . . . . ?
Pt1 P2 C93 C94 -179.9(10) . . . . ?
C93 P2 C95 C96 179.8(14) . . . . ?
C97 P2 C95 C96 71.2(15) . . . . ?
Pt1 P2 C95 C96 -52.2(16) . . . . ?
C93 P2 C97 C98 62.5(14) . . . . ?
C95 P2 C97 C98 171.6(13) . . . . ?
Pt1 P2 C97 C98 -66.7(14) . . . . ?
C101 P3 C99 C100 -82(3) . . . . ?
C103 P3 C99 C100 173(3) . . . . ?
Pt2 P3 C99 C100 56(3) . . . . ?
C103 P3 C101 C102 163(2) . . . . ?
C99 P3 C101 C102 60(3) . . . . ?
Pt2 P3 C101 C102 -76(3) . . . . ?
C101 P3 C103 C104 59(2) . . . . ?
C99 P3 C103 C104 169(2) . . . . ?
Pt2 P3 C103 C104 -69(2) . . . . ?
C107 P4 C105 C106 -59.7(17) . . . . ?
C109 P4 C105 C106 52.2(17) . . . . ?
Pt2 P4 C105 C106 174.7(14) . . . . ?
C109 P4 C107 C108 63.1(16) . . . . ?
C105 P4 C107 C108 170.1(14) . . . . ?
Pt2 P4 C107 C108 -73.8(15) . . . . ?
C107 P4 C109 C110 -87.1(15) . . . . ?
C105 P4 C109 C110 167.9(13) . . . . ?
Pt2 P4 C109 C110 51.6(14) . . . . ?
C115 P5 C111 C112 172.0(18) . . . . ?
C113 P5 C111 C112 -77(2) . . . . ?
Pt3 P5 C111 C112 46(2) . . . . ?
C115 P5 C113 C114 -68.4(17) . . . . ?
C111 P5 C113 C114 -174.1(16) . . . . ?
Pt3 P5 C113 C114 59.4(17) . . . . ?
C113 P5 C115 C116 -50.0(16) . . . . ?
C111 P5 C115 C116 57.9(16) . . . . ?
Pt3 P5 C115 C116 -175.0(12) . . . . ?
C119 P6 C117 C118 71(2) . . . . ?
C121 P6 C117 C118 -179.2(16) . . . . ?
Pt3 P6 C117 C118 -63.7(17) . . . . ?
C117 P6 C119 C120 -84(3) . . . . ?
C121 P6 C119 C120 172(3) . . . . ?
Pt3 P6 C119 C120 51(4) . . . . ?
C119 P6 C121 C122 51(3) . . . . ?
C117 P6 C121 C122 -55(3) . . . . ?
Pt3 P6 C121 C122 179(3) . . . . ?
C127 P7 C123 C124 -171.3(14) . . . . ?
C125 P7 C123 C124 -59.4(15) . . . . ?
Pt4 P7 C123 C124 63.3(14) . . . . ?
C127 P7 C125 C126 53.7(16) . . . . ?
C123 P7 C125 C126 -50.8(16) . . . . ?
Pt4 P7 C125 C126 -172.1(12) . . . . ?
C125 P7 C127 C128 66.4(14) . . . . ?
C123 P7 C127 C128 174.7(13) . . . . ?
Pt4 P7 C127 C128 -65.2(14) . . . . ?
C133 P8 C129 C130 -79(2) . . . . ?
C131 P8 C129 C130 172.5(19) . . . . ?
Pt4 P8 C129 C130 54(2) . . . . ?
C129 P8 C131 C132 -170(2) . . . . ?
C133 P8 C131 C132 79(2) . . . . ?
Pt4 P8 C131 C132 -52(2) . . . . ?
C129 P8 C133 C134 4(5) . . . . ?
C131 P8 C133 C134 108(4) . . . . ?
Pt4 P8 C133 C134 -124(4) . . . . ?
