#------------------------------------------------------------------------------
#$Date: 2016-03-21 06:36:07 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178523 $
#$URL: svn://www.crystallography.net/cod/cif/4/06/27/4062767.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4062767
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om0496232
_journal_year                    2004
_chemical_formula_sum            'C69 H109 Cl K9 N4 O8 Pt2'
_chemical_formula_weight         1900.15
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 114.75(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   23.154(5)
_cell_length_b                   14.737(3)
_cell_length_c                   27.657(6)
_cell_measurement_temperature    150(2)
_cell_volume                     8570(3)
_diffrn_ambient_temperature      150(2)
_exptl_crystal_density_diffrn    1.473
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4062767
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.82334(2) 0.35695(3) 0.118322(18) 0.03412(15) Uani 1 1 d . . .
Pt2 Pt 1.03526(2) 0.29689(3) 0.411626(19) 0.04021(16) Uani 1 1 d . . .
Cl1 Cl 1.00722(14) 0.3818(2) 0.25281(12) 0.0408(7) Uani 1 1 d . . .
K1 K 0.88297(12) 0.44969(19) 0.25894(11) 0.0422(7) Uani 1 1 d . . .
K2 K 0.86718(14) 0.5902(2) 0.14679(11) 0.0472(7) Uani 1 1 d . . .
K3 K 1.01970(16) 0.6045(2) 0.26065(13) 0.0633(9) Uani 1 1 d . . .
K4 K 0.97266(12) 0.42753(19) 0.13259(10) 0.0428(7) Uani 1 1 d . . .
K5 K 1.13184(18) 0.4716(3) 0.23539(14) 0.0756(11) Uani 1 1 d . . .
K6 K 1.12744(15) 0.4199(2) 0.35918(11) 0.0520(8) Uani 1 1 d . . .
K7 K 1.09565(15) 0.2434(2) 0.22458(12) 0.0536(8) Uani 1 1 d . . .
K8 K 1.13142(14) 0.1853(2) 0.36094(12) 0.0519(8) Uani 1 1 d . . .
K9 K 0.96846(13) 0.18569(19) 0.27519(12) 0.0469(7) Uani 1 1 d . . .
O1 O 0.7938(3) 0.4438(5) 0.1607(3) 0.041(2) Uani 1 1 d . . .
O2 O 0.9051(4) 0.6186(5) 0.2487(3) 0.044(2) Uani 1 1 d . . .
O3 O 0.9912(4) 0.5943(6) 0.1617(3) 0.048(2) Uani 1 1 d . . .
O4 O 1.1340(5) 0.5678(6) 0.3146(3) 0.069(3) Uani 1 1 d . . .
O5 O 1.0845(4) 0.3643(6) 0.1537(3) 0.043(2) Uani 1 1 d . . .
O6 O 1.1793(4) 0.3119(6) 0.3135(3) 0.055(2) Uani 1 1 d . . .
O7 O 1.0648(4) 0.1110(5) 0.2696(4) 0.054(2) Uani 1 1 d . . .
O8 O 1.0219(4) 0.1702(5) 0.3810(3) 0.046(2) Uani 1 1 d . . .
N1 N 0.8559(4) 0.2789(6) 0.0790(4) 0.034(2) Uani 1 1 d . . .
N2 N 0.8323(5) 0.4540(7) 0.0665(4) 0.040(3) Uani 1 1 d . . .
N3 N 1.0477(5) 0.4197(7) 0.4401(4) 0.046(3) Uani 1 1 d . . .
N4 N 1.1360(5) 0.2991(8) 0.4486(4) 0.057(3) Uani 1 1 d . . .
C1 C 0.8316(5) 0.2427(8) 0.1608(5) 0.045(3) Uani 1 1 d . . .
C2 C 0.8141(6) 0.2224(9) 0.2011(5) 0.046(3) Uani 1 1 d . . .
H2A H 0.7930 0.2697 0.2127 0.055 Uiso 1 1 calc R . .
C3 C 0.8200(6) 0.1369(9) 0.2237(6) 0.051(4) Uani 1 1 d . . .
H3A H 0.7987 0.1237 0.2470 0.061 Uiso 1 1 calc R . .
C4 C 0.8449(6) 0.0663(11) 0.2053(6) 0.059(4) Uani 1 1 d . . .
H4A H 0.8414 0.0036 0.2155 0.071 Uiso 1 1 calc R . .
C5 C 0.8623(6) 0.0840(9) 0.1636(6) 0.057(4) Uani 1 1 d . . .
H5A H 0.8762 0.0340 0.1476 0.068 Uiso 1 1 calc R . .
C6 C 0.8575(6) 0.1700(9) 0.1432(5) 0.046(3) Uani 1 1 d . . .
C7 C 0.8736(5) 0.1930(9) 0.0975(5) 0.042(3) Uani 1 1 d . . .
C8 C 0.9022(6) 0.1408(9) 0.0710(6) 0.056(4) Uani 1 1 d . . .
H8A H 0.9156 0.0820 0.0825 0.068 Uiso 1 1 calc R . .
C9 C 0.9102(6) 0.1754(10) 0.0291(5) 0.055(4) Uani 1 1 d . . .
H9A H 0.9305 0.1409 0.0127 0.065 Uiso 1 1 calc R . .
C10 C 0.8894(6) 0.2587(9) 0.0108(5) 0.044(3) Uani 1 1 d . . .
H10A H 0.8944 0.2808 -0.0187 0.053 Uiso 1 1 calc R . .
C11 C 0.8608(6) 0.3118(9) 0.0351(5) 0.044(3) Uani 1 1 d . . .
C12 C 0.8329(5) 0.4064(9) 0.0194(5) 0.041(3) Uani 1 1 d . . .
C13 C 0.7636(6) 0.3913(9) -0.0224(5) 0.052(4) Uani 1 1 d . . .
H13A H 0.7612 0.4010 -0.0575 0.079 Uiso 1 1 calc R . .
H13B H 0.7358 0.4332 -0.0159 0.079 Uiso 1 1 calc R . .
H13C H 0.7507 0.3303 -0.0196 0.079 Uiso 1 1 calc R . .
C14 C 0.8676(6) 0.4627(10) -0.0059(5) 0.059(4) Uani 1 1 d . . .
H14A H 0.8404 0.4725 -0.0428 0.088 Uiso 1 1 calc R . .
H14B H 0.9053 0.4312 -0.0029 0.088 Uiso 1 1 calc R . .
H14C H 0.8793 0.5201 0.0120 0.088 Uiso 1 1 calc R . .
C15 C 0.9446(6) 0.3386(9) 0.3813(5) 0.050(4) Uani 1 1 d . . .
C16 C 0.8866(6) 0.2860(9) 0.3477(5) 0.049(4) Uani 1 1 d . . .
H16A H 0.8897 0.2217 0.3401 0.059 Uiso 1 1 calc R . .
C17 C 0.8290(7) 0.3276(12) 0.3306(6) 0.065(4) Uani 1 1 d . . .
H17A H 0.7908 0.2909 0.3120 0.078 Uiso 1 1 calc R . .
C18 C 0.8218(7) 0.4150(12) 0.3441(5) 0.061(4) Uani 1 1 d . . .
H18A H 0.7795 0.4387 0.3373 0.073 Uiso 1 1 calc R . .
C19 C 0.8761(7) 0.4640(10) 0.3746(5) 0.058(4) Uani 1 1 d . . .
H19A H 0.8720 0.5237 0.3885 0.069 Uiso 1 1 calc R . .
C20 C 0.9355(6) 0.4232(9) 0.3925(5) 0.046(3) Uani 1 1 d . . .
C21 C 0.9926(7) 0.4720(9) 0.4254(5) 0.053(4) Uani 1 1 d . . .
C22 C 1.0019(8) 0.5590(10) 0.4444(6) 0.067(4) Uani 1 1 d . . .
H22A H 0.9668 0.5970 0.4347 0.080 Uiso 1 1 calc R . .
C23 C 1.0596(8) 0.5921(10) 0.4766(6) 0.070(5) Uani 1 1 d . . .
H23A H 1.0635 0.6517 0.4886 0.083 Uiso 1 1 calc R . .
C24 C 1.1139(7) 0.5363(10) 0.4921(5) 0.059(4) Uani 1 1 d . . .
H24A H 1.1539 0.5585 0.5142 0.071 Uiso 1 1 calc R . .
C25 C 1.1063(7) 0.4481(10) 0.4736(6) 0.058(4) Uani 1 1 d . . .
C26 C 1.1562(7) 0.3715(9) 0.4900(5) 0.049(4) Uani 1 1 d . . .
C27 C 1.2221(6) 0.4104(10) 0.4973(6) 0.062(4) Uani 1 1 d . . .
C28 C 1.1622(7) 0.3362(9) 0.5439(5) 0.059(4) Uani 1 1 d . . .
H28A H 1.1872 0.3779 0.5714 0.088 Uiso 1 1 calc R . .
H28B H 1.1826 0.2779 0.5507 0.088 Uiso 1 1 calc R . .
H28C H 1.1207 0.3306 0.5434 0.088 Uiso 1 1 calc R . .
C29 C 0.7275(6) 0.4617(9) 0.1453(6) 0.052(4) Uani 1 1 d . . .
C30 C 0.7178(8) 0.4570(15) 0.1969(7) 0.100(7) Uani 1 1 d . . .
C31 C 0.7115(9) 0.5471(16) 0.1201(12) 0.184(15) Uani 1 1 d . . .
C32 C 0.6877(7) 0.3881(13) 0.1139(9) 0.119(8) Uani 1 1 d . . .
H32A H 0.6903 0.3849 0.0802 0.178 Uiso 1 1 calc R . .
H32B H 0.6444 0.3989 0.1082 0.178 Uiso 1 1 calc R . .
H32C H 0.7020 0.3318 0.1326 0.178 Uiso 1 1 calc R . .
C33 C 0.8918(7) 0.6981(9) 0.2680(5) 0.052(4) Uani 1 1 d . . .
C34 C 0.9507(10) 0.7400(14) 0.3137(8) 0.117(8) Uani 1 1 d . . .
C35 C 0.8633(11) 0.7709(11) 0.2233(7) 0.109(8) Uani 1 1 d . . .
C36 C 0.8443(10) 0.6813(14) 0.2908(8) 0.118(7) Uiso 1 1 d . . .
H36A H 0.8148 0.7310 0.2819 0.176 Uiso 1 1 calc R . .
H36B H 0.8660 0.6762 0.3289 0.176 Uiso 1 1 calc R . .
H36C H 0.8216 0.6261 0.2764 0.176 Uiso 1 1 calc R . .
C37 C 1.0062(7) 0.6649(10) 0.1360(6) 0.059(4) Uani 1 1 d . . .
C38 C 0.9520(9) 0.7033(18) 0.0933(10) 0.167(13) Uani 1 1 d . . .
C39 C 1.0444(14) 0.6323(18) 0.1077(12) 0.190(13) Uiso 1 1 d . . .
H39A H 1.0800 0.6720 0.1153 0.286 Uiso 1 1 calc R . .
H39B H 1.0184 0.6318 0.0701 0.286 Uiso 1 1 calc R . .
H39C H 1.0594 0.5720 0.1194 0.286 Uiso 1 1 calc R . .
C40 C 1.0523(10) 0.7326(13) 0.1725(8) 0.104(6) Uiso 1 1 d . . .
C41 C 1.1819(8) 0.6354(11) 0.3400(7) 0.077(5) Uiso 1 1 d . . .
C42 C 1.2256(9) 0.6113(11) 0.3975(7) 0.104(7) Uani 1 1 d . . .
C43 C 1.1482(10) 0.7246(13) 0.3392(8) 0.104(6) Uiso 1 1 d . . .
C44 C 1.2217(12) 0.6540(16) 0.3082(10) 0.140(9) Uiso 1 1 d . . .
C45 C 1.1045(6) 0.3436(9) 0.1144(5) 0.050(4) Uani 1 1 d . . .
C46 C 1.1690(6) 0.3895(9) 0.1266(5) 0.056(4) Uani 1 1 d . . .
H46A H 1.1952 0.3493 0.1172 0.084 Uiso 1 1 calc R . .
H46B H 1.1898 0.4033 0.1639 0.084 Uiso 1 1 calc R . .
H46C H 1.1621 0.4446 0.1064 0.084 Uiso 1 1 calc R . .
C47 C 1.1107(9) 0.2405(12) 0.1109(7) 0.088(6) Uani 1 1 d . . .
C48 C 1.0541(7) 0.3767(13) 0.0597(6) 0.082(6) Uani 1 1 d . . .
C49 C 1.2455(6) 0.2988(13) 0.3277(5) 0.068(5) Uani 1 1 d . . .
C50 C 1.2617(8) 0.1942(13) 0.3282(7) 0.084(5) Uani 1 1 d . . .
C51 C 1.2839(7) 0.3353(11) 0.3832(6) 0.078(5) Uani 1 1 d . . .
H51A H 1.2749 0.3987 0.3842 0.116 Uiso 1 1 calc R . .
H51B H 1.3284 0.3275 0.3923 0.116 Uiso 1 1 calc R . .
H51C H 1.2728 0.3030 0.4082 0.116 Uiso 1 1 calc R . .
C52 C 1.2640(7) 0.3512(15) 0.2893(7) 0.112(8) Uani 1 1 d . . .
C53 C 1.0777(8) 0.0243(10) 0.2561(6) 0.065(4) Uani 1 1 d . . .
C54 C 1.1361(10) -0.0170(11) 0.3056(8) 0.118(8) Uani 1 1 d . . .
C55 C 1.0213(10) -0.0406(12) 0.2455(9) 0.129(9) Uani 1 1 d . . .
H55A H 1.0371 -0.0983 0.2618 0.194 Uiso 1 1 calc R . .
H55B H 0.9977 -0.0485 0.2079 0.194 Uiso 1 1 calc R . .
H55C H 0.9941 -0.0153 0.2604 0.194 Uiso 1 1 calc R . .
C56 C 1.0944(10) 0.0275(11) 0.2090(8) 0.101(7) Uani 1 1 d . . .
C57 C 1.0194(6) 0.0942(9) 0.4119(6) 0.050(4) Uani 1 1 d . . .
C58 C 0.9830(8) 0.1161(11) 0.4453(7) 0.092(6) Uani 1 1 d . . .
H58A H 1.0044 0.1638 0.4699 0.137 Uiso 1 1 calc R . .
H58B H 0.9809 0.0629 0.4645 0.137 Uiso 1 1 calc R . .
H58C H 0.9407 0.1353 0.4223 0.137 Uiso 1 1 calc R . .
C59 C 0.9843(8) 0.0187(10) 0.3736(6) 0.081(5) Uani 1 1 d . . .
H59A H 1.0066 0.0034 0.3522 0.121 Uiso 1 1 calc R . .
H59B H 0.9421 0.0385 0.3510 0.121 Uiso 1 1 calc R . .
H59C H 0.9822 -0.0337 0.3934 0.121 Uiso 1 1 calc R . .
C60 C 1.0864(7) 0.0608(11) 0.4488(7) 0.084(6) Uani 1 1 d . . .
C61 C 0.7856(16) 0.773(2) 0.0446(12) 0.172(12) Uiso 1 1 d . . .
H61A H 0.8247 0.8018 0.0561 0.206 Uiso 1 1 calc R . .
C62 C 0.7666(11) 0.7113(14) 0.0039(9) 0.116(7) Uiso 1 1 d . . .
H62A H 0.7949 0.6982 -0.0110 0.139 Uiso 1 1 calc R . .
C63 C 0.7092(14) 0.6675(18) -0.0166(11) 0.153(10) Uiso 1 1 d . . .
H63A H 0.7006 0.6253 -0.0437 0.184 Uiso 1 1 calc R . .
C64 C 0.6628(14) 0.6854(17) 0.0027(11) 0.154(10) Uiso 1 1 d . . .
H64A H 0.6223 0.6601 -0.0105 0.185 Uiso 1 1 calc R . .
C65 C 0.6894(11) 0.7518(14) 0.0478(9) 0.109(7) Uiso 1 1 d . . .
H65A H 0.6626 0.7682 0.0637 0.131 Uiso 1 1 calc R . .
C66 C 0.7458(12) 0.7892(17) 0.0675(9) 0.138(10) Uani 1 1 d . . .
H66A H 0.7582 0.8269 0.0971 0.166 Uiso 1 1 calc R . .
C67 C 1.0520(11) 0.0174(15) 0.0480(8) 0.093(7) Uani 1 1 d . . .
H67A H 1.0865 0.0305 0.0799 0.112 Uiso 1 1 calc R . .
C68 C 1.0056(15) -0.0438(13) 0.0460(9) 0.105(8) Uani 1 1 d . . .
H68A H 1.0091 -0.0747 0.0764 0.126 Uiso 1 1 calc R . .
C69 C 0.9545(10) -0.0578(13) -0.0016(11) 0.094(6) Uani 1 1 d . . .
H69A H 0.9226 -0.0969 -0.0024 0.112 Uiso 1 1 calc R . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Pt1 N1 1.939(9) . ?
Pt1 C1 2.015(13) . ?
Pt1 O1 2.039(8) . ?
Pt1 N2 2.096(9) . ?
Pt1 K4 3.471(3) . ?
Pt1 K2 3.577(3) . ?
Pt1 K1 3.795(3) . ?
Pt2 N3 1.946(11) . ?
Pt2 C15 2.003(13) . ?
Pt2 O8 2.019(9) . ?
Pt2 N4 2.118(10) . ?
Pt2 K8 3.499(3) . ?
Pt2 K6 3.541(3) . ?
Pt2 K9 3.799(3) . ?
Cl1 K1 3.117(4) . ?
Cl1 K6 3.140(4) . ?
Cl1 K4 3.150(4) . ?
Cl1 K9 3.163(4) . ?
Cl1 K7 3.209(4) . ?
Cl1 K3 3.295(4) . ?
Cl1 K5 3.388(5) . ?
K1 O2 2.580(8) . ?
K1 O1 2.637(8) . ?
K1 C18 3.256(13) . ?
K1 C19 3.275(13) . ?
K1 C17 3.286(14) . ?
K1 C20 3.394(12) . ?
K1 C16 3.418(13) . ?
K1 C30 3.477(18) . ?
K1 C15 3.482(13) . ?
K1 K2 3.618(4) . ?
K2 O2 2.610(9) . ?
K2 O3 2.725(9) . ?
K2 N2 2.848(10) . ?
K2 O1 2.870(9) . ?
K2 C38 3.35(2) . ?
K2 C31 3.423(19) . ?
K2 C35 3.425(17) . ?
K2 C37 3.530(15) . ?
K2 C33 3.534(13) . ?
K2 K4 3.559(4) . ?
K3 O4 2.492(11) . ?
K3 O3 2.536(8) . ?
K3 O2 2.542(9) . ?
K3 C34 3.26(2) . ?
K3 C33 3.349(14) . ?
K3 C43 3.36(2) . ?
K3 C40 3.41(2) . ?
K3 C37 3.445(15) . ?
K3 C41 3.498(18) . ?
K3 K5 3.547(5) . ?
K4 O3 2.565(8) . ?
K4 O5 2.578(8) . ?
K4 N2 3.014(10) . ?
K4 N1 3.308(9) . ?
K4 C11 3.323(12) . ?
K4 C48 3.372(16) . ?
K4 C12 3.447(11) . ?
K4 C45 3.519(14) . ?
K4 K5 3.649(5) . ?
K5 O4 2.592(10) . ?
K5 O5 2.595(9) . ?
K5 O6 3.070(10) . ?
K5 C52 3.304(18) . ?
K5 K7 3.450(5) . ?
K5 C44 3.48(2) . ?
K5 K6 3.550(5) . ?
K6 O4 2.540(9) . ?
K6 O6 2.616(10) . ?
K6 N4 2.986(12) . ?
K6 C25 3.422(14) . ?
K6 N3 3.445(11) . ?
K6 K8 3.459(4) . ?
K6 C26 3.467(12) . ?
K6 C42 3.497(17) . ?
K6 C27 3.521(14) . ?
K6 C41 3.539(17) . ?
K7 O7 2.571(9) . ?
K7 O5 2.581(8) . ?
K7 O6 2.613(9) . ?
K7 C56 3.209(16) . ?
K7 C47 3.305(16) . ?
K7 C53 3.414(16) . ?
K7 C45 3.469(13) . ?
K7 K8 3.609(4) . ?
K7 K9 3.848(4) . ?
K8 O7 2.587(9) . ?
K8 O6 2.766(9) . ?
K8 O8 2.823(9) . ?
K8 N4 2.913(12) . ?
K8 C54 3.373(17) . ?
K8 C50 3.496(17) . ?
K8 K9 3.517(4) . ?
K8 C60 3.532(16) . ?
K9 O7 2.549(9) . ?
K9 O8 2.668(8) . ?
K9 C3 3.204(12) . ?
K9 C4 3.223(14) . ?
K9 C2 3.336(13) . ?
K9 C5 3.386(13) . ?
K9 C6 3.483(13) . ?
K9 C1 3.517(12) . ?
O1 C29 1.433(14) . ?
O2 C33 1.375(14) . ?
O3 C37 1.385(15) . ?
O4 C41 1.438(18) . ?
O5 C45 1.382(15) . ?
O6 C49 1.427(15) . ?
O7 C53 1.398(15) . ?
O8 C57 1.425(14) . ?
N1 C11 1.356(14) . ?
N1 C7 1.363(15) . ?
N2 C12 1.485(15) . ?
N3 C25 1.351(17) . ?
N3 C21 1.397(16) . ?
N4 C26 1.490(16) . ?
C1 C2 1.370(18) . ?
C1 C6 1.409(17) . ?
C2 C3 1.387(16) . ?
C3 C4 1.387(19) . ?
C4 C5 1.396(19) . ?
C5 C6 1.374(17) . ?
C6 C7 1.499(18) . ?
C7 C8 1.404(18) . ?
C8 C9 1.350(19) . ?
C9 C10 1.339(18) . ?
C10 C11 1.366(17) . ?
C11 C12 1.522(18) . ?
C12 C14 1.514(17) . ?
C12 C13 1.553(15) . ?
C15 C20 1.322(17) . ?
C15 C16 1.491(18) . ?
C16 C17 1.360(17) . ?
C17 C18 1.37(2) . ?
C18 C19 1.389(19) . ?
C19 C20 1.389(17) . ?
C20 C21 1.444(19) . ?
C21 C22 1.368(18) . ?
C22 C23 1.35(2) . ?
C23 C24 1.411(19) . ?
C24 C25 1.381(19) . ?
C25 C26 1.542(19) . ?
C26 C28 1.529(17) . ?
C26 C27 1.561(19) . ?
C29 C31 1.41(2) . ?
C29 C32 1.45(2) . ?
C29 C30 1.54(2) . ?
C33 C36 1.50(2) . ?
C33 C34 1.55(2) . ?
C33 C35 1.56(2) . ?
C37 C38 1.43(2) . ?
C37 C39 1.49(3) . ?
C37 C40 1.50(2) . ?
C41 C43 1.52(2) . ?
C41 C42 1.53(2) . ?
C41 C44 1.54(3) . ?
C45 C47 1.53(2) . ?
C45 C46 1.543(17) . ?
C45 C48 1.553(19) . ?
C49 C52 1.51(2) . ?
C49 C51 1.515(19) . ?
C49 C50 1.58(2) . ?
C53 C56 1.51(2) . ?
C53 C55 1.55(2) . ?
C53 C54 1.59(2) . ?
C57 C59 1.516(19) . ?
C57 C58 1.52(2) . ?
C57 C60 1.538(18) . ?
C61 C66 1.34(3) . ?
C61 C62 1.36(3) . ?
C62 C63 1.37(3) . ?
C63 C64 1.41(3) . ?
C64 C65 1.50(3) . ?
C65 C66 1.31(3) . ?
C67 C69 1.36(2) 3_755 ?
C67 C68 1.39(3) . ?
C68 C69 1.37(3) . ?
C69 C67 1.36(2) 3_755 ?
