#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/06/15/4061516.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4061516
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om050269x
_journal_year                    2005
_chemical_formula_sum            'C63.5 H86 Cl6 O20 P4 Sn6'
_chemical_formula_weight         2218.04
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                109.129(7)
_cell_angle_beta                 90.972(8)
_cell_angle_gamma                97.352(7)
_cell_formula_units_Z            2
_cell_length_a                   13.500(5)
_cell_length_b                   15.974(5)
_cell_length_c                   20.487(7)
_cell_measurement_temperature    223(2)
_cell_volume                     4132(2)
_diffrn_ambient_temperature      223(2)
_exptl_crystal_density_diffrn    1.783
_cod_original_formula_sum        'C63.50 H86 Cl6 O20 P4 Sn6'
_cod_database_code               4061516
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Sn1 Sn 0.28046(4) 0.52892(4) 0.40668(3) 0.02842(16) Uani 1 1 d . . .
Sn2 Sn 0.34006(4) 0.34443(4) 0.43446(3) 0.02706(15) Uani 1 1 d . . .
Sn3 Sn 0.49167(4) 0.44888(4) 0.34789(3) 0.02745(15) Uani 1 1 d . . .
Cl1 Cl -0.20346(18) 0.27070(19) 0.29240(16) 0.0647(8) Uani 1 1 d . . .
Cl2 Cl 0.2718(3) 0.5886(3) 0.06913(17) 0.0985(13) Uani 1 1 d . . .
Cl3 Cl 0.5392(3) -0.0284(2) 0.17916(19) 0.0896(11) Uani 1 1 d . . .
P1 P 0.28768(17) 0.51419(16) 0.55987(12) 0.0290(5) Uani 1 1 d . . .
H1 H 0.2401 0.5227 0.5969 0.035 Uiso 1 1 calc R A .
P2 P 0.49349(17) 0.65762(16) 0.44096(12) 0.0300(6) Uani 1 1 d . . .
H2 H 0.5165 0.7150 0.4335 0.036 Uiso 1 1 calc R A .
O1 O 0.2196(4) 0.3912(4) 0.3866(3) 0.0305(14) Uani 1 1 d . A .
O2 O 0.3517(4) 0.4807(4) 0.3102(3) 0.0318(14) Uani 1 1 d . A .
O3 O 0.4215(4) 0.3169(4) 0.3433(3) 0.0286(14) Uani 1 1 d . A .
O4 O 0.3988(4) 0.4648(3) 0.4264(3) 0.0243(13) Uani 1 1 d . A .
O5 O 0.2474(4) 0.5546(4) 0.5088(3) 0.0294(14) Uani 1 1 d . A .
O6 O 0.3798(4) 0.6460(4) 0.4352(3) 0.0300(14) Uani 1 1 d . A .
O7 O 0.5359(4) 0.5859(3) 0.3843(3) 0.0252(13) Uani 1 1 d . A .
O8 O 0.6134(4) 0.4348(4) 0.4054(3) 0.0323(15) Uani 1 1 d . . .
O9 O 0.2853(4) 0.4138(4) 0.5274(3) 0.0291(14) Uani 1 1 d . A .
O10 O 0.4657(4) 0.3322(4) 0.4873(3) 0.0359(15) Uani 1 1 d . . .
C1 C 0.1579(6) 0.5736(6) 0.3690(5) 0.036(2) Uani 1 1 d . A 1
H1A H 0.1798 0.5970 0.3322 0.043 Uiso 1 1 calc R A 1
H1B H 0.1058 0.5223 0.3486 0.043 Uiso 1 1 calc R A 1
C2 C 0.1134(9) 0.6448(8) 0.4231(6) 0.076(4) Uani 1 1 d . A 1
H2A H 0.1669 0.6934 0.4470 0.091 Uiso 1 1 calc R A 1
H2B H 0.0848 0.6195 0.4573 0.091 Uiso 1 1 calc R A 1
C3 C 0.0303(10) 0.6847(10) 0.3937(8) 0.097(5) Uani 1 1 d . A 1
H3A H 0.0161 0.7407 0.4276 0.116 Uiso 1 1 calc R A 1
H3B H 0.0495 0.6957 0.3510 0.116 Uiso 1 1 calc R A 1
C4 C -0.0493(14) 0.6194(12) 0.3814(10) 0.106(6) Uiso 0.80 1 d P A 1
H4A H -0.0486 0.5776 0.3348 0.160 Uiso 1 1 calc R A 1
H4B H -0.1107 0.6460 0.3861 0.160 Uiso 1 1 calc R A 1
H4C H -0.0456 0.5880 0.4145 0.160 Uiso 1 1 calc R A 1
C5 C 0.2648(7) 0.2146(6) 0.4165(5) 0.040(2) Uani 1 1 d . A 1
H5A H 0.2058 0.2057 0.3852 0.048 Uiso 1 1 calc R A 1
H5B H 0.3090 0.1718 0.3923 0.048 Uiso 1 1 calc R A 1
C6 C 0.2326(12) 0.1927(8) 0.4765(7) 0.110(6) Uani 1 1 d . A 1
H6A H 0.1819 0.2306 0.4971 0.132 Uiso 1 1 calc R A 1
H6B H 0.2900 0.2098 0.5104 0.132 Uiso 1 1 calc R A 1
C7 C 0.1909(9) 0.0991(7) 0.4674(6) 0.073(4) Uani 1 1 d . A 1
H7A H 0.2454 0.0626 0.4573 0.088 Uiso 1 1 calc R A 1
H7B H 0.1429 0.0771 0.4270 0.088 Uiso 1 1 calc R A 1
C8 C 0.1388(14) 0.0850(11) 0.5290(9) 0.102(6) Uiso 0.80 1 d P A 1
H8A H 0.1842 0.1093 0.5700 0.153 Uiso 1 1 calc R A 1
H8B H 0.1188 0.0215 0.5199 0.153 Uiso 1 1 calc R A 1
H8C H 0.0800 0.1153 0.5364 0.153 Uiso 1 1 calc R A 1
C9 C 0.5528(7) 0.4102(7) 0.2499(5) 0.044(3) Uani 1 1 d . A 1
H9A H 0.5612 0.3469 0.2366 0.052 Uiso 1 1 calc R A 1
H9B H 0.5053 0.4164 0.2157 0.052 Uiso 1 1 calc R A 1
C10 C 0.6502(10) 0.4631(10) 0.2479(6) 0.097(5) Uani 1 1 d . A 1
H10A H 0.6989 0.4571 0.2815 0.117 Uiso 1 1 calc R A 1
H10B H 0.6428 0.5265 0.2600 0.117 Uiso 1 1 calc R A 1
C11 C 0.6879(16) 0.4281(13) 0.1734(10) 0.164(8) Uiso 1 1 d . A 1
H11A H 0.7605 0.4445 0.1747 0.197 Uiso 1 1 calc R A 1
H11B H 0.6722 0.3628 0.1544 0.197 Uiso 1 1 calc R A 1
C12 C 0.6417(18) 0.4656(14) 0.1337(12) 0.215(11) Uiso 1 1 d . A 1
H12A H 0.5876 0.4225 0.1053 0.322 Uiso 1 1 calc R A 1
H12B H 0.6894 0.4836 0.1042 0.322 Uiso 1 1 calc R A 1
H12C H 0.6149 0.5176 0.1630 0.322 Uiso 1 1 calc R A 1
C1A C 0.1194(6) 0.3592(6) 0.3672(4) 0.028(2) Uani 1 1 d . . .
C2A C 0.0922(7) 0.3027(6) 0.3003(4) 0.034(2) Uani 1 1 d . A .
H2A1 H 0.1429 0.2848 0.2699 0.041 Uiso 1 1 calc R . .
C3A C -0.0035(6) 0.2724(6) 0.2769(5) 0.035(2) Uani 1 1 d . . .
H3A1 H -0.0198 0.2319 0.2318 0.042 Uiso 1 1 calc R A .
C4A C -0.0778(7) 0.3027(6) 0.3213(5) 0.041(3) Uani 1 1 d . A .
C5A C -0.0530(7) 0.3559(6) 0.3887(5) 0.041(2) Uani 1 1 d . . .
H5A1 H -0.1031 0.3732 0.4196 0.049 Uiso 1 1 calc R A .
C6A C 0.0475(6) 0.3837(6) 0.4104(5) 0.034(2) Uani 1 1 d . A .
H6A1 H 0.0651 0.4205 0.4564 0.041 Uiso 1 1 calc R . .
C1B C 0.3379(6) 0.5056(6) 0.2524(4) 0.031(2) Uani 1 1 d . . .
C2B C 0.2558(8) 0.4619(7) 0.2069(5) 0.050(3) Uani 1 1 d . A .
H2B1 H 0.2162 0.4130 0.2137 0.060 Uiso 1 1 calc R . .
C3B C 0.2306(9) 0.4889(7) 0.1511(5) 0.065(3) Uani 1 1 d . . .
H3B1 H 0.1718 0.4637 0.1225 0.078 Uiso 1 1 calc R A .
C4B C 0.2994(11) 0.5559(8) 0.1412(5) 0.067(4) Uani 1 1 d . A .
C5B C 0.3847(9) 0.5984(8) 0.1849(6) 0.061(3) Uani 1 1 d . . .
H5B1 H 0.4308 0.6416 0.1755 0.073 Uiso 1 1 calc R A .
C6B C 0.3977(7) 0.5738(7) 0.2423(5) 0.045(3) Uani 1 1 d . A .
H6B1 H 0.4499 0.6056 0.2755 0.054 Uiso 1 1 calc R . .
C1C C 0.4507(7) 0.2354(6) 0.3056(4) 0.032(2) Uani 1 1 d . . .
C2C C 0.3873(7) 0.1774(6) 0.2518(5) 0.041(2) Uani 1 1 d . A .
H2C H 0.3254 0.1927 0.2415 0.050 Uiso 1 1 calc R . .
C3C C 0.4165(8) 0.0941(6) 0.2122(5) 0.049(3) Uani 1 1 d . . .
H3C H 0.3752 0.0544 0.1746 0.059 Uiso 1 1 calc R A .
C4C C 0.5010(7) 0.0740(7) 0.2290(5) 0.045(3) Uani 1 1 d . A .
C5C C 0.5644(9) 0.1311(8) 0.2822(6) 0.064(3) Uani 1 1 d . . .
H5C H 0.6259 0.1145 0.2920 0.077 Uiso 1 1 calc R A .
C6C C 0.5392(6) 0.2124(6) 0.3216(5) 0.041(3) Uani 1 1 d . A .
H6C H 0.5822 0.2512 0.3587 0.050 Uiso 1 1 calc R . .
Sn4 Sn 0.01790(5) 1.00700(4) 0.17966(3) 0.03042(16) Uani 1 1 d . . .
Sn5 Sn -0.10248(5) 0.85079(4) 0.03941(3) 0.03023(16) Uani 1 1 d . . .
Sn6 Sn 0.14926(5) 0.90159(4) 0.04724(3) 0.02976(16) Uani 1 1 d . . .
Cl4 Cl -0.3418(3) 0.7261(2) 0.31827(18) 0.0988(13) Uani 1 1 d . . .
Cl5 Cl 0.3145(3) 0.7803(3) 0.35411(19) 0.1018(13) Uani 1 1 d . . .
Cl6 Cl 0.0341(3) 0.4308(2) -0.18706(18) 0.0937(12) Uani 1 1 d . . .
P3 P -0.17268(18) 1.04707(16) 0.10001(12) 0.0303(6) Uani 1 1 d . . .
H3 H -0.2362 1.0684 0.1171 0.036 Uiso 1 1 calc R D .
P4 P 0.17237(17) 1.11796(16) 0.10890(12) 0.0304(6) Uani 1 1 d . . .
H4 H 0.2294 1.1666 0.1266 0.037 Uiso 1 1 calc R D .
O11 O -0.0813(5) 0.8821(4) 0.1520(3) 0.0370(16) Uani 1 1 d . D .
O12 O 0.1389(4) 0.9299(4) 0.1601(3) 0.0356(15) Uani 1 1 d . D .
O13 O 0.0319(4) 0.7869(4) 0.0172(3) 0.0304(14) Uani 1 1 d . D .
O14 O 0.0190(4) 0.9501(3) 0.0722(3) 0.0251(13) Uani 1 1 d . D .
O15 O 0.1180(4) 1.1133(4) 0.1715(3) 0.0335(15) Uani 1 1 d . D .
O16 O -0.0999(4) 1.0695(4) 0.1630(3) 0.0298(14) Uani 1 1 d . D .
O17 O -0.1962(4) 0.9462(4) 0.0635(3) 0.0318(14) Uani 1 1 d . D .
O18 O -0.1110(5) 0.8547(4) -0.0600(3) 0.0364(15) Uani 1 1 d . . .
O19 O 0.2181(4) 1.0335(4) 0.0760(3) 0.0305(14) Uani 1 1 d . D .
O20 O 0.1347(4) 0.9023(4) -0.0526(3) 0.0340(15) Uani 1 1 d . . .
C13 C 0.0159(7) 1.0470(6) 0.2884(4) 0.040(2) Uani 1 1 d . . .
H13A H 0.0367 0.9994 0.3036 0.048 Uiso 1 1 calc R . .
H13B H 0.0656 1.1004 0.3084 0.048 Uiso 1 1 calc R . .
C14 C -0.0829(7) 1.0676(6) 0.3175(5) 0.036(2) Uani 1 1 d . C .
H14A H -0.1093 1.1077 0.2963 0.043 Uiso 1 1 calc R . .
H14B H -0.1299 1.0119 0.3041 0.043 Uiso 1 1 calc R . .
C15 C -0.0794(8) 1.1100(7) 0.3945(5) 0.053(3) Uani 1 1 d . . .
H15A H -0.0518 1.0706 0.4158 0.063 Uiso 1 1 calc R B 1
H15B H -0.0337 1.1665 0.4079 0.063 Uiso 1 1 calc R B 1
C16 C -0.1777(9) 1.1282(8) 0.4223(6) 0.074(4) Uani 1 1 d . C 1
H16A H -0.2028 1.1716 0.4050 0.111 Uiso 1 1 calc R C 1
H16B H -0.1703 1.1517 0.4725 0.111 Uiso 1 1 calc R C 1
H16C H -0.2244 1.0731 0.4078 0.111 Uiso 1 1 calc R C 1
C17 C -0.2073(8) 0.7352(6) 0.0240(5) 0.051(3) Uani 1 1 d . D 1
H17A H -0.1788 0.6851 -0.0079 0.061 Uiso 1 1 calc R D 1
H17B H -0.2102 0.7247 0.0685 0.061 Uiso 1 1 calc R D 1
C18 C -0.2987(9) 0.7290(10) 0.0012(10) 0.125(7) Uani 1 1 d . D 1
H18A H -0.2960 0.7343 -0.0451 0.151 Uiso 1 1 calc R D 1
H18B H -0.3254 0.7819 0.0307 0.151 Uiso 1 1 calc R D 1
C19 C -0.3762(18) 0.6479(14) -0.0045(12) 0.191(10) Uiso 1 1 d . D 1
H19A H -0.4387 0.6542 -0.0263 0.230 Uiso 1 1 calc R D 1
H19B H -0.3523 0.5939 -0.0349 0.230 Uiso 1 1 calc R D 1
C20 C -0.395(2) 0.6374(16) 0.0548(13) 0.248(13) Uiso 1 1 d . D 1
H20A H -0.4658 0.6366 0.0615 0.372 Uiso 1 1 calc R D 1
H20B H -0.3574 0.6865 0.0918 0.372 Uiso 1 1 calc R D 1
H20C H -0.3749 0.5813 0.0552 0.372 Uiso 1 1 calc R D 1
C21 C 0.2775(7) 0.8345(7) 0.0422(5) 0.050(3) Uani 1 1 d . D 2
H21A H 0.3142 0.8550 0.0876 0.060 Uiso 1 1 calc R D 2
H21B H 0.2567 0.7698 0.0288 0.060 Uiso 1 1 calc R D 2
C22 C 0.3424(17) 0.8553(15) -0.0100(13) 0.112(4) Uiso 0.80 1 d P D 2
H22A H 0.3506 0.9201 -0.0004 0.134 Uiso 1 1 calc R D 2
H22B H 0.3071 0.8269 -0.0557 0.134 Uiso 1 1 calc R D 2
C23 C 0.4531(14) 0.8246(13) -0.0141(10) 0.112(4) Uiso 0.80 1 d P D 2
H23A H 0.4881 0.8491 0.0319 0.134 Uiso 1 1 calc R D 2
H23B H 0.4465 0.7592 -0.0285 0.134 Uiso 1 1 calc R D 2
C24 C 0.5126(14) 0.8559(12) -0.0635(10) 0.112(4) Uiso 0.80 1 d P D 2
H24A H 0.5360 0.8054 -0.0974 0.167 Uiso 1 1 calc R D 2
H24B H 0.5695 0.8987 -0.0387 0.167 Uiso 1 1 calc R D 2
H24C H 0.4713 0.8843 -0.0867 0.167 Uiso 1 1 calc R D 2
C4' C -0.029(7) 0.707(6) 0.432(5) 0.12(3) Uiso 0.20 1 d P E 3
C8A C 0.222(5) 0.048(4) 0.509(3) 0.077(19) Uiso 0.20 1 d P F 3
C22A C 0.311(5) 0.799(4) -0.012(3) 0.056(9) Uiso 0.20 1 d P G 3
C23A C 0.369(5) 0.886(4) -0.001(4) 0.056(9) Uiso 0.20 1 d P G 3
C24A C 0.488(4) 0.796(4) -0.096(3) 0.056(9) Uiso 0.20 1 d P H 3
C1D C -0.1452(7) 0.8477(6) 0.1917(5) 0.035(2) Uani 1 1 d . . .
C2D C -0.1072(9) 0.7961(7) 0.2272(6) 0.066(3) Uani 1 1 d . D .
H2D H -0.0402 0.7856 0.2246 0.079 Uiso 1 1 calc R . .
C3D C -0.1724(10) 0.7612(8) 0.2663(6) 0.076(4) Uani 1 1 d . . .
H3D H -0.1483 0.7263 0.2905 0.091 Uiso 1 1 calc R D .
C4D C -0.2627(9) 0.7742(7) 0.2711(5) 0.051(3) Uani 1 1 d . D .
C5D C -0.2979(8) 0.8277(8) 0.2392(6) 0.062(3) Uani 1 1 d . . .
H5D H -0.3639 0.8405 0.2440 0.074 Uiso 1 1 calc R D .
C6D C -0.2342(8) 0.8632(7) 0.1994(5) 0.051(3) Uani 1 1 d . D .
H6D H -0.2585 0.9002 0.1772 0.061 Uiso 1 1 calc R . .
C1E C 0.1813(7) 0.8953(6) 0.2051(5) 0.034(2) Uani 1 1 d . . .
C2E C 0.1661(8) 0.8051(6) 0.1935(5) 0.047(3) Uani 1 1 d . D .
H2E H 0.1244 0.7670 0.1554 0.057 Uiso 1 1 calc R . .
C3E C 0.2129(10) 0.7688(7) 0.2386(6) 0.070(4) Uani 1 1 d . . .
H3E H 0.2048 0.7066 0.2291 0.084 Uiso 1 1 calc R D .
C4E C 0.2684(8) 0.8231(8) 0.2944(6) 0.056(3) Uani 1 1 d . D .
C5E C 0.2839(9) 0.9133(8) 0.3073(6) 0.069(4) Uani 1 1 d . . .
H5E H 0.3251 0.9509 0.3459 0.082 Uiso 1 1 calc R D .
C6E C 0.2386(8) 0.9500(7) 0.2632(5) 0.050(3) Uani 1 1 d . D .
H6E H 0.2472 1.0124 0.2734 0.060 Uiso 1 1 calc R . .
C1F C 0.0345(7) 0.7052(6) -0.0310(5) 0.037(2) Uani 1 1 d . . .
C2F C 0.0202(7) 0.6921(7) -0.1001(5) 0.045(3) Uani 1 1 d . D .
H2F H 0.0072 0.7396 -0.1150 0.054 Uiso 1 1 calc R . .
C3F C 0.0250(9) 0.6076(8) -0.1485(5) 0.064(3) Uani 1 1 d . . .
H3F H 0.0155 0.5988 -0.1959 0.076 Uiso 1 1 calc R D .
C4F C 0.0436(8) 0.5360(7) -0.1275(6) 0.055(3) Uani 1 1 d . D .
C5F C 0.0586(9) 0.5493(7) -0.0599(6) 0.058(3) Uani 1 1 d . . .
H5F H 0.0729 0.5021 -0.0452 0.069 Uiso 1 1 calc R D .
C6F C 0.0529(8) 0.6335(6) -0.0112(5) 0.052(3) Uani 1 1 d . D .
H6F H 0.0618 0.6415 0.0362 0.063 Uiso 1 1 calc R . .
C1S C 0.518(3) -0.009(2) 0.4617(13) 0.166(7) Uiso 0.50 1 d PGD I -4
C2S C 0.533(2) -0.0736(18) 0.4907(14) 0.130(13) Uiso 0.50 1 d PGD I -4
H2SA H 0.5678 -0.1210 0.4668 0.156 Uiso 0.50 1 calc PR I -4
C3S C 0.498(2) -0.0684(18) 0.5551(13) 0.166(7) Uiso 0.50 1 d PG I -4
H3SA H 0.5088 -0.1124 0.5747 0.200 Uiso 0.50 1 calc PR I -4
C4S C 0.448(2) 0.002(2) 0.5905(12) 0.166(7) Uiso 0.50 1 d PG I -4
H4SA H 0.4238 0.0053 0.6340 0.200 Uiso 0.50 1 calc PR I -4
C5S C 0.432(2) 0.0668(19) 0.5615(14) 0.166(7) Uiso 0.50 1 d PG I -4
H5SA H 0.3978 0.1143 0.5854 0.200 Uiso 0.50 1 calc PR I -4
C6S C 0.467(3) 0.0617(19) 0.4971(15) 0.166(7) Uiso 0.50 1 d PGD I -4
H6SA H 0.4568 0.1057 0.4775 0.200 Uiso 0.50 1 calc PR I -4
C7S C 0.564(4) -0.010(3) 0.3933(17) 0.166(7) Uiso 0.50 1 d PD I -4
H7SA H 0.6068 -0.0569 0.3798 0.249 Uiso 0.50 1 calc PR I -4
H7SB H 0.6042 0.0472 0.3995 0.249 Uiso 0.50 1 calc PR I -4
H7SC H 0.5116 -0.0218 0.3575 0.249 Uiso 0.50 1 calc PR I -4
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sn1 O6 2.062(5) . ?
Sn1 O5 2.065(5) . ?
Sn1 O4 2.105(5) . ?
Sn1 C1 2.113(8) . ?
Sn1 O1 2.149(5) . ?
Sn1 O2 2.164(6) . ?
Sn2 O4 2.044(5) . ?
Sn2 O10 2.061(6) . ?
Sn2 O9 2.068(5) . ?
Sn2 C5 2.102(8) . ?
Sn2 O3 2.133(6) . ?
Sn2 O1 2.213(5) . ?
Sn3 O4 2.026(5) . ?
Sn3 O7 2.069(5) . ?
Sn3 O8 2.084(5) . ?
Sn3 C9 2.113(9) . ?
Sn3 O3 2.169(5) . ?
Sn3 O2 2.209(5) . ?
Cl1 C4A 1.742(9) . ?
Cl2 C4B 1.769(10) . ?
Cl3 C4C 1.767(10) . ?
P1 O8 1.504(6) 2_666 ?
P1 O9 1.517(6) . ?
P1 O5 1.523(5) . ?
P2 O10 1.511(6) 2_666 ?
P2 O7 1.519(6) . ?
P2 O6 1.520(6) . ?
O1 C1A 1.385(9) . ?
O2 C1B 1.383(9) . ?
O3 C1C 1.388(10) . ?
O8 P1 1.504(6) 2_666 ?
O10 P2 1.511(6) 2_666 ?
C1 C2 1.501(13) . ?
C2 C3 1.560(15) . ?
C3 C4 1.36(2) . ?
C5 C6 1.443(13) . ?
C6 C7 1.479(13) . ?
C7 C8 1.521(18) . ?
C9 C10 1.478(14) . ?
C10 C11 1.56(2) . ?
C11 C12 1.34(2) . ?
C1A C6A 1.334(11) . ?
C1A C2A 1.384(11) . ?
C2A C3A 1.341(12) . ?
C3A C4A 1.392(13) . ?
C4A C5A 1.373(12) . ?
C5A C6A 1.390(12) . ?
C1B C6B 1.346(12) . ?
C1B C2B 1.388(12) . ?
C2B C3B 1.397(12) . ?
C3B C4B 1.394(15) . ?
C4B C5B 1.399(16) . ?
C5B C6B 1.370(12) . ?
C1C C6C 1.359(11) . ?
C1C C2C 1.379(12) . ?
C2C C3C 1.421(12) . ?
C3C C4C 1.295(13) . ?
C4C C5C 1.367(13) . ?
C5C C6C 1.375(13) . ?
Sn4 O16 2.063(5) . ?
Sn4 O15 2.084(6) . ?
Sn4 O14 2.089(5) . ?
Sn4 C13 2.109(8) . ?
Sn4 O12 2.136(6) . ?
Sn4 O11 2.155(6) . ?
Sn5 O17 2.047(6) . ?
Sn5 O18 2.059(5) . ?
Sn5 O14 2.063(5) . ?
Sn5 C17 2.108(9) . ?
Sn5 O13 2.176(6) . ?
Sn5 O11 2.199(5) . ?
Sn6 O14 2.019(5) . ?
Sn6 O20 2.056(5) . ?
Sn6 O19 2.078(5) . ?
Sn6 C21 2.136(9) . ?
Sn6 O13 2.175(6) . ?
Sn6 O12 2.216(6) . ?
Cl4 C4D 1.726(10) . ?
Cl5 C4E 1.727(10) . ?
Cl6 C4F 1.710(11) . ?
P3 O20 1.511(6) 2_575 ?
P3 O16 1.524(6) . ?
P3 O17 1.525(6) . ?
P4 O18 1.494(6) 2_575 ?
P4 O15 1.506(6) . ?
P4 O19 1.513(6) . ?
O11 C1D 1.379(10) . ?
O12 C1E 1.372(9) . ?
O13 C1F 1.360(10) . ?
O18 P4 1.494(6) 2_575 ?
O20 P3 1.511(6) 2_575 ?
C13 C14 1.500(12) . ?
C14 C15 1.496(12) . ?
C15 C16 1.479(14) . ?
C17 C18 1.292(15) . ?
C18 C19 1.53(2) . ?
C19 C20 1.30(3) . ?
C21 C22 1.49(2) . ?
C22 C23 1.63(3) . ?
C23 C24 1.47(2) . ?
C22A C23A 1.45(8) . ?
C1D C6D 1.260(13) . ?
C1D C2D 1.400(12) . ?
C2D C3D 1.386(14) . ?
C3D C4D 1.263(15) . ?
C4D C5D 1.357(14) . ?
C5D C6D 1.389(13) . ?
C1E C2E 1.368(11) . ?
C1E C6E 1.376(12) . ?
C2E C3E 1.420(13) . ?
C3E C4E 1.332(14) . ?
C4E C5E 1.365(14) . ?
C5E C6E 1.397(13) . ?
C1F C2F 1.368(12) . ?
C1F C6F 1.383(12) . ?
C2F C3F 1.399(13) . ?
C3F C4F 1.396(14) . ?
C4F C5F 1.337(13) . ?
C5F C6F 1.400(13) . ?
C1S C2S 1.3900 . ?
C1S C6S 1.3900 . ?
C1S C7S 1.539(5) . ?
C2S C3S 1.3900 . ?
C3S C4S 1.3900 . ?
C4S C5S 1.3900 . ?
C5S C6S 1.3900 . ?
