#------------------------------------------------------------------------------
#$Date: 2016-03-21 06:51:35 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178537 $
#$URL: svn://www.crystallography.net/cod/cif/4/06/43/4064318.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4064318
loop_
_publ_author_name
'Cui, Peng'
'Chen, Yaofeng'
'Li, Guangyu'
'Xia, Wei'
_publ_section_title
;
 Versatile Reactivities ofansa-Heteroborabenzene Divalent Ytterbium Amide
 toward Alkali-Metal Salts and the Generation of Heterometallic
 Ytterbium−Alkali-Metal Boratabenzene Complexes
;
_journal_issue                   7
_journal_name_full               Organometallics
_journal_page_first              2012
_journal_paper_doi               10.1021/om200040z
_journal_volume                  30
_journal_year                    2011
_chemical_formula_sum            'C30 H66 B2 Li4 N4 Si4'
_chemical_formula_weight         644.61
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                112.587(2)
_cell_angle_beta                 103.302(2)
_cell_angle_gamma                93.817(2)
_cell_formula_units_Z            2
_cell_length_a                   8.9337(12)
_cell_length_b                   14.898(2)
_cell_length_c                   18.102(3)
_cell_measurement_reflns_used    4234
_cell_measurement_temperature    133(2)
_cell_measurement_theta_max      28.01
_cell_measurement_theta_min      2.33
_cell_volume                     2132.4(5)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      133(2)
_diffrn_measured_fraction_theta_full 0.981
_diffrn_measured_fraction_theta_max 0.981
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0373
_diffrn_reflns_av_sigmaI/netI    0.0705
_diffrn_reflns_limit_h_max       10
_diffrn_reflns_limit_h_min       -10
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            12903
_diffrn_reflns_theta_full        25.05
_diffrn_reflns_theta_max         25.05
_diffrn_reflns_theta_min         1.50
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.162
_exptl_absorpt_correction_T_max  0.9683
_exptl_absorpt_correction_T_min  0.9455
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   sadabs
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.004
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             704
_exptl_crystal_size_max          0.35
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.487
_refine_diff_density_min         -0.357
_refine_diff_density_rms         0.097
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.061
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     413
_refine_ls_number_reflns         7417
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.061
_refine_ls_R_factor_all          0.0936
_refine_ls_R_factor_gt           0.0612
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1379P)²+0.1305P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1804
_refine_ls_wR_factor_ref         0.2195
_reflns_number_gt                5211
_reflns_number_total             7417
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om200040z_si_001.cif
_cod_data_source_block           mo_dm10144_0m
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        2132.3(5)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4064318
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Li1 Li 0.7060(7) 0.2536(4) 0.3885(4) 0.0285(14) Uani 1 1 d .
Li2 Li 0.8078(8) 0.3046(5) 0.5743(4) 0.0341(15) Uani 1 1 d .
Li3 Li 0.7267(8) 0.5027(5) 0.7569(4) 0.0347(15) Uani 1 1 d .
Li4 Li 0.5682(7) 0.6739(5) 0.7642(4) 0.0304(14) Uani 1 1 d .
N1 N 0.5411(4) 0.0863(2) 0.1775(2) 0.0307(7) Uani 1 1 d .
N2 N 0.8367(3) 0.21325(19) 0.46904(17) 0.0176(6) Uani 1 1 d .
N3 N 0.8200(4) 0.2763(2) 0.7633(2) 0.0354(8) Uani 1 1 d .
N4 N 0.6925(3) 0.6239(2) 0.83913(17) 0.0204(6) Uani 1 1 d .
Si1 Si 0.74730(10) 0.10069(6) 0.45681(6) 0.0197(3) Uani 1 1 d .
Si2 Si 1.02860(10) 0.24194(7) 0.47446(6) 0.0212(3) Uani 1 1 d .
Si3 Si 0.86869(11) 0.70239(7) 0.88705(6) 0.0261(3) Uani 1 1 d .
Si4 Si 0.58144(11) 0.59005(8) 0.89310(7) 0.0276(3) Uani 1 1 d .
B1 B 0.5540(5) 0.1826(3) 0.2405(3) 0.0249(9) Uani 1 1 d .
B2 B 0.7958(5) 0.3352(3) 0.7180(3) 0.0267(9) Uani 1 1 d .
C1 C 0.6773(4) 0.2715(3) 0.2599(2) 0.0266(8) Uani 1 1 d .
H1A H 0.7576 0.2605 0.2322 0.032 Uiso 1 1 d R
C2 C 0.6851(4) 0.3632(3) 0.3237(2) 0.0288(9) Uani 1 1 d .
H2A H 0.7742 0.4120 0.3383 0.035 Uiso 1 1 d R
C3 C 0.5820(4) 0.3802(3) 0.3745(2) 0.0292(8) Uani 1 1 d .
H3A H 0.5982 0.4427 0.4202 0.035 Uiso 1 1 d R
C4 C 0.4646(4) 0.3033(3) 0.3594(2) 0.0283(8) Uani 1 1 d .
H4A H 0.4042 0.3126 0.3981 0.034 Uiso 1 1 d R
C5 C 0.4465(4) 0.2099(3) 0.2978(2) 0.0270(8) Uani 1 1 d .
H5A H 0.3765 0.1579 0.2967 0.032 Uiso 1 1 d R
C6 C 0.6408(5) 0.0640(3) 0.1201(3) 0.0386(10) Uani 1 1 d .
H6A H 0.6711 0.1241 0.1122 0.046 Uiso 1 1 calc R
H6B H 0.5798 0.0127 0.0652 0.046 Uiso 1 1 calc R
C7 C 0.7879(5) 0.0281(3) 0.1518(3) 0.0465(11) Uani 1 1 d .
H7A H 0.8508 0.0796 0.2051 0.070 Uiso 1 1 calc R
H7B H 0.8488 0.0132 0.1112 0.070 Uiso 1 1 calc R
H7C H 0.7587 -0.0317 0.1595 0.070 Uiso 1 1 calc R
C8 C 0.4358(5) 0.0003(3) 0.1686(3) 0.0408(10) Uani 1 1 d .
H8A H 0.4204 0.0109 0.2236 0.049 Uiso 1 1 calc R
H8B H 0.4856 -0.0589 0.1502 0.049 Uiso 1 1 calc R
C9 C 0.2766(6) -0.0188(4) 0.1062(4) 0.0615(15) Uani 1 1 d .
H9A H 0.2186 0.0341 0.1289 0.092 Uiso 1 1 calc R
H9B H 0.2176 -0.0823 0.0960 0.092 Uiso 1 1 calc R
H9C H 0.2914 -0.0204 0.0538 0.092 Uiso 1 1 calc R
C10 C 0.5377(4) 0.1046(3) 0.4557(3) 0.0321(9) Uani 1 1 d .
H10A H 0.5318 0.1468 0.5115 0.048 Uiso 1 1 calc R
H10B H 0.4827 0.0377 0.4389 0.048 Uiso 1 1 calc R
H10C H 0.4890 0.1314 0.4161 0.048 Uiso 1 1 calc R
C11 C 0.8364(4) 0.0674(3) 0.5456(2) 0.0305(9) Uani 1 1 d .
H11A H 0.9441 0.0580 0.5459 0.046 Uiso 1 1 calc R
H11B H 0.7754 0.0061 0.5388 0.046 Uiso 1 1 calc R
H11C H 0.8361 0.1206 0.5983 0.046 Uiso 1 1 calc R
C12 C 0.7442(5) -0.0042(3) 0.3570(2) 0.0321(9) Uani 1 1 d .
H12A H 0.6980 0.0119 0.3100 0.048 Uiso 1 1 calc R
H12B H 0.6818 -0.0641 0.3518 0.048 Uiso 1 1 calc R
H12C H 0.8511 -0.0152 0.3570 0.048 Uiso 1 1 calc R
C13 C 1.1684(4) 0.2493(3) 0.5722(3) 0.0402(10) Uani 1 1 d .
H13A H 1.1407 0.2951 0.6207 0.060 Uiso 1 1 calc R
H13B H 1.2748 0.2730 0.5741 0.060 Uiso 1 1 calc R
H13C H 1.1627 0.1837 0.5729 0.060 Uiso 1 1 calc R
C14 C 1.0936(5) 0.1565(3) 0.3853(3) 0.0379(10) Uani 1 1 d .
H14A H 1.0796 0.0896 0.3831 0.057 Uiso 1 1 calc R
H14B H 1.2041 0.1789 0.3933 0.057 Uiso 1 1 calc R
H14C H 1.0311 0.1563 0.3331 0.057 Uiso 1 1 calc R
C15 C 1.0652(5) 0.3678(3) 0.4738(3) 0.0400(10) Uani 1 1 d .
H15A H 1.0157 0.3640 0.4182 0.060 Uiso 1 1 calc R
H15B H 1.1779 0.3903 0.4884 0.060 Uiso 1 1 calc R
H15C H 1.0210 0.4145 0.5146 0.060 Uiso 1 1 calc R
C16 C 0.6369(4) 0.3346(3) 0.6628(2) 0.0265(8) Uani 1 1 d .
H16A H 0.5528 0.2835 0.6502 0.032 Uiso 1 1 d R
C17 C 0.6199(4) 0.3946(3) 0.6192(2) 0.0294(8) Uani 1 1 d .
H17A H 0.5215 0.3839 0.5795 0.035 Uiso 1 1 d R
C18 C 0.7455(5) 0.4594(3) 0.6228(2) 0.0326(9) Uani 1 1 d .
H18A H 0.7315 0.4953 0.5885 0.039 Uiso 1 1 d R
C19 C 0.8949(5) 0.4656(3) 0.6725(3) 0.0342(9) Uani 1 1 d .
H19A H 0.9815 0.5028 0.6687 0.041 Uiso 1 1 d R
C20 C 0.9261(4) 0.4092(3) 0.7178(2) 0.0308(9) Uani 1 1 d .
H20A H 1.0321 0.4093 0.7441 0.037 Uiso 1 1 d R
C21 C 0.9672(6) 0.2867(4) 0.8232(3) 0.0506(13) Uani 1 1 d .
H21A H 0.9449 0.2769 0.8709 0.061 Uiso 1 1 calc R
H21B H 1.0246 0.3548 0.8445 0.061 Uiso 1 1 calc R
C22 C 1.0710(7) 0.2147(5) 0.7876(3) 0.0707(17) Uani 1 1 d .
H22A H 1.0170 0.1470 0.7684 0.106 Uiso 1 1 calc R
H22B H 1.1685 0.2264 0.8307 0.106 Uiso 1 1 calc R
H22C H 1.0946 0.2242 0.7405 0.106 Uiso 1 1 calc R
C23 C 0.6933(6) 0.2032(3) 0.7571(3) 0.0486(12) Uani 1 1 d .
H23A H 0.7392 0.1488 0.7671 0.058 Uiso 1 1 calc R
H23B H 0.6232 0.1750 0.6996 0.058 Uiso 1 1 calc R
C24 C 0.5964(7) 0.2440(4) 0.8176(4) 0.0601(14) Uani 1 1 d .
H24A H 0.5077 0.1932 0.8053 0.090 Uiso 1 1 calc R
H24B H 0.5579 0.3017 0.8118 0.090 Uiso 1 1 calc R
H24C H 0.6612 0.2633 0.8747 0.090 Uiso 1 1 calc R
C25 C 0.9273(4) 0.7447(3) 0.8109(3) 0.0385(10) Uani 1 1 d .
H25A H 0.9218 0.6872 0.7596 0.058 Uiso 1 1 calc R
H25B H 1.0344 0.7815 0.8352 0.058 Uiso 1 1 calc R
H25C H 0.8564 0.7874 0.7981 0.058 Uiso 1 1 calc R
C26 C 0.8656(5) 0.8172(3) 0.9781(3) 0.0456(11) Uani 1 1 d .
H26A H 0.7854 0.8521 0.9603 0.068 Uiso 1 1 calc R
H26B H 0.9679 0.8600 1.0002 0.068 Uiso 1 1 calc R
H26C H 0.8419 0.7995 1.0216 0.068 Uiso 1 1 calc R
C27 C 1.0340(5) 0.6456(3) 0.9249(3) 0.0446(11) Uani 1 1 d .
H27A H 1.0090 0.6212 0.9645 0.067 Uiso 1 1 calc R
H27B H 1.1294 0.6953 0.9524 0.067 Uiso 1 1 calc R
H27C H 1.0500 0.5905 0.8775 0.067 Uiso 1 1 calc R
C28 C 0.4988(6) 0.6936(4) 0.9598(3) 0.0564(13) Uani 1 1 d .
H28A H 0.5841 0.7429 1.0045 0.085 Uiso 1 1 calc R
H28B H 0.4286 0.6677 0.9841 0.085 Uiso 1 1 calc R
H28C H 0.4405 0.7242 0.9257 0.085 Uiso 1 1 calc R
C29 C 0.6918(5) 0.5335(4) 0.9601(3) 0.0505(13) Uani 1 1 d .
H29A H 0.7504 0.4869 0.9288 0.076 Uiso 1 1 calc R
H29B H 0.6183 0.4985 0.9768 0.076 Uiso 1 1 calc R
H29C H 0.7644 0.5855 1.0099 0.076 Uiso 1 1 calc R
C30 C 0.4073(5) 0.4961(3) 0.8173(3) 0.0414(11) Uani 1 1 d .
H30A H 0.3398 0.5264 0.7862 0.062 Uiso 1 1 calc R
H30B H 0.3489 0.4721 0.8477 0.062 Uiso 1 1 calc R
H30C H 0.4421 0.4407 0.7785 0.062 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Li Li -0.0003 0.0001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 Li1 C3 143.8(4) . .
N2 Li1 C4 140.7(4) . .
C3 Li1 C4 34.96(15) . .
N2 Li1 C2 147.1(3) . .
C3 Li1 C2 35.35(16) . .
C4 Li1 C2 62.47(19) . .
N2 Li1 C5 139.2(3) . .
C3 Li1 C5 62.34(19) . .
C4 Li1 C5 33.87(15) . .
C2 Li1 C5 73.6(2) . .
N2 Li1 C1 145.2(3) . .
C3 Li1 C1 62.9(2) . .
C4 Li1 C1 73.9(2) . .
C2 Li1 C1 34.15(15) . .
C5 Li1 C1 63.97(19) . .
N2 Li1 B1 139.5(3) . .
C3 Li1 B1 76.3(2) . .
C4 Li1 B1 64.06(19) . .
C2 Li1 B1 64.1(2) . .
C5 Li1 B1 36.71(16) . .
C1 Li1 B1 36.76(15) . .
N2 Li1 Si1 33.07(13) . .
C3 Li1 Si1 150.4(3) . .
C4 Li1 Si1 121.3(3) . .
C2 Li1 Si1 173.9(3) . .
C5 Li1 Si1 106.8(2) . .
C1 Li1 Si1 140.3(3) . .
B1 Li1 Si1 112.4(2) . .
N2 Li1 Si2 32.63(13) . .
C3 Li1 Si2 134.6(3) . .
C4 Li1 Si2 162.7(3) . .
C2 Li1 Si2 116.9(2) . .
C5 Li1 Si2 162.4(3) . .
C1 Li1 Si2 115.9(3) . .
B1 Li1 Si2 132.5(3) . .
Si1 Li1 Si2 61.15(11) . .
N2 Li1 Li2 38.98(19) . .
C3 Li1 Li2 105.9(3) . .
C4 Li1 Li2 107.4(3) . .
C2 Li1 Li2 127.5(3) . .
C5 Li1 Li2 128.3(3) . .
C1 Li1 Li2 159.5(3) . .
B1 Li1 Li2 162.3(3) . .
Si1 Li1 Li2 57.19(16) . .
Si2 Li1 Li2 58.18(16) . .
N2 Li2 C18 135.4(4) . .
N2 Li2 C19 140.6(4) . .
C18 Li2 C19 35.47(17) . .
N2 Li2 C17 137.8(4) . .
C18 Li2 C17 35.46(16) . .
C19 Li2 C17 63.0(2) . .
N2 Li2 C20 147.1(4) . .
C18 Li2 C20 63.1(2) . .
C19 Li2 C20 34.11(17) . .
C17 Li2 C20 74.4(2) . .
N2 Li2 C16 144.0(3) . .
C18 Li2 C16 63.2(2) . .
C19 Li2 C16 74.2(2) . .
C17 Li2 C16 34.39(16) . .
C20 Li2 C16 64.3(2) . .
N2 Li2 B2 147.9(4) . .
C18 Li2 B2 76.6(2) . .
C19 Li2 B2 64.3(2) . .
C17 Li2 B2 64.3(2) . .
C20 Li2 B2 36.99(17) . .
C16 Li2 B2 36.49(16) . .
N2 Li2 Si1 35.41(14) . .
C18 Li2 Si1 152.4(3) . .
C19 Li2 Si1 171.5(3) . .
C17 Li2 Si1 125.3(3) . .
C20 Li2 Si1 141.9(3) . .
C16 Li2 Si1 111.6(3) . .
B2 Li2 Si1 116.3(3) . .
N2 Li2 Si2 34.03(13) . .
C18 Li2 Si2 125.3(3) . .
C19 Li2 Si2 110.4(3) . .
C17 Li2 Si2 154.8(3) . .
C20 Li2 Si2 114.7(3) . .
C16 Li2 Si2 170.7(3) . .
B2 Li2 Si2 137.4(3) . .
Si1 Li2 Si2 63.00(13) . .
N2 Li2 Li1 39.00(19) . .
C18 Li2 Li1 99.0(3) . .
C19 Li2 Li1 122.0(3) . .
C17 Li2 Li1 101.3(3) . .
C20 Li2 Li1 155.3(3) . .
C16 Li2 Li1 125.0(3) . .
B2 Li2 Li1 161.0(3) . .
Si1 Li2 Li1 60.43(17) . .
Si2 Li2 Li1 60.08(17) . .
N4 Li3 C17 140.0(4) . .
N4 Li3 C18 132.5(4) . .
C17 Li3 C18 35.35(17) . .
N4 Li3 C19 134.4(4) . .
C17 Li3 C19 62.9(2) . .
C18 Li3 C19 35.21(18) . .
N4 Li3 C16 149.9(4) . .
C17 Li3 C16 34.65(16) . .
C18 Li3 C16 63.2(2) . .
C19 Li3 C16 74.5(2) . .
N4 Li3 C20 142.9(4) . .
C17 Li3 C20 74.2(2) . .
C18 Li3 C20 62.6(2) . .
C19 Li3 C20 33.91(17) . .
C16 Li3 C20 64.4(2) . .
N4 Li3 B2 150.8(4) . .
C17 Li3 B2 64.5(2) . .
C18 Li3 B2 76.4(2) . .
C19 Li3 B2 64.3(2) . .
C16 Li3 B2 36.73(16) . .
C20 Li3 B2 36.98(16) . .
N4 Li3 Si4 33.90(15) . .
C17 Li3 Si4 131.3(3) . .
C18 Li3 Si4 153.7(3) . .
C19 Li3 Si4 165.3(3) . .
C16 Li3 Si4 119.0(3) . .
C20 Li3 Si4 143.6(3) . .
B2 Li3 Si4 122.2(3) . .
N4 Li3 Si3 33.58(14) . .
C17 Li3 Si3 151.4(3) . .
C18 Li3 Si3 120.1(3) . .
C19 Li3 Si3 104.4(2) . .
C16 Li3 Si3 172.5(3) . .
C20 Li3 Si3 110.4(2) . .
B2 Li3 Si3 136.0(3) . .
Si4 Li3 Si3 61.43(13) . .
N4 Li3 Li4 40.5(2) . .
C17 Li3 Li4 101.2(3) . .
C18 Li3 Li4 95.6(3) . .
C19 Li3 Li4 116.3(3) . .
C16 Li3 Li4 127.6(3) . .
C20 Li3 Li4 149.0(3) . .
B2 Li3 Li4 164.3(3) . .
Si4 Li3 Li4 61.46(18) . .
Si3 Li3 Li4 59.69(17) . .
N4 Li4 C2 137.9(3) . 2_666
N4 Li4 C4 146.1(4) . 2_666
C2 Li4 C4 62.4(2) 2_666 2_666
N4 Li4 C3 140.6(3) . 2_666
C2 Li4 C3 35.16(16) 2_666 2_666
C4 Li4 C3 34.68(16) 2_666 2_666
N4 Li4 C5 148.4(3) . 2_666
C2 Li4 C5 73.7(2) 2_666 2_666
C4 Li4 C5 33.82(16) 2_666 2_666
C3 Li4 C5 61.9(2) 2_666 2_666
N4 Li4 C1 139.4(4) . 2_666
C2 Li4 C1 34.24(15) 2_666 2_666
C4 Li4 C1 73.9(2) 2_666 2_666
C3 Li4 C1 62.59(19) 2_666 2_666
C5 Li4 C1 64.06(19) 2_666 2_666
N4 Li4 B1 143.5(4) . 2_666
C2 Li4 B1 63.94(19) 2_666 2_666
C4 Li4 B1 63.7(2) 2_666 2_666
C3 Li4 B1 75.4(2) 2_666 2_666
C5 Li4 B1 36.55(16) 2_666 2_666
C1 Li4 B1 36.65(15) 2_666 2_666
N4 Li4 Si3 33.80(13) . .
C2 Li4 Si3 171.2(3) 2_666 .
C4 Li4 Si3 125.9(3) 2_666 .
C3 Li4 Si3 150.2(3) 2_666 .
C5 Li4 Si3 114.7(2) 2_666 .
C1 Li4 Si3 145.6(3) 2_666 .
B1 Li4 Si3 120.9(3) 2_666 .
N4 Li4 Li3 40.26(19) . .
C2 Li4 Li3 116.1(3) 2_666 .
C4 Li4 Li3 111.2(3) 2_666 .
C3 Li4 Li3 101.5(3) 2_666 .
C5 Li4 Li3 138.0(3) 2_666 .
C1 Li4 Li3 145.8(3) 2_666 .
B1 Li4 Li3 174.5(3) 2_666 .
Si3 Li4 Li3 59.90(17) . .
N4 Li4 Si4 32.09(14) . .
C2 Li4 Si4 110.6(2) 2_666 .
C4 Li4 Si4 165.4(3) 2_666 .
C3 Li4 Si4 132.7(3) 2_666 .
C5 Li4 Si4 160.1(3) 2_666 .
C1 Li4 Si4 108.0(2) 2_666 .
B1 Li4 Si4 126.5(3) 2_666 .
Si3 Li4 Si4 60.61(12) . .
Li3 Li4 Si4 58.86(18) . .
B1 N1 C8 122.6(3) . .
B1 N1 C6 122.5(3) . .
C8 N1 C6 114.8(3) . .
Si2 N2 Si1 125.05(16) . .
Si2 N2 Li2 106.2(2) . .
Si1 N2 Li2 103.3(2) . .
Si2 N2 Li1 109.3(2) . .
Si1 N2 Li1 108.5(2) . .
Li2 N2 Li1 102.0(3) . .
B2 N3 C21 123.3(4) . .
B2 N3 C23 121.9(4) . .
C21 N3 C23 114.7(4) . .
Si3 N4 Si4 122.88(17) . .
Si3 N4 Li3 107.6(2) . .
Si4 N4 Li3 106.9(3) . .
Si3 N4 Li4 106.9(2) . .
Si4 N4 Li4 110.7(2) . .
Li3 N4 Li4 99.3(3) . .
N2 Si1 C12 114.33(16) . .
N2 Si1 C10 109.77(15) . .
C12 Si1 C10 105.68(19) . .
N2 Si1 C11 112.41(15) . .
C12 Si1 C11 108.31(18) . .
C10 Si1 C11 105.81(18) . .
N2 Si1 Li2 41.29(17) . .
C12 Si1 Li2 155.49(19) . .
C10 Si1 Li2 85.83(18) . .
C11 Si1 Li2 88.52(19) . .
N2 Si1 Li1 38.43(14) . .
C12 Si1 Li1 96.89(18) . .
C10 Si1 Li1 83.39(17) . .
C11 Si1 Li1 149.14(17) . .
Li2 Si1 Li1 62.38(19) . .
N2 Si2 C14 115.08(16) . .
N2 Si2 C13 113.78(17) . .
C14 Si2 C13 106.6(2) . .
N2 Si2 C15 109.29(15) . .
C14 Si2 C15 105.5(2) . .
C13 Si2 C15 105.9(2) . .
N2 Si2 Li2 39.82(16) . .
C14 Si2 Li2 154.47(18) . .
C13 Si2 Li2 86.38(19) . .
C15 Si2 Li2 91.34(19) . .
N2 Si2 Li1 38.11(15) . .
C14 Si2 Li1 101.83(19) . .
C13 Si2 Li1 147.92(19) . .
C15 Si2 Li1 79.92(17) . .
Li2 Si2 Li1 61.74(19) . .
N4 Si3 C26 114.01(17) . .
N4 Si3 C27 114.52(18) . .
C26 Si3 C27 106.5(2) . .
N4 Si3 C25 109.23(16) . .
C26 Si3 C25 106.0(2) . .
C27 Si3 C25 105.9(2) . .
N4 Si3 Li4 39.32(15) . .
C26 Si3 Li4 103.41(19) . .
C27 Si3 Li4 147.6(2) . .
C25 Si3 Li4 76.97(18) . .
N4 Si3 Li3 38.86(16) . .
C26 Si3 Li3 152.2(2) . .
C27 Si3 Li3 87.2(2) . .
C25 Si3 Li3 92.66(19) . .
Li4 Si3 Li3 60.40(18) . .
N4 Si4 C29 112.25(18) . .
N4 Si4 C30 109.24(18) . .
C29 Si4 C30 107.6(2) . .
N4 Si4 C28 114.0(2) . .
C29 Si4 C28 108.3(2) . .
C30 Si4 C28 105.1(2) . .
N4 Si4 Li3 39.18(16) . .
C29 Si4 Li3 94.7(2) . .
C30 Si4 Li3 82.88(19) . .
C28 Si4 Li3 151.5(2) . .
N4 Si4 Li4 37.17(14) . .
C29 Si4 Li4 149.27(19) . .
C30 Si4 Li4 87.10(18) . .
C28 Si4 Li4 93.0(2) . .
Li3 Si4 Li4 59.68(18) . .
N1 B1 C5 123.9(3) . .
N1 B1 C1 124.5(4) . .
C5 B1 C1 111.6(3) . .
N1 B1 Li1 129.2(3) . .
C5 B1 Li1 68.9(2) . .
C1 B1 Li1 69.2(3) . .
N1 B1 Li4 131.1(3) . 2_666
C5 B1 Li4 68.4(2) . 2_666
C1 B1 Li4 68.4(2) . 2_666
Li1 B1 Li4 99.7(3) . 2_666
N3 B2 C16 124.3(4) . .
N3 B2 C20 124.4(4) . .
C16 B2 C20 111.3(3) . .
N3 B2 Li3 130.8(3) . .
C16 B2 Li3 67.9(3) . .
C20 B2 Li3 68.7(3) . .
N3 B2 Li2 131.4(3) . .
C16 B2 Li2 68.5(3) . .
C20 B2 Li2 67.9(3) . .
Li3 B2 Li2 97.9(3) . .
C2 C1 B1 121.4(3) . .
C2 C1 Li4 70.6(3) . 2_666
B1 C1 Li4 74.9(2) . 2_666
C2 C1 Li1 70.6(3) . .
B1 C1 Li1 74.0(3) . .
Li4 C1 Li1 104.3(3) 2_666 .
C2 C1 H1A 120.0 . .
B1 C1 H1A 118.2 . .
Li4 C1 H1A 134.5 2_666 .
Li1 C1 H1A 121.1 . .
C1 C2 C3 122.6(3) . .
C1 C2 Li4 75.2(3) . 2_666
C3 C2 Li4 72.8(3) . 2_666
C1 C2 Li1 75.2(3) . .
C3 C2 Li1 71.3(3) . .
Li4 C2 Li1 108.0(3) 2_666 .
C1 C2 H2A 116.8 . .
C3 C2 H2A 119.8 . .
Li4 C2 H2A 134.3 2_666 .
Li1 C2 H2A 117.7 . .
C4 C3 C2 119.3(3) . .
C4 C3 Li1 73.4(3) . .
C2 C3 Li1 73.3(3) . .
C4 C3 Li4 72.6(3) . 2_666
C2 C3 Li4 72.0(3) . 2_666
Li1 C3 Li4 108.6(3) . 2_666
C4 C3 H3A 121.6 . .
C2 C3 H3A 119.0 . .
Li1 C3 H3A 121.4 . .
Li4 C3 H3A 130.0 2_666 .
C5 C4 C3 122.7(3) . .
C5 C4 Li1 75.2(3) . .
C3 C4 Li1 71.6(3) . .
C5 C4 Li4 75.0(3) . 2_666
C3 C4 Li4 72.7(3) . 2_666
Li1 C4 Li4 107.9(3) . 2_666
C5 C4 H4A 117.9 . .
C3 C4 H4A 118.7 . .
Li1 C4 H4A 118.2 . .
Li4 C4 H4A 133.8 2_666 .
C4 C5 B1 122.4(3) . .
C4 C5 Li1 70.9(3) . .
B1 C5 Li1 74.4(3) . .
C4 C5 Li4 71.2(3) . 2_666
B1 C5 Li4 75.0(3) . 2_666
Li1 C5 Li4 104.6(2) . 2_666
C4 C5 H5A 118.7 . .
B1 C5 H5A 118.1 . .
Li1 C5 H5A 118.8 . .
Li4 C5 H5A 136.5 2_666 .
N1 C6 C7 112.7(4) . .
N1 C6 H6A 109.0 . .
C7 C6 H6A 109.0 . .
N1 C6 H6B 109.0 . .
C7 C6 H6B 109.0 . .
H6A C6 H6B 107.8 . .
C6 C7 H7A 109.5 . .
C6 C7 H7B 109.5 . .
H7A C7 H7B 109.5 . .
C6 C7 H7C 109.5 . .
H7A C7 H7C 109.5 . .
H7B C7 H7C 109.5 . .
N1 C8 C9 112.9(4) . .
N1 C8 H8A 109.0 . .
C9 C8 H8A 109.0 . .
N1 C8 H8B 109.0 . .
C9 C8 H8B 109.0 . .
H8A C8 H8B 107.8 . .
C8 C9 H9A 109.5 . .
C8 C9 H9B 109.5 . .
H9A C9 H9B 109.5 . .
C8 C9 H9C 109.5 . .
H9A C9 H9C 109.5 . .
H9B C9 H9C 109.5 . .
Si1 C10 H10A 109.5 . .
Si1 C10 H10B 109.5 . .
H10A C10 H10B 109.5 . .
Si1 C10 H10C 109.5 . .
H10A C10 H10C 109.5 . .
H10B C10 H10C 109.5 . .
Si1 C11 H11A 109.5 . .
Si1 C11 H11B 109.5 . .
H11A C11 H11B 109.5 . .
Si1 C11 H11C 109.5 . .
H11A C11 H11C 109.5 . .
H11B C11 H11C 109.5 . .
Si1 C12 H12A 109.5 . .
Si1 C12 H12B 109.5 . .
H12A C12 H12B 109.5 . .
Si1 C12 H12C 109.5 . .
H12A C12 H12C 109.5 . .
H12B C12 H12C 109.5 . .
Si2 C13 H13A 109.5 . .
Si2 C13 H13B 109.5 . .
H13A C13 H13B 109.5 . .
Si2 C13 H13C 109.5 . .
H13A C13 H13C 109.5 . .
H13B C13 H13C 109.5 . .
Si2 C14 H14A 109.5 . .
Si2 C14 H14B 109.5 . .
H14A C14 H14B 109.5 . .
Si2 C14 H14C 109.5 . .
H14A C14 H14C 109.5 . .
H14B C14 H14C 109.5 . .
Si2 C15 H15A 109.5 . .
Si2 C15 H15B 109.5 . .
H15A C15 H15B 109.5 . .
Si2 C15 H15C 109.5 . .
H15A C15 H15C 109.5 . .
H15B C15 H15C 109.5 . .
C17 C16 B2 121.8(3) . .
C17 C16 Li3 70.1(3) . .
B2 C16 Li3 75.4(3) . .
C17 C16 Li2 69.6(3) . .
B2 C16 Li2 75.0(3) . .
Li3 C16 Li2 103.5(3) . .
C17 C16 H16A 119.1 . .
B2 C16 H16A 118.1 . .
Li3 C16 H16A 137.8 . .
Li2 C16 H16A 118.5 . .
C16 C17 C18 122.8(4) . .
C16 C17 Li3 75.2(3) . .
C18 C17 Li3 72.4(3) . .
C16 C17 Li2 76.1(3) . .
C18 C17 Li2 71.2(3) . .
Li3 C17 Li2 108.2(3) . .
C16 C17 H17A 117.7 . .
C18 C17 H17A 118.9 . .
Li3 C17 H17A 133.6 . .
Li2 C17 H17A 118.1 . .
C19 C18 C17 119.3(4) . .
C19 C18 Li2 73.2(3) . .
C17 C18 Li2 73.3(3) . .
C19 C18 Li3 73.0(3) . .
C17 C18 Li3 72.3(3) . .
Li2 C18 Li3 109.1(3) . .
C19 C18 H18A 120.0 . .
C17 C18 H18A 120.6 . .
Li2 C18 H18A 120.5 . .
Li3 C18 H18A 130.3 . .
C20 C19 C18 123.2(4) . .
C20 C19 Li2 75.8(3) . .
C18 C19 Li2 71.3(3) . .
C20 C19 Li3 76.0(3) . .
C18 C19 Li3 71.8(3) . .
Li2 C19 Li3 107.8(3) . .
C20 C19 H19A 117.7 . .
C18 C19 H19A 118.5 . .
Li2 C19 H19A 118.0 . .
Li3 C19 H19A 134.0 . .
C19 C20 B2 121.7(3) . .
C19 C20 Li2 70.1(3) . .
B2 C20 Li2 75.1(3) . .
C19 C20 Li3 70.1(3) . .
B2 C20 Li3 74.3(3) . .
Li2 C20 Li3 103.1(3) . .
C19 C20 H20A 119.6 . .
B2 C20 H20A 118.3 . .
Li2 C20 H20A 120.9 . .
Li3 C20 H20A 135.9 . .
N3 C21 C22 113.7(4) . .
N3 C21 H21A 108.8 . .
C22 C21 H21A 108.8 . .
N3 C21 H21B 108.8 . .
C22 C21 H21B 108.8 . .
H21A C21 H21B 107.7 . .
C21 C22 H22A 109.5 . .
C21 C22 H22B 109.5 . .
H22A C22 H22B 109.5 . .
C21 C22 H22C 109.5 . .
H22A C22 H22C 109.5 . .
H22B C22 H22C 109.5 . .
N3 C23 C24 114.5(4) . .
N3 C23 H23A 108.6 . .
C24 C23 H23A 108.6 . .
N3 C23 H23B 108.6 . .
C24 C23 H23B 108.6 . .
H23A C23 H23B 107.6 . .
C23 C24 H24A 109.5 . .
C23 C24 H24B 109.5 . .
H24A C24 H24B 109.5 . .
C23 C24 H24C 109.5 . .
H24A C24 H24C 109.5 . .
H24B C24 H24C 109.5 . .
Si3 C25 H25A 109.5 . .
Si3 C25 H25B 109.5 . .
H25A C25 H25B 109.5 . .
Si3 C25 H25C 109.5 . .
H25A C25 H25C 109.5 . .
H25B C25 H25C 109.5 . .
Si3 C26 H26A 109.5 . .
Si3 C26 H26B 109.5 . .
H26A C26 H26B 109.5 . .
Si3 C26 H26C 109.5 . .
H26A C26 H26C 109.5 . .
H26B C26 H26C 109.5 . .
Si3 C27 H27A 109.5 . .
Si3 C27 H27B 109.5 . .
H27A C27 H27B 109.5 . .
Si3 C27 H27C 109.5 . .
H27A C27 H27C 109.5 . .
H27B C27 H27C 109.5 . .
Si4 C28 H28A 109.5 . .
Si4 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
Si4 C28 H28C 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
Si4 C29 H29A 109.5 . .
Si4 C29 H29B 109.5 . .
H29A C29 H29B 109.5 . .
Si4 C29 H29C 109.5 . .
H29A C29 H29C 109.5 . .
H29B C29 H29C 109.5 . .
Si4 C30 H30A 109.5 . .
Si4 C30 H30B 109.5 . .
H30A C30 H30B 109.5 . .
Si4 C30 H30C 109.5 . .
H30A C30 H30C 109.5 . .
H30B C30 H30C 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Li1 N2 1.958(6) .
Li1 C3 2.316(7) .
Li1 C4 2.339(7) .
Li1 C2 2.342(7) .
Li1 C5 2.392(7) .
Li1 C1 2.401(7) .
Li1 B1 2.469(7) .
Li1 Si1 2.987(6) .
Li1 Si2 2.994(6) .
Li1 Li2 3.043(9) .
Li2 N2 1.957(7) .
Li2 C18 2.290(7) .
Li2 C19 2.315(7) .
Li2 C17 2.317(7) .
Li2 C20 2.387(7) .
Li2 C16 2.400(8) .
Li2 B2 2.491(8) .
Li2 Si1 2.886(6) .
Li2 Si2 2.936(7) .
Li3 N4 1.946(7) .
Li3 C17 2.310(8) .
Li3 C18 2.311(8) .
Li3 C19 2.327(8) .
Li3 C16 2.375(7) .
Li3 C20 2.402(7) .
Li3 B2 2.481(8) .
Li3 Si4 2.947(7) .
Li3 Si3 2.957(7) .
Li3 Li4 2.972(9) .
Li4 N4 1.954(6) .
Li4 C2 2.336(7) 2_666
Li4 C4 2.346(7) 2_666
Li4 C3 2.347(7) 2_666
Li4 C5 2.393(7) 2_666
Li4 C1 2.394(7) 2_666
Li4 B1 2.486(7) 2_666
Li4 Si3 2.951(6) .
Li4 Si4 3.025(6) .
N1 B1 1.425(5) .
N1 C8 1.471(5) .
N1 C6 1.477(5) .
N2 Si2 1.710(3) .
N2 Si1 1.719(3) .
N3 B2 1.409(5) .
N3 C21 1.456(5) .
N3 C23 1.471(6) .
N4 Si3 1.716(3) .
N4 Si4 1.718(3) .
Si1 C12 1.873(4) .
Si1 C10 1.873(4) .
Si1 C11 1.882(4) .
Si2 C14 1.874(4) .
Si2 C13 1.876(4) .
Si2 C15 1.886(4) .
Si3 C26 1.872(4) .
Si3 C27 1.874(4) .
Si3 C25 1.878(5) .
Si4 C29 1.870(4) .
Si4 C30 1.874(4) .
Si4 C28 1.874(5) .
B1 C5 1.532(6) .
B1 C1 1.537(5) .
B1 Li4 2.486(7) 2_666
B2 C16 1.534(6) .
B2 C20 1.551(6) .
C1 C2 1.394(5) .
C1 Li4 2.394(7) 2_666
C1 H1A 0.9545 .
C2 C3 1.415(5) .
C2 Li4 2.336(7) 2_666
C2 H2A 0.9537 .
C3 C4 1.398(5) .
C3 Li4 2.347(7) 2_666
C3 H3A 0.9528 .
C4 C5 1.379(5) .
C4 Li4 2.346(7) 2_666
C4 H4A 0.9544 .
C5 Li4 2.393(7) 2_666
C5 H5A 0.9535 .
C6 C7 1.525(6) .
C6 H6A 0.9900 .
C6 H6B 0.9900 .
C7 H7A 0.9800 .
C7 H7B 0.9800 .
C7 H7C 0.9800 .
C8 C9 1.530(6) .
C8 H8A 0.9900 .
C8 H8B 0.9900 .
C9 H9A 0.9800 .
C9 H9B 0.9800 .
C9 H9C 0.9800 .
C10 H10A 0.9800 .
C10 H10B 0.9800 .
C10 H10C 0.9800 .
C11 H11A 0.9800 .
C11 H11B 0.9800 .
C11 H11C 0.9800 .
C12 H12A 0.9800 .
C12 H12B 0.9800 .
C12 H12C 0.9800 .
C13 H13A 0.9800 .
C13 H13B 0.9800 .
C13 H13C 0.9800 .
C14 H14A 0.9800 .
C14 H14B 0.9800 .
C14 H14C 0.9800 .
C15 H15A 0.9800 .
C15 H15B 0.9800 .
C15 H15C 0.9800 .
C16 C17 1.397(5) .
C16 H16A 0.9536 .
C17 C18 1.403(6) .
C17 H17A 0.9573 .
C18 C19 1.403(6) .
C18 H18A 0.9558 .
C19 C20 1.381(6) .
C19 H19A 0.9540 .
C20 H20A 0.9572 .
C21 C22 1.517(7) .
C21 H21A 0.9900 .
C21 H21B 0.9900 .
C22 H22A 0.9800 .
C22 H22B 0.9800 .
C22 H22C 0.9800 .
C23 C24 1.521(7) .
C23 H23A 0.9900 .
C23 H23B 0.9900 .
C24 H24A 0.9800 .
C24 H24B 0.9800 .
C24 H24C 0.9800 .
C25 H25A 0.9800 .
C25 H25B 0.9800 .
C25 H25C 0.9800 .
C26 H26A 0.9800 .
C26 H26B 0.9800 .
C26 H26C 0.9800 .
C27 H27A 0.9800 .
C27 H27B 0.9800 .
C27 H27C 0.9800 .
C28 H28A 0.9800 .
C28 H28B 0.9800 .
C28 H28C 0.9800 .
C29 H29A 0.9800 .
C29 H29B 0.9800 .
C29 H29C 0.9800 .
C30 H30A 0.9800 .
C30 H30B 0.9800 .
C30 H30C 0.9800 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C3 Li1 Li2 N2 -169.0(4) . .
C4 Li1 Li2 N2 154.5(4) . .
C2 Li1 Li2 N2 -137.2(4) . .
C5 Li1 Li2 N2 123.9(4) . .
C1 Li1 Li2 N2 -115.0(9) . .
B1 Li1 Li2 N2 96.1(10) . .
Si1 Li1 Li2 N2 37.97(19) . .
Si2 Li1 Li2 N2 -36.02(19) . .
N2 Li1 Li2 C18 161.7(4) . .
C3 Li1 Li2 C18 -7.3(3) . .
C4 Li1 Li2 C18 -43.8(3) . .
C2 Li1 Li2 C18 24.5(4) . .
C5 Li1 Li2 C18 -74.3(4) . .
C1 Li1 Li2 C18 46.8(9) . .
B1 Li1 Li2 C18 -102.2(9) . .
Si1 Li1 Li2 C18 -160.3(3) . .
Si2 Li1 Li2 C18 125.7(3) . .
N2 Li1 Li2 C19 132.6(4) . .
C3 Li1 Li2 C19 -36.4(4) . .
C4 Li1 Li2 C19 -73.0(4) . .
C2 Li1 Li2 C19 -4.7(5) . .
C5 Li1 Li2 C19 -103.5(4) . .
C1 Li1 Li2 C19 17.6(10) . .
B1 Li1 Li2 C19 -131.3(9) . .
Si1 Li1 Li2 C19 170.5(4) . .
Si2 Li1 Li2 C19 96.5(3) . .
N2 Li1 Li2 C17 -162.3(4) . .
C3 Li1 Li2 C17 28.7(3) . .
C4 Li1 Li2 C17 -7.8(3) . .
C2 Li1 Li2 C17 60.5(4) . .
C5 Li1 Li2 C17 -38.4(4) . .
C1 Li1 Li2 C17 82.7(9) . .
B1 Li1 Li2 C17 -66.2(10) . .
Si1 Li1 Li2 C17 -124.3(3) . .
Si2 Li1 Li2 C17 161.7(3) . .
N2 Li1 Li2 C20 120.5(8) . .
C3 Li1 Li2 C20 -48.5(8) . .
C4 Li1 Li2 C20 -85.1(8) . .
C2 Li1 Li2 C20 -16.8(9) . .
C5 Li1 Li2 C20 -115.6(7) . .
C1 Li1 Li2 C20 5.5(14) . .
B1 Li1 Li2 C20 -143.4(8) . .
Si1 Li1 Li2 C20 158.4(8) . .
Si2 Li1 Li2 C20 84.4(7) . .
N2 Li1 Li2 C16 -134.8(4) . .
C3 Li1 Li2 C16 56.2(4) . .
C4 Li1 Li2 C16 19.7(4) . .
C2 Li1 Li2 C16 88.0(4) . .
C5 Li1 Li2 C16 -10.9(5) . .
C1 Li1 Li2 C16 110.2(8) . .
B1 Li1 Li2 C16 -38.7(11) . .
Si1 Li1 Li2 C16 -96.8(3) . .
Si2 Li1 Li2 C16 -170.8(4) . .
N2 Li1 Li2 B2 -123.3(10) . .
C3 Li1 Li2 B2 67.7(10) . .
C4 Li1 Li2 B2 31.2(10) . .
C2 Li1 Li2 B2 99.4(9) . .
C5 Li1 Li2 B2 0.6(11) . .
C1 Li1 Li2 B2 121.7(10) . .
B1 Li1 Li2 B2 -27.2(16) . .
Si1 Li1 Li2 B2 -85.3(9) . .
Si2 Li1 Li2 B2 -159.3(10) . .
N2 Li1 Li2 Si1 -37.97(19) . .
C3 Li1 Li2 Si1 153.0(3) . .
C4 Li1 Li2 Si1 116.5(3) . .
C2 Li1 Li2 Si1 -175.2(4) . .
C5 Li1 Li2 Si1 85.9(3) . .
C1 Li1 Li2 Si1 -153.0(8) . .
B1 Li1 Li2 Si1 58.1(9) . .
Si2 Li1 Li2 Si1 -73.99(12) . .
N2 Li1 Li2 Si2 36.02(19) . .
C3 Li1 Li2 Si2 -133.0(3) . .
C4 Li1 Li2 Si2 -169.5(3) . .
C2 Li1 Li2 Si2 -101.2(3) . .
C5 Li1 Li2 Si2 159.9(3) . .
C1 Li1 Li2 Si2 -79.0(8) . .
B1 Li1 Li2 Si2 132.1(10) . .
Si1 Li1 Li2 Si2 73.99(12) . .
C17 Li3 Li4 N4 166.2(4) . .
C18 Li3 Li4 N4 -158.4(4) . .
C19 Li3 Li4 N4 -128.6(4) . .
C16 Li3 Li4 N4 141.2(5) . .
C20 Li3 Li4 N4 -115.8(7) . .
B2 Li3 Li4 N4 143.1(13) . .
Si4 Li3 Li4 N4 35.08(19) . .
Si3 Li3 Li4 N4 -36.70(19) . .
N4 Li3 Li4 C2 -134.4(4) . 2_666
C17 Li3 Li4 C2 31.9(4) . 2_666
C18 Li3 Li4 C2 67.2(4) . 2_666
C19 Li3 Li4 C2 97.1(4) . 2_666
C16 Li3 Li4 C2 6.9(5) . 2_666
C20 Li3 Li4 C2 109.8(6) . 2_666
B2 Li3 Li4 C2 8.7(14) . 2_666
Si4 Li3 Li4 C2 -99.3(3) . 2_666
Si3 Li3 Li4 C2 -171.1(3) . 2_666
N4 Li3 Li4 C4 156.9(4) . 2_666
C17 Li3 Li4 C4 -36.9(4) . 2_666
C18 Li3 Li4 C4 -1.6(3) . 2_666
C19 Li3 Li4 C4 28.3(4) . 2_666
C16 Li3 Li4 C4 -61.9(5) . 2_666
C20 Li3 Li4 C4 41.1(7) . 2_666
B2 Li3 Li4 C4 -60.0(13) . 2_666
Si4 Li3 Li4 C4 -168.0(3) . 2_666
Si3 Li3 Li4 C4 120.2(3) . 2_666
N4 Li3 Li4 C3 -168.3(4) . 2_666
C17 Li3 Li4 C3 -2.1(3) . 2_666
C18 Li3 Li4 C3 33.2(3) . 2_666
C19 Li3 Li4 C3 63.1(4) . 2_666
C16 Li3 Li4 C3 -27.1(5) . 2_666
C20 Li3 Li4 C3 75.9(6) . 2_666
B2 Li3 Li4 C3 -25.2(13) . 2_666
Si4 Li3 Li4 C3 -133.3(3) . 2_666
Si3 Li3 Li4 C3 155.0(3) . 2_666
N4 Li3 Li4 C5 131.2(5) . 2_666
C17 Li3 Li4 C5 -62.6(5) . 2_666
C18 Li3 Li4 C5 -27.3(5) . 2_666
C19 Li3 Li4 C5 2.6(6) . 2_666
C16 Li3 Li4 C5 -87.6(5) . 2_666
C20 Li3 Li4 C5 15.3(9) . 2_666
B2 Li3 Li4 C5 -85.7(13) . 2_666
Si4 Li3 Li4 C5 166.2(4) . 2_666
Si3 Li3 Li4 C5 94.5(4) . 2_666
N4 Li3 Li4 C1 -110.7(6) . 2_666
C17 Li3 Li4 C1 55.5(6) . 2_666
C18 Li3 Li4 C1 90.8(6) . 2_666
C19 Li3 Li4 C1 120.7(5) . 2_666
C16 Li3 Li4 C1 30.5(8) . 2_666
C20 Li3 Li4 C1 133.4(6) . 2_666
B2 Li3 Li4 C1 32.4(16) . 2_666
Si4 Li3 Li4 C1 -75.7(5) . 2_666
Si3 Li3 Li4 C1 -147.4(6) . 2_666
N4 Li3 Li4 B1 136(3) . 2_666
C17 Li3 Li4 B1 -57(3) . 2_666
C18 Li3 Li4 B1 -22(3) . 2_666
C19 Li3 Li4 B1 8(3) . 2_666
C16 Li3 Li4 B1 -82(3) . 2_666
C20 Li3 Li4 B1 21(4) . 2_666
B2 Li3 Li4 B1 -80(4) . 2_666
Si4 Li3 Li4 B1 171(3) . 2_666
Si3 Li3 Li4 B1 100(3) . 2_666
N4 Li3 Li4 Si3 36.70(19) . .
C17 Li3 Li4 Si3 -157.1(3) . .
C18 Li3 Li4 Si3 -121.7(3) . .
C19 Li3 Li4 Si3 -91.9(3) . .
C16 Li3 Li4 Si3 177.9(4) . .
C20 Li3 Li4 Si3 -79.1(6) . .
B2 Li3 Li4 Si3 179.8(13) . .
Si4 Li3 Li4 Si3 71.78(13) . .
N4 Li3 Li4 Si4 -35.08(19) . .
C17 Li3 Li4 Si4 131.2(3) . .
C18 Li3 Li4 Si4 166.5(3) . .
C19 Li3 Li4 Si4 -163.7(3) . .
C16 Li3 Li4 Si4 106.2(4) . .
C20 Li3 Li4 Si4 -150.9(6) . .
B2 Li3 Li4 Si4 108.0(12) . .
Si3 Li3 Li4 Si4 -71.78(13) . .
C18 Li2 N2 Si2 88.2(5) . .
C19 Li2 N2 Si2 34.6(6) . .
C17 Li2 N2 Si2 140.7(5) . .
C20 Li2 N2 Si2 -24.1(7) . .
C16 Li2 N2 Si2 -164.2(5) . .
B2 Li2 N2 Si2 -96.5(6) . .
Si1 Li2 N2 Si2 -133.1(2) . .
Li1 Li2 N2 Si2 114.4(3) . .
C18 Li2 N2 Si1 -138.7(4) . .
C19 Li2 N2 Si1 167.6(5) . .
C17 Li2 N2 Si1 -86.2(5) . .
C20 Li2 N2 Si1 109.0(6) . .
C16 Li2 N2 Si1 -31.1(7) . .
B2 Li2 N2 Si1 36.6(7) . .
Si2 Li2 N2 Si1 133.1(2) . .
Li1 Li2 N2 Si1 -112.6(3) . .
C18 Li2 N2 Li1 -26.1(5) . .
C19 Li2 N2 Li1 -79.8(6) . .
C17 Li2 N2 Li1 26.4(6) . .
C20 Li2 N2 Li1 -138.5(7) . .
C16 Li2 N2 Li1 81.4(6) . .
B2 Li2 N2 Li1 149.1(6) . .
Si1 Li2 N2 Li1 112.6(3) . .
Si2 Li2 N2 Li1 -114.4(3) . .
C3 Li1 N2 Si2 -94.0(6) . .
C4 Li1 N2 Si2 -152.6(4) . .
C2 Li1 N2 Si2 -29.4(7) . .
C5 Li1 N2 Si2 153.6(4) . .
C1 Li1 N2 Si2 34.2(6) . .
B1 Li1 N2 Si2 95.7(5) . .
Si1 Li1 N2 Si2 139.3(3) . .
Li2 Li1 N2 Si2 -112.1(3) . .
C3 Li1 N2 Si1 126.7(5) . .
C4 Li1 N2 Si1 68.1(5) . .
C2 Li1 N2 Si1 -168.7(6) . .
C5 Li1 N2 Si1 14.3(6) . .
C1 Li1 N2 Si1 -105.2(5) . .
B1 Li1 N2 Si1 -43.6(6) . .
Si2 Li1 N2 Si1 -139.3(3) . .
Li2 Li1 N2 Si1 108.6(3) . .
C3 Li1 N2 Li2 18.1(6) . .
C4 Li1 N2 Li2 -40.5(6) . .
C2 Li1 N2 Li2 82.7(7) . .
C5 Li1 N2 Li2 -94.4(5) . .
C1 Li1 N2 Li2 146.2(5) . .
B1 Li1 N2 Li2 -152.2(5) . .
Si1 Li1 N2 Li2 -108.6(3) . .
Si2 Li1 N2 Li2 112.1(3) . .
C17 Li3 N4 Si3 -132.4(5) . .
C18 Li3 N4 Si3 -81.4(5) . .
C19 Li3 N4 Si3 -32.2(6) . .
C16 Li3 N4 Si3 167.4(7) . .
C20 Li3 N4 Si3 18.7(7) . .
B2 Li3 N4 Si3 88.3(7) . .
Si4 Li3 N4 Si3 133.7(3) . .
Li4 Li3 N4 Si3 -111.1(3) . .
C17 Li3 N4 Si4 93.9(6) . .
C18 Li3 N4 Si4 144.9(4) . .
C19 Li3 N4 Si4 -166.0(4) . .
C16 Li3 N4 Si4 33.7(8) . .
C20 Li3 N4 Si4 -115.1(6) . .
B2 Li3 N4 Si4 -45.4(8) . .
Si3 Li3 N4 Si4 -133.7(3) . .
Li4 Li3 N4 Si4 115.1(3) . .
C17 Li3 N4 Li4 -21.3(6) . .
C18 Li3 N4 Li4 29.7(5) . .
C19 Li3 N4 Li4 78.9(5) . .
C16 Li3 N4 Li4 -81.5(8) . .
C20 Li3 N4 Li4 129.8(6) . .
B2 Li3 N4 Li4 -160.6(7) . .
Si4 Li3 N4 Li4 -115.1(3) . .
Si3 Li3 N4 Li4 111.1(3) . .
C2 Li4 N4 Si3 -175.2(4) 2_666 .
C4 Li4 N4 Si3 70.6(6) 2_666 .
C3 Li4 N4 Si3 129.8(5) 2_666 .
C5 Li4 N4 Si3 5.6(8) 2_666 .
C1 Li4 N4 Si3 -122.3(5) 2_666 .
B1 Li4 N4 Si3 -62.0(6) 2_666 .
Li3 Li4 N4 Si3 111.7(3) . .
Si4 Li4 N4 Si3 -136.2(3) . .
C2 Li4 N4 Si4 -39.0(6) 2_666 .
C4 Li4 N4 Si4 -153.2(5) 2_666 .
C3 Li4 N4 Si4 -94.0(5) 2_666 .
C5 Li4 N4 Si4 141.8(6) 2_666 .
C1 Li4 N4 Si4 13.8(6) 2_666 .
B1 Li4 N4 Si4 74.2(6) 2_666 .
Si3 Li4 N4 Si4 136.2(3) . .
Li3 Li4 N4 Si4 -112.2(3) . .
C2 Li4 N4 Li3 73.1(6) 2_666 .
C4 Li4 N4 Li3 -41.1(7) 2_666 .
C3 Li4 N4 Li3 18.2(6) 2_666 .
C5 Li4 N4 Li3 -106.0(7) 2_666 .
C1 Li4 N4 Li3 126.0(5) 2_666 .
B1 Li4 N4 Li3 -173.7(5) 2_666 .
Si3 Li4 N4 Li3 -111.7(3) . .
Si4 Li4 N4 Li3 112.2(3) . .
Si2 N2 Si1 C12 -62.2(3) . .
Li2 N2 Si1 C12 176.8(3) . .
Li1 N2 Si1 C12 69.0(3) . .
Si2 N2 Si1 C10 179.2(2) . .
Li2 N2 Si1 C10 58.2(3) . .
Li1 N2 Si1 C10 -49.5(3) . .
Si2 N2 Si1 C11 61.8(3) . .
Li2 N2 Si1 C11 -59.2(3) . .
Li1 N2 Si1 C11 -167.0(3) . .
Si2 N2 Si1 Li2 121.0(3) . .
Li1 N2 Si1 Li2 -107.7(3) . .
Si2 N2 Si1 Li1 -131.3(3) . .
Li2 N2 Si1 Li1 107.7(3) . .
C18 Li2 Si1 N2 87.9(7) . .
C19 Li2 Si1 N2 -67(2) . .
C17 Li2 Si1 N2 124.7(5) . .
C20 Li2 Si1 N2 -123.7(6) . .
C16 Li2 Si1 N2 160.9(4) . .
B2 Li2 Si1 N2 -159.3(4) . .
Si2 Li2 Si1 N2 -27.31(16) . .
Li1 Li2 Si1 N2 41.9(2) . .
N2 Li2 Si1 C12 -7.1(5) . .
C18 Li2 Si1 C12 80.8(8) . .
C19 Li2 Si1 C12 -74(2) . .
C17 Li2 Si1 C12 117.6(4) . .
C20 Li2 Si1 C12 -130.8(5) . .
C16 Li2 Si1 C12 153.8(3) . .
B2 Li2 Si1 C12 -166.4(3) . .
Si2 Li2 Si1 C12 -34.4(5) . .
Li1 Li2 Si1 C12 34.8(5) . .
N2 Li2 Si1 C10 -126.6(2) . .
C18 Li2 Si1 C10 -38.8(7) . .
C19 Li2 Si1 C10 166(2) . .
C17 Li2 Si1 C10 -1.9(3) . .
C20 Li2 Si1 C10 109.7(5) . .
C16 Li2 Si1 C10 34.3(3) . .
B2 Li2 Si1 C10 74.0(3) . .
Si2 Li2 Si1 C10 -153.96(16) . .
Li1 Li2 Si1 C10 -84.72(19) . .
N2 Li2 Si1 C11 127.4(2) . .
C18 Li2 Si1 C11 -144.8(7) . .
C19 Li2 Si1 C11 60(2) . .
C17 Li2 Si1 C11 -107.9(4) . .
C20 Li2 Si1 C11 3.7(5) . .
C16 Li2 Si1 C11 -71.7(3) . .
B2 Li2 Si1 C11 -31.9(3) . .
Si2 Li2 Si1 C11 100.07(15) . .
Li1 Li2 Si1 C11 169.3(2) . .
N2 Li2 Si1 Li1 -41.9(2) . .
C18 Li2 Si1 Li1 45.9(6) . .
C19 Li2 Si1 Li1 -109(2) . .
C17 Li2 Si1 Li1 82.8(4) . .
C20 Li2 Si1 Li1 -165.6(5) . .
C16 Li2 Si1 Li1 119.0(3) . .
B2 Li2 Si1 Li1 158.7(3) . .
Si2 Li2 Si1 Li1 -69.24(16) . .
C3 Li1 Si1 N2 -107.0(6) . .
C4 Li1 Si1 N2 -136.6(4) . .
C2 Li1 Si1 N2 97(3) . .
C5 Li1 Si1 N2 -170.3(4) . .
C1 Li1 Si1 N2 120.4(5) . .
B1 Li1 Si1 N2 151.1(4) . .
Si2 Li1 Si1 N2 23.66(17) . .
Li2 Li1 Si1 N2 -45.2(2) . .
N2 Li1 Si1 C12 -121.0(2) . .
C3 Li1 Si1 C12 132.0(6) . .
C4 Li1 Si1 C12 102.4(3) . .
C2 Li1 Si1 C12 -24(3) . .
C5 Li1 Si1 C12 68.7(3) . .
C1 Li1 Si1 C12 -0.6(4) . .
B1 Li1 Si1 C12 30.0(3) . .
Si2 Li1 Si1 C12 -97.35(15) . .
Li2 Li1 Si1 C12 -166.2(2) . .
N2 Li1 Si1 C10 133.9(3) . .
C3 Li1 Si1 C10 26.9(6) . .
C4 Li1 Si1 C10 -2.7(3) . .
C2 Li1 Si1 C10 -130(3) . .
C5 Li1 Si1 C10 -36.4(3) . .
C1 Li1 Si1 C10 -105.7(4) . .
B1 Li1 Si1 C10 -75.0(3) . .
Si2 Li1 Si1 C10 157.58(16) . .
Li2 Li1 Si1 C10 88.7(2) . .
N2 Li1 Si1 C11 24.0(5) . .
C3 Li1 Si1 C11 -83.0(6) . .
C4 Li1 Si1 C11 -112.6(4) . .
C2 Li1 Si1 C11 121(3) . .
C5 Li1 Si1 C11 -146.3(3) . .
C1 Li1 Si1 C11 144.4(4) . .
B1 Li1 Si1 C11 175.0(3) . .
Si2 Li1 Si1 C11 47.6(4) . .
Li2 Li1 Si1 C11 -21.2(4) . .
N2 Li1 Si1 Li2 45.2(2) . .
C3 Li1 Si1 Li2 -61.9(6) . .
C4 Li1 Si1 Li2 -91.4(3) . .
C2 Li1 Si1 Li2 142(3) . .
C5 Li1 Si1 Li2 -125.1(3) . .
C1 Li1 Si1 Li2 165.6(5) . .
B1 Li1 Si1 Li2 -163.8(3) . .
Si2 Li1 Si1 Li2 68.84(16) . .
Si1 N2 Si2 C14 54.3(3) . .
Li2 N2 Si2 C14 174.0(3) . .
Li1 N2 Si2 C14 -76.7(3) . .
Si1 N2 Si2 C13 -69.2(3) . .
Li2 N2 Si2 C13 50.5(3) . .
Li1 N2 Si2 C13 159.8(3) . .
Si1 N2 Si2 C15 172.7(2) . .
Li2 N2 Si2 C15 -67.6(3) . .
Li1 N2 Si2 C15 41.7(3) . .
Si1 N2 Si2 Li2 -119.7(3) . .
Li1 N2 Si2 Li2 109.3(3) . .
Si1 N2 Si2 Li1 131.0(3) . .
Li2 N2 Si2 Li1 -109.3(3) . .
C18 Li2 Si2 N2 -120.7(5) . .
C19 Li2 Si2 N2 -157.4(4) . .
C17 Li2 Si2 N2 -87.7(7) . .
C20 Li2 Si2 N2 165.9(4) . .
C16 Li2 Si2 N2 84.3(18) . .
B2 Li2 Si2 N2 128.8(5) . .
Si1 Li2 Si2 N2 28.37(17) . .
Li1 Li2 Si2 N2 -41.4(2) . .
N2 Li2 Si2 C14 -12.8(6) . .
C18 Li2 Si2 C14 -133.4(4) . .
C19 Li2 Si2 C14 -170.2(4) . .
C17 Li2 Si2 C14 -100.5(8) . .
C20 Li2 Si2 C14 153.1(4) . .
C16 Li2 Si2 C14 71.5(19) . .
B2 Li2 Si2 C14 116.1(5) . .
Si1 Li2 Si2 C14 15.6(5) . .
Li1 Li2 Si2 C14 -54.2(5) . .
N2 Li2 Si2 C13 -135.0(3) . .
C18 Li2 Si2 C13 104.3(4) . .
C19 Li2 Si2 C13 67.6(3) . .
C17 Li2 Si2 C13 137.3(7) . .
C20 Li2 Si2 C13 30.9(3) . .
C16 Li2 Si2 C13 -50.7(18) . .
B2 Li2 Si2 C13 -6.2(4) . .
Si1 Li2 Si2 C13 -106.61(17) . .
Li1 Li2 Si2 C13 -176.4(2) . .
N2 Li2 Si2 C15 119.2(3) . .
C18 Li2 Si2 C15 -1.5(4) . .
C19 Li2 Si2 C15 -38.2(3) . .
C17 Li2 Si2 C15 31.5(7) . .
C20 Li2 Si2 C15 -74.9(3) . .
C16 Li2 Si2 C15 -156.5(18) . .
B2 Li2 Si2 C15 -112.0(4) . .
Si1 Li2 Si2 C15 147.57(17) . .
Li1 Li2 Si2 C15 77.8(2) . .
N2 Li2 Si2 Li1 41.4(2) . .
C18 Li2 Si2 Li1 -79.3(4) . .
C19 Li2 Si2 Li1 -116.0(3) . .
C17 Li2 Si2 Li1 -46.3(6) . .
C20 Li2 Si2 Li1 -152.8(4) . .
C16 Li2 Si2 Li1 125.7(18) . .
B2 Li2 Si2 Li1 170.2(5) . .
Si1 Li2 Si2 Li1 69.77(16) . .
C3 Li1 Si2 N2 124.3(5) . .
C4 Li1 Si2 N2 79.2(10) . .
C2 Li1 Si2 N2 162.6(4) . .
C5 Li1 Si2 N2 -73.8(9) . .
C1 Li1 Si2 N2 -159.1(4) . .
B1 Li1 Si2 N2 -118.8(4) . .
Si1 Li1 Si2 N2 -23.96(17) . .
Li2 Li1 Si2 N2 43.3(2) . .
N2 Li1 Si2 C14 115.8(3) . .
C3 Li1 Si2 C14 -120.0(4) . .
C4 Li1 Si2 C14 -165.0(9) . .
C2 Li1 Si2 C14 -81.6(3) . .
C5 Li1 Si2 C14 41.9(10) . .
C1 Li1 Si2 C14 -43.4(3) . .
B1 Li1 Si2 C14 -3.1(4) . .
Si1 Li1 Si2 C14 91.80(16) . .
Li2 Li1 Si2 C14 159.1(2) . .
N2 Li1 Si2 C13 -36.5(4) . .
C3 Li1 Si2 C13 87.8(5) . .
C4 Li1 Si2 C13 42.7(11) . .
C2 Li1 Si2 C13 126.1(4) . .
C5 Li1 Si2 C13 -110.3(10) . .
C1 Li1 Si2 C13 164.4(3) . .
B1 Li1 Si2 C13 -155.3(3) . .
Si1 Li1 Si2 C13 -60.5(4) . .
Li2 Li1 Si2 C13 6.8(4) . .
N2 Li1 Si2 C15 -140.4(3) . .
C3 Li1 Si2 C15 -16.1(4) . .
C4 Li1 Si2 C15 -61.2(10) . .
C2 Li1 Si2 C15 22.3(3) . .
C5 Li1 Si2 C15 145.8(10) . .
C1 Li1 Si2 C15 60.5(3) . .
B1 Li1 Si2 C15 100.8(4) . .
Si1 Li1 Si2 C15 -164.31(18) . .
Li2 Li1 Si2 C15 -97.0(2) . .
N2 Li1 Si2 Li2 -43.3(2) . .
C3 Li1 Si2 Li2 80.9(4) . .
C4 Li1 Si2 Li2 35.9(9) . .
C2 Li1 Si2 Li2 119.3(3) . .
C5 Li1 Si2 Li2 -117.2(10) . .
C1 Li1 Si2 Li2 157.5(3) . .
B1 Li1 Si2 Li2 -162.2(4) . .
Si1 Li1 Si2 Li2 -67.28(17) . .
Si4 N4 Si3 C26 -47.8(3) . .
Li3 N4 Si3 C26 -172.4(3) . .
Li4 N4 Si3 C26 81.8(3) . .
Si4 N4 Si3 C27 75.3(3) . .
Li3 N4 Si3 C27 -49.3(3) . .
Li4 N4 Si3 C27 -155.2(3) . .
Si4 N4 Si3 C25 -166.2(2) . .
Li3 N4 Si3 C25 69.2(3) . .
Li4 N4 Si3 C25 -36.6(3) . .
Si4 N4 Si3 Li4 -129.6(3) . .
Li3 N4 Si3 Li4 105.8(4) . .
Si4 N4 Si3 Li3 124.6(3) . .
Li4 N4 Si3 Li3 -105.8(4) . .
C2 Li4 Si3 N4 21.4(19) 2_666 .
C4 Li4 Si3 N4 -139.5(5) 2_666 .
C3 Li4 Si3 N4 -100.6(6) 2_666 .
C5 Li4 Si3 N4 -176.8(4) 2_666 .
C1 Li4 Si3 N4 103.7(6) 2_666 .
B1 Li4 Si3 N4 142.3(4) 2_666 .
Li3 Li4 Si3 N4 -44.0(2) . .
Si4 Li4 Si3 N4 24.97(18) . .
N4 Li4 Si3 C26 -111.7(3) . .
C2 Li4 Si3 C26 -90(2) 2_666 .
C4 Li4 Si3 C26 108.8(3) 2_666 .
C3 Li4 Si3 C26 147.7(5) 2_666 .
C5 Li4 Si3 C26 71.6(3) 2_666 .
C1 Li4 Si3 C26 -8.0(5) 2_666 .
B1 Li4 Si3 C26 30.6(4) 2_666 .
Li3 Li4 Si3 C26 -155.6(2) . .
Si4 Li4 Si3 C26 -86.69(19) . .
N4 Li4 Si3 C27 45.5(5) . .
C2 Li4 Si3 C27 67(2) 2_666 .
C4 Li4 Si3 C27 -94.0(5) 2_666 .
C3 Li4 Si3 C27 -55.2(7) 2_666 .
C5 Li4 Si3 C27 -131.3(4) 2_666 .
C1 Li4 Si3 C27 149.2(4) 2_666 .
B1 Li4 Si3 C27 -172.2(3) 2_666 .
Li3 Li4 Si3 C27 1.5(4) . .
Si4 Li4 Si3 C27 70.5(4) . .
N4 Li4 Si3 C25 144.7(3) . .
C2 Li4 Si3 C25 166(2) 2_666 .
C4 Li4 Si3 C25 5.2(3) 2_666 .
C3 Li4 Si3 C25 44.0(5) 2_666 .
C5 Li4 Si3 C25 -32.1(3) 2_666 .
C1 Li4 Si3 C25 -111.6(5) 2_666 .
B1 Li4 Si3 C25 -73.0(3) 2_666 .
Li3 Li4 Si3 C25 100.7(2) . .
Si4 Li4 Si3 C25 169.66(17) . .
N4 Li4 Si3 Li3 44.0(2) . .
C2 Li4 Si3 Li3 65(2) 2_666 .
C4 Li4 Si3 Li3 -95.5(4) 2_666 .
C3 Li4 Si3 Li3 -56.7(5) 2_666 .
C5 Li4 Si3 Li3 -132.8(3) 2_666 .
C1 Li4 Si3 Li3 147.6(6) 2_666 .
B1 Li4 Si3 Li3 -173.7(4) 2_666 .
Si4 Li4 Si3 Li3 68.93(18) . .
C17 Li3 Si3 N4 97.5(7) . .
C18 Li3 Si3 N4 122.5(4) . .
C19 Li3 Si3 N4 156.8(4) . .
C16 Li3 Si3 N4 -123(2) . .
C20 Li3 Si3 N4 -168.1(4) . .
B2 Li3 Si3 N4 -135.4(6) . .
Si4 Li3 Si3 N4 -27.31(19) . .
Li4 Li3 Si3 N4 44.5(2) . .
N4 Li3 Si3 C26 15.0(6) . .
C17 Li3 Si3 C26 112.5(7) . .
C18 Li3 Si3 C26 137.6(4) . .
C19 Li3 Si3 C26 171.9(4) . .
C16 Li3 Si3 C26 -108(2) . .
C20 Li3 Si3 C26 -153.1(4) . .
B2 Li3 Si3 C26 -120.4(5) . .
Si4 Li3 Si3 C26 -12.3(5) . .
Li4 Li3 Si3 C26 59.6(5) . .
N4 Li3 Si3 C27 136.3(3) . .
C17 Li3 Si3 C27 -126.2(6) . .
C18 Li3 Si3 C27 -101.2(3) . .
C19 Li3 Si3 C27 -66.9(3) . .
C16 Li3 Si3 C27 13(2) . .
C20 Li3 Si3 C27 -31.8(3) . .
B2 Li3 Si3 C27 0.9(4) . .
Si4 Li3 Si3 C27 108.99(18) . .
Li4 Li3 Si3 C27 -179.2(2) . .
N4 Li3 Si3 C25 -117.9(3) . .
C17 Li3 Si3 C25 -20.4(6) . .
C18 Li3 Si3 C25 4.6(3) . .
C19 Li3 Si3 C25 38.9(3) . .
C16 Li3 Si3 C25 119(2) . .
C20 Li3 Si3 C25 74.0(3) . .
B2 Li3 Si3 C25 106.7(4) . .
Si4 Li3 Si3 C25 -145.22(15) . .
Li4 Li3 Si3 C25 -73.4(2) . .
N4 Li3 Si3 Li4 -44.5(2) . .
C17 Li3 Si3 Li4 52.9(6) . .
C18 Li3 Si3 Li4 78.0(3) . .
C19 Li3 Si3 Li4 112.3(3) . .
C16 Li3 Si3 Li4 -167(2) . .
C20 Li3 Si3 Li4 147.4(4) . .
B2 Li3 Si3 Li4 -179.9(5) . .
Si4 Li3 Si3 Li4 -71.83(17) . .
Si3 N4 Si4 C29 -56.1(3) . .
Li3 N4 Si4 C29 68.8(3) . .
Li4 N4 Si4 C29 176.0(3) . .
Si3 N4 Si4 C30 -175.4(2) . .
Li3 N4 Si4 C30 -50.5(3) . .
Li4 N4 Si4 C30 56.7(3) . .
Si3 N4 Si4 C28 67.4(3) . .
Li3 N4 Si4 C28 -167.7(3) . .
Li4 N4 Si4 C28 -60.5(3) . .
Si3 N4 Si4 Li3 -124.9(3) . .
Li4 N4 Si4 Li3 107.2(3) . .
Si3 N4 Si4 Li4 127.9(3) . .
Li3 N4 Si4 Li4 -107.2(3) . .
C17 Li3 Si4 N4 -121.4(5) . .
C18 Li3 Si4 N4 -73.7(7) . .
C19 Li3 Si4 N4 43.1(12) . .
C16 Li3 Si4 N4 -161.5(5) . .
C20 Li3 Si4 N4 113.1(6) . .
B2 Li3 Si4 N4 155.7(5) . .
Si3 Li3 Si4 N4 27.07(17) . .
Li4 Li3 Si4 N4 -42.0(2) . .
N4 Li3 Si4 C29 -120.0(3) . .
C17 Li3 Si4 C29 118.6(4) . .
C18 Li3 Si4 C29 166.3(7) . .
C19 Li3 Si4 C29 -76.9(13) . .
C16 Li3 Si4 C29 78.5(3) . .
C20 Li3 Si4 C29 -6.9(5) . .
B2 Li3 Si4 C29 35.7(3) . .
Si3 Li3 Si4 C29 -92.96(17) . .
Li4 Li3 Si4 C29 -162.0(2) . .
N4 Li3 Si4 C30 132.8(3) . .
C17 Li3 Si4 C30 11.4(4) . .
C18 Li3 Si4 C30 59.1(7) . .
C19 Li3 Si4 C30 175.9(13) . .
C16 Li3 Si4 C30 -28.7(3) . .
C20 Li3 Si4 C30 -114.1(5) . .
B2 Li3 Si4 C30 -71.5(3) . .
Si3 Li3 Si4 C30 159.83(17) . .
Li4 Li3 Si4 C30 90.8(2) . .
N4 Li3 Si4 C28 24.1(6) . .
C17 Li3 Si4 C28 -97.2(5) . .
C18 Li3 Si4 C28 -49.6(9) . .
C19 Li3 Si4 C28 67.3(14) . .
C16 Li3 Si4 C28 -137.3(4) . .
C20 Li3 Si4 C28 137.3(5) . .
B2 Li3 Si4 C28 179.9(4) . .
Si3 Li3 Si4 C28 51.2(5) . .
Li4 Li3 Si4 C28 -17.8(5) . .
N4 Li3 Si4 Li4 42.0(2) . .
C17 Li3 Si4 Li4 -79.4(4) . .
C18 Li3 Si4 Li4 -31.8(6) . .
C19 Li3 Si4 Li4 85.1(13) . .
C16 Li3 Si4 Li4 -119.5(3) . .
C20 Li3 Si4 Li4 155.1(5) . .
B2 Li3 Si4 Li4 -162.3(4) . .
Si3 Li3 Si4 Li4 69.03(16) . .
C2 Li4 Si4 N4 153.2(4) 2_666 .
C4 Li4 Si4 N4 94.4(11) 2_666 .
C3 Li4 Si4 N4 120.5(5) 2_666 .
C5 Li4 Si4 N4 -107.8(8) 2_666 .
C1 Li4 Si4 N4 -170.6(4) 2_666 .
B1 Li4 Si4 N4 -134.6(4) 2_666 .
Si3 Li4 Si4 N4 -26.24(19) . .
Li3 Li4 Si4 N4 44.4(2) . .
N4 Li4 Si4 C29 -7.3(5) . .
C2 Li4 Si4 C29 145.9(4) 2_666 .
C4 Li4 Si4 C29 87.1(12) 2_666 .
C3 Li4 Si4 C29 113.2(5) 2_666 .
C5 Li4 Si4 C29 -115.0(8) 2_666 .
C1 Li4 Si4 C29 -177.9(3) 2_666 .
B1 Li4 Si4 C29 -141.9(4) 2_666 .
Si3 Li4 Si4 C29 -33.5(4) . .
Li3 Li4 Si4 C29 37.1(4) . .
N4 Li4 Si4 C30 -127.8(3) . .
C2 Li4 Si4 C30 25.4(3) 2_666 .
C4 Li4 Si4 C30 -33.4(11) 2_666 .
C3 Li4 Si4 C30 -7.3(4) 2_666 .
C5 Li4 Si4 C30 124.4(8) 2_666 .
C1 Li4 Si4 C30 61.6(3) 2_666 .
B1 Li4 Si4 C30 97.6(3) 2_666 .
Si3 Li4 Si4 C30 -154.04(17) . .
Li3 Li4 Si4 C30 -83.4(2) . .
N4 Li4 Si4 C28 127.2(3) . .
C2 Li4 Si4 C28 -79.6(3) 2_666 .
C4 Li4 Si4 C28 -138.4(11) 2_666 .
C3 Li4 Si4 C28 -112.3(4) 2_666 .
C5 Li4 Si4 C28 19.5(8) 2_666 .
C1 Li4 Si4 C28 -43.4(3) 2_666 .
B1 Li4 Si4 C28 -7.4(3) 2_666 .
Si3 Li4 Si4 C28 100.99(19) . .
Li3 Li4 Si4 C28 171.6(2) . .
N4 Li4 Si4 Li3 -44.4(2) . .
C2 Li4 Si4 Li3 108.8(3) 2_666 .
C4 Li4 Si4 Li3 50.0(11) 2_666 .
C3 Li4 Si4 Li3 76.1(4) 2_666 .
C5 Li4 Si4 Li3 -152.1(8) 2_666 .
C1 Li4 Si4 Li3 145.0(3) 2_666 .
B1 Li4 Si4 Li3 -179.0(4) 2_666 .
Si3 Li4 Si4 Li3 -70.60(17) . .
C8 N1 B1 C5 -8.3(5) . .
C6 N1 B1 C5 176.3(3) . .
C8 N1 B1 C1 171.4(3) . .
C6 N1 B1 C1 -4.1(5) . .
C8 N1 B1 Li1 81.1(5) . .
C6 N1 B1 Li1 -94.3(5) . .
C8 N1 B1 Li4 -98.2(5) . 2_666
C6 N1 B1 Li4 86.3(5) . 2_666
N2 Li1 B1 N1 -4.9(7) . .
C3 Li1 B1 N1 -179.0(4) . .
C4 Li1 B1 N1 -144.0(4) . .
C2 Li1 B1 N1 145.6(4) . .
C5 Li1 B1 N1 -117.2(5) . .
C1 Li1 B1 N1 118.1(4) . .
Si1 Li1 B1 N1 -28.9(5) . .
Si2 Li1 B1 N1 41.8(6) . .
Li2 Li1 B1 N1 -79.4(10) . .
N2 Li1 B1 C5 112.3(5) . .
C3 Li1 B1 C5 -61.8(2) . .
C4 Li1 B1 C5 -26.8(2) . .
C2 Li1 B1 C5 -97.2(3) . .
C1 Li1 B1 C5 -124.6(3) . .
Si1 Li1 B1 C5 88.3(3) . .
Si2 Li1 B1 C5 159.0(4) . .
Li2 Li1 B1 C5 37.8(9) . .
N2 Li1 B1 C1 -123.0(5) . .
C3 Li1 B1 C1 62.8(2) . .
C4 Li1 B1 C1 97.8(2) . .
C2 Li1 B1 C1 27.4(2) . .
C5 Li1 B1 C1 124.6(3) . .
Si1 Li1 B1 C1 -147.0(3) . .
Si2 Li1 B1 C1 -76.3(4) . .
Li2 Li1 B1 C1 162.4(10) . .
N2 Li1 B1 Li4 174.6(5) . 2_666
C3 Li1 B1 Li4 0.5(3) . 2_666
C4 Li1 B1 Li4 35.4(2) . 2_666
C2 Li1 B1 Li4 -35.0(2) . 2_666
C5 Li1 B1 Li4 62.3(2) . 2_666
C1 Li1 B1 Li4 -62.4(2) . 2_666
Si1 Li1 B1 Li4 150.6(2) . 2_666
Si2 Li1 B1 Li4 -138.7(3) . 2_666
Li2 Li1 B1 Li4 100.0(9) . 2_666
C21 N3 B2 C16 -172.1(4) . .
C23 N3 B2 C16 3.9(6) . .
C21 N3 B2 C20 7.6(6) . .
C23 N3 B2 C20 -176.4(3) . .
C21 N3 B2 Li3 -82.9(5) . .
C23 N3 B2 Li3 93.1(5) . .
C21 N3 B2 Li2 97.3(5) . .
C23 N3 B2 Li2 -86.7(5) . .
N4 Li3 B2 N3 7.7(10) . .
C17 Li3 B2 N3 -144.6(4) . .
C18 Li3 B2 N3 179.9(4) . .
C19 Li3 B2 N3 144.6(4) . .
C16 Li3 B2 N3 -116.9(5) . .
C20 Li3 B2 N3 117.7(5) . .
Si4 Li3 B2 N3 -20.3(6) . .
Si3 Li3 B2 N3 60.4(6) . .
Li4 Li3 B2 N3 -119.4(12) . .
N4 Li3 B2 C16 124.6(7) . .
C17 Li3 B2 C16 -27.8(2) . .
C18 Li3 B2 C16 -63.2(3) . .
C19 Li3 B2 C16 -98.5(3) . .
C20 Li3 B2 C16 -125.4(3) . .
Si4 Li3 B2 C16 96.5(3) . .
Si3 Li3 B2 C16 177.3(5) . .
Li4 Li3 B2 C16 -2.5(12) . .
N4 Li3 B2 C20 -110.0(7) . .
C17 Li3 B2 C20 97.7(3) . .
C18 Li3 B2 C20 62.2(3) . .
C19 Li3 B2 C20 26.9(2) . .
C16 Li3 B2 C20 125.4(3) . .
Si4 Li3 B2 C20 -138.1(4) . .
Si3 Li3 B2 C20 -57.3(4) . .
Li4 Li3 B2 C20 122.9(13) . .
N4 Li3 B2 Li2 -172.5(7) . .
C17 Li3 B2 Li2 35.2(2) . .
C18 Li3 B2 Li2 -0.3(3) . .
C19 Li3 B2 Li2 -35.6(2) . .
C16 Li3 B2 Li2 62.9(3) . .
C20 Li3 B2 Li2 -62.5(3) . .
Si4 Li3 B2 Li2 159.5(3) . .
Si3 Li3 B2 Li2 -119.8(4) . .
Li4 Li3 B2 Li2 60.4(13) . .
N2 Li2 B2 N3 3.5(9) . .
C18 Li2 B2 N3 -179.9(4) . .
C19 Li2 B2 N3 -144.4(4) . .
C17 Li2 B2 N3 144.7(4) . .
C20 Li2 B2 N3 -117.1(5) . .
C16 Li2 B2 N3 117.4(5) . .
Si1 Li2 B2 N3 26.2(5) . .
Si2 Li2 B2 N3 -51.7(6) . .
Li1 Li2 B2 N3 101.5(10) . .
N2 Li2 B2 C16 -113.9(7) . .
C18 Li2 B2 C16 62.7(2) . .
C19 Li2 B2 C16 98.2(3) . .
C17 Li2 B2 C16 27.3(2) . .
C20 Li2 B2 C16 125.5(3) . .
Si1 Li2 B2 C16 -91.2(3) . .
Si2 Li2 B2 C16 -169.1(4) . .
Li1 Li2 B2 C16 -15.9(9) . .
N2 Li2 B2 C20 120.6(7) . .
C18 Li2 B2 C20 -62.8(2) . .
C19 Li2 B2 C20 -27.3(2) . .
C17 Li2 B2 C20 -98.3(3) . .
C16 Li2 B2 C20 -125.5(3) . .
Si1 Li2 B2 C20 143.2(3) . .
Si2 Li2 B2 C20 65.4(4) . .
Li1 Li2 B2 C20 -141.5(10) . .
N2 Li2 B2 Li3 -176.3(6) . .
C18 Li2 B2 Li3 0.3(3) . .
C19 Li2 B2 Li3 35.8(2) . .
C17 Li2 B2 Li3 -35.1(2) . .
C20 Li2 B2 Li3 63.1(3) . .
C16 Li2 B2 Li3 -62.4(3) . .
Si1 Li2 B2 Li3 -153.6(3) . .
Si2 Li2 B2 Li3 128.5(4) . .
Li1 Li2 B2 Li3 -78.3(9) . .
N1 B1 C1 C2 -178.7(3) . .
C5 B1 C1 C2 1.0(5) . .
Li1 B1 C1 C2 -54.6(3) . .
Li4 B1 C1 C2 55.4(3) 2_666 .
N1 B1 C1 Li4 125.9(4) . 2_666
C5 B1 C1 Li4 -54.4(3) . 2_666
Li1 B1 C1 Li4 -110.1(3) . 2_666
N1 B1 C1 Li1 -124.0(4) . .
C5 B1 C1 Li1 55.7(3) . .
Li4 B1 C1 Li1 110.1(3) 2_666 .
N2 Li1 C1 C2 -120.0(6) . .
C3 Li1 C1 C2 28.6(2) . .
C4 Li1 C1 C2 64.4(2) . .
C5 Li1 C1 C2 99.3(3) . .
B1 Li1 C1 C2 132.4(3) . .
Si1 Li1 C1 C2 -175.6(4) . .
Si2 Li1 C1 C2 -100.3(3) . .
Li2 Li1 C1 C2 -32.3(8) . .
N2 Li1 C1 B1 107.5(6) . .
C3 Li1 C1 B1 -103.9(3) . .
C4 Li1 C1 B1 -68.0(2) . .
C2 Li1 C1 B1 -132.4(3) . .
C5 Li1 C1 B1 -33.2(2) . .
Si1 Li1 C1 B1 52.0(4) . .
Si2 Li1 C1 B1 127.2(3) . .
Li2 Li1 C1 B1 -164.8(8) . .
N2 Li1 C1 Li4 176.9(5) . 2_666
C3 Li1 C1 Li4 -34.5(2) . 2_666
C4 Li1 C1 Li4 1.4(3) . 2_666
C2 Li1 C1 Li4 -63.1(3) . 2_666
C5 Li1 C1 Li4 36.2(2) . 2_666
B1 Li1 C1 Li4 69.4(3) . 2_666
Si1 Li1 C1 Li4 121.3(4) . 2_666
Si2 Li1 C1 Li4 -163.4(2) . 2_666
Li2 Li1 C1 Li4 -95.4(8) . 2_666
B1 C1 C2 C3 0.4(5) . .
Li4 C1 C2 C3 57.8(3) 2_666 .
Li1 C1 C2 C3 -55.8(3) . .
B1 C1 C2 Li4 -57.5(3) . 2_666
Li1 C1 C2 Li4 -113.7(3) . 2_666
B1 C1 C2 Li1 56.2(3) . .
Li4 C1 C2 Li1 113.7(3) 2_666 .
N2 Li1 C2 C1 114.5(7) . .
C3 Li1 C2 C1 -132.6(3) . .
C4 Li1 C2 C1 -102.2(3) . .
C5 Li1 C2 C1 -67.6(2) . .
B1 Li1 C2 C1 -29.4(2) . .
Si1 Li1 C2 C1 27(3) . .
Si2 Li1 C2 C1 97.2(3) . .
Li2 Li1 C2 C1 166.3(4) . .
N2 Li1 C2 C3 -112.9(7) . .
C4 Li1 C2 C3 30.4(2) . .
C5 Li1 C2 C3 65.0(2) . .
C1 Li1 C2 C3 132.6(3) . .
B1 Li1 C2 C3 103.2(3) . .
Si1 Li1 C2 C3 160(3) . .
Si2 Li1 C2 C3 -130.2(3) . .
Li2 Li1 C2 C3 -61.0(4) . .
N2 Li1 C2 Li4 -176.9(6) . 2_666
C3 Li1 C2 Li4 -64.0(3) . 2_666
C4 Li1 C2 Li4 -33.6(3) . 2_666
C5 Li1 C2 Li4 1.0(3) . 2_666
C1 Li1 C2 Li4 68.6(3) . 2_666
B1 Li1 C2 Li4 39.2(3) . 2_666
Si1 Li1 C2 Li4 96(3) . 2_666
Si2 Li1 C2 Li4 165.8(3) . 2_666
Li2 Li1 C2 Li4 -125.0(3) . 2_666
C1 C2 C3 C4 -1.7(5) . .
Li4 C2 C3 C4 57.2(3) 2_666 .
Li1 C2 C3 C4 -59.4(3) . .
C1 C2 C3 Li1 57.6(3) . .
Li4 C2 C3 Li1 116.6(3) 2_666 .
C1 C2 C3 Li4 -58.9(3) . 2_666
Li1 C2 C3 Li4 -116.6(3) . 2_666
N2 Li1 C3 C4 -109.5(6) . .
C2 Li1 C3 C4 128.5(3) . .
C5 Li1 C3 C4 27.6(2) . .
C1 Li1 C3 C4 100.8(3) . .
B1 Li1 C3 C4 64.1(3) . .
Si1 Li1 C3 C4 -47.3(6) . .
Si2 Li1 C3 C4 -158.5(4) . .
Li2 Li1 C3 C4 -97.7(3) . .
N2 Li1 C3 C2 122.1(6) . .
C4 Li1 C3 C2 -128.5(3) . .
C5 Li1 C3 C2 -100.9(3) . .
C1 Li1 C3 C2 -27.6(2) . .
B1 Li1 C3 C2 -64.4(2) . .
Si1 Li1 C3 C2 -175.8(6) . .
Si2 Li1 C3 C2 73.0(4) . .
Li2 Li1 C3 C2 133.8(3) . .
N2 Li1 C3 Li4 -174.1(5) . 2_666
C4 Li1 C3 Li4 -64.6(3) . 2_666
C2 Li1 C3 Li4 63.9(3) . 2_666
C5 Li1 C3 Li4 -37.0(3) . 2_666
C1 Li1 C3 Li4 36.2(3) . 2_666
B1 Li1 C3 Li4 -0.5(3) . 2_666
Si1 Li1 C3 Li4 -111.9(5) . 2_666
Si2 Li1 C3 Li4 136.9(4) . 2_666
Li2 Li1 C3 Li4 -162.3(3) . 2_666
C2 C3 C4 C5 1.6(5) . .
Li1 C3 C4 C5 -57.8(4) . .
Li4 C3 C4 C5 58.5(4) 2_666 .
C2 C3 C4 Li1 59.3(3) . .
Li4 C3 C4 Li1 116.2(3) 2_666 .
C2 C3 C4 Li4 -56.9(3) . 2_666
Li1 C3 C4 Li4 -116.2(3) . 2_666
N2 Li1 C4 C5 -108.9(5) . .
C3 Li1 C4 C5 132.6(4) . .
C2 Li1 C4 C5 101.9(3) . .
C1 Li1 C4 C5 67.1(2) . .
B1 Li1 C4 C5 29.0(2) . .
Si1 Li1 C4 C5 -72.6(3) . .
Si2 Li1 C4 C5 -165.8(10) . .
Li2 Li1 C4 C5 -134.3(3) . .
N2 Li1 C4 C3 118.5(6) . .
C2 Li1 C4 C3 -30.7(2) . .
C5 Li1 C4 C3 -132.6(4) . .
C1 Li1 C4 C3 -65.5(2) . .
B1 Li1 C4 C3 -103.7(3) . .
Si1 Li1 C4 C3 154.8(4) . .
Si2 Li1 C4 C3 61.6(10) . .
Li2 Li1 C4 C3 93.1(3) . .
N2 Li1 C4 Li4 -177.4(5) . 2_666
C3 Li1 C4 Li4 64.1(3) . 2_666
C2 Li1 C4 Li4 33.4(3) . 2_666
C5 Li1 C4 Li4 -68.5(3) . 2_666
C1 Li1 C4 Li4 -1.4(3) . 2_666
B1 Li1 C4 Li4 -39.5(3) . 2_666
Si1 Li1 C4 Li4 -141.1(3) . 2_666
Si2 Li1 C4 Li4 125.8(9) . 2_666
Li2 Li1 C4 Li4 157.2(3) . 2_666
C3 C4 C5 B1 0.0(5) . .
Li1 C4 C5 B1 -56.1(3) . .
Li4 C4 C5 B1 57.4(3) 2_666 .
C3 C4 C5 Li1 56.1(4) . .
Li4 C4 C5 Li1 113.5(2) 2_666 .
C3 C4 C5 Li4 -57.4(4) . 2_666
Li1 C4 C5 Li4 -113.5(2) . 2_666
N1 B1 C5 C4 178.5(3) . .
C1 B1 C5 C4 -1.2(5) . .
Li1 B1 C5 C4 54.6(3) . .
Li4 B1 C5 C4 -55.6(3) 2_666 .
N1 B1 C5 Li1 123.9(4) . .
C1 B1 C5 Li1 -55.8(3) . .
Li4 B1 C5 Li1 -110.2(2) 2_666 .
N1 B1 C5 Li4 -125.9(4) . 2_666
C1 B1 C5 Li4 54.4(3) . 2_666
Li1 B1 C5 Li4 110.2(2) . 2_666
N2 Li1 C5 C4 113.6(6) . .
C3 Li1 C5 C4 -28.4(2) . .
C2 Li1 C5 C4 -64.7(3) . .
C1 Li1 C5 C4 -100.0(3) . .
B1 Li1 C5 C4 -133.2(3) . .
Si1 Li1 C5 C4 121.6(3) . .
Si2 Li1 C5 C4 166.0(10) . .
Li2 Li1 C5 C4 60.5(4) . .
N2 Li1 C5 B1 -113.2(5) . .
C3 Li1 C5 B1 104.8(3) . .
C4 Li1 C5 B1 133.2(3) . .
C2 Li1 C5 B1 68.5(2) . .
C1 Li1 C5 B1 33.2(2) . .
Si1 Li1 C5 B1 -105.1(3) . .
Si2 Li1 C5 B1 -60.7(10) . .
Li2 Li1 C5 B1 -166.3(4) . .
N2 Li1 C5 Li4 177.3(5) . 2_666
C3 Li1 C5 Li4 35.3(3) . 2_666
C4 Li1 C5 Li4 63.7(3) . 2_666
C2 Li1 C5 Li4 -1.0(3) . 2_666
C1 Li1 C5 Li4 -36.3(2) . 2_666
B1 Li1 C5 Li4 -69.5(3) . 2_666
Si1 Li1 C5 Li4 -174.6(2) . 2_666
Si2 Li1 C5 Li4 -130.2(9) . 2_666
Li2 Li1 C5 Li4 124.2(3) . 2_666
B1 N1 C6 C7 92.5(4) . .
C8 N1 C6 C7 -83.3(4) . .
B1 N1 C8 C9 93.9(5) . .
C6 N1 C8 C9 -90.4(5) . .
N3 B2 C16 C17 -179.9(3) . .
C20 B2 C16 C17 0.3(5) . .
Li3 B2 C16 C17 54.9(4) . .
Li2 B2 C16 C17 -53.7(4) . .
N3 B2 C16 Li3 125.2(4) . .
C20 B2 C16 Li3 -54.6(3) . .
Li2 B2 C16 Li3 -108.6(3) . .
N3 B2 C16 Li2 -126.2(4) . .
C20 B2 C16 Li2 54.0(3) . .
Li3 B2 C16 Li2 108.6(3) . .
N4 Li3 C16 C17 100.9(8) . .
C18 Li3 C16 C17 -28.7(2) . .
C19 Li3 C16 C17 -64.7(3) . .
C20 Li3 C16 C17 -99.4(3) . .
B2 Li3 C16 C17 -132.3(3) . .
Si4 Li3 C16 C17 121.6(3) . .
Si3 Li3 C16 C17 -147(2) . .
Li4 Li3 C16 C17 46.8(4) . .
N4 Li3 C16 B2 -126.8(8) . .
C17 Li3 C16 B2 132.3(3) . .
C18 Li3 C16 B2 103.6(3) . .
C19 Li3 C16 B2 67.7(3) . .
C20 Li3 C16 B2 32.9(2) . .
Si4 Li3 C16 B2 -106.1(3) . .
Si3 Li3 C16 B2 -15(2) . .
Li4 Li3 C16 B2 179.2(4) . .
N4 Li3 C16 Li2 163.0(7) . .
C17 Li3 C16 Li2 62.1(3) . .
C18 Li3 C16 Li2 33.4(3) . .
C19 Li3 C16 Li2 -2.6(3) . .
C20 Li3 C16 Li2 -37.3(3) . .
B2 Li3 C16 Li2 -70.2(3) . .
Si4 Li3 C16 Li2 -176.3(3) . .
Si3 Li3 C16 Li2 -85(2) . .
Li4 Li3 C16 Li2 108.9(4) . .
N2 Li2 C16 C17 -102.7(7) . .
C18 Li2 C16 C17 28.7(2) . .
C19 Li2 C16 C17 65.1(3) . .
C20 Li2 C16 C17 100.1(3) . .
B2 Li2 C16 C17 133.0(3) . .
Si1 Li2 C16 C17 -121.5(3) . .
Si2 Li2 C16 C17 -174.0(18) . .
Li1 Li2 C16 C17 -53.2(4) . .
N2 Li2 C16 B2 124.3(6) . .
C18 Li2 C16 B2 -104.3(3) . .
C19 Li2 C16 B2 -68.0(3) . .
C17 Li2 C16 B2 -133.0(3) . .
C20 Li2 C16 B2 -32.9(2) . .
Si1 Li2 C16 B2 105.5(3) . .
Si2 Li2 C16 B2 53.0(18) . .
Li1 Li2 C16 B2 173.7(4) . .
N2 Li2 C16 Li3 -165.1(6) . .
C18 Li2 C16 Li3 -33.7(3) . .
C19 Li2 C16 Li3 2.6(3) . .
C17 Li2 C16 Li3 -62.5(3) . .
C20 Li2 C16 Li3 37.6(3) . .
B2 Li2 C16 Li3 70.6(3) . .
Si1 Li2 C16 Li3 176.1(3) . .
Si2 Li2 C16 Li3 123.5(18) . .
Li1 Li2 C16 Li3 -115.7(3) . .
B2 C16 C17 C18 -0.2(6) . .
Li3 C16 C17 C18 57.2(4) . .
Li2 C16 C17 C18 -56.3(4) . .
B2 C16 C17 Li3 -57.3(4) . .
Li2 C16 C17 Li3 -113.5(3) . .
B2 C16 C17 Li2 56.2(4) . .
Li3 C16 C17 Li2 113.5(3) . .
N4 Li3 C17 C16 -130.0(6) . .
C18 Li3 C17 C16 132.1(3) . .
C19 Li3 C17 C16 102.1(3) . .
C20 Li3 C17 C16 67.6(3) . .
B2 Li3 C17 C16 29.3(2) . .
Si4 Li3 C17 C16 -82.2(4) . .
Si3 Li3 C17 C16 171.5(6) . .
Li4 Li3 C17 C16 -143.9(3) . .
N4 Li3 C17 C18 97.8(6) . .
C19 Li3 C17 C18 -30.0(2) . .
C16 Li3 C17 C18 -132.1(3) . .
C20 Li3 C17 C18 -64.5(3) . .
B2 Li3 C17 C18 -102.8(3) . .
Si4 Li3 C17 C18 145.6(4) . .
Si3 Li3 C17 C18 39.3(6) . .
Li4 Li3 C17 C18 83.9(3) . .
N4 Li3 C17 Li2 160.4(5) . .
C18 Li3 C17 Li2 62.6(3) . .
C19 Li3 C17 Li2 32.5(3) . .
C16 Li3 C17 Li2 -69.6(3) . .
C20 Li3 C17 Li2 -1.9(3) . .
B2 Li3 C17 Li2 -40.2(3) . .
Si4 Li3 C17 Li2 -151.8(3) . .
Si3 Li3 C17 Li2 101.9(6) . .
Li4 Li3 C17 Li2 146.5(3) . .
N2 Li2 C17 C16 121.4(6) . .
C18 Li2 C17 C16 -132.3(4) . .
C19 Li2 C17 C16 -101.7(3) . .
C20 Li2 C17 C16 -67.0(3) . .
B2 Li2 C17 C16 -28.9(2) . .
Si1 Li2 C17 C16 76.3(4) . .
Si2 Li2 C17 C16 177.7(7) . .
Li1 Li2 C17 C16 138.0(3) . .
N2 Li2 C17 C18 -106.2(6) . .
C19 Li2 C17 C18 30.6(2) . .
C20 Li2 C17 C18 65.3(3) . .
C16 Li2 C17 C18 132.3(4) . .
B2 Li2 C17 C18 103.5(3) . .
Si1 Li2 C17 C18 -151.3(4) . .
Si2 Li2 C17 C18 -49.9(7) . .
Li1 Li2 C17 C18 -89.7(3) . .
N2 Li2 C17 Li3 -169.6(5) . .
C18 Li2 C17 Li3 -63.3(3) . .
C19 Li2 C17 Li3 -32.7(3) . .
C20 Li2 C17 Li3 2.0(3) . .
C16 Li2 C17 Li3 69.0(3) . .
B2 Li2 C17 Li3 40.1(3) . .
Si1 Li2 C17 Li3 145.3(3) . .
Si2 Li2 C17 Li3 -113.3(7) . .
Li1 Li2 C17 Li3 -153.0(3) . .
C16 C17 C18 C19 -0.6(6) . .
Li3 C17 C18 C19 57.9(4) . .
Li2 C17 C18 C19 -59.1(4) . .
C16 C17 C18 Li2 58.6(4) . .
Li3 C17 C18 Li2 117.1(3) . .
C16 C17 C18 Li3 -58.5(4) . .
Li2 C17 C18 Li3 -117.1(3) . .
N2 Li2 C18 C19 -118.3(5) . .
C17 Li2 C18 C19 128.5(4) . .
C20 Li2 C18 C19 27.4(2) . .
C16 Li2 C18 C19 100.6(3) . .
B2 Li2 C18 C19 64.3(3) . .
Si1 Li2 C18 C19 -173.8(7) . .
Si2 Li2 C18 C19 -75.0(4) . .
Li1 Li2 C18 C19 -134.6(3) . .
N2 Li2 C18 C17 113.2(5) . .
C19 Li2 C18 C17 -128.5(4) . .
C20 Li2 C18 C17 -101.1(3) . .
C16 Li2 C18 C17 -27.9(2) . .
B2 Li2 C18 C17 -64.2(3) . .
Si1 Li2 C18 C17 57.6(7) . .
Si2 Li2 C18 C17 156.5(4) . .
Li1 Li2 C18 C17 96.9(3) . .
N2 Li2 C18 Li3 177.1(4) . .
C19 Li2 C18 Li3 -64.7(3) . .
C17 Li2 C18 Li3 63.9(3) . .
C20 Li2 C18 Li3 -37.2(3) . .
C16 Li2 C18 Li3 36.0(3) . .
B2 Li2 C18 Li3 -0.3(3) . .
Si1 Li2 C18 Li3 121.5(7) . .
Si2 Li2 C18 Li3 -139.7(3) . .
Li1 Li2 C18 Li3 160.8(3) . .
N4 Li3 C18 C19 110.4(5) . .
C17 Li3 C18 C19 -129.4(3) . .
C16 Li3 C18 C19 -101.2(3) . .
C20 Li3 C18 C19 -27.6(2) . .
B2 Li3 C18 C19 -64.5(3) . .
Si4 Li3 C18 C19 156.9(7) . .
Si3 Li3 C18 C19 71.2(3) . .
Li4 Li3 C18 C19 129.3(3) . .
N4 Li3 C18 C17 -120.2(5) . .
C19 Li3 C18 C17 129.4(3) . .
C16 Li3 C18 C17 28.2(2) . .
C20 Li3 C18 C17 101.7(3) . .
B2 Li3 C18 C17 64.9(2) . .
Si4 Li3 C18 C17 -73.7(7) . .
Si3 Li3 C18 C17 -159.5(3) . .
Li4 Li3 C18 C17 -101.4(3) . .
N4 Li3 C18 Li2 175.2(4) . .
C17 Li3 C18 Li2 -64.6(3) . .
C19 Li3 C18 Li2 64.8(3) . .
C16 Li3 C18 Li2 -36.4(3) . .
C20 Li3 C18 Li2 37.2(3) . .
B2 Li3 C18 Li2 0.3(3) . .
Si4 Li3 C18 Li2 -138.3(6) . .
Si3 Li3 C18 Li2 136.0(3) . .
Li4 Li3 C18 Li2 -165.9(3) . .
C17 C18 C19 C20 1.2(6) . .
Li2 C18 C19 C20 -58.0(4) . .
Li3 C18 C19 C20 58.8(4) . .
C17 C18 C19 Li2 59.2(4) . .
Li3 C18 C19 Li2 116.8(3) . .
C17 C18 C19 Li3 -57.6(4) . .
Li2 C18 C19 Li3 -116.8(3) . .
N2 Li2 C19 C20 -124.1(6) . .
C18 Li2 C19 C20 132.9(4) . .
C17 Li2 C19 C20 102.3(3) . .
C16 Li2 C19 C20 67.2(3) . .
B2 Li2 C19 C20 29.5(2) . .
Si1 Li2 C19 C20 -67(2) . .
Si2 Li2 C19 C20 -104.3(3) . .
Li1 Li2 C19 C20 -171.0(4) . .
N2 Li2 C19 C18 103.0(6) . .
C17 Li2 C19 C18 -30.6(2) . .
C20 Li2 C19 C18 -132.9(4) . .
C16 Li2 C19 C18 -65.7(3) . .
B2 Li2 C19 C18 -103.4(3) . .
Si1 Li2 C19 C18 160(2) . .
Si2 Li2 C19 C18 122.8(3) . .
Li1 Li2 C19 C18 56.1(4) . .
N2 Li2 C19 Li3 165.9(5) . .
C18 Li2 C19 Li3 63.0(3) . .
C17 Li2 C19 Li3 32.4(3) . .
C20 Li2 C19 Li3 -70.0(3) . .
C16 Li2 C19 Li3 -2.7(3) . .
B2 Li2 C19 Li3 -40.4(3) . .
Si1 Li2 C19 Li3 -137(2) . .
Si2 Li2 C19 Li3 -174.3(3) . .
Li1 Li2 C19 Li3 119.0(3) . .
N4 Li3 C19 C20 123.0(5) . .
C17 Li3 C19 C20 -102.3(3) . .
C18 Li3 C19 C20 -132.5(3) . .
C16 Li3 C19 C20 -67.1(2) . .
B2 Li3 C19 C20 -29.2(2) . .
Si4 Li3 C19 C20 90.7(13) . .
Si3 Li3 C19 C20 105.3(3) . .
Li4 Li3 C19 C20 168.3(3) . .
N4 Li3 C19 C18 -104.5(5) . .
C17 Li3 C19 C18 30.2(2) . .
C16 Li3 C19 C18 65.4(2) . .
C20 Li3 C19 C18 132.5(3) . .
B2 Li3 C19 C18 103.3(3) . .
Si4 Li3 C19 C18 -136.8(13) . .
Si3 Li3 C19 C18 -122.3(3) . .
Li4 Li3 C19 C18 -59.3(3) . .
N4 Li3 C19 Li2 -167.2(5) . .
C17 Li3 C19 Li2 -32.5(3) . .
C18 Li3 C19 Li2 -62.6(3) . .
C16 Li3 C19 Li2 2.7(3) . .
C20 Li3 C19 Li2 69.8(3) . .
B2 Li3 C19 Li2 40.6(3) . .
Si4 Li3 C19 Li2 160.5(12) . .
Si3 Li3 C19 Li2 175.1(3) . .
Li4 Li3 C19 Li2 -121.9(3) . .
C18 C19 C20 B2 -1.0(6) . .
Li2 C19 C20 B2 -57.0(4) . .
Li3 C19 C20 B2 55.8(4) . .
C18 C19 C20 Li2 55.9(4) . .
Li3 C19 C20 Li2 112.8(3) . .
C18 C19 C20 Li3 -56.8(4) . .
Li2 C19 C20 Li3 -112.8(3) . .
N3 B2 C20 C19 -179.5(4) . .
C16 B2 C20 C19 0.3(5) . .
Li3 B2 C20 C19 -53.9(4) . .
Li2 B2 C20 C19 54.6(4) . .
N3 B2 C20 Li2 125.9(4) . .
C16 B2 C20 Li2 -54.4(3) . .
Li3 B2 C20 Li2 -108.5(3) . .
N3 B2 C20 Li3 -125.6(4) . .
C16 B2 C20 Li3 54.1(3) . .
Li2 B2 C20 Li3 108.5(3) . .
N2 Li2 C20 C19 104.8(7) . .
C18 Li2 C20 C19 -28.5(2) . .
C17 Li2 C20 C19 -64.7(3) . .
C16 Li2 C20 C19 -99.9(3) . .
B2 Li2 C20 C19 -132.4(3) . .
Si1 Li2 C20 C19 167.3(5) . .
Si2 Li2 C20 C19 90.2(3) . .
Li1 Li2 C20 C19 18.5(7) . .
N2 Li2 C20 B2 -122.8(7) . .
C18 Li2 C20 B2 104.0(3) . .
C19 Li2 C20 B2 132.4(3) . .
C17 Li2 C20 B2 67.7(2) . .
C16 Li2 C20 B2 32.5(2) . .
Si1 Li2 C20 B2 -60.2(5) . .
Si2 Li2 C20 B2 -137.3(3) . .
Li1 Li2 C20 B2 150.9(7) . .
N2 Li2 C20 Li3 167.7(6) . .
C18 Li2 C20 Li3 34.4(3) . .
C19 Li2 C20 Li3 62.9(3) . .
C17 Li2 C20 Li3 -1.8(3) . .
C16 Li2 C20 Li3 -37.1(2) . .
B2 Li2 C20 Li3 -69.6(3) . .
Si1 Li2 C20 Li3 -129.8(4) . .
Si2 Li2 C20 Li3 153.1(3) . .
Li1 Li2 C20 Li3 81.3(7) . .
N4 Li3 C20 C19 -96.4(6) . .
C17 Li3 C20 C19 64.7(3) . .
C18 Li3 C20 C19 28.6(2) . .
C16 Li3 C20 C19 100.3(3) . .
B2 Li3 C20 C19 133.1(3) . .
Si4 Li3 C20 C19 -154.8(5) . .
Si3 Li3 C20 C19 -85.5(3) . .
Li4 Li3 C20 C19 -20.8(6) . .
N4 Li3 C20 B2 130.5(6) . .
C17 Li3 C20 B2 -68.4(3) . .
C18 Li3 C20 B2 -104.4(3) . .
C19 Li3 C20 B2 -133.1(3) . .
C16 Li3 C20 B2 -32.7(2) . .
Si4 Li3 C20 B2 72.2(5) . .
Si3 Li3 C20 B2 141.4(3) . .
Li4 Li3 C20 B2 -153.8(6) . .
N4 Li3 C20 Li2 -159.3(6) . .
C17 Li3 C20 Li2 1.8(3) . .
C18 Li3 C20 Li2 -34.2(3) . .
C19 Li3 C20 Li2 -62.8(3) . .
C16 Li3 C20 Li2 37.5(3) . .
B2 Li3 C20 Li2 70.2(3) . .
Si4 Li3 C20 Li2 142.4(4) . .
Si3 Li3 C20 Li2 -148.4(3) . .
Li4 Li3 C20 Li2 -83.6(6) . .
B2 N3 C21 C22 -96.6(5) . .
C23 N3 C21 C22 87.1(5) . .
B2 N3 C23 C24 -87.8(5) . .
C21 N3 C23 C24 88.5(5) . .
