#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/10/4071018.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4071018
loop_
_publ_author_name
'Mothes, Emmanuelle'
'Sentets, Stephane'
'Luquin, Maria Asuncion'
'Mathieu, René'
'Lugan, Noël'
'Lavigne, Guy'
_publ_section_title
;
 New Insight into the Reactivity of Pyridine-Functionalized Phosphine
 Complexes of Ruthenium(II) with Respect to Olefin Metathesis and Transfer
 Hydrogenation
;
_journal_issue                   6
_journal_name_full               Organometallics
_journal_page_first              1193
_journal_paper_doi               10.1021/om7012106
_journal_volume                  27
_journal_year                    2008
_chemical_compound_source        'synthesis as described'
_chemical_formula_moiety         'C72 H60 Cl4 P4 Ru2, C H2 Cl2 '
_chemical_formula_sum            'C73 H62 Cl6 P4 Ru2'
_chemical_formula_weight         1477.95
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_Int_Tables_number      2
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_date             2006-09-26T15:23:59-00:00
_audit_creation_method           'WinGX routine CIF_UPDATE'
_cell_angle_alpha                96.96(3)
_cell_angle_beta                 91.14(2)
_cell_angle_gamma                109.87(3)
_cell_formula_units_Z            1
_cell_length_a                   10.793(1)
_cell_length_b                   12.856(2)
_cell_length_c                   13.174(3)
_cell_measurement_reflns_used    9999
_cell_measurement_temperature    180(2)
_cell_measurement_theta_max      26.18
_cell_measurement_theta_min      2.01
_cell_measurement_wavelength     0.71073
_cell_volume                     1702.8(6)
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  'WinGX publication routines (Farrugia, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      180(2)
_diffrn_measured_fraction_theta_full 0.918
_diffrn_measured_fraction_theta_max 0.918
_diffrn_measurement_device_type  'Stoe IPDS'
_diffrn_measurement_method       φ
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_probe          x-ray
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0577
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       15
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            6254
_diffrn_reflns_theta_full        26.18
_diffrn_reflns_theta_max         26.18
_diffrn_reflns_theta_min         2.01
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 0
_diffrn_standards_interval_time  0
_diffrn_standards_number         0
_exptl_absorpt_coefficient_mu    0.814
_exptl_absorpt_correction_T_max  0.964
_exptl_absorpt_correction_T_min  0.898
_exptl_absorpt_correction_type   refdelf
_exptl_absorpt_process_details
;
        Parkin S,Moezzi B & Hope H, (1995) J. Appl. Cryst. 28, 53-56
        Cubic fit to sin(theta)/lambda - 24 parameters
;
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.439
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             750
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.05
_exptl_crystal_size_min          0.05
_refine_diff_density_max         1.846
_refine_diff_density_min         -0.938
_refine_diff_density_rms         0.149
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.046
_refine_ls_hydrogen_treatment    riding
_refine_ls_matrix_type           full
_refine_ls_number_parameters     424
_refine_ls_number_reflns         6246
_refine_ls_number_restraints     42
_refine_ls_restrained_S_all      1.057
_refine_ls_R_factor_all          0.0729
_refine_ls_R_factor_gt           0.0623
_refine_ls_shift/su_max          0
_refine_ls_shift/su_mean         0
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1328P)²+1.0550P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1691
_refine_ls_wR_factor_ref         0.1801
_reflns_number_gt                5206
_reflns_number_total             6254
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om7012106-file002.cif
_cod_data_source_block           complex_1
_cod_original_formula_sum        'C73 H62 Cl6 P4 Ru2 '
_cod_database_code               4071018
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
C1 C 0.2191(9) 0.2948(11) 0.3207(3) 0.035(3) Uani 0.33 1 d PDU A 1
H1 H 0.2537 0.2456 0.2779 0.042 Uiso 0.33 1 calc PR A 1
H2 H 0.1852 0.3353 0.2763 0.042 Uiso 0.33 1 calc PR A 1
Cl3 Cl 0.3448(3) 0.3882(3) 0.4023(3) 0.0335(8) Uani 0.33 1 d PDU A 1
Cl4 Cl 0.0922(4) 0.2162(4) 0.3862(4) 0.0611(14) Uani 0.33 1 d PDU A 1
C2 C 0.181(3) 0.2304(13) 0.3268(4) 0.020(5) Uani 0.17 1 d PDU B 2
H3 H 0.2657 0.2390 0.2981 0.024 Uiso 0.17 1 calc PR B 2
H4 H 0.1157 0.1648 0.2889 0.024 Uiso 0.17 1 calc PR B 2
Cl5 Cl 0.1912(8) 0.2112(6) 0.4533(4) 0.0327(15) Uani 0.17 1 d PDU B 2
Cl6 Cl 0.1396(7) 0.3459(4) 0.3128(4) 0.0253(13) Uani 0.17 1 d PDU B 2
C11 C 0.8917(5) 0.2537(5) 0.0583(4) 0.0322(11) Uani 1 1 d . . .
C12 C 0.9168(5) 0.1701(5) 0.1029(4) 0.0334(11) Uani 1 1 d . . .
H12 H 0.8600 0.1335 0.1496 0.040 Uiso 1 1 calc R . .
C13 C 1.0259(6) 0.1403(6) 0.0784(5) 0.0445(14) Uani 1 1 d . . .
H13 H 1.0419 0.0845 0.1095 0.053 Uiso 1 1 calc R . .
C14 C 1.1103(6) 0.1923(6) 0.0091(5) 0.0489(15) Uani 1 1 d . . .
H14 H 1.1819 0.1707 -0.0085 0.059 Uiso 1 1 calc R . .
C15 C 1.0868(6) 0.2789(6) -0.0350(5) 0.0495(16) Uani 1 1 d . . .
H15 H 1.1443 0.3160 -0.0811 0.059 Uiso 1 1 calc R . .
C16 C 0.9787(6) 0.3087(5) -0.0102(4) 0.0390(13) Uani 1 1 d . . .
H16 H 0.9638 0.3661 -0.0396 0.047 Uiso 1 1 calc R . .
C21 C 0.7045(5) 0.3436(4) -0.0262(4) 0.0288(10) Uani 1 1 d . . .
C22 C 0.7030(6) 0.2866(5) -0.1230(4) 0.0366(12) Uani 1 1 d . . .
H22 H 0.7250 0.2223 -0.1304 0.044 Uiso 1 1 calc R . .
C23 C 0.6683(6) 0.3263(5) -0.2087(4) 0.0452(14) Uani 1 1 d . . .
H23 H 0.6677 0.2886 -0.2737 0.054 Uiso 1 1 calc R . .
C24 C 0.6348(7) 0.4213(5) -0.1984(5) 0.0478(15) Uani 1 1 d . . .
H24 H 0.6113 0.4470 -0.2562 0.057 Uiso 1 1 calc R . .
C25 C 0.6361(7) 0.4778(5) -0.1032(5) 0.0474(15) Uani 1 1 d . . .
H25 H 0.6139 0.5421 -0.0964 0.057 Uiso 1 1 calc R . .
C26 C 0.6707(7) 0.4388(5) -0.0165(4) 0.0425(13) Uani 1 1 d . . .
H26 H 0.6712 0.4770 0.0482 0.051 Uiso 1 1 calc R . .
C31 C 0.8016(5) 0.4099(4) 0.1851(4) 0.0289(10) Uani 1 1 d . . .
C32 C 0.9335(6) 0.4721(5) 0.2026(4) 0.0356(12) Uani 1 1 d . . .
H32 H 0.9949 0.4508 0.1647 0.043 Uiso 1 1 calc R . .
C33 C 0.9768(6) 0.5662(5) 0.2760(4) 0.0419(13) Uani 1 1 d . . .
H33 H 1.0664 0.6075 0.2870 0.050 Uiso 1 1 calc R . .
C34 C 0.8855(7) 0.5988(5) 0.3332(4) 0.0436(14) Uani 1 1 d . . .
H34 H 0.9134 0.6612 0.3830 0.052 Uiso 1 1 calc R . .
C35 C 0.7531(6) 0.5368(5) 0.3145(4) 0.0398(13) Uani 1 1 d . . .
H35 H 0.6921 0.5593 0.3516 0.048 Uiso 1 1 calc R . .
C36 C 0.7076(6) 0.4417(5) 0.2422(4) 0.0374(12) Uani 1 1 d . . .
H36 H 0.6180 0.4002 0.2318 0.045 Uiso 1 1 calc R . .
C41 C 0.4117(5) 0.0150(4) 0.2885(4) 0.0273(10) Uani 1 1 d . . .
C42 C 0.4092(6) -0.0489(5) 0.3685(4) 0.0354(12) Uani 1 1 d . . .
H42 H 0.4875 -0.0525 0.3959 0.042 Uiso 1 1 calc R . .
C43 C 0.2912(6) -0.1058(5) 0.4061(4) 0.0413(13) Uani 1 1 d . . .
H43 H 0.2906 -0.1472 0.4594 0.050 Uiso 1 1 calc R . .
C44 C 0.1747(6) -0.1029(5) 0.3668(5) 0.0446(14) Uani 1 1 d . . .
H44 H 0.0955 -0.1424 0.3928 0.054 Uiso 1 1 calc R . .
C45 C 0.1755(6) -0.0400(6) 0.2871(5) 0.0451(14) Uani 1 1 d . . .
H45 H 0.0964 -0.0378 0.2598 0.054 Uiso 1 1 calc R . .
C46 C 0.2923(5) 0.0183(5) 0.2492(4) 0.0344(11) Uani 1 1 d . . .
H46 H 0.2920 0.0606 0.1968 0.041 Uiso 1 1 calc R . .
C51 C 0.6602(5) -0.0047(4) 0.2555(4) 0.0306(10) Uani 1 1 d . . .
C52 C 0.6184(6) -0.1038(5) 0.1901(4) 0.0381(12) Uani 1 1 d . . .
H52 H 0.5512 -0.1163 0.1399 0.046 Uiso 1 1 calc R . .
C53 C 0.6742(7) -0.1855(5) 0.1973(5) 0.0496(16) Uani 1 1 d . . .
H53 H 0.6434 -0.2525 0.1533 0.060 Uiso 1 1 calc R . .
C54 C 0.7742(9) -0.1668(6) 0.2694(7) 0.063(2) Uani 1 1 d . . .
H54 H 0.8141 -0.2202 0.2729 0.076 Uiso 1 1 calc R . .
C55 C 0.8165(8) -0.0702(7) 0.3365(6) 0.0585(18) Uani 1 1 d . . .
H55 H 0.8832 -0.0592 0.3867 0.070 Uiso 1 1 calc R . .
C56 C 0.7608(6) 0.0114(5) 0.3303(5) 0.0433(13) Uani 1 1 d . . .
H56 H 0.7904 0.0771 0.3761 0.052 Uiso 1 1 calc R . .
C61 C 0.6424(5) 0.2052(4) 0.3456(3) 0.0305(11) Uani 1 1 d . . .
C62 C 0.7773(6) 0.2639(5) 0.3599(4) 0.0358(12) Uani 1 1 d . . .
H62 H 0.8332 0.2467 0.3131 0.043 Uiso 1 1 calc R . .
C63 C 0.8309(7) 0.3470(5) 0.4415(4) 0.0442(14) Uani 1 1 d . . .
H63 H 0.9219 0.3819 0.4513 0.053 Uiso 1 1 calc R . .
C64 C 0.7501(8) 0.3778(5) 0.5078(5) 0.0519(17) Uani 1 1 d . . .
H64 H 0.7858 0.4356 0.5613 0.062 Uiso 1 1 calc R . .
C65 C 0.6139(7) 0.3226(5) 0.4951(4) 0.0485(15) Uani 1 1 d . . .
H65 H 0.5592 0.3430 0.5410 0.058 Uiso 1 1 calc R . .
C66 C 0.5594(6) 0.2376(5) 0.4147(4) 0.0370(12) Uani 1 1 d . . .
H66 H 0.4683 0.2019 0.4062 0.044 Uiso 1 1 calc R . .
Cl1 Cl 0.42527(13) 0.24903(10) 0.13014(10) 0.0336(3) Uani 1 1 d . . .
Cl2 Cl 0.64801(11) 0.01694(10) -0.01483(9) 0.0313(3) Uani 1 1 d . . .
P1 P 0.74219(12) 0.28590(10) 0.08767(9) 0.0253(3) Uani 1 1 d . . .
P2 P 0.57187(12) 0.09286(10) 0.24020(9) 0.0244(3) Uani 1 1 d . . .
Ru1 Ru 0.55465(4) 0.13655(3) 0.08506(3) 0.02290(16) Uani 1 1 d . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0 0 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
Cl3 C1 Cl4 112.00(11) .
Cl3 C1 H1 109.2 .
Cl4 C1 H1 109.2 .
Cl3 C1 H2 109.2 .
Cl4 C1 H2 109.2 .
H1 C1 H2 107.9 .
Cl6 C2 Cl5 111.95(11) .
Cl6 C2 H3 109.2 .
Cl5 C2 H3 109.2 .
Cl6 C2 H4 109.2 .
Cl5 C2 H4 109.2 .
H3 C2 H4 107.9 .
C12 C11 C16 119.0(5) .
C12 C11 P1 119.3(4) .
C16 C11 P1 121.6(4) .
C11 C12 C13 120.6(5) .
C11 C12 H12 119.7 .
C13 C12 H12 119.7 .
C14 C13 C12 120.8(6) .
C14 C13 H13 119.6 .
C12 C13 H13 119.6 .
C13 C14 C15 118.9(6) .
C13 C14 H14 120.5 .
C15 C14 H14 120.5 .
C16 C15 C14 120.2(6) .
C16 C15 H15 119.9 .
C14 C15 H15 119.9 .
C15 C16 C11 120.4(6) .
C15 C16 H16 119.8 .
C11 C16 H16 119.8 .
C26 C21 C22 119.5(5) .
C26 C21 P1 121.2(4) .
C22 C21 P1 119.2(4) .
C21 C22 C23 119.6(6) .
C21 C22 H22 120.2 .
C23 C22 H22 120.2 .
C24 C23 C22 120.6(6) .
C24 C23 H23 119.7 .
C22 C23 H23 119.7 .
C25 C24 C23 120.2(6) .
C25 C24 H24 119.9 .
C23 C24 H24 119.9 .
C24 C25 C26 119.8(6) .
C24 C25 H25 120.1 .
C26 C25 H25 120.1 .
C21 C26 C25 120.4(6) .
C21 C26 H26 119.8 .
C25 C26 H26 119.8 .
C32 C31 C36 119.9(5) .
C32 C31 P1 121.8(4) .
C36 C31 P1 118.3(4) .
C31 C32 C33 121.0(5) .
C31 C32 H32 119.5 .
C33 C32 H32 119.5 .
C32 C33 C34 119.9(5) .
C32 C33 H33 120.0 .
C34 C33 H33 120.0 .
C35 C34 C33 118.8(5) .
C35 C34 H34 120.6 .
C33 C34 H34 120.6 .
C34 C35 C36 122.4(6) .
C34 C35 H35 118.8 .
C36 C35 H35 118.8 .
C35 C36 C31 118.0(5) .
C35 C36 H36 121.0 .
C31 C36 H36 121.0 .
C46 C41 C42 118.4(5) .
C46 C41 P2 122.2(4) .
C42 C41 P2 119.4(4) .
C43 C42 C41 119.9(6) .
C43 C42 H42 120.0 .
C41 C42 H42 120.0 .
C44 C43 C42 121.4(5) .
C44 C43 H43 119.3 .
C42 C43 H43 119.3 .
C43 C44 C45 119.4(5) .
C43 C44 H44 120.3 .
C45 C44 H44 120.3 .
C46 C45 C44 120.2(6) .
C46 C45 H45 119.9 .
C44 C45 H45 119.9 .
C45 C46 C41 120.7(5) .
C45 C46 H46 119.7 .
C41 C46 H46 119.7 .
C52 C51 C56 117.9(5) .
C52 C51 P2 116.5(4) .
C56 C51 P2 125.5(4) .
C51 C52 C53 121.5(6) .
C51 C52 H52 119.2 .
C53 C52 H52 119.2 .
C54 C53 C52 119.4(7) .
C54 C53 H53 120.3 .
C52 C53 H53 120.3 .
C53 C54 C55 120.5(7) .
C53 C54 H54 119.8 .
C55 C54 H54 119.8 .
C54 C55 C56 120.5(7) .
C54 C55 H55 119.8 .
C56 C55 H55 119.8 .
C55 C56 C51 120.1(6) .
C55 C56 H56 119.9 .
C51 C56 H56 119.9 .
C62 C61 C66 117.6(5) .
C62 C61 P2 122.1(4) .
C66 C61 P2 120.2(4) .
C63 C62 C61 122.0(6) .
C63 C62 H62 119.0 .
C61 C62 H62 119.0 .
C64 C63 C62 120.0(6) .
C64 C63 H63 120.0 .
C62 C63 H63 120.0 .
C63 C64 C65 119.9(6) .
C63 C64 H64 120.0 .
C65 C64 H64 120.0 .
C66 C65 C64 120.6(6) .
C66 C65 H65 119.7 .
C64 C65 H65 119.7 .
C65 C66 C61 119.9(6) .
C65 C66 H66 120.1 .
C61 C66 H66 120.1 .
Ru1 Cl2 Ru1 100.30(7) 2_655
C11 P1 C31 103.8(2) .
C11 P1 C21 104.4(2) .
C31 P1 C21 102.6(2) .
C11 P1 Ru1 115.62(18) .
C31 P1 Ru1 127.48(17) .
C21 P1 Ru1 99.77(17) .
C61 P2 C51 103.8(2) .
C61 P2 C41 101.6(2) .
C51 P2 C41 99.5(2) .
C61 P2 Ru1 118.62(17) .
C51 P2 Ru1 116.97(17) .
C41 P2 Ru1 113.64(18) .
P2 Ru1 P1 100.65(9) .
P2 Ru1 Cl1 95.27(7) .
P1 Ru1 Cl1 93.00(6) .
P2 Ru1 Cl2 101.97(7) .
P1 Ru1 Cl2 92.04(7) .
Cl1 Ru1 Cl2 160.81(5) .
P2 Ru1 Cl2 100.22(8) 2_655
P1 Ru1 Cl2 158.75(5) 2_655
Cl1 Ru1 Cl2 89.08(6) 2_655
Cl2 Ru1 Cl2 79.70(7) 2_655
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 Cl3 1.7199(19) .
C1 Cl4 1.7200(17) .
C1 H1 0.9700 .
C1 H2 0.9700 .
C2 Cl6 1.7200(13) .
C2 Cl5 1.7200(14) .
C2 H3 0.9700 .
C2 H4 0.9700 .
C11 C12 1.384(8) .
C11 C16 1.391(7) .
C11 P1 1.835(6) .
C12 C13 1.389(9) .
C12 H12 0.9300 .
C13 C14 1.370(9) .
C13 H13 0.9300 .
C14 C15 1.409(10) .
C14 H14 0.9300 .
C15 C16 1.381(9) .
C15 H15 0.9300 .
C16 H16 0.9300 .
C21 C26 1.384(8) .
C21 C22 1.388(7) .
C21 P1 1.848(5) .
C22 C23 1.389(8) .
C22 H22 0.9300 .
C23 C24 1.380(10) .
C23 H23 0.9300 .
C24 C25 1.368(9) .
C24 H24 0.9300 .
C25 C26 1.396(9) .
C25 H25 0.9300 .
C26 H26 0.9300 .
C31 C32 1.374(8) .
C31 C36 1.415(8) .
C31 P1 1.838(5) .
C32 C33 1.391(8) .
C32 H32 0.9300 .
C33 C34 1.395(9) .
C33 H33 0.9300 .
C34 C35 1.379(9) .
C34 H34 0.9300 .
C35 C36 1.390(8) .
C35 H35 0.9300 .
C36 H36 0.9300 .
C41 C46 1.396(8) .
C41 C42 1.407(7) .
C41 P2 1.849(5) .
C42 C43 1.372(8) .
C42 H42 0.9300 .
C43 C44 1.363(9) .
C43 H43 0.9300 .
C44 C45 1.400(9) .
C44 H44 0.9300 .
C45 C46 1.368(8) .
C45 H45 0.9300 .
C46 H46 0.9300 .
C51 C52 1.378(8) .
C51 C56 1.395(8) .
C51 P2 1.841(6) .
C52 C53 1.388(9) .
C52 H52 0.9300 .
C53 C54 1.361(11) .
C53 H53 0.9300 .
C54 C55 1.366(11) .
C54 H54 0.9300 .
C55 C56 1.385(10) .
C55 H55 0.9300 .
C56 H56 0.9300 .
C61 C62 1.390(8) .
C61 C66 1.414(8) .
C61 P2 1.822(5) .
C62 C63 1.381(8) .
C62 H62 0.9300 .
C63 C64 1.364(10) .
C63 H63 0.9300 .
C64 C65 1.395(11) .
C64 H64 0.9300 .
C65 C66 1.386(8) .
C65 H65 0.9300 .
C66 H66 0.9300 .
Cl1 Ru1 2.3647(18) .
Cl2 Ru1 2.3933(18) .
Cl2 Ru1 2.4652(14) 2_655
P1 Ru1 2.264(2) .
P2 Ru1 2.2049(17) .
Ru1 Cl2 2.4652(14) 2_655
