#------------------------------------------------------------------------------
#$Date: 2016-03-21 06:50:10 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178536 $
#$URL: svn://www.crystallography.net/cod/cif/4/06/42/4064283.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4064283
loop_
_publ_author_name
'Li, Bo'
'Zang, Shuang-Quan'
'Liang, Ran'
'Wu, Yang-Jie'
'Mak, Thomas C. W.'
_publ_section_title
;
 Silver(I)−Organic Networks Assembled with Propargyl-Functionalized
 Di- and Trihydroxybenzenes
;
_journal_issue                   6
_journal_name_full               Organometallics
_journal_page_first              1710
_journal_paper_doi               10.1021/om2000162
_journal_volume                  30
_journal_year                    2011
_chemical_formula_sum            'C28 H13 Ag9 F21 N O17'
_chemical_formula_weight         2005.22
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                107.88(3)
_cell_angle_beta                 109.19(3)
_cell_angle_gamma                95.85(3)
_cell_formula_units_Z            2
_cell_length_a                   11.892(2)
_cell_length_b                   14.616(3)
_cell_length_c                   14.813(3)
_cell_measurement_reflns_used    6936
_cell_measurement_temperature    296
_cell_measurement_theta_max      29.1642
_cell_measurement_theta_min      1.7309
_cell_volume                     2254.5(11)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      296
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0635
_diffrn_reflns_av_sigmaI/netI    0.0573
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       17
_diffrn_reflns_limit_l_min       -17
_diffrn_reflns_number            22374
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.86
_exptl_absorpt_coefficient_mu    3.976
_exptl_absorpt_correction_T_max  0.5347
_exptl_absorpt_correction_T_min  0.5035
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS(2009)
_exptl_crystal_density_diffrn    2.954
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             1872
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.19
_exptl_crystal_size_min          0.18
_refine_diff_density_max         1.698
_refine_diff_density_min         -1.076
_refine_diff_density_rms         0.225
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.021
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     736
_refine_ls_number_reflns         7914
_refine_ls_number_restraints     120
_refine_ls_restrained_S_all      1.015
_refine_ls_R_factor_all          0.0728
_refine_ls_R_factor_gt           0.0661
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1330P)²+17.7885P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.2038
_refine_ls_wR_factor_ref         0.2112
_reflns_number_gt                7049
_reflns_number_total             7914
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om2000162_si_002.cif
_cod_data_source_block           2
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value ' triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_database_code               4064283
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.25399(9) 0.18462(6) 0.11475(7) 0.0464(3) Uani 1 1 d . . .
Ag2 Ag 0.40977(8) 0.19250(7) 0.31707(6) 0.0450(2) Uani 1 1 d . . .
Ag3 Ag 0.61907(8) 0.39512(7) 0.45082(7) 0.0501(3) Uani 1 1 d . . .
Ag4 Ag 0.39365(9) 0.44440(7) 0.34908(8) 0.0526(3) Uani 1 1 d . . .
Ag5 Ag 0.93401(9) 0.36976(7) 0.49803(8) 0.0519(3) Uani 1 1 d . . .
Ag6 Ag -0.11158(9) 0.05355(7) 0.00545(6) 0.0507(3) Uani 1 1 d . . .
Ag7 Ag 0.14110(8) 0.13789(8) 0.24812(7) 0.0531(3) Uani 1 1 d . . .
Ag8 Ag 0.20702(8) 0.36077(8) 0.38798(8) 0.0565(3) Uani 1 1 d . . .
Ag9 Ag 0.43363(11) 0.03041(8) 0.07474(8) 0.0616(3) Uani 1 1 d . . .
C1 C 0.4089(9) 0.3524(7) 0.4345(8) 0.036(2) Uani 1 1 d . . .
C2 C 0.4520(9) 0.3132(7) 0.4955(8) 0.034(2) Uani 1 1 d . . .
C11 C 0.2521(10) -0.0217(8) 0.1607(8) 0.039(2) Uani 1 1 d . . .
C12 C 0.2582(9) 0.0614(7) 0.1570(8) 0.036(2) Uani 1 1 d . . .
O1 O 0.5894(6) 0.2241(5) 0.5742(6) 0.0421(17) Uani 1 1 d . . .
O2 O 0.3145(8) -0.0670(6) 0.3057(6) 0.0466(18) Uani 1 1 d . . .
O3 O 0.5112(8) 0.5058(8) 0.2808(8) 0.066(3) Uani 1 1 d . . .
O4 O 0.6931(8) 0.4845(7) 0.3643(8) 0.062(2) Uani 1 1 d . . .
O5 O 0.0947(7) 0.2945(6) 0.4658(7) 0.0464(18) Uani 1 1 d . . .
O6 O 0.1687(8) 0.1648(6) 0.4106(6) 0.051(2) Uani 1 1 d . . .
O7 O 0.0461(8) 0.3619(6) 0.2509(7) 0.058(2) Uani 1 1 d . . .
O8 O 0.0088(7) 0.2087(6) 0.1422(6) 0.0483(19) Uani 1 1 d . . .
O9 O 0.0572(11) 0.1314(9) -0.0508(8) 0.078(3) Uani 1 1 d . . .
O10 O 0.0552(9) -0.0132(7) -0.1481(7) 0.061(2) Uani 1 1 d . . .
O11 O 0.4121(11) 0.1460(8) 0.0074(8) 0.076(3) Uani 1 1 d . . .
O12 O 0.5345(9) 0.1127(7) -0.0771(8) 0.062(2) Uani 1 1 d . . .
O13 O 0.5559(7) 0.1685(6) 0.2477(6) 0.050(2) Uani 1 1 d . . .
O14 O 0.7206(7) 0.2762(6) 0.3786(6) 0.0486(19) Uani 1 1 d . . .
O15 O 0.8044(7) 0.4248(7) 0.5930(6) 0.054(2) Uani 1 1 d . . .
O16 O 0.7259(7) 0.4605(6) 0.7147(6) 0.0461(18) Uani 1 1 d . . .
O1W O 1.0678(8) 0.5336(7) 0.6123(7) 0.061(2) Uani 1 1 d . . .
H1WA H 1.1404 0.5274 0.6387 0.092 Uiso 1 1 d R . .
H1WB H 1.0423 0.5587 0.6597 0.092 Uiso 1 1 d R . .
N1 N 0.2673(13) 0.3284(8) 0.1108(10) 0.067(3) Uani 1 1 d . . .
C3 C 0.4928(10) 0.2709(8) 0.5795(9) 0.042(2) Uani 1 1 d . . .
H3A H 0.5190 0.3236 0.6458 0.050 Uiso 1 1 calc R . .
H3B H 0.4243 0.2237 0.5729 0.050 Uiso 1 1 calc R . .
C4 C 0.5652(10) 0.1376(8) 0.4938(8) 0.039(2) Uani 1 1 d . . .
C5 C 0.6646(11) 0.1075(9) 0.4769(9) 0.046(3) Uani 1 1 d . . .
H5 H 0.7431 0.1460 0.5174 0.055 Uiso 1 1 calc R . .
C6 C 0.6464(12) 0.0192(10) 0.3988(10) 0.052(3) Uani 1 1 d . . .
H6 H 0.7134 -0.0005 0.3862 0.062 Uiso 1 1 calc R . .
C7 C 0.5306(12) -0.0407(9) 0.3387(9) 0.048(3) Uani 1 1 d . . .
H7 H 0.5199 -0.1008 0.2879 0.058 Uiso 1 1 calc R . .
C8 C 0.4309(10) -0.0088(8) 0.3561(8) 0.038(2) Uani 1 1 d . . .
C9 C 0.4453(9) 0.0814(7) 0.4327(8) 0.035(2) Uani 1 1 d . . .
H9 H 0.3901 0.0812 0.4693 0.043 Uiso 1 1 calc R . .
C10 C 0.2702(11) -0.1044(8) 0.1973(8) 0.043(2) Uani 1 1 d . . .
H10A H 0.1934 -0.1524 0.1696 0.052 Uiso 1 1 calc R . .
H10B H 0.3283 -0.1369 0.1744 0.052 Uiso 1 1 calc R . .
C13 C 0.6189(12) 0.5081(9) 0.2985(11) 0.052(3) Uani 1 1 d . . .
C14 C 0.6735(16) 0.5627(14) 0.2437(15) 0.077(5) Uani 1 1 d . . .
C15 C 0.1166(10) 0.2131(8) 0.4616(8) 0.040(2) Uani 1 1 d . D .
C16 C 0.0680(10) 0.1623(8) 0.5233(9) 0.063(3) Uani 1 1 d D . .
C17 C -0.0058(10) 0.2938(8) 0.1695(9) 0.042(2) Uani 1 1 d . . .
C18 C -0.0992(15) 0.3185(11) 0.0844(11) 0.067(4) Uani 1 1 d . . .
C19 C 0.0641(11) 0.0774(9) -0.1276(8) 0.044(3) Uani 1 1 d . C .
C20 C 0.0626(8) 0.1138(7) -0.2129(8) 0.058(3) Uani 1 1 d D . .
C21 C 0.4714(12) 0.1629(9) -0.0424(10) 0.050(3) Uani 1 1 d . E .
C22 C 0.4731(11) 0.2609(12) -0.0545(10) 0.086(5) Uani 1 1 d DU . .
C23 C 0.6688(10) 0.2068(9) 0.2947(8) 0.044(3) Uani 1 1 d . A .
C24 C 0.7496(12) 0.1605(8) 0.2428(9) 0.080(5) Uani 1 1 d D . .
C25 C 0.7946(9) 0.4244(8) 0.6742(8) 0.038(2) Uani 1 1 d . B .
C26 C 0.8810(12) 0.3788(10) 0.7374(10) 0.053(3) Uani 1 1 d . . .
C27 C 0.2613(15) 0.3947(12) 0.0806(12) 0.066(4) Uani 1 1 d . . .
C28 C 0.263(2) 0.4729(14) 0.0470(15) 0.102(7) Uani 1 1 d . . .
H28A H 0.3345 0.4828 0.0314 0.152 Uiso 1 1 calc R . .
H28B H 0.2643 0.5316 0.0996 0.152 Uiso 1 1 calc R . .
H28C H 0.1912 0.4587 -0.0136 0.152 Uiso 1 1 calc R . .
F1 F 0.7162(14) 0.0630(10) 0.2046(12) 0.104(4) Uani 0.708(11) 1 d PDU A 1
F2 F 0.8666(9) 0.1825(10) 0.2990(10) 0.104(7) Uani 0.708(11) 1 d PD A 1
F3 F 0.7401(15) 0.1863(12) 0.1630(13) 0.118(5) Uani 0.708(11) 1 d PDU A 1
F1' F 0.803(3) 0.109(2) 0.290(3) 0.104(4) Uani 0.292(11) 1 d PDU A 2
F3' F 0.705(4) 0.106(3) 0.150(2) 0.118(5) Uani 0.292(11) 1 d PDU A 2
F2' F 0.834(2) 0.226(2) 0.251(2) 0.104(7) Uani 0.292(11) 1 d PD A 2
F4 F 0.928(2) 0.4326(17) 0.8388(18) 0.097(5) Uani 0.500(10) 1 d PU B 1
F5 F 0.994(2) 0.394(2) 0.7328(18) 0.092(5) Uani 0.500(10) 1 d P B 1
F6 F 0.857(2) 0.2851(19) 0.708(2) 0.095(5) Uani 0.500(10) 1 d P B 1
F6' F 0.8340(19) 0.3333(17) 0.784(2) 0.095(5) Uani 0.500(10) 1 d P B 2
F4' F 0.985(2) 0.4348(18) 0.793(2) 0.097(5) Uani 0.500(10) 1 d PU B 2
F5' F 0.903(2) 0.298(2) 0.6698(18) 0.092(5) Uani 0.500(10) 1 d P B 2
F7 F 0.7795(12) 0.5541(13) 0.2489(14) 0.152(7) Uani 1 1 d . . .
F8 F 0.6848(16) 0.6625(9) 0.2893(12) 0.147(6) Uani 1 1 d . . .
F9 F 0.5986(13) 0.5442(11) 0.1507(9) 0.128(5) Uani 1 1 d . . .
F10 F 0.1430(15) 0.0845(14) -0.2535(15) 0.109(6) Uani 0.77(2) 1 d PD C 1
F11 F 0.0863(16) 0.2115(10) -0.1817(11) 0.094(4) Uani 0.77(2) 1 d PDU C 1
F12 F -0.0473(14) 0.0805(12) -0.2879(10) 0.102(5) Uani 0.77(2) 1 d PD C 1
F11' F 0.017(5) 0.191(3) -0.200(4) 0.094(4) Uani 0.23(2) 1 d PD C 2
F12' F -0.001(4) 0.050(4) -0.304(3) 0.102(5) Uani 0.23(2) 1 d PD C 2
F10' F 0.173(4) 0.139(4) -0.207(5) 0.109(6) Uani 0.23(2) 1 d PD C 2
F13 F -0.0464(14) 0.3533(12) 0.0353(11) 0.138(5) Uani 1 1 d . . .
F14 F -0.1498(10) 0.3866(8) 0.1226(8) 0.119(5) Uani 1 1 d . . .
F15 F -0.1873(9) 0.2432(7) 0.0195(7) 0.101(4) Uani 1 1 d . . .
F16 F -0.0077(17) 0.0742(15) 0.4634(16) 0.112(5) Uani 0.572(18) 1 d PDU D 1
F17 F 0.011(2) 0.2197(18) 0.5741(16) 0.120(9) Uani 0.572(18) 1 d PD D 1
F18 F 0.1671(17) 0.1501(15) 0.5911(15) 0.090(4) Uani 0.572(18) 1 d PDU D 1
F18' F 0.121(2) 0.0982(19) 0.5451(19) 0.090(4) Uani 0.428(18) 1 d PDU D 2
F17' F 0.069(3) 0.219(3) 0.606(2) 0.120(9) Uani 0.428(18) 1 d PD D 2
F16' F -0.042(2) 0.117(2) 0.474(2) 0.112(5) Uani 0.428(18) 1 d PDU D 2
F19 F 0.3635(14) 0.2799(11) -0.0825(15) 0.110(6) Uani 0.743(16) 1 d PD E 1
F20 F 0.520(2) 0.2717(14) -0.1205(15) 0.161(14) Uani 0.743(16) 1 d PD E 1
F21 F 0.5393(18) 0.3332(12) 0.0340(16) 0.165(10) Uani 0.743(16) 1 d PD E 1
F20' F 0.579(5) 0.310(4) -0.046(4) 0.161(14) Uani 0.257(16) 1 d PD E 2
F19' F 0.406(4) 0.230(3) -0.155(4) 0.110(6) Uani 0.257(16) 1 d PD E 2
F21' F 0.423(5) 0.331(3) -0.013(5) 0.165(10) Uani 0.257(16) 1 d PD E 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C12 Ag1 N1 166.0(5) . .
C12 Ag1 O9 104.5(4) . .
N1 Ag1 O9 86.9(5) . .
C12 Ag1 Ag2 57.0(3) . .
N1 Ag1 Ag2 109.8(4) . .
O9 Ag1 Ag2 157.0(3) . .
C12 Ag1 Ag7 53.4(3) . .
N1 Ag1 Ag7 117.8(3) . .
O9 Ag1 Ag7 97.9(3) . .
Ag2 Ag1 Ag7 60.71(4) . .
C12 Ag1 Ag9 55.8(3) . .
N1 Ag1 Ag9 128.6(3) . .
O9 Ag1 Ag9 108.4(2) . .
Ag2 Ag1 Ag9 73.96(4) . .
Ag7 Ag1 Ag9 108.43(4) . .
C12 Ag1 Ag6 45.9(3) . 2
N1 Ag1 Ag6 147.0(4) . 2
O9 Ag1 Ag6 60.4(3) . 2
Ag2 Ag1 Ag6 102.91(5) . 2
Ag7 Ag1 Ag6 74.63(4) . 2
Ag9 Ag1 Ag6 64.85(4) . 2
O13 Ag2 C1 123.6(3) . .
O13 Ag2 C12 88.6(3) . .
C1 Ag2 C12 136.1(3) . .
O13 Ag2 C2 124.0(3) . .
C1 Ag2 C2 28.1(3) . .
C12 Ag2 C2 147.3(3) . .
O13 Ag2 C9 102.4(3) . .
C1 Ag2 C9 103.4(3) . .
C12 Ag2 C9 96.5(3) . .
C2 Ag2 C9 76.2(3) . .
O13 Ag2 Ag1 85.0(2) . .
C1 Ag2 Ag1 104.3(3) . .
C12 Ag2 Ag1 44.3(2) . .
C2 Ag2 Ag1 131.4(2) . .
C9 Ag2 Ag1 140.4(2) . .
O13 Ag2 Ag7 138.1(2) . .
C1 Ag2 Ag7 88.9(2) . .
C12 Ag2 Ag7 50.8(2) . .
C2 Ag2 Ag7 97.3(2) . .
C9 Ag2 Ag7 93.3(2) . .
Ag1 Ag2 Ag7 59.74(4) . .
O13 Ag2 Ag3 77.1(2) . .
C1 Ag2 Ag3 48.0(2) . .
C12 Ag2 Ag3 155.7(3) . .
C2 Ag2 Ag3 51.3(2) . .
C9 Ag2 Ag3 105.6(2) . .
Ag1 Ag2 Ag3 113.95(5) . .
Ag7 Ag2 Ag3 135.52(5) . .
O4 Ag3 O15 98.9(3) . .
O4 Ag3 O14 82.8(3) . .
O15 Ag3 O14 77.9(3) . .
O4 Ag3 C1 126.7(3) . .
O15 Ag3 C1 129.8(3) . .
O14 Ag3 C1 122.8(3) . .
O4 Ag3 C2 154.6(3) . .
O15 Ag3 C2 104.7(3) . .
O14 Ag3 C2 111.1(3) . .
C1 Ag3 C2 27.8(3) . .
O4 Ag3 Ag4 81.7(2) . .
O15 Ag3 Ag4 152.8(2) . .
O14 Ag3 Ag4 128.8(2) . .
C1 Ag3 Ag4 45.3(3) . .
C2 Ag3 Ag4 73.0(2) . .
O4 Ag3 Ag4 107.0(3) . 2_666
O15 Ag3 Ag4 71.4(2) . 2_666
O14 Ag3 Ag4 148.8(2) . 2_666
C1 Ag3 Ag4 75.6(3) . 2_666
C2 Ag3 Ag4 72.6(2) . 2_666
Ag4 Ag3 Ag4 82.34(5) . 2_666
O4 Ag3 Ag2 119.2(3) . .
O15 Ag3 Ag2 128.6(2) . .
O14 Ag3 Ag2 74.61(19) . .
C1 Ag3 Ag2 48.6(2) . .
C2 Ag3 Ag2 50.0(2) . .
Ag4 Ag3 Ag2 71.47(4) . .
Ag4 Ag3 Ag2 121.32(5) 2_666 .
C1 Ag4 O3 135.5(4) . .
C1 Ag4 O16 143.4(3) . 2_666
O3 Ag4 O16 80.9(3) . 2_666
C1 Ag4 Ag8 54.9(3) . .
O3 Ag4 Ag8 166.3(3) . .
O16 Ag4 Ag8 89.7(2) 2_666 .
C1 Ag4 Ag3 55.5(3) . .
O3 Ag4 Ag3 81.2(2) . .
O16 Ag4 Ag3 156.4(2) 2_666 .
Ag8 Ag4 Ag3 110.30(4) . .
C1 Ag4 Ag3 84.0(3) . 2_666
O3 Ag4 Ag3 113.9(3) . 2_666
O16 Ag4 Ag3 75.9(2) 2_666 2_666
Ag8 Ag4 Ag3 73.01(5) . 2_666
Ag3 Ag4 Ag3 97.66(5) . 2_666
O5 Ag5 O15 155.6(3) 1_655 .
O5 Ag5 O1W 94.0(3) 1_655 2_766
O15 Ag5 O1W 108.7(3) . 2_766
O5 Ag5 O1W 95.6(3) 1_655 .
O15 Ag5 O1W 82.7(3) . .
O1W Ag5 O1W 73.9(4) 2_766 .
O5 Ag5 O14 115.5(3) 1_655 .
O15 Ag5 O14 74.7(3) . .
O1W Ag5 O14 89.3(3) 2_766 .
O1W Ag5 O14 145.7(3) . .
O10 Ag6 C11 148.6(4) 2 2
O10 Ag6 C12 121.4(4) 2 2
C11 Ag6 C12 29.9(4) 2 2
O10 Ag6 O8 76.5(3) 2 .
C11 Ag6 O8 130.6(3) 2 .
C12 Ag6 O8 160.3(3) 2 .
O10 Ag6 Ag6 75.8(3) 2 2
C11 Ag6 Ag6 110.0(3) 2 2
C12 Ag6 Ag6 94.9(2) 2 2
O8 Ag6 Ag6 97.81(19) . 2
O10 Ag6 Ag1 84.0(2) 2 2
C11 Ag6 Ag1 68.1(3) 2 2
C12 Ag6 Ag1 38.3(3) 2 2
O8 Ag6 Ag1 160.5(2) . 2
Ag6 Ag6 Ag1 77.47(5) 2 2
O6 Ag7 C12 127.6(3) . .
O6 Ag7 O8 124.6(3) . .
C12 Ag7 O8 106.9(3) . .
O6 Ag7 O10 104.3(3) . 2
C12 Ag7 O10 98.2(3) . 2
O8 Ag7 O10 73.5(3) . 2
O6 Ag7 Ag1 143.7(2) . .
C12 Ag7 Ag1 44.7(3) . .
O8 Ag7 Ag1 70.9(2) . .
O10 Ag7 Ag1 111.8(2) 2 .
O6 Ag7 Ag2 87.2(2) . .
C12 Ag7 Ag2 54.6(2) . .
O8 Ag7 Ag2 122.3(2) . .
O10 Ag7 Ag2 150.3(2) 2 .
Ag1 Ag7 Ag2 59.55(4) . .
O6 Ag7 Ag8 65.5(2) . .
C12 Ag7 Ag8 125.0(3) . .
O8 Ag7 Ag8 76.7(2) . .
O10 Ag7 Ag8 133.1(2) 2 .
Ag1 Ag7 Ag8 91.12(4) . .
Ag2 Ag7 Ag8 76.68(5) . .
O7 Ag8 C1 140.6(4) . .
O7 Ag8 O5 98.2(3) . .
C1 Ag8 O5 116.8(3) . .
O7 Ag8 Ag4 98.6(3) . .
C1 Ag8 Ag4 48.3(3) . .
O5 Ag8 Ag4 163.1(2) . .
O7 Ag8 Ag7 80.6(2) . .
C1 Ag8 Ag7 87.6(3) . .
O5 Ag8 Ag7 80.4(2) . .
Ag4 Ag8 Ag7 104.42(5) . .
O12 Ag9 O11 154.3(4) 2_655 .
O12 Ag9 O13 111.8(3) 2_655 .
O11 Ag9 O13 87.3(4) . .
O12 Ag9 Ag9 76.3(2) 2_655 2_655
O11 Ag9 Ag9 79.8(3) . 2_655
O13 Ag9 Ag9 116.81(18) . 2_655
O12 Ag9 Ag1 142.8(3) 2_655 .
O11 Ag9 Ag1 57.6(3) . .
O13 Ag9 Ag1 73.26(19) . .
Ag9 Ag9 Ag1 136.32(6) 2_655 .
C2 C1 Ag4 161.4(8) . .
C2 C1 Ag8 120.0(8) . .
Ag4 C1 Ag8 76.8(3) . .
C2 C1 Ag3 83.3(7) . .
Ag4 C1 Ag3 79.2(3) . .
Ag8 C1 Ag3 155.9(5) . .
C2 C1 Ag2 79.8(7) . .
Ag4 C1 Ag2 104.4(4) . .
Ag8 C1 Ag2 105.3(4) . .
Ag3 C1 Ag2 83.5(3) . .
C1 C2 C3 171.1(11) . .
C1 C2 Ag2 72.0(7) . .
C3 C2 Ag2 114.4(7) . .
C1 C2 Ag3 68.8(6) . .
C3 C2 Ag3 117.7(7) . .
Ag2 C2 Ag3 78.7(3) . .
C12 C11 C10 162.7(11) . .
C12 C11 Ag6 78.1(7) . 2
C10 C11 Ag6 119.2(7) . 2
C11 C12 Ag1 166.8(9) . .
C11 C12 Ag7 106.0(8) . .
Ag1 C12 Ag7 81.8(3) . .
C11 C12 Ag6 72.1(6) . 2
Ag1 C12 Ag6 95.8(4) . 2
Ag7 C12 Ag6 105.7(4) . 2
C11 C12 Ag2 113.3(8) . .
Ag1 C12 Ag2 78.7(3) . .
Ag7 C12 Ag2 74.6(3) . .
Ag6 C12 Ag2 174.4(5) 2 .
C4 O1 C3 118.4(8) . .
C8 O2 C10 116.4(8) . .
C13 O3 Ag4 128.1(9) . .
C13 O4 Ag3 119.2(8) . .
C15 O5 Ag8 107.6(7) . .
C15 O5 Ag5 132.0(7) . 1_455
Ag8 O5 Ag5 118.4(3) . 1_455
C15 O6 Ag7 128.1(7) . .
C17 O7 Ag8 126.0(8) . .
C17 O8 Ag7 126.1(7) . .
C17 O8 Ag6 135.0(7) . .
Ag7 O8 Ag6 96.3(3) . .
C19 O9 Ag1 115.7(9) . .
C19 O10 Ag6 112.7(8) . 2
C19 O10 Ag7 123.6(8) . 2
Ag6 O10 Ag7 97.9(3) 2 2
C21 O11 Ag9 123.0(9) . .
C21 O12 Ag9 130.3(9) . 2_655
C23 O13 Ag2 125.3(7) . .
C23 O13 Ag9 132.4(7) . .
Ag2 O13 Ag9 101.6(3) . .
C23 O14 Ag3 123.4(7) . .
C23 O14 Ag5 138.3(7) . .
Ag3 O14 Ag5 96.3(3) . .
C25 O15 Ag3 116.6(7) . .
C25 O15 Ag5 137.4(8) . .
Ag3 O15 Ag5 98.5(3) . .
C25 O16 Ag4 121.0(7) . 2_666
Ag5 O1W Ag5 106.1(4) 2_766 .
Ag5 O1W H1WA 108.3 2_766 .
Ag5 O1W H1WA 109.4 . .
Ag5 O1W H1WB 114.1 2_766 .
Ag5 O1W H1WB 109.3 . .
H1WA O1W H1WB 109.5 . .
C27 N1 Ag1 162.0(13) . .
O1 C3 C2 111.4(9) . .
O1 C3 H3A 109.3 . .
C2 C3 H3A 109.3 . .
O1 C3 H3B 109.3 . .
C2 C3 H3B 109.3 . .
H3A C3 H3B 108.0 . .
O1 C4 C5 116.3(10) . .
O1 C4 C9 122.1(9) . .
C5 C4 C9 121.6(10) . .
C4 C5 C6 119.0(11) . .
C4 C5 H5 120.5 . .
C6 C5 H5 120.5 . .
C5 C6 C7 121.7(11) . .
C5 C6 H6 119.2 . .
C7 C6 H6 119.2 . .
C6 C7 C8 118.6(11) . .
C6 C7 H7 120.7 . .
C8 C7 H7 120.7 . .
O2 C8 C7 122.2(10) . .
O2 C8 C9 116.1(9) . .
C7 C8 C9 121.5(10) . .
C8 C9 C4 117.6(9) . .
C8 C9 Ag2 98.3(6) . .
C4 C9 Ag2 91.7(6) . .
C8 C9 H9 115.2 . .
C4 C9 H9 115.2 . .
Ag2 C9 H9 115.2 . .
O2 C10 C11 108.8(9) . .
O2 C10 H10A 109.9 . .
C11 C10 H10A 109.9 . .
O2 C10 H10B 109.9 . .
C11 C10 H10B 109.9 . .
H10A C10 H10B 108.3 . .
O3 C13 O4 128.8(12) . .
O3 C13 C14 114.4(12) . .
O4 C13 C14 116.1(12) . .
F7 C14 F9 112.6(17) . .
F7 C14 F8 104.7(17) . .
F9 C14 F8 102.2(15) . .
F7 C14 C13 115.5(13) . .
F9 C14 C13 111.8(15) . .
F8 C14 C13 108.9(14) . .
O5 C15 O6 127.8(11) . .
O5 C15 C16 116.6(9) . .
O6 C15 C16 115.5(9) . .
F18' C16 F17' 105.1(14) . .
F18' C16 F16' 104.2(14) . .
F17' C16 F16' 104.4(15) . .
F18' C16 F16 72.6(12) . .
F17' C16 F16 127(3) . .
F18' C16 F17 128.6(19) . .
F16' C16 F17 78.2(16) . .
F16 C16 F17 109.5(11) . .
F17' C16 F18 78.5(13) . .
F16' C16 F18 136.7(18) . .
F16 C16 F18 109.3(10) . .
F17 C16 F18 109.2(10) . .
F18' C16 C15 115.3(15) . .
F17' C16 C15 115(2) . .
F16' C16 C15 111.2(17) . .
F16 C16 C15 112.2(14) . .
F17 C16 C15 110.8(15) . .
F18 C16 C15 105.7(12) . .
O7 C17 O8 129.9(11) . .
O7 C17 C18 115.5(10) . .
O8 C17 C18 114.5(10) . .
F13 C18 F14 105.5(15) . .
F13 C18 F15 109.0(14) . .
F14 C18 F15 106.7(14) . .
F13 C18 C17 110.9(14) . .
F14 C18 C17 111.3(12) . .
F15 C18 C17 113.0(12) . .
O9 C19 O10 122.9(12) . .
O9 C19 C20 120.4(11) . .
O10 C19 C20 116.0(10) . .
F12' C20 F10' 108.4(19) . .
F12' C20 F11' 108.5(19) . .
F10' C20 F11' 108.4(19) . .
F12' C20 F11 128(3) . .
F10' C20 F11 75(2) . .
F10' C20 F12 135(3) . .
F11' C20 F12 78(2) . .
F11 C20 F12 107.0(8) . .
F12' C20 F10 74(2) . .
F11' C20 F10 134(2) . .
F11 C20 F10 106.9(8) . .
F12 C20 F10 107.4(9) . .
F12' C20 C19 114(3) . .
F10' C20 C19 110(3) . .
F11' C20 C19 107(2) . .
F11 C20 C19 112.2(11) . .
F12 C20 C19 109.9(11) . .
F10 C20 C19 113.2(10) . .
O12 C21 O11 128.3(12) . .
O12 C21 C22 116.5(11) . .
O11 C21 C22 115.0(11) . .
F20 C22 F19 107.2(11) . .
F20 C22 F21 106.0(11) . .
F19 C22 F21 105.4(11) . .
F20 C22 F21' 119(4) . .
F19 C22 F21' 45.6(18) . .
F21 C22 F21' 60(2) . .
F20 C22 F20' 46(2) . .
F19 C22 F20' 130(3) . .
F21 C22 F20' 62(2) . .
F21' C22 F20' 104(2) . .
F20 C22 F19' 58.2(17) . .
F19 C22 F19' 62.2(17) . .
F21 C22 F19' 150(2) . .
F21' C22 F19' 104(2) . .
F20' C22 F19' 103(2) . .
F20 C22 C21 114.3(14) . .
F19 C22 C21 112.7(12) . .
F21 C22 C21 110.5(14) . .
F21' C22 C21 126(3) . .
F20' C22 C21 117(3) . .
F19' C22 C21 99.2(19) . .
O14 C23 O13 128.0(10) . .
O14 C23 C24 116.9(10) . .
O13 C23 C24 115.1(10) . .
F3' C24 F1' 106.0(16) . .
F3' C24 F2' 105.6(16) . .
F1' C24 F2' 105.0(16) . .
F3' C24 F2 123(2) . .
F1' C24 F2 55.1(15) . .
F2' C24 F2 50.5(14) . .
F3' C24 F3 52.4(14) . .
F1' C24 F3 141(2) . .
F2' C24 F3 61.2(13) . .
F2 C24 F3 105.9(11) . .
F3' C24 F1 53.2(14) . .
F1' C24 F1 58.7(14) . .
F2' C24 F1 137(2) . .
F2 C24 F1 106.1(10) . .
F3 C24 F1 105.0(10) . .
F3' C24 C23 120(2) . .
F1' C24 C23 109(2) . .
F2' C24 C23 110.3(17) . .
F2 C24 C23 116.5(11) . .
F3 C24 C23 110.2(13) . .
F1 C24 C23 112.2(13) . .
O16 C25 O15 129.2(11) . .
O16 C25 C26 112.9(10) . .
O15 C25 C26 117.8(10) . .
F4' C26 F6 125.5(18) . .
F4' C26 F6' 114.3(19) . .
F6 C26 F6' 58.8(16) . .
F4' C26 F4 50.4(14) . .
F6 C26 F4 119.2(18) . .
F6' C26 F4 70.9(16) . .
F6 C26 F5 99.3(17) . .
F6' C26 F5 133.4(15) . .
F4 C26 F5 91.2(16) . .
F4' C26 F5' 104.7(18) . .
F6' C26 F5' 99.6(17) . .
F4 C26 F5' 137.6(16) . .
F5 C26 F5' 65.0(15) . .
F4' C26 C25 113.8(15) . .
F6 C26 C25 117.0(14) . .
F6' C26 C25 114.6(13) . .
F4 C26 C25 113.4(14) . .
F5 C26 C25 112.0(13) . .
F5' C26 C25 108.1(13) . .
N1 C27 C28 176.0(19) . .
C27 C28 H28A 109.5 . .
C27 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
C27 C28 H28C 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 C12 2.080(11) .
Ag1 N1 2.112(10) .
Ag1 O9 2.604(11) .
Ag1 Ag2 2.9193(16) .
Ag1 Ag7 2.9252(15) .
Ag1 Ag9 3.3148(17) .
Ag1 Ag6 3.3417(19) 2
Ag2 O13 2.297(7) .
Ag2 C1 2.451(10) .
Ag2 C12 2.498(10) .
Ag2 C2 2.536(10) .
Ag2 C9 2.668(9) .
Ag2 Ag7 2.9535(16) .
Ag2 Ag3 3.247(2) .
Ag3 O4 2.378(9) .
Ag3 O15 2.382(8) .
Ag3 O14 2.400(8) .
Ag3 C1 2.427(10) .
Ag3 C2 2.585(10) .
Ag3 Ag4 2.8949(16) .
Ag3 Ag4 3.2263(19) 2_666
Ag4 C1 2.095(11) .
Ag4 O3 2.239(8) .
Ag4 O16 2.275(7) 2_666
Ag4 Ag8 2.7335(14) .
Ag4 Ag3 3.2263(19) 2_666
Ag5 O5 2.408(8) 1_655
Ag5 O15 2.446(8) .
Ag5 O1W 2.463(9) 2_766
Ag5 O1W 2.469(10) .
Ag5 O14 2.510(8) .
Ag6 O10 2.275(8) 2
Ag6 C11 2.345(10) 2
Ag6 C12 2.412(10) 2
Ag6 O8 2.431(8) .
Ag6 Ag6 3.239(2) 2
Ag6 Ag1 3.3417(19) 2
Ag7 O6 2.220(8) .
Ag7 C12 2.374(10) .
Ag7 O8 2.391(8) .
Ag7 O10 2.484(10) 2
Ag7 Ag8 3.128(2) .
Ag8 O7 2.293(8) .
Ag8 C1 2.297(10) .
Ag8 O5 2.342(7) .
Ag9 O12 2.172(9) 2_655
Ag9 O11 2.207(10) .
Ag9 O13 2.555(8) .
Ag9 Ag9 3.092(2) 2_655
C1 C2 1.216(15) .
C2 C3 1.517(14) .
C11 C12 1.228(15) .
C11 C10 1.477(15) .
C11 Ag6 2.345(10) 2
C12 Ag6 2.412(10) 2
O1 C4 1.370(13) .
O1 C3 1.408(13) .
O2 C8 1.374(13) .
O2 C10 1.415(13) .
O3 C13 1.215(15) .
O4 C13 1.246(15) .
O5 C15 1.231(13) .
O5 Ag5 2.408(8) 1_455
O6 C15 1.233(13) .
O7 C17 1.215(14) .
O8 C17 1.233(13) .
O9 C19 1.203(15) .
O10 C19 1.249(15) .
O10 Ag6 2.275(8) 2
O10 Ag7 2.484(10) 2
O11 C21 1.233(15) .
O12 C21 1.225(15) .
O12 Ag9 2.172(9) 2_655
O13 C23 1.263(14) .
O14 C23 1.244(14) .
O15 C25 1.249(14) .
O16 C25 1.233(13) .
O16 Ag4 2.275(7) 2_666
O1W Ag5 2.463(9) 2_766
O1W H1WA 0.8500 .
O1W H1WB 0.8500 .
N1 C27 1.185(19) .
C3 H3A 0.9700 .
C3 H3B 0.9700 .
C4 C5 1.374(15) .
C4 C9 1.408(15) .
C5 C6 1.383(18) .
C5 H5 0.9300 .
C6 C7 1.387(18) .
C6 H6 0.9300 .
C7 C8 1.388(16) .
C7 H7 0.9300 .
C8 C9 1.401(15) .
C9 H9 0.9800 .
C10 H10A 0.9700 .
C10 H10B 0.9700 .
C13 C14 1.536(19) .
C14 F7 1.258(18) .
C14 F9 1.30(2) .
C14 F8 1.38(2) .
C15 C16 1.549(18) .
C16 F18' 1.25(2) .
C16 F17' 1.25(2) .
C16 F16' 1.26(2) .
C16 F16 1.339(16) .
C16 F17 1.341(16) .
C16 F18 1.343(16) .
C17 C18 1.547(18) .
C18 F13 1.28(2) .
C18 F14 1.293(18) .
C18 F15 1.299(17) .
C19 C20 1.509(16) .
C20 F12' 1.29(4) .
C20 F10' 1.29(4) .
C20 F11' 1.29(4) .
C20 F11 1.327(12) .
C20 F12 1.328(12) .
C20 F10 1.328(12) .
C21 C22 1.50(2) .
C22 F20 1.314(14) .
C22 F19 1.318(14) .
C22 F21 1.326(14) .
C22 F21' 1.33(5) .
C22 F20' 1.33(4) .
C22 F19' 1.34(4) .
C23 C24 1.51(2) .
C24 F3' 1.25(3) .
C24 F1' 1.25(3) .
C24 F2' 1.26(3) .
C24 F2 1.310(13) .
C24 F3 1.321(13) .
C24 F1 1.323(13) .
C25 C26 1.506(16) .
C26 F4' 1.26(3) .
C26 F6 1.27(3) .
C26 F6' 1.30(2) .
C26 F4 1.35(3) .
C26 F5 1.36(2) .
C26 F5' 1.41(3) .
C27 C28 1.38(2) .
C28 H28A 0.9600 .
C28 H28B 0.9600 .
C28 H28C 0.9600 .
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_atom_site_label_H
_geom_hbond_atom_site_label_A
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_angle_DHA
_geom_hbond_site_symmetry_A
O1W H1WA O4 0.85 2.02 2.800(12) 152.4 2_766
O1W H1WA F7 0.85 2.35 2.968(15) 130.2 2_766
O1W H1WB O7 0.85 2.10 2.932(14) 164.5 2_666
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C12 Ag1 Ag2 O13 93.2(4) . .
N1 Ag1 Ag2 O13 -92.1(4) . .
O9 Ag1 Ag2 O13 133.3(7) . .
Ag7 Ag1 Ag2 O13 156.4(2) . .
Ag9 Ag1 Ag2 O13 33.8(2) . .
Ag6 Ag1 Ag2 O13 92.5(2) 2 .
C12 Ag1 Ag2 C1 -143.4(4) . .
N1 Ag1 Ag2 C1 31.3(4) . .
O9 Ag1 Ag2 C1 -103.2(7) . .
Ag7 Ag1 Ag2 C1 -80.2(2) . .
Ag9 Ag1 Ag2 C1 157.2(2) . .
Ag6 Ag1 Ag2 C1 -144.0(2) 2 .
N1 Ag1 Ag2 C12 174.7(5) . .
O9 Ag1 Ag2 C12 40.2(7) . .
Ag7 Ag1 Ag2 C12 63.2(3) . .
Ag9 Ag1 Ag2 C12 -59.3(3) . .
Ag6 Ag1 Ag2 C12 -0.6(3) 2 .
C12 Ag1 Ag2 C2 -134.7(4) . .
N1 Ag1 Ag2 C2 40.0(5) . .
O9 Ag1 Ag2 C2 -94.5(7) . .
Ag7 Ag1 Ag2 C2 -71.5(3) . .
Ag9 Ag1 Ag2 C2 166.0(3) . .
Ag6 Ag1 Ag2 C2 -135.3(3) 2 .
C12 Ag1 Ag2 C9 -10.3(5) . .
N1 Ag1 Ag2 C9 164.4(5) . .
O9 Ag1 Ag2 C9 29.9(7) . .
Ag7 Ag1 Ag2 C9 52.9(3) . .
Ag9 Ag1 Ag2 C9 -69.6(3) . .
Ag6 Ag1 Ag2 C9 -10.9(3) 2 .
C12 Ag1 Ag2 Ag7 -63.2(3) . .
N1 Ag1 Ag2 Ag7 111.5(4) . .
O9 Ag1 Ag2 Ag7 -23.0(6) . .
Ag9 Ag1 Ag2 Ag7 -122.57(4) . .
Ag6 Ag1 Ag2 Ag7 -63.87(5) 2 .
C12 Ag1 Ag2 Ag3 166.6(3) . .
N1 Ag1 Ag2 Ag3 -18.7(4) . .
O9 Ag1 Ag2 Ag3 -153.2(6) . .
Ag7 Ag1 Ag2 Ag3 -130.15(5) . .
Ag9 Ag1 Ag2 Ag3 107.28(4) . .
Ag6 Ag1 Ag2 Ag3 165.99(4) 2 .
O13 Ag2 Ag3 O4 51.5(3) . .
C1 Ag2 Ag3 O4 -114.8(4) . .
C12 Ag2 Ag3 O4 -3.8(6) . .
C2 Ag2 Ag3 O4 -151.8(4) . .
C9 Ag2 Ag3 O4 151.0(3) . .
Ag1 Ag2 Ag3 O4 -27.0(2) . .
Ag7 Ag2 Ag3 O4 -97.5(2) . .
O13 Ag2 Ag3 O15 -80.9(3) . .
C1 Ag2 Ag3 O15 112.7(4) . .
C12 Ag2 Ag3 O15 -136.2(6) . .
C2 Ag2 Ag3 O15 75.8(4) . .
C9 Ag2 Ag3 O15 18.5(3) . .
Ag1 Ag2 Ag3 O15 -159.4(3) . .
Ag7 Ag2 Ag3 O15 130.1(3) . .
O13 Ag2 Ag3 O14 -20.8(3) . .
C1 Ag2 Ag3 O14 172.8(4) . .
C12 Ag2 Ag3 O14 -76.1(6) . .
C2 Ag2 Ag3 O14 135.9(4) . .
C9 Ag2 Ag3 O14 78.6(3) . .
Ag1 Ag2 Ag3 O14 -99.3(2) . .
Ag7 Ag2 Ag3 O14 -169.8(2) . .
O13 Ag2 Ag3 C1 166.3(4) . .
C12 Ag2 Ag3 C1 111.0(6) . .
C2 Ag2 Ag3 C1 -37.0(4) . .
C9 Ag2 Ag3 C1 -94.2(4) . .
Ag1 Ag2 Ag3 C1 87.8(3) . .
Ag7 Ag2 Ag3 C1 17.4(3) . .
O13 Ag2 Ag3 C2 -156.7(4) . .
C1 Ag2 Ag3 C2 37.0(4) . .
C12 Ag2 Ag3 C2 148.0(6) . .
C9 Ag2 Ag3 C2 -57.2(4) . .
Ag1 Ag2 Ag3 C2 124.8(3) . .
Ag7 Ag2 Ag3 C2 54.3(3) . .
O13 Ag2 Ag3 Ag4 120.2(2) . .
C1 Ag2 Ag3 Ag4 -46.1(3) . .
C12 Ag2 Ag3 Ag4 64.9(5) . .
C2 Ag2 Ag3 Ag4 -83.1(3) . .
C9 Ag2 Ag3 Ag4 -140.3(2) . .
Ag1 Ag2 Ag3 Ag4 41.73(4) . .
Ag7 Ag2 Ag3 Ag4 -28.73(6) . .
O13 Ag2 Ag3 Ag4 -171.4(2) . 2_666
C1 Ag2 Ag3 Ag4 22.3(3) . 2_666
C12 Ag2 Ag3 Ag4 133.3(5) . 2_666
C2 Ag2 Ag3 Ag4 -14.7(3) . 2_666
C9 Ag2 Ag3 Ag4 -71.9(2) . 2_666
Ag1 Ag2 Ag3 Ag4 110.10(5) . 2_666
Ag7 Ag2 Ag3 Ag4 39.64(7) . 2_666
O4 Ag3 Ag4 C1 174.2(4) . .
O15 Ag3 Ag4 C1 -92.5(6) . .
O14 Ag3 Ag4 C1 100.5(4) . .
C2 Ag3 Ag4 C1 -3.2(4) . .
Ag4 Ag3 Ag4 C1 -77.3(4) 2_666 .
Ag2 Ag3 Ag4 C1 49.5(3) . .
O4 Ag3 Ag4 O3 4.6(4) . .
O15 Ag3 Ag4 O3 97.9(6) . .
O14 Ag3 Ag4 O3 -69.1(4) . .
C1 Ag3 Ag4 O3 -169.6(5) . .
C2 Ag3 Ag4 O3 -172.8(4) . .
Ag4 Ag3 Ag4 O3 113.1(3) 2_666 .
Ag2 Ag3 Ag4 O3 -120.2(3) . .
O4 Ag3 Ag4 O16 -36.4(6) . 2_666
O15 Ag3 Ag4 O16 56.9(7) . 2_666
O14 Ag3 Ag4 O16 -110.1(6) . 2_666
C1 Ag3 Ag4 O16 149.4(6) . 2_666
C2 Ag3 Ag4 O16 146.2(6) . 2_666
Ag4 Ag3 Ag4 O16 72.1(5) 2_666 2_666
Ag2 Ag3 Ag4 O16 -161.1(5) . 2_666
O4 Ag3 Ag4 Ag8 176.8(3) . .
O15 Ag3 Ag4 Ag8 -89.9(5) . .
O14 Ag3 Ag4 Ag8 103.1(3) . .
C1 Ag3 Ag4 Ag8 2.6(3) . .
C2 Ag3 Ag4 Ag8 -0.6(2) . .
Ag4 Ag3 Ag4 Ag8 -74.66(5) 2_666 .
Ag2 Ag3 Ag4 Ag8 52.09(5) . .
O4 Ag3 Ag4 Ag3 -108.6(3) . 2_666
O15 Ag3 Ag4 Ag3 -15.2(5) . 2_666
O14 Ag3 Ag4 Ag3 177.8(3) . 2_666
C1 Ag3 Ag4 Ag3 77.3(3) . 2_666
C2 Ag3 Ag4 Ag3 74.1(2) . 2_666
Ag4 Ag3 Ag4 Ag3 0.0 2_666 2_666
Ag2 Ag3 Ag4 Ag3 126.75(4) . 2_666
C12 Ag1 Ag7 O6 95.2(5) . .
N1 Ag1 Ag7 O6 -71.9(6) . .
O9 Ag1 Ag7 O6 -162.6(4) . .
Ag2 Ag1 Ag7 O6 26.3(4) . .
Ag9 Ag1 Ag7 O6 84.9(4) . .
Ag6 Ag1 Ag7 O6 141.2(4) 2 .
N1 Ag1 Ag7 C12 -167.1(6) . .
O9 Ag1 Ag7 C12 102.3(4) . .
Ag2 Ag1 Ag7 C12 -68.8(3) . .
Ag9 Ag1 Ag7 C12 -10.2(3) . .
Ag6 Ag1 Ag7 C12 46.0(3) 2 .
C12 Ag1 Ag7 O8 -141.8(4) . .
N1 Ag1 Ag7 O8 51.1(5) . .
O9 Ag1 Ag7 O8 -39.5(3) . .
Ag2 Ag1 Ag7 O8 149.4(2) . .
Ag9 Ag1 Ag7 O8 -152.0(2) . .
Ag6 Ag1 Ag7 O8 -95.8(2) 2 .
C12 Ag1 Ag7 O10 -79.3(4) . 2
N1 Ag1 Ag7 O10 113.5(5) . 2
O9 Ag1 Ag7 O10 22.9(3) . 2
Ag2 Ag1 Ag7 O10 -148.2(2) . 2
Ag9 Ag1 Ag7 O10 -89.6(2) . 2
Ag6 Ag1 Ag7 O10 -33.4(2) 2 2
C12 Ag1 Ag7 Ag2 68.8(3) . .
N1 Ag1 Ag7 Ag2 -98.3(5) . .
O9 Ag1 Ag7 Ag2 171.1(3) . .
Ag9 Ag1 Ag7 Ag2 58.62(5) . .
Ag6 Ag1 Ag7 Ag2 114.83(5) 2 .
C12 Ag1 Ag7 Ag8 142.7(3) . .
N1 Ag1 Ag7 Ag8 -24.5(4) . .
O9 Ag1 Ag7 Ag8 -115.1(3) . .
Ag2 Ag1 Ag7 Ag8 73.81(5) . .
Ag9 Ag1 Ag7 Ag8 132.42(4) . .
Ag6 Ag1 Ag7 Ag8 -171.36(4) 2 .
O13 Ag2 Ag7 O6 158.5(4) . .
C1 Ag2 Ag7 O6 -57.6(3) . .
C12 Ag2 Ag7 O6 141.6(4) . .
C2 Ag2 Ag7 O6 -30.6(3) . .
C9 Ag2 Ag7 O6 45.8(3) . .
Ag1 Ag2 Ag7 O6 -164.8(2) . .
Ag3 Ag2 Ag7 O6 -70.4(2) . .
O13 Ag2 Ag7 C12 16.9(5) . .
C1 Ag2 Ag7 C12 160.9(4) . .
C2 Ag2 Ag7 C12 -172.2(4) . .
C9 Ag2 Ag7 C12 -95.8(4) . .
Ag1 Ag2 Ag7 C12 53.6(3) . .
Ag3 Ag2 Ag7 C12 148.0(3) . .
O13 Ag2 Ag7 O8 -71.5(4) . .
C1 Ag2 Ag7 O8 72.5(3) . .
C12 Ag2 Ag7 O8 -88.4(4) . .
C2 Ag2 Ag7 O8 99.4(3) . .
C9 Ag2 Ag7 O8 175.9(3) . .
Ag1 Ag2 Ag7 O8 -34.8(2) . .
Ag3 Ag2 Ag7 O8 59.7(2) . .
O13 Ag2 Ag7 O10 44.0(5) . 2
C1 Ag2 Ag7 O10 -172.1(5) . 2
C12 Ag2 Ag7 O10 27.1(5) . 2
C2 Ag2 Ag7 O10 -145.1(5) . 2
C9 Ag2 Ag7 O10 -68.7(5) . 2
Ag1 Ag2 Ag7 O10 80.7(4) . 2
Ag3 Ag2 Ag7 O10 175.1(4) . 2
O13 Ag2 Ag7 Ag1 -36.7(4) . .
C1 Ag2 Ag7 Ag1 107.2(3) . .
C12 Ag2 Ag7 Ag1 -53.6(3) . .
C2 Ag2 Ag7 Ag1 134.2(2) . .
C9 Ag2 Ag7 Ag1 -149.4(2) . .
Ag3 Ag2 Ag7 Ag1 94.41(6) . .
O13 Ag2 Ag7 Ag8 -136.1(4) . .
C1 Ag2 Ag7 Ag8 7.9(3) . .
C12 Ag2 Ag7 Ag8 -153.0(3) . .
C2 Ag2 Ag7 Ag8 34.8(2) . .
C9 Ag2 Ag7 Ag8 111.3(2) . .
Ag1 Ag2 Ag7 Ag8 -99.36(4) . .
Ag3 Ag2 Ag7 Ag8 -4.95(6) . .
C1 Ag4 Ag8 O7 -155.7(4) . .
O3 Ag4 Ag8 O7 -12.6(12) . .
O16 Ag4 Ag8 O7 34.3(3) 2_666 .
Ag3 Ag4 Ag8 O7 -158.4(2) . .
Ag3 Ag4 Ag8 O7 109.6(2) 2_666 .
O3 Ag4 Ag8 C1 143.1(12) . .
O16 Ag4 Ag8 C1 -170.0(4) 2_666 .
Ag3 Ag4 Ag8 C1 -2.6(4) . .
Ag3 Ag4 Ag8 C1 -94.7(4) 2_666 .
C1 Ag4 Ag8 O5 31.5(8) . .
O3 Ag4 Ag8 O5 174.6(13) . .
O16 Ag4 Ag8 O5 -138.5(7) 2_666 .
Ag3 Ag4 Ag8 O5 28.8(7) . .
Ag3 Ag4 Ag8 O5 -63.2(7) 2_666 .
C1 Ag4 Ag8 Ag7 -73.3(4) . .
O3 Ag4 Ag8 Ag7 69.8(12) . .
O16 Ag4 Ag8 Ag7 116.7(2) 2_666 .
Ag3 Ag4 Ag8 Ag7 -75.93(6) . .
Ag3 Ag4 Ag8 Ag7 -167.98(4) 2_666 .
O6 Ag7 Ag8 O7 -133.1(3) . .
C12 Ag7 Ag8 O7 107.0(4) . .
O8 Ag7 Ag8 O7 5.5(3) . .
O10 Ag7 Ag8 O7 -46.2(4) 2 .
Ag1 Ag7 Ag8 O7 75.5(3) . .
Ag2 Ag7 Ag8 O7 133.8(3) . .
O6 Ag7 Ag8 C1 84.7(4) . .
C12 Ag7 Ag8 C1 -35.3(4) . .
O8 Ag7 Ag8 C1 -136.8(3) . .
O10 Ag7 Ag8 C1 171.5(4) 2 .
Ag1 Ag7 Ag8 C1 -66.7(3) . .
Ag2 Ag7 Ag8 C1 -8.4(3) . .
O6 Ag7 Ag8 O5 -33.1(3) . .
C12 Ag7 Ag8 O5 -153.0(4) . .
O8 Ag7 Ag8 O5 105.5(3) . .
O10 Ag7 Ag8 O5 53.8(3) 2 .
Ag1 Ag7 Ag8 O5 175.6(2) . .
Ag2 Ag7 Ag8 O5 -126.2(2) . .
O6 Ag7 Ag8 Ag4 130.4(2) . .
C12 Ag7 Ag8 Ag4 10.4(3) . .
O8 Ag7 Ag8 Ag4 -91.1(2) . .
O10 Ag7 Ag8 Ag4 -142.8(3) 2 .
Ag1 Ag7 Ag8 Ag4 -21.01(5) . .
Ag2 Ag7 Ag8 Ag4 37.28(4) . .
C12 Ag1 Ag9 O12 12.1(5) . 2_655
N1 Ag1 Ag9 O12 175.6(7) . 2_655
O9 Ag1 Ag9 O12 -83.3(5) . 2_655
Ag2 Ag1 Ag9 O12 72.8(5) . 2_655
Ag7 Ag1 Ag9 O12 22.0(5) . 2_655
Ag6 Ag1 Ag9 O12 -40.3(5) 2 2_655
C12 Ag1 Ag9 O11 170.3(5) . .
N1 Ag1 Ag9 O11 -26.2(6) . .
O9 Ag1 Ag9 O11 74.9(5) . .
Ag2 Ag1 Ag9 O11 -129.0(4) . .
Ag7 Ag1 Ag9 O11 -179.8(4) . .
Ag6 Ag1 Ag9 O11 117.9(4) 2 .
C12 Ag1 Ag9 O13 -92.1(4) . .
N1 Ag1 Ag9 O13 71.4(5) . .
O9 Ag1 Ag9 O13 172.6(4) . .
Ag2 Ag1 Ag9 O13 -31.4(2) . .
Ag7 Ag1 Ag9 O13 -82.2(2) . .
Ag6 Ag1 Ag9 O13 -144.4(2) 2 .
C12 Ag1 Ag9 Ag9 156.4(3) . 2_655
N1 Ag1 Ag9 Ag9 -40.1(5) . 2_655
O9 Ag1 Ag9 Ag9 61.0(3) . 2_655
Ag2 Ag1 Ag9 Ag9 -142.91(9) . 2_655
Ag7 Ag1 Ag9 Ag9 166.32(8) . 2_655
Ag6 Ag1 Ag9 Ag9 104.03(9) 2 2_655
O3 Ag4 C1 C2 35(3) . .
O16 Ag4 C1 C2 -139(3) 2_666 .
Ag8 Ag4 C1 C2 -156(3) . .
Ag3 Ag4 C1 C2 21(3) . .
Ag3 Ag4 C1 C2 -83(3) 2_666 .
O3 Ag4 C1 Ag8 -168.3(4) . .
O16 Ag4 C1 Ag8 17.0(7) 2_666 .
Ag3 Ag4 C1 Ag8 177.0(4) . .
Ag3 Ag4 C1 Ag8 73.4(2) 2_666 .
O3 Ag4 C1 Ag3 14.7(6) . .
O16 Ag4 C1 Ag3 -160.0(4) 2_666 .
Ag8 Ag4 C1 Ag3 -177.0(4) . .
Ag3 Ag4 C1 Ag3 -103.6(2) 2_666 .
O3 Ag4 C1 Ag2 -65.6(7) . .
O16 Ag4 C1 Ag2 119.7(5) 2_666 .
Ag8 Ag4 C1 Ag2 102.7(4) . .
Ag3 Ag4 C1 Ag2 -80.3(3) . .
Ag3 Ag4 C1 Ag2 176.1(3) 2_666 .
O7 Ag8 C1 C2 -148.7(8) . .
O5 Ag8 C1 C2 1.3(10) . .
Ag4 Ag8 C1 C2 171.5(11) . .
Ag7 Ag8 C1 C2 -76.7(9) . .
O7 Ag8 C1 Ag4 39.8(6) . .
O5 Ag8 C1 Ag4 -170.2(3) . .
Ag7 Ag8 C1 Ag4 111.8(2) . .
O7 Ag8 C1 Ag3 47.0(15) . .
O5 Ag8 C1 Ag3 -163.0(11) . .
Ag4 Ag8 C1 Ag3 7.2(10) . .
Ag7 Ag8 C1 Ag3 119.0(12) . .
O7 Ag8 C1 Ag2 -61.8(6) . .
O5 Ag8 C1 Ag2 88.2(4) . .
Ag4 Ag8 C1 Ag2 -101.6(5) . .
Ag7 Ag8 C1 Ag2 10.2(3) . .
O4 Ag3 C1 C2 179.3(6) . .
O15 Ag3 C1 C2 -30.0(8) . .
O14 Ag3 C1 C2 72.3(8) . .
Ag4 Ag3 C1 C2 -173.5(8) . .
Ag4 Ag3 C1 C2 -80.0(7) 2_666 .
Ag2 Ag3 C1 C2 80.5(7) . .
O4 Ag3 C1 Ag4 -7.2(5) . .
O15 Ag3 C1 Ag4 143.5(3) . .
O14 Ag3 C1 Ag4 -114.3(3) . .
C2 Ag3 C1 Ag4 173.5(8) . .
Ag4 Ag3 C1 Ag4 93.5(3) 2_666 .
Ag2 Ag3 C1 Ag4 -106.0(4) . .
O4 Ag3 C1 Ag8 -14.3(14) . .
O15 Ag3 C1 Ag8 136.4(11) . .
O14 Ag3 C1 Ag8 -121.4(11) . .
C2 Ag3 C1 Ag8 166.4(17) . .
Ag4 Ag3 C1 Ag8 -7.1(10) . .
Ag4 Ag3 C1 Ag8 86.3(12) 2_666 .
Ag2 Ag3 C1 Ag8 -113.2(13) . .
O4 Ag3 C1 Ag2 98.8(4) . .
O15 Ag3 C1 Ag2 -110.4(4) . .
O14 Ag3 C1 Ag2 -8.2(5) . .
C2 Ag3 C1 Ag2 -80.5(7) . .
Ag4 Ag3 C1 Ag2 106.0(4) . .
Ag4 Ag3 C1 Ag2 -160.5(3) 2_666 .
O13 Ag2 C1 C2 -100.4(7) . .
C12 Ag2 C1 C2 129.2(7) . .
C9 Ag2 C1 C2 14.6(7) . .
Ag1 Ag2 C1 C2 166.1(6) . .
Ag7 Ag2 C1 C2 107.7(6) . .
Ag3 Ag2 C1 C2 -84.4(7) . .
O13 Ag2 C1 Ag4 61.0(5) . .
C12 Ag2 C1 Ag4 -69.4(6) . .
C2 Ag2 C1 Ag4 161.5(9) . .
C9 Ag2 C1 Ag4 176.1(4) . .
Ag1 Ag2 C1 Ag4 -32.5(4) . .
Ag7 Ag2 C1 Ag4 -90.8(3) . .
Ag3 Ag2 C1 Ag4 77.1(3) . .
O13 Ag2 C1 Ag8 141.0(4) . .
C12 Ag2 C1 Ag8 10.6(7) . .
C2 Ag2 C1 Ag8 -118.6(8) . .
C9 Ag2 C1 Ag8 -103.9(4) . .
Ag1 Ag2 C1 Ag8 47.5(4) . .
Ag7 Ag2 C1 Ag8 -10.8(3) . .
Ag3 Ag2 C1 Ag8 157.1(6) . .
O13 Ag2 C1 Ag3 -16.0(5) . .
C12 Ag2 C1 Ag3 -146.4(4) . .
C2 Ag2 C1 Ag3 84.4(7) . .
C9 Ag2 C1 Ag3 99.0(3) . .
Ag1 Ag2 C1 Ag3 -109.6(2) . .
Ag7 Ag2 C1 Ag3 -167.9(2) . .
Ag4 C1 C2 Ag2 -105(3) . .
Ag8 C1 C2 Ag2 101.9(7) . .
Ag3 C1 C2 Ag2 -84.5(3) . .
Ag4 C1 C2 Ag3 -20(3) . .
Ag8 C1 C2 Ag3 -173.6(8) . .
Ag2 C1 C2 Ag3 84.5(3) . .
C12 Ag2 C2 C1 -85.0(9) . .
C9 Ag2 C2 C1 -165.3(7) . .
Ag1 Ag2 C2 C1 -18.1(8) . .
Ag7 Ag2 C2 C1 -73.8(6) . .
Ag3 Ag2 C2 C1 71.2(6) . .
O13 Ag2 C2 C3 -87.8(8) . .
C1 Ag2 C2 C3 173.4(11) . .
C12 Ag2 C2 C3 88.3(9) . .
C9 Ag2 C2 C3 8.0(7) . .
Ag1 Ag2 C2 C3 155.2(6) . .
Ag7 Ag2 C2 C3 99.6(7) . .
Ag3 Ag2 C2 C3 -115.5(8) . .
O13 Ag2 C2 Ag3 27.7(4) . .
C1 Ag2 C2 Ag3 -71.2(6) . .
C12 Ag2 C2 Ag3 -156.2(5) . .
C9 Ag2 C2 Ag3 123.5(3) . .
Ag1 Ag2 C2 Ag3 -89.3(3) . .
Ag7 Ag2 C2 Ag3 -144.97(15) . .
O4 Ag3 C2 C1 -1.3(12) . .
O15 Ag3 C2 C1 156.6(7) . .
O14 Ag3 C2 C1 -120.9(7) . .
Ag4 Ag3 C2 C1 4.8(6) . .
Ag4 Ag3 C2 C1 91.9(7) 2_666 .
Ag2 Ag3 C2 C1 -74.9(7) . .
O4 Ag3 C2 C3 -174.6(8) . .
O15 Ag3 C2 C3 -16.8(8) . .
O14 Ag3 C2 C3 65.7(8) . .
C1 Ag3 C2 C3 -173.4(12) . .
Ag4 Ag3 C2 C3 -168.5(8) . .
Ag4 Ag3 C2 C3 -81.4(7) 2_666 .
Ag2 Ag3 C2 C3 111.7(8) . .
O4 Ag3 C2 Ag2 73.7(8) . .
O15 Ag3 C2 Ag2 -128.5(3) . .
O14 Ag3 C2 Ag2 -46.0(3) . .
C1 Ag3 C2 Ag2 74.9(7) . .
Ag4 Ag3 C2 Ag2 79.76(19) . .
Ag4 Ag3 C2 Ag2 166.9(2) 2_666 .
C10 C11 C12 Ag1 161(3) . .
Ag6 C11 C12 Ag1 -24(4) 2 .
C10 C11 C12 Ag7 -74(4) . .
Ag6 C11 C12 Ag7 101.7(4) 2 .
C10 C11 C12 Ag6 -176(4) . 2
C10 C11 C12 Ag2 6(4) . .
Ag6 C11 C12 Ag2 -178.5(5) 2 .
N1 Ag1 C12 C11 -177(3) . .
O9 Ag1 C12 C11 39(4) . .
Ag2 Ag1 C12 C11 -156(4) . .
Ag7 Ag1 C12 C11 128(4) . .
Ag9 Ag1 C12 C11 -64(4) . .
Ag6 Ag1 C12 C11 23(4) 2 .
N1 Ag1 C12 Ag7 54.8(19) . .
O9 Ag1 C12 Ag7 -89.1(3) . .
Ag2 Ag1 C12 Ag7 75.8(2) . .
Ag9 Ag1 C12 Ag7 168.3(4) . .
Ag6 Ag1 C12 Ag7 -105.0(4) 2 .
N1 Ag1 C12 Ag6 159.9(17) . 2
O9 Ag1 C12 Ag6 15.9(4) . 2
Ag2 Ag1 C12 Ag6 -179.1(4) . 2
Ag7 Ag1 C12 Ag6 105.0(4) . 2
Ag9 Ag1 C12 Ag6 -86.7(3) . 2
N1 Ag1 C12 Ag2 -21.0(19) . .
O9 Ag1 C12 Ag2 -164.9(3) . .
Ag7 Ag1 C12 Ag2 -75.8(2) . .
Ag9 Ag1 C12 Ag2 92.4(3) . .
Ag6 Ag1 C12 Ag2 179.1(4) 2 .
O6 Ag7 C12 C11 58.8(9) . .
O8 Ag7 C12 C11 -131.6(7) . .
O10 Ag7 C12 C11 -56.4(8) 2 .
Ag1 Ag7 C12 C11 -169.2(9) . .
Ag2 Ag7 C12 C11 110.4(8) . .
Ag8 Ag7 C12 C11 143.0(7) . .
O6 Ag7 C12 Ag1 -132.0(4) . .
O8 Ag7 C12 Ag1 37.6(4) . .
O10 Ag7 C12 Ag1 112.8(3) 2 .
Ag2 Ag7 C12 Ag1 -80.4(3) . .
Ag8 Ag7 C12 Ag1 -47.8(4) . .
O6 Ag7 C12 Ag6 134.2(4) . 2
O8 Ag7 C12 Ag6 -56.2(4) . 2
O10 Ag7 C12 Ag6 19.0(4) 2 2
Ag1 Ag7 C12 Ag6 -93.8(4) . 2
Ag2 Ag7 C12 Ag6 -174.2(5) . 2
Ag8 Ag7 C12 Ag6 -141.6(2) . 2
O6 Ag7 C12 Ag2 -51.6(5) . .
O8 Ag7 C12 Ag2 118.0(3) . .
O10 Ag7 C12 Ag2 -166.8(2) 2 .
Ag1 Ag7 C12 Ag2 80.4(3) . .
Ag8 Ag7 C12 Ag2 32.6(4) . .
O13 Ag2 C12 C11 90.1(8) . .
C1 Ag2 C12 C11 -129.3(8) . .
C2 Ag2 C12 C11 -86.7(10) . .
C9 Ag2 C12 C11 -12.3(9) . .
Ag1 Ag2 C12 C11 174.3(10) . .
Ag7 Ag2 C12 C11 -101.1(9) . .
Ag3 Ag2 C12 C11 143.3(7) . .
O13 Ag2 C12 Ag1 -84.3(3) . .
C1 Ag2 C12 Ag1 56.3(6) . .
C2 Ag2 C12 Ag1 99.0(6) . .
C9 Ag2 C12 Ag1 173.4(3) . .
Ag7 Ag2 C12 Ag1 84.5(3) . .
Ag3 Ag2 C12 Ag1 -31.0(7) . .
O13 Ag2 C12 Ag7 -168.8(3) . .
C1 Ag2 C12 Ag7 -28.2(6) . .
C2 Ag2 C12 Ag7 14.4(7) . .
C9 Ag2 C12 Ag7 88.9(3) . .
Ag1 Ag2 C12 Ag7 -84.5(3) . .
Ag3 Ag2 C12 Ag7 -115.5(5) . .
C1 Ag4 O3 C13 -14.3(15) . .
O16 Ag4 O3 C13 162.5(13) 2_666 .
Ag8 Ag4 O3 C13 -149.8(9) . .
Ag3 Ag4 O3 C13 -2.1(12) . .
Ag3 Ag4 O3 C13 92.4(12) 2_666 .
O15 Ag3 O4 C13 -162.4(10) . .
O14 Ag3 O4 C13 121.1(10) . .
C1 Ag3 O4 C13 -4.8(12) . .
C2 Ag3 O4 C13 -4.0(15) . .
Ag4 Ag3 O4 C13 -9.9(9) . .
Ag4 Ag3 O4 C13 -89.2(10) 2_666 .
Ag2 Ag3 O4 C13 53.3(10) . .
O7 Ag8 O5 C15 114.6(8) . .
C1 Ag8 O5 C15 -46.7(8) . .
Ag4 Ag8 O5 C15 -72.6(11) . .
Ag7 Ag8 O5 C15 35.7(7) . .
O7 Ag8 O5 Ag5 -51.3(4) . 1_455
C1 Ag8 O5 Ag5 147.4(4) . 1_455
Ag4 Ag8 O5 Ag5 121.5(6) . 1_455
Ag7 Ag8 O5 Ag5 -130.3(4) . 1_455
C12 Ag7 O6 C15 172.0(9) . .
O8 Ag7 O6 C15 4.1(11) . .
O10 Ag7 O6 C15 -75.5(10) 2 .
Ag1 Ag7 O6 C15 109.7(10) . .
Ag2 Ag7 O6 C15 132.2(10) . .
Ag8 Ag7 O6 C15 55.6(10) . .
C1 Ag8 O7 C17 66.7(12) . .
O5 Ag8 O7 C17 -86.5(10) . .
Ag4 Ag8 O7 C17 95.6(10) . .
Ag7 Ag8 O7 C17 -7.7(10) . .
O6 Ag7 O8 C17 39.2(10) . .
C12 Ag7 O8 C17 -130.8(9) . .
O10 Ag7 O8 C17 135.4(10) 2 .
Ag1 Ag7 O8 C17 -103.8(9) . .
Ag2 Ag7 O8 C17 -72.4(9) . .
Ag8 Ag7 O8 C17 -7.8(9) . .
O6 Ag7 O8 Ag6 -124.5(3) . .
C12 Ag7 O8 Ag6 65.5(4) . .
O10 Ag7 O8 Ag6 -28.3(3) 2 .
Ag1 Ag7 O8 Ag6 92.6(2) . .
Ag2 Ag7 O8 Ag6 123.89(19) . .
Ag8 Ag7 O8 Ag6 -171.5(3) . .
O10 Ag6 O8 C17 -130.6(11) 2 .
C11 Ag6 O8 C17 31.2(12) 2 .
C12 Ag6 O8 C17 26.4(16) 2 .
Ag6 Ag6 O8 C17 156.1(11) 2 .
Ag1 Ag6 O8 C17 -129.5(10) 2 .
O10 Ag6 O8 Ag7 30.6(3) 2 .
C11 Ag6 O8 Ag7 -167.5(3) 2 .
C12 Ag6 O8 Ag7 -172.4(8) 2 .
Ag6 Ag6 O8 Ag7 -42.7(2) 2 .
Ag1 Ag6 O8 Ag7 31.7(7) 2 .
C12 Ag1 O9 C19 -76.0(11) . .
N1 Ag1 O9 C19 112.2(11) . .
Ag2 Ag1 O9 C19 -110.0(10) . .
Ag7 Ag1 O9 C19 -130.2(10) . .
Ag9 Ag1 O9 C19 -17.7(11) . .
Ag6 Ag1 O9 C19 -62.9(10) 2 .
O12 Ag9 O11 C21 -35.9(18) 2_655 .
O13 Ag9 O11 C21 103.3(12) . .
Ag9 Ag9 O11 C21 -14.5(11) 2_655 .
Ag1 Ag9 O11 C21 175.2(13) . .
C1 Ag2 O13 C23 39.9(11) . .
C12 Ag2 O13 C23 -172.0(10) . .
C2 Ag2 O13 C23 5.9(11) . .
C9 Ag2 O13 C23 -75.6(10) . .
Ag1 Ag2 O13 C23 143.8(10) . .
Ag7 Ag2 O13 C23 175.0(8) . .
Ag3 Ag2 O13 C23 27.8(9) . .
C1 Ag2 O13 Ag9 -148.9(3) . .
C12 Ag2 O13 Ag9 -0.9(4) . .
C2 Ag2 O13 Ag9 177.0(3) . .
C9 Ag2 O13 Ag9 95.5(4) . .
Ag1 Ag2 O13 Ag9 -45.1(3) . .
Ag7 Ag2 O13 Ag9 -13.9(5) . .
Ag3 Ag2 O13 Ag9 -161.1(3) . .
O12 Ag9 O13 C23 69.8(11) 2_655 .
O11 Ag9 O13 C23 -92.5(11) . .
Ag9 Ag9 O13 C23 -15.4(11) 2_655 .
Ag1 Ag9 O13 C23 -149.3(11) . .
O12 Ag9 O13 Ag2 -100.4(4) 2_655 .
O11 Ag9 O13 Ag2 97.3(4) . .
Ag9 Ag9 O13 Ag2 174.44(18) 2_655 .
Ag1 Ag9 O13 Ag2 40.5(2) . .
O4 Ag3 O14 C23 -92.5(9) . .
O15 Ag3 O14 C23 166.7(9) . .
C1 Ag3 O14 C23 36.9(10) . .
C2 Ag3 O14 C23 65.4(9) . .
Ag4 Ag3 O14 C23 -19.4(10) . .
Ag4 Ag3 O14 C23 156.4(7) 2_666 .
Ag2 Ag3 O14 C23 30.5(8) . .
O4 Ag3 O14 Ag5 74.3(3) . .
O15 Ag3 O14 Ag5 -26.5(3) . .
C1 Ag3 O14 Ag5 -156.3(3) . .
C2 Ag3 O14 Ag5 -127.9(3) . .
Ag4 Ag3 O14 Ag5 147.40(13) . .
Ag4 Ag3 O14 Ag5 -36.8(5) 2_666 .
Ag2 Ag3 O14 Ag5 -162.7(3) . .
O5 Ag5 O14 C23 -14.2(13) 1_655 .
O15 Ag5 O14 C23 -170.5(12) . .
O1W Ag5 O14 C23 79.8(12) 2_766 .
O1W Ag5 O14 C23 139.0(11) . .
O5 Ag5 O14 Ag3 -177.5(3) 1_655 .
O15 Ag5 O14 Ag3 26.2(3) . .
O1W Ag5 O14 Ag3 -83.4(3) 2_766 .
O1W Ag5 O14 Ag3 -24.3(6) . .
O4 Ag3 O15 C25 151.8(8) . .
O14 Ag3 O15 C25 -127.6(9) . .
C1 Ag3 O15 C25 -4.8(10) . .
C2 Ag3 O15 C25 -18.8(9) . .
Ag4 Ag3 O15 C25 62.7(11) . .
Ag4 Ag3 O15 C25 46.8(8) 2_666 .
Ag2 Ag3 O15 C25 -68.9(9) . .
O4 Ag3 O15 Ag5 -53.1(4) . .
O14 Ag3 O15 Ag5 27.4(3) . .
C1 Ag3 O15 Ag5 150.3(3) . .
C2 Ag3 O15 Ag5 136.3(3) . .
Ag4 Ag3 O15 Ag5 -142.2(3) . .
Ag4 Ag3 O15 Ag5 -158.2(3) 2_666 .
Ag2 Ag3 O15 Ag5 86.2(3) . .
O5 Ag5 O15 C25 1.1(16) 1_655 .
O1W Ag5 O15 C25 -156.5(11) 2_766 .
O1W Ag5 O15 C25 -86.3(11) . .
O14 Ag5 O15 C25 119.7(12) . .
O5 Ag5 O15 Ag3 -145.1(6) 1_655 .
O1W Ag5 O15 Ag3 57.3(4) 2_766 .
O1W Ag5 O15 Ag3 127.5(4) . .
O14 Ag5 O15 Ag3 -26.5(3) . .
O5 Ag5 O1W Ag5 92.5(3) 1_655 2_766
O15 Ag5 O1W Ag5 -111.9(4) . 2_766
O1W Ag5 O1W Ag5 0.0 2_766 2_766
O14 Ag5 O1W Ag5 -63.4(6) . 2_766
C12 Ag1 N1 C27 -178(3) . .
O9 Ag1 N1 C27 -33(4) . .
Ag2 Ag1 N1 C27 163(4) . .
Ag7 Ag1 N1 C27 -131(4) . .
Ag9 Ag1 N1 C27 78(4) . .
Ag6 Ag1 N1 C27 -25(4) 2 .
C4 O1 C3 C2 -69.6(11) . .
Ag2 C2 C3 O1 50.3(10) . .
Ag3 C2 C3 O1 -39.3(10) . .
C3 O1 C4 C5 164.2(9) . .
C3 O1 C4 C9 -16.9(14) . .
O1 C4 C5 C6 178.0(10) . .
C9 C4 C5 C6 -0.9(16) . .
C4 C5 C6 C7 -1.5(17) . .
C5 C6 C7 C8 2.1(17) . .
C10 O2 C8 C7 -54.8(13) . .
C10 O2 C8 C9 130.6(10) . .
C6 C7 C8 O2 -174.7(10) . .
C6 C7 C8 C9 -0.3(16) . .
O2 C8 C9 C4 172.8(8) . .
C7 C8 C9 C4 -1.9(14) . .
O2 C8 C9 Ag2 -90.9(8) . .
C7 C8 C9 Ag2 94.4(9) . .
O1 C4 C9 C8 -176.3(9) . .
C5 C4 C9 C8 2.5(14) . .
O1 C4 C9 Ag2 83.4(9) . .
C5 C4 C9 Ag2 -97.7(9) . .
O13 Ag2 C9 C8 -56.6(7) . .
C1 Ag2 C9 C8 173.9(6) . .
C12 Ag2 C9 C8 33.4(7) . .
C2 Ag2 C9 C8 -179.0(7) . .
Ag1 Ag2 C9 C8 40.6(8) . .
Ag7 Ag2 C9 C8 84.3(6) . .
Ag3 Ag2 C9 C8 -136.5(6) . .
O13 Ag2 C9 C4 61.5(7) . .
C1 Ag2 C9 C4 -67.9(7) . .
C12 Ag2 C9 C4 151.6(6) . .
C2 Ag2 C9 C4 -60.8(6) . .
Ag1 Ag2 C9 C4 158.8(5) . .
Ag7 Ag2 C9 C4 -157.6(6) . .
Ag3 Ag2 C9 C4 -18.3(7) . .
C8 O2 C10 C11 -68.5(12) . .
C12 C11 C10 O2 20(4) . .
Ag6 C11 C10 O2 -155.6(7) 2 .
Ag4 O3 C13 O4 -6(2) . .
Ag4 O3 C13 C14 -175.7(11) . .
Ag3 O4 C13 O3 13(2) . .
Ag3 O4 C13 C14 -178.1(10) . .
O3 C13 C14 F7 -170.3(17) . .
O4 C13 C14 F7 19(2) . .
O3 C13 C14 F9 -40(2) . .
O4 C13 C14 F9 149.4(15) . .
O3 C13 C14 F8 72.4(19) . .
O4 C13 C14 F8 -98.4(16) . .
Ag8 O5 C15 O6 -12.4(15) . .
Ag5 O5 C15 O6 150.9(9) 1_455 .
Ag8 O5 C15 C16 170.8(7) . .
Ag5 O5 C15 C16 -25.9(15) 1_455 .
Ag7 O6 C15 O5 -44.4(17) . .
Ag7 O6 C15 C16 132.5(8) . .
O5 C15 C16 F18' -158.2(16) . .
O6 C15 C16 F18' 24.5(18) . .
O5 C15 C16 F17' -35.2(19) . .
O6 C15 C16 F17' 147.6(17) . .
O5 C15 C16 F16' 83.5(18) . .
O6 C15 C16 F16' -93.8(17) . .
O5 C15 C16 F16 121.2(13) . .
O6 C15 C16 F16 -56.0(15) . .
O5 C15 C16 F17 -1.5(15) . .
O6 C15 C16 F17 -178.7(13) . .
O5 C15 C16 F18 -119.7(13) . .
O6 C15 C16 F18 63.1(14) . .
Ag8 O7 C17 O8 4.3(19) . .
Ag8 O7 C17 C18 -171.6(9) . .
Ag7 O8 C17 O7 5.1(19) . .
Ag6 O8 C17 O7 161.8(10) . .
Ag7 O8 C17 C18 -179.1(9) . .
Ag6 O8 C17 C18 -22.3(17) . .
O7 C17 C18 F13 85.9(16) . .
O8 C17 C18 F13 -90.6(15) . .
O7 C17 C18 F14 -31.3(19) . .
O8 C17 C18 F14 152.2(13) . .
O7 C17 C18 F15 -151.3(13) . .
O8 C17 C18 F15 32.2(19) . .
Ag1 O9 C19 O10 79.3(15) . .
Ag1 O9 C19 C20 -111.1(10) . .
Ag6 O10 C19 O9 -26.3(16) 2 .
Ag7 O10 C19 O9 90.9(14) 2 .
Ag6 O10 C19 C20 163.8(7) 2 .
Ag7 O10 C19 C20 -79.0(12) 2 .
O9 C19 C20 F12' -139(3) . .
O10 C19 C20 F12' 31(3) . .
O9 C19 C20 F10' 99(3) . .
O10 C19 C20 F10' -91(3) . .
O9 C19 C20 F11' -19(3) . .
O10 C19 C20 F11' 151(3) . .
O9 C19 C20 F11 17.0(17) . .
O10 C19 C20 F11 -172.8(12) . .
O9 C19 C20 F12 -101.9(15) . .
O10 C19 C20 F12 68.3(14) . .
O9 C19 C20 F10 138.0(14) . .
O10 C19 C20 F10 -51.8(15) . .
Ag9 O12 C21 O11 3(2) 2_655 .
Ag9 O12 C21 C22 178.0(9) 2_655 .
Ag9 O11 C21 O12 13(2) . .
Ag9 O11 C21 C22 -162.3(9) . .
O12 C21 C22 F20 14.4(17) . .
O11 C21 C22 F20 -170.0(14) . .
O12 C21 C22 F19 137.2(14) . .
O11 C21 C22 F19 -47.2(17) . .
O12 C21 C22 F21 -105.1(14) . .
O11 C21 C22 F21 70.5(16) . .
O12 C21 C22 F21' -172(3) . .
O11 C21 C22 F21' 3(3) . .
O12 C21 C22 F20' -37(3) . .
O11 C21 C22 F20' 139(3) . .
O12 C21 C22 F19' 74(2) . .
O11 C21 C22 F19' -111(2) . .
Ag3 O14 C23 O13 -21.9(17) . .
Ag5 O14 C23 O13 178.2(9) . .
Ag3 O14 C23 C24 159.5(7) . .
Ag5 O14 C23 C24 -0.5(17) . .
Ag2 O13 C23 O14 -13.7(18) . .
Ag9 O13 C23 O14 178.1(9) . .
Ag2 O13 C23 C24 164.9(7) . .
Ag9 O13 C23 C24 -3.3(16) . .
O14 C23 C24 F3' -164.4(18) . .
O13 C23 C24 F3' 17(2) . .
O14 C23 C24 F1' 73.4(19) . .
O13 C23 C24 F1' -105.4(18) . .
O14 C23 C24 F2' -41.2(19) . .
O13 C23 C24 F2' 140.0(17) . .
O14 C23 C24 F2 13.8(15) . .
O13 C23 C24 F2 -165.0(11) . .
O14 C23 C24 F3 -106.9(12) . .
O13 C23 C24 F3 74.3(13) . .
O14 C23 C24 F1 136.4(11) . .
O13 C23 C24 F1 -42.4(14) . .
Ag4 O16 C25 O15 -6.5(16) 2_666 .
Ag4 O16 C25 C26 170.2(7) 2_666 .
Ag3 O15 C25 O16 -41.9(15) . .
Ag5 O15 C25 O16 176.0(8) . .
Ag3 O15 C25 C26 141.5(8) . .
Ag5 O15 C25 C26 -0.6(17) . .
O16 C25 C26 F4' -96.4(19) . .
O15 C25 C26 F4' 81(2) . .
O16 C25 C26 F6 103.8(19) . .
O15 C25 C26 F6 -79(2) . .
O16 C25 C26 F6' 38(2) . .
O15 C25 C26 F6' -145.1(17) . .
O16 C25 C26 F4 -41.0(18) . .
O15 C25 C26 F4 136.1(15) . .
O16 C25 C26 F5 -142.5(16) . .
O15 C25 C26 F5 35(2) . .
O16 C25 C26 F5' 147.8(15) . .
O15 C25 C26 F5' -35.1(19) . .
