#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/06/15/4061517.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4061517
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om050269x
_journal_year                    2005
_chemical_formula_sum            'C63.5 H86 Br6 O20 P4 Sn6'
_chemical_formula_weight         2484.80
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                109.5120(10)
_cell_angle_beta                 91.1720(10)
_cell_angle_gamma                97.4960(10)
_cell_formula_units_Z            2
_cell_length_a                   13.5706(7)
_cell_length_b                   16.0101(8)
_cell_length_c                   20.7547(11)
_cell_measurement_temperature    223(2)
_cell_volume                     4204.1(4)
_diffrn_ambient_temperature      223(2)
_exptl_crystal_density_diffrn    1.963
_cod_original_formula_sum        'C63.50 H86 Br6 O20 P4 Sn6'
_cod_database_code               4061517
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Sn1 Sn 0.28119(3) 0.53104(3) 0.40991(2) 0.02414(10) Uani 1 1 d . . .
Sn2 Sn 0.33919(3) 0.34535(3) 0.434118(19) 0.02303(10) Uani 1 1 d . . .
Sn3 Sn 0.48988(3) 0.45074(3) 0.349103(19) 0.02354(10) Uani 1 1 d . . .
Br1 Br -0.21047(5) 0.26785(5) 0.28571(4) 0.0557(2) Uani 1 1 d . . .
Br2 Br 0.27058(8) 0.58571(7) 0.06510(4) 0.0836(3) Uani 1 1 d . . .
Br3 Br 0.53404(7) -0.03815(6) 0.17576(5) 0.0851(3) Uani 1 1 d . . .
P1 P 0.28978(11) 0.51431(11) 0.56084(8) 0.0251(4) Uani 1 1 d . . .
H1 H 0.2433 0.5226 0.5979 0.030 Uiso 1 1 calc R . .
P2 P 0.49425(11) 0.65981(11) 0.44447(8) 0.0250(4) Uani 1 1 d . . .
H2 H 0.5175 0.7177 0.4382 0.030 Uiso 1 1 calc R . .
O1 O 0.2191(3) 0.3930(3) 0.38849(18) 0.0242(9) Uani 1 1 d . . .
O2 O 0.3498(3) 0.4839(3) 0.31351(18) 0.0269(10) Uani 1 1 d . . .
O3 O 0.4201(3) 0.3185(3) 0.34260(18) 0.0245(9) Uani 1 1 d . . .
O4 O 0.3974(2) 0.4668(2) 0.42848(17) 0.0217(9) Uani 1 1 d . . .
O5 O 0.2495(3) 0.5560(3) 0.51144(17) 0.0240(9) Uani 1 1 d . . .
O6 O 0.3806(3) 0.6491(2) 0.43879(18) 0.0253(9) Uani 1 1 d . . .
O7 O 0.5344(3) 0.5885(3) 0.38591(18) 0.0248(9) Uani 1 1 d . . .
O8 O 0.6092(3) 0.4349(3) 0.40496(18) 0.0270(9) Uani 1 1 d . . .
O9 O 0.2872(3) 0.4136(3) 0.52747(17) 0.0250(9) Uani 1 1 d . . .
O10 O 0.4651(3) 0.3308(3) 0.48471(18) 0.0267(10) Uani 1 1 d . . .
C1 C 0.1594(4) 0.5783(4) 0.3746(3) 0.0316(15) Uani 1 1 d D . .
H1A H 0.1808 0.6022 0.3386 0.038 Uiso 1 1 calc R . .
H1B H 0.1063 0.5278 0.3542 0.038 Uiso 1 1 calc R . .
C2 C 0.1183(5) 0.6497(5) 0.4300(3) 0.057(2) Uani 1 1 d D . .
H2A H 0.1722 0.6991 0.4515 0.068 Uiso 1 1 calc R . .
H2B H 0.0947 0.6250 0.4651 0.068 Uiso 1 1 calc R . .
C3 C 0.0331(5) 0.6865(6) 0.4046(4) 0.069(3) Uani 1 1 d D . .
H3A H 0.0222 0.7423 0.4401 0.083 Uiso 1 1 calc R . .
H3B H 0.0523 0.7008 0.3638 0.083 Uiso 1 1 calc R . .
C4 C -0.0591(6) 0.6248(7) 0.3880(5) 0.105(4) Uani 1 1 d D . .
H4A H -0.0513 0.5726 0.3489 0.157 Uiso 1 1 calc R . .
H4B H -0.1120 0.6540 0.3768 0.157 Uiso 1 1 calc R . .
H4C H -0.0758 0.6065 0.4270 0.157 Uiso 1 1 calc R . .
C5 C 0.2646(4) 0.2136(4) 0.4146(3) 0.0315(15) Uani 1 1 d D . .
H5A H 0.2108 0.2012 0.3790 0.038 Uiso 1 1 calc R . .
H5B H 0.3117 0.1713 0.3964 0.038 Uiso 1 1 calc R . .
C6 C 0.2212(6) 0.1964(5) 0.4756(3) 0.057(2) Uani 1 1 d D . .
H6A H 0.1654 0.2304 0.4886 0.068 Uiso 1 1 calc R . .
H6B H 0.2719 0.2189 0.5140 0.068 Uiso 1 1 calc R . .
C7 C 0.1848(5) 0.0990(4) 0.4639(3) 0.0500(19) Uani 1 1 d D . .
H7A H 0.2416 0.0657 0.4546 0.060 Uiso 1 1 calc R . .
H7B H 0.1380 0.0751 0.4232 0.060 Uiso 1 1 calc R . .
C8 C 0.1338(7) 0.0837(6) 0.5242(4) 0.089(3) Uani 1 1 d D . .
H8A H 0.1787 0.1093 0.5650 0.134 Uiso 1 1 calc R . .
H8B H 0.1159 0.0199 0.5148 0.134 Uiso 1 1 calc R . .
H8C H 0.0741 0.1121 0.5312 0.134 Uiso 1 1 calc R . .
C9 C 0.5476(4) 0.4112(4) 0.2507(3) 0.0385(17) Uani 1 1 d D . .
H9A H 0.5484 0.3464 0.2351 0.046 Uiso 1 1 calc R . .
H9B H 0.5023 0.4233 0.2186 0.046 Uiso 1 1 calc R . .
C10 C 0.6489(5) 0.4561(6) 0.2478(3) 0.081(3) Uani 1 1 d D . .
H10A H 0.6941 0.4455 0.2807 0.098 Uiso 1 1 calc R . .
H10B H 0.6479 0.5208 0.2618 0.098 Uiso 1 1 calc R . .
C11 C 0.6899(7) 0.4238(8) 0.1759(5) 0.122(4) Uani 1 1 d D . .
H11A H 0.7629 0.4343 0.1806 0.147 Uiso 1 1 calc R . .
H11B H 0.6685 0.3593 0.1542 0.147 Uiso 1 1 calc R . .
C12 C 0.6560(10) 0.4692(10) 0.1341(6) 0.184(6) Uiso 1 1 d D . .
H12A H 0.5848 0.4693 0.1370 0.276 Uiso 1 1 calc R . .
H12B H 0.6700 0.4390 0.0870 0.276 Uiso 1 1 calc R . .
H12C H 0.6899 0.5304 0.1494 0.276 Uiso 1 1 calc R . .
C1A C 0.1219(4) 0.3600(4) 0.3677(3) 0.0232(13) Uani 1 1 d . . .
C2A C 0.0976(4) 0.3025(4) 0.3008(3) 0.0301(15) Uani 1 1 d . . .
H2A1 H 0.1483 0.2826 0.2717 0.036 Uiso 1 1 calc R . .
C3A C -0.0012(4) 0.2746(4) 0.2771(3) 0.0306(15) Uani 1 1 d . . .
H3A1 H -0.0180 0.2360 0.2319 0.037 Uiso 1 1 calc R . .
C4A C -0.0749(4) 0.3035(4) 0.3200(3) 0.0323(15) Uani 1 1 d . . .
C5A C -0.0528(4) 0.3576(4) 0.3867(3) 0.0355(16) Uani 1 1 d . . .
H5A1 H -0.1038 0.3757 0.4159 0.043 Uiso 1 1 calc R . .
C6A C 0.0463(4) 0.3851(4) 0.4102(3) 0.0330(16) Uani 1 1 d . . .
H6A1 H 0.0623 0.4217 0.4561 0.040 Uiso 1 1 calc R . .
C1B C 0.3326(4) 0.5069(4) 0.2566(3) 0.0291(15) Uani 1 1 d . . .
C2B C 0.2540(5) 0.4619(5) 0.2110(3) 0.0415(18) Uani 1 1 d . . .
H2B1 H 0.2129 0.4139 0.2178 0.050 Uiso 1 1 calc R . .
C3B C 0.2345(5) 0.4867(5) 0.1549(3) 0.050(2) Uani 1 1 d . . .
H3B1 H 0.1782 0.4579 0.1249 0.060 Uiso 1 1 calc R . .
C4B C 0.2971(6) 0.5530(6) 0.1432(3) 0.050(2) Uani 1 1 d . . .
C5B C 0.3769(6) 0.5977(5) 0.1872(4) 0.056(2) Uani 1 1 d . . .
H5B1 H 0.4200 0.6435 0.1790 0.067 Uiso 1 1 calc R . .
C6B C 0.3937(5) 0.5737(5) 0.2456(3) 0.0479(19) Uani 1 1 d . . .
H6B1 H 0.4479 0.6046 0.2772 0.057 Uiso 1 1 calc R . .
C1C C 0.4474(4) 0.2370(4) 0.3057(3) 0.0256(14) Uani 1 1 d . . .
C2C C 0.3873(4) 0.1804(4) 0.2499(3) 0.0345(16) Uani 1 1 d . . .
H2C H 0.3281 0.1978 0.2378 0.041 Uiso 1 1 calc R . .
C3C C 0.4127(5) 0.0988(5) 0.2117(3) 0.0414(17) Uani 1 1 d . . .
H3C H 0.3712 0.0602 0.1738 0.050 Uiso 1 1 calc R . .
C4C C 0.4988(5) 0.0749(5) 0.2298(4) 0.0466(19) Uani 1 1 d . . .
C5C C 0.5601(5) 0.1294(5) 0.2844(4) 0.0451(18) Uani 1 1 d . . .
H5C H 0.6191 0.1112 0.2959 0.054 Uiso 1 1 calc R . .
C6C C 0.5356(4) 0.2113(5) 0.3228(3) 0.0415(18) Uani 1 1 d . . .
H6C H 0.5780 0.2496 0.3602 0.050 Uiso 1 1 calc R . .
Sn4 Sn 0.02061(3) 1.00916(3) 0.178381(19) 0.02534(10) Uani 1 1 d . . .
Sn5 Sn -0.10082(3) 0.85091(3) 0.03957(2) 0.02543(10) Uani 1 1 d . . .
Sn6 Sn 0.14929(3) 0.90317(3) 0.04592(2) 0.02516(10) Uani 1 1 d . . .
Br4 Br -0.33143(7) 0.72186(6) 0.32517(4) 0.0741(3) Uani 1 1 d . . .
Br5 Br 0.32229(7) 0.78954(7) 0.36035(4) 0.0742(3) Uani 1 1 d . . .
Br6 Br 0.03424(9) 0.42102(6) -0.19178(5) 0.0988(4) Uani 1 1 d . . .
P3 P -0.17089(11) 1.04743(11) 0.10048(8) 0.0261(4) Uani 1 1 d . . .
H3 H -0.2337 1.0687 0.1181 0.031 Uiso 1 1 calc R A .
P4 P 0.17283(11) 1.11956(11) 0.10744(8) 0.0254(4) Uani 1 1 d . . .
H4 H 0.2296 1.1685 0.1245 0.030 Uiso 1 1 calc R A .
O11 O -0.0759(3) 0.8825(3) 0.15134(18) 0.0294(10) Uani 1 1 d . A .
O12 O 0.1412(3) 0.9318(3) 0.15775(18) 0.0301(10) Uani 1 1 d . A .
O13 O 0.0331(3) 0.7875(3) 0.01673(19) 0.0303(10) Uani 1 1 d . A .
O14 O 0.0185(3) 0.9520(2) 0.07163(17) 0.0226(9) Uani 1 1 d . A .
O15 O 0.1181(3) 1.1170(3) 0.17033(18) 0.0267(10) Uani 1 1 d . A .
O16 O -0.0978(3) 1.0714(3) 0.16291(17) 0.0273(10) Uani 1 1 d . A .
O17 O -0.1959(3) 0.9467(3) 0.06507(18) 0.0277(10) Uani 1 1 d . A .
O18 O -0.1079(3) 0.8532(3) -0.05953(18) 0.0273(10) Uani 1 1 d . . .
O19 O 0.2182(3) 1.0349(3) 0.07382(18) 0.0257(9) Uani 1 1 d . A .
O20 O 0.1359(3) 0.9012(3) -0.05374(18) 0.0261(9) Uani 1 1 d . . .
C13 C 0.0195(4) 1.0493(4) 0.2866(2) 0.0306(15) Uani 1 1 d D . .
H13A H 0.0416 1.0025 0.3015 0.037 Uiso 1 1 calc R . .
H13B H 0.0677 1.1038 0.3068 0.037 Uiso 1 1 calc R . .
C14 C -0.0813(4) 1.0673(4) 0.3142(3) 0.0332(16) Uani 1 1 d D . .
H14A H -0.1074 1.1088 0.2949 0.040 Uiso 1 1 calc R . .
H14B H -0.1276 1.0110 0.2988 0.040 Uiso 1 1 calc R . .
C15 C -0.0776(5) 1.1065(5) 0.3918(3) 0.0453(19) Uani 1 1 d D . .
H15A H -0.0498 1.0659 0.4113 0.054 Uiso 1 1 calc R . .
H15B H -0.0330 1.1638 0.4072 0.054 Uiso 1 1 calc R . .
C16 C -0.1793(5) 1.1214(6) 0.4184(3) 0.066(2) Uani 1 1 d D . .
H16A H -0.2053 1.1645 0.4016 0.100 Uiso 1 1 calc R . .
H16B H -0.1735 1.1441 0.4681 0.100 Uiso 1 1 calc R . .
H16C H -0.2242 1.0652 0.4025 0.100 Uiso 1 1 calc R . .
C17 C -0.1999(4) 0.7309(4) 0.0246(3) 0.0400(17) Uani 1 1 d D A 1
H17A H -0.1757 0.6815 -0.0106 0.048 Uiso 1 1 calc R A 1
H17B H -0.2001 0.7173 0.0673 0.048 Uiso 1 1 calc R A 1
C18 C -0.3061(5) 0.7367(5) 0.0031(5) 0.079(3) Uani 1 1 d D A 1
H18A H -0.3286 0.7880 0.0375 0.094 Uiso 1 1 calc R A 1
H18B H -0.3054 0.7486 -0.0403 0.094 Uiso 1 1 calc R A 1
C19 C -0.3809(6) 0.6547(6) -0.0059(5) 0.095(3) Uani 1 1 d D A 1
H19A H -0.4430 0.6599 -0.0282 0.115 Uiso 1 1 calc R A 1
H19B H -0.3552 0.6017 -0.0358 0.115 Uiso 1 1 calc R A 1
C20 C -0.4020(12) 0.6427(11) 0.0604(6) 0.111(6) Uiso 0.70 1 d PD A 1
H20A H -0.4223 0.6969 0.0914 0.166 Uiso 1 1 calc R A 1
H20B H -0.3424 0.6304 0.0801 0.166 Uiso 1 1 calc R A 1
H20C H -0.4549 0.5929 0.0531 0.166 Uiso 1 1 calc R A 1
C21 C 0.2744(4) 0.8348(5) 0.0388(3) 0.0416(18) Uani 1 1 d D A -2
H21A H 0.3097 0.8528 0.0840 0.050 Uiso 1 1 calc R A -2
H21B H 0.2519 0.7702 0.0237 0.050 Uiso 1 1 calc R A -2
C22 C 0.3456(7) 0.8561(8) -0.0123(6) 0.0597(18) Uiso 0.70 1 d PD A -2
H22A H 0.3092 0.8364 -0.0573 0.072 Uiso 1 1 calc R A -2
H22B H 0.3637 0.9213 0.0020 0.072 Uiso 1 1 calc R A -2
C23 C 0.4387(6) 0.8156(8) -0.0202(5) 0.0597(18) Uiso 0.70 1 d PD A -2
H23A H 0.4791 0.8411 0.0233 0.072 Uiso 1 1 calc R A -2
H23B H 0.4212 0.7513 -0.0290 0.072 Uiso 1 1 calc R A -2
C24 C 0.5005(7) 0.8275(8) -0.0749(5) 0.0597(18) Uiso 0.70 1 d PD A -2
H24A H 0.5468 0.7843 -0.0855 0.089 Uiso 1 1 calc R A -2
H24B H 0.5373 0.8876 -0.0596 0.089 Uiso 1 1 calc R A -2
H24C H 0.4580 0.8184 -0.1155 0.089 Uiso 1 1 calc R A -2
C20A C -0.450(2) 0.665(2) 0.0507(15) 0.111(14) Uiso 0.30 1 d PD B -3
C22A C 0.336(2) 0.8164(18) -0.0225(13) 0.107(7) Uiso 0.30 1 d PD C -3
C23A C 0.4168(19) 0.8951(19) -0.0118(13) 0.107(7) Uiso 0.30 1 d PD C -3
C24A C 0.479(2) 0.890(2) -0.0710(15) 0.107(7) Uiso 0.30 1 d PD C -3
C1D C -0.1347(5) 0.8500(4) 0.1928(3) 0.0302(15) Uani 1 1 d . . .
C2D C -0.0925(5) 0.8098(5) 0.2333(3) 0.0453(19) Uani 1 1 d . A .
H2D H -0.0239 0.8063 0.2330 0.054 Uiso 1 1 calc R . .
C3D C -0.1505(6) 0.7746(5) 0.2745(4) 0.052(2) Uani 1 1 d . . .
H3D H -0.1212 0.7480 0.3028 0.062 Uiso 1 1 calc R A .
C4D C -0.2513(6) 0.7783(5) 0.2742(3) 0.0455(19) Uani 1 1 d . A .
C5D C -0.2922(5) 0.8204(5) 0.2355(4) 0.054(2) Uani 1 1 d . . .
H5D H -0.3606 0.8247 0.2363 0.065 Uiso 1 1 calc R A .
C6D C -0.2339(5) 0.8570(5) 0.1953(3) 0.0467(19) Uani 1 1 d . A .
H6D H -0.2626 0.8869 0.1694 0.056 Uiso 1 1 calc R . .
C1E C 0.1852(4) 0.8985(4) 0.2028(3) 0.0279(15) Uani 1 1 d . . .
C2E C 0.1726(5) 0.8088(5) 0.1921(3) 0.0383(17) Uani 1 1 d . A .
H2E H 0.1354 0.7689 0.1526 0.046 Uiso 1 1 calc R . .
C3E C 0.2134(5) 0.7756(5) 0.2383(3) 0.0433(18) Uani 1 1 d . . .
H3E H 0.2037 0.7138 0.2308 0.052 Uiso 1 1 calc R A .
C4E C 0.2682(5) 0.8341(5) 0.2950(3) 0.0421(18) Uani 1 1 d . A .
C5E C 0.2832(5) 0.9243(5) 0.3067(3) 0.0475(19) Uani 1 1 d . . .
H5E H 0.3217 0.9637 0.3458 0.057 Uiso 1 1 calc R A .
C6E C 0.2413(4) 0.9569(5) 0.2603(3) 0.0390(17) Uani 1 1 d . A .
H6E H 0.2509 1.0188 0.2679 0.047 Uiso 1 1 calc R . .
C1F C 0.0368(4) 0.7045(4) -0.0319(3) 0.0304(15) Uani 1 1 d . . .
C2F C 0.0265(5) 0.6931(5) -0.1010(3) 0.0388(17) Uani 1 1 d . A .
H2F H 0.0194 0.7420 -0.1153 0.047 Uiso 1 1 calc R . .
C3F C 0.0266(5) 0.6077(5) -0.1490(3) 0.0486(19) Uani 1 1 d . . .
H3F H 0.0192 0.5986 -0.1961 0.058 Uiso 1 1 calc R A .
C4F C 0.0376(5) 0.5381(5) -0.1273(4) 0.0488(19) Uani 1 1 d . A .
C5F C 0.0505(6) 0.5503(5) -0.0589(4) 0.053(2) Uani 1 1 d . . .
H5F H 0.0596 0.5019 -0.0445 0.063 Uiso 1 1 calc R A .
C6F C 0.0500(5) 0.6343(4) -0.0116(3) 0.0425(18) Uani 1 1 d . A .
H6F H 0.0590 0.6432 0.0354 0.051 Uiso 1 1 calc R . .
C1S C 0.5252(12) -0.0065(11) 0.4591(6) 0.112(7) Uiso 0.50 1 d PGD D -4
C2S C 0.5486(10) -0.0672(9) 0.4897(6) 0.084(7) Uiso 0.50 1 d PGD D -4
H2SA H 0.5904 -0.1094 0.4686 0.101 Uiso 0.50 1 calc PR D -4
C3S C 0.5100(10) -0.0654(9) 0.5516(6) 0.086(6) Uiso 0.50 1 d PG D -4
H3SA H 0.5258 -0.1065 0.5723 0.103 Uiso 0.50 1 calc PR D -4
C4S C 0.4482(10) -0.0030(11) 0.5829(5) 0.102(7) Uiso 0.50 1 d PG D -4
H4SA H 0.4222 -0.0018 0.6248 0.122 Uiso 0.50 1 calc PR D -4
C5S C 0.4249(10) 0.0576(10) 0.5523(7) 0.102(7) Uiso 0.50 1 d PG D -4
H5SA H 0.3831 0.0998 0.5734 0.123 Uiso 0.50 1 calc PR D -4
C6S C 0.4634(12) 0.0559(10) 0.4904(7) 0.106(9) Uiso 0.50 1 d PGD D -4
H6SA H 0.4476 0.0969 0.4696 0.127 Uiso 0.50 1 calc PR D -4
C7S C 0.555(2) -0.0185(17) 0.3858(7) 0.154(11) Uiso 0.50 1 d PD D -4
H7SA H 0.5978 -0.0649 0.3718 0.230 Uiso 0.50 1 calc PR D -4
H7SB H 0.5913 0.0374 0.3846 0.230 Uiso 0.50 1 calc PR D -4
H7SC H 0.4961 -0.0356 0.3547 0.230 Uiso 0.50 1 calc PR D -4
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Sn1 O6 2.073(4) . ?
Sn1 O5 2.075(3) . ?
Sn1 O4 2.087(3) . ?
Sn1 C1 2.118(5) . ?
Sn1 O1 2.153(4) . ?
Sn1 O2 2.166(4) . ?
Sn2 O4 2.043(4) . ?
Sn2 O10 2.067(3) . ?
Sn2 O9 2.071(3) . ?
Sn2 C5 2.120(6) . ?
Sn2 O3 2.159(3) . ?
Sn2 O1 2.208(3) . ?
Sn3 O4 2.059(3) . ?
Sn3 O8 2.063(4) . ?
Sn3 O7 2.079(4) . ?
Sn3 C9 2.125(5) . ?
Sn3 O3 2.162(4) . ?
Sn3 O2 2.216(3) . ?
Br1 C4A 1.902(6) . ?
Br2 C4B 1.904(6) . ?
Br3 C4C 1.911(7) . ?
P1 O9 1.522(4) . ?
P1 O5 1.525(4) . ?
P1 O8 1.526(4) 2_666 ?
P2 O10 1.512(4) 2_666 ?
P2 O6 1.528(4) . ?
P2 O7 1.530(4) . ?
O1 C1A 1.360(6) . ?
O2 C1B 1.374(6) . ?
O3 C1C 1.378(6) . ?
O8 P1 1.526(4) 2_666 ?
O10 P2 1.512(4) 2_666 ?
C1 C2 1.501(7) . ?
C2 C3 1.524(7) . ?
C3 C4 1.447(9) . ?
C5 C6 1.498(7) . ?
C6 C7 1.509(8) . ?
C7 C8 1.517(8) . ?
C9 C10 1.477(8) . ?
C10 C11 1.549(9) . ?
C11 C12 1.409(10) . ?
C1A C6A 1.379(7) . ?
C1A C2A 1.390(7) . ?
C2A C3A 1.382(7) . ?
C3A C4A 1.374(8) . ?
C4A C5A 1.367(8) . ?
C5A C6A 1.384(8) . ?
C1B C6B 1.350(8) . ?
C1B C2B 1.362(8) . ?
C2B C3B 1.381(8) . ?
C3B C4B 1.361(10) . ?
C4B C5B 1.357(10) . ?
C5B C6B 1.410(9) . ?
C1C C2C 1.377(8) . ?
C1C C6C 1.390(8) . ?
C2C C3C 1.375(8) . ?
C3C C4C 1.360(9) . ?
C4C C5C 1.360(9) . ?
C5C C6C 1.375(9) . ?
Sn4 O16 2.070(4) . ?
Sn4 O15 2.090(4) . ?
Sn4 O14 2.094(3) . ?
Sn4 C13 2.121(5) . ?
Sn4 O12 2.145(4) . ?
Sn4 O11 2.158(4) . ?
Sn5 O14 2.058(4) . ?
Sn5 O18 2.069(3) . ?
Sn5 O17 2.074(4) . ?
Sn5 C17 2.123(6) . ?
Sn5 O13 2.180(4) . ?
Sn5 O11 2.212(4) . ?
Sn6 O14 2.041(3) . ?
Sn6 O20 2.062(3) . ?
Sn6 O19 2.075(4) . ?
Sn6 C21 2.118(6) . ?
Sn6 O13 2.176(4) . ?
Sn6 O12 2.219(3) . ?
Br4 C4D 1.883(6) . ?
Br5 C4E 1.905(6) . ?
Br6 C4F 1.899(7) . ?
P3 O20 1.514(4) 2_575 ?
P3 O17 1.520(4) . ?
P3 O16 1.525(4) . ?
P4 O19 1.519(4) . ?
P4 O18 1.520(4) 2_575 ?
P4 O15 1.525(4) . ?
O11 C1D 1.366(6) . ?
O12 C1E 1.379(6) . ?
O13 C1F 1.383(7) . ?
O18 P4 1.520(4) 2_575 ?
O20 P3 1.514(4) 2_575 ?
C13 C14 1.519(7) . ?
C14 C15 1.518(7) . ?
C15 C16 1.516(7) . ?
C17 C18 1.524(8) . ?
C18 C19 1.507(8) . ?
C19 C20 1.479(11) . ?
C21 C22 1.540(9) . ?
C22 C23 1.481(10) . ?
C23 C24 1.472(9) . ?
C22A C23A 1.512(15) . ?
C23A C24A 1.488(14) . ?
C1D C6D 1.366(8) . ?
C1D C2D 1.375(8) . ?
C2D C3D 1.379(8) . ?
C3D C4D 1.377(9) . ?
C4D C5D 1.359(9) . ?
C5D C6D 1.377(8) . ?
C1E C2E 1.365(8) . ?
C1E C6E 1.382(8) . ?
C2E C3E 1.381(8) . ?
C3E C4E 1.364(9) . ?
C4E C5E 1.368(9) . ?
C5E C6E 1.385(8) . ?
C1F C6F 1.356(8) . ?
C1F C2F 1.384(8) . ?
C2F C3F 1.397(9) . ?
C3F C4F 1.358(9) . ?
C4F C5F 1.371(9) . ?
C5F C6F 1.376(9) . ?
C1S C2S 1.3900 . ?
C1S C6S 1.3900 . ?
C1S C7S 1.540(5) . ?
C2S C3S 1.3900 . ?
C3S C4S 1.3900 . ?
C4S C5S 1.3900 . ?
C5S C6S 1.3900 . ?
