#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/06/71/4067152.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4067152
loop_
_publ_author_name
'Yuki, Masahiro'
'Miyake, Yoshihiro'
'Nishibayashi, Yoshiaki'
_publ_section_title
;
 Preparation of Thiolate-Bridged Dinuclear Ruthenium Complexes Bearing a
 Phosphine Ligand and Application to Propargylic Reduction of Propargylic
 Alcohols with 2-Propanol
;
_journal_issue                   22
_journal_name_full               Organometallics
_journal_page_first              5994
_journal_paper_doi               10.1021/om100852x
_journal_volume                  29
_journal_year                    2010
_chemical_formula_sum            'C40.5 H44 Cl F6 O6 P Ru2 S4'
_chemical_formula_weight         1137.56
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           12
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2y'
_symmetry_space_group_name_H-M   'C 1 2/m 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 109.7230(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   18.0789(7)
_cell_length_b                   12.7091(6)
_cell_length_c                   20.9807(7)
_cell_measurement_temperature    173(1)
_cell_volume                     4537.9(3)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      173(1)
_diffrn_measured_fraction_theta_full 0.989
_diffrn_measured_fraction_theta_max 0.989
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71069
_diffrn_reflns_av_R_equivalents  0.0407
_diffrn_reflns_av_sigmaI/netI    0.0343
_diffrn_reflns_limit_h_max       23
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       26
_diffrn_reflns_limit_l_min       -27
_diffrn_reflns_number            22117
_diffrn_reflns_theta_full        27.45
_diffrn_reflns_theta_max         27.45
_diffrn_reflns_theta_min         3.09
_exptl_absorpt_coefficient_mu    1.013
_exptl_absorpt_correction_T_max  0.9427
_exptl_absorpt_correction_T_min  0.7973
_exptl_absorpt_correction_type   numerical
_exptl_crystal_colour            green
_exptl_crystal_density_diffrn    1.665
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       platelet
_exptl_crystal_F_000             2292
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.03
_refine_diff_density_max         1.683
_refine_diff_density_min         -1.461
_refine_diff_density_rms         0.147
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.077
_refine_ls_hydrogen_treatment    riding
_refine_ls_matrix_type           full
_refine_ls_number_parameters     267
_refine_ls_number_reflns         5375
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.077
_refine_ls_R_factor_all          0.0617
_refine_ls_R_factor_gt           0.0543
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0993P)²+28.5079P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1652
_refine_ls_wR_factor_ref         0.1704
_reflns_number_gt                4635
_reflns_number_total             5375
_reflns_threshold_expression     >2σ(I)
_cod_data_source_file            om100852x_si_002.cif
_cod_data_source_block           4a
_cod_original_formula_sum        'C40.50 H44 Cl F6 O6 P Ru2 S4'
_cod_database_code               4067152
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
'-x, -y, -z'
'x, -y, z'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
P1 P 0.32522(9) 0.0000 0.26529(8) 0.0241(3) Uani 1 2 d S
S1 S 0.45261(6) 0.14846(8) 0.24450(5) 0.0260(2) Uani 1 1 d .
S2 S 0.29644(9) 0.5000 0.50355(8) 0.0282(3) Uani 1 2 d S
S3 S 0.2665 0.0000 0.8994 0.164(3) Uani 1 2 d S
Ru1 Ru 0.39206(3) 0.0000 0.18943(2) 0.02500(16) Uani 1 2 d S
Ru2 Ru 0.52467(3) 0.0000 0.29114(2) 0.02150(15) Uani 1 2 d S
Cl1 Cl 0.5000 0.3887(5) 0.0000 0.160(2) Uani 1 2 d S
C1 C 0.4230(4) 0.0000 0.0914(3) 0.064(5) Uiso 0.50 2 d SPG
C2 C 0.3692(4) 0.0870(3) 0.0884(4) 0.059(9) Uiso 0.25 1 d PG
C3 C 0.2956(4) 0.0421(5) 0.0874(3) 0.058(12) Uiso 0.25 1 d PG
C4 C 0.3040(4) -0.0707(5) 0.0898(3) 0.042(7) Uiso 0.25 1 d PG
C5 C 0.3827(4) -0.0955(3) 0.0924(4) 0.048(7) Uiso 0.25 1 d PG
C6 C 0.5081(5) 0.0133(3) 0.0935(5) 0.155(18) Uiso 0.25 1 d PG
C7 C 0.3871(6) 0.2046(5) 0.0865(7) 0.085(10) Uiso 0.25 1 d PG
C8 C 0.2216(5) 0.1035(8) 0.0842(5) 0.039(4) Uiso 0.25 1 d PG
C9 C 0.2403(5) -0.1503(8) 0.0897(6) 0.051(6) Uiso 0.25 1 d PG
C10 C 0.4174(6) -0.2061(5) 0.0955(7) 0.121(16) Uiso 0.25 1 d PG
C1B C 0.2926(4) -0.0357(5) 0.0944(3) 0.022(5) Uiso 0.25 1 d PG
C2B C 0.3198(4) 0.0689(4) 0.0925(3) 0.016(4) Uiso 0.25 1 d PG
C3B C 0.3981(4) 0.06340(19) 0.0917(3) 0.018(3) Uiso 0.25 1 d PG
C4B C 0.4193(4) -0.04461(11) 0.0932(3) 0.018(3) Uiso 0.25 1 d PG
C5B C 0.3542(4) -0.1059(4) 0.0948(4) 0.019(3) Uiso 0.25 1 d PG
C6B C 0.2124(5) -0.0669(8) 0.0957(5) 0.109(14) Uiso 0.25 1 d PG
C7B C 0.2736(6) 0.1685(7) 0.0914(6) 0.066(7) Uiso 0.25 1 d PG
C8B C 0.4498(6) 0.1561(4) 0.0897(6) 0.054(6) Uiso 0.25 1 d PG
C9B C 0.4975(5) -0.0869(4) 0.0930(5) 0.056(6) Uiso 0.25 1 d PG
C10B C 0.3508(6) -0.2247(6) 0.0967(8) 0.064(7) Uiso 0.25 1 d PG
C11 C 0.3533(2) 0.1163(3) 0.3188(2) 0.0265(8) Uani 1 1 d .
C12 C 0.4063(2) 0.1846(3) 0.3051(2) 0.0258(8) Uani 1 1 d .
C13 C 0.4246(3) 0.2816(4) 0.3384(3) 0.0341(10) Uani 1 1 d .
H13 H 0.4581 0.3285 0.3277 0.041 Uiso 1 1 calc R
C14 C 0.3924(3) 0.3064(4) 0.3872(3) 0.0403(12) Uani 1 1 d .
H14 H 0.4049 0.3703 0.4099 0.048 Uiso 1 1 calc R
C15 C 0.3419(3) 0.2378(5) 0.4031(3) 0.0400(11) Uani 1 1 d .
H15 H 0.3218 0.2550 0.4371 0.048 Uiso 1 1 calc R
C16 C 0.3211(3) 0.1431(4) 0.3684(2) 0.0342(10) Uani 1 1 d .
H16 H 0.2859 0.0979 0.3783 0.041 Uiso 1 1 calc R
C17 C 0.2186(4) 0.0000 0.2379(3) 0.0335(14) Uani 1 2 d S
C18 C 0.1776(3) 0.0943(6) 0.2257(3) 0.0572(17) Uani 1 1 d .
H18 H 0.2045 0.1580 0.2327 0.069 Uiso 1 1 calc R
C19 C 0.0959(4) 0.0929(8) 0.2030(5) 0.091(3) Uani 1 1 d .
H19 H 0.0681 0.1559 0.1953 0.110 Uiso 1 1 calc R
C20 C 0.0564(6) 0.0000 0.1918(8) 0.105(5) Uani 1 2 d S
H20 H 0.0018 0.0000 0.1764 0.126 Uiso 1 2 calc SR
C21 C 0.5961(4) 0.0000 0.3999(3) 0.0369(15) Uani 1 2 d S
C22 C 0.6164(3) 0.0915(4) 0.3689(3) 0.0364(11) Uani 1 1 d .
C23 C 0.6441(3) 0.0563(4) 0.3172(2) 0.0315(10) Uani 1 1 d .
C24 C 0.5623(6) 0.0000 0.4561(4) 0.066(3) Uani 1 2 d S
H24A H 0.6032 0.0142 0.4983 0.099 Uiso 0.50 1 calc PR
H24B H 0.5395 -0.0675 0.4584 0.099 Uiso 0.50 1 calc PR
H24C H 0.5225 0.0533 0.4477 0.099 Uiso 0.50 1 calc PR
C25 C 0.6151(4) 0.2015(5) 0.3926(4) 0.0602(18) Uani 1 1 d .
H25A H 0.6658 0.2194 0.4242 0.090 Uiso 1 1 calc R
H25B H 0.5764 0.2077 0.4144 0.090 Uiso 1 1 calc R
H25C H 0.6022 0.2485 0.3546 0.090 Uiso 1 1 calc R
C26 C 0.6737(4) 0.1238(6) 0.2730(4) 0.0574(17) Uani 1 1 d .
H26A H 0.6514 0.1929 0.2703 0.086 Uiso 1 1 calc R
H26B H 0.6587 0.0936 0.2285 0.086 Uiso 1 1 calc R
H26C H 0.7299 0.1284 0.2917 0.086 Uiso 1 1 calc R
C27 C 0.3983(4) 0.5000 0.5596(4) 0.0383(15) Uani 1 2 d S
C29 C 0.474(3) 0.5000 0.028(2) 0.140(14) Uiso 0.50 2 d SP
O1 O 0.2659(2) 0.4043(4) 0.5212(2) 0.0580(12) Uani 1 1 d .
O2 O 0.3039(3) 0.5000 0.4375(3) 0.0402(11) Uani 1 2 d S
F1 F 0.4044(4) 0.5000 0.6241(3) 0.086(2) Uani 1 2 d S
F2 F 0.4371(2) 0.4151(3) 0.5496(2) 0.0592(9) Uani 1 1 d .
F3 F 0.1825 0.0000 0.7604 0.258(10) Uani 1 2 d S
F4 F 0.1235 0.0850 0.8118 0.240(6) Uani 1 1 d .
C28 C 0.1784 0.0000 0.8329 0.184(12) Uani 1 2 d S
O4 O 0.2825 0.0959 0.9424 0.44(2) Uani 1 1 d .
O3 O 0.3250 0.0000 0.8688 0.62(5) Uani 1 2 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
S S 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C17 P1 C11 103.89(19) . .
C17 P1 C11 103.89(19) . 6
C11 P1 C11 108.5(3) . 6
C17 P1 Ru1 122.1(2) . .
C11 P1 Ru1 108.92(15) . .
C11 P1 Ru1 108.92(15) 6 .
C12 S1 Ru1 108.02(15) . .
C12 S1 Ru2 103.82(14) . .
Ru1 S1 Ru2 69.29(3) . .
O1 S2 O1 115.9(4) 6_565 .
O1 S2 O2 114.7(2) 6_565 .
O1 S2 O2 114.7(2) . .
O1 S2 C27 103.1(2) 6_565 .
O1 S2 C27 103.1(2) . .
O2 S2 C27 102.7(3) . .
O3 S3 O4 104.696(2) . .
O3 S3 O4 104.696(2) . 6
O4 S3 O4 110.276(3) . 6
O3 S3 C28 105.130(3) . .
O4 S3 C28 115.356(1) . .
O4 S3 C28 115.356(1) 6 .
C2B Ru1 C2B 47.0(3) 6 .
C2B Ru1 C1B 17.07(17) 6 .
C2B Ru1 C1B 37.46(11) . .
C2B Ru1 C1B 37.46(13) 6 6
C2B Ru1 C1B 17.1(2) . 6
C1B Ru1 C1B 23.5(3) . 6
C2B Ru1 C3B 37.41(13) 6 6
C2B Ru1 C3B 59.51(12) . 6
C1B Ru1 C3B 51.92(15) . 6
C1B Ru1 C3B 61.93(16) 6 6
C2B Ru1 C3B 59.5(2) 6 .
C2B Ru1 C3B 37.41(12) . .
C1B Ru1 C3B 61.93(16) . .
C1B Ru1 C3B 51.92(18) 6 .
C3B Ru1 C3B 42.17(10) 6 .
C2B Ru1 S1 146.12(15) 6 .
C2B Ru1 S1 99.94(16) . .
C1B Ru1 S1 136.18(16) . .
C1B Ru1 S1 112.73(16) 6 .
C3B Ru1 S1 126.57(13) 6 .
C3B Ru1 S1 90.15(12) . .
C2B Ru1 S1 99.94(14) 6 6
C2B Ru1 S1 146.12(14) . 6
C1B Ru1 S1 112.73(16) . 6
C1B Ru1 S1 136.18(16) 6 6
C3B Ru1 S1 90.15(9) 6 6
C3B Ru1 S1 126.57(10) . 6
S1 Ru1 S1 111.03(5) . 6
C2B Ru1 P1 110.74(17) 6 .
C2B Ru1 P1 110.74(17) . .
C1B Ru1 P1 99.51(17) . .
C1B Ru1 P1 99.51(17) 6 .
C3B Ru1 P1 146.39(16) 6 .
C3B Ru1 P1 146.39(14) . .
S1 Ru1 P1 85.65(4) . .
S1 Ru1 P1 85.65(4) 6 .
C2B Ru1 C2 24.34(10) 6 6
C2B Ru1 C2 58.15(14) . 6
C1B Ru1 C2 40.55(11) . 6
C1B Ru1 C2 55.63(16) 6 6
C3B Ru1 C2 14.76(5) 6 6
C3B Ru1 C2 51.59(14) . 6
S1 Ru1 C2 140.15(15) . 6
S1 Ru1 C2 88.59(11) 6 6
P1 Ru1 C2 131.63(17) . 6
C2B Ru1 C2 58.1(2) 6 .
C2B Ru1 C2 24.34(8) . .
C1B Ru1 C2 55.63(15) . .
C1B Ru1 C2 40.5(2) 6 .
C3B Ru1 C2 51.59(10) 6 .
C3B Ru1 C2 14.8 . .
S1 Ru1 C2 88.59(15) . .
S1 Ru1 C2 140.15(12) 6 .
P1 Ru1 C2 131.63(14) . .
C2 Ru1 C2 57.45(14) 6 .
C2B Ru1 C5B 19.44(18) 6 .
C2B Ru1 C5B 61.52(17) . .
C1B Ru1 C5B 36.51(12) . .
C1B Ru1 C5B 55.5(3) 6 .
C3B Ru1 C5B 24.90(13) 6 .
C3B Ru1 C5B 60.88(16) . .
S1 Ru1 C5B 150.38(14) . .
S1 Ru1 C5B 84.60(16) 6 .
P1 Ru1 C5B 121.56(15) . .
C2 Ru1 C5B 10.41(13) 6 .
C2 Ru1 C5B 65.05(16) . .
C23 Ru2 C23 38.7(2) 6 .
C23 Ru2 C21 63.5(2) 6 .
C23 Ru2 C21 63.5(2) . .
C23 Ru2 C22 63.46(17) 6 .
C23 Ru2 C22 37.53(19) . .
C21 Ru2 C22 37.88(17) . .
C23 Ru2 C22 37.52(19) 6 6
C23 Ru2 C22 63.46(17) . 6
C21 Ru2 C22 37.88(17) . 6
C22 Ru2 C22 63.1(3) . 6
C23 Ru2 S1 102.04(13) 6 6
C23 Ru2 S1 138.46(13) . 6
C21 Ru2 S1 119.08(7) . 6
C22 Ru2 S1 155.68(14) . 6
C22 Ru2 S1 93.34(13) 6 6
C23 Ru2 S1 138.46(13) 6 .
C23 Ru2 S1 102.04(13) . .
C21 Ru2 S1 119.08(7) . .
C22 Ru2 S1 93.34(13) . .
C22 Ru2 S1 155.68(14) 6 .
S1 Ru2 S1 109.25(5) 6 .
C23 Ru2 Ru1 140.17(13) 6 .
C23 Ru2 Ru1 140.17(13) . .
C21 Ru2 Ru1 153.79(18) . .
C22 Ru2 Ru1 148.23(13) . .
C22 Ru2 Ru1 148.23(13) 6 .
S1 Ru2 Ru1 54.90(3) 6 .
S1 Ru2 Ru1 54.90(3) . .
C29 Cl1 C29 63(3) 5_665 .
C4B C1 C4B 162.9 6 .
C4B C1 C3B 21.6 6 .
C4B C1 C3B 142.7 . .
C4B C1 C3B 142.70(17) 6 6
C4B C1 C3B 21.60(14) . 6
C3B C1 C3B 121.47(14) . 6
C4B C1 C5 140.7 6 .
C4B C1 C5 23.5 . .
C3B C1 C5 119.5 . .
C3B C1 C5 1.98(14) 6 .
C4B C1 C5 23.46(12) 6 6
C4B C1 C5 140.73(15) . 6
C3B C1 C5 1.98(15) . 6
C3B C1 C5 119.5(3) 6 6
C5 C1 C5 117.59(15) . 6
C4B C1 C2 33.3 6 .
C4B C1 C2 131.5 . .
C3B C1 C2 11.7 . .
C3B C1 C2 110.05(14) 6 .
C5 C1 C2 108.1 . .
C5 C1 C2 9.98(14) 6 .
C4B C1 C2 131.5(2) 6 6
C4B C1 C2 33.30(19) . 6
C3B C1 C2 110.05(19) . 6
C3B C1 C2 11.73(6) 6 6
C5 C1 C2 9.98(18) . 6
C5 C1 C2 108.1(3) 6 6
C2 C1 C2 98.52(19) . 6
C4B C1 C6 104.1(3) 6 6
C4B C1 C6 91.5(3) . 6
C3B C1 C6 125.5(3) . 6
C3B C1 C6 112.9(3) 6 6
C5 C1 C6 114.9(3) . 6
C5 C1 C6 127.5(2) 6 6
C2 C1 C6 137.0(3) . 6
C2 C1 C6 124.4(2) 6 6
C4B C1 C6 91.5 6 .
C4B C1 C6 104.1 . .
C3B C1 C6 112.9 . .
C3B C1 C6 125.55(14) 6 .
C5 C1 C6 127.5 . .
C5 C1 C6 114.86(15) 6 .
C2 C1 C6 124.4 . .
C2 C1 C6 137.01(19) 6 .
C6 C1 C6 12.6(3) 6 .
C4B C1 C9B 58.3(2) 6 6
C4B C1 C9B 137.2(2) . 6
C3B C1 C9B 79.7(2) . 6
C3B C1 C9B 158.80(11) 6 6
C5 C1 C9B 160.7(2) . 6
C5 C1 C9B 81.6(3) 6 6
C2 C1 C9B 91.1(2) . 6
C2 C1 C9B 170.18(5) 6 6
C6 C1 C9B 45.9(2) 6 6
C6 C1 C9B 33.3(2) . 6
C4B C1 C9B 137.2 6 .
C4B C1 C9B 58.3 . .
C3B C1 C9B 158.8 . .
C3B C1 C9B 79.68(14) 6 .
C5 C1 C9B 81.6 . .
C5 C1 C9B 160.70(15) 6 .
C2 C1 C9B 170.2 . .
C2 C1 C9B 91.14(19) 6 .
C6 C1 C9B 33.3(3) 6 .
C6 C1 C9B 45.9 . .
C9B C1 C9B 79.1(2) 6 .
C5 C2 C5B 108(2) 6 6
C5 C2 C3B 57.2(15) 6 .
C5B C2 C3B 155.2 6 .
C5 C2 C2B 154.0(5) 6 .
C5B C2 C2B 51.5(10) 6 .
C3B C2 C2B 133.6 . .
C5 C2 C4B 58.2(13) 6 6
C5B C2 C4B 156.48(5) 6 6
C3B C2 C4B 1.34(9) . 6
C2B C2 C4B 133.19(13) . 6
C5 C2 C4 154.6(11) 6 6
C5B C2 C4 48.8(5) 6 6
C3B C2 C4 138.4(6) . 6
C2B C2 C4 5.4(4) . 6
C4B C2 C4 137.9(6) 6 6
C5 C2 C3 162.47(8) 6 .
C5B C2 C3 62.2(10) 6 .
C3B C2 C3 125.5 . .
C2B C2 C3 10.9 . .
C4B C2 C3 124.85(14) 6 .
C4 C2 C3 13.6(6) 6 .
C5 C2 C1 75.8(15) 6 .
C5B C2 C1 156.6(8) 6 .
C3B C2 C1 18.7 . .
C2B C2 C1 116.3 . .
C4B C2 C1 17.80(14) 6 .
C4 C2 C1 120.7(6) 6 .
C3 C2 C1 107.3 . .
C5 C2 C7 53.6(15) 6 .
C5B C2 C7 67.4(11) 6 .
C3B C2 C7 108.4 . .
C2B C2 C7 116.8 . .
C4B C2 C7 109.08(14) 6 .
C4 C2 C7 112.6(6) 6 .
C3 C2 C7 126.0 . .
C1 C2 C7 126.7 . .
C5 C2 C1B 157.54(9) 6 6
C5B C2 C1B 61.6(7) 6 6
C3B C2 C1B 123.5(4) . 6
C2B C2 C1B 10.5(4) . 6
C4B C2 C1B 123.0(5) 6 6
C4 C2 C1B 14.95(18) 6 6
C3 C2 C1B 5.26(9) . 6
C1 C2 C1B 105.9(4) . 6
C7 C2 C1B 127.2(4) . 6
C5 C2 C8B 17.8(6) 6 .
C5B C2 C8B 110.4(10) 6 .
C3B C2 C8B 62.4 . .
C2B C2 C8B 161.9 . .
C4B C2 C8B 63.00(14) 6 .
C4 C2 C8B 158.5(6) 6 .
C3 C2 C8B 172.1 . .
C1 C2 C8B 80.5 . .
C7 C2 C8B 46.1 . .
C1B C2 C8B 171.5(3) 6 .
C5 C2 C10 36.7(13) 6 6
C5B C2 C10 80.5(12) 6 6
C3B C2 C10 92.0(2) . 6
C2B C2 C10 131.7(2) . 6
C4B C2 C10 92.76(8) 6 6
C4 C2 C10 128.1(7) 6 6
C3 C2 C10 141.7(2) . 6
C1 C2 C10 110.5(2) . 6
C7 C2 C10 16.9(2) . 6
C1B C2 C10 142.0(5) 6 6
C8B C2 C10 30.4(2) . 6
C1B C3 C4 119(3) 6 6
C1B C3 C2B 122.7(19) 6 .
C4 C3 C2B 29.4(6) 6 .
C1B C3 C1B 55(3) 6 .
C4 C3 C1B 159.4(6) 6 .
C2B C3 C1B 132.7 . .
C1B C3 C3 65(3) 6 6
C4 C3 C3 158.7(6) 6 6
C2B C3 C3 129.5 . 6
C1B C3 C3 9.9 . 6
C1B C3 C5B 127.0(17) 6 6
C4 C3 C5B 30.8(3) 6 6
C2B C3 C5B 4.55(8) . 6
C1B C3 C5B 132.8(3) . 6
C3 C3 C5B 128.6(3) 6 6
C1B C3 C4 67(3) 6 .
C4 C3 C4 153.0(6) 6 .
C2B C3 C4 123.8 . .
C1B C3 C4 12.8 . .
C3 C3 C4 5.7 6 .
C5B C3 C4 123.1(3) 6 .
C1B C3 C2 131.0(6) 6 .
C4 C3 C2 46.8(6) 6 .
C2B C3 C2 19.6 . .
C1B C3 C2 118.9 . .
C3 C3 C2 113.4 6 .
C5B C3 C2 16.5(3) 6 .
C4 C3 C2 108.0 . .
C1B C3 C2B 72(3) 6 6
C4 C3 C2B 142.4(6) 6 6
C2B C3 C2B 113.13(11) . 6
C1B C3 C2B 22.12(10) . 6
C3 C3 C2B 16.34(12) 6 6
C5B C3 C2B 112.3(3) 6 6
C4 C3 C2B 10.73(12) . 6
C2 C3 C2B 97.41(11) . 6
C1B C3 C8 77(2) 6 .
C4 C3 C8 79.9(6) 6 .
C2B C3 C8 109.1 . .
C1B C3 C8 114.7 . .
C3 C3 C8 120.6 6 .
C5B C3 C8 110.6(3) 6 .
C4 C3 C8 126.0 . .
C2 C3 C8 126.0 . .
C2B C3 C8 136.56(11) 6 .
C1B C3 C6B 58.5(14) 6 6
C4 C3 C6B 97.9(13) 6 6
C2B C3 C6B 125.9(7) . 6
C1B C3 C6B 94.5(7) . 6
C3 C3 C6B 101.3(7) 6 6
C5B C3 C6B 128.3(10) 6 6
C4 C3 C6B 106.4(7) . 6
C2 C3 C6B 144.6(7) . 6
C2B C3 C6B 116.6(8) 6 6
C8 C3 C6B 20.9(7) . 6
C1B C3 C7B 103(3) 6 .
C4 C3 C7B 35.2(6) 6 .
C2B C3 C7B 64.5 . .
C1B C3 C7B 156.6 . .
C3 C3 C7B 164.9 6 .
C5B C3 C7B 65.9(3) 6 .
C4 C3 C7B 169.3 . .
C2 C3 C7B 81.5 . .
C2B C3 C7B 173.3 6 .
C8 C3 C7B 44.7 . .
C6B C3 C7B 63.6(7) 6 .
C2B C4 C3 106(3) 6 6
C2B C4 C1B 110(2) 6 .
C3 C4 C1B 19.02(7) 6 .
C2B C4 C5B 32(2) 6 .
C3 C4 C5B 137.5(6) 6 .
C1B C4 C5B 141.9 . .
C2B C4 C2 19.2(15) 6 6
C3 C4 C2 119.6(9) 6 6
C1B C4 C2 127.6(3) . 6
C5B C4 C2 18.6(3) . 6
C2B C4 C7B 118(2) 6 6
C3 C4 C7B 135.3(4) 6 6
C1B C4 C7B 126.6(3) . 6
C5B C4 C7B 87.0(3) . 6
C2 C4 C7B 104.4(6) 6 6
C2B C4 C1B 94(2) 6 6
C3 C4 C1B 14.9(5) 6 6
C1B C4 C1B 19.10(10) . 6
C5B C4 C1B 126.32(8) . 6
C2 C4 C1B 109.9(4) 6 6
C7B C4 C1B 145.4(2) 6 6
C2B C4 C3 91(2) 6 .
C3 C4 C3 15.7(6) 6 .
C1B C4 C3 25.7 . .
C5B C4 C3 122.5 . .
C2 C4 C3 105.1(3) 6 .
C7B C4 C3 150.4(3) 6 .
C1B C4 C3 7.34(8) 6 .
C2B C4 C5 20(2) 6 .
C3 C4 C5 122.8(6) 6 .
C1B C4 C5 129.5 . .
C5B C4 C5 15.0 . .
C2 C4 C5 4.3(2) 6 .
C7B C4 C5 101.6(3) 6 .
C1B C4 C5 112.38(9) 6 .
C3 C4 C5 108.0 . .
C2B C4 C8 167(3) 6 6
C3 C4 C8 85.41(12) 6 6
C1B C4 C8 78.9(7) . 6
C5B C4 C8 137.0(7) . 6
C2 C4 C8 153.5(10) 6 6
C7B C4 C8 50.0(4) 6 6
C1B C4 C8 96.3(6) 6 6
C3 C4 C8 100.5(7) . 6
C5 C4 C8 151.3(7) . 6
C2B C4 C9 142(2) 6 .
C3 C4 C9 111.0(6) 6 .
C1B C4 C9 103.0 . .
C5B C4 C9 111.4 . .
C2 C4 C9 128.8(3) 6 .
C7B C4 C9 24.4(3) 6 .
C1B C4 C9 121.32(9) 6 .
C3 C4 C9 126.0 . .
C5 C4 C9 126.0 . .
C8 C4 C9 25.6(7) 6 .
C2B C4 C3B 9.9(4) 6 6
C3 C4 C3B 107.0(7) 6 6
C1B C4 C3B 114.29(15) . 6
C5B C4 C3B 30.57(15) . 6
C2 C4 C3B 13.30(19) 6 6
C7B C4 C3B 117.4(4) 6 6
C1B C4 C3B 96.7(2) 6 6
C3 C4 C3B 92.20(16) . 6
C5 C4 C3B 15.80(16) . 6
C8 C4 C3B 166.8(8) 6 6
C9 C4 C3B 141.80(16) . 6
C2 C5 C3B 97.4(18) 6 6
C2 C5 C5B 46.0(12) 6 .
C3B C5 C5B 138.6(3) 6 .
C2 C5 C4B 108.3(15) 6 .
C3B C5 C4B 10.9(3) 6 .
C5B C5 C4B 148.8 . .
C2 C5 C2B 20.6(4) 6 6
C3B C5 C2B 108.2(8) 6 6
C5B C5 C2B 30.8(5) . 6
C4B C5 C2B 118.9(5) . 6
C2 C5 C7 118.0(15) 6 6
C3B C5 C7 139.8(3) 6 6
C5B C5 C7 81.58(5) . 6
C4B C5 C7 129.54(5) . 6
C2B C5 C7 111.5(5) 6 6
C2 C5 C1 94.2(15) 6 .
C3B C5 C1 3.7(3) 6 .
C5B C5 C1 134.9 . .
C4B C5 C1 14.3 . .
C2B C5 C1 104.6(5) 6 .
C7 C5 C1 143.46(5) 6 .
C2 C5 C4 21.1(8) 6 .
C3B C5 C4 112.1(3) 6 .
C5B C5 C4 27.4 . .
C4B C5 C4 122.8 . .
C2B C5 C4 4.4(4) 6 .
C7 C5 C4 107.4 6 .
C1 C5 C4 108.5 . .
C2 C5 C8B 159.1(7) 6 6
C3B C5 C8B 87.2(3) 6 6
C5B C5 C8B 134.1(3) . 6
C4B C5 C8B 76.6(3) . 6
C2B C5 C8B 164.4(6) 6 6
C7 C5 C8B 53.0(3) 6 6
C1 C5 C8B 90.8(3) . 6
C4 C5 C8B 160.2(3) . 6
C2 C5 C10 137.6(15) 6 .
C3B C5 C10 121.9(3) 6 .
C5B C5 C10 99.2 . .
C4B C5 C10 111.2 . .
C2B C5 C10 129.8(5) 6 .
C7 C5 C10 19.6 6 .
C1 C5 C10 125.5 . .
C4 C5 C10 126.0 . .
C8B C5 C10 34.9(3) 6 .
C2 C5 C3 14.9 6 6
C3B C5 C3 100.9(6) 6 6
C5B C5 C3 38.6(4) . 6
C4B C5 C3 111.6(4) . 6
C2B C5 C3 8.02(14) 6 6
C7 C5 C3 118.3(4) 6 6
C1 C5 C3 97.3(4) . 6
C4 C5 C3 11.2(4) . 6
C8B C5 C3 170.1(4) 6 6
C10 C5 C3 137.2(4) . 6
C2 C5 C10B 96.8(15) 6 .
C3B C5 C10B 165.5(3) 6 .
C5B C5 C10B 55.7 . .
C4B C5 C10B 154.6 . .
C2B C5 C10B 86.3(5) 6 .
C7 C5 C10B 26.35(6) 6 .
C1 C5 C10B 168.9 . .
C4 C5 C10B 82.5 . .
C8B C5 C10B 78.4(3) 6 .
C10 C5 C10B 43.6 . .
C3 C5 C10B 93.7(4) 6 .
C6 C6 C9B 168.58(11) 6 6
C6 C6 C9B 8.4 6 .
C9B C6 C9B 160.13(10) 6 .
C6 C6 C1 83.7 6 .
C9B C6 C1 84.89(10) 6 .
C9B C6 C1 75.2 . .
C6 C6 C4B 103.96(10) 6 6
C9B C6 C4B 64.63(10) 6 6
C9B C6 C4B 95.52(10) . 6
C1 C6 C4B 20.31(10) . 6
C6 C6 C4B 65.4 6 .
C9B C6 C4B 103.24(10) 6 .
C9B C6 C4B 56.9 . .
C1 C6 C4B 18.4 . .
C4B C6 C4B 38.61(10) 6 .
C10 C7 C10B 139.4(13) 6 6
C10 C7 C8B 35.0(13) 6 .
C10B C7 C8B 160.1(6) 6 .
C10 C7 C5 95.1(15) 6 6
C10B C7 C5 102.7(11) 6 6
C8B C7 C5 65.8 . 6
C10 C7 C5B 115.1(15) 6 6
C10B C7 C5B 80.5(9) 6 6
C8B C7 C5B 88.21(18) . 6
C5 C7 C5B 22.54(15) 6 6
C10 C7 C2 103.5(15) 6 .
C10B C7 C2 96.1(11) 6 .
C8B C7 C2 73.6 . .
C5 C7 C2 8.4 6 .
C5B C7 C2 15.71(18) 6 .
C10 C7 C3B 86.1(15) 6 .
C10B C7 C3B 112.8(11) 6 .
C8B C7 C3B 55.7 . .
C5 C7 C3B 10.2 6 .
C5B C7 C3B 32.78(18) 6 .
C2 C7 C3B 18.0 . .
C6B C8 C9 147.3(6) 6 6
C6B C8 C7B 144.58(5) 6 .
C9 C8 C7B 20.3(7) 6 .
C6B C8 C1B 80.2(12) 6 6
C9 C8 C1B 97.2(4) 6 6
C7B C8 C1B 77.5(4) . 6
C6B C8 C4 99.2(12) 6 6
C9 C8 C4 78.8(3) 6 6
C7B C8 C4 58.7(4) . 6
C1B C8 C4 19.56(10) 6 6
C6B C8 C3 86.6(9) 6 .
C9 C8 C3 93.5(8) 6 .
C7B C8 C3 73.4 . .
C1B C8 C3 7.1(2) 6 .
C4 C8 C3 14.7(4) 6 .
C6B C8 C2B 100.3(8) 6 .
C9 C8 C2B 77.0(8) 6 .
C7B C8 C2B 56.9 . .
C1B C8 C2B 21.0(4) 6 .
C4 C8 C2B 2.0(4) 6 .
C3 C8 C2B 16.5 . .
C7B C9 C8 138(2) 6 6
C7B C9 C6B 137.8(14) 6 .
C8 C9 C6B 15.0(2) 6 .
C7B C9 C4 62.7(15) 6 .
C8 C9 C4 75.6(8) 6 .
C6B C9 C4 76.0 . .
C7B C9 C3 75.0(13) 6 6
C8 C9 C3 63.3(10) 6 6
C6B C9 C3 64.1(2) . 6
C4 C9 C3 12.3(2) . 6
C7B C9 C1B 79.1(15) 6 .
C8 C9 C1B 59.9(8) 6 .
C6B C9 C1B 59.2 . .
C4 C9 C1B 16.8 . .
C3 C9 C1B 6.38(17) 6 .
C7B C9 C2B 57.4(12) 6 6
C8 C9 C2B 81.0(10) 6 6
C6B C9 C2B 81.0(3) . 6
C4 C9 C2B 5.5(3) . 6
C3 C9 C2B 17.71(7) 6 6
C1B C9 C2B 21.8(3) . 6
C7 C10 C8B 125.7(17) 6 6
C7 C10 C10B 24.8(8) 6 .
C8B C10 C10B 145.1(4) 6 .
C7 C10 C5 65.2(15) 6 .
C8B C10 C5 67.8(5) 6 .
C10B C10 C5 77.8 . .
C7 C10 C5B 49.0(14) 6 .
C8B C10 C5B 86.3(5) 6 .
C10B C10 C5B 59.2 . .
C5 C10 C5B 18.6 . .
C7 C10 C2 59.5(14) 6 6
C8B C10 C2 72.6(5) 6 6
C10B C10 C2 72.69(12) . 6
C5 C10 C2 5.68(11) . 6
C5B C10 C2 13.95(11) . 6
C7 C10 C3B 77.6(15) 6 6
C8B C10 C3B 54.6(5) 6 6
C10B C10 C3B 91.0 . 6
C5 C10 C3B 13.2 . 6
C5B C10 C3B 31.8 . 6
C2 C10 C3B 18.54(9) 6 6
C3 C1B C4 42(3) 6 .
C3 C1B C2B 43.2(17) 6 6
C4 C1B C2B 22.9(7) . 6
C3 C1B C1B 115(3) 6 6
C4 C1B C1B 150.3 . 6
C2B C1B C1B 129.7(7) 6 6
C3 C1B C3 105(3) 6 .
C4 C1B C3 141.5 . .
C2B C1B C3 122.8(7) 6 .
C1B C1B C3 9.9 6 .
C3 C1B C4 106(3) 6 6
C4 C1B C4 139.64(9) . 6
C2B C1B C4 119.5(6) 6 6
C1B C1B C4 10.63(9) 6 6
C3 C1B C4 5.7 . 6
C3 C1B C5B 46.8(17) 6 .
C4 C1B C5B 25.3 . .
C2B C1B C5B 3.80(17) 6 .
C1B C1B C5B 128.8 6 .
C3 C1B C5B 122.5 . .
C4 C1B C5B 118.80(9) 6 .
C3 C1B C2B 101(3) 6 .
C4 C1B C2B 130.0 . .
C2B C1B C2B 108.9(7) 6 .
C1B C1B C2B 20.9 6 .
C3 C1B C2B 16.1 . .
C4 C1B C2B 11.06(8) 6 .
C5B C1B C2B 108.0 . .
C3 C1B C8 96(3) 6 6
C4 C1B C8 81.5(6) . 6
C2B C1B C8 104.2(13) 6 6
C1B C1B C8 125.0(6) 6 6
C3 C1B C8 129.1(6) . 6
C4 C1B C8 134.0(7) 6 6
C5B C1B C8 105.7(6) . 6
C2B C1B C8 145.0(6) . 6
C3 C1B C6B 115.3(18) 6 .
C4 C1B C6B 102.9 . .
C2B C1B C6B 125.0(7) 6 .
C1B C1B C6B 105.2 6 .
C3 C1B C6B 111.1 . .
C4 C1B C6B 115.15(9) 6 .
C5B C1B C6B 126.0 . .
C2B C1B C6B 126.0 . .
C8 C1B C6B 21.9(5) 6 .
C3 C1B C2 43.7(6) 6 6
C4 C1B C2 37.5(2) . 6
C2B C1B C2 15.3(5) 6 6
C1B C1B C2 114.5(2) 6 6
C3 C1B C2 107.7(2) . 6
C4 C1B C2 104.2(2) 6 6
C5B C1B C2 15.0(2) . 6
C2B C1B C2 93.6(2) . 6
C8 C1B C2 119.0(8) 6 6
C6B C1B C2 140.2(2) . 6
C3 C1B C7B 70(3) 6 6
C4 C1B C7B 39.55(10) . 6
C2B C1B C7B 61.0(8) 6 6
C1B C1B C7B 168.98(11) 6 6
C3 C1B C7B 168.98(7) . 6
C4 C1B C7B 174.2 6 6
C5B C1B C7B 62.09(11) . 6
C2B C1B C7B 169.45(10) . 6
C8 C1B C7B 44.0(5) 6 6
C6B C1B C7B 64.02(11) . 6
C2 C1B C7B 76.2(4) 6 6
C4 C2B C3 44(3) 6 .
C4 C2B C1B 46.8(17) 6 6
C3 C2B C1B 14.15(7) . 6
C4 C2B C5B 137(3) 6 6
C3 C2B C5B 172.28(16) . 6
C1B C2B C5B 172.9(4) 6 6
C4 C2B C2 155.3(19) 6 .
C3 C2B C2 149.5 . .
C1B C2B C2 154.2(8) 6 .
C5B C2B C2 25.2(5) 6 .
C4 C2B C5 156(2) 6 6
C3 C2B C5 154.0(3) . 6
C1B C2B C5 156.5(11) 6 6
C5B C2B C5 21.6(2) 6 6
C2 C2B C5 5.37(16) . 6
C4 C2B C3B 168.2(5) 6 .
C3 C2B C3B 135.6 . .
C1B C2B C3B 137.3(8) 6 .
C5B C2B C3B 40.9(6) 6 .
C2 C2B C3B 17.4 . .
C5 C2B C3B 19.4(3) 6 .
C4 C2B C1B 75(2) 6 .
C3 C2B C1B 31.3 . .
C1B C2B C1B 29.4(8) 6 .
C5B C2B C1B 148.3(6) 6 .
C2 C2B C1B 124.9 . .
C5 C2B C1B 127.4(3) 6 .
C3B C2B C1B 108.0 . .
C4 C2B C3 79(2) 6 6
C3 C2B C3 34.19(13) . 6
C1B C2B C3 35.0(7) 6 6
C5B C2B C3 143.9(6) 6 6
C2 C2B C3 119.35(12) . 6
C5 C2B C3 122.3(4) 6 6
C3B C2B C3 102.99(13) . 6
C1B C2B C3 7.35(6) . 6
C4 C2B C7B 52(2) 6 .
C3 C2B C7B 96.8 . .
C1B C2B C7B 96.7(8) 6 .
C5B C2B C7B 85.4(6) 6 .
C2 C2B C7B 109.0 . .
C5 C2B C7B 106.6(3) 6 .
C3B C2B C7B 126.0 . .
C1B C2B C7B 126.0 . .
C3 C2B C7B 130.73(13) 6 .
C4 C2B C2B 95(3) 6 6
C3 C2B C2B 50.5 . 6
C1B C2B C2B 50.3(8) 6 6
C5B C2B C2B 127.8(6) 6 6
C2 C2B C2B 104.0 . 6
C5 C2B C2B 106.6(3) 6 6
C3B C2B C2B 87.2 . 6
C1B C2B C2B 20.9 . 6
C3 C2B C2B 16.34(13) 6 6
C7B C2B C2B 146.8 . 6
C4 C2B C9 32.3(19) 6 6
C3 C2B C9 76.4(5) . 6
C1B C2B C9 76.1(4) 6 6
C5B C2B C9 106.0(11) 6 6
C2 C2B C9 129.4(5) . 6
C5 C2B C9 127.3(8) 6 6
C3B C2B C9 146.6(5) . 6
C1B C2B C9 105.4(5) . 6
C3 C2B C9 110.1(4) 6 6
C7B C2B C9 20.7(5) . 6
C2B C2B C9 126.1(5) 6 6
C4B C3B C5 156.8(8) 6 6
C4B C3B C2 176.9(2) 6 .
C5 C3B C2 25.4(4) 6 .
C4B C3B C1 28.4(3) 6 .
C5 C3B C1 174.3(5) 6 .
C2 C3B C1 149.6 . .
C4B C3B C5B 172.63(10) 6 6
C5 C3B C5B 21.83(10) 6 6
C2 C3B C5B 10.28(10) . 6
C1 C3B C5B 152.5(5) . 6
C4B C3B C2B 149.9(3) 6 .
C5 C3B C2B 52.4(5) 6 .
C2 C3B C2B 29.0 . .
C1 C3B C2B 122.1 . .
C5B C3B C2B 30.8(5) 6 .
C4B C3B C4B 42.2(3) 6 .
C5 C3B C4B 160.2(5) 6 .
C2 C3B C4B 136.0 . .
C1 C3B C4B 14.1 . .
C5B C3B C4B 138.4(5) 6 .
C2B C3B C4B 108.0 . .
C4B C3B C8B 83.9(3) 6 .
C5 C3B C8B 73.7(5) 6 .
C2 C3B C8B 97.6 . .
C1 C3B C8B 111.9 . .
C5B C3B C8B 95.4(5) 6 .
C2B C3B C8B 126.0 . .
C4B C3B C8B 126.0 . .
C4B C3B C3B 57.5(3) 6 6
C5 C3B C3B 145.2(5) 6 6
C2 C3B C3B 120.8 . 6
C1 C3B C3B 29.3 . 6
C5B C3B C3B 123.4(5) 6 6
C2B C3B C3B 92.8 . 6
C4B C3B C3B 15.3 . 6
C8B C3B C3B 141.2 . 6
C4B C3B C4 150.5(6) 6 6
C5 C3B C4 52.1(3) 6 6
C2 C3B C4 28.3(4) . 6
C1 C3B C4 122.4(4) . 6
C5B C3B C4 30.67(19) 6 6
C2B C3B C4 1.89(9) . 6
C4B C3B C4 108.4(4) . 6
C8B C3B C4 125.6(4) . 6
C3B C3B C4 93.2(4) 6 6
C4B C3B C7 127.9(3) 6 .
C5 C3B C7 30.0(5) 6 .
C2 C3B C7 53.7 . .
C1 C3B C7 155.7 . .
C5B C3B C7 51.8(5) 6 .
C2B C3B C7 82.0 . .
C4B C3B C7 169.8 . .
C8B C3B C7 44.0 . .
C3B C3B C7 173.9 6 .
C4 C3B C7 81.6(4) 6 .
C4B C3B C9B 42.2(3) 6 6
C5 C3B C9B 115.3(6) 6 6
C2 C3B C9B 139.2(3) . 6
C1 C3B C9B 70.2(3) . 6
C5B C3B C9B 136.9(5) 6 6
C2B C3B C9B 167.6(3) . 6
C4B C3B C9B 84.3(3) . 6
C8B C3B C9B 41.8(3) . 6
C3B C3B C9B 99.5(3) 6 6
C4 C3B C9B 167.4(4) 6 6
C7 C3B C9B 85.8(3) . 6
C3B C4B C1 130.0(5) 6 .
C3B C4B C5 12.3(5) 6 .
C1 C4B C5 142.2 . .
C3B C4B C2 1.77(11) 6 6
C1 C4B C2 128.9(3) . 6
C5 C4B C2 13.5(3) . 6
C3B C4B C4B 122.5(5) 6 6
C1 C4B C4B 8.6 . 6
C5 C4B C4B 134.6 . 6
C2 C4B C4B 121.6(3) 6 6
C3B C4B C5B 5.08(8) 6 .
C1 C4B C5B 131.1 . .
C5 C4B C5B 11.6 . .
C2 C4B C5B 6.73(10) 6 .
C4B C4B C5B 123.2 6 .
C3B C4B C3B 107.3(5) 6 .
C1 C4B C3B 23.2 . .
C5 C4B C3B 119.3 . .
C2 C4B C3B 106.3(4) 6 .
C4B C4B C3B 15.3 6 .
C5B C4B C3B 108.0 . .
C3B C4B C9B 126.5(5) 6 .
C1 C4B C9B 102.9 . .
C5 C4B C9B 114.6 . .
C2 C4B C9B 127.3(3) 6 .
C4B C4B C9B 110.8 6 .
C5B C4B C9B 126.0 . .
C3B C4B C9B 126.0 . .
C3B C4B C8B 79.3(6) 6 6
C1 C4B C8B 149.49(15) . 6
C5 C4B C8B 67.47(15) . 6
C2 C4B C8B 80.2(4) 6 6
C4B C4B C8B 157.80(15) 6 6
C5B C4B C8B 78.94(15) . 6
C3B C4B C8B 172.20(14) . 6
C9B C4B C8B 47.18(15) . 6
C3B C4B C6 161.0(5) 6 6
C1 C4B C6 68.2(3) . 6
C5 C4B C6 149.4(3) . 6
C2 C4B C6 161.6(3) 6 6
C4B C4B C6 76.0(3) 6 6
C5B C4B C6 160.7(3) . 6
C3B C4B C6 91.2(3) . 6
C9B C4B C6 34.8(3) . 6
C8B C4B C6 81.9(3) 6 6
C3B C4B C6 171.3(5) 6 .
C1 C4B C6 57.6 . .
C5 C4B C6 160.1 . .
C2 C4B C6 171.3(3) 6 .
C4B C4B C6 65.4 6 .
C5B C4B C6 171.3 . .
C3B C4B C6 80.6 . .
C9B C4B C6 45.5 . .
C8B C4B C6 92.59(15) 6 .
C6 C4B C6 10.7(3) 6 .
C3B C4B C2B 23.1(3) 6 6
C1 C4B C2B 107.6(3) . 6
C5 C4B C2B 34.8(3) . 6
C2 C4B C2B 22.45(15) 6 6
C4B C4B C2B 99.8(3) 6 6
C5B C4B C2B 23.5(3) . 6
C3B C4B C2B 84.5(3) . 6
C9B C4B C2B 149.4(3) . 6
C8B C4B C2B 102.3(4) 6 6
C6 C4B C2B 175.79(17) 6 6
C6 C4B C2B 165.1(3) . 6
C2 C5B C5 25.9(6) 6 .
C2 C5B C2B 103.2(13) 6 6
C5 C5B C2B 127.6(6) . 6
C2 C5B C3B 14.5 6 6
C5 C5B C3B 19.6(2) . 6
C2B C5B C3B 108.3(8) 6 6
C2 C5B C4 112.5(7) 6 .
C5 C5B C4 137.6 . .
C2B C5B C4 11.0(6) 6 .
C3B C5B C4 118.8(2) 6 .
C2 C5B C3 101.3(11) 6 6
C5 C5B C3 126.1(4) . 6
C2B C5B C3 3.17(8) 6 6
C3B C5B C3 107.1(6) 6 6
C4 C5B C3 11.7(4) . 6
C2 C5B C4B 16.8 6 .
C5 C5B C4B 19.6 . .
C2B C5B C4B 108.8(6) 6 .
C3B C5B C4B 2.3 6 .
C4 C5B C4B 119.3 . .
C3 C5B C4B 107.6(4) 6 .
C2 C5B C1B 103.4(8) 6 .
C5 C5B C1B 127.1 . .
C2B C5B C1B 3.3(2) 6 .
C3B C5B C1B 107.7(2) 6 .
C4 C5B C1B 12.8 . .
C3 C5B C1B 6.2 6 .
C4B C5B C1B 108.0 . .
C2 C5B C7 96.9(6) 6 6
C5 C5B C7 75.9(3) . 6
C2B C5B C7 153.5(7) 6 6
C3B C5B C7 95.44(8) 6 6
C4 C5B C7 142.7(2) . 6
C3 C5B C7 153.1(5) 6 6
C4B C5B C7 95.5(3) . 6
C1B C5B C7 155.4(2) . 6
C2 C5B C10B 128.1(8) 6 .
C5 C5B C10B 106.7 . .
C2B C5B C10B 125.1(6) 6 .
C3B C5B C10B 126.3(2) 6 .
C4 C5B C10B 114.4 . .
C3 C5B C10B 126.0(4) 6 .
C4B C5B C10B 126.0 . .
C1B C5B C10B 126.0 . .
C7 C5B C10B 31.3(3) 6 .
C2 C5B C7B 158.5(3) 6 6
C5 C5B C7B 163.1(5) . 6
C2B C5B C7B 66.86(16) 6 6
C3B C5B C7B 172.6(5) 6 6
C4 C5B C7B 56.1(5) . 6
C3 C5B C7B 67.8(2) 6 6
C4B C5B C7B 174.5(4) . 6
C1B C5B C7B 67.8(5) . 6
C7 C5B C7B 88.2(7) 6 6
C10B C5B C7B 58.3(5) . 6
C2 C5B C10 85.5(8) 6 .
C5 C5B C10 62.2 . .
C2B C5B C10 169.3(6) 6 .
C3B C5B C10 81.7(2) 6 .
C4 C5B C10 158.3 . .
C3 C5B C10 168.9(4) 6 .
C4B C5B C10 81.4 . .
C1B C5B C10 170.6 . .
C7 C5B C10 15.9(2) 6 .
C10B C5B C10 44.6 . .
C7B C5B C10 102.8(5) 6 .
C8 C6B C9 17.7(7) 6 .
C8 C6B C1B 77.9(9) 6 .
C9 C6B C1B 77.9 . .
C8 C6B C3 72.5(5) 6 6
C9 C6B C3 73.7(4) . 6
C1B C6B C3 6.2(3) . 6
C8 C6B C6B 144.1(12) 6 6
C9 C6B C6B 152.2 . 6
C1B C6B C6B 74.8 . 6
C3 C6B C6B 78.7(4) 6 6
C8 C6B C4 61.3(8) 6 .
C9 C6B C4 60.9 . .
C1B C6B C4 17.1 . .
C3 C6B C4 13.1(4) 6 .
C6B C6B C4 91.6 6 .
C8 C6B C7B 24.3(2) 6 6
C9 C6B C7B 14.3(4) . 6
C1B C6B C7B 63.8(4) . 6
C3 C6B C7B 59.92(18) 6 6
C6B C6B C7B 138.6(4) 6 6
C4 C6B C7B 46.9(4) . 6
C8 C6B C1B 102.3(8) 6 6
C9 C6B C1B 104.4(3) . 6
C1B C6B C1B 26.6(3) . 6
C3 C6B C1B 30.8(2) 6 6
C6B C6B C1B 48.2(3) 6 6
C4 C6B C1B 43.5(3) . 6
C7B C6B C1B 90.4(3) 6 6
C8 C6B C2B 63.0(5) 6 6
C9 C6B C2B 61.9(3) . 6
C1B C6B C2B 15.9(3) . 6
C3 C6B C2B 12.76(13) 6 6
C6B C6B C2B 90.7(3) 6 6
C4 C6B C2B 2.24(13) . 6
C7B C6B C2B 47.87(11) 6 6
C1B C6B C2B 42.53(18) 6 6
C9 C7B C8 21.8(16) 6 .
C9 C7B C4 92.9(19) 6 6
C8 C7B C4 71.4(2) . 6
C9 C7B C2B 101.9(17) 6 .
C8 C7B C2B 80.5 . .
C4 C7B C2B 9.2(2) 6 .
C9 C7B C10B 174(2) 6 6
C8 C7B C10B 164.7(5) . 6
C4 C7B C10B 93.5(4) 6 6
C2B C7B C10B 84.5(5) . 6
C9 C7B C5B 129.7(19) 6 6
C8 C7B C5B 108.2(3) . 6
C4 C7B C5B 36.84(13) 6 6
C2B C7B C5B 27.8(3) . 6
C10B C7B C5B 56.7(3) 6 6
C9 C7B C3 83.4(17) 6 .
C8 C7B C3 61.9 . .
C4 C7B C3 9.5(2) 6 .
C2B C7B C3 18.6 . .
C10B C7B C3 103.0(5) 6 .
C5B C7B C3 46.3(3) 6 .
C9 C7B C1B 79.6(17) 6 6
C8 C7B C1B 58.51(8) . 6
C4 C7B C1B 13.84(13) 6 6
C2B C7B C1B 22.38(8) . 6
C10B C7B C1B 106.7(5) 6 6
C5B C7B C1B 50.1(2) 6 6
C3 C7B C1B 6.2 . 6
C9 C7B C6B 27.9(12) 6 6
C8 C7B C6B 11.1(2) . 6
C4 C7B C6B 65.8(7) 6 6
C2B C7B C6B 74.6(4) . 6
C10B C7B C6B 158.1(8) 6 6
C5B C7B C6B 102.2(7) 6 6
C3 C7B C6B 56.5(4) . 6
C1B C7B C6B 52.2(5) 6 6
C9 C7B C2 127.9(17) 6 .
C8 C7B C2 106.2 . .
C4 C7B C2 35.1(2) 6 .
C2B C7B C2 26.3 . .
C10B C7B C2 58.6(5) 6 .
C5B C7B C2 4.32(11) 6 .
C3 C7B C2 44.5 . .
C1B C7B C2 48.69(8) 6 .
C6B C7B C2 100.8(4) 6 .
C10 C8B C9B 169.61(15) 6 6
C10 C8B C7 19.3(5) 6 .
C9B C8B C7 162.7(3) 6 .
C10 C8B C5 77.3(4) 6 6
C9B C8B C5 101.5(4) 6 6
C7 C8B C5 61.2(2) . 6
C10 C8B C3B 96.4(6) 6 .
C9B C8B C3B 82.4(3) 6 .
C7 C8B C3B 80.3 . .
C5 C8B C3B 19.2(2) 6 .
C10 C8B C4B 112.8(6) 6 6
C9B C8B C4B 65.6(3) 6 6
C7 C8B C4B 97.1 . 6
C5 C8B C4B 35.9(2) 6 6
C3B C8B C4B 16.8 . 6
C10 C8B C2 76.9(6) 6 .
C9B C8B C2 102.4(3) 6 .
C7 C8B C2 60.3 . .
C5 C8B C2 3.06(6) 6 .
C3B C8B C2 20.1 . .
C4B C8B C2 36.8 6 .
C10 C8B C5B 65.2(4) 6 6
C9B C8B C5B 113.5(4) 6 6
C7 C8B C5B 49.2(3) . 6
C5 C8B C5B 12.17(6) 6 6
C3B C8B C5B 31.3(3) . 6
C4B C8B C5B 48.0(2) 6 6
C2 C8B C5B 12.0(3) . 6
C10 C8B C10B 20.3(3) 6 6
C9B C8B C10B 157.9(5) 6 6
C7 C8B C10B 7.6(2) . 6
C5 C8B C10B 57.35(17) 6 6
C3B C8B C10B 76.5(4) . 6
C4B C8B C10B 93.1(4) 6 6
C2 C8B C10B 56.8(4) . 6
C5B C8B C10B 45.18(17) 6 6
C6 C9B C8B 147.7(4) 6 6
C6 C9B C6 2.97(9) 6 .
C8B C9B C6 144.7(3) 6 .
C6 C9B C4B 80.60(9) 6 .
C8B C9B C4B 67.2(3) 6 .
C6 C9B C4B 77.6 . .
C6 C9B C1 61.84(9) 6 .
C8B C9B C1 85.9(3) 6 .
C6 C9B C1 58.9 . .
C4B C9B C1 18.8 . .
C6 C9B C3B 91.94(14) 6 6
C8B C9B C3B 55.8(3) 6 6
C6 C9B C3B 88.97(14) . 6
C4B C9B C3B 11.36(14) . 6
C1 C9B C3B 30.10(14) . 6
C7 C10B C10 15.8(4) 6 .
C7 C10B C5B 68.2(9) 6 .
C10 C10B C5B 76.1 . .
C7 C10B C7B 129.8(13) 6 6
C10 C10B C7B 140.9(6) . 6
C5B C10B C7B 65.0(6) . 6
C7 C10B C5 51.0(9) 6 .
C10 C10B C5 58.6 . .
C5B C10B C5 17.5 . .
C7B C10B C5 82.4(6) 6 .
C7 C10B C2 57.8(9) 6 6
C10 C10B C2 66.35(5) . 6
C5B C10B C2 10.52(6) . 6
C7B C10B C2 74.6(6) 6 6
C5 C10B C2 8.0 . 6
C7 C10B C8B 12.2(4) 6 6
C10 C10B C8B 14.6(3) . 6
C5B C10B C8B 61.8(3) . 6
C7B C10B C8B 126.3(7) 6 6
C5 C10B C8B 44.3(3) . 6
C2 C10B C8B 51.9(2) 6 6
C12 C11 C16 119.4(4) . .
C12 C11 P1 116.5(3) . .
C16 C11 P1 123.9(4) . .
C11 C12 C13 120.5(4) . .
C11 C12 S1 120.2(3) . .
C13 C12 S1 119.3(4) . .
C14 C13 C12 119.1(5) . .
C14 C13 H13 120.5 . .
C12 C13 H13 120.5 . .
C13 C14 C15 121.1(5) . .
C13 C14 H14 119.5 . .
C15 C14 H14 119.5 . .
C14 C15 C16 120.2(5) . .
C14 C15 H15 119.9 . .
C16 C15 H15 119.9 . .
C15 C16 C11 119.6(5) . .
C15 C16 H16 120.2 . .
C11 C16 H16 120.2 . .
C18 C17 C18 119.5(7) . 6
C18 C17 P1 120.2(4) . .
C18 C17 P1 120.2(4) 6 .
C17 C18 C19 119.5(7) . .
C17 C18 H18 120.3 . .
C19 C18 H18 120.3 . .
C20 C19 C18 120.3(8) . .
C20 C19 H19 119.8 . .
C18 C19 H19 119.8 . .
C19 C20 C19 120.8(10) 6 .
C19 C20 H20 119.6 6 .
C19 C20 H20 119.6 . .
C22 C21 C22 107.8(6) . 6
C22 C21 C24 126.1(3) . .
C22 C21 C24 126.1(3) 6 .
C22 C21 Ru2 71.6(3) . .
C22 C21 Ru2 71.6(3) 6 .
C24 C21 Ru2 124.1(5) . .
C23 C22 C21 107.6(4) . .
C23 C22 C25 127.2(5) . .
C21 C22 C25 125.0(5) . .
C23 C22 Ru2 68.9(3) . .
C21 C22 Ru2 70.6(3) . .
C25 C22 Ru2 130.2(4) . .
C22 C23 C23 108.4(3) . 6
C22 C23 C26 126.3(5) . .
C23 C23 C26 125.2(4) 6 .
C22 C23 Ru2 73.5(3) . .
C23 C23 Ru2 70.67(12) 6 .
C26 C23 Ru2 124.8(4) . .
C21 C24 H24A 109.5 . .
C21 C24 H24B 109.5 . .
H24A C24 H24B 109.5 . .
C21 C24 H24C 109.5 . .
H24A C24 H24C 109.5 . .
H24B C24 H24C 109.5 . .
C22 C25 H25A 109.5 . .
C22 C25 H25B 109.5 . .
H25A C25 H25B 109.5 . .
C22 C25 H25C 109.5 . .
H25A C25 H25C 109.5 . .
H25B C25 H25C 109.5 . .
C23 C26 H26A 109.5 . .
C23 C26 H26B 109.5 . .
H26A C26 H26B 109.5 . .
C23 C26 H26C 109.5 . .
H26A C26 H26C 109.5 . .
H26B C26 H26C 109.5 . .
F1 C27 F2 107.1(4) . 6_565
F1 C27 F2 107.1(4) . .
F2 C27 F2 107.2(6) 6_565 .
F1 C27 S2 112.2(6) . .
F2 C27 S2 111.5(4) 6_565 .
F2 C27 S2 111.5(4) . .
Cl1 C29 Cl1 117(3) 5_665 .
Cl1 C29 C29 58.6(13) 5_665 5_665
Cl1 C29 C29 58.6(13) . 5_665
F4 C28 F4 97.923(4) 6 .
F4 C28 F3 87.385(2) 6 .
F4 C28 F3 87.385(2) . .
F4 C28 S3 127.112(2) 6 .
F4 C28 S3 127.112(2) . .
F3 C28 S3 117.207(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
P1 C17 1.816(7) .
P1 C11 1.821(4) .
P1 C11 1.821(4) 6
P1 Ru1 2.3005(16) .
S1 C12 1.801(4) .
S1 Ru1 2.2890(11) .
S1 Ru2 2.3140(11) .
S2 O1 1.435(4) 6_565
S2 O1 1.435(4) .
S2 O2 1.437(5) .
S2 C27 1.820(7) .
S3 O3 1.4109 .
S3 O4 1.4854 .
S3 O4 1.4854 6
S3 C28 1.7269 .
Ru1 C2B 2.195(6) 6
Ru1 C2B 2.195(6) .
Ru1 C1B 2.235(6) .
Ru1 C1B 2.235(6) 6
Ru1 C3B 2.240(5) 6
Ru1 C3B 2.240(6) .
Ru1 S1 2.2890(11) 6
Ru1 P1 2.3005(16) .
Ru1 Ru2 2.6170(6) .
Ru1 C2 2.302(6) 6
Ru1 C2 2.302(6) .
Ru1 C5B 2.303(7) .
Ru2 C23 2.163(4) 6
Ru2 C23 2.163(4) .
Ru2 C21 2.209(6) .
Ru2 C22 2.222(5) .
Ru2 C22 2.222(5) 6
Ru2 S1 2.3140(11) 6
Cl1 C29 1.66(2) 5_665
Cl1 C29 1.66(2) .
C1 C4B 0.5734(15) 6
C1 C4B 0.5734(14) .
C1 C3B 0.924(2) .
C1 C3B 0.924(2) 6
C1 C5 1.419(4) .
C1 C5 1.419(4) 6
C1 C2 1.460(4) .
C1 C2 1.460(4) 6
C1 C6 1.534(4) 6
C1 C6 1.534(4) .
C1 C9B 1.733(4) 6
C1 C9B 1.733(4) .
C2 C5 0.254(3) 6
C2 C5B 0.418(5) 6
C2 C3B 0.5865(15) .
C2 C2B 0.954(2) .
C2 C4B 1.030(4) 6
C2 C4 1.208(4) 6
C2 C3 1.441(4) .
C2 C7 1.532(4) .
C2 C1B 1.573(7) 6
C2 C8B 1.693(4) .
C2 C10 1.727(7) 6
C3 C1B 0.191(5) 6
C3 C4 0.391(11) 6
C3 C2B 0.5356(14) .
C3 C1B 1.004(3) .
C3 C3 1.070(12) 6
C3 C5B 1.299(4) 6
C3 C4 1.441(4) .
C3 C2B 1.470(9) 6
C3 C8 1.532(4) .
C3 C6B 1.604(5) 6
C3 C7B 1.664(4) .
C4 C2B 0.2736(14) 6
C4 C3 0.391(11) 6
C4 C1B 0.5120(13) .
C4 C5B 0.984(2) .
C4 C2 1.208(2) 6
C4 C7B 1.363(14) 6
C4 C1B 1.377(12) 6
C4 C5 1.441(4) .
C4 C8 1.513(6) 6
C4 C9 1.532(4) .
C4 C3B 1.692(4) 6
C5 C2 0.254(4) 6
C5 C3B 0.497(5) 6
C5 C5B 0.5518(14) .
C5 C4B 0.922(2) .
C5 C2B 1.187(5) 6
C5 C7 1.396(10) 6
C5 C8B 1.453(2) 6
C5 C10 1.532(4) .
C5 C3 1.685(7) 6
C5 C10B 1.753(4) .
C6 C6 0.337(8) 6
C6 C9B 0.955(7) 6
C6 C9B 1.287(3) .
C6 C4B 1.652(3) 6
C6 C4B 1.763(4) .
C7 C10 0.5171 6
C7 C10B 0.797(4) 6
C7 C8B 1.272(3) .
C7 C5 1.396(10) 6
C7 C5B 1.424(11) 6
C7 C3B 1.805(5) .
C8 C6B 0.573(17) 6
C8 C9 0.676(17) 6
C8 C7B 1.222(3) .
C8 C1B 1.501(9) 6
C8 C4 1.513(6) 6
C8 C2B 1.781(4) .
C9 C7B 0.634(6) 6
C9 C8 0.676(18) 6
C9 C6B 1.199(3) .
C9 C3 1.711(11) 6
C9 C1B 1.721(4) .
C9 C2B 1.756(9) 6
C10 C7 0.5171(18) 6
C10 C8B 0.899(10) 6
C10 C10B 1.236(3) .
C10 C5B 1.709(4) .
C10 C2 1.727(10) 6
C10 C3B 1.843(9) 6
C1B C3 0.191(5) 6
C1B C2B 0.659(6) 6
C1B C1B 0.908(12) 6
C1B C4 1.377(11) 6
C1B C5B 1.423(4) .
C1B C2B 1.423(4) .
C1B C8 1.501(11) 6
C1B C6B 1.513(4) .
C1B C2 1.573(3) 6
C1B C7B 1.718(15) 6
C2B C4 0.2736(10) 6
C2B C1B 0.659(9) 6
C2B C5B 0.767(5) 6
C2B C5 1.1868(16) 6
C2B C3B 1.423(4) .
C2B C3 1.470(11) 6
C2B C7B 1.513(4) .
C2B C2B 1.751(10) 6
C2B C9 1.756(10) 6
C3B C4B 0.444(3) 6
C3B C5 0.497(5) 6
C3B C5B 0.981(4) 6
C3B C4B 1.423(4) .
C3B C8B 1.512(4) .
C3B C3B 1.612(2) 6
C3B C4 1.692(4) 6
C3B C9B 1.812(4) 6
C4B C3B 0.4440(16) 6
C4B C2 1.030(3) 6
C4B C4B 1.1340 6
C4B C5B 1.423(4) .
C4B C9B 1.513(4) .
C4B C8B 1.531(6) 6
C4B C6 1.652(5) 6
C4B C2B 1.821(4) 6
C5B C2 0.418(5) 6
C5B C2B 0.767(7) 6
C5B C3B 0.981(5) 6
C5B C3 1.299(9) 6
C5B C7 1.424(8) 6
C5B C10B 1.513(4) .
C5B C7B 1.640(7) 6
C6B C8 0.573(15) 6
C6B C3 1.604(5) 6
C6B C6B 1.70(2) 6
C6B C7B 1.721(11) 6
C6B C1B 1.958(9) 6
C6B C2B 1.966(5) 6
C7B C9 0.634(8) 6
C7B C4 1.363(13) 6
C7B C10B 1.539(4) 6
C7B C5B 1.640(8) 6
C7B C1B 1.718(14) 6
C7B C6B 1.721(17) 6
C8B C10 0.899(7) 6
C8B C9B 1.218(9) 6
C8B C5 1.453(7) 6
C8B C4B 1.531(7) 6
C8B C5B 1.879(7) 6
C8B C10B 2.039(3) 6
C9B C6 0.955(8) 6
C9B C8B 1.218(5) 6
C9B C3B 1.812(5) 6
C10B C7 0.797(6) 6
C10B C7B 1.539(11) 6
C10B C2 1.801(11) 6
C10B C8B 2.039(10) 6
C11 C12 1.394(6) .
C11 C16 1.396(6) .
C12 C13 1.400(6) .
C13 C14 1.374(7) .
C13 H13 0.9300 .
C14 C15 1.383(8) .
C14 H14 0.9300 .
C15 C16 1.391(7) .
C15 H15 0.9300 .
C16 H16 0.9300 .
C17 C18 1.387(7) .
C17 C18 1.387(7) 6
C18 C19 1.391(9) .
C18 H18 0.9300 .
C19 C20 1.358(11) .
C19 H19 0.9300 .
C20 C19 1.358(11) 6
C20 H20 0.9300 .
C21 C22 1.438(7) .
C21 C22 1.438(7) 6
C21 C24 1.502(11) .
C22 C23 1.412(7) .
C22 C25 1.487(7) .
C23 C23 1.432(9) 6
C23 C26 1.489(7) .
C24 H24A 0.9600 .
C24 H24B 0.9600 .
C24 H24C 0.9600 .
C25 H25A 0.9600 .
C25 H25B 0.9600 .
C25 H25C 0.9600 .
C26 H26A 0.9600 .
C26 H26B 0.9600 .
C26 H26C 0.9600 .
C27 F1 1.320(9) .
C27 F2 1.341(6) 6_565
C27 F2 1.341(6) .
C29 Cl1 1.66(2) 5_665
C29 C29 1.73(9) 5_665
F3 C28 1.5477 .
F4 C28 1.4322 .
C28 F4 1.4322 6
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C12 S1 Ru1 C2B 115.2(3) . 6
Ru2 S1 Ru1 C2B -146.4(3) . 6
C12 S1 Ru1 C2B 104.0(2) . .
Ru2 S1 Ru1 C2B -157.67(17) . .
C12 S1 Ru1 C1B 92.9(3) . .
Ru2 S1 Ru1 C1B -168.8(2) . .
C12 S1 Ru1 C1B 92.1(2) . 6
Ru2 S1 Ru1 C1B -169.48(18) . 6
C12 S1 Ru1 C3B 163.2(2) . 6
Ru2 S1 Ru1 C3B -98.42(16) . 6
C12 S1 Ru1 C3B 140.3(2) . .
Ru2 S1 Ru1 C3B -121.37(15) . .
C12 S1 Ru1 S1 -90.00(15) . 6
Ru2 S1 Ru1 S1 8.37(6) . 6
C12 S1 Ru1 P1 -6.36(15) . .
Ru2 S1 Ru1 P1 92.01(4) . .
C12 S1 Ru1 C2 155.2(2) . 6
Ru2 S1 Ru1 C2 -106.4(2) . 6
C12 S1 Ru1 C2 125.6(2) . .
Ru2 S1 Ru1 C2 -136.04(15) . .
C12 S1 Ru1 C5B 151.8(4) . .
Ru2 S1 Ru1 C5B -109.8(3) . .
C17 P1 Ru1 C2B -25.24(14) . 6
C11 P1 Ru1 C2B -146.2(2) . 6
C11 P1 Ru1 C2B 95.7(2) 6 6
C17 P1 Ru1 C2B 25.24(17) . .
C11 P1 Ru1 C2B -95.7(2) . .
C11 P1 Ru1 C2B 146.2(2) 6 .
C17 P1 Ru1 C1B -11.89(16) . .
C11 P1 Ru1 C1B -132.8(2) . .
C11 P1 Ru1 C1B 109.0(2) 6 .
C17 P1 Ru1 C1B 11.89(16) . 6
C11 P1 Ru1 C1B -109.0(2) . 6
C11 P1 Ru1 C1B 132.8(2) 6 6
C17 P1 Ru1 C3B -40.53(18) . 6
C11 P1 Ru1 C3B -161.5(2) . 6
C11 P1 Ru1 C3B 80.4(2) 6 6
C17 P1 Ru1 C3B 40.5(2) . .
C11 P1 Ru1 C3B -80.4(3) . .
C11 P1 Ru1 C3B 161.5(3) 6 .
C17 P1 Ru1 S1 124.24(3) . .
C11 P1 Ru1 S1 3.30(15) . .
C11 P1 Ru1 S1 -114.82(15) 6 .
C17 P1 Ru1 S1 -124.24(3) . 6
C11 P1 Ru1 S1 114.82(15) . 6
C11 P1 Ru1 S1 -3.30(15) 6 6
C17 P1 Ru1 C2 -40.02(14) . 6
C11 P1 Ru1 C2 -161.0(2) . 6
C11 P1 Ru1 C2 80.9(2) 6 6
C17 P1 Ru1 C2 40.0(2) . .
C11 P1 Ru1 C2 -80.9(3) . .
C11 P1 Ru1 C2 161.0(2) 6 .
C17 P1 Ru1 C5B -43.30(19) . .
C11 P1 Ru1 C5B -164.2(2) . .
C11 P1 Ru1 C5B 77.6(2) 6 .
C12 S1 Ru2 C23 -127.2(2) . 6
Ru1 S1 Ru2 C23 128.5(2) . 6
C12 S1 Ru2 C23 -111.59(19) . .
Ru1 S1 Ru2 C23 144.08(13) . .
C12 S1 Ru2 C21 -45.4(2) . .
Ru1 S1 Ru2 C21 -149.76(19) . .
C12 S1 Ru2 C22 -74.7(2) . .
Ru1 S1 Ru2 C22 -179.04(14) . .
C12 S1 Ru2 C22 -61.2(4) . 6
Ru1 S1 Ru2 C22 -165.5(3) . 6
C12 S1 Ru2 S1 96.15(15) . 6
Ru1 S1 Ru2 S1 -8.19(6) . 6
C12 S1 Ru2 Ru1 104.33(15) . .
C2B Ru1 Ru2 C23 18.2(4) 6 6
C2B Ru1 Ru2 C23 -80.5(3) . 6
C1B Ru1 Ru2 C23 22.1(7) . 6
C1B Ru1 Ru2 C23 -84.3(7) 6 6
C3B Ru1 Ru2 C23 -7.6(2) 6 6
C3B Ru1 Ru2 C23 -54.6(2) . 6
S1 Ru1 Ru2 C23 -125.8(2) . 6
S1 Ru1 Ru2 C23 63.6(2) 6 6
P1 Ru1 Ru2 C23 148.9(2) . 6
C2 Ru1 Ru2 C23 5.1(3) 6 6
C2 Ru1 Ru2 C23 -67.3(2) . 6
C5B Ru1 Ru2 C23 17.5(3) . 6
C2B Ru1 Ru2 C23 80.5(4) 6 .
C2B Ru1 Ru2 C23 -18.2(3) . .
C1B Ru1 Ru2 C23 84.3(6) . .
C1B Ru1 Ru2 C23 -22.1(7) 6 .
C3B Ru1 Ru2 C23 54.6(2) 6 .
C3B Ru1 Ru2 C23 7.6(2) . .
S1 Ru1 Ru2 C23 -63.6(2) . .
S1 Ru1 Ru2 C23 125.8(2) 6 .
P1 Ru1 Ru2 C23 -148.9(2) . .
C2 Ru1 Ru2 C23 67.3(3) 6 .
C2 Ru1 Ru2 C23 -5.1(2) . .
C5B Ru1 Ru2 C23 79.7(3) . .
C2B Ru1 Ru2 C21 -130.7(3) 6 .
C2B Ru1 Ru2 C21 130.7(3) . .
C1B Ru1 Ru2 C21 -126.8(6) . .
C1B Ru1 Ru2 C21 126.8(7) 6 .
C3B Ru1 Ru2 C21 -156.49(10) 6 .
C3B Ru1 Ru2 C21 156.49(8) . .
S1 Ru1 Ru2 C21 85.27(3) . .
S1 Ru1 Ru2 C21 -85.27(3) 6 .
P1 Ru1 Ru2 C21 0.0 . .
C2 Ru1 Ru2 C21 -143.79(16) 6 .
C2 Ru1 Ru2 C21 143.79(13) . .
C5B Ru1 Ru2 C21 -131.38(18) . .
C2B Ru1 Ru2 C22 145.9(4) 6 .
C2B Ru1 Ru2 C22 47.2(4) . .
C1B Ru1 Ru2 C22 149.7(7) . .
C1B Ru1 Ru2 C22 43.4(7) 6 .
C3B Ru1 Ru2 C22 120.1(3) 6 .
C3B Ru1 Ru2 C22 73.0(3) . .
S1 Ru1 Ru2 C22 1.8(3) . .
S1 Ru1 Ru2 C22 -168.7(3) 6 .
P1 Ru1 Ru2 C22 -83.4(3) . .
C2 Ru1 Ru2 C22 132.8(3) 6 .
C2 Ru1 Ru2 C22 60.3(3) . .
C5B Ru1 Ru2 C22 145.2(3) . .
C2B Ru1 Ru2 C22 -47.2(4) 6 6
C2B Ru1 Ru2 C22 -145.9(4) . 6
C1B Ru1 Ru2 C22 -43.4(7) . 6
C1B Ru1 Ru2 C22 -149.7(7) 6 6
C3B Ru1 Ru2 C22 -73.0(3) 6 6
C3B Ru1 Ru2 C22 -120.1(3) . 6
S1 Ru1 Ru2 C22 168.7(3) . 6
S1 Ru1 Ru2 C22 -1.8(3) 6 6
P1 Ru1 Ru2 C22 83.4(3) . 6
C2 Ru1 Ru2 C22 -60.3(3) 6 6
C2 Ru1 Ru2 C22 -132.8(3) . 6
C5B Ru1 Ru2 C22 -47.9(3) . 6
C2B Ru1 Ru2 S1 -45.4(3) 6 6
C2B Ru1 Ru2 S1 -144.1(3) . 6
C1B Ru1 Ru2 S1 -41.5(6) . 6
C1B Ru1 Ru2 S1 -147.9(7) 6 6
C3B Ru1 Ru2 S1 -71.22(11) 6 6
C3B Ru1 Ru2 S1 -118.24(8) . 6
S1 Ru1 Ru2 S1 170.54(7) . 6
P1 Ru1 Ru2 S1 85.27(3) . 6
C2 Ru1 Ru2 S1 -58.52(16) 6 6
C2 Ru1 Ru2 S1 -130.94(14) . 6
C5B Ru1 Ru2 S1 -46.11(18) . 6
C2B Ru1 Ru2 S1 144.1(3) 6 .
C2B Ru1 Ru2 S1 45.4(3) . .
C1B Ru1 Ru2 S1 147.9(6) . .
C1B Ru1 Ru2 S1 41.5(7) 6 .
C3B Ru1 Ru2 S1 118.24(11) 6 .
C3B Ru1 Ru2 S1 71.22(8) . .
S1 Ru1 Ru2 S1 -170.54(7) 6 .
P1 Ru1 Ru2 S1 -85.27(3) . .
C2 Ru1 Ru2 S1 130.94(17) 6 .
C2 Ru1 Ru2 S1 58.52(14) . .
C5B Ru1 Ru2 S1 143.34(18) . .
C4B C1 C2 C5 -8.2(3) 6 6
C4B C1 C2 C5 159.5(3) . 6
C3B C1 C2 C5 -4.9(3) . 6
C3B C1 C2 C5 162.5(3) 6 6
C5 C1 C2 C5 161.9(3) . 6
C2 C1 C2 C5 164.7(3) 6 6
C6 C1 C2 C5 -18.3(3) 6 6
C6 C1 C2 C5 -17.8(3) . 6
C9B C1 C2 C5 -17.1(3) 6 6
C9B C1 C2 C5 -25.7(3) . 6
C4B C1 C2 C5B -110.9(19) 6 6
C4B C1 C2 C5B 56.8(19) . 6
C3B C1 C2 C5B -107.6(19) . 6
C3B C1 C2 C5B 59.8(19) 6 6
C5 C1 C2 C5B 59.2(19) . 6
C5 C1 C2 C5B -102.7(16) 6 6
C2 C1 C2 C5B 62.0(19) 6 6
C6 C1 C2 C5B -121.0(19) 6 6
C6 C1 C2 C5B -120.5(19) . 6
C9B C1 C2 C5B -119.8(19) 6 6
C9B C1 C2 C5B -128.4(19) . 6
C4B C1 C2 C3B -3.2 6 .
C4B C1 C2 C3B 164.4 . .
C3B C1 C2 C3B 167.4 6 .
C5 C1 C2 C3B 166.9 . .
C5 C1 C2 C3B 4.9(3) 6 .
C2 C1 C2 C3B 169.6 6 .
C6 C1 C2 C3B -13.4 6 .
C6 C1 C2 C3B -12.9 . .
C9B C1 C2 C3B -12.1 6 .
C9B C1 C2 C3B -20.8 . .
C4B C1 C2 C2B -163.6 6 .
C4B C1 C2 C2B 4.1 . .
C3B C1 C2 C2B -160.3 . .
C3B C1 C2 C2B 7.1 6 .
C5 C1 C2 C2B 6.5 . .
C5 C1 C2 C2B -155.4(3) 6 .
C2 C1 C2 C2B 9.3 6 .
C6 C1 C2 C2B -173.7 6 .
C6 C1 C2 C2B -173.2 . .
C9B C1 C2 C2B -172.5 6 .
C4B C1 C2 C4B 167.7 . 6
C3B C1 C2 C4B 3.2 . 6
C3B C1 C2 C4B 170.7 6 6
C5 C1 C2 C4B 170.1 . 6
C5 C1 C2 C4B 8.2(3) 6 6
C2 C1 C2 C4B 172.9 6 6
C6 C1 C2 C4B -10.2 6 6
C6 C1 C2 C4B -9.6 . 6
C9B C1 C2 C4B -8.9 6 6
C9B C1 C2 C4B -17.6 . 6
C4B C1 C2 C4 -167.2 6 6
C4B C1 C2 C4 0.5 . 6
C3B C1 C2 C4 -163.9 . 6
C3B C1 C2 C4 3.5 6 6
C5 C1 C2 C4 2.9 . 6
C5 C1 C2 C4 -159.0(3) 6 6
C2 C1 C2 C4 5.7 6 6
C6 C1 C2 C4 -177.3 6 6
C6 C1 C2 C4 -176.8 . 6
C9B C1 C2 C4 -176.1 6 6
C9B C1 C2 C4 175.3 . 6
C4B C1 C2 C3 -170.3 6 .
C4B C1 C2 C3 -2.6 . .
C3B C1 C2 C3 -167.0 . .
C3B C1 C2 C3 0.4 6 .
C5 C1 C2 C3 -0.1 . .
C5 C1 C2 C3 -162.1(3) 6 .
C2 C1 C2 C3 2.6 6 .
C6 C1 C2 C3 179.6 6 .
C6 C1 C2 C3 -179.9 . .
C9B C1 C2 C3 -179.1 6 .
C9B C1 C2 C3 172.2 . .
C4B C1 C2 C7 9.8 6 .
C4B C1 C2 C7 177.5 . .
C3B C1 C2 C7 13.1 . .
C3B C1 C2 C7 -179.5 6 .
C5 C1 C2 C7 179.9 . .
C5 C1 C2 C7 18.0(3) 6 .
C2 C1 C2 C7 -177.3 6 .
C6 C1 C2 C7 -0.3 6 .
C6 C1 C2 C7 0.2 . .
C9B C1 C2 C7 0.9 6 .
C9B C1 C2 C7 -7.7 . .
C4B C1 C2 C1B -165.0 6 6
C4B C1 C2 C1B 2.7 . 6
C3B C1 C2 C1B -161.7 . 6
C3B C1 C2 C1B 5.7 6 6
C5 C1 C2 C1B 5.1 . 6
C5 C1 C2 C1B -156.8(3) 6 6
C2 C1 C2 C1B 7.9 6 6
C6 C1 C2 C1B -175.1 6 6
C6 C1 C2 C1B -174.6 . 6
C9B C1 C2 C1B -173.9 6 6
C9B C1 C2 C1B 177.5 . 6
C4B C1 C2 C8B 9.4 6 .
C4B C1 C2 C8B 177.0 . .
C3B C1 C2 C8B 12.6 . .
C3B C1 C2 C8B -180.0 6 .
C5 C1 C2 C8B 179.5 . .
C5 C1 C2 C8B 17.5(3) 6 .
C2 C1 C2 C8B -177.8 6 .
C6 C1 C2 C8B -0.8 6 .
C6 C1 C2 C8B -0.3 . .
C9B C1 C2 C8B 0.5 6 .
C9B C1 C2 C8B -8.2 . .
C4B C1 C2 C10 4.0 6 6
C4B C1 C2 C10 171.7 . 6
C3B C1 C2 C10 7.2 . 6
C3B C1 C2 C10 174.7 6 6
C5 C1 C2 C10 174.1 . 6
C5 C1 C2 C10 12.2(3) 6 6
C2 C1 C2 C10 176.9 6 6
C6 C1 C2 C10 -6.2 6 6
C6 C1 C2 C10 -5.6 . 6
C9B C1 C2 C10 -4.9 6 6
C9B C1 C2 C10 -13.6 . 6
C5 C2 C3 C1B -23(4) 6 6
C5B C2 C3 C1B -83(4) 6 6
C3B C2 C3 C1B 70(4) . 6
C2B C2 C3 C1B -72(4) . 6
C4B C2 C3 C1B 71(4) 6 6
C4 C2 C3 C1B -94(4) 6 6
C1 C2 C3 C1B 75(4) . 6
C7 C2 C3 C1B -105(4) . 6
C8B C2 C3 C1B -103(4) . 6
C10 C2 C3 C1B -97(4) 6 6
C5 C2 C3 C4 71(5) 6 6
C5B C2 C3 C4 11.5(2) 6 6
C3B C2 C3 C4 163.6(4) . 6
C2B C2 C3 C4 22.3(4) . 6
C4B C2 C3 C4 165.1(4) 6 6
C1 C2 C3 C4 168.7(4) . 6
C7 C2 C3 C4 -11.4(4) . 6
C1B C2 C3 C4 94(4) 6 6
C8B C2 C3 C4 -8.5(4) . 6
C10 C2 C3 C4 -2.6(3) 6 6
C5 C2 C3 C2B 49(5) 6 .
C5B C2 C3 C2B -10.8(5) 6 .
C3B C2 C3 C2B 141.4 . .
C4B C2 C3 C2B 142.8 6 .
C4 C2 C3 C2B -22.3(4) 6 .
C1 C2 C3 C2B 146.4 . .
C7 C2 C3 C2B -33.6 . .
C1B C2 C3 C2B 72(4) 6 .
C8B C2 C3 C2B -30.8 . .
C10 C2 C3 C2B -24.85(8) 6 .
C5 C2 C3 C1B -90(5) 6 .
C5B C2 C3 C1B -149.9(5) 6 .
C3B C2 C3 C1B 2.2 . .
C2B C2 C3 C1B -139.1 . .
C4B C2 C3 C1B 3.7 6 .
C4 C2 C3 C1B -161.4(4) 6 .
C1 C2 C3 C1B 7.3 . .
C7 C2 C3 C1B -172.8 . .
C1B C2 C3 C1B -67(4) 6 .
C8B C2 C3 C1B -169.9 . .
C10 C2 C3 C1B -163.98(8) 6 .
C5 C2 C3 C3 -100(5) 6 6
C5B C2 C3 C3 -159.1(5) 6 6
C3B C2 C3 C3 -6.9 . 6
C2B C2 C3 C3 -148.3 . 6
C4B C2 C3 C3 -5.5 6 6
C4 C2 C3 C3 -170.6(4) 6 6
C1 C2 C3 C3 -1.9 . 6
C7 C2 C3 C3 178.1 . 6
C1B C2 C3 C3 -76(4) 6 6
C10 C2 C3 C3 -173.16(8) 6 6
C5 C2 C3 C5B 59(4) 6 6
C3B C2 C3 C5B 152.2(5) . 6
C2B C2 C3 C5B 10.8(5) . 6
C4B C2 C3 C5B 153.6(5) 6 6
C4 C2 C3 C5B -11.5(2) 6 6
C1 C2 C3 C5B 157.2(5) . 6
C7 C2 C3 C5B -22.9(5) . 6
C1B C2 C3 C5B 83(4) 6 6
C8B C2 C3 C5B -20.0(5) . 6
C10 C2 C3 C5B -14.1(4) 6 6
C5 C2 C3 C4 -98(5) 6 .
C5B C2 C3 C4 -157.1(5) 6 .
C3B C2 C3 C4 -5.0 . .
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C7B C3 C4 C5 -152.5 . .
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C1B C3 C4 C9 52.3(4) 6 .
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C1B C3 C4 C9 29.9 . .
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C8 C3 C4 C9 0.0 . .
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C7B C3 C4 C9 27.5 . .
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C5 C1 C6 C4B -1.8 . .
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C6 C1 C6 C4B -3.7 6 .
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C9B C1 C6 C4B -4.0 . .
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C3B C2 C7 C10 -14.69(15) . 6
C2B C2 C7 C10 154.31(15) . 6
C4B C2 C7 C10 -15.90(15) 6 6
C4 C2 C7 C10 158.15(16) 6 6
C3 C2 C7 C10 161.03(15) . 6
C1 C2 C7 C10 -19.06(15) . 6
C1B C2 C7 C10 154.65(15) 6 6
C8B C2 C7 C10 -18.43(15) . 6
C5 C2 C7 C10B -141.37(19) 6 6
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C1B C3 C1B C6B 54.7 6 .
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C2 C3 C2B C4 145.7(2) . 6
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C6B C3 C2B C1B 72(3) 6 6
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C1B C3 C2B C2 51.2 . .
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C4 C3 C2B C5 33.0(3) . 6
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C2B C3 C2B C5 32.3(3) 6 6
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C4 C3 C2B C3B 21.9 . .
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C7B C3 C2B C3B -165.7 . .
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C4 C3 C2B C1B -11.8 . .
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C7B C3 C2B C1B 160.6 . .
C1B C3 C2B C3 83(3) 6 6
C4 C3 C2B C3 175.6(2) 6 6
C1B C3 C2B C3 12.5 . 6
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C4 C3 C2B C3 0.7 . 6
C2 C3 C2B C3 -38.7 . 6
C2B C3 C2B C3 0.0 6 6
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C7B C3 C2B C3 173.1 . 6
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C5B C3 C2B C7B 106(4) 6 .
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C8 C3 C2B C7B -3.4 . .
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C4 C3 C2B C2B 175.6(2) 6 6
C1B C3 C2B C2B 12.5 . 6
C3 C3 C2B C2B 0.0 6 6
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C4 C3 C2B C2B 0.7 . 6
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C4 C3 C2B C9 5.48(13) 6 6
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C5B C3 C2B C9 109(4) 6 6
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C6B C3 C2B C9 -14.7(2) 6 6
C7B C3 C2B C9 2.95(9) . 6
C5 C2 C2B C4 102(7) 6 6
C5B C2 C2B C4 59(4) 6 6
C3B C2 C2B C4 -154(4) . 6
C4B C2 C2B C4 -152(4) 6 6
C3 C2 C2B C4 -109(4) . 6
C1 C2 C2B C4 -145(4) . 6
C7 C2 C2B C4 41(4) . 6
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C8B C2 C2B C4 58(4) . 6
C10 C2 C2B C4 50(4) 6 6
C5 C2 C2B C3 -149(3) 6 .
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C3B C2 C2B C3 -44.6 . .
C4B C2 C2B C3 -42.85(5) 6 .
C4 C2 C2B C3 109(4) 6 .
C1 C2 C2B C3 -36.0 . .
C7 C2 C2B C3 149.9 . .
C1B C2 C2B C3 -28.62(5) 6 .
C8B C2 C2B C3 166.9 . .
C10 C2 C2B C3 159.60(10) 6 .
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C5B C2 C2B C1B -163.6(5) 6 6
C3B C2 C2B C1B -16.0 . 6
C4B C2 C2B C1B -14.22(8) 6 6
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C3 C2 C2B C1B 28.62(5) . 6
C1 C2 C2B C1B -7.42(5) . 6
C7 C2 C2B C1B 178.50(5) . 6
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C5 C2 C2B C5B 43(3) 6 6
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C1B C2 C2B C5B 163.6(5) 6 6
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C10 C2 C2B C5B -8.2(4) 6 6
C5B C2 C2B C5 -43(3) 6 6
C3B C2 C2B C5 104(3) . 6
C4B C2 C2B C5 106(3) 6 6
C4 C2 C2B C5 -102(7) 6 6
C3 C2 C2B C5 149(3) . 6
C1 C2 C2B C5 113(3) . 6
C7 C2 C2B C5 -61(3) . 6
C1B C2 C2B C5 120(3) 6 6
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C10 C2 C2B C5 -51(3) 6 6
C5 C2 C2B C3B -104(3) 6 .
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C3 C2 C2B C3B 44.6 . .
C1 C2 C2B C3B 8.6 . .
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C8B C2 C2B C3B -148.5 . .
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C3 C2 C2B C1B 29.5 . .
C1 C2 C2B C1B -6.5 . .
C7 C2 C2B C1B 179.4 . .
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C5 C2 C2B C3 -125(3) 6 6
C5B C2 C2B C3 -168.4(5) 6 6
C3B C2 C2B C3 -20.85(6) . 6
C4B C2 C2B C3 -19.10(7) 6 6
C4 C2 C2B C3 133(4) 6 6
C3 C2 C2B C3 23.75(6) . 6
C1 C2 C2B C3 -12.29(6) . 6
C7 C2 C2B C3 173.63(5) . 6
C1B C2 C2B C3 -4.9 6 6
C8B C2 C2B C3 -169.32(6) . 6
C10 C2 C2B C3 -176.65(10) 6 6
C5 C2 C2B C7B 65(3) 6 .
C5B C2 C2B C7B 21.3(5) 6 .
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C4B C2 C2B C7B 170.7 6 .
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C3 C2 C2B C7B -146.5 . .
C1 C2 C2B C7B 177.5 . .
C7 C2 C2B C7B 3.4 . .
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C8B C2 C2B C7B 20.4 . .
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C5B C2 C2B C2B -162.4(5) 6 6
C3B C2 C2B C2B -14.8 . 6
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C3 C2 C2B C2B 29.8 . 6
C1 C2 C2B C2B -6.2 . 6
C7 C2 C2B C2B 179.7 . 6
C1B C2 C2B C2B 1.18(5) 6 6
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C5 C2 C2B C9 68(3) 6 6
C5B C2 C2B C9 25.1(6) 6 6
C3B C2 C2B C9 172.68(11) . 6
C4B C2 C2B C9 174.43(14) 6 6
C4 C2 C2B C9 -34(4) 6 6
C3 C2 C2B C9 -142.73(10) . 6
C1 C2 C2B C9 -178.77(11) . 6
C7 C2 C2B C9 7.15(11) . 6
C1B C2 C2B C9 -171.35(6) 6 6
C8B C2 C2B C9 24.20(11) . 6
C10 C2 C2B C9 16.88(18) 6 6
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C3 C1B C2B C3 108.1(9) 6 .
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C6B C1B C2B C3 -24.1 . .
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C8 C1B C2B C1B 19.82(16) 6 6
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C7B C1B C2B C1B 164.7(3) 6 6
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C4 C1B C2B C5B -177.4(4) 6 6
C5B C1B C2B C5B -9.30(11) . 6
C8 C1B C2B C5B -173.4(2) 6 6
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C3 C1B C2B C2 -43.1(9) 6 .
C4 C1B C2B C2 -9.8 . .
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C3 C1B C2B C3B -47.8(9) 6 .
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C5B C1B C2B C3B 0.0 . .
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C7B C1B C2B C3 28.6(6) 6 6
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C2B C1B C2B C7B 176.1 6 .
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C8 C1B C2B C7B 15.93(16) 6 .
C6B C1B C2B C7B 0.0 . .
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C7B C1B C2B C7B 160.8(3) 6 .
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C4 C1B C2B C2B -10.6 . 6
C1B C1B C2B C2B 180.0 6 6
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C5B C1B C2B C2B 3.9 . 6
C8 C1B C2B C2B -160.18(16) 6 6
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C2B C1B C2B C9 174.6 6 6
C1B C1B C2B C9 -5.4 6 6
C3 C1B C2B C9 22.6 . 6
C4 C1B C2B C9 10.4(2) 6 6
C5B C1B C2B C9 178.5 . 6
C8 C1B C2B C9 14.40(14) 6 6
C6B C1B C2B C9 -1.5 . 6
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C5 C2 C3B C4B -138(7) 6 6
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C2B C2 C3B C4B 72(7) . 6
C4 C2 C3B C4B 69(7) 6 6
C3 C2 C3B C4B 63(7) . 6
C1 C2 C3B C4B 48(7) . 6
C7 C2 C3B C4B -121(7) . 6
C1B C2 C3B C4B 69(7) 6 6
C8B C2 C3B C4B -118(7) . 6
C10 C2 C3B C4B -126(7) 6 6
C5B C2 C3B C5 -59(2) 6 6
C2B C2 C3B C5 -149.7(4) . 6
C4B C2 C3B C5 138(7) 6 6
C4 C2 C3B C5 -153.3(3) 6 6
C3 C2 C3B C5 -159.0(4) . 6
C1 C2 C3B C5 -174.3(4) . 6
C7 C2 C3B C5 16.7(4) . 6
C1B C2 C3B C5 -153.1(3) 6 6
C8B C2 C3B C5 19.8(4) . 6
C10 C2 C3B C5 12.5(4) 6 6
C5 C2 C3B C1 174.3(4) 6 .
C5B C2 C3B C1 115(3) 6 .
C2B C2 C3B C1 24.6 . .
C4B C2 C3B C1 -48(7) 6 .
C4 C2 C3B C1 21.01(17) 6 .
C3 C2 C3B C1 15.3 . .
C7 C2 C3B C1 -169.0 . .
C1B C2 C3B C1 21.18(11) 6 .
C8B C2 C3B C1 -165.9 . .
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C2B C2 C3B C5B -91(3) . 6
C4B C2 C3B C5B -163(9) 6 6
C4 C2 C3B C5B -94(2) 6 6
C3 C2 C3B C5B -100(3) . 6
C1 C2 C3B C5B -115(3) . 6
C7 C2 C3B C5B 76(3) . 6
C1B C2 C3B C5B -94(2) 6 6
C8B C2 C3B C5B 79(3) . 6
C10 C2 C3B C5B 71(3) 6 6
C5 C2 C3B C2B 149.7(4) 6 .
C5B C2 C3B C2B 91(3) 6 .
C4B C2 C3B C2B -72(7) 6 .
C4 C2 C3B C2B -3.62(17) 6 .
C3 C2 C3B C2B -9.4 . .
C1 C2 C3B C2B -24.6 . .
C7 C2 C3B C2B 166.4 . .
C1B C2 C3B C2B -3.44(11) 6 .
C8B C2 C3B C2B 169.4 . .
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C5 C2 C3B C4B 167.6(4) 6 .
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C3B C1 C4B C9B -175.9 . .
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C6 C1 C4B C9B -2.5 6 .
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C2 C5 C5B C10 152.0(12) 6 .
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C7 C5 C5B C10 8.7 6 .
C1 C5 C5B C10 -172.9 . .
C4 C5 C5B C10 168.9 . .
C8B C5 C5B C10 1.2 6 .
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C10B C5 C5B C10 3.2 . .
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C5 C4 C5B C2 -7.9(4) . 6
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C7B C4 C5B C5 167.1 6 .
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C3 C4 C5B C5 -15.3 . .
C8 C4 C5B C5 166.04(5) 6 .
C9 C4 C5B C5 168.2 . .
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C3B C4 C5B C2B 18.8(6) 6 6
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C3 C4 C5B C3B -3.0(3) 6 6
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C5 C4 C5B C3B 6.6 . 6
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C9 C4 C5B C4B 177.4 . .
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C9 C4 C5B C1B -153.3 . .
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C7B C4 C5B C10B 2.1 6 .
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C8 C4 C5B C10B 1.0 6 .
C9 C4 C5B C10B 3.2 . .
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C8 C4 C5B C7B -1.0 6 6
C9 C4 C5B C7B 1.2 . 6
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C7B C4 C5B C10 14.5 6 .
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C3 C4 C5B C10 -167.9 . .
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C8 C4 C5B C10 13.5 6 .
C9 C4 C5B C10 15.7 . .
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C4B C4B C5B C2 78(3) 6 6
C3B C4B C5B C2 77(3) . 6
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C6 C4B C5B C2 -113(3) . 6
C2B C4B C5B C2 73(3) 6 6
C3B C4B C5B C5 85(6) 6 .
C1 C4B C5B C5 165.3 . .
C2 C4B C5B C5 91(3) 6 .
C4B C4B C5B C5 169.6 6 .
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C9B C4B C5B C5 -12.1 . .
C8B C4B C5B C5 -8.4 6 .
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C6 C4B C5B C5 -21.4 . .
C2B C4B C5B C5 164.56(6) 6 .
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C1 C4B C5B C2B 0.76(6) . 6
C5 C4B C5B C2B -164.56(6) . 6
C2 C4B C5B C2B -73(3) 6 6
C4B C4B C5B C2B 5.00(6) 6 6
C3B C4B C5B C2B 3.34(6) . 6
C9B C4B C5B C2B -176.66(6) . 6
C8B C4B C5B C2B -173.00(6) 6 6
C6 C4B C5B C2B 179.7 6 6
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C1 C4B C5B C3B 80(6) . 6
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C2 C4B C5B C3B 6(3) 6 6
C4B C4B C5B C3B 84(6) 6 6
C3B C4B C5B C3B 83(6) . 6
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C8B C4B C5B C3B -94(6) 6 6
C6 C4B C5B C3B -101(6) 6 6
C6 C4B C5B C3B -107(6) . 6
C2B C4B C5B C3B 79(6) 6 6
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C1 C4B C5B C4 4.0 . .
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C4B C4B C5B C4 8.2 6 .
C3B C4B C5B C4 6.6 . .
C9B C4B C5B C4 -173.4 . .
C8B C4B C5B C4 -169.8 6 .
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C2B C4B C5B C4 3.21(6) 6 .
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C1 C4B C5B C3 3.88(7) . 6
C5 C4B C5B C3 -161.45(7) . 6
C2 C4B C5B C3 -70(3) 6 6
C4B C4B C5B C3 8.12(7) 6 6
C3B C4B C5B C3 6.46(7) . 6
C9B C4B C5B C3 -173.54(7) . 6
C8B C4B C5B C3 -169.88(7) 6 6
C6 C4B C5B C3 -177.2 6 6
C6 C4B C5B C3 177.15(7) . 6
C2B C4B C5B C3 3.1 6 6
C3B C4B C5B C1B -83(6) 6 .
C1 C4B C5B C1B -2.6 . .
C5 C4B C5B C1B -167.9 . .
C2 C4B C5B C1B -77(3) 6 .
C4B C4B C5B C1B 1.7 6 .
C3B C4B C5B C1B 0.0 . .
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C8B C4B C5B C1B -176.3 6 .
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C3B C4B C5B C7 90(6) 6 6
C1 C4B C5B C7 169.9 . 6
C5 C4B C5B C7 4.53(5) . 6
C2 C4B C5B C7 96(3) 6 6
C4B C4B C5B C7 174.1 6 6
C3B C4B C5B C7 172.4 . 6
C9B C4B C5B C7 -7.6 . 6
C8B C4B C5B C7 -3.9 6 6
C6 C4B C5B C7 -11.23(8) 6 6
C6 C4B C5B C7 -16.9 . 6
C2B C4B C5B C7 169.1 6 6
C3B C4B C5B C10B 97(6) 6 .
C1 C4B C5B C10B 177.4 . .
C5 C4B C5B C10B 12.1 . .
C2 C4B C5B C10B 103(3) 6 .
C4B C4B C5B C10B -178.3 6 .
C3B C4B C5B C10B 180.0 . .
C9B C4B C5B C10B 0.0 . .
C8B C4B C5B C10B 3.7 6 .
C6 C4B C5B C10B -3.67(7) 6 .
C6 C4B C5B C10B -9.3 . .
C2B C4B C5B C10B 176.65(6) 6 .
C3B C4B C5B C7B -42(3) 6 6
C1 C4B C5B C7B 38(4) . 6
C5 C4B C5B C7B -127(4) . 6
C2 C4B C5B C7B -35.8(11) 6 6
C4B C4B C5B C7B 42(4) 6 6
C3B C4B C5B C7B 41(4) . 6
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C8B C4B C5B C7B -136(4) 6 6
C6 C4B C5B C7B -143(4) 6 6
C6 C4B C5B C7B -149(4) . 6
C2B C4B C5B C7B 37(4) 6 6
C3B C4B C5B C10 97(6) 6 .
C1 C4B C5B C10 177.3 . .
C5 C4B C5B C10 11.9 . .
C2 C4B C5B C10 103(3) 6 .
C4B C4B C5B C10 -178.5 6 .
C3B C4B C5B C10 179.9 . .
C9B C4B C5B C10 -0.1 . .
C8B C4B C5B C10 3.5 6 .
C6 C4B C5B C10 -3.82(7) 6 .
C6 C4B C5B C10 -9.5 . .
C2B C4B C5B C10 176.51(6) 6 .
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C4 C1B C5B C2 136.6(3) . 6
C2B C1B C5B C2 87(10) 6 6
C1B C1B C5B C2 -18.6(3) 6 6
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C2B C1B C5B C2 -16.8(3) . 6
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C7B C1B C5B C2 159.3(2) 6 6
C3 C1B C5B C5 83(4) 6 .
C4 C1B C5B C5 148.3 . .
C2B C1B C5B C5 99(10) 6 .
C1B C1B C5B C5 -6.8 6 .
C3 C1B C5B C5 2.6 . .
C4 C1B C5B C5 -2.5 6 .
C2B C1B C5B C5 -5.1 . .
C8 C1B C5B C5 165.53(8) 6 .
C6B C1B C5B C5 174.9 . .
C2 C1B C5B C5 11.7(3) 6 .
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C2B C1B C5B C2B -104(10) . 6
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C6B C1B C5B C2B 76(10) . 6
C2 C1B C5B C2B -87(10) 6 6
C7B C1B C5B C2B 72(10) 6 6
C3 C1B C5B C3B 85(4) 6 6
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C1B C1B C5B C3B -4.2 6 6
C3 C1B C5B C3B 5.3 . 6
C4 C1B C5B C3B 0.2 6 6
C2B C1B C5B C3B -2.4 . 6
C8 C1B C5B C3B 168.21(7) 6 6
C6B C1B C5B C3B 177.6 . 6
C2 C1B C5B C3B 14.4(2) 6 6
C7B C1B C5B C3B 173.7 6 6
C3 C1B C5B C4 -66(4) 6 .
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C2B C1B C5B C4 -153.3 . .
C8 C1B C5B C4 17.25(8) 6 .
C6B C1B C5B C4 26.7 . .
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C7B C1B C5B C4 22.7 6 .
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C2B C1B C5B C3 17(7) 6 6
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C2B C1B C5B C3 -88(4) . 6
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C6B C1B C5B C3 92(4) . 6
C2 C1B C5B C3 -71(4) 6 6
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C1B C1B C5B C4B -1.8 6 .
C3 C1B C5B C4B 7.7 . .
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C2B C1B C5B C4B 0.0 . .
C8 C1B C5B C4B 170.60(8) 6 .
C6B C1B C5B C4B 180.0 . .
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C7B C1B C5B C4B 176.1 6 .
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C7B C1B C5B C10B -3.9 6 .
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C4 C1B C5B C7B -22.7 . 6
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C6B C1B C5B C7B 3.9 . 6
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C4 C1B C5B C10 -25.8 . .
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C4 C1B C5B C10 -176.5 6 .
C8 C1B C5B C10 -8.51(8) 6 .
C6B C1B C5B C10 0.9 . .
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C7B C1B C5B C10 -3.0 6 .
C7 C10 C5B C2 -135.7(4) 6 6
C8B C10 C5B C2 10.50(19) 6 6
C10B C10 C5B C2 -163.8(2) . 6
C5 C10 C5B C2 11.9(2) . 6
C3B C10 C5B C2 14.1(2) 6 6
C7 C10 C5B C5 -147.5(6) 6 .
C8B C10 C5B C5 -1.38(6) 6 .
C10B C10 C5B C5 -175.7 . .
C2 C10 C5B C5 -11.9(2) 6 .
C3B C10 C5B C5 2.2 6 .
C7 C10 C5B C2B 9.9(6) 6 6
C8B C10 C5B C2B 156.0(8) 6 6
C10B C10 C5B C2B -18.3(8) . 6
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C2 C10 C5B C2B 145.5(6) 6 6
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C8B C10 C5B C3B -3.59(5) 6 6
C10B C10 C5B C3B -177.9 . 6
C5 C10 C5B C3B -2.2 . 6
C2 C10 C5B C3B -14.1(2) 6 6
C7 C10 C5B C4 11.9(6) 6 .
C8B C10 C5B C4 158.10(6) 6 .
C10B C10 C5B C4 -16.2 . .
C5 C10 C5B C4 159.5 . .
C2 C10 C5B C4 147.6(2) 6 .
C3B C10 C5B C4 161.7 6 .
C7 C10 C5B C3 -6.9(9) 6 6
C8B C10 C5B C3 139.3(10) 6 6
C10B C10 C5B C3 -35.0(10) . 6
C5 C10 C5B C3 140.7(10) . 6
C2 C10 C5B C3 128.8(8) 6 6
C3B C10 C5B C3 142.9(10) 6 6
C7 C10 C5B C4B -152.0(6) 6 .
C8B C10 C5B C4B -5.89(6) 6 .
C10B C10 C5B C4B 179.8 . .
C5 C10 C5B C4B -4.5 . .
C2 C10 C5B C4B -16.4(2) 6 .
C3B C10 C5B C4B -2.3 6 .
C7 C10 C5B C1B 27.1(6) 6 .
C8B C10 C5B C1B 173.25(6) 6 .
C10B C10 C5B C1B -1.0 . .
C5 C10 C5B C1B 174.6 . .
C2 C10 C5B C1B 162.8(2) 6 .
C3B C10 C5B C1B 176.8 6 .
C8B C10 C5B C7 146.2(5) 6 6
C10B C10 C5B C7 -28.1(6) . 6
C5 C10 C5B C7 147.5(6) . 6
C2 C10 C5B C7 135.7(4) 6 6
C3B C10 C5B C7 149.7(6) 6 6
C7 C10 C5B C10B 28.1(6) 6 .
C8B C10 C5B C10B 174.28(6) 6 .
C5 C10 C5B C10B 175.7 . .
C2 C10 C5B C10B 163.8(2) 6 .
C3B C10 C5B C10B 177.9 6 .
C7 C10 C5B C7B 24.2(6) 6 6
C8B C10 C5B C7B 170.39(6) 6 6
C10B C10 C5B C7B -3.9 . 6
C5 C10 C5B C7B 171.8 . 6
C2 C10 C5B C7B 159.9(2) 6 6
C3B C10 C5B C7B 174.0 6 6
C7B C9 C6B C8 99(3) 6 6
C4 C9 C6B C8 87(3) . 6
C3 C9 C6B C8 83(3) 6 6
C1B C9 C6B C8 88(3) . 6
C2B C9 C6B C8 89(3) 6 6
C7B C9 C6B C1B 10.6(4) 6 .
C8 C9 C6B C1B -88(3) 6 .
C4 C9 C6B C1B -1.5 . .
C3 C9 C6B C1B -4.7 6 .
C2B C9 C6B C1B 0.7 6 .
C7B C9 C6B C3 15.3(4) 6 6
C8 C9 C6B C3 -83(3) 6 6
C4 C9 C6B C3 3.2 . 6
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C2B C9 C6B C3 5.4 6 6
C7B C9 C6B C6B 21.6(4) 6 6
C8 C9 C6B C6B -77(3) 6 6
C4 C9 C6B C6B 9.5 . 6
C3 C9 C6B C6B 6.3 6 6
C1B C9 C6B C6B 11.0 . 6
C2B C9 C6B C6B 11.7 6 6
C7B C9 C6B C4 12.1(4) 6 .
C8 C9 C6B C4 -87(3) 6 .
C3 C9 C6B C4 -3.2 6 .
C1B C9 C6B C4 1.5 . .
C2B C9 C6B C4 2.2 6 .
C8 C9 C6B C7B -99(3) 6 6
C4 C9 C6B C7B -12.1(4) . 6
C3 C9 C6B C7B -15.3(4) 6 6
C1B C9 C6B C7B -10.6(4) . 6
C2B C9 C6B C7B -9.9(4) 6 6
C7B C9 C6B C1B 13.0(4) 6 6
C8 C9 C6B C1B -86(3) 6 6
C4 C9 C6B C1B 0.9 . 6
C3 C9 C6B C1B -2.3 6 6
C1B C9 C6B C1B 2.4 . 6
C2B C9 C6B C1B 3.1 6 6
C7B C9 C6B C2B 9.9(4) 6 6
C8 C9 C6B C2B -89(3) 6 6
C4 C9 C6B C2B -2.2 . 6
C3 C9 C6B C2B -5.4 6 6
C1B C9 C6B C2B -0.7 . 6
C3 C1B C6B C8 29(2) 6 6
C4 C1B C6B C8 -13.6(8) . 6
C2B C1B C6B C8 -20.4(7) 6 6
C1B C1B C6B C8 156.5(8) 6 6
C3 C1B C6B C8 148.1(8) . 6
C4 C1B C6B C8 152.6(7) 6 6
C5B C1B C6B C8 -24.9(8) . 6
C2B C1B C6B C8 155.1(8) . 6
C2 C1B C6B C8 -18.2(7) 6 6
C7B C1B C6B C8 -21.1(7) 6 6
C3 C1B C6B C9 47(3) 6 .
C4 C1B C6B C9 4.6 . .
C2B C1B C6B C9 -2.24(6) 6 .
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C3 C1B C6B C9 166.3 . .
C4 C1B C6B C9 170.7 6 .
C5B C1B C6B C9 -6.7 . .
C2B C1B C6B C9 173.3 . .
C8 C1B C6B C9 18.2(8) 6 .
C2 C1B C6B C9 0.0 6 .
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C4 C1B C6B C3 -42(3) . 6
C2B C1B C6B C3 -49(3) 6 6
C1B C1B C6B C3 128(3) 6 6
C3 C1B C6B C3 119(3) . 6
C4 C1B C6B C3 124(3) 6 6
C5B C1B C6B C3 -54(3) . 6
C2B C1B C6B C3 126(3) . 6
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C1B C1B C6B C6B 0.0 6 6
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C4 C1B C6B C6B -3.9 6 6
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C2B C1B C6B C6B -1.4 . 6
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C7B C1B C6B C6B -177.6 6 6
C3 C1B C6B C4 42(3) 6 .
C2B C1B C6B C4 -6.82(6) 6 .
C1B C1B C6B C4 170.1 6 .
C3 C1B C6B C4 161.7 . .
C4 C1B C6B C4 166.2 6 .
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C8 C1B C6B C4 13.6(8) 6 .
C2 C1B C6B C4 -4.6 6 .
C7B C1B C6B C4 -7.5 6 .
C3 C1B C6B C7B 50(3) 6 6
C4 C1B C6B C7B 7.5 . 6
C2B C1B C6B C7B 0.7 6 6
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C4 C1B C6B C7B 173.6 6 6
C5B C1B C6B C7B -3.8 . 6
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C8 C1B C6B C7B 21.1(7) 6 6
C2 C1B C6B C7B 2.8 6 6
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C2B C1B C6B C1B -176.93(6) 6 6
C3 C1B C6B C1B -8.4 . 6
C4 C1B C6B C1B -3.9 6 6
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C2B C1B C6B C1B -1.4 . 6
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C7B C1B C6B C1B -177.6 6 6
C3 C1B C6B C2B 49(3) 6 6
C4 C1B C6B C2B 6.82(6) . 6
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C3 C1B C6B C2B 168.54(6) . 6
C4 C1B C6B C2B 173.0 6 6
C5B C1B C6B C2B -4.50(6) . 6
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C8 C1B C6B C2B 20.4(7) 6 6
C2 C1B C6B C2B 2.2 6 6
C7B C1B C6B C2B -0.7 6 6
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C3 C4 C6B C8 146.2(6) 6 6
C1B C4 C6B C8 164.8(9) . 6
C5B C4 C6B C8 -45.2(9) . 6
C2 C4 C6B C8 -41.8(16) 6 6
C7B C4 C6B C8 -24.4(9) 6 6
C1B C4 C6B C8 158.4(10) 6 6
C3 C4 C6B C8 153.0(9) . 6
C5 C4 C6B C8 -52.8(9) . 6
C9 C4 C6B C8 -20.3(9) . 6
C3B C4 C6B C8 -157.4(18) 6 6
C2B C4 C6B C9 -118(7) 6 .
C3 C4 C6B C9 166.5(3) 6 .
C1B C4 C6B C9 -174.9 . .
C5B C4 C6B C9 -25.0 . .
C2 C4 C6B C9 -21.5(7) 6 .
C7B C4 C6B C9 -4.1 6 .
C1B C4 C6B C9 178.7 6 .
C3 C4 C6B C9 173.3 . .
C5 C4 C6B C9 -32.5 . .
C8 C4 C6B C9 20.3(9) 6 .
C3B C4 C6B C9 -137.1(10) 6 .
C2B C4 C6B C1B 57(7) 6 .
C3 C4 C6B C1B -18.6(3) 6 .
C5B C4 C6B C1B 149.9 . .
C2 C4 C6B C1B 153.4(7) 6 .
C7B C4 C6B C1B 170.8 6 .
C1B C4 C6B C1B -6.4 6 .
C3 C4 C6B C1B -11.9 . .
C5 C4 C6B C1B 142.4 . .
C8 C4 C6B C1B -164.8(9) 6 .
C9 C4 C6B C1B 174.9 . .
C3B C4 C6B C1B 37.8(10) 6 .
C2B C4 C6B C3 75(8) 6 6
C1B C4 C6B C3 18.6(3) . 6
C5B C4 C6B C3 168.6(3) . 6
C2 C4 C6B C3 172.0(10) 6 6
C7B C4 C6B C3 -170.6(3) 6 6
C1B C4 C6B C3 12.2(3) 6 6
C3 C4 C6B C3 6.8(3) . 6
C5 C4 C6B C3 161.0(3) . 6
C8 C4 C6B C3 -146.2(6) 6 6
C9 C4 C6B C3 -166.5(3) . 6
C3B C4 C6B C3 56.4(12) 6 6
C2B C4 C6B C6B 66(7) 6 6
C3 C4 C6B C6B -9.1(3) 6 6
C1B C4 C6B C6B 9.5 . 6
C5B C4 C6B C6B 159.5 . 6
C2 C4 C6B C6B 162.9(7) 6 6
C7B C4 C6B C6B -179.7 6 6
C1B C4 C6B C6B 3.1 6 6
C3 C4 C6B C6B -2.3 . 6
C5 C4 C6B C6B 151.9 . 6
C8 C4 C6B C6B -155.3(9) 6 6
C9 C4 C6B C6B -175.6 . 6
C3B C4 C6B C6B 47.3(10) 6 6
C2B C4 C6B C7B -114(7) 6 6
C3 C4 C6B C7B 170.6(3) 6 6
C1B C4 C6B C7B -170.8 . 6
C5B C4 C6B C7B -20.9 . 6
C2 C4 C6B C7B -17.4(7) 6 6
C1B C4 C6B C7B -177.2 6 6
C3 C4 C6B C7B 177.4 . 6
C5 C4 C6B C7B -28.4 . 6
C8 C4 C6B C7B 24.4(9) 6 6
C9 C4 C6B C7B 4.1 . 6
C3B C4 C6B C7B -133.0(10) 6 6
C2B C4 C6B C1B 63(7) 6 6
C3 C4 C6B C1B -12.2(3) 6 6
C1B C4 C6B C1B 6.4 . 6
C5B C4 C6B C1B 156.3 . 6
C2 C4 C6B C1B 159.8(7) 6 6
C7B C4 C6B C1B 177.2 6 6
C3 C4 C6B C1B -5.4 . 6
C5 C4 C6B C1B 148.8 . 6
C8 C4 C6B C1B -158.4(10) 6 6
C9 C4 C6B C1B -178.7 . 6
C3B C4 C6B C1B 44.2(10) 6 6
C3 C4 C6B C2B -75(8) 6 6
C1B C4 C6B C2B -57(7) . 6
C5B C4 C6B C2B 93(7) . 6
C2 C4 C6B C2B 97(7) 6 6
C7B C4 C6B C2B 114(7) 6 6
C1B C4 C6B C2B -63(7) 6 6
C3 C4 C6B C2B -69(7) . 6
C5 C4 C6B C2B 86(7) . 6
C8 C4 C6B C2B 138(8) 6 6
C9 C4 C6B C2B 118(7) . 6
C3B C4 C6B C2B -19(7) 6 6
C6B C8 C7B C9 -112.5(12) 6 6
C1B C8 C7B C9 -164.8(9) 6 6
C4 C8 C7B C9 -170.3(10) 6 6
C3 C8 C7B C9 -170.8(9) . 6
C2B C8 C7B C9 -169.3(9) . 6
C6B C8 C7B C4 58(2) 6 6
C9 C8 C7B C4 170.3(10) 6 6
C1B C8 C7B C4 5.6 6 6
C3 C8 C7B C4 -0.4 . 6
C2B C8 C7B C4 1.1 . 6
C6B C8 C7B C2B 57(2) 6 .
C9 C8 C7B C2B 169.3(9) 6 .
C1B C8 C7B C2B 4.5 6 .
C4 C8 C7B C2B -1.1 6 .
C3 C8 C7B C2B -1.5 . .
C6B C8 C7B C10B 68(2) 6 6
C1B C8 C7B C10B 16.1(5) 6 6
C4 C8 C7B C10B 10.5(4) 6 6
C3 C8 C7B C10B 10.1(5) . 6
C2B C8 C7B C10B 11.6(5) . 6
C6B C8 C7B C5B 58(2) 6 6
C9 C8 C7B C5B 170.9(9) 6 6
C1B C8 C7B C5B 6.2 6 6
C4 C8 C7B C5B 0.6 6 6
C3 C8 C7B C5B 0.2 . 6
C2B C8 C7B C5B 1.6 . 6
C6B C8 C7B C3 58(2) 6 .
C9 C8 C7B C3 170.8(9) 6 .
C1B C8 C7B C3 6.0 6 .
C4 C8 C7B C3 0.4 6 .
C2B C8 C7B C3 1.5 . .
C6B C8 C7B C1B 52(2) 6 6
C9 C8 C7B C1B 164.8(9) 6 6
C4 C8 C7B C1B -5.6 6 6
C3 C8 C7B C1B -6.0 . 6
C2B C8 C7B C1B -4.5 . 6
C9 C8 C7B C6B 112.5(12) 6 6
C1B C8 C7B C6B -52(2) 6 6
C4 C8 C7B C6B -58(2) 6 6
C3 C8 C7B C6B -58(2) . 6
C2B C8 C7B C6B -57(2) . 6
C6B C8 C7B C2 62(2) 6 .
C9 C8 C7B C2 174.9(9) 6 .
C1B C8 C7B C2 10.2 6 .
C4 C8 C7B C2 4.6 6 .
C3 C8 C7B C2 4.2 . .
C2B C8 C7B C2 5.6 . .
C4 C2B C7B C9 10.4(3) 6 6
C3 C2B C7B C9 8.1 . 6
C1B C2B C7B C9 -6.11(7) 6 6
C5B C2B C7B C9 -179.3 6 6
C2 C2B C7B C9 171.8 . 6
C5 C2B C7B C9 176.8 6 6
C3B C2B C7B C9 175.8 . 6
C1B C2B C7B C9 -4.2 . 6
C3 C2B C7B C9 3.0 6 6
C2B C2B C7B C9 -1.7 6 6
C4 C2B C7B C8 6.3(4) 6 .
C3 C2B C7B C8 4.1 . .
C1B C2B C7B C8 -10.2 6 .
C5B C2B C7B C8 176.7 6 .
C2 C2B C7B C8 167.7 . .
C5 C2B C7B C8 172.8 6 .
C3B C2B C7B C8 171.8 . .
C1B C2B C7B C8 -8.2 . .
C3 C2B C7B C8 -1.0 6 .
C2B C2B C7B C8 -5.7 6 .
C9 C2B C7B C8 -4.0 6 .
C3 C2B C7B C4 -2.2(4) . 6
C1B C2B C7B C4 -16.5(4) 6 6
C5B C2B C7B C4 170.3(4) 6 6
C2 C2B C7B C4 161.4(4) . 6
C5 C2B C7B C4 166.4(4) 6 6
C3B C2B C7B C4 165.4(4) . 6
C1B C2B C7B C4 -14.6(4) . 6
C3 C2B C7B C4 -7.4(3) 6 6
C2B C2B C7B C4 -12.0(4) 6 6
C9 C2B C7B C4 -10.4(3) 6 6
C4 C2B C7B C10B -170.6(4) 6 6
C3 C2B C7B C10B -172.8 . 6
C1B C2B C7B C10B 172.9 6 6
C5B C2B C7B C10B -0.3 6 6
C2 C2B C7B C10B -9.2 . 6
C5 C2B C7B C10B -4.2 6 6
C3B C2B C7B C10B -5.2 . 6
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C9 C2B C7B C10B 179.0 6 6
C4 C2B C7B C5B -170.3(4) 6 6
C3 C2B C7B C5B -172.6 . 6
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C2 C2B C7B C5B -8.9 . 6
C5 C2B C7B C5B -3.9 6 6
C3B C2B C7B C5B -4.9 . 6
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C2B C2B C7B C5B 177.6 6 6
C9 C2B C7B C5B 179.3 6 6
C4 C2B C7B C3 2.2(4) 6 .
C1B C2B C7B C3 -14.2 6 .
C5B C2B C7B C3 172.6 6 .
C2 C2B C7B C3 163.6 . .
C5 C2B C7B C3 168.7 6 .
C3B C2B C7B C3 167.7 . .
C1B C2B C7B C3 -12.3 . .
C3 C2B C7B C3 -5.1 6 .
C2B C2B C7B C3 -9.8 6 .
C9 C2B C7B C3 -8.1 6 .
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C3 C2B C7B C1B 14.2 . 6
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C2 C2B C7B C1B 177.9 . 6
C5 C2B C7B C1B -177.07(5) 6 6
C3B C2B C7B C1B -178.1 . 6
C1B C2B C7B C1B 1.9 . 6
C3 C2B C7B C1B 9.11(7) 6 6
C2B C2B C7B C1B 4.5 6 6
C9 C2B C7B C1B 6.11(8) 6 6
C4 C2B C7B C6B 16.0(4) 6 6
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C1B C2B C7B C6B -0.5 6 6
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C3B C2B C7B C6B -178.6 . 6
C1B C2B C7B C6B 1.4 . 6
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C2B C2B C7B C6B 3.9 6 6
C9 C2B C7B C6B 5.60(6) 6 6
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C3 C2B C7B C2 -163.6 . .
C1B C2B C7B C2 -177.9 6 .
C5B C2B C7B C2 8.9 6 .
C5 C2B C7B C2 5.1 6 .
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C9 C2B C7B C2 -171.8 6 .
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C5B C3 C7B C9 -176.77(14) 6 6
C4 C3 C7B C9 -28.60(11) . 6
C2 C3 C7B C9 177.74(10) . 6
C2B C3 C7B C9 -100.9(10) 6 6
C8 C3 C7B C9 3.44(10) . 6
C6B C3 C7B C9 -7.91(9) 6 6
C1B C3 C7B C8 -55.4(6) 6 .
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C2B C3 C7B C8 -175.4 . .
C1B C3 C7B C8 -33.4 . .
C3 C3 C7B C8 -16.3 6 .
C5B C3 C7B C8 179.8 6 .
C4 C3 C7B C8 -32.0 . .
C2 C3 C7B C8 174.3 . .
C2B C3 C7B C8 -104.4(9) 6 .
C6B C3 C7B C8 -11.4 6 .
C1B C3 C7B C4 122.2(4) 6 6
C2B C3 C7B C4 2.2(3) . 6
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C3 C3 C7B C4 161.3(3) 6 6
C5B C3 C7B C4 -2.6(2) 6 6
C4 C3 C7B C4 145.5(3) . 6
C2 C3 C7B C4 -8.1(3) . 6
C2B C3 C7B C4 73.2(8) 6 6
C8 C3 C7B C4 177.6(3) . 6
C6B C3 C7B C4 166.2(3) 6 6
C1B C3 C7B C2B 120.0(6) 6 .
C4 C3 C7B C2B -2.2(3) 6 .
C1B C3 C7B C2B 142.0 . .
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C5B C3 C7B C2B -4.8 6 .
C4 C3 C7B C2B 143.4 . .
C2 C3 C7B C2B -10.3 . .
C2B C3 C7B C2B 71.1(9) 6 .
C8 C3 C7B C2B 175.4 . .
C6B C3 C7B C2B 164.1 6 .
C1B C3 C7B C10B 127.3(6) 6 6
C4 C3 C7B C10B 5.1(2) 6 6
C2B C3 C7B C10B 7.3 . 6
C1B C3 C7B C10B 149.3 . 6
C3 C3 C7B C10B 166.4 6 6
C5B C3 C7B C10B 2.5 6 6
C4 C3 C7B C10B 150.69(5) . 6
C2 C3 C7B C10B -3.0 . 6
C2B C3 C7B C10B 78.4(9) 6 6
C8 C3 C7B C10B -177.3 . 6
C6B C3 C7B C10B 171.37(5) 6 6
C1B C3 C7B C5B 124.8(6) 6 6
C4 C3 C7B C5B 2.6(2) 6 6
C2B C3 C7B C5B 4.8 . 6
C1B C3 C7B C5B 146.8 . 6
C3 C3 C7B C5B 163.9 6 6
C4 C3 C7B C5B 148.2 . 6
C2 C3 C7B C5B -5.5 . 6
C2B C3 C7B C5B 75.8(9) 6 6
C8 C3 C7B C5B -179.8 . 6
C6B C3 C7B C5B 168.9 6 6
C4 C3 C7B C1B -122.2(4) 6 6
C2B C3 C7B C1B -120.0(6) . 6
C1B C3 C7B C1B 22.0(6) . 6
C3 C3 C7B C1B 39.1(6) 6 6
C5B C3 C7B C1B -124.8(6) 6 6
C4 C3 C7B C1B 23.4(6) . 6
C2 C3 C7B C1B -130.3(6) . 6
C2B C3 C7B C1B -49.0(6) 6 6
C8 C3 C7B C1B 55.4(6) . 6
C6B C3 C7B C1B 44.0(7) 6 6
C1B C3 C7B C6B -44.0(7) 6 6
C4 C3 C7B C6B -166.2(3) 6 6
C2B C3 C7B C6B -164.1 . 6
C1B C3 C7B C6B -22.0 . 6
C3 C3 C7B C6B -5.0 6 6
C5B C3 C7B C6B -168.9 6 6
C4 C3 C7B C6B -20.7 . 6
C2 C3 C7B C6B -174.3 . 6
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C8 C3 C7B C6B 11.4 . 6
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C5B C3 C7B C2 5.5 6 .
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C4 C2 C7B C5B 111(4) 6 6
C3 C2 C7B C5B 113(4) . 6
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C1 C2 C7B C3 -14.3 . .
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C5 C7 C8B C9B 2.76(6) 6 6
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C10B C7 C8B C3B 60(3) 6 .
C5 C7 C8B C3B 1.9 6 .
C5B C7 C8B C3B 4.5 6 .
C2 C7 C8B C3B -1.4 . .
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C5 C7 C8B C4B 1.7 6 6
C5B C7 C8B C4B 4.3 6 6
C2 C7 C8B C4B -1.6 . 6
C3B C7 C8B C4B -0.2 . 6
C10 C7 C8B C2 147.6(11) 6 .
C10B C7 C8B C2 61(3) 6 .
C5 C7 C8B C2 3.3 6 .
C5B C7 C8B C2 5.9 6 .
C3B C7 C8B C2 1.4 . .
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C5B C3B C8B C10 4.0 6 6
C2B C3B C8B C10 7.87(5) . 6
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C4 C3B C8B C10 10.14(7) 6 6
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C2 C3B C8B C7 3.5 . .
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C5B C3B C8B C7 -6.6 6 .
C2B C3B C8B C7 -2.8 . .
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C7 C3B C8B C4B 179.2 . 6
C9B C3B C8B C4B -1.0 6 6
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C5 C3B C8B C2 -8.7 6 .
C1 C3B C8B C2 172.4 . .
C5B C3B C8B C2 -10.1 6 .
C2B C3B C8B C2 -6.3 . .
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C4 C3B C8B C2 -4.0 6 .
C7 C3B C8B C2 -3.5 . .
C9B C3B C8B C2 176.2 6 .
C4B C3B C8B C5B -172.6 6 6
C5 C3B C8B C5B 1.4 6 6
C2 C3B C8B C5B 10.1 . 6
C1 C3B C8B C5B -177.5 . 6
C2B C3B C8B C5B 3.8 . 6
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C10 C2 C8B C5 97(4) 6 6
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C4B C2 C8B C3B -1.3 6 .
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C10 C2 C8B C3B 165.53(11) 6 .
C5 C2 C8B C4B 70(4) 6 6
C5B C2 C8B C4B 155.3(4) 6 6
C3B C2 C8B C4B 1.3 . 6
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C10 C2 C8B C4B 166.85(9) 6 6
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C9B C6 C9B C4B -3.1 6 .
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C2 C1 C9B C6 9.1 . .
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C6 C1 C9B C6 -0.1 6 .
C9B C1 C9B C6 0.3 6 .
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C3B C1 C9B C4B 173.1 . .
C3B C1 C9B C4B -3.2 6 .
C5 C1 C9B C4B -2.8 . .
C5 C1 C9B C4B 171.44(5) 6 .
C2 C1 C9B C4B -175.4 . .
C2 C1 C9B C4B -5.7 6 .
C6 C1 C9B C4B 175.4 6 .
C6 C1 C9B C4B 175.5 . .
C9B C1 C9B C4B 175.8 6 .
C4B C1 C9B C3B 173.7 6 6
C4B C1 C9B C3B 3.2 . 6
C3B C1 C9B C3B 176.3 . 6
C5 C1 C9B C3B 0.5 . 6
C5 C1 C9B C3B 174.68(5) 6 6
C2 C1 C9B C3B -172.2 . 6
C2 C1 C9B C3B -2.5 6 6
C6 C1 C9B C3B 178.6 6 6
C6 C1 C9B C3B 178.7 . 6
C9B C1 C9B C3B 179.0 6 6
C8B C10 C10B C7 48(3) 6 6
C5 C10 C10B C7 56(3) . 6
C5B C10 C10B C7 58(3) . 6
C2 C10 C10B C7 54(3) 6 6
C3B C10 C10B C7 57(3) 6 6
C7 C10 C10B C5B -58(3) 6 .
C8B C10 C10B C5B -10.0(2) 6 .
C5 C10 C10B C5B -1.4 . .
C2 C10 C10B C5B -4.0 6 .
C3B C10 C10B C5B -1.1 6 .
C7 C10 C10B C7B -51(3) 6 6
C8B C10 C10B C7B -3.6(2) 6 6
C5 C10 C10B C7B 5.01(14) . 6
C5B C10 C10B C7B 6.42(14) . 6
C2 C10 C10B C7B 2.38(11) 6 6
C3B C10 C10B C7B 5.30(13) 6 6
C7 C10 C10B C5 -56(3) 6 .
C8B C10 C10B C5 -8.6(2) 6 .
C5B C10 C10B C5 1.4 . .
C2 C10 C10B C5 -2.6 6 .
C3B C10 C10B C5 0.3 6 .
C7 C10 C10B C2 -54(3) 6 6
C8B C10 C10B C2 -6.0(2) 6 6
C5 C10 C10B C2 2.6 . 6
C5B C10 C10B C2 4.0 . 6
C3B C10 C10B C2 2.9 6 6
C7 C10 C10B C8B -48(3) 6 6
C5 C10 C10B C8B 8.6(2) . 6
C5B C10 C10B C8B 10.0(2) . 6
C2 C10 C10B C8B 6.0(2) 6 6
C3B C10 C10B C8B 8.9(2) 6 6
C2 C5B C10B C7 6.3 6 6
C5 C5B C10B C7 -10.4 . 6
C2B C5B C10B C7 161.5 6 6
C3B C5B C10B C7 -11.8 6 6
C4 C5B C10B C7 159.1 . 6
C3 C5B C10B C7 157.8 6 6
C4B C5B C10B C7 -14.6 . 6
C1B C5B C10B C7 165.4 . 6
C7B C5B C10B C7 161.2 6 6
C10 C5B C10B C7 -14.4 . 6
C2 C5B C10B C10 20.7 6 .
C5 C5B C10B C10 4.0 . .
C2B C5B C10B C10 175.9 6 .
C3B C5B C10B C10 2.6 6 .
C4 C5B C10B C10 173.5 . .
C3 C5B C10B C10 172.2 6 .
C4B C5B C10B C10 -0.2 . .
C1B C5B C10B C10 179.8 . .
C7 C5B C10B C10 14.4 6 .
C7B C5B C10B C10 175.5 6 .
C2 C5B C10B C7B -154.8 6 6
C5 C5B C10B C7B -171.5 . 6
C2B C5B C10B C7B 0.4 6 6
C3B C5B C10B C7B -172.9 6 6
C4 C5B C10B C7B -2.0 . 6
C3 C5B C10B C7B -3.4 6 6
C4B C5B C10B C7B -175.7 . 6
C1B C5B C10B C7B 4.3 . 6
C7 C5B C10B C7B -161.2 6 6
C10 C5B C10B C7B -175.5 . 6
C2 C5B C10B C5 16.7 6 .
C2B C5B C10B C5 171.9 6 .
C3B C5B C10B C5 -1.4 6 .
C4 C5B C10B C5 169.5 . .
C3 C5B C10B C5 168.2 6 .
C4B C5B C10B C5 -4.2 . .
C1B C5B C10B C5 175.8 . .
C7 C5B C10B C5 10.4 6 .
C7B C5B C10B C5 171.5 6 .
C10 C5B C10B C5 -4.0 . .
C5 C5B C10B C2 -16.7 . 6
C2B C5B C10B C2 155.2 6 6
C3B C5B C10B C2 -18.1 6 6
C4 C5B C10B C2 152.8 . 6
C3 C5B C10B C2 151.5 6 6
C4B C5B C10B C2 -20.9 . 6
C1B C5B C10B C2 159.1 . 6
C7 C5B C10B C2 -6.3 6 6
C7B C5B C10B C2 154.8 6 6
C10 C5B C10B C2 -20.7 . 6
C2 C5B C10B C8B 17.9 6 6
C5 C5B C10B C8B 1.2 . 6
C2B C5B C10B C8B 173.1 6 6
C3B C5B C10B C8B -0.2 6 6
C4 C5B C10B C8B 170.7 . 6
C3 C5B C10B C8B 169.3 6 6
C4B C5B C10B C8B -3.1 . 6
C1B C5B C10B C8B 176.9 . 6
C7 C5B C10B C8B 11.5 6 6
C7B C5B C10B C8B 172.7 6 6
C10 C5B C10B C8B -2.8 . 6
C2 C5 C10B C7 145.5(2) 6 6
C3B C5 C10B C7 -21.3(2) 6 6
C5B C5 C10B C7 167.57(7) . 6
C4B C5 C10B C7 -24.77(7) . 6
C2B C5 C10B C7 163.30(6) 6 6
C1 C5 C10B C7 -27.04(7) . 6
C4 C5 C10B C7 161.01(7) . 6
C8B C5 C10B C7 -13.89(8) 6 6
C10 C5 C10B C7 -16.98(7) . 6
C3 C5 C10B C7 160.21(6) 6 6
C2 C5 C10B C10 162.5(3) 6 .
C3B C5 C10B C10 -4.31(16) 6 .
C5B C5 C10B C10 -175.4 . .
C4B C5 C10B C10 -7.8 . .
C2B C5 C10B C10 -179.7 6 .
C7 C5 C10B C10 16.98(7) 6 .
C1 C5 C10B C10 -10.1 . .
C4 C5 C10B C10 178.0 . .
C8B C5 C10B C10 3.1 6 .
C3 C5 C10B C10 177.2 6 .
C2 C5 C10B C5B -22.0(3) 6 .
C3B C5 C10B C5B 171.14(16) 6 .
C4B C5 C10B C5B 167.7 . .
C2B C5 C10B C5B -4.3 6 .
C7 C5 C10B C5B -167.57(7) 6 .
C1 C5 C10B C5B 165.4 . .
C4 C5 C10B C5B -6.6 . .
C8B C5 C10B C5B 178.5 6 .
C10 C5 C10B C5B 175.4 . .
C3 C5 C10B C5B -7.4 6 .
C2 C5 C10B C7B -14.3(2) 6 6
C5B C5 C10B C7B 7.7 . 6
C4B C5 C10B C7B 175.4 . 6
C2B C5 C10B C7B 3.5 6 6
C7 C5 C10B C7B -159.8 6 6
C1 C5 C10B C7B 173.1 . 6
C4 C5 C10B C7B 1.2 . 6
C8B C5 C10B C7B -173.72(5) 6 6
C10 C5 C10B C7B -176.8 . 6
C3 C5 C10B C7B 0.4 6 6
C3B C5 C10B C2 -166.8(4) 6 6
C5B C5 C10B C2 22.0(3) . 6
C4B C5 C10B C2 -170.3(3) . 6
C2B C5 C10B C2 17.8(2) 6 6
C7 C5 C10B C2 -145.5(2) 6 6
C1 C5 C10B C2 -172.6(2) . 6
C4 C5 C10B C2 15.5(3) . 6
C8B C5 C10B C2 -159.4(3) 6 6
C10 C5 C10B C2 -162.5(3) . 6
C3 C5 C10B C2 14.7(2) 6 6
C2 C5 C10B C8B 159.4(3) 6 6
C3B C5 C10B C8B -7.40(15) 6 6
C5B C5 C10B C8B -178.5 . 6
C4B C5 C10B C8B -10.9 . 6
C2B C5 C10B C8B 177.2 6 6
C7 C5 C10B C8B 13.89(8) 6 6
C1 C5 C10B C8B -13.2 . 6
C4 C5 C10B C8B 174.9 . 6
C10 C5 C10B C8B -3.1 . 6
C3 C5 C10B C8B 174.1 6 6
C17 P1 C11 C12 -130.0(4) . .
C11 P1 C11 C12 119.9(3) 6 .
Ru1 P1 C11 C12 1.5(4) . .
C17 P1 C11 C16 45.6(4) . .
C11 P1 C11 C16 -64.5(5) 6 .
Ru1 P1 C11 C16 177.1(3) . .
C16 C11 C12 C13 -2.9(6) . .
P1 C11 C12 C13 172.9(3) . .
C16 C11 C12 S1 176.7(3) . .
P1 C11 C12 S1 -7.6(5) . .
Ru1 S1 C12 C11 9.9(4) . .
Ru2 S1 C12 C11 -62.5(4) . .
Ru1 S1 C12 C13 -170.6(3) . .
Ru2 S1 C12 C13 117.0(3) . .
C11 C12 C13 C14 3.0(7) . .
S1 C12 C13 C14 -176.5(4) . .
C12 C13 C14 C15 -0.7(8) . .
C13 C14 C15 C16 -1.7(8) . .
C14 C15 C16 C11 1.8(7) . .
C12 C11 C16 C15 0.4(7) . .
P1 C11 C16 C15 -175.0(4) . .
C11 P1 C17 C18 35.0(6) . .
C11 P1 C17 C18 148.4(6) 6 .
Ru1 P1 C17 C18 -88.3(6) . .
C11 P1 C17 C18 -148.4(6) . 6
C11 P1 C17 C18 -35.0(6) 6 6
Ru1 P1 C17 C18 88.3(6) . 6
C18 C17 C18 C19 1.5(13) 6 .
P1 C17 C18 C19 178.2(6) . .
C17 C18 C19 C20 -0.9(15) . .
C18 C19 C20 C19 0(2) . 6
C23 Ru2 C21 C22 80.1(3) 6 .
C23 Ru2 C21 C22 36.7(3) . .
C22 Ru2 C21 C22 116.8(6) 6 .
S1 Ru2 C21 C22 169.5(2) 6 .
S1 Ru2 C21 C22 -52.7(4) . .
Ru1 Ru2 C21 C22 -121.6(3) . .
C23 Ru2 C21 C22 -36.7(3) 6 6
C23 Ru2 C21 C22 -80.1(3) . 6
C22 Ru2 C21 C22 -116.8(6) . 6
S1 Ru2 C21 C22 52.7(4) 6 6
S1 Ru2 C21 C22 -169.5(2) . 6
Ru1 Ru2 C21 C22 121.6(3) . 6
C23 Ru2 C21 C24 -158.28(14) 6 .
C23 Ru2 C21 C24 158.28(14) . .
C22 Ru2 C21 C24 121.6(3) . .
C22 Ru2 C21 C24 -121.6(3) 6 .
S1 Ru2 C21 C24 -68.91(10) 6 .
S1 Ru2 C21 C24 68.91(10) . .
Ru1 Ru2 C21 C24 0.000(2) . .
C22 C21 C22 C23 3.5(7) 6 .
C24 C21 C22 C23 -178.4(6) . .
Ru2 C21 C22 C23 -59.2(3) . .
C22 C21 C22 C25 -171.2(3) 6 .
C24 C21 C22 C25 6.8(10) . .
Ru2 C21 C22 C25 126.0(5) . .
C22 C21 C22 Ru2 62.8(4) 6 .
C24 C21 C22 Ru2 -119.2(7) . .
C23 Ru2 C22 C23 38.5(3) 6 .
C21 Ru2 C22 C23 118.6(4) . .
C22 Ru2 C22 C23 80.7(3) 6 .
S1 Ru2 C22 C23 95.9(4) 6 .
S1 Ru2 C22 C23 -105.5(3) . .
Ru1 Ru2 C22 C23 -107.0(3) . .
C23 Ru2 C22 C21 -80.1(3) 6 .
C23 Ru2 C22 C21 -118.6(4) . .
C22 Ru2 C22 C21 -37.9(3) 6 .
S1 Ru2 C22 C21 -22.7(5) 6 .
S1 Ru2 C22 C21 135.9(3) . .
Ru1 Ru2 C22 C21 134.4(3) . .
C23 Ru2 C22 C25 160.0(7) 6 .
C23 Ru2 C22 C25 121.5(7) . .
C21 Ru2 C22 C25 -119.9(7) . .
C22 Ru2 C22 C25 -157.8(5) 6 .
S1 Ru2 C22 C25 -142.6(5) 6 .
S1 Ru2 C22 C25 16.0(6) . .
Ru1 Ru2 C22 C25 14.5(8) . .
C21 C22 C23 C23 -2.2(4) . 6
C25 C22 C23 C23 172.4(4) . 6
Ru2 C22 C23 C23 -62.45(13) . 6
C21 C22 C23 C26 -178.3(5) . .
C25 C22 C23 C26 -3.7(8) . .
Ru2 C22 C23 C26 121.4(5) . .
C21 C22 C23 Ru2 60.3(4) . .
C25 C22 C23 Ru2 -125.1(5) . .
C23 Ru2 C23 C22 -117.0(3) 6 .
C21 Ru2 C23 C22 -37.0(3) . .
C22 Ru2 C23 C22 -79.6(4) 6 .
S1 Ru2 C23 C22 -141.9(3) 6 .
S1 Ru2 C23 C22 79.6(3) . .
Ru1 Ru2 C23 C22 128.2(3) . .
C21 Ru2 C23 C23 79.91(11) . 6
C22 Ru2 C23 C23 117.0(3) . 6
C22 Ru2 C23 C23 37.37(19) 6 6
S1 Ru2 C23 C23 -24.90(11) 6 6
S1 Ru2 C23 C23 -163.41(8) . 6
Ru1 Ru2 C23 C23 -114.87(18) . 6
C23 Ru2 C23 C26 120.0(5) 6 .
C21 Ru2 C23 C26 -160.1(5) . .
C22 Ru2 C23 C26 -123.1(6) . .
C22 Ru2 C23 C26 157.3(6) 6 .
S1 Ru2 C23 C26 95.1(5) 6 .
S1 Ru2 C23 C26 -43.4(5) . .
Ru1 Ru2 C23 C26 5.1(6) . .
O1 S2 C27 F1 60.5(2) 6_565 .
O1 S2 C27 F1 -60.5(2) . .
O2 S2 C27 F1 180.000(1) . .
O1 S2 C27 F2 -59.6(5) 6_565 6_565
O1 S2 C27 F2 179.4(4) . 6_565
O2 S2 C27 F2 59.9(4) . 6_565
O1 S2 C27 F2 -179.4(4) 6_565 .
O1 S2 C27 F2 59.6(5) . .
O2 S2 C27 F2 -59.9(4) . .
C29 Cl1 C29 Cl1 0.000(6) 5_665 5_665
O3 S3 C28 F4 108.944(1) . 6
O4 S3 C28 F4 -136.288(2) . 6
O4 S3 C28 F4 -5.825(1) 6 6
O3 S3 C28 F4 -108.944(1) . .
O4 S3 C28 F4 5.825(2) . .
O4 S3 C28 F4 136.288(2) 6 .
O3 S3 C28 F3 0.0 . .
O4 S3 C28 F3 114.769(1) . .
O4 S3 C28 F3 -114.769(1) 6 .
