#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/06/02/4060221.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4060221
loop_
_publ_author_name
'Young-Joo Lee'
'Jong-Dae Lee'
'Sung-Joon Kim'
'Samrok Keum'
'Jaejung Ko'
'Il-Hwan Suh'
'Minserk Cheong'
'Sang Ook Kang'
_publ_section_title
;
 Synthesis, Structure, and DFT Calculation of
 (Phosphino-o-carboranyl)silyl Group 10 Metal Complexes: Formation of
 Stable trans-Bis(P,Si-chelate)metal Complexes
;
_journal_name_full               Organometallics
_journal_page_first              203
_journal_page_last               214
_journal_paper_doi               10.1021/om034112l
_journal_volume                  23
_journal_year                    2004
_chemical_formula_moiety
;
?
;
_chemical_formula_sum            'C19 H44 B20 P2 Pt Si2'
_chemical_formula_weight         810.03
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                104.516(5)
_cell_angle_beta                 106.106(4)
_cell_angle_gamma                98.033(4)
_cell_formula_units_Z            1
_cell_length_a                   8.6548(3)
_cell_length_b                   11.0158(8)
_cell_length_c                   11.0685(7)
_cell_measurement_reflns_used    25
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      14.11
_cell_measurement_theta_min      11.30
_cell_volume                     956.32(10)
_computing_cell_refinement       'CAD-4 software (Enraf-Nonius, 1988)'
_computing_data_collection       'CAD-4 software (Enraf-Nonius, 1988)'
_computing_data_reduction        'Xtal3.2 (Hall & Stewart, 1992)'
_computing_molecular_graphics    'ORTEP3 (Jonson & Burrett, 1998)'
_computing_publication_material  SHELXL-97(Sheldrick,1997)
_computing_structure_refinement  'SHELXL-93 (Sheldrick, 1993)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measurement_device_type  'Enraf-Nonius CAD-4'
_diffrn_measurement_method       ω/2θ
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71070
_diffrn_reflns_av_R_equivalents  0.0209
_diffrn_reflns_av_sigmaI/netI    0.0322
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       13
_diffrn_reflns_limit_k_min       -13
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -13
_diffrn_reflns_number            4060
_diffrn_reflns_theta_max         25.97
_diffrn_reflns_theta_min         1.96
_diffrn_standards_decay_%        2.83
_diffrn_standards_interval_count 3600
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    3.830
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  0.8110
_exptl_absorpt_correction_type   '\y scans'
_exptl_crystal_colour            'Pale Yellow'
_exptl_crystal_density_diffrn    1.413
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             400
_exptl_crystal_size_max          0.45
_exptl_crystal_size_mid          0.45
_exptl_crystal_size_min          0.3
_refine_diff_density_max         1.101
_refine_diff_density_min         -0.789
_refine_diff_density_rms         0.096
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_all   1.078
_refine_ls_goodness_of_fit_obs   1.071
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     199
_refine_ls_number_reflns         3758
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.078
_refine_ls_restrained_S_obs      1.071
_refine_ls_R_factor_all          0.0309
_refine_ls_R_factor_obs          0.0288
_refine_ls_shift/esd_max         5.158
_refine_ls_shift/esd_mean        0.236
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0479P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.0732
_refine_ls_wR_factor_obs         0.0722
_reflns_number_observed          3709
_reflns_number_total             3758
_reflns_observed_criterion       >2sigma(I)
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 

The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.0479P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(Fo^2^)+(0.0479P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_sg_symbol_H-M      P-1
_cod_original_formula_sum        'C19 H44 B20 P2 Si2 Pt'
_cod_database_code               4060221
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
Pt1 Pt 0.5000 0.0000 0.0000 0.03775(9) Uani 1 d S
P1 P 0.43397(13) 0.18993(10) 0.06950(10) 0.0447(2) Uani 1 d .
Si1 Si 0.32984(14) -0.01861(12) -0.21962(10) 0.0442(2) Uani 1 d .
C1 C 0.2456(5) 0.2101(4) -0.0492(4) 0.0444(9) Uani 1 d .
C2 C 0.1896(5) 0.1041(4) -0.2003(4) 0.0434(9) Uani 1 d .
C3 C 0.3837(7) 0.2266(6) 0.2212(5) 0.0698(15) Uani 1 d .
H3A H 0.2911(36) 0.1622(25) 0.2129(17) 0.105 Uiso 1 calc R
H3B H 0.3564(55) 0.3094(20) 0.2378(24) 0.105 Uiso 1 calc R
H3C H 0.4769(20) 0.2277(44) 0.2931(9) 0.105 Uiso 1 calc R
C4 C 0.5931(7) 0.3293(5) 0.0937(6) 0.0733(15) Uani 1 d .
H4A H 0.6192(42) 0.3219(23) 0.0137(15) 0.110 Uiso 1 calc R
H4B H 0.6904(22) 0.3331(26) 0.1636(32) 0.110 Uiso 1 calc R
H4C H 0.5536(23) 0.4063(6) 0.1165(47) 0.110 Uiso 1 calc R
C5 C 0.4314(7) 0.0242(7) -0.3375(5) 0.073(2) Uani 1 d .
H5A H 0.4965(48) -0.0365(27) -0.3587(37) 0.109 Uiso 1 calc R
H5B H 0.5012(46) 0.1091(19) -0.2973(19) 0.109 Uiso 1 calc R
H5C H 0.3483(7) 0.0221(46) -0.4168(20) 0.109 Uiso 1 calc R
C6 C 0.1731(6) -0.1748(5) -0.3165(5) 0.0659(13) Uani 1 d .
H6A H 0.1100(37) -0.1973(22) -0.2632(16) 0.099 Uiso 1 calc R
H6B H 0.2291(7) -0.2417(11) -0.3406(38) 0.099 Uiso 1 calc R
H6C H 0.1007(35) -0.1649(14) -0.3947(22) 0.099 Uiso 1 calc R
B3 B 0.0790(6) 0.0850(5) -0.0971(5) 0.0491(11) Uani 1 d .
H3 H 0.0769(6) 0.0049(5) -0.0546(5) 0.059 Uiso 1 calc R
B4 B 0.0758(7) 0.2434(6) -0.0081(6) 0.0580(13) Uani 1 d .
H4 H 0.0689(7) 0.2666(6) 0.0926(6) 0.070 Uiso 1 calc R
B5 B 0.1975(8) 0.3536(6) -0.0566(6) 0.0630(14) Uani 1 d .
H5 H 0.2700(8) 0.4478(6) 0.0127(6) 0.076 Uiso 1 calc R
B6 B 0.2715(7) 0.2636(5) -0.1757(6) 0.0566(13) Uani 1 d .
H6 H 0.3926(7) 0.2985(5) -0.1837(6) 0.068 Uiso 1 calc R
B7 B -0.0215(6) 0.0631(6) -0.2665(5) 0.0534(12) Uani 1 d .
H7 H -0.0926(6) -0.0316(6) -0.3353(5) 0.064 Uiso 1 calc R
B8 B -0.0955(7) 0.1508(6) -0.1458(6) 0.0607(13) Uani 1 d .
H8 H -0.2139(7) 0.1133(6) -0.1351(6) 0.073 Uiso 1 calc R
B9 B -0.0220(8) 0.3183(6) -0.1230(7) 0.069(2) Uani 1 d .
H9 H -0.0938(8) 0.3902(6) -0.0984(7) 0.083 Uiso 1 calc R
B10 B 0.0998(9) 0.3311(6) -0.2258(7) 0.071(2) Uani 1 d .
H10 H 0.1076(9) 0.4113(6) -0.2679(7) 0.086 Uiso 1 calc R
B11 B 0.1002(8) 0.1731(6) -0.3155(6) 0.0603(14) Uani 1 d .
H11 H 0.1089(8) 0.1498(6) -0.4157(6) 0.072 Uiso 1 calc R
B12 B -0.0825(8) 0.2069(6) -0.2818(6) 0.067(2) Uani 1 d .
H12 H -0.1936(8) 0.2063(6) -0.3601(6) 0.080 Uiso 1 calc R
C10 C 0.5647(18) 0.4271(14) 0.5766(14) 0.154(4) Uiso 1 d .
C11 C 0.4145(17) 0.4133(13) 0.5491(13) 0.157(4) Uiso 1 d .
C12 C 0.3564(20) 0.4880(15) 0.4774(16) 0.170(5) Uiso 1 d .
C13 C 0.2149(32) 0.4825(23) 0.4327(25) 0.276(11) Uiso 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
P1 Pt1 P1 180.0 . 2_655
P1 Pt1 Si1 87.88(4) . .
P1 Pt1 Si1 92.12(4) 2_655 .
P1 Pt1 Si1 92.12(4) . 2_655
P1 Pt1 Si1 87.88(4) 2_655 2_655
Si1 Pt1 Si1 180.0 . 2_655
C3 P1 C4 103.9(3) . .
C3 P1 C1 101.2(2) . .
C4 P1 C1 104.2(2) . .
C3 P1 Pt1 118.5(2) . .
C4 P1 Pt1 113.9(2) . .
C1 P1 Pt1 113.34(13) . .
C5 Si1 C6 105.9(3) . .
C5 Si1 C2 103.7(2) . .
C6 Si1 C2 102.1(2) . .
C5 Si1 Pt1 118.9(2) . .
C6 Si1 Pt1 117.6(2) . .
C2 Si1 Pt1 106.54(12) . .
C2 C1 B6 61.3(3) . .
C2 C1 B5 111.2(4) . .
B6 C1 B5 62.4(3) . .
C2 C1 B3 60.8(3) . .
B6 C1 B3 113.5(3) . .
B5 C1 B3 114.5(4) . .
C2 C1 B4 110.9(3) . .
B6 C1 B4 113.8(4) . .
B5 C1 B4 62.6(3) . .
B3 C1 B4 62.9(3) . .
C2 C1 P1 113.6(3) . .
B6 C1 P1 117.1(3) . .
B5 C1 P1 125.4(3) . .
B3 C1 P1 113.7(3) . .
B4 C1 P1 123.6(3) . .
C1 C2 B11 109.6(4) . .
C1 C2 B3 60.5(3) . .
B11 C2 B3 113.7(4) . .
C1 C2 B7 109.5(3) . .
B11 C2 B7 62.7(3) . .
B3 C2 B7 62.3(3) . .
C1 C2 B6 60.2(3) . .
B11 C2 B6 62.1(3) . .
B3 C2 B6 112.3(4) . .
B7 C2 B6 113.1(4) . .
C1 C2 Si1 114.6(3) . .
B11 C2 Si1 126.5(3) . .
B3 C2 Si1 113.5(3) . .
B7 C2 Si1 123.6(3) . .
B6 C2 Si1 118.4(3) . .
C1 B3 C2 58.7(3) . .
C1 B3 B7 105.5(4) . .
C2 B3 B7 58.9(3) . .
C1 B3 B8 105.2(4) . .
C2 B3 B8 105.9(4) . .
B7 B3 B8 59.8(3) . .
C1 B3 B4 58.8(3) . .
C2 B3 B4 106.0(4) . .
B7 B3 B4 107.1(4) . .
B8 B3 B4 59.4(3) . .
C1 B4 B8 105.4(4) . .
C1 B4 B9 105.1(4) . .
B8 B4 B9 61.0(4) . .
C1 B4 B5 58.5(3) . .
B8 B4 B5 109.2(4) . .
B9 B4 B5 60.3(4) . .
C1 B4 B3 58.4(3) . .
B8 B4 B3 60.0(3) . .
B9 B4 B3 108.3(4) . .
B5 B4 B3 107.5(4) . .
C1 B5 B10 105.1(4) . .
C1 B5 B6 58.8(3) . .
B10 B5 B6 60.1(4) . .
C1 B5 B4 58.9(3) . .
B10 B5 B4 107.7(4) . .
B6 B5 B4 107.9(4) . .
C1 B5 B9 105.1(4) . .
B10 B5 B9 59.8(4) . .
B6 B5 B9 107.9(4) . .
B4 B5 B9 59.8(4) . .
C1 B6 C2 58.5(3) . .
C1 B6 B11 105.4(4) . .
C2 B6 B11 58.4(3) . .
C1 B6 B5 58.8(3) . .
C2 B6 B5 106.2(4) . .
B11 B6 B5 108.3(4) . .
C1 B6 B10 105.0(4) . .
C2 B6 B10 105.4(4) . .
B11 B6 B10 60.2(3) . .
B5 B6 B10 59.9(4) . .
C2 B7 B8 106.0(4) . .
C2 B7 B12 105.7(4) . .
B8 B7 B12 60.7(4) . .
C2 B7 B3 58.8(3) . .
B8 B7 B3 60.1(3) . .
B12 B7 B3 108.3(4) . .
C2 B7 B11 58.4(3) . .
B8 B7 B11 109.0(4) . .
B12 B7 B11 60.5(4) . .
B3 B7 B11 107.5(4) . .
B4 B8 B7 108.2(4) . .
B4 B8 B3 60.6(3) . .
B7 B8 B3 60.0(3) . .
B4 B8 B12 107.0(4) . .
B7 B8 B12 59.7(3) . .
B3 B8 B12 107.4(4) . .
B4 B8 B9 59.8(3) . .
B7 B8 B9 106.9(5) . .
B3 B8 B9 107.7(4) . .
B12 B8 B9 58.8(4) . .
B12 B9 B10 60.6(4) . .
B12 B9 B4 107.8(4) . .
B10 B9 B4 107.6(4) . .
B12 B9 B5 108.2(5) . .
B10 B9 B5 59.6(4) . .
B4 B9 B5 60.0(3) . .
B12 B9 B8 60.4(4) . .
B10 B9 B8 108.4(5) . .
B4 B9 B8 59.2(3) . .
B5 B9 B8 107.4(4) . .
B5 B10 B6 60.0(3) . .
B5 B10 B9 60.6(4) . .
B6 B10 B9 108.4(4) . .
B5 B10 B11 108.1(4) . .
B6 B10 B11 59.9(3) . .
B9 B10 B11 108.1(5) . .
B5 B10 B12 108.0(5) . .
B6 B10 B12 108.1(4) . .
B9 B10 B12 59.4(4) . .
B11 B10 B12 60.4(4) . .
C2 B11 B6 59.4(3) . .
C2 B11 B10 105.8(4) . .
B6 B11 B10 59.9(3) . .
C2 B11 B7 58.9(3) . .
B6 B11 B7 107.9(4) . .
B10 B11 B7 107.6(4) . .
C2 B11 B12 105.3(4) . .
B6 B11 B12 107.7(4) . .
B10 B11 B12 60.0(4) . .
B7 B11 B12 59.5(3) . .
B9 B12 B7 108.4(4) . .
B9 B12 B10 59.9(4) . .
B7 B12 B10 107.7(4) . .
B9 B12 B11 107.9(4) . .
B7 B12 B11 59.9(3) . .
B10 B12 B11 59.6(4) . .
B9 B12 B8 60.8(4) . .
B7 B12 B8 59.6(3) . .
B10 B12 B8 108.1(4) . .
B11 B12 B8 107.6(4) . .
C11 C10 C12 116.2(14) . 2_666
C10 C11 C12 111.9(14) . .
C13 C12 C11 122.7(21) . .
C13 C12 C10 105.1(21) . 2_666
C11 C12 C10 131.7(15) . 2_666
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pt1 P1 2.2510(11) .
Pt1 P1 2.2510(11) 2_655
Pt1 Si1 2.4082(11) .
Pt1 Si1 2.4082(11) 2_655
P1 C3 1.813(5) .
P1 C4 1.824(5) .
P1 C1 1.869(4) .
Si1 C5 1.878(5) .
Si1 C6 1.888(5) .
Si1 C2 1.950(4) .
C1 C2 1.676(6) .
C1 B6 1.706(7) .
C1 B5 1.706(7) .
C1 B3 1.707(6) .
C1 B4 1.714(7) .
C2 B11 1.705(7) .
C2 B3 1.713(6) .
C2 B7 1.714(6) .
C2 B6 1.723(7) .
B3 B7 1.772(7) .
B3 B8 1.774(8) .
B3 B4 1.784(8) .
B4 B8 1.762(8) .
B4 B9 1.773(9) .
B4 B5 1.776(9) .
B5 B10 1.765(9) .
B5 B6 1.767(9) .
B5 B9 1.782(9) .
B6 B11 1.769(8) .
B6 B10 1.768(9) .
B7 B8 1.769(8) .
B7 B12 1.771(8) .
B7 B11 1.778(8) .
B8 B12 1.789(9) .
B8 B9 1.795(9) .
B9 B12 1.760(9) .
B9 B10 1.769(11) .
B10 B11 1.775(9) .
B10 B12 1.781(9) .
B11 B12 1.788(9) .
C10 C11 1.23(2) .
C10 C12 1.42(2) 2_666
C11 C12 1.34(2) .
C12 C13 1.17(3) .
C12 C10 1.42(2) 2_666
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
P1 Pt1 P1 C3 175.6(1000) 2_655 .
Si1 Pt1 P1 C3 137.0(2) . .
Si1 Pt1 P1 C3 -43.0(2) 2_655 .
P1 Pt1 P1 C4 -61.7(1000) 2_655 .
Si1 Pt1 P1 C4 -100.3(2) . .
Si1 Pt1 P1 C4 79.7(2) 2_655 .
P1 Pt1 P1 C1 57.2(1000) 2_655 .
Si1 Pt1 P1 C1 18.6(2) . .
Si1 Pt1 P1 C1 -161.4(2) 2_655 .
P1 Pt1 Si1 C5 99.6(2) . .
P1 Pt1 Si1 C5 -80.4(2) 2_655 .
Si1 Pt1 Si1 C5 -114.1(1000) 2_655 .
P1 Pt1 Si1 C6 -130.6(2) . .
P1 Pt1 Si1 C6 49.4(2) 2_655 .
Si1 Pt1 Si1 C6 15.7(1000) 2_655 .
P1 Pt1 Si1 C2 -16.94(14) . .
P1 Pt1 Si1 C2 163.06(14) 2_655 .
Si1 Pt1 Si1 C2 129.4(1000) 2_655 .
C3 P1 C1 C2 -143.4(3) . .
C4 P1 C1 C2 109.0(3) . .
Pt1 P1 C1 C2 -15.4(3) . .
C3 P1 C1 B6 148.1(4) . .
C4 P1 C1 B6 40.5(4) . .
Pt1 P1 C1 B6 -83.9(3) . .
C3 P1 C1 B5 74.0(5) . .
C4 P1 C1 B5 -33.6(5) . .
Pt1 P1 C1 B5 -158.0(4) . .
C3 P1 C1 B3 -76.3(4) . .
C4 P1 C1 B3 176.1(3) . .
Pt1 P1 C1 B3 51.7(3) . .
C3 P1 C1 B4 -4.1(4) . .
C4 P1 C1 B4 -111.8(4) . .
Pt1 P1 C1 B4 123.9(3) . .
B6 C1 C2 B11 -39.1(4) . .
B5 C1 C2 B11 -0.3(5) . .
B3 C1 C2 B11 106.8(4) . .
B4 C1 C2 B11 67.3(5) . .
P1 C1 C2 B11 -148.2(3) . .
B6 C1 C2 B3 -145.8(4) . .
B5 C1 C2 B3 -107.1(4) . .
B3 C1 C2 B3 0.0 . .
B4 C1 C2 B3 -39.4(4) . .
P1 C1 C2 B3 105.0(3) . .
B6 C1 C2 B7 -106.1(4) . .
B5 C1 C2 B7 -67.3(5) . .
B3 C1 C2 B7 39.8(3) . .
B4 C1 C2 B7 0.4(5) . .
P1 C1 C2 B7 144.8(3) . .
B6 C1 C2 B6 0.0 . .
B5 C1 C2 B6 38.8(4) . .
B3 C1 C2 B6 145.8(4) . .
B4 C1 C2 B6 106.4(4) . .
P1 C1 C2 B6 -109.1(3) . .
B6 C1 C2 Si1 110.0(3) . .
B5 C1 C2 Si1 148.8(3) . .
B3 C1 C2 Si1 -104.2(3) . .
B4 C1 C2 Si1 -143.6(3) . .
P1 C1 C2 Si1 0.8(4) . .
C5 Si1 C2 C1 -113.7(3) . .
C6 Si1 C2 C1 136.4(3) . .
Pt1 Si1 C2 C1 12.5(3) . .
C5 Si1 C2 B11 29.2(4) . .
C6 Si1 C2 B11 -80.7(4) . .
Pt1 Si1 C2 B11 155.5(3) . .
C5 Si1 C2 B3 179.4(3) . .
C6 Si1 C2 B3 69.5(3) . .
Pt1 Si1 C2 B3 -54.4(3) . .
C5 Si1 C2 B7 108.0(4) . .
C6 Si1 C2 B7 -1.8(4) . .
Pt1 Si1 C2 B7 -125.7(3) . .
C5 Si1 C2 B6 -45.6(4) . .
C6 Si1 C2 B6 -155.5(3) . .
Pt1 Si1 C2 B6 80.6(3) . .
C2 C1 B3 C2 0.0 . .
B6 C1 B3 C2 32.5(4) . .
B5 C1 B3 C2 101.6(4) . .
B4 C1 B3 C2 138.2(4) . .
P1 C1 B3 C2 -104.8(3) . .
C2 C1 B3 B7 -37.3(3) . .
B6 C1 B3 B7 -4.8(5) . .
B5 C1 B3 B7 64.3(5) . .
B4 C1 B3 B7 100.9(4) . .
P1 C1 B3 B7 -142.0(3) . .
C2 C1 B3 B8 -99.6(4) . .
B6 C1 B3 B8 -67.1(5) . .
B5 C1 B3 B8 2.0(5) . .
B4 C1 B3 B8 38.6(4) . .
P1 C1 B3 B8 155.7(3) . .
C2 C1 B3 B4 -138.2(4) . .
B6 C1 B3 B4 -105.7(4) . .
B5 C1 B3 B4 -36.6(4) . .
B4 C1 B3 B4 0.0 . .
P1 C1 B3 B4 117.0(4) . .
C1 C2 B3 C1 0.0 . .
B11 C2 B3 C1 -100.0(4) . .
B7 C2 B3 C1 -137.0(4) . .
B6 C2 B3 C1 -31.8(3) . .
Si1 C2 B3 C1 106.0(3) . .
C1 C2 B3 B7 137.0(4) . .
B11 C2 B3 B7 37.1(4) . .
B7 C2 B3 B7 0.000(1) . .
B6 C2 B3 B7 105.2(4) . .
Si1 C2 B3 B7 -117.0(3) . .
C1 C2 B3 B8 98.4(4) . .
B11 C2 B3 B8 -1.6(5) . .
B7 C2 B3 B8 -38.7(4) . .
B6 C2 B3 B8 66.6(4) . .
Si1 C2 B3 B8 -155.7(3) . .
C1 C2 B3 B4 36.4(3) . .
B11 C2 B3 B4 -63.6(5) . .
B7 C2 B3 B4 -100.7(4) . .
B6 C2 B3 B4 4.6(5) . .
Si1 C2 B3 B4 142.3(3) . .
C2 C1 B4 B8 -0.4(5) . .
B6 C1 B4 B8 66.4(5) . .
B5 C1 B4 B8 103.4(5) . .
B3 C1 B4 B8 -39.0(4) . .
P1 C1 B4 B8 -140.6(4) . .
C2 C1 B4 B9 -63.9(5) . .
B6 C1 B4 B9 2.9(5) . .
B5 C1 B4 B9 39.8(4) . .
B3 C1 B4 B9 -102.5(4) . .
P1 C1 B4 B9 155.9(3) . .
C2 C1 B4 B5 -103.8(4) . .
B6 C1 B4 B5 -37.0(4) . .
B5 C1 B4 B5 0.0 . .
B3 C1 B4 B5 -142.3(4) . .
P1 C1 B4 B5 116.1(4) . .
C2 C1 B4 B3 38.5(3) . .
B6 C1 B4 B3 105.3(4) . .
B5 C1 B4 B3 142.3(4) . .
B3 C1 B4 B3 0.0 . .
P1 C1 B4 B3 -101.6(4) . .
C1 B3 B4 C1 0.0 . .
C2 B3 B4 C1 -36.3(3) . .
B7 B3 B4 C1 -98.1(4) . .
B8 B3 B4 C1 -135.6(4) . .
C1 B3 B4 B8 135.6(4) . .
C2 B3 B4 B8 99.3(4) . .
B7 B3 B4 B8 37.5(4) . .
B8 B3 B4 B8 0.0 . .
C1 B3 B4 B9 96.8(5) . .
C2 B3 B4 B9 60.5(5) . .
B7 B3 B4 B9 -1.2(5) . .
B8 B3 B4 B9 -38.8(4) . .
C1 B3 B4 B5 33.1(3) . .
C2 B3 B4 B5 -3.2(5) . .
B7 B3 B4 B5 -64.9(5) . .
B8 B3 B4 B5 -102.5(5) . .
C2 C1 B5 B10 1.5(5) . .
B6 C1 B5 B10 39.8(4) . .
B3 C1 B5 B10 -65.0(5) . .
B4 C1 B5 B10 -101.8(5) . .
P1 C1 B5 B10 144.8(4) . .
C2 C1 B5 B6 -38.3(3) . .
B6 C1 B5 B6 0.0 . .
B3 C1 B5 B6 -104.9(4) . .
B4 C1 B5 B6 -141.6(4) . .
P1 C1 B5 B6 105.0(4) . .
C2 C1 B5 B4 103.3(4) . .
B6 C1 B5 B4 141.6(4) . .
B3 C1 B5 B4 36.7(4) . .
B4 C1 B5 B4 0.0 . .
P1 C1 B5 B4 -113.4(4) . .
C2 C1 B5 B9 63.7(5) . .
B6 C1 B5 B9 102.0(5) . .
B3 C1 B5 B9 -2.8(6) . .
B4 C1 B5 B9 -39.6(4) . .
P1 C1 B5 B9 -152.9(4) . .
C1 B4 B5 C1 0.0 . .
B8 B4 B5 C1 -96.7(4) . .
B9 B4 B5 C1 -134.6(4) . .
B3 B4 B5 C1 -33.1(3) . .
C1 B4 B5 B10 97.4(4) . .
B8 B4 B5 B10 0.7(5) . .
B9 B4 B5 B10 -37.2(4) . .
B3 B4 B5 B10 64.3(5) . .
C1 B4 B5 B6 33.9(3) . .
B8 B4 B5 B6 -62.7(5) . .
B9 B4 B5 B6 -100.7(5) . .
B3 B4 B5 B6 0.8(5) . .
C1 B4 B5 B9 134.6(4) . .
B8 B4 B5 B9 37.9(4) . .
B9 B4 B5 B9 0.0 . .
B3 B4 B5 B9 101.5(4) . .
C2 C1 B6 C2 0.0 . .
B5 C1 B6 C2 -138.8(4) . .
B3 C1 B6 C2 -32.3(4) . .
B4 C1 B6 C2 -101.7(4) . .
P1 C1 B6 C2 103.4(3) . .
C2 C1 B6 B11 36.4(3) . .
B5 C1 B6 B11 -102.4(4) . .
B3 C1 B6 B11 4.1(5) . .
B4 C1 B6 B11 -65.3(5) . .
P1 C1 B6 B11 139.8(3) . .
C2 C1 B6 B5 138.8(4) . .
B5 C1 B6 B5 0.0 . .
B3 C1 B6 B5 106.5(4) . .
B4 C1 B6 B5 37.1(4) . .
P1 C1 B6 B5 -117.9(4) . .
C2 C1 B6 B10 99.1(4) . .
B5 C1 B6 B10 -39.7(4) . .
B3 C1 B6 B10 66.8(5) . .
B4 C1 B6 B10 -2.6(5) . .
P1 C1 B6 B10 -157.6(3) . .
C1 C2 B6 C1 0.0 . .
B11 C2 B6 C1 137.8(4) . .
B3 C2 B6 C1 31.9(3) . .
B7 C2 B6 C1 100.0(4) . .
Si1 C2 B6 C1 -103.6(3) . .
C1 C2 B6 B11 -137.8(4) . .
B11 C2 B6 B11 0.0 . .
B3 C2 B6 B11 -105.9(4) . .
B7 C2 B6 B11 -37.8(4) . .
Si1 C2 B6 B11 118.6(4) . .
C1 C2 B6 B5 -35.9(3) . .
B11 C2 B6 B5 101.9(4) . .
B3 C2 B6 B5 -4.1(5) . .
B7 C2 B6 B5 64.1(5) . .
Si1 C2 B6 B5 -139.6(3) . .
C1 C2 B6 B10 -98.4(4) . .
B11 C2 B6 B10 39.4(4) . .
B3 C2 B6 B10 -66.6(5) . .
B7 C2 B6 B10 1.6(5) . .
Si1 C2 B6 B10 158.0(4) . .
C1 B5 B6 C1 0.0 . .
B10 B5 B6 C1 -134.5(4) . .
B4 B5 B6 C1 -34.0(3) . .
B9 B5 B6 C1 -97.1(4) . .
C1 B5 B6 C2 35.8(3) . .
B10 B5 B6 C2 -98.7(4) . .
B4 B5 B6 C2 1.8(5) . .
B9 B5 B6 C2 -61.3(5) . .
C1 B5 B6 B11 97.3(4) . .
B10 B5 B6 B11 -37.2(4) . .
B4 B5 B6 B11 63.3(5) . .
B9 B5 B6 B11 0.2(5) . .
C1 B5 B6 B10 134.5(4) . .
B10 B5 B6 B10 0.0 . .
B4 B5 B6 B10 100.5(5) . .
B9 B5 B6 B10 37.4(4) . .
C1 C2 B7 B8 -0.2(5) . .
B11 C2 B7 B8 -102.8(5) . .
B3 C2 B7 B8 38.8(4) . .
B6 C2 B7 B8 -65.2(5) . .
Si1 C2 B7 B8 139.9(3) . .
C1 C2 B7 B12 63.2(5) . .
B11 C2 B7 B12 -39.4(4) . .
B3 C2 B7 B12 102.2(4) . .
B6 C2 B7 B12 -1.8(5) . .
Si1 C2 B7 B12 -156.7(3) . .
C1 C2 B7 B3 -39.0(3) . .
B11 C2 B7 B3 -141.6(4) . .
B3 C2 B7 B3 0.0 . .
B6 C2 B7 B3 -104.0(4) . .
Si1 C2 B7 B3 101.0(4) . .
C1 C2 B7 B11 102.6(4) . .
B11 C2 B7 B11 0.000(1) . .
B3 C2 B7 B11 141.6(4) . .
B6 C2 B7 B11 37.5(4) . .
Si1 C2 B7 B11 -117.4(4) . .
C1 B3 B7 C2 37.2(3) . .
C2 B3 B7 C2 0.0 . .
B8 B3 B7 C2 136.0(4) . .
B4 B3 B7 C2 98.7(4) . .
C1 B3 B7 B8 -98.8(4) . .
C2 B3 B7 B8 -136.0(4) . .
B8 B3 B7 B8 0.0 . .
B4 B3 B7 B8 -37.3(4) . .
C1 B3 B7 B12 -60.5(5) . .
C2 B3 B7 B12 -97.7(4) . .
B8 B3 B7 B12 38.3(4) . .
B4 B3 B7 B12 1.0(5) . .
C1 B3 B7 B11 3.5(5) . .
C2 B3 B7 B11 -33.7(4) . .
B8 B3 B7 B11 102.3(4) . .
B4 B3 B7 B11 64.9(5) . .
C1 B4 B8 B7 0.3(6) . .
B9 B4 B8 B7 99.3(5) . .
B5 B4 B8 B7 61.7(5) . .
B3 B4 B8 B7 -37.9(4) . .
C1 B4 B8 B3 38.2(4) . .
B9 B4 B8 B3 137.2(4) . .
B5 B4 B8 B3 99.6(4) . .
B3 B4 B8 B3 0.0 . .
C1 B4 B8 B12 -62.6(5) . .
B9 B4 B8 B12 36.4(4) . .
B5 B4 B8 B12 -1.2(5) . .
B3 B4 B8 B12 -100.8(4) . .
C1 B4 B8 B9 -99.0(5) . .
B9 B4 B8 B9 0.0 . .
B5 B4 B8 B9 -37.6(4) . .
B3 B4 B8 B9 -137.2(4) . .
C2 B7 B8 B4 -0.1(5) . .
B12 B7 B8 B4 -99.4(5) . .
B3 B7 B8 B4 38.1(4) . .
B11 B7 B8 B4 -61.6(5) . .
C2 B7 B8 B3 -38.2(3) . .
B12 B7 B8 B3 -137.6(4) . .
B3 B7 B8 B3 0.0 . .
B11 B7 B8 B3 -99.7(4) . .
C2 B7 B8 B12 99.3(4) . .
B12 B7 B8 B12 0.000(1) . .
B3 B7 B8 B12 137.6(4) . .
B11 B7 B8 B12 37.9(4) . .
C2 B7 B8 B9 62.9(5) . .
B12 B7 B8 B9 -36.5(4) . .
B3 B7 B8 B9 101.1(4) . .
B11 B7 B8 B9 1.4(5) . .
C1 B3 B8 B4 -38.3(4) . .
C2 B3 B8 B4 -99.5(4) . .
B7 B3 B8 B4 -137.7(4) . .
B4 B3 B8 B4 0.0 . .
C1 B3 B8 B7 99.4(4) . .
C2 B3 B8 B7 38.2(3) . .
B7 B3 B8 B7 0.000(2) . .
B4 B3 B8 B7 137.7(4) . .
C1 B3 B8 B12 61.7(5) . .
C2 B3 B8 B12 0.6(5) . .
B7 B3 B8 B12 -37.6(4) . .
B4 B3 B8 B12 100.0(5) . .
C1 B3 B8 B9 -0.3(5) . .
C2 B3 B8 B9 -61.4(5) . .
B7 B3 B8 B9 -99.6(5) . .
B4 B3 B8 B9 38.1(4) . .
C1 B4 B9 B12 62.2(5) . .
B8 B4 B9 B12 -37.3(4) . .
B5 B4 B9 B12 101.1(5) . .
B3 B4 B9 B12 1.0(6) . .
C1 B4 B9 B10 -1.8(6) . .
B8 B4 B9 B10 -101.3(5) . .
B5 B4 B9 B10 37.1(4) . .
B3 B4 B9 B10 -63.0(5) . .
C1 B4 B9 B5 -39.0(4) . .
B8 B4 B9 B5 -138.4(4) . .
B5 B4 B9 B5 0.0 . .
B3 B4 B9 B5 -100.1(4) . .
C1 B4 B9 B8 99.5(4) . .
B8 B4 B9 B8 0.0 . .
B5 B4 B9 B8 138.4(4) . .
B3 B4 B9 B8 38.3(4) . .
C1 B5 B9 B12 -61.3(6) . .
B10 B5 B9 B12 37.7(4) . .
B6 B5 B9 B12 0.2(6) . .
B4 B5 B9 B12 -100.5(5) . .
C1 B5 B9 B10 -99.0(5) . .
B10 B5 B9 B10 0.000(1) . .
B6 B5 B9 B10 -37.5(4) . .
B4 B5 B9 B10 -138.2(4) . .
C1 B5 B9 B4 39.2(4) . .
B10 B5 B9 B4 138.2(4) . .
B6 B5 B9 B4 100.7(4) . .
B4 B5 B9 B4 0.0 . .
C1 B5 B9 B8 2.5(6) . .
B10 B5 B9 B8 101.5(5) . .
B6 B5 B9 B8 64.0(6) . .
B4 B5 B9 B8 -36.7(4) . .
B4 B8 B9 B12 138.5(4) . .
B7 B8 B9 B12 36.9(4) . .
B3 B8 B9 B12 100.0(4) . .
B12 B8 B9 B12 0.0 . .
B4 B8 B9 B10 100.0(5) . .
B7 B8 B9 B10 -1.6(5) . .
B3 B8 B9 B10 61.6(5) . .
B12 B8 B9 B10 -38.5(4) . .
B4 B8 B9 B4 0.0 . .
B7 B8 B9 B4 -101.6(4) . .
B3 B8 B9 B4 -38.4(4) . .
B12 B8 B9 B4 -138.5(4) . .
B4 B8 B9 B5 37.0(4) . .
B7 B8 B9 B5 -64.6(5) . .
B3 B8 B9 B5 -1.4(6) . .
B12 B8 B9 B5 -101.4(5) . .
C1 B5 B10 B6 -39.2(4) . .
B6 B5 B10 B6 0.0 . .
B4 B5 B10 B6 -100.8(4) . .
B9 B5 B10 B6 -138.0(4) . .
C1 B5 B10 B9 98.9(5) . .
B6 B5 B10 B9 138.0(4) . .
B4 B5 B10 B9 37.2(4) . .
B9 B5 B10 B9 0.0 . .
C1 B5 B10 B11 -2.1(6) . .
B6 B5 B10 B11 37.1(4) . .
B4 B5 B10 B11 -63.8(6) . .
B9 B5 B10 B11 -101.0(5) . .
C1 B5 B10 B12 61.8(6) . .
B6 B5 B10 B12 100.9(5) . .
B4 B5 B10 B12 0.1(6) . .
B9 B5 B10 B12 -37.1(4) . .
C1 B6 B10 B5 39.2(4) . .
C2 B6 B10 B5 100.0(4) . .
B11 B6 B10 B5 138.6(4) . .
B5 B6 B10 B5 0.0 . .
C1 B6 B10 B9 1.3(5) . .
C2 B6 B10 B9 62.2(5) . .
B11 B6 B10 B9 100.7(5) . .
B5 B6 B10 B9 -37.8(4) . .
C1 B6 B10 B11 -99.4(4) . .
C2 B6 B10 B11 -38.5(4) . .
B11 B6 B10 B11 0.0 . .
B5 B6 B10 B11 -138.6(4) . .
C1 B6 B10 B12 -61.6(5) . .
C2 B6 B10 B12 -0.7(6) . .
B11 B6 B10 B12 37.8(4) . .
B5 B6 B10 B12 -100.8(5) . .
B12 B9 B10 B5 -138.2(4) . .
B4 B9 B10 B5 -37.3(4) . .
B5 B9 B10 B5 0.0 . .
B8 B9 B10 B5 -99.9(4) . .
B12 B9 B10 B6 -100.6(5) . .
B4 B9 B10 B6 0.3(6) . .
B5 B9 B10 B6 37.6(4) . .
B8 B9 B10 B6 -62.2(5) . .
B12 B9 B10 B11 -37.2(4) . .
B4 B9 B10 B11 63.8(5) . .
B5 B9 B10 B11 101.0(5) . .
B8 B9 B10 B11 1.2(6) . .
B12 B9 B10 B12 0.0 . .
B4 B9 B10 B12 100.9(5) . .
B5 B9 B10 B12 138.2(4) . .
B8 B9 B10 B12 38.4(4) . .
C1 C2 B11 B6 38.2(4) . .
B3 C2 B11 B6 103.7(4) . .
B7 C2 B11 B6 140.6(4) . .
B6 C2 B11 B6 0.0 . .
Si1 C2 B11 B6 -106.2(4) . .
C1 C2 B11 B10 -1.1(5) . .
B3 C2 B11 B10 64.4(5) . .
B7 C2 B11 B10 101.3(5) . .
B6 C2 B11 B10 -39.3(4) . .
Si1 C2 B11 B10 -145.5(4) . .
C1 C2 B11 B7 -102.4(4) . .
B3 C2 B11 B7 -36.9(4) . .
B7 C2 B11 B7 0.0 . .
B6 C2 B11 B7 -140.6(4) . .
Si1 C2 B11 B7 113.2(4) . .
C1 C2 B11 B12 -63.6(5) . .
B3 C2 B11 B12 1.9(5) . .
B7 C2 B11 B12 38.8(4) . .
B6 C2 B11 B12 -101.8(5) . .
Si1 C2 B11 B12 152.0(3) . .
C1 B6 B11 C2 -36.5(3) . .
C2 B6 B11 C2 0.0 . .
B5 B6 B11 C2 -98.1(4) . .
B10 B6 B11 C2 -135.2(4) . .
C1 B6 B11 B10 98.7(5) . .
C2 B6 B11 B10 135.2(4) . .
B5 B6 B11 B10 37.1(4) . .
B10 B6 B11 B10 0.0 . .
C1 B6 B11 B7 -1.6(5) . .
C2 B6 B11 B7 34.8(4) . .
B5 B6 B11 B7 -63.3(5) . .
B10 B6 B11 B7 -100.4(5) . .
C1 B6 B11 B12 61.2(5) . .
C2 B6 B11 B12 97.7(4) . .
B5 B6 B11 B12 -0.4(5) . .
B10 B6 B11 B12 -37.5(4) . .
B5 B10 B11 C2 2.0(6) . .
B6 B10 B11 C2 39.1(4) . .
B9 B10 B11 C2 -62.1(5) . .
B12 B10 B11 C2 -98.8(4) . .
B5 B10 B11 B6 -37.1(4) . .
B6 B10 B11 B6 0.0 . .
B9 B10 B11 B6 -101.2(5) . .
B12 B10 B11 B6 -137.9(5) . .
B5 B10 B11 B7 63.8(5) . .
B6 B10 B11 B7 100.9(4) . .
B9 B10 B11 B7 -0.3(5) . .
B12 B10 B11 B7 -37.1(4) . .
B5 B10 B11 B12 100.8(5) . .
B6 B10 B11 B12 137.9(5) . .
B9 B10 B11 B12 36.8(4) . .
B12 B10 B11 B12 0.0 . .
C2 B7 B11 C2 0.0 . .
B8 B7 B11 C2 97.5(4) . .
B12 B7 B11 C2 135.5(4) . .
B3 B7 B11 C2 33.9(3) . .
C2 B7 B11 B6 -35.0(4) . .
B8 B7 B11 B6 62.5(5) . .
B12 B7 B11 B6 100.5(5) . .
B3 B7 B11 B6 -1.2(5) . .
C2 B7 B11 B10 -98.2(4) . .
B8 B7 B11 B10 -0.7(5) . .
B12 B7 B11 B10 37.3(4) . .
B3 B7 B11 B10 -64.4(5) . .
C2 B7 B11 B12 -135.5(4) . .
B8 B7 B11 B12 -38.0(4) . .
B12 B7 B11 B12 0.000(1) . .
B3 B7 B11 B12 -101.6(4) . .
B10 B9 B12 B7 100.2(5) . .
B4 B9 B12 B7 -0.4(6) . .
B5 B9 B12 B7 63.0(6) . .
B8 B9 B12 B7 -37.2(4) . .
B10 B9 B12 B10 0.0 . .
B4 B9 B12 B10 -100.6(5) . .
B5 B9 B12 B10 -37.2(4) . .
B8 B9 B12 B10 -137.4(4) . .
B10 B9 B12 B11 36.8(4) . .
B4 B9 B12 B11 -63.8(6) . .
B5 B9 B12 B11 -0.4(6) . .
B8 B9 B12 B11 -100.6(4) . .
B10 B9 B12 B8 137.4(4) . .
B4 B9 B12 B8 36.8(4) . .
B5 B9 B12 B8 100.1(5) . .
B8 B9 B12 B8 0.0 . .
C2 B7 B12 B9 -62.1(5) . .
B8 B7 B12 B9 37.7(4) . .
B3 B7 B12 B9 -0.4(6) . .
B11 B7 B12 B9 -100.5(5) . .
C2 B7 B12 B10 1.3(6) . .
B8 B7 B12 B10 101.1(5) . .
B3 B7 B12 B10 63.0(6) . .
B11 B7 B12 B10 -37.1(4) . .
C2 B7 B12 B11 38.4(4) . .
B8 B7 B12 B11 138.2(4) . .
B3 B7 B12 B11 100.1(4) . .
B11 B7 B12 B11 0.000(1) . .
C2 B7 B12 B8 -99.8(4) . .
B8 B7 B12 B8 0.0 . .
B3 B7 B12 B8 -38.1(4) . .
B11 B7 B12 B8 -138.2(4) . .
B5 B10 B12 B9 37.6(4) . .
B6 B10 B12 B9 101.1(5) . .
B9 B10 B12 B9 0.0 . .
B11 B10 B12 B9 138.7(4) . .
B5 B10 B12 B7 -63.8(6) . .
B6 B10 B12 B7 -0.3(7) . .
B9 B10 B12 B7 -101.4(5) . .
B11 B10 B12 B7 37.2(4) . .
B5 B10 B12 B11 -101.1(5) . .
B6 B10 B12 B11 -37.6(4) . .
B9 B10 B12 B11 -138.7(4) . .
B11 B10 B12 B11 0.0 . .
B5 B10 B12 B8 -0.9(6) . .
B6 B10 B12 B8 62.6(6) . .
B9 B10 B12 B8 -38.5(4) . .
B11 B10 B12 B8 100.2(4) . .
C2 B11 B12 B9 62.8(5) . .
B6 B11 B12 B9 0.5(6) . .
B10 B11 B12 B9 -36.9(4) . .
B7 B11 B12 B9 101.3(5) . .
C2 B11 B12 B7 -38.5(4) . .
B6 B11 B12 B7 -100.8(4) . .
B10 B11 B12 B7 -138.2(4) . .
B7 B11 B12 B7 0.000(1) . .
C2 B11 B12 B10 99.7(4) . .
B6 B11 B12 B10 37.5(4) . .
B10 B11 B12 B10 0.0 . .
B7 B11 B12 B10 138.2(4) . .
C2 B11 B12 B8 -1.4(5) . .
B6 B11 B12 B8 -63.6(5) . .
B10 B11 B12 B8 -101.1(5) . .
B7 B11 B12 B8 37.1(4) . .
B4 B8 B12 B9 -36.8(4) . .
B7 B8 B12 B9 -138.3(4) . .
B3 B8 B12 B9 -100.6(4) . .
B9 B8 B12 B9 0.0 . .
B4 B8 B12 B7 101.5(4) . .
B7 B8 B12 B7 0.000(2) . .
B3 B8 B12 B7 37.8(4) . .
B9 B8 B12 B7 138.3(4) . .
B4 B8 B12 B10 1.3(6) . .
B7 B8 B12 B10 -100.2(5) . .
B3 B8 B12 B10 -62.5(5) . .
B9 B8 B12 B10 38.1(4) . .
B4 B8 B12 B11 64.3(5) . .
B7 B8 B12 B11 -37.3(4) . .
B3 B8 B12 B11 0.5(6) . .
B9 B8 B12 B11 101.1(5) . .
C12 C10 C11 C12 -3.2(24) 2_666 .
C10 C11 C12 C13 174.2(22) . .
C10 C11 C12 C10 3.8(29) . 2_666
