#------------------------------------------------------------------------------
#$Date: 2018-08-16 19:56:20 +0300 (Thu, 16 Aug 2018) $
#$Revision: 209818 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/06/08/4060885.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4060885
loop_
_publ_author_name
'Landis, Clark R.'
'Nelson, Ryan C.'
'Jin, Wiechang'
'Bowman, Amanda C.'
_publ_section_title
;
 Synthesis, Characterization, and Transition-Metal Complexes of
 3,4-Diazaphospholanes
;
_journal_coden_ASTM              ORGND7
_journal_issue                   6
_journal_name_full               Organometallics
_journal_page_first              1377
_journal_page_last               1391
_journal_paper_doi               10.1021/om050922g
_journal_volume                  25
_journal_year                    2006
_chemical_formula_sum            'C105 H82 Cl12 N8 O8 P4 Rh2'
_chemical_formula_weight         2338.89
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 101.197(2)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   25.768(2)
_cell_length_b                   13.8071(12)
_cell_length_c                   33.211(3)
_cell_measurement_temperature    173(2)
_cell_volume                     11591.1(17)
_diffrn_ambient_temperature      173(2)
_exptl_crystal_density_diffrn    1.340
_cod_duplicate_entry             4074830
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4060885
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Rh1 Rh 0.198186(15) 0.46442(3) 0.329432(11) 0.02714(12) Uani 1 1 d . . .
Rh2 Rh 0.313311(15) 0.53412(3) 0.397188(11) 0.02753(12) Uani 1 1 d . . .
Cl1 Cl 0.29144(5) 0.45352(12) 0.33280(4) 0.0433(4) Uani 1 1 d . . .
Cl2 Cl 0.22070(5) 0.52472(12) 0.39803(4) 0.0439(4) Uani 1 1 d . . .
P1 P 0.18040(5) 0.41596(11) 0.26687(4) 0.0313(3) Uani 1 1 d . . .
P2 P 0.11396(5) 0.46372(11) 0.32559(4) 0.0264(3) Uani 1 1 d . . .
P3 P 0.39719(5) 0.53875(11) 0.39951(4) 0.0263(3) Uani 1 1 d . . .
P4 P 0.33056(5) 0.60948(11) 0.45455(4) 0.0311(4) Uani 1 1 d . . .
O1 O 0.26671(15) 0.1670(3) 0.21793(12) 0.0515(11) Uani 1 1 d . . .
O2 O 0.1929(2) 0.4919(4) 0.13929(12) 0.0748(15) Uani 1 1 d . . .
O5 O 0.47443(15) 0.6668(3) 0.29852(11) 0.0515(11) Uani 1 1 d . . .
O6 O 0.53518(15) 0.3499(3) 0.38846(11) 0.0485(11) Uani 1 1 d . . .
N1 N 0.22203(19) 0.3077(3) 0.21465(13) 0.0396(12) Uani 1 1 d . . .
N2 N 0.20579(19) 0.3968(4) 0.19476(12) 0.0419(12) Uani 1 1 d . . .
N5 N 0.46702(17) 0.5634(3) 0.34969(12) 0.0341(11) Uani 1 1 d . . .
N6 N 0.48104(16) 0.4774(3) 0.37160(12) 0.0324(11) Uani 1 1 d . . .
C1 C 0.1101(2) 0.4038(4) 0.24750(15) 0.0344(13) Uani 1 1 d . . .
C2 C 0.0875(2) 0.3790(4) 0.20699(17) 0.0483(16) Uani 1 1 d . . .
H2 H 0.1092 0.3687 0.1873 0.058 Uiso 1 1 calc R . .
C3 C 0.0321(2) 0.3697(5) 0.19584(17) 0.0504(17) Uani 1 1 d . . .
H3 H 0.0161 0.3552 0.1683 0.060 Uiso 1 1 calc R . .
C4 C 0.0014(2) 0.3817(4) 0.22513(17) 0.0430(15) Uani 1 1 d . . .
H4 H -0.0357 0.3716 0.2177 0.052 Uiso 1 1 calc R . .
C5 C 0.0230(2) 0.4081(4) 0.26472(17) 0.0415(15) Uani 1 1 d . . .
H5 H 0.0011 0.4184 0.2842 0.050 Uiso 1 1 calc R . .
C6 C 0.07857(19) 0.4195(4) 0.27594(15) 0.0296(12) Uani 1 1 d . . .
C7 C 0.2128(2) 0.3001(4) 0.25684(14) 0.0343(14) Uani 1 1 d . . .
H7 H 0.2480 0.2971 0.2758 0.041 Uiso 1 1 calc R . .
C8 C 0.1814(2) 0.2148(4) 0.26545(15) 0.0336(13) Uani 1 1 d . . .
C9 C 0.1837(2) 0.1882(5) 0.30615(16) 0.0479(16) Uani 1 1 d . . .
H9 H 0.2069 0.2220 0.3272 0.058 Uiso 1 1 calc R . .
C10 C 0.1529(3) 0.1133(5) 0.3167(2) 0.067(2) Uani 1 1 d . . .
H10 H 0.1546 0.0963 0.3447 0.081 Uiso 1 1 calc R . .
C11 C 0.1201(3) 0.0644(6) 0.2859(2) 0.075(2) Uani 1 1 d . . .
H11 H 0.0991 0.0124 0.2926 0.090 Uiso 1 1 calc R . .
C12 C 0.1170(3) 0.0896(6) 0.2456(2) 0.066(2) Uani 1 1 d . . .
H12 H 0.0938 0.0555 0.2247 0.079 Uiso 1 1 calc R . .
C13 C 0.1472(2) 0.1631(5) 0.23547(19) 0.0473(16) Uani 1 1 d . . .
H13 H 0.1449 0.1794 0.2074 0.057 Uiso 1 1 calc R . .
C14 C 0.2470(2) 0.2365(5) 0.19753(18) 0.0447(16) Uani 1 1 d . . .
C15 C 0.2469(2) 0.2501(5) 0.15285(16) 0.0439(16) Uani 1 1 d . . .
C16 C 0.2669(2) 0.1758(5) 0.13184(19) 0.0562(19) Uani 1 1 d . . .
H16 H 0.2819 0.1193 0.1458 0.067 Uiso 1 1 calc R . .
C17 C 0.2643(2) 0.1866(6) 0.09012(19) 0.068(2) Uani 1 1 d . . .
H17 H 0.2774 0.1362 0.0753 0.082 Uiso 1 1 calc R . .
C18 C 0.2438(3) 0.2664(7) 0.06996(19) 0.077(3) Uani 1 1 d . . .
H18 H 0.2424 0.2712 0.0412 0.093 Uiso 1 1 calc R . .
C19 C 0.2248(3) 0.3413(6) 0.09015(18) 0.072(2) Uani 1 1 d . . .
H19 H 0.2113 0.3981 0.0757 0.087 Uiso 1 1 calc R . .
C20 C 0.2255(2) 0.3328(5) 0.13228(16) 0.0489(17) Uani 1 1 d . . .
C21 C 0.2072(3) 0.4128(5) 0.15446(16) 0.0503(17) Uani 1 1 d . . .
C22 C 0.2034(2) 0.4764(4) 0.22352(15) 0.0383(14) Uani 1 1 d . . .
H22 H 0.1753 0.5226 0.2104 0.046 Uiso 1 1 calc R . .
C23 C 0.2546(2) 0.5315(4) 0.23459(14) 0.0352(14) Uani 1 1 d . . .
C24 C 0.3031(2) 0.4931(4) 0.23067(16) 0.0431(15) Uani 1 1 d . . .
H24 H 0.3050 0.4287 0.2211 0.052 Uiso 1 1 calc R . .
C25 C 0.3486(2) 0.5474(5) 0.24050(16) 0.0488(17) Uani 1 1 d . . .
H25 H 0.3814 0.5207 0.2370 0.059 Uiso 1 1 calc R . .
C26 C 0.3467(3) 0.6409(5) 0.25545(18) 0.0533(18) Uani 1 1 d . . .
H26 H 0.3780 0.6787 0.2621 0.064 Uiso 1 1 calc R . .
C27 C 0.2990(3) 0.6782(5) 0.26045(17) 0.0523(17) Uani 1 1 d . . .
H27 H 0.2974 0.7416 0.2712 0.063 Uiso 1 1 calc R . .
C28 C 0.2534(2) 0.6242(4) 0.24993(16) 0.0409(15) Uani 1 1 d . . .
H28 H 0.2207 0.6512 0.2533 0.049 Uiso 1 1 calc R . .
C29 C 0.08343(19) 0.5847(4) 0.33307(14) 0.0296(12) Uani 1 1 d . . .
H29 H 0.1084 0.6221 0.3542 0.035 Uiso 1 1 calc R . .
C30 C 0.0735(2) 0.6410(4) 0.29387(16) 0.0352(14) Uani 1 1 d . . .
C31 C 0.1169(2) 0.6873(5) 0.28325(18) 0.0499(17) Uani 1 1 d . . .
H31 H 0.1496 0.6912 0.3021 0.060 Uiso 1 1 calc R . .
C32 C 0.1108(3) 0.7286(6) 0.2435(2) 0.081(3) Uani 1 1 d . . .
H32 H 0.1402 0.7594 0.2356 0.098 Uiso 1 1 calc R . .
C33 C 0.0638(3) 0.7252(6) 0.2166(2) 0.081(3) Uani 1 1 d . . .
H33 H 0.0606 0.7541 0.1902 0.098 Uiso 1 1 calc R . .
C34 C 0.0218(3) 0.6808(5) 0.22715(19) 0.066(2) Uani 1 1 d . . .
H34 H -0.0108 0.6779 0.2081 0.079 Uiso 1 1 calc R . .
C35 C 0.0258(2) 0.6393(4) 0.26585(17) 0.0466(16) Uani 1 1 d . . .
H35 H -0.0043 0.6096 0.2732 0.056 Uiso 1 1 calc R . .
O3 O 0.02171(15) 0.7161(3) 0.36456(11) 0.0448(10) Uani 1 1 d . . .
O4 O -0.01791(15) 0.3399(3) 0.37775(13) 0.0549(12) Uani 1 1 d . . .
N3 N 0.03589(16) 0.5608(3) 0.34959(12) 0.0337(11) Uani 1 1 d . . .
N4 N 0.02905(16) 0.4622(3) 0.35804(13) 0.0339(11) Uani 1 1 d . . .
C36 C 0.0076(2) 0.6316(4) 0.36464(15) 0.0355(14) Uani 1 1 d . . .
C37 C -0.0418(2) 0.5978(5) 0.37656(16) 0.0441(16) Uani 1 1 d . . .
C38 C -0.0768(2) 0.6657(6) 0.38686(18) 0.0579(19) Uani 1 1 d . . .
H38 H -0.0686 0.7328 0.3866 0.070 Uiso 1 1 calc R . .
C39 C -0.1233(3) 0.6357(6) 0.3974(2) 0.066(2) Uani 1 1 d . . .
H39 H -0.1472 0.6823 0.4043 0.079 Uiso 1 1 calc R . .
C40 C -0.1351(3) 0.5399(7) 0.3979(2) 0.077(2) Uani 1 1 d . . .
H40 H -0.1673 0.5203 0.4053 0.093 Uiso 1 1 calc R . .
C41 C -0.1009(2) 0.4701(6) 0.3878(2) 0.063(2) Uani 1 1 d . . .
H41 H -0.1095 0.4032 0.3878 0.076 Uiso 1 1 calc R . .
C42 C -0.0536(2) 0.5012(5) 0.37743(16) 0.0410(15) Uani 1 1 d . . .
C43 C -0.0146(2) 0.4269(5) 0.37120(16) 0.0413(15) Uani 1 1 d . . .
C44 C 0.07831(19) 0.4055(4) 0.36340(15) 0.0325(13) Uani 1 1 d . . .
H44 H 0.0696 0.3370 0.3548 0.039 Uiso 1 1 calc R . .
C45 C 0.1092(2) 0.4063(4) 0.40720(16) 0.0355(14) Uani 1 1 d . . .
C46 C 0.1424(2) 0.3288(5) 0.42053(18) 0.0492(16) Uani 1 1 d . . .
H46 H 0.1444 0.2753 0.4029 0.059 Uiso 1 1 calc R . .
C47 C 0.1729(3) 0.3307(5) 0.4602(2) 0.064(2) Uani 1 1 d . . .
H47 H 0.1970 0.2795 0.4690 0.077 Uiso 1 1 calc R . .
C48 C 0.1685(2) 0.4050(5) 0.48652(19) 0.0595(19) Uani 1 1 d . . .
H48 H 0.1885 0.4040 0.5138 0.071 Uiso 1 1 calc R . .
C49 C 0.1351(2) 0.4814(5) 0.47332(17) 0.0534(18) Uani 1 1 d . . .
H49 H 0.1323 0.5337 0.4914 0.064 Uiso 1 1 calc R . .
C50 C 0.1056(2) 0.4819(5) 0.43386(17) 0.0466(16) Uani 1 1 d . . .
H50 H 0.0827 0.5348 0.4249 0.056 Uiso 1 1 calc R . .
C51 C 0.43316(19) 0.5895(4) 0.44762(15) 0.0308(13) Uani 1 1 d . . .
C52 C 0.48855(19) 0.5954(4) 0.45922(15) 0.0345(14) Uani 1 1 d . . .
H52 H 0.5105 0.5679 0.4423 0.041 Uiso 1 1 calc R . .
C53 C 0.5108(2) 0.6412(4) 0.49519(15) 0.0393(15) Uani 1 1 d . . .
H53 H 0.5482 0.6453 0.5030 0.047 Uiso 1 1 calc R . .
C54 C 0.4792(2) 0.6813(4) 0.52011(15) 0.0389(14) Uani 1 1 d . . .
H54 H 0.4949 0.7162 0.5440 0.047 Uiso 1 1 calc R . .
C55 C 0.4247(2) 0.6707(4) 0.51029(14) 0.0352(14) Uani 1 1 d . . .
H55 H 0.4033 0.6950 0.5283 0.042 Uiso 1 1 calc R . .
C56 C 0.40147(19) 0.6246(4) 0.47404(14) 0.0309(13) Uani 1 1 d . . .
C57 C 0.41867(19) 0.6106(4) 0.35791(14) 0.0308(13) Uani 1 1 d . . .
H57 H 0.3906 0.6051 0.3326 0.037 Uiso 1 1 calc R . .
C58 C 0.4251(2) 0.7165(4) 0.36931(15) 0.0369(14) Uani 1 1 d . . .
C59 C 0.3810(2) 0.7746(5) 0.36344(18) 0.0491(16) Uani 1 1 d . . .
H59 H 0.3475 0.7486 0.3511 0.059 Uiso 1 1 calc R . .
C60 C 0.3850(3) 0.8710(5) 0.3755(2) 0.069(2) Uani 1 1 d . . .
H60 H 0.3542 0.9105 0.3710 0.083 Uiso 1 1 calc R . .
C61 C 0.4327(3) 0.9103(6) 0.3937(2) 0.079(2) Uani 1 1 d . . .
H61 H 0.4351 0.9761 0.4021 0.094 Uiso 1 1 calc R . .
C62 C 0.4766(3) 0.8533(6) 0.3995(2) 0.071(2) Uani 1 1 d . . .
H62 H 0.5099 0.8800 0.4120 0.085 Uiso 1 1 calc R . .
C63 C 0.4737(2) 0.7564(5) 0.38751(17) 0.0503(17) Uani 1 1 d . . .
H63 H 0.5047 0.7176 0.3917 0.060 Uiso 1 1 calc R . .
C64 C 0.4924(2) 0.5964(5) 0.31945(16) 0.0452(16) Uani 1 1 d . . .
C65 C 0.5413(2) 0.5459(5) 0.31667(16) 0.0470(17) Uani 1 1 d . . .
C66 C 0.5720(2) 0.5821(6) 0.28934(19) 0.073(2) Uani 1 1 d . . .
H66 H 0.5612 0.6381 0.2733 0.087 Uiso 1 1 calc R . .
C67 C 0.6178(3) 0.5348(7) 0.2864(2) 0.083(3) Uani 1 1 d . . .
H67 H 0.6387 0.5579 0.2678 0.099 Uiso 1 1 calc R . .
C68 C 0.6341(3) 0.4535(7) 0.3101(2) 0.091(3) Uani 1 1 d . . .
H68 H 0.6663 0.4226 0.3075 0.109 Uiso 1 1 calc R . .
C69 C 0.6049(2) 0.4164(6) 0.33732(18) 0.061(2) Uani 1 1 d . . .
H69 H 0.6165 0.3610 0.3535 0.073 Uiso 1 1 calc R . .
C70 C 0.5576(2) 0.4630(5) 0.34022(16) 0.0446(16) Uani 1 1 d . . .
C71 C 0.5249(2) 0.4243(4) 0.36903(15) 0.0359(14) Uani 1 1 d . . .
C72 C 0.43936(19) 0.4342(4) 0.39026(15) 0.0314(13) Uani 1 1 d . . .
H72 H 0.4564 0.4071 0.4176 0.038 Uiso 1 1 calc R . .
C73 C 0.4095(2) 0.3534(4) 0.36544(16) 0.0362(14) Uani 1 1 d . . .
C74 C 0.3854(2) 0.2837(5) 0.3846(2) 0.0552(18) Uani 1 1 d . . .
H74 H 0.3885 0.2856 0.4136 0.066 Uiso 1 1 calc R . .
C75 C 0.3560(3) 0.2096(6) 0.3620(3) 0.080(2) Uani 1 1 d . . .
H75 H 0.3395 0.1612 0.3755 0.095 Uiso 1 1 calc R . .
C76 C 0.3512(3) 0.2076(6) 0.3199(3) 0.080(2) Uani 1 1 d . . .
H76 H 0.3306 0.1586 0.3043 0.096 Uiso 1 1 calc R . .
C77 C 0.3758(3) 0.2756(5) 0.3009(2) 0.063(2) Uani 1 1 d . . .
H77 H 0.3730 0.2732 0.2720 0.075 Uiso 1 1 calc R . .
C78 C 0.4049(2) 0.3483(5) 0.32322(17) 0.0473(16) Uani 1 1 d . . .
H78 H 0.4219 0.3954 0.3095 0.057 Uiso 1 1 calc R . .
C79 C 0.3048(2) 0.7310(4) 0.46325(17) 0.0443(15) Uani 1 1 d . . .
H79 H 0.3305 0.7818 0.4584 0.053 Uiso 1 1 calc R . .
C80 C 0.2497(2) 0.7542(4) 0.43845(17) 0.0420(15) Uani 1 1 d . . .
C81 C 0.2038(2) 0.7418(5) 0.4529(2) 0.0565(18) Uani 1 1 d . . .
H81 H 0.2057 0.7177 0.4799 0.068 Uiso 1 1 calc R . .
C82 C 0.1551(3) 0.7631(5) 0.4296(2) 0.068(2) Uani 1 1 d . . .
H82 H 0.1240 0.7544 0.4406 0.081 Uiso 1 1 calc R . .
C83 C 0.1515(3) 0.7974(5) 0.3898(2) 0.072(2) Uani 1 1 d . . .
H83 H 0.1180 0.8119 0.3733 0.087 Uiso 1 1 calc R . .
C84 C 0.1971(3) 0.8101(5) 0.3748(2) 0.072(2) Uani 1 1 d . . .
H84 H 0.1950 0.8331 0.3476 0.086 Uiso 1 1 calc R . .
C85 C 0.2462(3) 0.7899(5) 0.3988(2) 0.0596(19) Uani 1 1 d . . .
H85 H 0.2774 0.8005 0.3882 0.072 Uiso 1 1 calc R . .
O7 O 0.31871(18) 0.8902(3) 0.51424(16) 0.107(2) Uani 1 1 d D . .
O8 O 0.26133(17) 0.5523(3) 0.56798(12) 0.0843(19) Uani 1 1 d D . .
N7 N 0.30072(15) 0.7298(3) 0.50723(13) 0.0551(15) Uani 1 1 d D . .
N8 N 0.29553(17) 0.6387(3) 0.52518(10) 0.0501(14) Uani 1 1 d D . .
C86 C 0.3051(2) 0.8161(3) 0.52795(12) 0.074(2) Uani 1 1 d DU . .
C87 C 0.29388(15) 0.7970(2) 0.56898(10) 0.085(3) Uani 1 1 d GDU . .
C88 C 0.3033(2) 0.8819(3) 0.59174(14) 0.129(4) Uani 1 1 d GDU . .
H88 H 0.3157 0.9379 0.5800 0.154 Uiso 1 1 calc R . .
C89 C 0.29445(18) 0.8848(3) 0.63171(13) 0.137(4) Uani 1 1 d GDU . .
H89 H 0.3009 0.9428 0.6473 0.164 Uiso 1 1 calc R . .
C90 C 0.27623(18) 0.8028(4) 0.64891(9) 0.108(3) Uani 1 1 d GDU . .
H90 H 0.2702 0.8048 0.6762 0.129 Uiso 1 1 calc R . .
C91 C 0.26684(18) 0.7179(3) 0.62614(9) 0.107(3) Uani 1 1 d GDU . .
H91 H 0.2544 0.6619 0.6379 0.128 Uiso 1 1 calc R . .
C92 C 0.27567(11) 0.7150(3) 0.58618(7) 0.086(3) Uani 1 1 d GDU . .
C93 C 0.27298(13) 0.6331(2) 0.55965(8) 0.065(2) Uani 1 1 d GDU . .
C94 C 0.30380(18) 0.5574(3) 0.49428(11) 0.0424(16) Uani 1 1 d G . .
H94 H 0.2673 0.5366 0.4810 0.051 Uiso 1 1 calc R . .
C95 C 0.3285(2) 0.4700(5) 0.51586(15) 0.0381(14) Uani 1 1 d . . .
C96 C 0.3195(2) 0.3834(5) 0.49502(17) 0.0458(16) Uani 1 1 d . . .
H96 H 0.2960 0.3821 0.4692 0.055 Uiso 1 1 calc R . .
C97 C 0.3439(2) 0.2983(5) 0.51066(18) 0.0525(17) Uani 1 1 d . . .
H97 H 0.3378 0.2397 0.4955 0.063 Uiso 1 1 calc R . .
C98 C 0.3777(2) 0.2999(5) 0.54892(18) 0.0510(17) Uani 1 1 d . . .
H98 H 0.3935 0.2416 0.5605 0.061 Uiso 1 1 calc R . .
C99 C 0.3878(2) 0.3841(5) 0.56951(17) 0.0529(18) Uani 1 1 d . . .
H99 H 0.4113 0.3848 0.5954 0.063 Uiso 1 1 calc R . .
C100 C 0.3639(2) 0.4713(5) 0.55323(16) 0.0455(16) Uani 1 1 d . . .
H100 H 0.3720 0.5305 0.5677 0.055 Uiso 1 1 calc R . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Rh1 P1 2.1458(13) . ?
Rh1 P2 2.1494(13) . ?
Rh1 Cl1 2.3885(13) . ?
Rh1 Cl2 2.3887(13) . ?
Rh2 P4 2.1402(14) . ?
Rh2 P3 2.1489(13) . ?
Rh2 Cl1 2.3793(13) . ?
Rh2 Cl2 2.3955(13) . ?
P1 C1 1.808(5) . ?
P1 C22 1.858(5) . ?
P1 C7 1.864(6) . ?
P2 C6 1.827(5) . ?
P2 C44 1.875(5) . ?
P2 C29 1.884(5) . ?
P3 C51 1.825(5) . ?
P3 C57 1.870(5) . ?
P3 C72 1.868(5) . ?
P4 C94 1.757(4) . ?
P4 C56 1.828(5) . ?
P4 C79 1.848(6) . ?
O1 C14 1.227(7) . ?
O2 C21 1.228(7) . ?
O5 C64 1.232(7) . ?
O6 C71 1.215(6) . ?
N1 C14 1.358(7) . ?
N1 N2 1.420(6) . ?
N1 C7 1.470(6) . ?
N2 C21 1.364(6) . ?
N2 C22 1.466(7) . ?
N5 C64 1.377(6) . ?
N5 N6 1.404(6) . ?
N5 C57 1.477(6) . ?
N6 C71 1.363(6) . ?
N6 C72 1.467(6) . ?
C1 C6 1.377(7) . ?
C1 C2 1.401(7) . ?
C2 C3 1.409(8) . ?
C3 C4 1.378(8) . ?
C4 C5 1.374(7) . ?
C5 C6 1.416(7) . ?
C7 C8 1.488(7) . ?
C8 C13 1.392(7) . ?
C8 C9 1.391(7) . ?
C9 C10 1.388(8) . ?
C10 C11 1.373(9) . ?
C11 C12 1.368(9) . ?
C12 C13 1.360(9) . ?
C14 C15 1.495(8) . ?
C15 C20 1.388(8) . ?
C15 C16 1.395(8) . ?
C16 C17 1.382(9) . ?
C17 C18 1.344(10) . ?
C18 C19 1.372(10) . ?
C19 C20 1.401(8) . ?
C20 C21 1.456(9) . ?
C22 C23 1.506(8) . ?
C23 C28 1.380(7) . ?
C23 C24 1.386(8) . ?
C24 C25 1.375(8) . ?
C25 C26 1.388(8) . ?
C26 C27 1.371(8) . ?
C27 C28 1.378(8) . ?
C29 N3 1.474(6) . ?
C29 C30 1.494(7) . ?
C30 C35 1.391(7) . ?
C30 C31 1.391(8) . ?
C31 C32 1.417(8) . ?
C32 C33 1.359(10) . ?
C33 C34 1.349(10) . ?
C34 C35 1.393(8) . ?
O3 C36 1.222(6) . ?
O4 C43 1.227(7) . ?
N3 C36 1.371(6) . ?
N3 N4 1.408(6) . ?
N4 C43 1.372(7) . ?
N4 C44 1.472(6) . ?
C36 C37 1.479(7) . ?
C37 C42 1.371(8) . ?
C37 C38 1.389(8) . ?
C38 C39 1.375(9) . ?
C39 C40 1.358(10) . ?
C40 C41 1.391(10) . ?
C41 C42 1.396(8) . ?
C42 C43 1.480(8) . ?
C44 C45 1.516(7) . ?
C45 C50 1.383(8) . ?
C45 C46 1.389(7) . ?
C46 C47 1.396(8) . ?
C47 C48 1.367(9) . ?
C48 C49 1.379(9) . ?
C49 C50 1.381(8) . ?
C51 C56 1.396(7) . ?
C51 C52 1.407(7) . ?
C52 C53 1.374(7) . ?
C53 C54 1.386(7) . ?
C54 C55 1.385(7) . ?
C55 C56 1.391(7) . ?
C57 C58 1.511(8) . ?
C58 C59 1.375(7) . ?
C58 C63 1.393(8) . ?
C59 C60 1.388(9) . ?
C60 C61 1.373(10) . ?
C61 C62 1.361(10) . ?
C62 C63 1.394(9) . ?
C64 C65 1.459(8) . ?
C65 C70 1.404(8) . ?
C65 C66 1.406(8) . ?
C66 C67 1.370(9) . ?
C67 C68 1.387(10) . ?
C68 C69 1.384(9) . ?
C69 C70 1.397(8) . ?
C70 C71 1.492(7) . ?
C72 C73 1.506(7) . ?
C73 C74 1.368(8) . ?
C73 C78 1.386(7) . ?
C74 C75 1.402(9) . ?
C75 C76 1.377(10) . ?
C76 C77 1.356(10) . ?
C77 C78 1.379(8) . ?
C79 N7 1.485(7) . ?
C79 C80 1.530(8) . ?
C80 C81 1.371(8) . ?
C80 C85 1.393(8) . ?
C81 C82 1.371(8) . ?
C82 C83 1.390(10) . ?
C83 C84 1.375(10) . ?
C84 C85 1.384(8) . ?
O7 C86 1.199(2) . ?
O8 C93 1.202(2) . ?
N7 C86 1.370(2) . ?
N7 N8 1.410(2) . ?
N8 C93 1.3831(19) . ?
N8 C94 1.564(5) . ?
C86 C87 1.471(2) . ?
C87 C88 1.3900 . ?
C87 C92 1.3900 . ?
C88 C89 1.3900 . ?
C89 C90 1.3900 . ?
C90 C91 1.3900 . ?
C91 C92 1.3900 . ?
C92 C93 1.4273 . ?
C94 C95 1.483(7) . ?
C95 C96 1.377(8) . ?
C95 C100 1.390(7) . ?
C96 C97 1.385(8) . ?
C97 C98 1.393(8) . ?
C98 C99 1.348(9) . ?
C99 C100 1.411(8) . ?
