#------------------------------------------------------------------------------
#$Date: 2016-03-21 06:46:16 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178533 $
#$URL: svn://www.crystallography.net/cod/cif/4/06/38/4063837.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4063837
loop_
_publ_author_name
'Arii, Hidekazu'
'Takahashi, Makiko'
'Nanjo, Masato'
'Mochida, Kunio'
_publ_section_title
;
 Polyhedral and Spiro Platinum−Silyl Clusters Bearing Phosphine
 Ligands
;
_journal_issue                   4
_journal_name_full               Organometallics
_journal_page_first              917
_journal_paper_doi               10.1021/om100976v
_journal_volume                  30
_journal_year                    2011
_chemical_formula_sum            'C132 H130 P8 Pt4 Si2'
_chemical_formula_weight         2800.66
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           85
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_Hall  '-P 4a'
_symmetry_space_group_name_H-M   'P 4/n :2'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   19.3177(17)
_cell_length_b                   19.3177(17)
_cell_length_c                   17.1015(15)
_cell_measurement_reflns_used    9900
_cell_measurement_temperature    123
_cell_measurement_theta_max      28.18
_cell_measurement_theta_min      2.42
_cell_volume                     6381.8(10)
_computing_cell_refinement       'APEX2 (Bruker AXS, 2006)'
_computing_data_collection       'APEX2 (Bruker AXS, 2006)'
_computing_data_reduction        'SAINT (Bruker AXS, 2004)'
_computing_molecular_graphics    'XSHEL (Bruker AXS,2002)'
_computing_publication_material  'XCIF (Bruker AXS, 2001)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      123(2)
_diffrn_detector_area_resol_mean 8.333
_diffrn_measured_fraction_theta_full 0.955
_diffrn_measured_fraction_theta_max 0.955
_diffrn_measurement_device_type  'Bruker APEXII CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  'Bruker Helios multilayer confocal mirror'
_diffrn_radiation_source         'Bruker TXS fine-focus rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0300
_diffrn_reflns_av_sigmaI/netI    0.0264
_diffrn_reflns_limit_h_max       19
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       -24
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            35291
_diffrn_reflns_theta_full        28.30
_diffrn_reflns_theta_max         28.30
_diffrn_reflns_theta_min         1.59
_exptl_absorpt_coefficient_mu    4.535
_exptl_absorpt_correction_T_max  0.4641
_exptl_absorpt_correction_T_min  0.4641
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details
;
SADABS Sheldrick 1996
;
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.457
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             2764
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.20
_exptl_crystal_size_min          0.20
_refine_diff_density_max         5.511
_refine_diff_density_min         -0.912
_refine_diff_density_rms         0.276
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.089
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     336
_refine_ls_number_reflns         7601
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      1.088
_refine_ls_R_factor_all          0.0621
_refine_ls_R_factor_gt           0.0483
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0870P)²+86.5322P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1576
_refine_ls_wR_factor_ref         0.1704
_reflns_number_gt                6095
_reflns_number_total             7601
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om100976v_si_002.cif
_cod_data_source_block           complex5
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Tetragonal' changed to 'tetragonal'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      'P4/n  '
_cod_database_code               4063837
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y+1/2, z'
'-y+1/2, x, z'
'y, -x+1/2, z'
'-x, -y, -z'
'x-1/2, y-1/2, -z'
'y-1/2, -x, -z'
'-y, x-1/2, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pt1 Pt 0.804367(13) 0.844162(13) 0.555522(15) 0.01370(11) Uani 1 1 d .
P1 P 0.86561(9) 0.89684(9) 0.65280(11) 0.0172(3) Uani 1 1 d .
P2 P 0.83908(9) 0.93312(9) 0.47461(11) 0.0169(3) Uani 1 1 d .
Si1 Si 0.7500 0.7500 0.6296(2) 0.0151(7) Uani 1 4 d SD
H1H H 0.7500 0.7500 0.7094(17) -0.030(17) Uiso 1 4 d SD
Si2 Si 0.7500 0.7500 0.4810(2) 0.0142(7) Uani 1 4 d SD
H2H H 0.7500 0.7500 0.4014(18) 0.04(5) Uiso 1 4 d SD
C1 C 0.8894(4) 0.9836(4) 0.6144(4) 0.0205(14) Uani 1 1 d .
H1A H 0.8493 1.0153 0.6180 0.025 Uiso 1 1 calc R
H1B H 0.9279 1.0033 0.6454 0.025 Uiso 1 1 calc R
C2 C 0.9116(4) 0.9748(4) 0.5281(4) 0.0204(14) Uani 1 1 d .
H2A H 0.9536 0.9457 0.5248 0.024 Uiso 1 1 calc R
H2B H 0.9221 1.0206 0.5048 0.024 Uiso 1 1 calc R
C3 C 0.8319(4) 0.9139(4) 0.7509(4) 0.0205(14) Uani 1 1 d .
C4 C 0.8043(4) 0.9777(4) 0.7733(5) 0.0279(16) Uani 1 1 d .
H4 H 0.8036 1.0154 0.7376 0.033 Uiso 1 1 calc R
C5 C 0.7776(5) 0.9856(5) 0.8491(5) 0.0333(19) Uani 1 1 d .
H5 H 0.7577 1.0286 0.8639 0.040 Uiso 1 1 calc R
C6 C 0.7795(4) 0.9324(5) 0.9023(5) 0.0333(19) Uani 1 1 d .
H6 H 0.7617 0.9388 0.9536 0.040 Uiso 1 1 calc R
C7 C 0.8078(4) 0.8690(5) 0.8806(5) 0.0288(17) Uani 1 1 d .
H7 H 0.8099 0.8321 0.9171 0.035 Uiso 1 1 calc R
C8 C 0.8332(4) 0.8599(4) 0.8048(5) 0.0253(16) Uani 1 1 d .
H8 H 0.8517 0.8163 0.7898 0.030 Uiso 1 1 calc R
C9 C 0.9532(4) 0.8649(4) 0.6759(4) 0.0197(14) Uani 1 1 d .
C10 C 0.9900(4) 0.8863(4) 0.7422(5) 0.0228(15) Uani 1 1 d .
H10 H 0.9675 0.9135 0.7809 0.027 Uiso 1 1 calc R
C11 C 1.0588(4) 0.8685(4) 0.7520(5) 0.0267(16) Uani 1 1 d .
H11 H 1.0833 0.8837 0.7970 0.032 Uiso 1 1 calc R
C12 C 1.0920(4) 0.8281(4) 0.6958(5) 0.0289(17) Uani 1 1 d .
H12 H 1.1394 0.8160 0.7023 0.035 Uiso 1 1 calc R
C13 C 1.0559(4) 0.8057(4) 0.6306(5) 0.0272(16) Uani 1 1 d .
H13 H 1.0786 0.7789 0.5918 0.033 Uiso 1 1 calc R
C14 C 0.9857(4) 0.8228(4) 0.6220(5) 0.0224(15) Uani 1 1 d .
H14 H 0.9603 0.8053 0.5786 0.027 Uiso 1 1 calc R
C15 C 0.7831(4) 1.0071(4) 0.4516(4) 0.0199(14) Uani 1 1 d .
C16 C 0.7138(4) 0.9941(4) 0.4339(5) 0.0237(15) Uani 1 1 d .
H16 H 0.6971 0.9478 0.4360 0.028 Uiso 1 1 calc R
C17 C 0.6687(4) 1.0467(5) 0.4134(5) 0.0291(17) Uani 1 1 d .
H17 H 0.6221 1.0362 0.4003 0.035 Uiso 1 1 calc R
C18 C 0.6914(4) 1.1149(4) 0.4118(5) 0.0303(17) Uani 1 1 d .
H18 H 0.6603 1.1512 0.3988 0.036 Uiso 1 1 calc R
C19 C 0.7599(5) 1.1293(4) 0.4296(5) 0.0291(17) Uani 1 1 d .
H19 H 0.7758 1.1759 0.4283 0.035 Uiso 1 1 calc R
C20 C 0.8057(4) 1.0765(4) 0.4493(5) 0.0246(16) Uani 1 1 d .
H20 H 0.8525 1.0873 0.4612 0.030 Uiso 1 1 calc R
C21 C 0.8760(4) 0.9164(4) 0.3773(4) 0.0211(14) Uani 1 1 d .
C22 C 0.8548(4) 0.8559(4) 0.3394(5) 0.0262(16) Uani 1 1 d .
H22 H 0.8216 0.8265 0.3633 0.031 Uiso 1 1 calc R
C23 C 0.8825(5) 0.8387(5) 0.2660(5) 0.0346(19) Uani 1 1 d .
H23 H 0.8690 0.7970 0.2409 0.041 Uiso 1 1 calc R
C24 C 0.9295(5) 0.8827(5) 0.2302(5) 0.037(2) Uani 1 1 d .
H24 H 0.9484 0.8710 0.1807 0.045 Uiso 1 1 calc R
C25 C 0.9488(5) 0.9439(5) 0.2667(5) 0.0341(19) Uani 1 1 d .
H25 H 0.9805 0.9743 0.2417 0.041 Uiso 1 1 calc R
C26 C 0.9224(4) 0.9610(4) 0.3392(5) 0.0280(17) Uani 1 1 d .
H26 H 0.9358 1.0032 0.3635 0.034 Uiso 1 1 calc R
C27 C 0.2700(8) 0.8767(10) 0.8384(9) 0.081(5) Uani 1 1 d .
C28 C 0.2389(10) 0.8648(11) 0.9131(9) 0.088(5) Uani 1 1 d .
H28 H 0.2501 0.8237 0.9408 0.106 Uiso 1 1 calc R
C29 C 0.1961(9) 0.9084(14) 0.9442(9) 0.095(7) Uani 1 1 d .
H29 H 0.1777 0.9001 0.9949 0.114 Uiso 1 1 calc R
C30 C 0.1763(7) 0.9696(10) 0.9011(10) 0.082(5) Uani 1 1 d .
H30 H 0.1449 1.0019 0.9233 0.098 Uiso 1 1 calc R
C31 C 0.2034(6) 0.9811(8) 0.8272(8) 0.062(3) Uani 1 1 d .
H31 H 0.1904 1.0207 0.7978 0.074 Uiso 1 1 calc R
C32 C 0.2502(6) 0.9331(7) 0.7970(7) 0.054(3) Uani 1 1 d .
H32 H 0.2687 0.9402 0.7461 0.065 Uiso 1 1 calc R
C33 C 0.3181(12) 0.8237(13) 0.8026(14) 0.138(10) Uani 1 1 d .
H33A H 0.2997 0.8087 0.7519 0.207 Uiso 1 1 calc R
H33B H 0.3219 0.7836 0.8375 0.207 Uiso 1 1 calc R
H33C H 0.3640 0.8443 0.7951 0.207 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
P1 Pt1 P2 87.38(7) . .
P1 Pt1 Si1 100.15(9) . .
P2 Pt1 Si1 170.78(7) . .
P1 Pt1 Si2 158.49(7) . .
P2 Pt1 Si2 111.40(9) . .
Si1 Pt1 Si2 62.34(11) . .
P1 Pt1 Pt1 128.06(5) . 3_655
P2 Pt1 Pt1 118.28(5) . 3_655
Si1 Pt1 Pt1 52.74(4) . 3_655
Si2 Pt1 Pt1 52.80(3) . 3_655
P1 Pt1 Pt1 107.26(5) . 4_565
P2 Pt1 Pt1 130.13(5) . 4_565
Si1 Pt1 Pt1 52.74(4) . 4_565
Si2 Pt1 Pt1 52.80(3) . 4_565
Pt1 Pt1 Pt1 90.0 3_655 4_565
C3 P1 C9 101.0(3) . .
C3 P1 C1 104.5(3) . .
C9 P1 C1 98.7(3) . .
C3 P1 Pt1 124.4(2) . .
C9 P1 Pt1 118.9(2) . .
C1 P1 Pt1 105.8(2) . .
C15 P2 C21 99.9(3) . .
C15 P2 C2 102.2(3) . .
C21 P2 C2 103.3(3) . .
C15 P2 Pt1 122.6(2) . .
C21 P2 Pt1 121.6(2) . .
C2 P2 Pt1 104.3(2) . .
Pt1 Si1 Pt1 117.80(15) . 2_665
Pt1 Si1 Pt1 74.53(7) . 3_655
Pt1 Si1 Pt1 74.52(7) 2_665 3_655
Pt1 Si1 Pt1 74.53(7) . 4_565
Pt1 Si1 Pt1 74.52(7) 2_665 4_565
Pt1 Si1 Pt1 117.80(15) 3_655 4_565
Pt1 Si1 Si2 58.90(8) . .
Pt1 Si1 Si2 58.90(8) 2_665 .
Pt1 Si1 Si2 58.90(8) 3_655 .
Pt1 Si1 Si2 58.90(8) 4_565 .
Pt1 Si1 H1H 121.10(8) . .
Pt1 Si1 H1H 121.10(8) 2_665 .
Pt1 Si1 H1H 121.10(8) 3_655 .
Pt1 Si1 H1H 121.10(8) 4_565 .
Si2 Si1 H1H 180.000(10) . .
Pt1 Si2 Pt1 74.40(7) 4_565 2_665
Pt1 Si2 Pt1 117.52(15) 4_565 3_655
Pt1 Si2 Pt1 74.40(7) 2_665 3_655
Pt1 Si2 Pt1 74.40(7) 4_565 .
Pt1 Si2 Pt1 117.52(15) 2_665 .
Pt1 Si2 Pt1 74.40(7) 3_655 .
Pt1 Si2 Si1 58.76(7) 4_565 .
Pt1 Si2 Si1 58.76(7) 2_665 .
Pt1 Si2 Si1 58.76(7) 3_655 .
Pt1 Si2 Si1 58.76(7) . .
Pt1 Si2 H2H 121.24(7) 4_565 .
Pt1 Si2 H2H 121.24(7) 2_665 .
Pt1 Si2 H2H 121.24(7) 3_655 .
Pt1 Si2 H2H 121.24(7) . .
Si1 Si2 H2H 180.000(9) . .
C2 C1 P1 107.9(5) . .
C2 C1 H1A 110.1 . .
P1 C1 H1A 110.1 . .
C2 C1 H1B 110.1 . .
P1 C1 H1B 110.1 . .
H1A C1 H1B 108.4 . .
C1 C2 P2 108.0(5) . .
C1 C2 H2A 110.1 . .
P2 C2 H2A 110.1 . .
C1 C2 H2B 110.1 . .
P2 C2 H2B 110.1 . .
H2A C2 H2B 108.4 . .
C8 C3 C4 119.2(7) . .
C8 C3 P1 117.7(6) . .
C4 C3 P1 123.1(6) . .
C3 C4 C5 119.3(8) . .
C3 C4 H4 120.4 . .
C5 C4 H4 120.4 . .
C6 C5 C4 121.4(8) . .
C6 C5 H5 119.3 . .
C4 C5 H5 119.3 . .
C5 C6 C7 119.4(8) . .
C5 C6 H6 120.3 . .
C7 C6 H6 120.3 . .
C6 C7 C8 119.8(8) . .
C6 C7 H7 120.1 . .
C8 C7 H7 120.1 . .
C3 C8 C7 120.8(8) . .
C3 C8 H8 119.6 . .
C7 C8 H8 119.6 . .
C14 C9 C10 118.9(7) . .
C14 C9 P1 118.1(6) . .
C10 C9 P1 122.7(6) . .
C11 C10 C9 120.8(7) . .
C11 C10 H10 119.6 . .
C9 C10 H10 119.6 . .
C10 C11 C12 120.0(7) . .
C10 C11 H11 120.0 . .
C12 C11 H11 120.0 . .
C13 C12 C11 119.8(7) . .
C13 C12 H12 120.1 . .
C11 C12 H12 120.1 . .
C12 C13 C14 119.9(7) . .
C12 C13 H13 120.1 . .
C14 C13 H13 120.1 . .
C9 C14 C13 120.5(7) . .
C9 C14 H14 119.8 . .
C13 C14 H14 119.8 . .
C16 C15 C20 117.5(7) . .
C16 C15 P2 118.1(6) . .
C20 C15 P2 124.4(6) . .
C17 C16 C15 121.7(8) . .
C17 C16 H16 119.1 . .
C15 C16 H16 119.1 . .
C16 C17 C18 120.2(8) . .
C16 C17 H17 119.9 . .
C18 C17 H17 119.9 . .
C19 C18 C17 119.2(8) . .
C19 C18 H18 120.4 . .
C17 C18 H18 120.4 . .
C18 C19 C20 120.8(8) . .
C18 C19 H19 119.6 . .
C20 C19 H19 119.6 . .
C19 C20 C15 120.5(8) . .
C19 C20 H20 119.8 . .
C15 C20 H20 119.8 . .
C22 C21 C26 119.1(7) . .
C22 C21 P2 116.9(6) . .
C26 C21 P2 124.0(6) . .
C21 C22 C23 120.0(7) . .
C21 C22 H22 120.0 . .
C23 C22 H22 120.0 . .
C24 C23 C22 119.9(8) . .
C24 C23 H23 120.0 . .
C22 C23 H23 120.0 . .
C23 C24 C25 120.0(8) . .
C23 C24 H24 120.0 . .
C25 C24 H24 120.0 . .
C26 C25 C24 120.5(8) . .
C26 C25 H25 119.8 . .
C24 C25 H25 119.8 . .
C25 C26 C21 120.4(8) . .
C25 C26 H26 119.8 . .
C21 C26 H26 119.8 . .
C32 C27 C28 118.5(14) . .
C32 C27 C33 120.4(15) . .
C28 C27 C33 120.8(17) . .
C29 C28 C27 122.1(18) . .
C29 C28 H28 118.9 . .
C27 C28 H28 118.9 . .
C28 C29 C30 119.4(15) . .
C28 C29 H29 120.3 . .
C30 C29 H29 120.3 . .
C31 C30 C29 119.8(14) . .
C31 C30 H30 120.1 . .
C29 C30 H30 120.1 . .
C30 C31 C32 118.5(15) . .
C30 C31 H31 120.8 . .
C32 C31 H31 120.8 . .
C27 C32 C31 121.6(13) . .
C27 C32 H32 119.2 . .
C31 C32 H32 119.2 . .
C27 C33 H33A 109.5 . .
C27 C33 H33B 109.5 . .
H33A C33 H33B 109.5 . .
C27 C33 H33C 109.5 . .
H33A C33 H33C 109.5 . .
H33B C33 H33C 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pt1 P1 2.2810(18) .
Pt1 P2 2.3059(18) .
Pt1 Si1 2.453(2) .
Pt1 Si2 2.4567(19) .
Pt1 Pt1 2.9704(4) 3_655
Pt1 Pt1 2.9704(5) 4_565
P1 C3 1.830(7) .
P1 C9 1.844(8) .
P1 C1 1.857(7) .
P2 C15 1.835(8) .
P2 C21 1.840(8) .
P2 C2 1.856(7) .
Si1 Pt1 2.453(2) 2_665
Si1 Pt1 2.453(2) 3_655
Si1 Pt1 2.453(2) 4_565
Si1 Si2 2.541(6) .
Si1 H1H 1.37(3) .
Si2 Pt1 2.4566(19) 4_565
Si2 Pt1 2.4566(19) 2_665
Si2 Pt1 2.4566(19) 3_655
Si2 H2H 1.36(3) .
C1 C2 1.546(10) .
C1 H1A 0.9900 .
C1 H1B 0.9900 .
C2 H2A 0.9900 .
C2 H2B 0.9900 .
C3 C8 1.392(11) .
C3 C4 1.397(11) .
C4 C5 1.403(12) .
C4 H4 0.9500 .
C5 C6 1.373(13) .
C5 H5 0.9500 .
C6 C7 1.391(13) .
C6 H6 0.9500 .
C7 C8 1.397(12) .
C7 H7 0.9500 .
C8 H8 0.9500 .
C9 C14 1.380(10) .
C9 C10 1.402(10) .
C10 C11 1.382(11) .
C10 H10 0.9500 .
C11 C12 1.394(12) .
C11 H11 0.9500 .
C12 C13 1.385(12) .
C12 H12 0.9500 .
C13 C14 1.404(11) .
C13 H13 0.9500 .
C14 H14 0.9500 .
C15 C16 1.397(10) .
C15 C20 1.410(11) .
C16 C17 1.384(11) .
C16 H16 0.9500 .
C17 C18 1.388(12) .
C17 H17 0.9500 .
C18 C19 1.386(13) .
C18 H18 0.9500 .
C19 C20 1.392(11) .
C19 H19 0.9500 .
C20 H20 0.9500 .
C21 C22 1.397(11) .
C21 C26 1.403(11) .
C22 C23 1.405(12) .
C22 H22 0.9500 .
C23 C24 1.387(13) .
C23 H23 0.9500 .
C24 C25 1.389(13) .
C24 H24 0.9500 .
C25 C26 1.380(12) .
C25 H25 0.9500 .
C26 H26 0.9500 .
C27 C32 1.36(2) .
C27 C28 1.43(2) .
C27 C33 1.51(2) .
C28 C29 1.29(3) .
C28 H28 0.9500 .
C29 C30 1.44(3) .
C29 H29 0.9500 .
C30 C31 1.39(2) .
C30 H30 0.9500 .
C31 C32 1.393(17) .
C31 H31 0.9500 .
C32 H32 0.9500 .
C33 H33A 0.9800 .
C33 H33B 0.9800 .
C33 H33C 0.9800 .
