#------------------------------------------------------------------------------
#$Date: 2016-03-21 06:47:46 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178534 $
#$URL: svn://www.crystallography.net/cod/cif/4/06/39/4063908.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4063908
loop_
_publ_author_name
'Cabeza, Javier A.'
'Damonte, Marina'
'García-Álvarez, Pablo'
'Kennedy, Alan R.'
'Pérez-Carreño, Enrique'
_publ_section_title
;
 Reactivity of [Ru3(CO)12] with a Phosphine-Functionalized
 Imidazol-2-ylidene and Its Imidazolium Salt
;
_journal_issue                   4
_journal_name_full               Organometallics
_journal_page_first              826
_journal_paper_doi               10.1021/om101021s
_journal_volume                  30
_journal_year                    2011
_chemical_formula_moiety         'C63 H60 N6 O9 P3 Ru3, 3(B F4)'
_chemical_formula_sum            'C63 H60 B3 F12 N6 O9 P3 Ru3'
_chemical_formula_weight         1701.72
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           165
_symmetry_cell_setting           trigonal
_symmetry_space_group_name_Hall  '-P 3 2"c'
_symmetry_space_group_name_H-M   'P -3 c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            4
_cell_length_a                   14.8250(10)
_cell_length_b                   14.8250(10)
_cell_length_c                   41.080(3)
_cell_measurement_reflns_used    3450
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      73.8146
_cell_measurement_theta_min      3.2247
_cell_volume                     7819.0(9)
_computing_cell_refinement
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.34.36 (release 02-08-2010 CrysAlis171 .NET)
(compiled Aug  2 2010,13:00:58)
;
_computing_data_collection
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.34.36 (release 02-08-2010 CrysAlis171 .NET)
(compiled Aug  2 2010,13:00:58)
;
_computing_data_reduction
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.34.36 (release 02-08-2010 CrysAlis171 .NET)
(compiled Aug  2 2010,13:00:58)
;
_computing_molecular_graphics    'PLATON (Spek, 2008)'
_computing_publication_material  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'DIRDIF-08 (Beurskens et al., 2008)'
_diffrn_ambient_temperature      293(2)
_diffrn_detector_area_resol_mean 8.2640
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Goniometer Xcalibur, detector: Onyx (Nova)'
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_source         'Nova (Cu) X-ray Source'
_diffrn_radiation_type           CuK\a
_diffrn_radiation_wavelength     1.54184
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0497
_diffrn_reflns_limit_h_max       0
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       46
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            3860
_diffrn_reflns_theta_full        60.00
_diffrn_reflns_theta_max         60.00
_diffrn_reflns_theta_min         3.44
_exptl_absorpt_coefficient_mu    5.920
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.14511
_exptl_absorpt_correction_type   refdelf
_exptl_absorpt_process_details
;
Parkin S,Moezzi B & Hope H, (1995) J. Appl. Cryst. 28, 53-56
Cubic fit to sin(theta)/lambda - 24 parameters
;
_exptl_crystal_colour            purple
_exptl_crystal_density_diffrn    1.446
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             3408
_exptl_crystal_size_max          0.090
_exptl_crystal_size_mid          0.065
_exptl_crystal_size_min          0.028
_refine_diff_density_max         1.347
_refine_diff_density_min         -1.026
_refine_diff_density_rms         0.128
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.044
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     316
_refine_ls_number_reflns         3860
_refine_ls_number_restraints     83
_refine_ls_restrained_S_all      1.060
_refine_ls_R_factor_all          0.1186
_refine_ls_R_factor_gt           0.0962
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1636P)²+26.9535P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2796
_refine_ls_wR_factor_ref         0.2964
_reflns_number_gt                2702
_reflns_number_total             3860
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            om101021s_si_002.cif
_cod_data_source_block           md71_(compound_4)
_cod_original_sg_symbol_H-M      P-3c1
_cod_database_code               4063908
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'-x+y, y, z+1/2'
'x, x-y, z+1/2'
'-y, -x, z+1/2'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'x-y, -y, -z-1/2'
'-x, -x+y, -z-1/2'
'y, x, -z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ru1 Ru 0.61774(8) 0.20596(7) 0.39856(3) 0.0822(5) Uani 1 1 d U
P1 P 0.4634(3) 0.0554(3) 0.38284(8) 0.0835(9) Uani 1 1 d .
O100 O 0.5306(10) 0.2110(9) 0.4654(3) 0.115(3) Uani 1 1 d .
O101 O 0.7007(9) 0.2244(9) 0.3294(3) 0.118(3) Uani 1 1 d U
O102 O 0.7133(10) 0.0833(10) 0.4256(3) 0.141(4) Uani 1 1 d .
N1 N 0.5880(10) -0.0798(9) 0.3245(3) 0.097(3) Uani 1 1 d .
N2 N 0.5912(11) -0.1322(10) 0.2754(3) 0.110(4) Uani 1 1 d .
C1 C 0.5378(12) -0.1071(11) 0.2964(4) 0.097(4) Uani 1 1 d .
H1 H 0.4756 -0.1086 0.2919 0.116 Uiso 1 1 calc R
C2 C 0.6810(15) -0.1157(18) 0.2913(5) 0.142(7) Uani 1 1 d .
H2 H 0.7349 -0.1225 0.2823 0.171 Uiso 1 1 calc R
C3 C 0.6757(13) -0.0888(15) 0.3214(5) 0.130(6) Uani 1 1 d .
H3 H 0.7233 -0.0776 0.3378 0.156 Uiso 1 1 calc R
C4 C 0.5545(13) -0.0510(13) 0.3543(3) 0.105(4) Uani 1 1 d .
H4A H 0.6151 0.0022 0.3657 0.125 Uiso 1 1 calc R
H4B H 0.5199 -0.1113 0.3684 0.125 Uiso 1 1 calc R
C5 C 0.4814(11) -0.0107(11) 0.3472(3) 0.088(3) Uani 1 1 d .
H5A H 0.4143 -0.0684 0.3407 0.105 Uiso 1 1 calc R
H5B H 0.5086 0.0379 0.3291 0.105 Uiso 1 1 calc R
C6 C 0.5595(17) -0.1682(15) 0.2422(4) 0.131(6) Uani 1 1 d .
H6A H 0.5104 -0.2416 0.2423 0.196 Uiso 1 1 calc R
H6B H 0.6195 -0.1551 0.2296 0.196 Uiso 1 1 calc R
H6C H 0.5278 -0.1317 0.2327 0.196 Uiso 1 1 calc R
C7 C 0.3506(10) 0.0631(10) 0.3698(4) 0.089(3) Uani 1 1 d .
C8 C 0.3243(12) 0.0661(11) 0.3385(4) 0.105(4) Uani 1 1 d .
H8 H 0.3671 0.0646 0.3222 0.126 Uiso 1 1 calc R
C9 C 0.2362(14) 0.0712(14) 0.3293(5) 0.120(5) Uani 1 1 d .
H9 H 0.2215 0.0742 0.3075 0.144 Uiso 1 1 calc R
C10 C 0.1741(14) 0.0718(15) 0.3524(7) 0.128(6) Uani 1 1 d .
H10 H 0.1137 0.0724 0.3467 0.153 Uiso 1 1 calc R
C11 C 0.1959(17) 0.072(2) 0.3818(7) 0.155(8) Uani 1 1 d .
H11 H 0.1521 0.0745 0.3975 0.185 Uiso 1 1 calc R
C12 C 0.2875(14) 0.0671(14) 0.3924(5) 0.120(5) Uani 1 1 d .
H12 H 0.3019 0.0671 0.4145 0.144 Uiso 1 1 calc R
C13 C 0.4073(11) -0.0480(11) 0.4133(3) 0.090(3) Uani 1 1 d .
C14 C 0.3203(16) -0.1427(14) 0.4048(4) 0.131(6) Uani 1 1 d .
H14 H 0.2948 -0.1519 0.3836 0.158 Uiso 1 1 calc R
C15 C 0.2722(15) -0.2212(14) 0.4263(5) 0.132(6) Uani 1 1 d .
H15 H 0.2155 -0.2844 0.4199 0.158 Uiso 1 1 calc R
C16 C 0.3093(17) -0.2058(15) 0.4586(4) 0.127(6) Uani 1 1 d .
H16 H 0.2757 -0.2580 0.4740 0.152 Uiso 1 1 calc R
C17 C 0.3905(16) -0.1182(15) 0.4665(4) 0.128(6) Uani 1 1 d .
H17 H 0.4141 -0.1082 0.4879 0.154 Uiso 1 1 calc R
C18 C 0.4430(14) -0.0397(13) 0.4443(4) 0.105(4) Uani 1 1 d .
H18 H 0.5038 0.0200 0.4505 0.126 Uiso 1 1 calc R
C100 C 0.5616(11) 0.2164(11) 0.4393(4) 0.092(4) Uani 1 1 d .
C101 C 0.6749(12) 0.2265(12) 0.3556(4) 0.103(4) Uani 1 1 d U
C102 C 0.6791(11) 0.1348(12) 0.4148(4) 0.100(4) Uani 1 1 d .
B1 B 0.3333 0.6667 0.3236(5) 0.111(7) Uani 1 3 d SDU
B2 B 0.3947(6) 0.0000 0.2500 0.127(6) Uani 1 2 d SDU
B3 B 1.0000 0.0000 0.2500 0.138(19) Uiso 1 6 d SD
F1 F 0.3333 0.6667 0.2910(4) 0.157(7) Uani 1 3 d SDU
F2 F 0.4274(7) 0.6859(9) 0.3336(3) 0.152(4) Uani 1 1 d DU
F3 F 0.3106 0.0079 0.2568 0.161(7) Uani 0.50 1 d PDU
F4 F 0.4369(13) 0.0723(15) 0.2240(4) 0.138(6) Uani 0.50 1 d PDU
F5 F 0.4702(15) 0.0475(17) 0.2726(5) 0.139(8) Uani 0.50 1 d PDU
F6 F 0.392(2) -0.0801(16) 0.2355(7) 0.149(8) Uani 0.50 1 d PDU
F7 F 0.913(4) -0.003(7) 0.2391(5) 0.150 Uiso 0.17 1 d PD
F8 F 1.0000 0.0000 0.2827(2) 0.150 Uiso 0.50 3 d SPD
F9 F 0.998(3) 0.064(2) 0.2274(12) 0.150 Uiso 0.17 1 d PD
F10 F 0.9095(7) -0.0905(7) 0.2500 0.150 Uiso 0.33 2 d SPD
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ru Ru 0.0552 3.2960 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.2955 0.4335 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0727 0.0534 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0090 0.0039 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C102 Ru1 C100 95.2(7) . .
C102 Ru1 C101 96.8(7) . .
C100 Ru1 C101 166.1(6) . .
C102 Ru1 P1 94.6(5) . .
C100 Ru1 P1 93.5(4) . .
C101 Ru1 P1 92.3(5) . .
C102 Ru1 Ru1 99.4(5) . 2_655
C100 Ru1 Ru1 96.7(4) . 2_655
C101 Ru1 Ru1 74.6(5) . 2_655
P1 Ru1 Ru1 161.82(9) . 2_655
C102 Ru1 Ru1 151.1(5) . 3_665
C100 Ru1 Ru1 69.7(4) . 3_665
C101 Ru1 Ru1 96.5(5) . 3_665
P1 Ru1 Ru1 110.29(10) . 3_665
Ru1 Ru1 Ru1 60.0 2_655 3_665
C7 P1 C13 102.0(7) . .
C7 P1 C5 100.4(6) . .
C13 P1 C5 102.9(6) . .
C7 P1 Ru1 120.8(4) . .
C13 P1 Ru1 115.3(5) . .
C5 P1 Ru1 112.9(5) . .
C1 N1 C3 107.7(13) . .
C1 N1 C4 126.8(12) . .
C3 N1 C4 125.5(14) . .
C1 N2 C2 107.2(14) . .
C1 N2 C6 125.2(15) . .
C2 N2 C6 127.6(15) . .
N1 C1 N2 109.0(14) . .
N1 C1 H1 125.5 . .
N2 C1 H1 125.5 . .
C3 C2 N2 107.3(15) . .
C3 C2 H2 126.3 . .
N2 C2 H2 126.3 . .
C2 C3 N1 108.6(16) . .
C2 C3 H3 125.7 . .
N1 C3 H3 125.7 . .
N1 C4 C5 111.8(12) . .
N1 C4 H4A 109.3 . .
C5 C4 H4A 109.3 . .
N1 C4 H4B 109.3 . .
C5 C4 H4B 109.3 . .
H4A C4 H4B 107.9 . .
C4 C5 P1 112.3(9) . .
C4 C5 H5A 109.1 . .
P1 C5 H5A 109.1 . .
C4 C5 H5B 109.1 . .
P1 C5 H5B 109.1 . .
H5A C5 H5B 107.9 . .
N2 C6 H6A 109.5 . .
N2 C6 H6B 109.5 . .
H6A C6 H6B 109.5 . .
N2 C6 H6C 109.5 . .
H6A C6 H6C 109.5 . .
H6B C6 H6C 109.5 . .
C12 C7 C8 116.1(15) . .
C12 C7 P1 118.9(12) . .
C8 C7 P1 125.1(12) . .
C7 C8 C9 123.5(16) . .
C7 C8 H8 118.3 . .
C9 C8 H8 118.3 . .
C10 C9 C8 118.6(18) . .
C10 C9 H9 120.7 . .
C8 C9 H9 120.7 . .
C11 C10 C9 120.6(19) . .
C11 C10 H10 119.7 . .
C9 C10 H10 119.7 . .
C10 C11 C12 122(2) . .
C10 C11 H11 118.8 . .
C12 C11 H11 118.8 . .
C7 C12 C11 118.7(18) . .
C7 C12 H12 120.6 . .
C11 C12 H12 120.6 . .
C18 C13 C14 116.6(14) . .
C18 C13 P1 124.9(12) . .
C14 C13 P1 118.5(12) . .
C15 C14 C13 121.9(17) . .
C15 C14 H14 119.0 . .
C13 C14 H14 119.0 . .
C14 C15 C16 118.8(17) . .
C14 C15 H15 120.6 . .
C16 C15 H15 120.6 . .
C17 C16 C15 119.3(16) . .
C17 C16 H16 120.3 . .
C15 C16 H16 120.3 . .
C16 C17 C18 122.1(17) . .
C16 C17 H17 118.9 . .
C18 C17 H17 118.9 . .
C13 C18 C17 121.0(17) . .
C13 C18 H18 119.5 . .
C17 C18 H18 119.5 . .
O100 C100 Ru1 169.6(13) . .
O101 C101 Ru1 170.7(15) . .
O102 C102 Ru1 176.1(14) . .
F2 B1 F2 111.1(8) 2_665 3_565
F2 B1 F2 111.1(8) 2_665 .
F2 B1 F2 111.1(8) 3_565 .
F2 B1 F1 107.8(9) 2_665 .
F2 B1 F1 107.8(9) 3_565 .
F2 B1 F1 107.8(9) . .
F6 B2 F6 130(2) 10_556 .
F6 B2 F3 124.5(12) 10_556 10_556
F6 B2 F3 105.1(13) . 10_556
F6 B2 F3 105.1(13) 10_556 .
F6 B2 F3 124.5(12) . .
F3 B2 F3 25.57(18) 10_556 .
F6 B2 F5 115.2(12) 10_556 10_556
F6 B2 F5 24.9(16) . 10_556
F3 B2 F5 112.1(12) 10_556 10_556
F3 B2 F5 137.0(13) . 10_556
F6 B2 F5 24.9(16) 10_556 .
F6 B2 F5 115.2(12) . .
F3 B2 F5 137.0(13) 10_556 .
F3 B2 F5 112.1(12) . .
F5 B2 F5 111(3) 10_556 .
F6 B2 F4 78.6(16) 10_556 .
F6 B2 F4 98.3(16) . .
F3 B2 F4 87.4(7) 10_556 .
F3 B2 F4 99.7(8) . .
F5 B2 F4 75.1(12) 10_556 .
F5 B2 F4 100.7(11) . .
F6 B2 F4 98.3(16) 10_556 10_556
F6 B2 F4 78.6(16) . 10_556
F3 B2 F4 99.7(8) 10_556 10_556
F3 B2 F4 87.4(7) . 10_556
F5 B2 F4 100.7(11) 10_556 10_556
F5 B2 F4 75.1(12) . 10_556
F4 B2 F4 172.7(15) . 10_556
F10 B3 F10 120.000(1) 3_765 .
F10 B3 F10 120.000(5) 3_765 2_645
F10 B3 F10 120.000(2) . 2_645
F10 B3 F9 112(2) 3_765 2_645
F10 B3 F9 44(3) . 2_645
F10 B3 F9 110.0(11) 2_645 2_645
F10 B3 F9 110.0(11) 3_765 3_765
F10 B3 F9 112(2) . 3_765
F10 B3 F9 44(3) 2_645 3_765
F9 B3 F9 78(4) 2_645 3_765
F10 B3 F9 44(3) 3_765 11_766
F10 B3 F9 112(2) . 11_766
F10 B3 F9 110.0(11) 2_645 11_766
F9 B3 F9 140(2) 2_645 11_766
F9 B3 F9 135(5) 3_765 11_766
F10 B3 F9 44(3) 3_765 .
F10 B3 F9 110.0(11) . .
F10 B3 F9 112(2) 2_645 .
F9 B3 F9 78(4) 2_645 .
F9 B3 F9 78(4) 3_765 .
F9 B3 F9 87(6) 11_766 .
F10 B3 F9 110.0(11) 3_765 10_556
F10 B3 F9 44(3) . 10_556
F10 B3 F9 112(2) 2_645 10_556
F9 B3 F9 87(6) 2_645 10_556
F9 B3 F9 140(2) 3_765 10_556
F9 B3 F9 78(4) 11_766 10_556
F9 B3 F9 135(5) . 10_556
F10 B3 F9 112(2) 3_765 12_646
F10 B3 F9 110.0(11) . 12_646
F10 B3 F9 44(3) 2_645 12_646
F9 B3 F9 135(5) 2_645 12_646
F9 B3 F9 87(6) 3_765 12_646
F9 B3 F9 78(4) 11_766 12_646
F9 B3 F9 140(2) . 12_646
F9 B3 F9 78(4) 10_556 12_646
F10 B3 F8 90.0 3_765 10_556
F10 B3 F8 90.000(1) . 10_556
F10 B3 F8 90.0 2_645 10_556
F9 B3 F8 46(3) 2_645 10_556
F9 B3 F8 46(3) 3_765 10_556
F9 B3 F8 134(3) 11_766 10_556
F9 B3 F8 46(3) . 10_556
F9 B3 F8 134(3) 10_556 10_556
F9 B3 F8 134(3) 12_646 10_556
F10 B3 F8 90.0 3_765 .
F10 B3 F8 90.000(1) . .
F10 B3 F8 90.0 2_645 .
F9 B3 F8 134(3) 2_645 .
F9 B3 F8 134(3) 3_765 .
F9 B3 F8 46(3) 11_766 .
F9 B3 F8 134(3) . .
F9 B3 F8 46(3) 10_556 .
F9 B3 F8 46(3) 12_646 .
F8 B3 F8 180.000(2) 10_556 .
F10 B3 F7 60(4) 3_765 3_765
F10 B3 F7 160.6(11) . 3_765
F10 B3 F7 63(4) 2_645 3_765
F9 B3 F7 117(3) 2_645 3_765
F9 B3 F7 55(3) 3_765 3_765
F9 B3 F7 82(4) 11_766 3_765
F9 B3 F7 55(3) . 3_765
F9 B3 F7 155(3) 10_556 3_765
F9 B3 F7 86(3) 12_646 3_765
F8 B3 F7 70.6(11) 10_556 3_765
F8 B3 F7 109.4(11) . 3_765
F3 F3 B2 77.21(9) 10_556 .
B2 F4 F5 50.7(7) . 10_556
B2 F4 F6 48.0(8) . 10_556
F5 F4 F6 82.3(12) 10_556 10_556
F6 F5 B2 73.8(14) 10_556 .
F6 F5 F4 124(2) 10_556 10_556
B2 F5 F4 54.3(7) . 10_556
F5 F6 B2 81.3(19) 10_556 .
F5 F6 F4 128(4) 10_556 10_556
B2 F6 F4 53.4(9) . 10_556
F7 F7 F9 109(10) 10_556 .
F7 F7 F9 116(9) 10_556 2_645
F9 F7 F9 85(6) . 2_645
F7 F7 B3 70.6(11) 10_556 .
F9 F7 B3 62.3(18) . .
F9 F7 B3 62.2(17) 2_645 .
F7 F7 F10 75(9) 10_556 .
F9 F7 F10 116(3) . .
F9 F7 F10 45(4) 2_645 .
B3 F7 F10 60(2) . .
F7 F7 F10 67(10) 10_556 3_765
F9 F7 F10 44(4) . 3_765
F9 F7 F10 114(2) 2_645 3_765
B3 F7 F10 58(2) . 3_765
F10 F7 F10 114.5(9) . 3_765
F7 F7 F8 125.0(15) 10_556 10_556
F9 F7 F8 43(3) . 10_556
F9 F7 F8 43(3) 2_645 10_556
B3 F7 F8 54.6(7) . 10_556
F10 F7 F8 81(3) . 10_556
F10 F7 F8 79(2) 3_765 10_556
F7 F7 F9 42(7) 10_556 10_556
F9 F7 F9 111(2) . 10_556
F9 F7 F9 74(4) 2_645 10_556
B3 F7 F9 49(2) . 10_556
F10 F7 F9 34.5(17) . 10_556
F10 F7 F9 87.2(19) 3_765 10_556
F8 F7 F9 96(2) 10_556 10_556
F9 F8 F9 105.5(18) 11_766 10_556
F9 F8 F9 105.5(17) 11_766 12_646
F9 F8 F9 105.5(18) 10_556 12_646
F9 F8 B3 66.8(16) 11_766 .
F9 F8 B3 66.8(16) 10_556 .
F9 F8 B3 66.8(16) 12_646 .
F9 F8 F7 53(4) 11_766 10_556
F9 F8 F7 53(4) 10_556 10_556
F9 F8 F7 121.5(19) 12_646 10_556
B3 F8 F7 54.7(7) . 10_556
F9 F8 F7 53(4) 11_766 11_766
F9 F8 F7 121.5(18) 10_556 11_766
F9 F8 F7 53(4) 12_646 11_766
B3 F8 F7 54.7(7) . 11_766
F7 F8 F7 90.0(10) 10_556 11_766
F9 F8 F7 121.5(19) 11_766 12_646
F9 F8 F7 53(4) 10_556 12_646
F9 F8 F7 53(4) 12_646 12_646
B3 F8 F7 54.7(7) . 12_646
F7 F8 F7 90.0(10) 10_556 12_646
F7 F8 F7 90.0(10) 11_766 12_646
F10 F9 F8 134.9(14) 3_765 10_556
F10 F9 F7 77(5) 3_765 .
F8 F9 F7 85(4) 10_556 .
F10 F9 F7 73(3) 3_765 3_765
F8 F9 F7 84(4) 10_556 3_765
F7 F9 F7 123.8(17) . 3_765
F10 F9 B3 68.0(16) 3_765 .
F8 F9 B3 66.9(16) 10_556 .
F7 F9 B3 62.6(17) . .
F7 F9 B3 62.4(17) 3_765 .
F10 F9 F9 110.0(13) 3_765 2_645
F8 F9 F9 37.3(9) 10_556 2_645
F7 F9 F9 48(4) . 2_645
F7 F9 F9 102(4) 3_765 2_645
B3 F9 F9 51(2) . 2_645
F10 F9 F9 107(3) 3_765 3_765
F8 F9 F9 37.3(9) 10_556 3_765
F7 F9 F9 102(3) . 3_765
F7 F9 F9 47(5) 3_765 3_765
B3 F9 F9 51(2) . 3_765
F9 F9 F9 60.000(13) 2_645 3_765
F10 F9 F7 50(3) 3_765 10_556
F8 F9 F7 100(3) 10_556 10_556
F7 F9 F7 29(4) . 10_556
F7 F9 F7 101(2) 3_765 10_556
B3 F9 F7 49(2) . 10_556
F9 F9 F7 64(3) 2_645 10_556
F9 F9 F7 99.7(19) 3_765 10_556
F9 F10 F9 136(3) 2_645 10_556
F9 F10 B3 68.2(16) 2_645 .
F9 F10 B3 68.2(16) 10_556 .
F9 F10 F7 62(3) 2_645 .
F9 F10 F7 96(2) 10_556 .
B3 F10 F7 60(2) . .
F9 F10 F7 96(2) 2_645 12_646
F9 F10 F7 62(3) 10_556 12_646
B3 F10 F7 60(2) . 12_646
F7 F10 F7 120(4) . 12_646
F9 F10 F7 59(2) 2_645 2_645
F9 F10 F7 97(3) 10_556 2_645
B3 F10 F7 58(2) . 2_645
F7 F10 F7 105.6(19) . 2_645
F7 F10 F7 37.7(19) 12_646 2_645
F9 F10 F7 97(3) 2_645 10_556
F9 F10 F7 59(2) 10_556 10_556
B3 F10 F7 58(2) . 10_556
F7 F10 F7 37.7(19) . 10_556
F7 F10 F7 105.6(19) 12_646 10_556
F7 F10 F7 117(4) 2_645 10_556
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ru1 C102 1.828(15) .
Ru1 C100 1.911(16) .
Ru1 C101 1.916(18) .
Ru1 P1 2.351(4) .
Ru1 Ru1 2.8578(17) 2_655
Ru1 Ru1 2.8578(17) 3_665
P1 C7 1.813(14) .
P1 C13 1.826(14) .
P1 C5 1.854(13) .
O100 C100 1.153(16) .
O101 C101 1.148(17) .
O102 C102 1.195(17) .
N1 C1 1.321(18) .
N1 C3 1.38(2) .
N1 C4 1.463(17) .
N2 C1 1.343(17) .
N2 C2 1.39(2) .
N2 C6 1.455(19) .
C1 H1 0.9300 .
C2 C3 1.31(2) .
C2 H2 0.9300 .
C3 H3 0.9300 .
C4 C5 1.504(18) .
C4 H4A 0.9700 .
C4 H4B 0.9700 .
C5 H5A 0.9700 .
C5 H5B 0.9700 .
C6 H6A 0.9600 .
C6 H6B 0.9600 .
C6 H6C 0.9600 .
C7 C12 1.34(2) .
C7 C8 1.349(19) .
C8 C9 1.40(2) .
C8 H8 0.9300 .
C9 C10 1.33(3) .
C9 H9 0.9300 .
C10 C11 1.25(3) .
C10 H10 0.9300 .
C11 C12 1.46(3) .
C11 H11 0.9300 .
C12 H12 0.9300 .
C13 C18 1.359(19) .
C13 C14 1.40(2) .
C14 C15 1.35(2) .
C14 H14 0.9300 .
C15 C16 1.41(2) .
C15 H15 0.9300 .
C16 C17 1.30(3) .
C16 H16 0.9300 .
C17 C18 1.37(2) .
C17 H17 0.9300 .
C18 H18 0.9300 .
B1 F2 1.341(7) 2_665
B1 F2 1.341(7) 3_565
B1 F2 1.341(7) .
B1 F1 1.341(10) .
B2 F6 1.312(9) 10_556
B2 F6 1.312(9) .
B2 F3 1.339(9) 10_556
B2 F3 1.339(9) .
B2 F5 1.350(9) 10_556
B2 F5 1.350(9) .
B2 F4 1.417(9) .
B2 F4 1.417(9) 10_556
B3 F10 1.341(10) 3_765
B3 F10 1.341(10) .
B3 F10 1.341(10) 2_645
B3 F9 1.342(10) 2_645
B3 F9 1.342(10) 3_765
B3 F9 1.342(10) 11_766
B3 F9 1.342(10) .
B3 F9 1.342(10) 10_556
B3 F9 1.342(10) 12_646
B3 F8 1.344(10) 10_556
B3 F8 1.344(10) .
B3 F7 1.346(10) 3_765
F3 F3 0.5926 10_556
F4 F5 1.69(3) 10_556
F4 F6 1.73(3) 10_556
F5 F6 0.57(4) 10_556
F5 F4 1.69(3) 10_556
F6 F5 0.57(4) 10_556
F6 F4 1.73(3) 10_556
F7 F7 0.89(5) 10_556
F7 F9 1.24(7) .
F7 F9 1.25(7) 2_645
F7 F10 1.35(8) .
F7 F10 1.41(8) 3_765
F7 F8 1.56(3) 10_556
F7 F9 1.76(7) 10_556
F8 F9 1.06(6) 11_766
F8 F9 1.06(6) 10_556
F8 F9 1.06(6) 12_646
F8 F7 1.56(3) 10_556
F8 F7 1.56(3) 11_766
F8 F7 1.56(3) 12_646
F9 F10 1.00(6) 3_765
F9 F8 1.06(6) 10_556
F9 F7 1.25(7) 3_765
F9 F9 1.68(8) 2_645
F9 F9 1.68(8) 3_765
F9 F7 1.76(7) 10_556
F10 F9 1.00(6) 2_645
F10 F9 1.00(6) 10_556
F10 F7 1.35(8) 12_646
F10 F7 1.41(8) 2_645
F10 F7 1.41(8) 10_556
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C102 Ru1 P1 C7 170.0(8) . .
C100 Ru1 P1 C7 74.5(7) . .
C101 Ru1 P1 C7 -93.0(7) . .
Ru1 Ru1 P1 C7 -49.6(7) 2_655 .
Ru1 Ru1 P1 C7 4.8(6) 3_665 .
C102 Ru1 P1 C13 46.6(7) . .
C100 Ru1 P1 C13 -48.9(7) . .
C101 Ru1 P1 C13 143.6(7) . .
Ru1 Ru1 P1 C13 -173.0(5) 2_655 .
Ru1 Ru1 P1 C13 -118.6(5) 3_665 .
C102 Ru1 P1 C5 -71.3(7) . .
C100 Ru1 P1 C5 -166.8(6) . .
C101 Ru1 P1 C5 25.7(7) . .
Ru1 Ru1 P1 C5 69.1(6) 2_655 .
Ru1 Ru1 P1 C5 123.5(4) 3_665 .
C3 N1 C1 N2 -0.6(18) . .
C4 N1 C1 N2 -177.3(13) . .
C2 N2 C1 N1 -2.2(19) . .
C6 N2 C1 N1 178.7(15) . .
C1 N2 C2 C3 4(2) . .
C6 N2 C2 C3 -176.7(17) . .
N2 C2 C3 N1 -5(3) . .
C1 N1 C3 C2 3(2) . .
C4 N1 C3 C2 -179.9(17) . .
C1 N1 C4 C5 -25(2) . .
C3 N1 C4 C5 159.2(16) . .
N1 C4 C5 P1 -166.1(11) . .
C7 P1 C5 C4 -166.2(11) . .
C13 P1 C5 C4 -61.2(12) . .
Ru1 P1 C5 C4 63.8(11) . .
C13 P1 C7 C12 48.0(14) . .
C5 P1 C7 C12 153.7(13) . .
Ru1 P1 C7 C12 -81.5(13) . .
C13 P1 C7 C8 -132.7(13) . .
C5 P1 C7 C8 -27.0(14) . .
Ru1 P1 C7 C8 97.8(13) . .
C12 C7 C8 C9 -1(2) . .
P1 C7 C8 C9 179.5(13) . .
C7 C8 C9 C10 -1(3) . .
C8 C9 C10 C11 3(3) . .
C9 C10 C11 C12 -2(4) . .
C8 C7 C12 C11 2(3) . .
P1 C7 C12 C11 -179.1(16) . .
C10 C11 C12 C7 0(4) . .
C7 P1 C13 C18 -126.9(13) . .
C5 P1 C13 C18 129.4(13) . .
Ru1 P1 C13 C18 6.0(15) . .
C7 P1 C13 C14 52.1(15) . .
C5 P1 C13 C14 -51.6(15) . .
Ru1 P1 C13 C14 -175.0(13) . .
C18 C13 C14 C15 2(3) . .
P1 C13 C14 C15 -177.4(18) . .
C13 C14 C15 C16 2(3) . .
C14 C15 C16 C17 -2(3) . .
C15 C16 C17 C18 -1(3) . .
C14 C13 C18 C17 -5(3) . .
P1 C13 C18 C17 174.2(15) . .
C16 C17 C18 C13 5(3) . .
C102 Ru1 C100 O100 -16(8) . .
C101 Ru1 C100 O100 -167(6) . .
P1 Ru1 C100 O100 79(7) . .
Ru1 Ru1 C100 O100 -116(7) 2_655 .
Ru1 Ru1 C100 O100 -171(8) 3_665 .
C102 Ru1 C101 O101 68(9) . .
C100 Ru1 C101 O101 -142(8) . .
P1 Ru1 C101 O101 -27(9) . .
Ru1 Ru1 C101 O101 166(9) 2_655 .
Ru1 Ru1 C101 O101 -138(9) 3_665 .
C100 Ru1 C102 O102 69(22) . .
C101 Ru1 C102 O102 -118(22) . .
P1 Ru1 C102 O102 -25(22) . .
Ru1 Ru1 C102 O102 167(22) 2_655 .
Ru1 Ru1 C102 O102 126(22) 3_665 .
F6 B2 F3 F3 142.9(14) 10_556 10_556
F6 B2 F3 F3 -45.0(17) . 10_556
F5 B2 F3 F3 -16.3(15) 10_556 10_556
F5 B2 F3 F3 168.1(11) . 10_556
F4 B2 F3 F3 62.2(9) . 10_556
F4 B2 F3 F3 -119.2(9) 10_556 10_556
F6 B2 F4 F5 120.3(12) 10_556 10_556
F6 B2 F4 F5 -9(2) . 10_556
F3 B2 F4 F5 -113.7(13) 10_556 10_556
F3 B2 F4 F5 -136.2(13) . 10_556
F5 B2 F4 F5 109(3) . 10_556
F4 B2 F4 F5 55.1(13) 10_556 10_556
F6 B2 F4 F6 -129(3) . 10_556
F3 B2 F4 F6 126.0(13) 10_556 10_556
F3 B2 F4 F6 103.5(12) . 10_556
F5 B2 F4 F6 -120.3(12) 10_556 10_556
F5 B2 F4 F6 -11(2) . 10_556
F4 B2 F4 F6 -65.1(13) 10_556 10_556
F6 B2 F5 F6 132(5) . 10_556
F3 B2 F5 F6 -70(6) 10_556 10_556
F3 B2 F5 F6 -78(5) . 10_556
F5 B2 F5 F6 105(5) 10_556 10_556
F4 B2 F5 F6 27(5) . 10_556
F4 B2 F5 F6 -159(6) 10_556 10_556
F6 B2 F5 F4 159(6) 10_556 10_556
F6 B2 F5 F4 -69(2) . 10_556
F3 B2 F5 F4 88.3(12) 10_556 10_556
F3 B2 F5 F4 80.8(9) . 10_556
F5 B2 F5 F4 -96.0(9) 10_556 10_556
F4 B2 F5 F4 -173.9(13) . 10_556
F6 B2 F6 F5 -61(5) 10_556 10_556
F3 B2 F6 F5 110(5) 10_556 10_556
F3 B2 F6 F5 129(5) . 10_556
F5 B2 F6 F5 -85(6) . 10_556
F4 B2 F6 F5 21(6) . 10_556
F4 B2 F6 F5 -153(5) 10_556 10_556
F6 B2 F6 F4 91.3(10) 10_556 10_556
F3 B2 F6 F4 -97.1(9) 10_556 10_556
F3 B2 F6 F4 -78.7(13) . 10_556
F5 B2 F6 F4 153(5) 10_556 10_556
F5 B2 F6 F4 67.3(16) . 10_556
F4 B2 F6 F4 173.3(14) . 10_556
F10 B3 F7 F7 -75(11) 3_765 10_556
F10 B3 F7 F7 83(11) . 10_556
F10 B3 F7 F7 180.000(7) 2_645 10_556
F9 B3 F7 F7 135(13) 2_645 10_556
F9 B3 F7 F7 -175(10) 3_765 10_556
F9 B3 F7 F7 -35(11) 11_766 10_556
F9 B3 F7 F7 -125(14) . 10_556
F9 B3 F7 F7 43(11) 10_556 10_556
F9 B3 F7 F7 11(21) 12_646 10_556
F8 B3 F7 F7 -175(13) 10_556 10_556
F8 B3 F7 F7 5(13) . 10_556
F7 B3 F7 F7 -115(13) 3_765 10_556
F10 B3 F7 F9 51(4) 3_765 .
F10 B3 F7 F9 -151(4) . .
F10 B3 F7 F9 -55(14) 2_645 .
F9 B3 F7 F9 -99(7) 2_645 .
F9 B3 F7 F9 -49(5) 3_765 .
F9 B3 F7 F9 90(7) 11_766 .
F9 B3 F7 F9 168(3) 10_556 .
F9 B3 F7 F9 136(8) 12_646 .
F8 B3 F7 F9 -50(3) 10_556 .
F8 B3 F7 F9 130(3) . .
F7 B3 F7 F9 11(4) 3_765 .
F10 B3 F7 F9 150(4) 3_765 2_645
F10 B3 F7 F9 -52(4) . 2_645
F10 B3 F7 F9 45(13) 2_645 2_645
F9 B3 F7 F9 50(6) 3_765 2_645
F9 B3 F7 F9 -171(2) 11_766 2_645
F9 B3 F7 F9 99(7) . 2_645
F9 B3 F7 F9 -93(6) 10_556 2_645
F9 B3 F7 F9 -124(11) 12_646 2_645
F8 B3 F7 F9 50(4) 10_556 2_645
F8 B3 F7 F9 -130(4) . 2_645
F7 B3 F7 F9 110(4) 3_765 2_645
F10 B3 F7 F10 -158.3(11) 3_765 .
F10 B3 F7 F10 97(11) 2_645 .
F9 B3 F7 F10 52(4) 2_645 .
F9 B3 F7 F10 102(2) 3_765 .
F9 B3 F7 F10 -119(3) 11_766 .
F9 B3 F7 F10 151(4) . .
F9 B3 F7 F10 -40.9(19) 10_556 .
F9 B3 F7 F10 -72(11) 12_646 .
F8 B3 F7 F10 101.5(19) 10_556 .
F8 B3 F7 F10 -78.5(19) . .
F7 B3 F7 F10 162(2) 3_765 .
F10 B3 F7 F10 158.3(11) . 3_765
F10 B3 F7 F10 -105(11) 2_645 3_765
F9 B3 F7 F10 -150(4) 2_645 3_765
F9 B3 F7 F10 -100(2) 3_765 3_765
F9 B3 F7 F10 39(3) 11_766 3_765
F9 B3 F7 F10 -51(4) . 3_765
F9 B3 F7 F10 117.4(19) 10_556 3_765
F9 B3 F7 F10 86(11) 12_646 3_765
F8 B3 F7 F10 -100.1(18) 10_556 3_765
F8 B3 F7 F10 79.9(18) . 3_765
F7 B3 F7 F10 -40(3) 3_765 3_765
F10 B3 F7 F8 100.1(18) 3_765 10_556
F10 B3 F7 F8 -101.5(19) . 10_556
F10 B3 F7 F8 -5(13) 2_645 10_556
F9 B3 F7 F8 -50(4) 2_645 10_556
F9 B3 F7 F8 0(4) 3_765 10_556
F9 B3 F7 F8 140(4) 11_766 10_556
F9 B3 F7 F8 50(3) . 10_556
F9 B3 F7 F8 -142(3) 10_556 10_556
F9 B3 F7 F8 -174(9) 12_646 10_556
F8 B3 F7 F8 180.00(2) . 10_556
F7 B3 F7 F8 60.1(13) 3_765 10_556
F10 B3 F7 F9 -117.4(19) 3_765 10_556
F10 B3 F7 F9 40.9(19) . 10_556
F10 B3 F7 F9 137(11) 2_645 10_556
F9 B3 F7 F9 93(6) 2_645 10_556
F9 B3 F7 F9 143(3) 3_765 10_556
F9 B3 F7 F9 -78(5) 11_766 10_556
F9 B3 F7 F9 -168(3) . 10_556
F9 B3 F7 F9 -32(11) 12_646 10_556
F8 B3 F7 F9 142(3) 10_556 10_556
F8 B3 F7 F9 -38(3) . 10_556
F7 B3 F7 F9 -157(3) 3_765 10_556
F10 B3 F8 F9 -2(2) 3_765 11_766
F10 B3 F8 F9 -122(2) . 11_766
F10 B3 F8 F9 118(2) 2_645 11_766
F9 B3 F8 F9 -124(4) 2_645 11_766
F9 B3 F8 F9 116(4) 3_765 11_766
F9 B3 F8 F9 -4(4) . 11_766
F9 B3 F8 F9 -120.000(13) 10_556 11_766
F9 B3 F8 F9 120.000(13) 12_646 11_766
F8 B3 F8 F9 118(55) 10_556 11_766
F7 B3 F8 F9 57(5) 3_765 11_766
F10 B3 F8 F9 118(2) 3_765 10_556
F10 B3 F8 F9 -2(2) . 10_556
F10 B3 F8 F9 -122(2) 2_645 10_556
F9 B3 F8 F9 -4(4) 2_645 10_556
F9 B3 F8 F9 -124(4) 3_765 10_556
F9 B3 F8 F9 120.000(3) 11_766 10_556
F9 B3 F8 F9 116(4) . 10_556
F9 B3 F8 F9 -120.000(1) 12_646 10_556
F8 B3 F8 F9 -122(55) 10_556 10_556
F7 B3 F8 F9 177(5) 3_765 10_556
F10 B3 F8 F9 -122(2) 3_765 12_646
F10 B3 F8 F9 118(2) . 12_646
F10 B3 F8 F9 -2(2) 2_645 12_646
F9 B3 F8 F9 116(4) 2_645 12_646
F9 B3 F8 F9 -4(4) 3_765 12_646
F9 B3 F8 F9 -120.000(12) 11_766 12_646
F9 B3 F8 F9 -124(4) . 12_646
F9 B3 F8 F9 120.000(13) 10_556 12_646
F8 B3 F8 F9 -2(55) 10_556 12_646
F7 B3 F8 F9 -63(5) 3_765 12_646
F10 B3 F8 F7 58(4) 3_765 10_556
F10 B3 F8 F7 -62(4) . 10_556
F10 B3 F8 F7 178(4) 2_645 10_556
F9 B3 F8 F7 -63(5) 2_645 10_556
F9 B3 F8 F7 177(5) 3_765 10_556
F9 B3 F8 F7 60(4) 11_766 10_556
F9 B3 F8 F7 57(5) . 10_556
F9 B3 F8 F7 -60(4) 10_556 10_556
F9 B3 F8 F7 -180(4) 12_646 10_556
F8 B3 F8 F7 178(56) 10_556 10_556
F7 B3 F8 F7 117(8) 3_765 10_556
F10 B3 F8 F7 -62(4) 3_765 11_766
F10 B3 F8 F7 178(4) . 11_766
F10 B3 F8 F7 58(4) 2_645 11_766
F9 B3 F8 F7 177(5) 2_645 11_766
F9 B3 F8 F7 57(5) 3_765 11_766
F9 B3 F8 F7 -60(4) 11_766 11_766
F9 B3 F8 F7 -63(5) . 11_766
F9 B3 F8 F7 -180(4) 10_556 11_766
F9 B3 F8 F7 60(4) 12_646 11_766
F8 B3 F8 F7 58(56) 10_556 11_766
F7 B3 F8 F7 -3(8) 3_765 11_766
F10 B3 F8 F7 178(4) 3_765 12_646
F10 B3 F8 F7 58(4) . 12_646
F10 B3 F8 F7 -62(4) 2_645 12_646
F9 B3 F8 F7 57(5) 2_645 12_646
F9 B3 F8 F7 -63(5) 3_765 12_646
F9 B3 F8 F7 -180(4) 11_766 12_646
F9 B3 F8 F7 177(5) . 12_646
F9 B3 F8 F7 60(4) 10_556 12_646
F9 B3 F8 F7 -60(4) 12_646 12_646
F8 B3 F8 F7 -62(56) 10_556 12_646
F7 B3 F8 F7 -123(8) 3_765 12_646
F7 F7 F9 F10 -17(9) 10_556 3_765
F9 F7 F9 F10 -133(4) 2_645 3_765
B3 F7 F9 F10 -71.7(14) . 3_765
F10 F7 F9 F10 -99(4) . 3_765
F8 F7 F9 F10 -138(2) 10_556 3_765
F9 F7 F9 F10 -62(4) 10_556 3_765
F7 F7 F9 F8 121(9) 10_556 10_556
F9 F7 F9 F8 5(3) 2_645 10_556
B3 F7 F9 F8 66.7(18) . 10_556
F10 F7 F9 F8 39(4) . 10_556
F10 F7 F9 F8 138(2) 3_765 10_556
F9 F7 F9 F8 76(4) 10_556 10_556
F7 F7 F9 F7 42(10) 10_556 3_765
F9 F7 F9 F7 -74(8) 2_645 3_765
B3 F7 F9 F7 -13(5) . 3_765
F10 F7 F9 F7 -40(8) . 3_765
F10 F7 F9 F7 59(4) 3_765 3_765
F8 F7 F9 F7 -80(6) 10_556 3_765
F9 F7 F9 F7 -3(7) 10_556 3_765
F7 F7 F9 B3 54(8) 10_556 .
F9 F7 F9 B3 -61(3) 2_645 .
F10 F7 F9 B3 -28(3) . .
F10 F7 F9 B3 71.7(14) 3_765 .
F8 F7 F9 B3 -66.7(18) 10_556 .
F9 F7 F9 B3 10(3) 10_556 .
F7 F7 F9 F9 116(9) 10_556 2_645
B3 F7 F9 F9 61(3) . 2_645
F10 F7 F9 F9 34(3) . 2_645
F10 F7 F9 F9 133(4) 3_765 2_645
F8 F7 F9 F9 -5(3) 10_556 2_645
F9 F7 F9 F9 71(4) 10_556 2_645
F7 F7 F9 F9 88(9) 10_556 3_765
F9 F7 F9 F9 -27.6(19) 2_645 3_765
B3 F7 F9 F9 34(2) . 3_765
F10 F7 F9 F9 6(4) . 3_765
F10 F7 F9 F9 105(2) 3_765 3_765
F8 F7 F9 F9 -33.1(10) 10_556 3_765
F9 F7 F9 F9 43(4) 10_556 3_765
F9 F7 F9 F7 -116(9) 2_645 10_556
B3 F7 F9 F7 -54(8) . 10_556
F10 F7 F9 F7 -82(7) . 10_556
F10 F7 F9 F7 17(9) 3_765 10_556
F8 F7 F9 F7 -121(9) 10_556 10_556
F9 F7 F9 F7 -45(6) 10_556 10_556
F10 B3 F9 F10 113.0(11) . 3_765
F10 B3 F9 F10 -111(2) 2_645 3_765
F9 B3 F9 F10 143(3) 2_645 3_765
F9 B3 F9 F10 -137(4) 3_765 3_765
F9 B3 F9 F10 0.000(6) 11_766 3_765
F9 B3 F9 F10 69(2) 10_556 3_765
F9 B3 F9 F10 -67.0(11) 12_646 3_765
F8 B3 F9 F10 -177(3) 10_556 3_765
F8 B3 F9 F10 3(3) . 3_765
F7 B3 F9 F10 -81(4) 3_765 3_765
F10 B3 F9 F8 177(3) 3_765 10_556
F10 B3 F9 F8 -70(2) . 10_556
F10 B3 F9 F8 66.8(14) 2_645 10_556
F9 B3 F9 F8 -39.9(14) 2_645 10_556
F9 B3 F9 F8 39.9(14) 3_765 10_556
F9 B3 F9 F8 177(3) 11_766 10_556
F9 B3 F9 F8 -113.2(14) 10_556 10_556
F9 B3 F9 F8 110(2) 12_646 10_556
F8 B3 F9 F8 180.000(17) . 10_556
F7 B3 F9 F8 96(4) 3_765 10_556
F10 B3 F9 F7 -86(5) 3_765 .
F10 B3 F9 F7 26(5) . .
F10 B3 F9 F7 163(4) 2_645 .
F9 B3 F9 F7 56(4) 2_645 .
F9 B3 F9 F7 136(3) 3_765 .
F9 B3 F9 F7 -86(5) 11_766 .
F9 B3 F9 F7 -17(4) 10_556 .
F9 B3 F9 F7 -154(5) 12_646 .
F8 B3 F9 F7 96(4) 10_556 .
F8 B3 F9 F7 -84(4) . .
F7 B3 F9 F7 -168(4) 3_765 .
F10 B3 F9 F7 81(4) 3_765 3_765
F10 B3 F9 F7 -166(3) . 3_765
F10 B3 F9 F7 -29(4) 2_645 3_765
F9 B3 F9 F7 -136(4) 2_645 3_765
F9 B3 F9 F7 -56(5) 3_765 3_765
F9 B3 F9 F7 81(4) 11_766 3_765
F9 B3 F9 F7 151(4) 10_556 3_765
F9 B3 F9 F7 14(3) 12_646 3_765
F8 B3 F9 F7 -96(4) 10_556 3_765
F8 B3 F9 F7 84(4) . 3_765
F10 B3 F9 F9 -143(3) 3_765 2_645
F10 B3 F9 F9 -29.8(14) . 2_645
F10 B3 F9 F9 107(2) 2_645 2_645
F9 B3 F9 F9 80(3) 3_765 2_645
F9 B3 F9 F9 -143(3) 11_766 2_645
F9 B3 F9 F9 -73(2) 10_556 2_645
F9 B3 F9 F9 150.2(14) 12_646 2_645
F8 B3 F9 F9 39.9(14) 10_556 2_645
F8 B3 F9 F9 -140.1(14) . 2_645
F7 B3 F9 F9 136(4) 3_765 2_645
F10 B3 F9 F9 137(4) 3_765 3_765
F10 B3 F9 F9 -110(4) . 3_765
F10 B3 F9 F9 27(2) 2_645 3_765
F9 B3 F9 F9 -80(3) 2_645 3_765
F9 B3 F9 F9 137(4) 11_766 3_765
F9 B3 F9 F9 -153(2) 10_556 3_765
F9 B3 F9 F9 70(4) 12_646 3_765
F8 B3 F9 F9 -39.9(14) 10_556 3_765
F8 B3 F9 F9 140.1(14) . 3_765
F7 B3 F9 F9 56(5) 3_765 3_765
F10 B3 F9 F7 -55(3) 3_765 10_556
F10 B3 F9 F7 58(3) . 10_556
F10 B3 F9 F7 -166(3) 2_645 10_556
F9 B3 F9 F7 87(4) 2_645 10_556
F9 B3 F9 F7 167(4) 3_765 10_556
F9 B3 F9 F7 -55(3) 11_766 10_556
F9 B3 F9 F7 14(3) 10_556 10_556
F9 B3 F9 F7 -122(3) 12_646 10_556
F8 B3 F9 F7 127(4) 10_556 10_556
F8 B3 F9 F7 -53(4) . 10_556
F7 B3 F9 F7 -137(7) 3_765 10_556
F10 B3 F10 F9 92(2) 3_765 2_645
F10 B3 F10 F9 -88(2) 2_645 2_645
F9 B3 F10 F9 -40(2) 3_765 2_645
F9 B3 F10 F9 140(2) 11_766 2_645
F9 B3 F10 F9 45(5) . 2_645
F9 B3 F10 F9 180.0 10_556 2_645
F9 B3 F10 F9 -135(5) 12_646 2_645
F8 B3 F10 F9 2(2) 10_556 2_645
F8 B3 F10 F9 -178(2) . 2_645
F7 B3 F10 F9 7(13) 3_765 2_645
F10 B3 F10 F9 -88(2) 3_765 10_556
F10 B3 F10 F9 92(2) 2_645 10_556
F9 B3 F10 F9 180.0 2_645 10_556
F9 B3 F10 F9 140(2) 3_765 10_556
F9 B3 F10 F9 -40(2) 11_766 10_556
F9 B3 F10 F9 -135(5) . 10_556
F9 B3 F10 F9 45(5) 12_646 10_556
F8 B3 F10 F9 -178(2) 10_556 10_556
F8 B3 F10 F9 2(2) . 10_556
F7 B3 F10 F9 -173(13) 3_765 10_556
F10 B3 F10 F7 22.4(15) 3_765 .
F10 B3 F10 F7 -157.6(15) 2_645 .
F9 B3 F10 F7 -69(3) 2_645 .
F9 B3 F10 F7 -109(3) 3_765 .
F9 B3 F10 F7 71(3) 11_766 .
F9 B3 F10 F7 -25(4) . .
F9 B3 F10 F7 111(3) 10_556 .
F9 B3 F10 F7 155(4) 12_646 .
F8 B3 F10 F7 -67.6(15) 10_556 .
F8 B3 F10 F7 112.4(15) . .
F7 B3 F10 F7 -63(13) 3_765 .
F10 B3 F10 F7 -157.6(15) 3_765 12_646
F10 B3 F10 F7 22.4(15) 2_645 12_646
F9 B3 F10 F7 111(3) 2_645 12_646
F9 B3 F10 F7 71(3) 3_765 12_646
F9 B3 F10 F7 -109(3) 11_766 12_646
F9 B3 F10 F7 155(4) . 12_646
F9 B3 F10 F7 -69(3) 10_556 12_646
F9 B3 F10 F7 -25(4) 12_646 12_646
F8 B3 F10 F7 112.4(15) 10_556 12_646
F8 B3 F10 F7 -67.6(15) . 12_646
F7 B3 F10 F7 117(13) 3_765 12_646
F10 B3 F10 F7 158.2(14) 3_765 2_645
F10 B3 F10 F7 -21.8(14) 2_645 2_645
F9 B3 F10 F7 66(3) 2_645 2_645
F9 B3 F10 F7 27(3) 3_765 2_645
F9 B3 F10 F7 -153(3) 11_766 2_645
F9 B3 F10 F7 111(4) . 2_645
F9 B3 F10 F7 -114(3) 10_556 2_645
F9 B3 F10 F7 -69(4) 12_646 2_645
F8 B3 F10 F7 68.2(14) 10_556 2_645
F8 B3 F10 F7 -111.8(14) . 2_645
F7 B3 F10 F7 73(13) 3_765 2_645
F10 B3 F10 F7 -21.8(14) 3_765 10_556
F10 B3 F10 F7 158.2(14) 2_645 10_556
F9 B3 F10 F7 -114(3) 2_645 10_556
F9 B3 F10 F7 -153(3) 3_765 10_556
F9 B3 F10 F7 27(3) 11_766 10_556
F9 B3 F10 F7 -69(4) . 10_556
F9 B3 F10 F7 66(3) 10_556 10_556
F9 B3 F10 F7 111(4) 12_646 10_556
F8 B3 F10 F7 -111.8(14) 10_556 10_556
F8 B3 F10 F7 68.2(14) . 10_556
F7 B3 F10 F7 -107(13) 3_765 10_556
F7 F7 F10 F9 -156(6) 10_556 2_645
F9 F7 F10 F9 -51(4) . 2_645
B3 F7 F10 F9 -79.6(16) . 2_645
F10 F7 F10 F9 -100(2) 3_765 2_645
F8 F7 F10 F9 -25.7(14) 10_556 2_645
F9 F7 F10 F9 -141(3) 10_556 2_645
F7 F7 F10 F9 -15(6) 10_556 10_556
F9 F7 F10 F9 89(3) . 10_556
F9 F7 F10 F9 141(3) 2_645 10_556
B3 F7 F10 F9 61(2) . 10_556
F10 F7 F10 F9 41(3) 3_765 10_556
F8 F7 F10 F9 115(3) 10_556 10_556
F7 F7 F10 B3 -76(6) 10_556 .
F9 F7 F10 B3 28(4) . .
F9 F7 F10 B3 79.6(16) 2_645 .
F10 F7 F10 B3 -20.2(11) 3_765 .
F8 F7 F10 B3 53.9(11) 10_556 .
F9 F7 F10 B3 -61(2) 10_556 .
F7 F7 F10 F7 -76(6) 10_556 12_646
F9 F7 F10 F7 28(4) . 12_646
F9 F7 F10 F7 79.6(16) 2_645 12_646
B3 F7 F10 F7 0.000(2) . 12_646
F10 F7 F10 F7 -20.2(11) 3_765 12_646
F8 F7 F10 F7 53.9(11) 10_556 12_646
F9 F7 F10 F7 -61(2) 10_556 12_646
F7 F7 F10 F7 -114(7) 10_556 2_645
F9 F7 F10 F7 -10(4) . 2_645
F9 F7 F10 F7 41.6(13) 2_645 2_645
B3 F7 F10 F7 -38.1(17) . 2_645
F10 F7 F10 F7 -58(3) 3_765 2_645
F8 F7 F10 F7 15.8(14) 10_556 2_645
F9 F7 F10 F7 -99(3) 10_556 2_645
F9 F7 F10 F7 104(9) . 10_556
F9 F7 F10 F7 156(6) 2_645 10_556
B3 F7 F10 F7 76(6) . 10_556
F10 F7 F10 F7 56(6) 3_765 10_556
F8 F7 F10 F7 130(7) 10_556 10_556
F9 F7 F10 F7 15(6) 10_556 10_556
