#------------------------------------------------------------------------------
#$Date: 2016-03-21 06:52:50 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178538 $
#$URL: svn://www.crystallography.net/cod/cif/4/06/44/4064429.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4064429
loop_
_publ_author_name
'Peitz, Stephan'
'Peulecke, Normen'
'Müller, Bernd H.'
'Spannenberg, Anke'
'Drexler, Hans-Joachim'
'Rosenthal, Uwe'
'Al-Hazmi, Mohammed H.'
'Al-Eidan, Khalid E.'
'Wöhl, Anina'
'Müller, Wolfgang'
_publ_section_title
;
 Heterobimetallic Al−Cl−Cr Intermediates with Relevance to
 the Selective Catalytic Ethene Trimerization Systems Consisting of
 CrCl3(THF)3, the Aminophosphorus Ligands Ph2PN(R)P(Ph)N(R)H, and
 Triethylaluminum
;
_journal_issue                   8
_journal_name_full               Organometallics
_journal_page_first              2364
_journal_paper_doi               10.1021/om200100g
_journal_volume                  30
_journal_year                    2011
_chemical_formula_sum            'C56 H78 Al2 Cl4 Cr2 N4 P4'
_chemical_formula_weight         1230.86
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yn'
_symmetry_space_group_name_H-M   'P 1 21/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 98.103(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   11.4748(5)
_cell_length_b                   15.2374(4)
_cell_length_c                   17.9504(7)
_cell_measurement_reflns_used    6243
_cell_measurement_temperature    150(2)
_cell_measurement_theta_max      28.35
_cell_measurement_theta_min      1.75
_cell_volume                     3107.2(2)
_computing_cell_refinement       X-AREA
_computing_data_collection       'X-AREA (Stoe & Cie, 2005)'
_computing_data_reduction        X-AREA
_computing_molecular_graphics    'DIAMOND (Brandenburg, 2007)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      150(2)
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.993
_diffrn_measurement_device_type  'STOE IPDS II'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0659
_diffrn_reflns_av_sigmaI/netI    0.0591
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -20
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_number            54911
_diffrn_reflns_theta_full        27.99
_diffrn_reflns_theta_max         27.99
_diffrn_reflns_theta_min         1.76
_exptl_absorpt_coefficient_mu    0.691
_exptl_absorpt_correction_T_max  0.9150
_exptl_absorpt_correction_T_min  0.5982
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details   'X-SHAPE and X-RED32 (Stoe & Cie, 2005)'
_exptl_crystal_colour            blue
_exptl_crystal_density_diffrn    1.316
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             1288
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.25
_exptl_crystal_size_min          0.07
_refine_diff_density_max         1.084
_refine_diff_density_min         -0.708
_refine_diff_density_rms         0.079
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.946
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     286
_refine_ls_number_reflns         7419
_refine_ls_number_restraints     23
_refine_ls_restrained_S_all      0.948
_refine_ls_R_factor_all          0.0851
_refine_ls_R_factor_gt           0.0534
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0843P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1315
_refine_ls_wR_factor_ref         0.1407
_reflns_number_gt                4891
_reflns_number_total             7419
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om200100g_si_002.cif
_cod_data_source_block           2a
_cod_original_sg_symbol_H-M      'P 21/n'
_cod_database_code               4064429
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C25A C 0.4884(5) 0.0920(5) 0.6489(3) 0.0666(16) Uiso 0.779(8) 1 d PDU A 1
H25A H 0.4737 0.0348 0.6232 0.080 Uiso 0.779(8) 1 calc PR A 1
H25B H 0.4666 0.1389 0.6114 0.080 Uiso 0.779(8) 1 calc PR A 1
C26A C 0.6177(5) 0.0997(5) 0.6793(4) 0.0767(17) Uiso 0.779(8) 1 d PDU A 1
H26A H 0.6643 0.0954 0.6377 0.115 Uiso 0.779(8) 1 calc PR A 1
H26B H 0.6400 0.0522 0.7153 0.115 Uiso 0.779(8) 1 calc PR A 1
H26C H 0.6325 0.1564 0.7046 0.115 Uiso 0.779(8) 1 calc PR A 1
C25B C 0.5184(17) 0.1122(13) 0.6682(14) 0.069(2) Uiso 0.221(8) 1 d PDU A 2
H25C H 0.4835 0.1410 0.6208 0.083 Uiso 0.221(8) 1 calc PR A 2
H25D H 0.5749 0.1548 0.6947 0.083 Uiso 0.221(8) 1 calc PR A 2
C26B C 0.592(2) 0.0371(14) 0.6453(14) 0.071(2) Uiso 0.221(8) 1 d PDU A 2
H26D H 0.6543 0.0602 0.6190 0.107 Uiso 0.221(8) 1 calc PR A 2
H26E H 0.5415 -0.0026 0.6119 0.107 Uiso 0.221(8) 1 calc PR A 2
H26F H 0.6267 0.0050 0.6903 0.107 Uiso 0.221(8) 1 calc PR A 2
C27A C 0.2242(5) 0.0569(6) 0.7058(4) 0.0690(17) Uiso 0.628(8) 1 d PDU A 1
H27A H 0.2250 -0.0058 0.7201 0.083 Uiso 0.628(8) 1 calc PR A 1
H27B H 0.1756 0.0879 0.7389 0.083 Uiso 0.628(8) 1 calc PR A 1
C28A C 0.1609(8) 0.0638(6) 0.6263(4) 0.078(2) Uiso 0.628(8) 1 d PDU A 1
H28A H 0.0818 0.0388 0.6239 0.117 Uiso 0.628(8) 1 calc PR A 1
H28B H 0.2050 0.0315 0.5922 0.117 Uiso 0.628(8) 1 calc PR A 1
H28C H 0.1548 0.1257 0.6112 0.117 Uiso 0.628(8) 1 calc PR A 1
C27B C 0.2460(8) 0.0520(10) 0.6688(6) 0.074(2) Uiso 0.372(8) 1 d PDU A 2
H27C H 0.2170 0.0919 0.6267 0.089 Uiso 0.372(8) 1 calc PR A 2
H27D H 0.2636 -0.0059 0.6480 0.089 Uiso 0.372(8) 1 calc PR A 2
C28B C 0.1558(13) 0.0431(10) 0.7221(8) 0.073(3) Uiso 0.372(8) 1 d PDU A 2
H28D H 0.0821 0.0204 0.6947 0.110 Uiso 0.372(8) 1 calc PR A 2
H28E H 0.1416 0.1007 0.7434 0.110 Uiso 0.372(8) 1 calc PR A 2
H28F H 0.1853 0.0025 0.7628 0.110 Uiso 0.372(8) 1 calc PR A 2
C1 C 0.3690(3) 0.2928(2) 0.7417(2) 0.0407(8) Uani 1 1 d . . .
H1 H 0.3446 0.3384 0.7764 0.049 Uiso 1 1 calc R . .
C2 C 0.4814(4) 0.3239(3) 0.7140(3) 0.0634(12) Uani 1 1 d . . .
H2A H 0.5410 0.3369 0.7572 0.095 Uiso 1 1 calc R . .
H2B H 0.4648 0.3769 0.6834 0.095 Uiso 1 1 calc R . .
H2C H 0.5107 0.2777 0.6834 0.095 Uiso 1 1 calc R . .
C3 C 0.2723(4) 0.2831(3) 0.6765(2) 0.0528(10) Uani 1 1 d . . .
H3A H 0.2992 0.2454 0.6381 0.079 Uiso 1 1 calc R . .
H3B H 0.2513 0.3410 0.6549 0.079 Uiso 1 1 calc R . .
H3C H 0.2033 0.2566 0.6941 0.079 Uiso 1 1 calc R . .
C4A C 0.5327(6) 0.2921(3) 0.8999(4) 0.032(4) Uiso 0.526(11) 1 d PG A 1
C5A C 0.5131(4) 0.3797(4) 0.9156(4) 0.0408(18) Uiso 0.526(11) 1 d PG A 1
H5A H 0.4354 0.3999 0.9182 0.049 Uiso 0.526(11) 1 calc PR A 1
C6A C 0.6071(4) 0.4379(3) 0.9275(4) 0.054(2) Uiso 0.526(11) 1 d PG A 1
H6A H 0.5937 0.4979 0.9382 0.064 Uiso 0.526(11) 1 calc PR A 1
C7A C 0.7208(4) 0.4085(4) 0.9237(4) 0.0419(19) Uiso 0.526(11) 1 d PG A 1
H7A H 0.7851 0.4483 0.9318 0.050 Uiso 0.526(11) 1 calc PR A 1
C8A C 0.7404(5) 0.3208(4) 0.9080(5) 0.047(7) Uiso 0.526(11) 1 d PG A 1
H8A H 0.8181 0.3007 0.9055 0.056 Uiso 0.526(11) 1 calc PR A 1
C9A C 0.6464(7) 0.2626(3) 0.8961(6) 0.038(4) Uiso 0.526(11) 1 d PG A 1
H9A H 0.6598 0.2027 0.8854 0.046 Uiso 0.526(11) 1 calc PR A 1
C4B C 0.5356(6) 0.2870(4) 0.9061(5) 0.033(5) Uiso 0.474(11) 1 d PG A 2
C5B C 0.5232(4) 0.3632(4) 0.9469(4) 0.0351(19) Uiso 0.474(11) 1 d PG A 2
H5B H 0.4481 0.3794 0.9590 0.042 Uiso 0.474(11) 1 calc PR A 2
C6B C 0.6206(5) 0.4157(4) 0.9699(5) 0.048(2) Uiso 0.474(11) 1 d PG A 2
H6B H 0.6122 0.4678 0.9977 0.058 Uiso 0.474(11) 1 calc PR A 2
C7B C 0.7304(4) 0.3921(4) 0.9522(5) 0.046(2) Uiso 0.474(11) 1 d PG A 2
H7B H 0.7970 0.4280 0.9679 0.056 Uiso 0.474(11) 1 calc PR A 2
C8B C 0.7428(5) 0.3159(5) 0.9114(5) 0.044(7) Uiso 0.474(11) 1 d PG A 2
H8B H 0.8179 0.2998 0.8993 0.053 Uiso 0.474(11) 1 calc PR A 2
C9B C 0.6454(7) 0.2634(4) 0.8884(6) 0.036(5) Uiso 0.474(11) 1 d PG A 2
H9B H 0.6539 0.2113 0.8606 0.044 Uiso 0.474(11) 1 calc PR A 2
C10 C 0.2255(3) 0.3210(2) 0.9035(2) 0.0335(7) Uani 1 1 d . . .
H10 H 0.2722 0.3637 0.8774 0.040 Uiso 1 1 calc R . .
C11 C 0.1928(3) 0.3671(2) 0.9722(2) 0.0436(8) Uani 1 1 d . . .
H11A H 0.1502 0.3263 1.0008 0.065 Uiso 1 1 calc R . .
H11B H 0.1425 0.4176 0.9564 0.065 Uiso 1 1 calc R . .
H11C H 0.2644 0.3871 1.0038 0.065 Uiso 1 1 calc R . .
C12 C 0.1165(3) 0.2988(3) 0.8488(2) 0.0433(8) Uani 1 1 d . . .
H12A H 0.1387 0.2630 0.8077 0.065 Uiso 1 1 calc R . .
H12B H 0.0792 0.3532 0.8282 0.065 Uiso 1 1 calc R . .
H12C H 0.0611 0.2661 0.8751 0.065 Uiso 1 1 calc R . .
C13 C 0.3122(2) 0.19265(17) 1.07708(10) 0.0400(8) Uani 1 1 d G A .
C14 C 0.2659(2) 0.14585(16) 1.13256(14) 0.0502(10) Uani 1 1 d G . .
H14 H 0.2148 0.0976 1.1191 0.060 Uiso 1 1 calc R . .
C15 C 0.2944(3) 0.1696(2) 1.20768(12) 0.0664(14) Uani 1 1 d G . .
H15 H 0.2628 0.1376 1.2456 0.080 Uiso 1 1 calc R . .
C16 C 0.3693(3) 0.2402(2) 1.22733(11) 0.0777(17) Uani 1 1 d G . .
H16 H 0.3887 0.2564 1.2787 0.093 Uiso 1 1 calc R . .
C17 C 0.4156(2) 0.2870(2) 1.17184(16) 0.0795(16) Uani 1 1 d G . .
H17 H 0.4667 0.3352 1.1853 0.095 Uiso 1 1 calc R . .
C18 C 0.3871(2) 0.26321(18) 1.09672(13) 0.0569(11) Uani 1 1 d G . .
H18 H 0.4187 0.2952 1.0588 0.068 Uiso 1 1 calc R . .
C19 C 0.1256(3) 0.1280(2) 0.96372(19) 0.0330(7) Uani 1 1 d . A .
C20 C 0.0912(3) 0.0741(2) 0.9033(2) 0.0438(8) Uani 1 1 d . . .
H20 H 0.1486 0.0501 0.8757 0.053 Uiso 1 1 calc R . .
C21 C -0.0276(4) 0.0542(3) 0.8822(3) 0.0540(10) Uani 1 1 d . . .
H21 H -0.0514 0.0181 0.8397 0.065 Uiso 1 1 calc R . .
C22 C -0.1098(3) 0.0871(3) 0.9231(3) 0.0522(10) Uani 1 1 d . . .
H22 H -0.1907 0.0739 0.9086 0.063 Uiso 1 1 calc R . .
C23 C -0.0761(3) 0.1391(3) 0.9851(2) 0.0469(9) Uani 1 1 d . . .
H23 H -0.1334 0.1603 1.0141 0.056 Uiso 1 1 calc R . .
C24 C 0.0411(3) 0.1604(2) 1.0052(2) 0.0387(8) Uani 1 1 d . . .
H24 H 0.0641 0.1972 1.0474 0.046 Uiso 1 1 calc R . .
N1 N 0.3889(2) 0.20828(17) 0.78466(15) 0.0306(5) Uani 1 1 d . A .
N2 N 0.3022(2) 0.24223(16) 0.92240(14) 0.0267(5) Uani 1 1 d . A .
Al1 Al 0.38849(12) 0.10168(7) 0.73054(6) 0.0475(3) Uani 1 1 d D . .
P1 P 0.41694(7) 0.20902(5) 0.87639(4) 0.02633(17) Uani 1 1 d . . .
P2 P 0.28050(7) 0.15760(5) 0.97981(5) 0.02921(18) Uani 1 1 d . . .
Cl2 Cl 0.62261(7) 0.06921(5) 1.01239(5) 0.0411(2) Uani 1 1 d . . .
Cr1 Cr 0.42799(4) 0.06437(3) 0.93359(3) 0.02582(13) Uani 1 1 d . . .
Cl1 Cl 0.46905(14) 0.00235(7) 0.81657(6) 0.0707(4) Uani 1 1 d . A .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
C26A C25A Al1 111.5(4) .
C26B C25B Al1 125.5(14) .
C28A C27A Al1 120.0(6) .
C28B C27B Al1 105.3(8) .
C3 C1 N1 111.0(3) .
C3 C1 C2 110.1(3) .
N1 C1 C2 111.2(3) .
C5A C4A C9A 120.0 .
C5A C4A P1 125.1(4) .
C9A C4A P1 114.8(4) .
C4A C5A C6A 120.0 .
C7A C6A C5A 120.0 .
C6A C7A C8A 120.0 .
C9A C8A C7A 120.0 .
C8A C9A C4A 120.0 .
C5B C4B C9B 120.0 .
C5B C4B P1 124.7(4) .
C9B C4B P1 115.2(4) .
C4B C5B C6B 120.0 .
C7B C6B C5B 120.0 .
C6B C7B C8B 120.0 .
C7B C8B C9B 120.0 .
C8B C9B C4B 120.0 .
N2 C10 C11 113.1(3) .
N2 C10 C12 112.0(3) .
C11 C10 C12 110.8(3) .
C14 C13 C18 120.0 .
C14 C13 P2 119.59(14) .
C18 C13 P2 120.34(14) .
C15 C14 C13 120.0 .
C14 C15 C16 120.0 .
C15 C16 C17 120.0 .
C18 C17 C16 120.0 .
C17 C18 C13 120.0 .
C20 C19 C24 119.3(3) .
C20 C19 P2 116.1(3) .
C24 C19 P2 124.5(3) .
C19 C20 C21 120.3(4) .
C22 C21 C20 119.7(4) .
C21 C22 C23 120.6(4) .
C22 C23 C24 119.9(4) .
C23 C24 C19 120.2(4) .
C1 N1 P1 120.4(2) .
C1 N1 Al1 118.9(2) .
P1 N1 Al1 120.64(15) .
C10 N2 P2 128.1(2) .
C10 N2 P1 126.1(2) .
P2 N2 P1 104.82(13) .
N1 Al1 C25A 118.8(2) .
N1 Al1 C27B 123.6(4) .
C25A Al1 C27B 94.3(4) .
N1 Al1 C25B 105.8(7) .
C27B Al1 C25B 109.8(9) .
N1 Al1 C27A 109.9(3) .
C25A Al1 C27A 115.8(3) .
C25B Al1 C27A 131.4(9) .
N1 Al1 Cl1 104.62(10) .
C25A Al1 Cl1 103.3(2) .
C27B Al1 Cl1 110.5(5) .
C25B Al1 Cl1 99.8(7) .
C27A Al1 Cl1 101.9(2) .
N1 P1 N2 115.42(13) .
N1 P1 C4B 109.4(3) .
N2 P1 C4B 104.9(2) .
N1 P1 C4A 105.6(3) .
N2 P1 C4A 105.3(2) .
N1 P1 Cr1 114.29(10) .
N2 P1 Cr1 93.54(9) .
C4B P1 Cr1 118.3(3) .
C4A P1 Cr1 122.3(2) .
N2 P2 C13 109.60(12) .
N2 P2 C19 108.50(14) .
C13 P2 C19 106.58(14) .
N2 P2 Cr1 93.89(9) .
C13 P2 Cr1 116.34(9) .
C19 P2 Cr1 120.71(11) .
Cr1 Cl2 Cr1 87.40(3) 3_657
Cl2 Cr1 Cl1 96.28(4) 3_657
Cl2 Cr1 P1 162.74(3) 3_657
Cl1 Cr1 P1 89.56(3) .
Cl2 Cr1 P2 98.02(3) 3_657
Cl1 Cr1 P2 138.95(4) .
P1 Cr1 P2 67.55(3) .
Cl2 Cr1 Cl2 92.60(3) 3_657
Cl1 Cr1 Cl2 103.82(5) .
P1 Cr1 Cl2 101.78(3) .
P2 Cr1 Cl2 113.69(4) .
Al1 Cl1 Cr1 102.78(5) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C25A C26A 1.511(7) .
C25A Al1 1.989(4) .
C25B C26B 1.510(7) .
C25B Al1 1.992(5) .
C27A C28A 1.511(7) .
C27A Al1 1.995(5) .
C27B C28B 1.510(7) .
C27B Al1 1.991(5) .
C1 C3 1.501(6) .
C1 N1 1.502(4) .
C1 C2 1.521(6) .
C4A C5A 1.3900 .
C4A C9A 1.3900 .
C4A P1 1.840(4) .
C5A C6A 1.3900 .
C6A C7A 1.3900 .
C7A C8A 1.3900 .
C8A C9A 1.3900 .
C4B C5B 1.3900 .
C4B C9B 1.3900 .
C4B P1 1.829(5) .
C5B C6B 1.3900 .
C6B C7B 1.3900 .
C7B C8B 1.3900 .
C8B C9B 1.3900 .
C10 N2 1.499(4) .
C10 C11 1.512(5) .
C10 C12 1.514(5) .
C13 C14 1.3900 .
C13 C18 1.3900 .
C13 P2 1.8130(19) .
C14 C15 1.3900 .
C15 C16 1.3900 .
C16 C17 1.3900 .
C17 C18 1.3900 .
C19 C20 1.374(5) .
C19 C24 1.394(5) .
C19 P2 1.817(3) .
C20 C21 1.396(5) .
C21 C22 1.369(6) .
C22 C23 1.377(6) .
C23 C24 1.381(5) .
N1 P1 1.633(3) .
N1 Al1 1.892(3) .
N2 P2 1.691(3) .
N2 P1 1.726(3) .
Al1 Cl1 2.2644(15) .
P1 Cr1 2.4273(9) .
P2 Cr1 2.4426(9) .
Cl2 Cr1 2.3620(9) 3_657
Cl2 Cr1 2.4703(9) .
Cr1 Cl2 2.3620(9) 3_657
Cr1 Cl1 2.4098(11) .
