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#$Date: 2022-09-15 01:26:15 +0300 (Thu, 15 Sep 2022) $
#$Revision: 277847 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/06/27/4062774.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4062774
loop_
_publ_author_name
'Filippou, Alexander C.'
'Philippopoulos, Athanassios I.'
'Portius, Peter'
'Schnakenburg, Gregor'
_journal_name_full               Organometallics
_journal_paper_doi               10.1021/om049625m
_journal_year                    2004
_chemical_formula_moiety         'C64 H66 Ge N P4 W, C24 B F20'
_chemical_formula_sum            'C88 H66 B F20 Ge N P4 W'
_chemical_formula_weight         1908.55
_space_group_IT_number           2
_space_group_name_Hall           '-P 1'
_space_group_name_H-M_alt        'P -1'
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_cell_angle_alpha                104.17(4)
_cell_angle_beta                 97.74(3)
_cell_angle_gamma                90.75(3)
_cell_formula_units_Z            2
_cell_length_a                   11.655(4)
_cell_length_b                   17.604(6)
_cell_length_c                   20.121(6)
_cell_measurement_temperature    180(2)
_cell_volume                     3962(2)
_diffrn_ambient_temperature      180(2)
_exptl_crystal_density_diffrn    1.600
_cod_database_code               4062774
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.7086(2) 0.87109(14) 0.55527(11) 0.0293(5) Uani 1 1 d . . .
C2 C 0.6972(2) 0.95752(14) 0.58308(12) 0.0318(5) Uani 1 1 d . . .
C3 C 0.5839(2) 0.97142(14) 0.58701(11) 0.0330(5) Uani 1 1 d . . .
C4 C 0.5156(2) 0.89727(15) 0.56182(11) 0.0321(5) Uani 1 1 d . . .
C5 C 0.5863(2) 0.83781(14) 0.54246(11) 0.0314(5) Uani 1 1 d . . .
C6 C 0.7753(2) 0.84870(19) 0.49330(13) 0.0456(7) Uani 1 1 d . . .
H6C H 0.7789 0.7915 0.4791 0.055 Uiso 1 1 calc R . .
H6B H 0.8540 0.8726 0.5064 0.055 Uiso 1 1 calc R . .
H6A H 0.7355 0.8676 0.4548 0.055 Uiso 1 1 calc R . .
C7 C 0.7989(2) 1.01527(17) 0.59957(15) 0.0483(7) Uani 1 1 d . . .
H7C H 0.7729 1.0683 0.6169 0.058 Uiso 1 1 calc R . .
H7B H 0.8341 1.0129 0.5576 0.058 Uiso 1 1 calc R . .
H7A H 0.8562 1.0024 0.6350 0.058 Uiso 1 1 calc R . .
C8 C 0.5317(3) 1.04923(16) 0.60981(15) 0.0487(7) Uani 1 1 d . . .
H8C H 0.4903 1.0490 0.6490 0.058 Uiso 1 1 calc R . .
H8B H 0.4774 1.0588 0.5714 0.058 Uiso 1 1 calc R . .
H8A H 0.5933 1.0908 0.6239 0.058 Uiso 1 1 calc R . .
C9 C 0.3858(2) 0.89132(19) 0.55654(16) 0.0522(7) Uani 1 1 d . . .
H9C H 0.3586 0.8361 0.5400 0.063 Uiso 1 1 calc R . .
H9B H 0.3513 0.9207 0.5239 0.063 Uiso 1 1 calc R . .
H9A H 0.3628 0.9132 0.6022 0.063 Uiso 1 1 calc R . .
C10 C 0.5536(3) 0.75341(16) 0.50818(14) 0.0486(7) Uani 1 1 d . . .
H10A H 0.6036 0.7200 0.5308 0.058 Uiso 1 1 calc R . .
H10B H 0.5631 0.7427 0.4591 0.058 Uiso 1 1 calc R . .
H10C H 0.4725 0.7423 0.5122 0.058 Uiso 1 1 calc R . .
C11 C 0.56553(18) 0.70949(12) 0.68971(11) 0.0239(4) Uani 1 1 d . . .
H11A H 0.4934 0.6951 0.7056 0.029 Uiso 1 1 calc R . .
H11B H 0.5445 0.7402 0.6551 0.029 Uiso 1 1 calc R . .
C12 C 0.62242(18) 0.63503(13) 0.65589(12) 0.0286(5) Uani 1 1 d . . .
H12A H 0.5843 0.6157 0.6075 0.034 Uiso 1 1 calc R . .
H12B H 0.6093 0.5942 0.6806 0.034 Uiso 1 1 calc R . .
C13 C 1.12060(19) 0.88510(12) 0.73976(11) 0.0270(4) Uani 1 1 d . . .
H13A H 1.2059 0.8854 0.7413 0.032 Uiso 1 1 calc R . .
H13B H 1.0894 0.9205 0.7111 0.032 Uiso 1 1 calc R . .
C14 C 1.08967(18) 0.91312(13) 0.81296(11) 0.0272(5) Uani 1 1 d . . .
H14A H 1.1186 0.9682 0.8332 0.033 Uiso 1 1 calc R . .
H14B H 1.1267 0.8804 0.8426 0.033 Uiso 1 1 calc R . .
C15 C 0.56843(17) 0.85196(12) 0.79120(11) 0.0220(4) Uani 1 1 d . . .
C16 C 0.51747(19) 0.89002(12) 0.74210(12) 0.0270(4) Uani 1 1 d . . .
H16A H 0.5326 0.8737 0.6956 0.032 Uiso 1 1 calc R . .
C17 C 0.4452(2) 0.95126(13) 0.76044(12) 0.0317(5) Uani 1 1 d . . .
H17A H 0.4108 0.9763 0.7264 0.038 Uiso 1 1 calc R . .
C18 C 0.4228(2) 0.97614(13) 0.82820(13) 0.0335(5) Uani 1 1 d . . .
H18A H 0.3736 1.0183 0.8408 0.040 Uiso 1 1 calc R . .
C19 C 0.4726(2) 0.93921(14) 0.87692(13) 0.0366(5) Uani 1 1 d . . .
H19A H 0.4577 0.9562 0.9234 0.044 Uiso 1 1 calc R . .
C20 C 0.5444(2) 0.87726(13) 0.85891(11) 0.0289(5) Uani 1 1 d . . .
H20A H 0.5775 0.8520 0.8931 0.035 Uiso 1 1 calc R . .
C21 C 0.65601(18) 0.71958(12) 0.83319(10) 0.0225(4) Uani 1 1 d . . .
C22 C 0.5833(2) 0.65360(13) 0.82502(12) 0.0288(5) Uani 1 1 d . . .
H22A H 0.5347 0.6331 0.7823 0.035 Uiso 1 1 calc R . .
C23 C 0.5815(2) 0.61747(15) 0.87915(14) 0.0392(6) Uani 1 1 d . . .
H23A H 0.5329 0.5718 0.8728 0.047 Uiso 1 1 calc R . .
C24 C 0.6495(2) 0.64734(16) 0.94171(14) 0.0423(6) Uani 1 1 d . . .
H24A H 0.6471 0.6228 0.9786 0.051 Uiso 1 1 calc R . .
C25 C 0.7214(2) 0.71298(15) 0.95082(12) 0.0366(5) Uani 1 1 d . . .
H25A H 0.7679 0.7340 0.9942 0.044 Uiso 1 1 calc R . .
C26 C 0.72587(19) 0.74837(13) 0.89690(11) 0.0272(5) Uani 1 1 d . . .
H26A H 0.7771 0.7928 0.9033 0.033 Uiso 1 1 calc R . .
C27 C 0.7893(2) 0.61401(13) 0.56238(11) 0.0279(5) Uani 1 1 d . . .
C28 C 0.8524(2) 0.65583(14) 0.52821(12) 0.0335(5) Uani 1 1 d . . .
H28A H 0.8959 0.7023 0.5536 0.040 Uiso 1 1 calc R . .
C29 C 0.8524(2) 0.63042(16) 0.45688(13) 0.0422(6) Uani 1 1 d . . .
H29A H 0.8953 0.6598 0.4340 0.051 Uiso 1 1 calc R . .
C30 C 0.7905(2) 0.56278(16) 0.41955(13) 0.0441(6) Uani 1 1 d . . .
H30A H 0.7906 0.5455 0.3710 0.053 Uiso 1 1 calc R . .
C31 C 0.7281(2) 0.52012(15) 0.45291(13) 0.0405(6) Uani 1 1 d . . .
H31A H 0.6855 0.4734 0.4272 0.049 Uiso 1 1 calc R . .
C32 C 0.7274(2) 0.54503(13) 0.52379(12) 0.0341(5) Uani 1 1 d . . .
H32A H 0.6845 0.5151 0.5463 0.041 Uiso 1 1 calc R . .
C33 C 0.83322(19) 0.56142(12) 0.68506(11) 0.0272(5) Uani 1 1 d . . .
C34 C 0.8030(2) 0.54895(14) 0.74647(13) 0.0372(6) Uani 1 1 d . . .
H34A H 0.7562 0.5854 0.7724 0.045 Uiso 1 1 calc R . .
C35 C 0.8394(3) 0.48489(16) 0.77042(15) 0.0490(7) Uani 1 1 d . . .
H35A H 0.8162 0.4770 0.8118 0.059 Uiso 1 1 calc R . .
C36 C 0.9097(3) 0.43215(16) 0.73413(16) 0.0495(7) Uani 1 1 d . . .
H36A H 0.9356 0.3883 0.7506 0.059 Uiso 1 1 calc R . .
C37 C 0.9418(2) 0.44398(15) 0.67389(15) 0.0442(6) Uani 1 1 d . . .
H37A H 0.9904 0.4080 0.6490 0.053 Uiso 1 1 calc R . .
C38 C 0.9044(2) 0.50741(13) 0.64907(12) 0.0323(5) Uani 1 1 d . . .
H38A H 0.9271 0.5144 0.6073 0.039 Uiso 1 1 calc R . .
C39 C 1.15531(18) 0.72549(13) 0.74589(11) 0.0259(4) Uani 1 1 d . . .
C40 C 1.25252(19) 0.75659(14) 0.79358(12) 0.0330(5) Uani 1 1 d . . .
H40A H 1.2760 0.8103 0.8012 0.040 Uiso 1 1 calc R . .
C41 C 1.3152(2) 0.70963(16) 0.82997(14) 0.0443(6) Uani 1 1 d . . .
H41A H 1.3802 0.7317 0.8633 0.053 Uiso 1 1 calc R . .
C42 C 1.2837(2) 0.63079(16) 0.81807(15) 0.0454(6) Uani 1 1 d . . .
H42A H 1.3266 0.5989 0.8434 0.054 Uiso 1 1 calc R . .
C43 C 1.1892(2) 0.59864(15) 0.76905(14) 0.0405(6) Uani 1 1 d . . .
H43A H 1.1686 0.5443 0.7597 0.049 Uiso 1 1 calc R . .
C44 C 1.1252(2) 0.64572(14) 0.73390(13) 0.0328(5) Uani 1 1 d . . .
H44A H 1.0596 0.6235 0.7011 0.039 Uiso 1 1 calc R . .
C45 C 1.10148(18) 0.76495(13) 0.61518(11) 0.0275(5) Uani 1 1 d . . .
C46 C 1.0757(2) 0.81822(14) 0.57507(12) 0.0317(5) Uani 1 1 d . . .
H46A H 1.0383 0.8647 0.5935 0.038 Uiso 1 1 calc R . .
C47 C 1.1040(2) 0.80432(16) 0.50841(13) 0.0390(6) Uani 1 1 d . . .
H47A H 1.0862 0.8413 0.4817 0.047 Uiso 1 1 calc R . .
C48 C 1.1580(2) 0.73682(18) 0.48100(13) 0.0452(7) Uani 1 1 d . . .
H48A H 1.1763 0.7269 0.4352 0.054 Uiso 1 1 calc R . .
C49 C 1.1849(3) 0.68433(19) 0.52016(14) 0.0520(7) Uani 1 1 d . . .
H49A H 1.2227 0.6381 0.5015 0.062 Uiso 1 1 calc R . .
C50 C 1.1574(2) 0.69811(16) 0.58703(13) 0.0423(6) Uani 1 1 d . . .
H50A H 1.1772 0.6613 0.6138 0.051 Uiso 1 1 calc R . .
C51 C 0.9152(2) 0.91653(13) 0.90130(11) 0.0302(5) Uani 1 1 d . . .
C52 C 0.8223(2) 0.95485(15) 0.92911(13) 0.0408(6) Uani 1 1 d . . .
H52A H 0.7736 0.9834 0.9032 0.049 Uiso 1 1 calc R . .
C53 C 0.8001(3) 0.95166(17) 0.99464(15) 0.0543(8) Uani 1 1 d . . .
H53A H 0.7361 0.9778 1.0128 0.065 Uiso 1 1 calc R . .
C54 C 0.8695(3) 0.91134(19) 1.03337(14) 0.0585(9) Uani 1 1 d . . .
H54A H 0.8518 0.9075 1.0772 0.070 Uiso 1 1 calc R . .
C55 C 0.9652(3) 0.87640(19) 1.00808(14) 0.0543(8) Uani 1 1 d . . .
H55A H 1.0159 0.8507 1.0356 0.065 Uiso 1 1 calc R . .
C56 C 0.9878(2) 0.87857(16) 0.94234(12) 0.0403(6) Uani 1 1 d . . .
H56A H 1.0536 0.8538 0.9253 0.048 Uiso 1 1 calc R . .
C57 C 0.88493(19) 1.00063(12) 0.79479(11) 0.0256(4) Uani 1 1 d . . .
C58 C 0.9627(2) 1.06228(13) 0.79643(12) 0.0318(5) Uani 1 1 d . . .
H58A H 1.0436 1.0547 0.8018 0.038 Uiso 1 1 calc R . .
C59 C 0.9228(2) 1.13480(14) 0.79021(14) 0.0410(6) Uani 1 1 d . . .
H59A H 0.9766 1.1762 0.7912 0.049 Uiso 1 1 calc R . .
C60 C 0.8051(3) 1.14701(15) 0.78255(15) 0.0445(6) Uani 1 1 d . . .
H60A H 0.7782 1.1969 0.7796 0.053 Uiso 1 1 calc R . .
C61 C 0.7273(2) 1.08584(15) 0.77918(15) 0.0439(6) Uani 1 1 d . . .
H61A H 0.6464 1.0935 0.7734 0.053 Uiso 1 1 calc R . .
C62 C 0.7669(2) 1.01370(14) 0.78425(14) 0.0370(5) Uani 1 1 d . . .
H62A H 0.7123 0.9718 0.7805 0.044 Uiso 1 1 calc R . .
C63 C 0.9606(2) 0.69527(14) 0.84809(12) 0.0338(5) Uani 1 1 d . . .
C64 C 1.0086(3) 0.6575(2) 0.90201(16) 0.0582(8) Uani 1 1 d . . .
H64A H 1.0812 0.6854 0.9266 0.087 Uiso 1 1 calc R . .
H64B H 1.0238 0.6029 0.8808 0.087 Uiso 1 1 calc R . .
H64C H 0.9531 0.6587 0.9347 0.087 Uiso 1 1 calc R . .
C65 C 0.54889(19) 0.66351(12) 0.24025(11) 0.0248(4) Uani 1 1 d . . .
C66 C 0.5679(2) 0.59347(13) 0.25873(11) 0.0301(5) Uani 1 1 d . . .
C67 C 0.5127(2) 0.56930(14) 0.30743(12) 0.0370(6) Uani 1 1 d . . .
C68 C 0.4350(2) 0.61602(17) 0.34089(13) 0.0429(6) Uani 1 1 d . . .
C69 C 0.4137(2) 0.68666(16) 0.32600(13) 0.0391(6) Uani 1 1 d . . .
C70 C 0.4711(2) 0.70909(13) 0.27764(12) 0.0302(5) Uani 1 1 d . . .
C71 C 0.71144(18) 0.76277(12) 0.24213(11) 0.0240(4) Uani 1 1 d . . .
C72 C 0.70372(19) 0.84346(12) 0.26238(11) 0.0259(4) Uani 1 1 d . . .
C73 C 0.7843(2) 0.89340(13) 0.31093(12) 0.0308(5) Uani 1 1 d . . .
C74 C 0.8778(2) 0.86344(14) 0.34295(12) 0.0328(5) Uani 1 1 d . . .
C75 C 0.8889(2) 0.78383(14) 0.32609(12) 0.0335(5) Uani 1 1 d . . .
C76 C 0.8065(2) 0.73619(13) 0.27863(12) 0.0296(5) Uani 1 1 d . . .
C77 C 0.68241(19) 0.63195(12) 0.13292(11) 0.0258(4) Uani 1 1 d . . .
C78 C 0.7934(2) 0.63868(15) 0.11663(13) 0.0368(5) Uani 1 1 d . . .
C79 C 0.8429(2) 0.57921(18) 0.07155(15) 0.0487(7) Uani 1 1 d . . .
C80 C 0.7818(3) 0.51051(16) 0.04017(14) 0.0465(7) Uani 1 1 d . . .
C81 C 0.6705(2) 0.50154(14) 0.05282(12) 0.0363(5) Uani 1 1 d . . .
C82 C 0.6234(2) 0.56204(13) 0.09694(11) 0.0283(5) Uani 1 1 d . . .
C83 C 0.5283(2) 0.73738(12) 0.13316(11) 0.0270(5) Uani 1 1 d . . .
C84 C 0.4105(2) 0.71989(14) 0.11432(12) 0.0330(5) Uani 1 1 d . . .
C85 C 0.3406(2) 0.75208(16) 0.06765(13) 0.0431(6) Uani 1 1 d . . .
C86 C 0.3887(3) 0.80429(16) 0.03738(13) 0.0464(7) Uani 1 1 d . . .
C87 C 0.5054(3) 0.82225(15) 0.05272(12) 0.0412(6) Uani 1 1 d . . .
C88 C 0.5722(2) 0.78869(13) 0.09894(11) 0.0325(5) Uani 1 1 d . . .
B B 0.6173(2) 0.69906(14) 0.18644(12) 0.0239(5) Uani 1 1 d . . .
F1 F 0.64410(13) 0.54277(8) 0.22952(7) 0.0383(3) Uani 1 1 d . . .
F2 F 0.53703(15) 0.49953(9) 0.32132(8) 0.0520(4) Uani 1 1 d . . .
F3 F 0.38097(17) 0.59331(12) 0.38850(9) 0.0660(5) Uani 1 1 d . . .
F4 F 0.33821(15) 0.73466(11) 0.35842(9) 0.0609(5) Uani 1 1 d . . .
F5 F 0.44799(12) 0.78045(8) 0.26691(7) 0.0390(3) Uani 1 1 d . . .
F6 F 0.61352(12) 0.87858(7) 0.23466(7) 0.0342(3) Uani 1 1 d . . .
F7 F 0.77078(14) 0.97136(8) 0.32731(8) 0.0461(4) Uani 1 1 d . . .
F8 F 0.95604(13) 0.91132(9) 0.39038(8) 0.0485(4) Uani 1 1 d . . .
F9 F 0.98080(14) 0.75258(9) 0.35636(9) 0.0525(4) Uani 1 1 d . . .
F10 F 0.82315(13) 0.65825(8) 0.26650(8) 0.0433(4) Uani 1 1 d . . .
F11 F 0.86164(13) 0.70441(9) 0.14436(8) 0.0500(4) Uani 1 1 d . . .
F12 F 0.95145(16) 0.59102(13) 0.05839(12) 0.0822(7) Uani 1 1 d . . .
F13 F 0.82922(18) 0.45280(11) -0.00267(10) 0.0743(6) Uani 1 1 d . . .
F14 F 0.60814(16) 0.43414(8) 0.02250(8) 0.0498(4) Uani 1 1 d . . .
F15 F 0.51240(12) 0.54991(8) 0.10556(7) 0.0351(3) Uani 1 1 d . . .
F16 F 0.35467(12) 0.66982(9) 0.14167(8) 0.0425(3) Uani 1 1 d . . .
F17 F 0.22629(15) 0.73273(11) 0.05267(10) 0.0636(5) Uani 1 1 d . . .
F18 F 0.32216(18) 0.83682(12) -0.00736(9) 0.0716(6) Uani 1 1 d . . .
F19 F 0.55475(17) 0.87330(10) 0.02327(8) 0.0580(5) Uani 1 1 d . . .
F20 F 0.68678(13) 0.80878(9) 0.11069(7) 0.0416(3) Uani 1 1 d . . .
Ge Ge 0.779447(18) 0.834645(12) 0.637765(11) 0.02176(5) Uani 1 1 d . . .
N N 0.92365(16) 0.72519(10) 0.80618(9) 0.0255(4) Uani 1 1 d . . .
P1 P 0.66334(4) 0.77048(3) 0.76419(3) 0.01955(10) Uani 1 1 d . . .
P2 P 0.78252(5) 0.64900(3) 0.65588(3) 0.02245(11) Uani 1 1 d . . .
P3 P 1.05701(5) 0.78445(3) 0.70189(3) 0.02225(11) Uani 1 1 d . . .
P4 P 0.93040(5) 0.90577(3) 0.80939(3) 0.02200(11) Uani 1 1 d . . .
W W 0.854273(7) 0.780353(4) 0.726553(4) 0.01764(3) Uani 1 1 d . . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
C1 C5 1.500(3) . ?
C1 C2 1.502(3) . ?
C1 C6 1.530(3) . ?
C1 Ge 2.004(2) . ?
C2 C3 1.355(3) . ?
C2 C7 1.499(3) . ?
C3 C4 1.461(3) . ?
C3 C8 1.499(4) . ?
C4 C5 1.355(3) . ?
C4 C9 1.503(3) . ?
C5 C10 1.497(4) . ?
C6 H6C 0.9800 . ?
C6 H6B 0.9800 . ?
C6 H6A 0.9800 . ?
C7 H7C 0.9800 . ?
C7 H7B 0.9800 . ?
C7 H7A 0.9800 . ?
C8 H8C 0.9800 . ?
C8 H8B 0.9800 . ?
C8 H8A 0.9800 . ?
C9 H9C 0.9800 . ?
C9 H9B 0.9800 . ?
C9 H9A 0.9800 . ?
C10 H10A 0.9800 . ?
C10 H10B 0.9800 . ?
C10 H10C 0.9800 . ?
C11 C12 1.526(3) . ?
C11 P1 1.849(2) . ?
C11 H11A 0.9900 . ?
C11 H11B 0.9900 . ?
C12 P2 1.879(2) . ?
C12 H12A 0.9900 . ?
C12 H12B 0.9900 . ?
C13 C14 1.528(3) . ?
C13 P3 1.850(2) . ?
C13 H13A 0.9900 . ?
C13 H13B 0.9900 . ?
C14 P4 1.850(2) . ?
C14 H14A 0.9900 . ?
C14 H14B 0.9900 . ?
C15 C20 1.393(3) . ?
C15 C16 1.398(3) . ?
C15 P1 1.844(2) . ?
C16 C17 1.386(3) . ?
C16 H16A 0.9500 . ?
C17 C18 1.388(3) . ?
C17 H17A 0.9500 . ?
C18 C19 1.374(3) . ?
C18 H18A 0.9500 . ?
C19 C20 1.391(3) . ?
C19 H19A 0.9500 . ?
C20 H20A 0.9500 . ?
C21 C22 1.392(3) . ?
C21 C26 1.397(3) . ?
C21 P1 1.838(2) . ?
C22 C23 1.392(3) . ?
C22 H22A 0.9500 . ?
C23 C24 1.373(4) . ?
C23 H23A 0.9500 . ?
C24 C25 1.378(4) . ?
C24 H24A 0.9500 . ?
C25 C26 1.383(3) . ?
C25 H25A 0.9500 . ?
C26 H26A 0.9500 . ?
C27 C28 1.387(3) . ?
C27 C32 1.401(3) . ?
C27 P2 1.844(2) . ?
C28 C29 1.395(3) . ?
C28 H28A 0.9500 . ?
C29 C30 1.377(4) . ?
C29 H29A 0.9500 . ?
C30 C31 1.380(4) . ?
C30 H30A 0.9500 . ?
C31 C32 1.387(3) . ?
C31 H31A 0.9500 . ?
C32 H32A 0.9500 . ?
C33 C34 1.396(3) . ?
C33 C38 1.400(3) . ?
C33 P2 1.856(2) . ?
C34 C35 1.381(3) . ?
C34 H34A 0.9500 . ?
C35 C36 1.384(4) . ?
C35 H35A 0.9500 . ?
C36 C37 1.377(4) . ?
C36 H36A 0.9500 . ?
C37 C38 1.383(3) . ?
C37 H37A 0.9500 . ?
C38 H38A 0.9500 . ?
C39 C40 1.392(3) . ?
C39 C44 1.397(3) . ?
C39 P3 1.839(2) . ?
C40 C41 1.386(3) . ?
C40 H40A 0.9500 . ?
C41 C42 1.385(4) . ?
C41 H41A 0.9500 . ?
C42 C43 1.387(4) . ?
C42 H42A 0.9500 . ?
C43 C44 1.380(3) . ?
C43 H43A 0.9500 . ?
C44 H44A 0.9500 . ?
C45 C50 1.387(3) . ?
C45 C46 1.391(3) . ?
C45 P3 1.840(2) . ?
C46 C47 1.388(3) . ?
C46 H46A 0.9500 . ?
C47 C48 1.380(4) . ?
C47 H47A 0.9500 . ?
C48 C49 1.368(4) . ?
C48 H48A 0.9500 . ?
C49 C50 1.389(4) . ?
C49 H49A 0.9500 . ?
C50 H50A 0.9500 . ?
C51 C52 1.393(4) . ?
C51 C56 1.393(4) . ?
C51 P4 1.845(2) . ?
C52 C53 1.391(4) . ?
C52 H52A 0.9500 . ?
C53 C54 1.371(5) . ?
C53 H53A 0.9500 . ?
C54 C55 1.377(5) . ?
C54 H54A 0.9500 . ?
C55 C56 1.393(4) . ?
C55 H55A 0.9500 . ?
C56 H56A 0.9500 . ?
C57 C62 1.394(3) . ?
C57 C58 1.396(3) . ?
C57 P4 1.838(2) . ?
C58 C59 1.393(3) . ?
C58 H58A 0.9500 . ?
C59 C60 1.384(4) . ?
C59 H59A 0.9500 . ?
C60 C61 1.381(4) . ?
C60 H60A 0.9500 . ?
C61 C62 1.379(3) . ?
C61 H61A 0.9500 . ?
C62 H62A 0.9500 . ?
C63 N 1.140(3) . ?
C63 C64 1.461(3) . ?
C64 H64A 0.9800 . ?
C64 H64B 0.9800 . ?
C64 H64C 0.9800 . ?
C65 C66 1.385(3) . ?
C65 C70 1.393(3) . ?
C65 B 1.658(3) . ?
C66 F1 1.355(3) . ?
C66 C67 1.386(3) . ?
C67 F2 1.350(3) . ?
C67 C68 1.365(4) . ?
C68 F3 1.348(3) . ?
C68 C69 1.367(4) . ?
C69 F4 1.349(3) . ?
C69 C70 1.381(3) . ?
C70 F5 1.350(3) . ?
C71 C72 1.386(3) . ?
C71 C76 1.396(3) . ?
C71 B 1.655(3) . ?
C72 F6 1.352(2) . ?
C72 C73 1.385(3) . ?
C73 F7 1.347(3) . ?
C73 C74 1.369(3) . ?
C74 F8 1.343(3) . ?
C74 C75 1.371(3) . ?
C75 F9 1.351(3) . ?
C75 C76 1.370(3) . ?
C76 F10 1.355(3) . ?
C77 C82 1.386(3) . ?
C77 C78 1.387(3) . ?
C77 B 1.659(3) . ?
C78 F11 1.350(3) . ?
C78 C79 1.394(4) . ?
C79 F12 1.350(3) . ?
C79 C80 1.361(4) . ?
C80 F13 1.340(3) . ?
C80 C81 1.370(4) . ?
C81 F14 1.346(3) . ?
C81 C82 1.381(3) . ?
C82 F15 1.349(3) . ?
C83 C84 1.384(3) . ?
C83 C88 1.392(3) . ?
C83 B 1.659(3) . ?
C84 F16 1.350(3) . ?
C84 C85 1.390(3) . ?
C85 F17 1.346(3) . ?
C85 C86 1.372(4) . ?
C86 F18 1.347(3) . ?
C86 C87 1.368(4) . ?
C87 F19 1.352(3) . ?
C87 C88 1.381(3) . ?
C88 F20 1.351(3) . ?
Ge W 2.3030(8) . ?
N W 2.1440(19) . ?
P1 W 2.4625(9) . ?
P2 W 2.4674(13) . ?
P3 W 2.4827(9) . ?
P4 W 2.4878(14) . ?
