#------------------------------------------------------------------------------
#$Date: 2017-02-15 10:49:39 +0200 (Wed, 15 Feb 2017) $
#$Revision: 192124 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/06/23/4062379.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4062379
loop_
_publ_author_name
'Kunrath, Fábio A.'
'de Souza, Roberto F.'
'Casagrande, Jr., Osvaldo L.'
'Brooks, Neil R.'
'Young, Victor G.'
_publ_section_title
;
 Highly Selective Nickel Ethylene Oligomerization Catalysts Based on
 Sterically Hindered Tris(pyrazolyl)borate Ligands
;
_journal_issue                   23
_journal_name_full               Organometallics
_journal_page_first              4739
_journal_page_last               4743
_journal_paper_doi               10.1021/om034035u
_journal_volume                  22
_journal_year                    2003
_chemical_formula_moiety         'C36 H40 B Cl N6 Ni'
_chemical_formula_sum            'C36 H40 B Cl N6 Ni'
_chemical_formula_weight         661.71
_space_group_IT_number           1
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  'P 1'
_symmetry_space_group_name_H-M   'P 1'
_cell_angle_alpha                102.601(2)
_cell_angle_beta                 97.437(2)
_cell_angle_gamma                95.017(2)
_cell_formula_units_Z            2
_cell_length_a                   9.1756(10)
_cell_length_b                   10.9562(12)
_cell_length_c                   17.497(2)
_cell_measurement_temperature    173(2)
_cell_volume                     1690.0(3)
_diffrn_ambient_temperature      173(2)
_exptl_crystal_density_diffrn    1.300
_cod_depositor_comments
;
The following automatic conversions were performed:
'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to '/home/saulius/struct/CIF-dictionaries/cif_core.dic'
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_enum 1527 2010-12-29 10:47:43Z saulius 
;
_cod_database_code               4062379
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ni1 Ni -0.50719(4) 0.21847(4) -0.13078(3) 0.02269(11) Uani 1 1 d . . .
Cl1 Cl -0.32073(11) 0.24688(12) -0.19015(6) 0.0461(3) Uani 1 1 d . . .
B1 B -0.7471(5) 0.1957(4) -0.0300(3) 0.0263(9) Uani 1 1 d . . .
H1 H -0.839(4) 0.184(3) 0.006(2) 0.025(10) Uiso 1 1 d . . .
N1 N -0.5044(3) 0.3271(3) -0.02233(18) 0.0242(6) Uani 1 1 d . . .
N2 N -0.6242(3) 0.3042(3) 0.01358(19) 0.0253(7) Uani 1 1 d . . .
C3 C -0.6078(4) 0.3820(4) 0.0853(2) 0.0267(8) Uani 1 1 d . . .
H3A H -0.6758 0.3842 0.1220 0.032 Uiso 1 1 calc R . .
C4 C -0.4749(4) 0.4592(3) 0.0970(2) 0.0278(8) Uani 1 1 d . . .
H4A H -0.4346 0.5238 0.1424 0.033 Uiso 1 1 calc R . .
C5 C -0.4126(4) 0.4219(3) 0.0280(2) 0.0241(7) Uani 1 1 d . . .
C6 C -0.2716(4) 0.4714(3) 0.0065(2) 0.0251(7) Uani 1 1 d . . .
C7 C -0.2733(5) 0.5432(4) -0.0501(2) 0.0323(9) Uani 1 1 d . . .
C8 C -0.1411(5) 0.5910(4) -0.0681(3) 0.0413(11) Uani 1 1 d . . .
H8A H -0.1423 0.6408 -0.1063 0.050 Uiso 1 1 calc R . .
C9 C -0.0055(5) 0.5677(5) -0.0311(3) 0.0457(11) Uani 1 1 d . . .
C10 C -0.0057(4) 0.4973(4) 0.0249(2) 0.0350(9) Uani 1 1 d . . .
H10A H 0.0861 0.4809 0.0503 0.042 Uiso 1 1 calc R . .
C11 C -0.1367(4) 0.4491(3) 0.0457(2) 0.0276(8) Uani 1 1 d . . .
C12 C -0.4169(5) 0.5687(4) -0.0936(3) 0.0448(11) Uani 1 1 d . . .
H12A H -0.5006 0.5294 -0.0743 0.067 Uiso 1 1 calc R . .
H12B H -0.4225 0.5334 -0.1505 0.067 Uiso 1 1 calc R . .
H12C H -0.4208 0.6598 -0.0840 0.067 Uiso 1 1 calc R . .
C13 C 0.1399(6) 0.6180(6) -0.0521(4) 0.0726(18) Uani 1 1 d . . .
H13A H 0.2223 0.5912 -0.0208 0.109 Uiso 1 1 calc R . .
H13B H 0.1489 0.7102 -0.0405 0.109 Uiso 1 1 calc R . .
H13C H 0.1422 0.5850 -0.1087 0.109 Uiso 1 1 calc R . .
C14 C -0.1293(5) 0.3746(4) 0.1082(2) 0.0372(9) Uani 1 1 d . . .
H14A H -0.2299 0.3479 0.1162 0.056 Uiso 1 1 calc R . .
H14B H -0.0743 0.4270 0.1580 0.056 Uiso 1 1 calc R . .
H14C H -0.0790 0.3002 0.0913 0.056 Uiso 1 1 calc R . .
N21 N -0.5620(3) 0.0654(3) -0.09175(17) 0.0242(6) Uani 1 1 d . . .
N22 N -0.6742(3) 0.0731(3) -0.04732(18) 0.0260(6) Uani 1 1 d . . .
C23 C -0.6999(4) -0.0357(4) -0.0255(2) 0.0297(8) Uani 1 1 d . . .
H23A H -0.7723 -0.0541 0.0059 0.036 Uiso 1 1 calc R . .
C24 C -0.6036(4) -0.1166(4) -0.0563(2) 0.0292(8) Uani 1 1 d . . .
H24A H -0.5975 -0.2004 -0.0507 0.035 Uiso 1 1 calc R . .
C25 C -0.5182(4) -0.0508(3) -0.0967(2) 0.0248(8) Uani 1 1 d . . .
C26 C -0.3906(4) -0.0880(3) -0.1373(2) 0.0257(8) Uani 1 1 d . . .
C27 C -0.2469(4) -0.0345(3) -0.1024(2) 0.0292(8) Uani 1 1 d . . .
C28 C -0.1278(4) -0.0736(4) -0.1396(3) 0.0351(9) Uani 1 1 d . . .
H28A H -0.0304 -0.0365 -0.1160 0.042 Uiso 1 1 calc R . .
C29 C -0.1474(5) -0.1642(4) -0.2091(3) 0.0383(10) Uani 1 1 d . . .
C30 C -0.2904(5) -0.2170(4) -0.2434(3) 0.0355(10) Uani 1 1 d . . .
H30A H -0.3055 -0.2790 -0.2918 0.043 Uiso 1 1 calc R . .
C31 C -0.4123(4) -0.1805(3) -0.2079(2) 0.0308(8) Uani 1 1 d . . .
C32 C -0.2176(4) 0.0645(4) -0.0260(2) 0.0372(9) Uani 1 1 d . . .
H32A H -0.3116 0.0821 -0.0076 0.056 Uiso 1 1 calc R . .
H32B H -0.1670 0.1418 -0.0347 0.056 Uiso 1 1 calc R . .
H32C H -0.1550 0.0342 0.0140 0.056 Uiso 1 1 calc R . .
C33 C -0.0153(6) -0.2039(5) -0.2488(3) 0.0590(14) Uani 1 1 d . . .
H33A H 0.0761 -0.1568 -0.2167 0.089 Uiso 1 1 calc R . .
H33B H -0.0256 -0.1860 -0.3016 0.089 Uiso 1 1 calc R . .
H33C H -0.0115 -0.2943 -0.2537 0.089 Uiso 1 1 calc R . .
C34 C -0.5660(5) -0.2444(4) -0.2460(3) 0.0413(10) Uani 1 1 d . . .
H34A H -0.5591 -0.3064 -0.2947 0.062 Uiso 1 1 calc R . .
H34B H -0.6282 -0.1811 -0.2588 0.062 Uiso 1 1 calc R . .
H34C H -0.6099 -0.2869 -0.2092 0.062 Uiso 1 1 calc R . .
N41 N -0.7189(3) 0.2346(3) -0.16454(18) 0.0250(7) Uani 1 1 d . . .
N42 N -0.8100(3) 0.2246(3) -0.10873(19) 0.0268(7) Uani 1 1 d . . .
C43 C -0.9481(4) 0.2375(4) -0.1382(3) 0.0329(9) Uani 1 1 d . . .
H43A H -1.0315 0.2344 -0.1113 0.040 Uiso 1 1 calc R . .
C44 C -0.9503(4) 0.2558(4) -0.2125(2) 0.0358(9) Uani 1 1 d . . .
H44A H -1.0338 0.2682 -0.2469 0.043 Uiso 1 1 calc R . .
C45 C -0.8049(4) 0.2527(3) -0.2282(2) 0.0264(8) Uani 1 1 d . . .
C46 C -0.7497(4) 0.2653(3) -0.3026(2) 0.0262(8) Uani 1 1 d . . .
C47 C -0.7763(4) 0.3716(4) -0.3332(2) 0.0303(8) Uani 1 1 d . . .
C48 C -0.7336(5) 0.3781(4) -0.4052(2) 0.0349(9) Uani 1 1 d . . .
H48A H -0.7519 0.4498 -0.4256 0.042 Uiso 1 1 calc R . .
C49 C -0.6655(4) 0.2852(4) -0.4489(2) 0.0337(9) Uani 1 1 d . . .
C50 C -0.6377(4) 0.1812(4) -0.4180(2) 0.0297(8) Uani 1 1 d . . .
H50A H -0.5879 0.1176 -0.4462 0.036 Uiso 1 1 calc R . .
C51 C -0.6815(4) 0.1684(3) -0.3465(2) 0.0265(8) Uani 1 1 d . . .
C52 C -0.8512(5) 0.4767(4) -0.2905(3) 0.0454(11) Uani 1 1 d . . .
H52A H -0.8589 0.5413 -0.3212 0.068 Uiso 1 1 calc R . .
H52B H -0.7931 0.5138 -0.2382 0.068 Uiso 1 1 calc R . .
H52C H -0.9505 0.4435 -0.2842 0.068 Uiso 1 1 calc R . .
C53 C -0.6254(6) 0.2935(5) -0.5290(3) 0.0482(12) Uani 1 1 d . . .
H53A H -0.6533 0.3722 -0.5414 0.072 Uiso 1 1 calc R . .
H53B H -0.6786 0.2218 -0.5697 0.072 Uiso 1 1 calc R . .
H53C H -0.5186 0.2920 -0.5279 0.072 Uiso 1 1 calc R . .
C54 C -0.6567(5) 0.0488(4) -0.3195(2) 0.0368(9) Uani 1 1 d . . .
H54A H -0.6076 -0.0057 -0.3579 0.055 Uiso 1 1 calc R . .
H54B H -0.7523 0.0047 -0.3158 0.055 Uiso 1 1 calc R . .
H54C H -0.5943 0.0698 -0.2675 0.055 Uiso 1 1 calc R . .
Ni2 Ni -0.38328(4) -0.13530(4) 0.35207(3) 0.02505(12) Uani 1 1 d . . .
Cl2 Cl -0.55701(12) -0.03217(11) 0.39346(7) 0.0513(3) Uani 1 1 d . . .
B101 B -0.1490(5) -0.2841(4) 0.2817(2) 0.0258(9) Uani 1 1 d . . .
H101 H -0.072(4) -0.340(4) 0.258(2) 0.032(11) Uiso 1 1 d . . .
N101 N -0.1662(3) -0.0936(3) 0.38840(19) 0.0270(7) Uani 1 1 d . . .
N102 N -0.0788(3) -0.1728(3) 0.35043(19) 0.0270(7) Uani 1 1 d . . .
C103 C 0.0653(4) -0.1308(4) 0.3791(2) 0.0307(9) Uani 1 1 d . . .
H10B H 0.1482 -0.1690 0.3622 0.037 Uiso 1 1 calc R . .
C104 C 0.0701(4) -0.0220(4) 0.4377(2) 0.0340(9) Uani 1 1 d . . .
H10C H 0.1561 0.0280 0.4689 0.041 Uiso 1 1 calc R . .
C105 C -0.0769(4) -0.0009(3) 0.4418(2) 0.0285(8) Uani 1 1 d . . .
C106 C -0.1361(4) 0.1075(3) 0.4898(2) 0.0283(8) Uani 1 1 d . . .
C107 C -0.1541(5) 0.2130(4) 0.4587(3) 0.0389(10) Uani 1 1 d . . .
C108 C -0.2078(5) 0.3167(4) 0.5044(3) 0.0449(11) Uani 1 1 d . . .
H10D H -0.2203 0.3889 0.4836 0.054 Uiso 1 1 calc R . .
C109 C -0.2432(5) 0.3160(4) 0.5792(3) 0.0411(10) Uani 1 1 d . . .
C110 C -0.2229(4) 0.2110(4) 0.6080(2) 0.0385(10) Uani 1 1 d . . .
H11A H -0.2485 0.2091 0.6587 0.046 Uiso 1 1 calc R . .
C111 C -0.1663(4) 0.1067(4) 0.5662(2) 0.0312(8) Uani 1 1 d . . .
C112 C -0.1186(7) 0.2171(5) 0.3776(3) 0.0653(16) Uani 1 1 d . . .
H11B H -0.0831 0.1377 0.3539 0.098 Uiso 1 1 calc R . .
H11C H -0.0416 0.2872 0.3821 0.098 Uiso 1 1 calc R . .
H11D H -0.2079 0.2288 0.3441 0.098 Uiso 1 1 calc R . .
C113 C -0.2980(6) 0.4293(5) 0.6277(3) 0.0574(14) Uani 1 1 d . . .
H11E H -0.3046 0.4947 0.5975 0.086 Uiso 1 1 calc R . .
H11F H -0.2289 0.4620 0.6771 0.086 Uiso 1 1 calc R . .
H11G H -0.3960 0.4049 0.6400 0.086 Uiso 1 1 calc R . .
C114 C -0.1319(5) 0.0001(4) 0.6042(3) 0.0448(11) Uani 1 1 d . . .
H11H H -0.0935 -0.0647 0.5666 0.067 Uiso 1 1 calc R . .
H11I H -0.2223 -0.0362 0.6192 0.067 Uiso 1 1 calc R . .
H11J H -0.0574 0.0318 0.6515 0.067 Uiso 1 1 calc R . .
N121 N -0.3733(3) -0.3182(3) 0.34916(18) 0.0272(7) Uani 1 1 d . . .
N122 N -0.2604(3) -0.3689(3) 0.31398(18) 0.0263(6) Uani 1 1 d . . .
C123 C -0.2721(4) -0.4931(3) 0.3116(2) 0.0300(8) Uani 1 1 d . . .
H12D H -0.2072 -0.5495 0.2899 0.036 Uiso 1 1 calc R . .
C124 C -0.3913(5) -0.5252(4) 0.3451(2) 0.0340(9) Uani 1 1 d . . .
H12E H -0.4249 -0.6061 0.3518 0.041 Uiso 1 1 calc R . .
C125 C -0.4542(4) -0.4121(3) 0.3677(2) 0.0263(8) Uani 1 1 d . . .
C126 C -0.5888(4) -0.3933(3) 0.4053(2) 0.0276(8) Uani 1 1 d . . .
C127 C -0.5787(4) -0.3141(4) 0.4829(2) 0.0308(9) Uani 1 1 d . . .
C128 C -0.7065(5) -0.3000(4) 0.5167(2) 0.0355(9) Uani 1 1 d . . .
H12F H -0.6996 -0.2474 0.5683 0.043 Uiso 1 1 calc R . .
C129 C -0.8424(5) -0.3594(4) 0.4785(3) 0.0358(9) Uani 1 1 d . . .
C130 C -0.8517(4) -0.4376(4) 0.4038(2) 0.0321(9) Uani 1 1 d . . .
H13D H -0.9455 -0.4793 0.3770 0.038 Uiso 1 1 calc R . .
C131 C -0.7275(4) -0.4565(3) 0.3672(2) 0.0275(8) Uani 1 1 d . . .
C132 C -0.4313(5) -0.2462(5) 0.5278(3) 0.0471(11) Uani 1 1 d . . .
H13E H -0.4458 -0.1965 0.5795 0.071 Uiso 1 1 calc R . .
H13F H -0.3895 -0.1902 0.4974 0.071 Uiso 1 1 calc R . .
H13G H -0.3632 -0.3081 0.5356 0.071 Uiso 1 1 calc R . .
C133 C -0.9817(5) -0.3403(5) 0.5160(3) 0.0498(12) Uani 1 1 d . . .
H13H H -0.9558 -0.2830 0.5685 0.075 Uiso 1 1 calc R . .
H13I H -1.0278 -0.4216 0.5212 0.075 Uiso 1 1 calc R . .
H13J H -1.0513 -0.3040 0.4824 0.075 Uiso 1 1 calc R . .
C134 C -0.7452(5) -0.5439(4) 0.2861(3) 0.0413(11) Uani 1 1 d . . .
H13K H -0.6485 -0.5474 0.2680 0.062 Uiso 1 1 calc R . .
H13L H -0.8130 -0.5126 0.2488 0.062 Uiso 1 1 calc R . .
H13M H -0.7854 -0.6285 0.2887 0.062 Uiso 1 1 calc R . .
N141 N -0.3558(3) -0.1665(3) 0.23857(18) 0.0260(6) Uani 1 1 d . . .
N142 N -0.2395(3) -0.2303(3) 0.21860(19) 0.0247(7) Uani 1 1 d . . .
C143 C -0.2327(4) -0.2395(3) 0.1411(2) 0.0276(8) Uani 1 1 d . . .
H14D H -0.1615 -0.2792 0.1127 0.033 Uiso 1 1 calc R . .
C144 C -0.3458(4) -0.1818(4) 0.1101(2) 0.0314(8) Uani 1 1 d . . .
H14E H -0.3681 -0.1740 0.0569 0.038 Uiso 1 1 calc R . .
C145 C -0.4218(4) -0.1368(3) 0.1735(2) 0.0259(8) Uani 1 1 d . . .
C146 C -0.5591(4) -0.0750(3) 0.1752(2) 0.0270(8) Uani 1 1 d . . .
C147 C -0.5585(4) 0.0522(3) 0.1758(2) 0.0295(8) Uani 1 1 d . . .
C148 C -0.6889(5) 0.1059(4) 0.1794(2) 0.0334(9) Uani 1 1 d . . .
H14F H -0.6876 0.1926 0.1792 0.040 Uiso 1 1 calc R . .
C149 C -0.8217(4) 0.0382(4) 0.1831(2) 0.0338(9) Uani 1 1 d . . .
C150 C -0.8195(4) -0.0876(4) 0.1828(2) 0.0357(9) Uani 1 1 d . . .
H15A H -0.9091 -0.1360 0.1853 0.043 Uiso 1 1 calc R . .
C151 C -0.6923(4) -0.1463(4) 0.1791(2) 0.0309(8) Uani 1 1 d . . .
C152 C -0.4186(5) 0.1328(4) 0.1700(3) 0.0462(11) Uani 1 1 d . . .
H15B H -0.4403 0.2193 0.1716 0.069 Uiso 1 1 calc R . .
H15C H -0.3833 0.0983 0.1201 0.069 Uiso 1 1 calc R . .
H15D H -0.3421 0.1328 0.2147 0.069 Uiso 1 1 calc R . .
C153 C -0.9618(5) 0.0975(5) 0.1881(3) 0.0498(12) Uani 1 1 d . . .
H15E H -0.9424 0.1870 0.1883 0.075 Uiso 1 1 calc R . .
H15F H -0.9991 0.0890 0.2369 0.075 Uiso 1 1 calc R . .
H15G H -1.0359 0.0555 0.1422 0.075 Uiso 1 1 calc R . .
C154 C -0.6964(5) -0.2830(4) 0.1826(3) 0.0465(11) Uani 1 1 d . . .
H15H H -0.7978 -0.3167 0.1850 0.070 Uiso 1 1 calc R . .
H15I H -0.6308 -0.2900 0.2299 0.070 Uiso 1 1 calc R . .
H15J H -0.6632 -0.3310 0.1352 0.070 Uiso 1 1 calc R . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Ni1 N41 1.990(3) . ?
Ni1 N21 1.993(3) . ?
Ni1 N1 2.004(3) . ?
Ni1 Cl1 2.1473(10) . ?
B1 N42 1.532(5) . ?
B1 N22 1.541(5) . ?
B1 N2 1.554(5) . ?
N1 C5 1.349(5) . ?
N1 N2 1.366(4) . ?
N2 C3 1.336(5) . ?
C3 C4 1.386(5) . ?
C4 C5 1.399(5) . ?
C5 C6 1.484(5) . ?
C6 C7 1.393(5) . ?
C6 C11 1.402(5) . ?
C7 C8 1.380(6) . ?
C7 C12 1.513(6) . ?
C8 C9 1.397(7) . ?
C9 C10 1.374(6) . ?
C9 C13 1.518(6) . ?
C10 C11 1.393(5) . ?
C11 C14 1.500(6) . ?
N21 C25 1.357(4) . ?
N21 N22 1.366(4) . ?
N22 C23 1.339(5) . ?
C23 C24 1.382(5) . ?
C24 C25 1.378(5) . ?
C25 C26 1.489(5) . ?
C26 C31 1.395(5) . ?
C26 C27 1.399(5) . ?
C27 C28 1.394(5) . ?
C27 C32 1.503(5) . ?
C28 C29 1.372(6) . ?
C29 C30 1.389(6) . ?
C29 C33 1.522(6) . ?
C30 C31 1.394(6) . ?
C31 C34 1.518(6) . ?
N41 C45 1.341(5) . ?
N41 N42 1.381(4) . ?
N42 C43 1.336(5) . ?
C43 C44 1.355(6) . ?
C44 C45 1.399(5) . ?
C45 C46 1.486(5) . ?
C46 C47 1.411(5) . ?
C46 C51 1.411(5) . ?
C47 C48 1.380(6) . ?
C47 C52 1.501(6) . ?
C48 C49 1.381(6) . ?
C49 C50 1.393(5) . ?
C49 C53 1.515(6) . ?
C50 C51 1.394(5) . ?
C51 C54 1.511(5) . ?
Ni2 N101 1.992(3) . ?
Ni2 N141 1.993(3) . ?
Ni2 N121 2.004(3) . ?
Ni2 Cl2 2.1446(11) . ?
B101 N102 1.540(5) . ?
B101 N142 1.545(5) . ?
B101 N122 1.561(5) . ?
N101 C105 1.349(5) . ?
N101 N102 1.358(4) . ?
N102 C103 1.353(5) . ?
C103 C104 1.385(6) . ?
C104 C105 1.397(5) . ?
C105 C106 1.485(5) . ?
C106 C107 1.394(6) . ?
C106 C111 1.400(5) . ?
C107 C108 1.406(6) . ?
C107 C112 1.505(7) . ?
C108 C109 1.390(7) . ?
C109 C110 1.371(6) . ?
C109 C113 1.508(6) . ?
C110 C111 1.396(6) . ?
C111 C114 1.502(6) . ?
N121 C125 1.338(5) . ?
N121 N122 1.369(4) . ?
N122 C123 1.346(5) . ?
C123 C124 1.361(6) . ?
C124 C125 1.412(5) . ?
C125 C126 1.482(5) . ?
C126 C131 1.403(5) . ?
C126 C127 1.430(5) . ?
C127 C128 1.385(6) . ?
C127 C132 1.515(6) . ?
C128 C129 1.371(6) . ?
C129 C130 1.384(6) . ?
C129 C133 1.521(6) . ?
C130 C131 1.388(5) . ?
C131 C134 1.510(6) . ?
N141 C145 1.336(5) . ?
N141 N142 1.367(4) . ?
N142 C143 1.347(5) . ?
C143 C144 1.375(5) . ?
C144 C145 1.408(5) . ?
C145 C146 1.482(5) . ?
C146 C147 1.390(5) . ?
C146 C151 1.410(5) . ?
C147 C148 1.382(6) . ?
C147 C152 1.520(6) . ?
C148 C149 1.386(6) . ?
C149 C150 1.379(6) . ?
C149 C153 1.495(6) . ?
C150 C151 1.383(5) . ?
C151 C154 1.509(5) . ?
