#------------------------------------------------------------------------------
#$Date: 2016-03-21 06:30:19 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178515 $
#$URL: svn://www.crystallography.net/cod/cif/4/06/18/4061811.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4061811
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om050760o
_journal_year                    2005
_chemical_formula_moiety         'C72 H78 Ca4 O13'
_chemical_formula_sum            'C72 H78 Ca4 O13'
_chemical_formula_weight         1311.66
_chemical_name_common
'[bis(2,6-dimethoxyphenylcalcium)]3.[calciumoxide].[benzen'
_space_group_IT_number           4
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P 2yb'
_symmetry_space_group_name_H-M   'P 1 21 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 111.60(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   16.168(3)
_cell_length_b                   10.617(2)
_cell_length_c                   21.241(4)
_cell_measurement_temperature    183(2)
_cell_volume                     3390.0(12)
_diffrn_ambient_temperature      183(2)
_exptl_crystal_density_diffrn    1.285
_cod_original_sg_symbol_H-M      'P 21'
_cod_database_code               4061811
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ca1 Ca 0.41355(4) 0.57901(7) 0.26568(3) 0.03185(17) Uani 1 1 d . . .
Ca2 Ca 0.18241(4) 0.57796(7) 0.21421(3) 0.03090(17) Uani 1 1 d . . .
Ca3 Ca 0.28096(4) 0.58552(7) 0.09386(3) 0.03061(17) Uani 1 1 d . . .
Ca4 Ca 0.29239(5) 0.31367(6) 0.18899(3) 0.03211(18) Uani 1 1 d . . .
O1 O 0.36103(17) 0.1750(2) 0.13201(13) 0.0441(7) Uani 1 1 d . . .
O2 O 0.20687(16) 0.4918(2) -0.01529(11) 0.0399(6) Uani 1 1 d . . .
O3 O 0.55733(16) 0.4819(2) 0.29893(13) 0.0472(7) Uani 1 1 d . . .
O4 O 0.34970(18) 0.1706(2) 0.28455(13) 0.0468(7) Uani 1 1 d . . .
O5 O 0.45219(16) 0.6130(2) 0.38557(11) 0.0462(7) Uani 1 1 d . . .
O6 O 0.16672(16) 0.7676(2) 0.27048(12) 0.0418(6) Uani 1 1 d . . .
O7 O 0.12035(17) 0.4800(2) 0.28931(12) 0.0435(6) Uani 1 1 d . . .
O8 O 0.16528(16) 0.1769(2) 0.14792(13) 0.0447(7) Uani 1 1 d . . .
O9 O 0.21224(16) 0.7739(2) 0.03640(12) 0.0422(6) Uani 1 1 d . . .
O10 O 0.02957(15) 0.6081(2) 0.14158(12) 0.0410(6) Uani 1 1 d . . .
O11 O 0.49433(16) 0.7710(2) 0.27083(12) 0.0415(6) Uani 1 1 d . . .
O12 O 0.39468(16) 0.6286(2) 0.04797(12) 0.0418(6) Uani 1 1 d . . .
O13 O 0.29264(14) 0.5150(2) 0.19072(11) 0.0289(5) Uani 1 1 d . . .
C1 C 0.3268(2) 0.2197(3) 0.06538(17) 0.0346(9) Uani 1 1 d . . .
C2 C 0.2855(2) 0.3352(3) 0.05918(18) 0.0357(9) Uani 1 1 d . . .
C3 C 0.2490(2) 0.3748(3) -0.00733(18) 0.0340(9) Uani 1 1 d . . .
C4 C 0.2529(2) 0.3100(4) -0.06276(19) 0.0423(9) Uani 1 1 d . . .
H4 H 0.2267 0.3442 -0.1076 0.051 Uiso 1 1 d R . .
C5 C 0.2955(3) 0.1975(4) -0.0508(2) 0.0468(11) Uani 1 1 d . . .
H5 H 0.2993 0.1511 -0.0884 0.056 Uiso 1 1 d R . .
C6 C 0.3330(3) 0.1494(4) 0.0129(2) 0.0421(10) Uani 1 1 d . . .
H6 H 0.3619 0.0688 0.0211 0.051 Uiso 1 1 d R . .
C7 C 0.3995(3) 0.0534(4) 0.1453(2) 0.0687(14) Uani 1 1 d . . .
H7A H 0.3552 -0.0093 0.1200 0.103 Uiso 1 1 d R . .
H7B H 0.4189 0.0356 0.1939 0.103 Uiso 1 1 d R . .
H7C H 0.4508 0.0496 0.1313 0.103 Uiso 1 1 d R . .
C8 C 0.1515(3) 0.5323(4) -0.08045(19) 0.0563(12) Uani 1 1 d . . .
H8A H 0.1867 0.5439 -0.1090 0.085 Uiso 1 1 d R . .
H8B H 0.1238 0.6124 -0.0764 0.085 Uiso 1 1 d R . .
H8C H 0.1052 0.4691 -0.1009 0.085 Uiso 1 1 d R . .
C11 C 0.5404(3) 0.3637(3) 0.32065(19) 0.0392(9) Uani 1 1 d . . .
C12 C 0.4524(2) 0.3282(3) 0.29273(17) 0.0354(8) Uani 1 1 d . . .
C13 C 0.4378(3) 0.2121(4) 0.31534(18) 0.0407(9) Uani 1 1 d . . .
C14 C 0.5004(3) 0.1385(4) 0.36249(19) 0.0492(11) Uani 1 1 d . . .
H14 H 0.4843 0.0595 0.3768 0.059 Uiso 1 1 d R . .
C15 C 0.5861(3) 0.1833(4) 0.3879(2) 0.0604(13) Uani 1 1 d . . .
H15 H 0.6312 0.1351 0.4215 0.072 Uiso 1 1 d R . .
C16 C 0.6081(3) 0.2957(4) 0.3666(2) 0.0520(11) Uani 1 1 d . . .
H16A H 0.6677 0.3254 0.3830 0.062 Uiso 1 1 calc R . .
C17 C 0.6460(2) 0.5199(4) 0.3126(2) 0.0584(12) Uani 1 1 d . . .
H17A H 0.6768 0.5302 0.3616 0.088 Uiso 1 1 d R . .
H17B H 0.6462 0.6001 0.2899 0.088 Uiso 1 1 d R . .
H17C H 0.6765 0.4557 0.2960 0.088 Uiso 1 1 d R . .
C18 C 0.3275(3) 0.0464(4) 0.2981(3) 0.0655(13) Uani 1 1 d . . .
H18A H 0.3629 -0.0144 0.2839 0.098 Uiso 1 1 d R . .
H18B H 0.2641 0.0310 0.2729 0.098 Uiso 1 1 d R . .
H18C H 0.3404 0.0370 0.3467 0.098 Uiso 1 1 d R . .
C21 C 0.2424(2) 0.7675(3) 0.32993(18) 0.0368(9) Uani 1 1 d . . .
C22 C 0.3090(2) 0.6904(3) 0.32706(17) 0.0348(9) Uani 1 1 d . . .
C23 C 0.3830(3) 0.6918(4) 0.38686(18) 0.0391(9) Uani 1 1 d . . .
C24 C 0.3931(3) 0.7622(4) 0.44400(19) 0.0476(10) Uani 1 1 d . . .
H24 H 0.4472 0.7607 0.4831 0.057 Uiso 1 1 d R . .
C25 C 0.3210(3) 0.8346(4) 0.4416(2) 0.0516(11) Uani 1 1 d . . .
H25 H 0.3247 0.8835 0.4805 0.062 Uiso 1 1 d R . .
C26 C 0.2458(3) 0.8384(4) 0.38565(19) 0.0450(10) Uani 1 1 d . . .
H26 H 0.1960 0.8890 0.3843 0.054 Uiso 1 1 d R . .
C27 C 0.0920(3) 0.8382(4) 0.2680(2) 0.0588(12) Uani 1 1 d . . .
H27A H 0.0719 0.8094 0.3038 0.088 Uiso 1 1 d R . .
H27B H 0.0442 0.8265 0.2238 0.088 Uiso 1 1 d R . .
H27C H 0.1079 0.9276 0.2747 0.088 Uiso 1 1 d R . .
C28 C 0.5248(3) 0.5889(6) 0.44715(18) 0.0667(13) Uani 1 1 d . . .
H28A H 0.5582 0.6671 0.4631 0.100 Uiso 1 1 d R . .
H28B H 0.5642 0.5252 0.4397 0.100 Uiso 1 1 d R . .
H28C H 0.5021 0.5584 0.4812 0.100 Uiso 1 1 d R . .
C31 C 0.1163(2) 0.2143(3) 0.18675(17) 0.0363(9) Uani 1 1 d . . .
C32 C 0.1425(2) 0.3288(3) 0.21814(17) 0.0346(8) Uani 1 1 d . . .
C33 C 0.0955(2) 0.3627(3) 0.25766(18) 0.0360(9) Uani 1 1 d . . .
C34 C 0.0281(3) 0.2940(4) 0.2663(2) 0.0481(10) Uani 1 1 d . . .
H34 H -0.0030 0.3242 0.2940 0.058 Uiso 1 1 d R . .
C35 C 0.0063(3) 0.1815(4) 0.2327(2) 0.0542(11) Uani 1 1 d . . .
H35 H -0.0409 0.1317 0.2371 0.065 Uiso 1 1 d R . .
C36 C 0.0502(2) 0.1390(4) 0.1930(2) 0.0467(10) Uani 1 1 d . . .
H36 H 0.0361 0.0591 0.1704 0.056 Uiso 1 1 d R . .
C37 C 0.0920(3) 0.5132(4) 0.3427(2) 0.0567(11) Uani 1 1 d . . .
H37A H 0.0277 0.5285 0.3249 0.085 Uiso 1 1 d R . .
H37B H 0.1232 0.5896 0.3651 0.085 Uiso 1 1 d R . .
H37C H 0.1061 0.4439 0.3754 0.085 Uiso 1 1 d R . .
C38 C 0.1392(3) 0.0654(4) 0.1074(2) 0.0603(12) Uani 1 1 d . . .
H38A H 0.1478 -0.0084 0.1369 0.090 Uiso 1 1 d R . .
H38B H 0.1752 0.0564 0.0793 0.090 Uiso 1 1 d R . .
H38C H 0.0762 0.0722 0.0782 0.090 Uiso 1 1 d R . .
C41 C 0.1257(2) 0.7669(3) 0.03815(17) 0.0343(8) Uani 1 1 d . . .
C42 C 0.1218(2) 0.6903(3) 0.08956(18) 0.0341(9) Uani 1 1 d . . .
C43 C 0.0369(2) 0.6855(3) 0.08991(17) 0.0349(9) Uani 1 1 d . . .
C44 C -0.0365(3) 0.7480(4) 0.04683(19) 0.0448(10) Uani 1 1 d . . .
H44 H -0.0932 0.7402 0.0515 0.054 Uiso 1 1 d R . .
C45 C -0.0255(2) 0.8213(4) -0.0030(2) 0.0496(11) Uani 1 1 d . . .
H45 H -0.0751 0.8668 -0.0340 0.059 Uiso 1 1 d R . .
C46 C 0.0558(2) 0.8321(4) -0.00826(18) 0.0427(10) Uani 1 1 d . . .
H46 H 0.0646 0.8823 -0.0429 0.051 Uiso 1 1 d R . .
C47 C 0.2250(3) 0.8468(4) -0.0148(2) 0.0516(11) Uani 1 1 d . . .
H47A H 0.1859 0.8164 -0.0594 0.077 Uiso 1 1 d R . .
H47B H 0.2872 0.8394 -0.0108 0.077 Uiso 1 1 d R . .
H47C H 0.2113 0.9352 -0.0095 0.077 Uiso 1 1 d R . .
C48 C -0.0548(2) 0.5931(5) 0.1470(2) 0.0513(10) Uani 1 1 d . . .
H48A H -0.0746 0.6724 0.1604 0.077 Uiso 1 1 d R . .
H48B H -0.0503 0.5282 0.1809 0.077 Uiso 1 1 d R . .
H48C H -0.0978 0.5664 0.1029 0.077 Uiso 1 1 d R . .
C51 C 0.5027(2) 0.7745(3) 0.20729(17) 0.0342(9) Uani 1 1 d . . .
C52 C 0.4427(2) 0.6997(3) 0.15926(18) 0.0347(8) Uani 1 1 d . . .
C53 C 0.4539(2) 0.7042(3) 0.09784(18) 0.0346(9) Uani 1 1 d . . .
C54 C 0.5151(2) 0.7780(3) 0.0831(2) 0.0412(9) Uani 1 1 d . . .
H54 H 0.5174 0.7786 0.0386 0.049 Uiso 1 1 d R . .
C55 C 0.5727(3) 0.8486(4) 0.1349(2) 0.0451(10) Uani 1 1 d . . .
H55 H 0.6174 0.8987 0.1270 0.054 Uiso 1 1 d R . .
C56 C 0.5679(2) 0.8481(3) 0.1978(2) 0.0413(9) Uani 1 1 d . . .
H56A H 0.6078 0.8966 0.2338 0.050 Uiso 1 1 calc R . .
C57 C 0.5580(3) 0.8320(4) 0.3264(2) 0.0543(11) Uani 1 1 d . . .
H57A H 0.6170 0.7976 0.3335 0.081 Uiso 1 1 d R . .
H57B H 0.5443 0.8186 0.3672 0.081 Uiso 1 1 d R . .
H57C H 0.5574 0.9224 0.3170 0.081 Uiso 1 1 d R . .
C58 C 0.4081(3) 0.6084(5) -0.01338(19) 0.0585(12) Uani 1 1 d . . .
H58A H 0.3953 0.6859 -0.0403 0.088 Uiso 1 1 d R . .
H58B H 0.3685 0.5411 -0.0390 0.088 Uiso 1 1 d R . .
H58C H 0.4701 0.5836 -0.0031 0.088 Uiso 1 1 d R . .
C61 C 0.7049(3) 0.8435(5) 0.58448(18) 0.099(2) Uani 1 1 d G . .
H61 H 0.6807 0.8685 0.6176 0.118 Uiso 1 1 d R . .
C62 C 0.6936(2) 0.9200(3) 0.5288(2) 0.0847(16) Uani 1 1 d G . .
H62 H 0.6615 0.9978 0.5234 0.102 Uiso 1 1 d R . .
C63 C 0.7288(2) 0.8837(3) 0.48090(16) 0.0749(14) Uani 1 1 d G . .
H63 H 0.7210 0.9364 0.4424 0.090 Uiso 1 1 d R . .
C64 C 0.7752(2) 0.7710(4) 0.4887(2) 0.0853(17) Uani 1 1 d G . .
H64 H 0.7995 0.7459 0.4556 0.102 Uiso 1 1 d R . .
C65 C 0.7865(2) 0.6945(3) 0.5444(2) 0.0988(19) Uani 1 1 d G . .
H65 H 0.8186 0.6167 0.5498 0.119 Uiso 1 1 d R . .
C66 C 0.7513(3) 0.7308(5) 0.59228(18) 0.106(2) Uani 1 1 d G . .
H66 H 0.7591 0.6780 0.6307 0.127 Uiso 1 1 d R . .
C71 C 0.7522(2) 0.2939(5) 0.1998(2) 0.102(2) Uani 1 1 d G . .
H71 H 0.8148 0.2770 0.2141 0.122 Uiso 1 1 d R . .
C72 C 0.7153(3) 0.3983(4) 0.1599(2) 0.0808(16) Uani 1 1 d G . .
H72 H 0.7524 0.4542 0.1463 0.097 Uiso 1 1 d R . .
C73 C 0.6246(3) 0.4217(4) 0.13944(18) 0.0884(17) Uani 1 1 d G . .
H73 H 0.5991 0.4938 0.1118 0.106 Uiso 1 1 d R . .
C74 C 0.5708(2) 0.3408(5) 0.1590(2) 0.0956(19) Uani 1 1 d G . .
H74 H 0.5082 0.3570 0.1449 0.115 Uiso 1 1 d R . .
C75 C 0.6077(4) 0.2365(4) 0.1990(2) 0.110(2) Uani 1 1 d G . .
H75 H 0.5706 0.1806 0.2125 0.133 Uiso 1 1 d R . .
C76 C 0.6984(4) 0.2130(3) 0.2194(2) 0.123(3) Uani 1 1 d G . .
H76 H 0.7239 0.1409 0.2470 0.147 Uiso 1 1 d R . .
C81 C 0.8127(2) 0.8671(3) 0.25861(15) 0.0782(15) Uani 1 1 d G . .
H81 H 0.7787 0.9225 0.2227 0.094 Uiso 1 1 d R . .
C82 C 0.7967(2) 0.7381(4) 0.25282(15) 0.0830(16) Uani 1 1 d G . .
H82 H 0.7515 0.7046 0.2130 0.100 Uiso 1 1 d R . .
C83 C 0.8462(3) 0.6578(3) 0.3047(2) 0.0828(16) Uani 1 1 d G . .
H83A H 0.8353 0.5697 0.3007 0.099 Uiso 1 1 calc R . .
C84 C 0.9117(2) 0.7064(4) 0.36231(16) 0.0892(18) Uani 1 1 d G . .
H84 H 0.9459 0.6509 0.3981 0.107 Uiso 1 1 d R . .
C85 C 0.9277(2) 0.8353(4) 0.36810(15) 0.101(2) Uani 1 1 d G . .
H85 H 0.9729 0.8689 0.4079 0.121 Uiso 1 1 d R . .
C86 C 0.8781(3) 0.9157(3) 0.31626(19) 0.0923(18) Uani 1 1 d G . .
H86 H 0.8892 1.0047 0.3203 0.111 Uiso 1 1 d R . .
C91 C 0.0901(4) 0.8836(4) 0.5522(2) 0.163(4) Uani 1 1 d G . .
H91 H 0.0870 0.9721 0.5604 0.196 Uiso 1 1 d R . .
C92 C 0.1496(3) 0.8386(4) 0.5240(2) 0.103(2) Uani 1 1 d G . .
H92A H 0.1874 0.8954 0.5128 0.124 Uiso 1 1 calc R . .
C93 C 0.1537(2) 0.7103(5) 0.51231(17) 0.0803(16) Uani 1 1 d G . .
H93 H 0.1947 0.6792 0.4929 0.096 Uiso 1 1 d R . .
C94 C 0.0983(3) 0.6271(4) 0.5287(2) 0.104(2) Uani 1 1 d G . .
H94 H 0.1011 0.5386 0.5206 0.125 Uiso 1 1 d R . .
C95 C 0.0389(3) 0.6722(6) 0.5568(2) 0.157(4) Uani 1 1 d G . .
H95 H 0.0006 0.6148 0.5682 0.189 Uiso 1 1 d R . .
C96 C 0.0348(3) 0.8005(7) 0.5686(2) 0.199(7) Uani 1 1 d G . .
H96 H -0.0063 0.8316 0.5880 0.239 Uiso 1 1 d R . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ca1 O13 2.128(2) . ?
Ca1 O3 2.399(3) . ?
Ca1 O11 2.402(2) . ?
Ca1 O5 2.415(2) . ?
Ca1 C12 2.748(4) . ?
Ca1 C22 2.752(4) . ?
Ca1 C52 2.785(4) . ?
Ca1 C11 3.006(4) . ?
Ca1 C23 3.039(4) . ?
Ca1 C51 3.039(4) . ?
Ca1 Ca4 3.4753(12) . ?
Ca1 Ca2 3.4862(13) . ?
Ca2 O13 2.128(2) . ?
Ca2 O6 2.402(2) . ?
Ca2 O10 2.405(2) . ?
Ca2 O7 2.411(2) . ?
Ca2 C32 2.732(4) . ?
Ca2 C42 2.735(4) . ?
Ca2 C22 2.784(4) . ?
Ca2 C33 3.000(4) . ?
Ca2 C43 3.039(4) . ?
Ca2 C21 3.046(4) . ?
Ca2 Ca4 3.4675(11) . ?
Ca2 Ca3 3.4755(12) . ?
Ca3 O13 2.131(2) . ?
Ca3 O9 2.393(2) . ?
Ca3 O2 2.399(2) . ?
Ca3 O12 2.421(2) . ?
Ca3 C52 2.750(4) . ?
Ca3 C2 2.766(4) . ?
Ca3 C42 2.773(4) . ?
Ca3 C3 3.012(4) . ?
Ca3 C41 3.036(4) . ?
Ca3 C53 3.039(4) . ?
Ca4 O13 2.138(2) . ?
Ca4 O8 2.403(3) . ?
Ca4 O1 2.419(2) . ?
Ca4 O4 2.429(3) . ?
Ca4 C12 2.716(4) . ?
Ca4 C32 2.718(4) . ?
Ca4 C2 2.728(4) . ?
Ca4 C31 3.021(4) . ?
Ca4 C13 3.041(4) . ?
Ca4 C1 3.046(3) . ?
O1 C1 1.399(4) . ?
O1 C7 1.416(5) . ?
O2 C3 1.397(4) . ?
O2 C8 1.410(4) . ?
O3 C11 1.398(5) . ?
O3 C17 1.413(4) . ?
O4 C13 1.402(5) . ?
O4 C18 1.423(5) . ?
O5 C23 1.405(4) . ?
O5 C28 1.423(4) . ?
O6 C21 1.398(4) . ?
O6 C27 1.406(4) . ?
O7 C33 1.402(4) . ?
O7 C37 1.415(4) . ?
O8 C31 1.396(4) . ?
O8 C38 1.432(5) . ?
O9 C47 1.410(4) . ?
O9 C41 1.415(4) . ?
O10 C43 1.411(4) . ?
O10 C48 1.419(4) . ?
O11 C57 1.406(4) . ?
O11 C51 1.406(4) . ?
O12 C53 1.391(4) . ?
O12 C58 1.414(4) . ?
C1 C6 1.375(5) . ?
C1 C2 1.380(5) . ?
C2 C3 1.381(5) . ?
C3 C4 1.384(5) . ?
C4 C5 1.355(6) . ?
C5 C6 1.362(5) . ?
C11 C16 1.373(5) . ?
C11 C12 1.377(5) . ?
C12 C13 1.374(5) . ?
C13 C14 1.375(5) . ?
C14 C15 1.374(6) . ?
C15 C16 1.369(6) . ?
C21 C22 1.373(5) . ?
C21 C26 1.387(5) . ?
C22 C23 1.388(5) . ?
C23 C24 1.383(5) . ?
C24 C25 1.381(6) . ?
C25 C26 1.352(6) . ?
C31 C32 1.376(5) . ?
C31 C36 1.380(5) . ?
C32 C33 1.371(5) . ?
C33 C34 1.379(5) . ?
C34 C35 1.369(6) . ?
C35 C36 1.363(6) . ?
C41 C42 1.382(5) . ?
C41 C46 1.382(5) . ?
C42 C43 1.377(5) . ?
C43 C44 1.374(5) . ?
C44 C45 1.377(6) . ?
C45 C46 1.365(5) . ?
C51 C52 1.373(5) . ?
C51 C56 1.385(5) . ?
C52 C53 1.382(5) . ?
C53 C54 1.386(5) . ?
C54 C55 1.374(5) . ?
C55 C56 1.366(5) . ?
C61 C62 1.3900 . ?
C61 C66 1.3900 . ?
C62 C63 1.3900 . ?
C63 C64 1.3900 . ?
C64 C65 1.3900 . ?
C65 C66 1.3900 . ?
C71 C72 1.3900 . ?
C71 C76 1.3900 . ?
C72 C73 1.3900 . ?
C73 C74 1.3900 . ?
C74 C75 1.3900 . ?
C75 C76 1.3900 . ?
C81 C82 1.3900 . ?
C81 C86 1.3900 . ?
C82 C83 1.3900 . ?
C83 C84 1.3900 . ?
C84 C85 1.3900 . ?
C85 C86 1.3900 . ?
C91 C92 1.3900 . ?
C91 C96 1.3900 . ?
C92 C93 1.3900 . ?
C93 C94 1.3900 . ?
C94 C95 1.3900 . ?
C95 C96 1.3900 . ?
