#------------------------------------------------------------------------------
#$Date: 2016-03-21 09:18:06 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178621 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/32/4073213.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4073213
loop_
_publ_author_name
'Harvey, Benjamin G.'
'Arif, Atta M.'
'Glöckner, Andreas'
'Ernst, Richard D.'
_publ_section_title
;
 SF6as a Selective and Reactive Fluorinating Agent for Low-Valent
 Transition Metal Complexes#
;
_journal_issue                   11
_journal_name_full               Organometallics
_journal_page_first              2872
_journal_paper_doi               10.1021/om070175i
_journal_volume                  26
_journal_year                    2007
_chemical_formula_moiety         'C60 H90 Cr8 F18,4(C7 H8)'
_chemical_formula_sum            'C88 H122 Cr8 F18'
_chemical_formula_weight         1937.86
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                97.213(4)
_cell_angle_beta                 111.974(5)
_cell_angle_gamma                102.408(5)
_cell_formula_units_Z            1
_cell_length_a                   11.7587(7)
_cell_length_b                   14.4911(12)
_cell_length_c                   14.8362(13)
_cell_measurement_reflns_used    199149
_cell_measurement_temperature    150(1)
_cell_measurement_theta_max      27.485
_cell_measurement_theta_min      2.91
_cell_volume                     2229.6(3)
_computing_cell_refinement       DENZO-SMN
_computing_data_collection       'Nonius COLLECT'
_computing_data_reduction        DENZO-SMN
_computing_molecular_graphics    'WinGX, Ortep3'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    SIR97
_diffrn_ambient_temperature      150(1)
_diffrn_measured_fraction_theta_full 0.979
_diffrn_measured_fraction_theta_max 0.924
_diffrn_measurement_device_type  'Nonius KappaCCD Diffractometer'
_diffrn_measurement_method       'Phi and Omega scan'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0466
_diffrn_reflns_av_sigmaI/netI    0.0635
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            17089
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         27.66
_diffrn_reflns_theta_min         2.93
_exptl_absorpt_coefficient_mu    1.016
_exptl_absorpt_correction_T_max  0.7999
_exptl_absorpt_correction_T_min  0.7175
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'DENZO-SMN (Otwinowski & Minor, 1997)'
_exptl_crystal_colour            blue
_exptl_crystal_density_diffrn    1.443
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1004
_exptl_crystal_size_max          0.35
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.23
_refine_diff_density_max         0.558
_refine_diff_density_min         -0.796
_refine_diff_density_rms         0.089
_refine_ls_extinction_coef       0.0042(7)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.060
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     605
_refine_ls_number_reflns         9615
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.060
_refine_ls_R_factor_all          0.0931
_refine_ls_R_factor_gt           0.0568
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0578P)²+3.8344P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1308
_refine_ls_wR_factor_ref         0.1538
_reflns_number_gt                6761
_reflns_number_total             9615
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om070175i-file002.cif
_cod_data_source_block           rde132
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Multi-scan'
changed to 'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4073213
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Cr1 Cr 0.99765(6) 0.84960(5) 0.28659(5) 0.03125(17) Uani 1 1 d . . .
Cr2 Cr 1.18860(5) 0.88967(5) 0.13247(5) 0.03071(17) Uani 1 1 d . . .
Cr3 Cr 0.69975(6) 0.75604(5) 0.03446(5) 0.03198(17) Uani 1 1 d . . .
Cr4 Cr 1.09452(5) 1.09622(4) 0.06128(5) 0.02954(17) Uani 1 1 d . . .
F1 F 1.0231(2) 0.72777(17) 0.2919(2) 0.0432(6) Uani 1 1 d . . .
F2 F 1.1312(2) 0.88598(17) 0.23853(17) 0.0351(5) Uani 1 1 d . . .
F3 F 0.8612(2) 0.80931(16) 0.15244(18) 0.0370(5) Uani 1 1 d . . .
F4 F 1.0133(2) 0.84429(16) 0.02967(17) 0.0341(5) Uani 1 1 d . . .
F5 F 1.1981(2) 1.02699(16) 0.14393(17) 0.0350(5) Uani 1 1 d . . .
F6 F 0.7589(2) 0.82948(16) -0.05032(18) 0.0366(5) Uani 1 1 d . . .
F7 F 0.6255(2) 0.84868(17) 0.0668(2) 0.0423(6) Uani 1 1 d . . .
F8 F 1.1129(2) 1.18348(17) 0.16898(18) 0.0402(6) Uani 1 1 d . . .
F9 F 0.94203(19) 1.00692(16) 0.05407(17) 0.0330(5) Uani 1 1 d . . .
C1 C 1.0911(4) 0.9202(3) 0.4453(3) 0.0375(9) Uani 1 1 d . . .
C2 C 1.0786(4) 0.9943(3) 0.3906(3) 0.0379(9) Uani 1 1 d . . .
C3 C 0.9465(4) 0.9806(3) 0.3338(3) 0.0349(9) Uani 1 1 d . . .
C4 C 0.8766(4) 0.8993(3) 0.3555(3) 0.0359(9) Uani 1 1 d . . .
C5 C 0.9657(4) 0.8624(3) 0.4243(3) 0.0345(9) Uani 1 1 d . . .
C6 C 1.2130(4) 0.9027(4) 0.5118(4) 0.0504(12) Uani 1 1 d . . .
H6A H 1.2282 0.9238 0.5818 0.076 Uiso 1 1 calc R . .
H6B H 1.2844 0.9394 0.5001 0.076 Uiso 1 1 calc R . .
H6C H 1.2059 0.8333 0.4971 0.076 Uiso 1 1 calc R . .
C7 C 1.1874(5) 1.0700(3) 0.3904(4) 0.0508(12) Uani 1 1 d . . .
H7A H 1.1583 1.0938 0.3291 0.076 Uiso 1 1 calc R . .
H7B H 1.2570 1.0416 0.3935 0.076 Uiso 1 1 calc R . .
H7C H 1.2182 1.1240 0.4484 0.076 Uiso 1 1 calc R . .
C8 C 0.8876(5) 1.0379(3) 0.2597(4) 0.0470(11) Uani 1 1 d . . .
H8A H 0.8598 1.0866 0.2916 0.071 Uiso 1 1 calc R . .
H8B H 0.8138 0.9939 0.2021 0.071 Uiso 1 1 calc R . .
H8C H 0.9511 1.0703 0.2375 0.071 Uiso 1 1 calc R . .
C9 C 0.7330(4) 0.8606(4) 0.3110(4) 0.0468(11) Uani 1 1 d . . .
H9A H 0.7088 0.7932 0.3167 0.070 Uiso 1 1 calc R . .
H9B H 0.6982 0.8632 0.2404 0.070 Uiso 1 1 calc R . .
H9C H 0.6985 0.9001 0.3468 0.070 Uiso 1 1 calc R . .
C10 C 0.9352(5) 0.7761(3) 0.4664(4) 0.0474(11) Uani 1 1 d . . .
H10A H 0.9874 0.7334 0.4601 0.071 Uiso 1 1 calc R . .
H10B H 0.8444 0.7406 0.4297 0.071 Uiso 1 1 calc R . .
H10C H 0.9541 0.7981 0.5371 0.071 Uiso 1 1 calc R . .
C11 C 1.3655(4) 0.8545(3) 0.2184(3) 0.0391(10) Uani 1 1 d . . .
C12 C 1.2707(4) 0.7680(3) 0.1535(3) 0.0365(9) Uani 1 1 d . . .
C13 C 1.2405(4) 0.7774(3) 0.0542(3) 0.0383(10) Uani 1 1 d . . .
C14 C 1.3142(4) 0.8700(3) 0.0564(3) 0.0385(10) Uani 1 1 d . . .
C15 C 1.3938(4) 0.9173(3) 0.1583(3) 0.0374(10) Uani 1 1 d . . .
C16 C 1.4216(4) 0.8740(4) 0.3300(4) 0.0502(12) Uani 1 1 d . . .
H16A H 1.3528 0.8579 0.3525 0.075 Uiso 1 1 calc R . .
H16B H 1.4692 0.9428 0.3579 0.075 Uiso 1 1 calc R . .
H16C H 1.4797 0.8341 0.3528 0.075 Uiso 1 1 calc R . .
C17 C 1.2175(4) 0.6823(3) 0.1880(4) 0.0485(12) Uani 1 1 d . . .
H17A H 1.2864 0.6550 0.2234 0.073 Uiso 1 1 calc R . .
H17B H 1.1515 0.6329 0.1302 0.073 Uiso 1 1 calc R . .
H17C H 1.1799 0.7031 0.2331 0.073 Uiso 1 1 calc R . .
C18 C 1.1420(4) 0.7055(4) -0.0390(4) 0.0492(12) Uani 1 1 d . . .
H18A H 1.0768 0.7355 -0.0753 0.074 Uiso 1 1 calc R . .
H18B H 1.1016 0.6485 -0.0210 0.074 Uiso 1 1 calc R . .
H18C H 1.1834 0.6856 -0.0815 0.074 Uiso 1 1 calc R . .
C19 C 1.3144(5) 0.9093(4) -0.0324(4) 0.0505(12) Uani 1 1 d . . .
H19A H 1.3883 0.9011 -0.0446 0.076 Uiso 1 1 calc R . .
H19B H 1.3195 0.9785 -0.0193 0.076 Uiso 1 1 calc R . .
H19C H 1.2355 0.8742 -0.0911 0.076 Uiso 1 1 calc R . .
C20 C 1.4862(4) 1.0149(4) 0.1931(4) 0.0532(12) Uani 1 1 d . . .
H20A H 1.5627 1.0113 0.1824 0.080 Uiso 1 1 calc R . .
H20B H 1.5103 1.0390 0.2643 0.080 Uiso 1 1 calc R . .
H20C H 1.4470 1.0592 0.1555 0.080 Uiso 1 1 calc R . .
C21 C 0.6377(5) 0.6225(3) -0.0829(4) 0.0542(13) Uani 1 1 d . . .
C22 C 0.5303(4) 0.6421(3) -0.0713(4) 0.0516(13) Uani 1 1 d . . .
C23 C 0.5438(4) 0.6344(3) 0.0258(4) 0.0420(10) Uani 1 1 d . . .
C24 C 0.6614(4) 0.6148(3) 0.0757(4) 0.0390(10) Uani 1 1 d . . .
C25 C 0.7192(4) 0.6070(3) 0.0085(4) 0.0461(11) Uani 1 1 d . . .
C26 C 0.6616(9) 0.6200(5) -0.1752(6) 0.116(3) Uani 1 1 d . . .
H26A H 0.5896 0.6316 -0.2281 0.174 Uiso 1 1 calc R . .
H26B H 0.6706 0.5562 -0.1969 0.174 Uiso 1 1 calc R . .
H26C H 0.7404 0.6704 -0.1610 0.174 Uiso 1 1 calc R . .
C27 C 0.4223(6) 0.6700(5) -0.1455(6) 0.105(3) Uani 1 1 d . . .
H27A H 0.4283 0.7377 -0.1214 0.158 Uiso 1 1 calc R . .
H27B H 0.3403 0.6280 -0.1533 0.158 Uiso 1 1 calc R . .
H27C H 0.4282 0.6623 -0.2101 0.158 Uiso 1 1 calc R . .
C28 C 0.4526(5) 0.6510(4) 0.0702(6) 0.0761(19) Uani 1 1 d . . .
H28A H 0.4551 0.7196 0.0796 0.114 Uiso 1 1 calc R . .
H28B H 0.4772 0.6328 0.1349 0.114 Uiso 1 1 calc R . .
H28C H 0.3657 0.6112 0.0253 0.114 Uiso 1 1 calc R . .
C29 C 0.7137(6) 0.6016(4) 0.1808(4) 0.0742(18) Uani 1 1 d . . .
H29A H 0.7105 0.5333 0.1798 0.111 Uiso 1 1 calc R . .
H29B H 0.6622 0.6208 0.2147 0.111 Uiso 1 1 calc R . .
H29C H 0.8025 0.6420 0.2166 0.111 Uiso 1 1 calc R . .
C30 C 0.8483(5) 0.5895(4) 0.0321(7) 0.099(3) Uani 1 1 d . . .
H30A H 0.9077 0.6256 0.1000 0.148 Uiso 1 1 calc R . .
H30B H 0.8814 0.6116 -0.0155 0.148 Uiso 1 1 calc R . .
H30C H 0.8395 0.5201 0.0270 0.148 Uiso 1 1 calc R . .
C31 C 1.0877(19) 0.4497(13) 0.2584(15) 0.096(7) Uani 0.50 1 d PD A 1
H31A H 1.1032 0.3892 0.2353 0.144 Uiso 0.50 1 calc PR A 1
H31B H 1.1687 0.4954 0.3071 0.144 Uiso 0.50 1 calc PR A 1
H31C H 1.0511 0.4782 0.2015 0.144 Uiso 0.50 1 calc PR A 1
C32 C 0.9991(8) 0.4297(7) 0.3050(7) 0.066(3) Uani 0.50 1 d PGD A 1
C33 C 0.9646(12) 0.5065(5) 0.3432(9) 0.074(6) Uani 0.50 1 d PG A 1
H33 H 1.0015 0.5708 0.3409 0.089 Uiso 0.50 1 calc PR A 1
C34 C 0.8762(13) 0.4892(6) 0.3848(11) 0.094(8) Uani 0.50 1 d PG A 1
H34 H 0.8527 0.5417 0.4110 0.112 Uiso 0.50 1 calc PR A 1
C35 C 0.8223(10) 0.3952(7) 0.3882(9) 0.077(4) Uani 0.50 1 d PG A 1
H35 H 0.7619 0.3834 0.4167 0.093 Uiso 0.50 1 calc PR A 1
C36 C 0.8568(10) 0.3184(5) 0.3500(8) 0.081(5) Uani 0.50 1 d PG A 1
H36 H 0.8200 0.2541 0.3523 0.097 Uiso 0.50 1 calc PR A 1
C37 C 0.9452(10) 0.3356(6) 0.3084(8) 0.053(4) Uani 0.50 1 d PG A 1
H37 H 0.9688 0.2832 0.2822 0.063 Uiso 0.50 1 calc PR A 1
C31A C 0.821(3) 0.464(3) 0.399(2) 0.202(17) Uani 0.50 1 d P B 2
H31D H 0.8238 0.5324 0.4079 0.302 Uiso 0.50 1 calc PR B 2
H31E H 0.8479 0.4464 0.4639 0.302 Uiso 0.50 1 calc PR B 2
H31F H 0.7342 0.4237 0.3552 0.302 Uiso 0.50 1 calc PR B 2
C32A C 0.9059(7) 0.4474(5) 0.3550(6) 0.078(5) Uani 0.50 1 d PG B 2
C33A C 0.9058(8) 0.3507(5) 0.3410(7) 0.070(5) Uani 0.50 1 d PG B 2
H33A H 0.8495 0.3047 0.3568 0.085 Uiso 0.50 1 calc PR B 2
C34A C 0.9879(10) 0.3214(6) 0.3039(9) 0.084(6) Uani 0.50 1 d PG B 2
H34A H 0.9878 0.2553 0.2943 0.101 Uiso 0.50 1 calc PR B 2
C35A C 1.0702(7) 0.3888(6) 0.2808(6) 0.085(5) Uani 0.50 1 d PG B 2
H35A H 1.1263 0.3687 0.2554 0.102 Uiso 0.50 1 calc PR B 2
C36A C 1.0703(9) 0.4855(6) 0.2949(9) 0.101(8) Uani 0.50 1 d PG B 2
H36A H 1.1266 0.5315 0.2791 0.121 Uiso 0.50 1 calc PR B 2
C37A C 0.9882(10) 0.5148(5) 0.3320(10) 0.083(6) Uani 0.50 1 d PG B 2
H37A H 0.9883 0.5809 0.3416 0.100 Uiso 0.50 1 calc PR B 2
C38 C 0.3755(12) 0.4184(11) 0.5472(12) 0.070(4) Uani 0.50 1 d PG B 1
H38A H 0.4371 0.4561 0.6139 0.105 Uiso 0.50 1 calc PR B 1
H38B H 0.3021 0.3760 0.5522 0.105 Uiso 0.50 1 calc PR B 1
H38C H 0.3463 0.4627 0.5047 0.105 Uiso 0.50 1 calc PR B 1
C39 C 0.4382(9) 0.3581(6) 0.5026(7) 0.070(3) Uani 0.50 1 d PG B 1
C40 C 0.3700(6) 0.2982(7) 0.4075(8) 0.062(5) Uani 0.50 1 d PG B 1
H40 H 0.2827 0.2944 0.3711 0.075 Uiso 0.50 1 calc PR B 1
C41 C 0.4296(8) 0.2439(7) 0.3659(6) 0.083(6) Uani 0.50 1 d PG B 1
H41 H 0.3830 0.2029 0.3009 0.099 Uiso 0.50 1 calc PR B 1
C42 C 0.5573(8) 0.2495(6) 0.4192(7) 0.078(4) Uani 0.50 1 d PG B 1
H42 H 0.5981 0.2123 0.3907 0.094 Uiso 0.50 1 calc PR B 1
C43 C 0.6255(7) 0.3094(7) 0.5143(7) 0.075(4) Uani 0.50 1 d PG B 1
H43 H 0.7129 0.3132 0.5507 0.090 Uiso 0.50 1 calc PR B 1
C44 C 0.5660(10) 0.3637(7) 0.5559(6) 0.067(5) Uani 0.50 1 d PG B 1
H44 H 0.6126 0.4046 0.6209 0.080 Uiso 0.50 1 calc PR B 1
C38A C 0.4659(19) 0.2066(11) 0.3674(14) 0.090(6) Uani 0.50 1 d P C 2
H38D H 0.3863 0.1820 0.3066 0.136 Uiso 0.50 1 calc PR C 2
H38E H 0.4822 0.1537 0.4009 0.136 Uiso 0.50 1 calc PR C 2
H38F H 0.5370 0.2324 0.3498 0.136 Uiso 0.50 1 calc PR C 2
C39A C 0.4541(9) 0.2844(6) 0.4348(6) 0.061(3) Uani 0.50 1 d PG C 2
C40A C 0.5564(7) 0.3299(6) 0.5261(7) 0.061(4) Uani 0.50 1 d PG C 2
H40A H 0.6340 0.3125 0.5435 0.073 Uiso 0.50 1 calc PR C 2
C41A C 0.5452(9) 0.4009(7) 0.5919(6) 0.086(5) Uani 0.50 1 d PG C 2
H41A H 0.6151 0.4320 0.6543 0.104 Uiso 0.50 1 calc PR C 2
C42A C 0.4316(10) 0.4264(7) 0.5663(7) 0.080(5) Uani 0.50 1 d PG C 2
H42A H 0.4239 0.4749 0.6113 0.095 Uiso 0.50 1 calc PR C 2
C43A C 0.3293(7) 0.3809(7) 0.4750(8) 0.068(3) Uani 0.50 1 d PG C 2
H43A H 0.2517 0.3984 0.4576 0.082 Uiso 0.50 1 calc PR C 2
C44A C 0.3406(8) 0.3099(7) 0.4092(6) 0.059(4) Uani 0.50 1 d PG C 2
H44A H 0.2707 0.2789 0.3468 0.071 Uiso 0.50 1 calc PR C 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
F1 Cr1 F3 95.44(11) . .
F1 Cr1 F2 91.36(10) . .
F3 Cr1 F2 93.13(10) . .
F1 Cr1 C1 100.23(14) . .
F3 Cr1 C1 156.32(12) . .
F2 Cr1 C1 104.05(13) . .
F1 Cr1 C5 92.78(13) . .
F3 Cr1 C5 124.20(13) . .
F2 Cr1 C5 141.77(13) . .
C1 Cr1 C5 37.91(15) . .
F1 Cr1 C2 135.67(14) . .
F3 Cr1 C2 128.84(13) . .
F2 Cr1 C2 88.43(13) . .
C1 Cr1 C2 37.81(16) . .
C5 Cr1 C2 62.86(15) . .
F1 Cr1 C3 155.30(13) . .
F3 Cr1 C3 96.13(13) . .
F2 Cr1 C3 109.69(12) . .
C1 Cr1 C3 62.98(15) . .
C5 Cr1 C3 62.73(15) . .
C2 Cr1 C3 37.25(15) . .
F1 Cr1 C4 119.82(13) . .
F3 Cr1 C4 93.91(13) . .
F2 Cr1 C4 147.12(13) . .
C1 Cr1 C4 62.89(15) . .
C5 Cr1 C4 37.28(15) . .
C2 Cr1 C4 62.49(15) . .
C3 Cr1 C4 37.57(14) . .
F2 Cr2 F5 90.61(10) . .
F2 Cr2 F4 92.19(10) . .
F5 Cr2 F4 94.69(9) . .
F2 Cr2 C12 96.09(13) . .
F5 Cr2 C12 153.94(13) . .
F4 Cr2 C12 110.13(14) . .
F2 Cr2 C11 92.86(13) . .
F5 Cr2 C11 116.76(14) . .
F4 Cr2 C11 148.07(14) . .
C12 Cr2 C11 37.95(17) . .
F2 Cr2 C13 129.73(13) . .
F5 Cr2 C13 139.21(13) . .
F4 Cr2 C13 90.10(13) . .
C12 Cr2 C13 37.55(16) . .
C11 Cr2 C13 62.88(16) . .
F2 Cr2 C14 155.53(13) . .
F5 Cr2 C14 103.09(13) . .
F4 Cr2 C14 106.54(14) . .
C12 Cr2 C14 63.05(15) . .
C11 Cr2 C14 62.92(16) . .
C13 Cr2 C14 37.58(16) . .
F2 Cr2 C15 123.17(13) . .
F5 Cr2 C15 92.39(13) . .
F4 Cr2 C15 143.85(14) . .
C12 Cr2 C15 62.93(15) . .
C11 Cr2 C15 37.48(15) . .
C13 Cr2 C15 62.58(16) . .
C14 Cr2 C15 37.49(16) . .
F7 Cr3 F3 94.66(11) . .
F7 Cr3 F6 92.71(10) . .
F3 Cr3 F6 94.21(10) . .
F7 Cr3 C22 100.79(16) . .
F3 Cr3 C22 155.27(14) . .
F6 Cr3 C22 104.13(16) . .
F7 Cr3 C23 92.99(13) . .
F3 Cr3 C23 123.13(15) . .
F6 Cr3 C23 141.54(15) . .
C22 Cr3 C23 37.52(19) . .
F7 Cr3 C24 119.33(14) . .
F3 Cr3 C24 92.72(13) . .
F6 Cr3 C24 146.51(14) . .
C22 Cr3 C24 62.89(17) . .
C23 Cr3 C24 37.31(15) . .
F7 Cr3 C21 136.37(17) . .
F3 Cr3 C21 128.77(17) . .
F6 Cr3 C21 88.47(15) . .
C22 Cr3 C21 37.6(2) . .
C23 Cr3 C21 62.08(18) . .
C24 Cr3 C21 62.12(18) . .
F7 Cr3 C25 154.57(13) . .
F3 Cr3 C25 95.67(15) . .
F6 Cr3 C25 109.60(15) . .
C22 Cr3 C25 62.79(17) . .
C23 Cr3 C25 61.99(15) . .
C24 Cr3 C25 37.02(17) . .
C21 Cr3 C25 37.21(19) . .
F8 Cr4 F6 94.16(11) . 2_775
F8 Cr4 F4 92.11(10) . 2_775
F6 Cr4 F4 91.09(9) 2_775 2_775
F8 Cr4 F5 92.47(11) . .
F6 Cr4 F5 89.89(9) 2_775 .
F4 Cr4 F5 175.24(11) 2_775 .
F8 Cr4 F9 94.74(10) . .
F6 Cr4 F9 171.09(11) 2_775 .
F4 Cr4 F9 88.18(9) 2_775 .
F5 Cr4 F9 90.13(9) . .
F8 Cr4 F9 173.69(10) . 2_775
F6 Cr4 F9 92.16(10) 2_775 2_775
F4 Cr4 F9 87.85(10) 2_775 2_775
F5 Cr4 F9 87.46(10) . 2_775
F9 Cr4 F9 78.94(10) . 2_775
Cr2 F2 Cr1 151.68(13) . .
Cr1 F3 Cr3 166.17(13) . .
Cr4 F4 Cr2 134.02(12) 2_775 .
Cr4 F5 Cr2 132.98(13) . .
Cr4 F6 Cr3 144.38(13) 2_775 .
Cr4 F9 Cr4 101.05(10) . 2_775
C5 C1 C2 107.8(3) . .
C5 C1 C6 125.0(4) . .
C2 C1 C6 127.2(4) . .
C5 C1 Cr1 71.8(2) . .
C2 C1 Cr1 72.3(2) . .
C6 C1 Cr1 120.5(3) . .
C3 C2 C1 108.0(3) . .
C3 C2 C7 126.6(4) . .
C1 C2 C7 125.3(4) . .
C3 C2 Cr1 71.5(2) . .
C1 C2 Cr1 69.9(2) . .
C7 C2 Cr1 122.1(3) . .
C2 C3 C4 107.9(3) . .
C2 C3 C8 127.0(4) . .
C4 C3 C8 125.1(4) . .
C2 C3 Cr1 71.3(2) . .
C4 C3 Cr1 71.3(2) . .
C8 C3 Cr1 121.2(3) . .
C5 C4 C3 108.1(3) . .
C5 C4 C9 126.9(4) . .
C3 C4 C9 125.0(4) . .
C5 C4 Cr1 70.7(2) . .
C3 C4 Cr1 71.1(2) . .
C9 C4 Cr1 123.3(3) . .
C4 C5 C1 108.1(4) . .
C4 C5 C10 126.6(4) . .
C1 C5 C10 125.4(4) . .
C4 C5 Cr1 72.0(2) . .
C1 C5 Cr1 70.3(2) . .
C10 C5 Cr1 122.2(3) . .
C1 C6 H6A 109.5 . .
C1 C6 H6B 109.5 . .
H6A C6 H6B 109.5 . .
C1 C6 H6C 109.5 . .
H6A C6 H6C 109.5 . .
H6B C6 H6C 109.5 . .
C2 C7 H7A 109.5 . .
C2 C7 H7B 109.5 . .
H7A C7 H7B 109.5 . .
C2 C7 H7C 109.5 . .
H7A C7 H7C 109.5 . .
H7B C7 H7C 109.5 . .
C3 C8 H8A 109.5 . .
C3 C8 H8B 109.5 . .
H8A C8 H8B 109.5 . .
C3 C8 H8C 109.5 . .
H8A C8 H8C 109.5 . .
H8B C8 H8C 109.5 . .
C4 C9 H9A 109.5 . .
C4 C9 H9B 109.5 . .
H9A C9 H9B 109.5 . .
C4 C9 H9C 109.5 . .
H9A C9 H9C 109.5 . .
H9B C9 H9C 109.5 . .
C5 C10 H10A 109.5 . .
C5 C10 H10B 109.5 . .
H10A C10 H10B 109.5 . .
C5 C10 H10C 109.5 . .
H10A C10 H10C 109.5 . .
H10B C10 H10C 109.5 . .
C15 C11 C12 108.0(4) . .
C15 C11 C16 127.3(4) . .
C12 C11 C16 124.7(4) . .
C15 C11 Cr2 72.5(2) . .
C12 C11 Cr2 70.5(2) . .
C16 C11 Cr2 122.0(3) . .
C13 C12 C11 108.0(4) . .
C13 C12 C17 127.5(4) . .
C11 C12 C17 124.5(4) . .
C13 C12 Cr2 71.8(2) . .
C11 C12 Cr2 71.5(2) . .
C17 C12 Cr2 123.5(3) . .
C12 C13 C14 108.4(4) . .
C12 C13 C18 126.7(4) . .
C14 C13 C18 124.8(4) . .
C12 C13 Cr2 70.6(2) . .
C14 C13 Cr2 71.5(2) . .
C18 C13 Cr2 121.0(3) . .
C13 C14 C15 107.9(4) . .
C13 C14 C19 126.3(4) . .
C15 C14 C19 125.6(4) . .
C13 C14 Cr2 71.0(2) . .
C15 C14 Cr2 72.1(2) . .
C19 C14 Cr2 125.2(3) . .
C11 C15 C14 107.6(4) . .
C11 C15 C20 127.2(4) . .
C14 C15 C20 125.1(4) . .
C11 C15 Cr2 70.1(2) . .
C14 C15 Cr2 70.4(2) . .
C20 C15 Cr2 124.0(3) . .
C11 C16 H16A 109.5 . .
C11 C16 H16B 109.5 . .
H16A C16 H16B 109.5 . .
C11 C16 H16C 109.5 . .
H16A C16 H16C 109.5 . .
H16B C16 H16C 109.5 . .
C12 C17 H17A 109.5 . .
C12 C17 H17B 109.5 . .
H17A C17 H17B 109.5 . .
C12 C17 H17C 109.5 . .
H17A C17 H17C 109.5 . .
H17B C17 H17C 109.5 . .
C13 C18 H18A 109.5 . .
C13 C18 H18B 109.5 . .
H18A C18 H18B 109.5 . .
C13 C18 H18C 109.5 . .
H18A C18 H18C 109.5 . .
H18B C18 H18C 109.5 . .
C14 C19 H19A 109.5 . .
C14 C19 H19B 109.5 . .
H19A C19 H19B 109.5 . .
C14 C19 H19C 109.5 . .
H19A C19 H19C 109.5 . .
H19B C19 H19C 109.5 . .
C15 C20 H20A 109.5 . .
C15 C20 H20B 109.5 . .
H20A C20 H20B 109.5 . .
C15 C20 H20C 109.5 . .
H20A C20 H20C 109.5 . .
H20B C20 H20C 109.5 . .
C25 C21 C22 108.1(4) . .
C25 C21 C26 126.0(6) . .
C22 C21 C26 125.9(6) . .
C25 C21 Cr3 71.6(3) . .
C22 C21 Cr3 69.9(3) . .
C26 C21 Cr3 123.5(4) . .
C23 C22 C21 107.4(4) . .
C23 C22 C27 124.8(6) . .
C21 C22 C27 127.7(6) . .
C23 C22 Cr3 72.2(3) . .
C21 C22 Cr3 72.5(3) . .
C27 C22 Cr3 119.1(4) . .
C22 C23 C24 108.5(4) . .
C22 C23 C28 125.4(5) . .
C24 C23 C28 125.9(5) . .
C22 C23 Cr3 70.3(2) . .
C24 C23 Cr3 71.6(2) . .
C28 C23 Cr3 120.9(3) . .
C25 C24 C23 107.9(4) . .
C25 C24 C29 126.0(4) . .
C23 C24 C29 126.1(5) . .
C25 C24 Cr3 71.8(2) . .
C23 C24 Cr3 71.1(2) . .
C29 C24 Cr3 124.0(3) . .
C24 C25 C21 108.0(4) . .
C24 C25 C30 125.6(6) . .
C21 C25 C30 126.3(6) . .
C24 C25 Cr3 71.1(2) . .
C21 C25 Cr3 71.2(3) . .
C30 C25 Cr3 121.4(3) . .
C21 C26 H26A 109.5 . .
C21 C26 H26B 109.5 . .
H26A C26 H26B 109.5 . .
C21 C26 H26C 109.5 . .
H26A C26 H26C 109.5 . .
H26B C26 H26C 109.5 . .
C22 C27 H27A 109.5 . .
C22 C27 H27B 109.5 . .
H27A C27 H27B 109.5 . .
C22 C27 H27C 109.5 . .
H27A C27 H27C 109.5 . .
H27B C27 H27C 109.5 . .
C23 C28 H28A 109.5 . .
C23 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
C23 C28 H28C 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
C24 C29 H29A 109.5 . .
C24 C29 H29B 109.5 . .
H29A C29 H29B 109.5 . .
C24 C29 H29C 109.5 . .
H29A C29 H29C 109.5 . .
H29B C29 H29C 109.5 . .
C25 C30 H30A 109.5 . .
C25 C30 H30B 109.5 . .
H30A C30 H30B 109.5 . .
C25 C30 H30C 109.5 . .
H30A C30 H30C 109.5 . .
H30B C30 H30C 109.5 . .
C32 C31 H31A 109.5 . .
C32 C31 H31B 109.5 . .
H31A C31 H31B 109.5 . .
C32 C31 H31C 109.5 . .
H31A C31 H31C 109.5 . .
H31B C31 H31C 109.5 . .
C33 C32 C37 120.0 . .
C33 C32 C31 118.6(10) . .
C37 C32 C31 121.4(10) . .
C32 C33 C34 120.0 . .
C32 C33 H33 120.0 . .
C34 C33 H33 120.0 . .
C35 C34 C33 120.0 . .
C35 C34 H34 120.0 . .
C33 C34 H34 120.0 . .
C36 C35 C34 120.0 . .
C36 C35 H35 120.0 . .
C34 C35 H35 120.0 . .
C37 C36 C35 120.0 . .
C37 C36 H36 120.0 . .
C35 C36 H36 120.0 . .
C36 C37 C32 120.0 . .
C36 C37 H37 120.0 . .
C32 C37 H37 120.0 . .
C32A C31A H31D 109.5 . .
C32A C31A H31E 109.5 . .
H31D C31A H31E 109.5 . .
C32A C31A H31F 109.5 . .
H31D C31A H31F 109.5 . .
H31E C31A H31F 109.5 . .
C33A C32A C37A 120.0 . .
C33A C32A C31A 111.5(15) . .
C37A C32A C31A 128.4(15) . .
C32A C33A C34A 120.0 . .
C32A C33A H33A 120.0 . .
C34A C33A H33A 120.0 . .
C35A C34A C33A 120.0 . .
C35A C34A H34A 120.0 . .
C33A C34A H34A 120.0 . .
C34A C35A C36A 120.0 . .
C34A C35A H35A 120.0 . .
C36A C35A H35A 120.0 . .
C37A C36A C35A 120.0 . .
C37A C36A H36A 120.0 . .
C35A C36A H36A 120.0 . .
C36A C37A C32A 120.0 . .
C36A C37A H37A 120.0 . .
C32A C37A H37A 120.0 . .
C39 C38 H38A 109.5 . .
C39 C38 H38B 109.5 . .
H38A C38 H38B 109.5 . .
C39 C38 H38C 109.5 . .
H38A C38 H38C 109.5 . .
H38B C38 H38C 109.5 . .
C40 C39 C44 120.0 . .
C40 C39 C38 120.3(10) . .
C44 C39 C38 119.6(10) . .
C41 C40 C39 120.0 . .
C41 C40 H40 120.0 . .
C39 C40 H40 120.0 . .
C40 C41 C42 120.0 . .
C40 C41 H41 120.0 . .
C42 C41 H41 120.0 . .
C43 C42 C41 120.0 . .
C43 C42 H42 120.0 . .
C41 C42 H42 120.0 . .
C42 C43 C44 120.0 . .
C42 C43 H43 120.0 . .
C44 C43 H43 120.0 . .
C43 C44 C39 120.0 . .
C43 C44 H44 120.0 . .
C39 C44 H44 120.0 . .
C39A C38A H38D 109.5 . .
C39A C38A H38E 109.5 . .
H38D C38A H38E 109.5 . .
C39A C38A H38F 109.5 . .
H38D C38A H38F 109.5 . .
H38E C38A H38F 109.5 . .
C40A C39A C44A 120.0 . .
C40A C39A C38A 119.3(10) . .
C44A C39A C38A 120.6(10) . .
C41A C40A C39A 120.0 . .
C41A C40A H40A 120.0 . .
C39A C40A H40A 120.0 . .
C40A C41A C42A 120.0 . .
C40A C41A H41A 120.0 . .
C42A C41A H41A 120.0 . .
C43A C42A C41A 120.0 . .
C43A C42A H42A 120.0 . .
C41A C42A H42A 120.0 . .
C42A C43A C44A 120.0 . .
C42A C43A H43A 120.0 . .
C44A C43A H43A 120.0 . .
C43A C44A C39A 120.0 . .
C43A C44A H44A 120.0 . .
C39A C44A H44A 120.0 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Cr1 F1 1.859(2) .
Cr1 F3 1.947(2) .
Cr1 F2 1.957(2) .
Cr1 C1 2.185(4) .
Cr1 C5 2.204(4) .
Cr1 C2 2.217(4) .
Cr1 C3 2.220(4) .
Cr1 C4 2.222(4) .
Cr2 F2 1.932(2) .
Cr2 F5 1.951(2) .
Cr2 F4 1.955(2) .
Cr2 C12 2.187(4) .
Cr2 C11 2.201(4) .
Cr2 C13 2.203(4) .
Cr2 C14 2.209(4) .
Cr2 C15 2.232(4) .
Cr3 F7 1.857(2) .
Cr3 F3 1.952(2) .
Cr3 F6 1.968(2) .
Cr3 C22 2.181(4) .
Cr3 C23 2.206(4) .
Cr3 C24 2.212(4) .
Cr3 C21 2.215(5) .
Cr3 C25 2.221(4) .
Cr4 F8 1.821(2) .
Cr4 F6 1.900(2) 2_775
Cr4 F4 1.911(2) 2_775
Cr4 F5 1.926(2) .
Cr4 F9 1.930(2) .
Cr4 F9 1.969(2) 2_775
F4 Cr4 1.911(2) 2_775
F6 Cr4 1.900(2) 2_775
F9 Cr4 1.969(2) 2_775
C1 C5 1.426(6) .
C1 C2 1.427(6) .
C1 C6 1.500(6) .
C2 C3 1.417(6) .
C2 C7 1.496(6) .
C3 C4 1.430(6) .
C3 C8 1.511(6) .
C4 C5 1.415(6) .
C4 C9 1.506(6) .
C5 C10 1.501(6) .
C6 H6A 0.9800 .
C6 H6B 0.9800 .
C6 H6C 0.9800 .
C7 H7A 0.9800 .
C7 H7B 0.9800 .
C7 H7C 0.9800 .
C8 H8A 0.9800 .
C8 H8B 0.9800 .
C8 H8C 0.9800 .
C9 H9A 0.9800 .
C9 H9B 0.9800 .
C9 H9C 0.9800 .
C10 H10A 0.9800 .
C10 H10B 0.9800 .
C10 H10C 0.9800 .
C11 C15 1.425(6) .
C11 C12 1.427(6) .
C11 C16 1.497(7) .
C12 C13 1.413(6) .
C12 C17 1.503(6) .
C13 C14 1.421(6) .
C13 C18 1.504(7) .
C14 C15 1.427(6) .
C14 C19 1.500(6) .
C15 C20 1.478(6) .
C16 H16A 0.9800 .
C16 H16B 0.9800 .
C16 H16C 0.9800 .
C17 H17A 0.9800 .
C17 H17B 0.9800 .
C17 H17C 0.9800 .
C18 H18A 0.9800 .
C18 H18B 0.9800 .
C18 H18C 0.9800 .
C19 H19A 0.9800 .
C19 H19B 0.9800 .
C19 H19C 0.9800 .
C20 H20A 0.9800 .
C20 H20B 0.9800 .
C20 H20C 0.9800 .
C21 C25 1.415(7) .
C21 C22 1.417(7) .
C21 C26 1.494(8) .
C22 C23 1.411(7) .
C22 C27 1.508(7) .
C23 C24 1.413(6) .
C23 C28 1.498(7) .
C24 C25 1.407(6) .
C24 C29 1.502(7) .
C25 C30 1.511(6) .
C26 H26A 0.9800 .
C26 H26B 0.9800 .
C26 H26C 0.9800 .
C27 H27A 0.9800 .
C27 H27B 0.9800 .
C27 H27C 0.9800 .
C28 H28A 0.9800 .
C28 H28B 0.9800 .
C28 H28C 0.9800 .
C29 H29A 0.9800 .
C29 H29B 0.9800 .
C29 H29C 0.9800 .
C30 H30A 0.9800 .
C30 H30B 0.9800 .
C30 H30C 0.9800 .
C31 C32 1.451(15) .
C31 H31A 0.9800 .
C31 H31B 0.9800 .
C31 H31C 0.9800 .
C32 C33 1.3900 .
C32 C37 1.3900 .
C33 C34 1.3900 .
C33 H33 0.9500 .
C34 C35 1.3900 .
C34 H34 0.9500 .
C35 C36 1.3900 .
C35 H35 0.9500 .
C36 C37 1.3900 .
C36 H36 0.9500 .
C37 H37 0.9500 .
C31A C32A 1.42(3) .
C31A H31D 0.9800 .
C31A H31E 0.9800 .
C31A H31F 0.9800 .
C32A C33A 1.3900 .
C32A C37A 1.3900 .
C33A C34A 1.3900 .
C33A H33A 0.9500 .
C34A C35A 1.3900 .
C34A H34A 0.9500 .
C35A C36A 1.3900 .
C35A H35A 0.9500 .
C36A C37A 1.3900 .
C36A H36A 0.9500 .
C37A H37A 0.9500 .
C38 C39 1.497(13) .
C38 H38A 0.9800 .
C38 H38B 0.9800 .
C38 H38C 0.9800 .
C39 C40 1.3900 .
C39 C44 1.3900 .
C40 C41 1.3900 .
C40 H40 0.9500 .
C41 C42 1.3900 .
C41 H41 0.9500 .
C42 C43 1.3900 .
C42 H42 0.9500 .
C43 C44 1.3900 .
C43 H43 0.9500 .
C44 H44 0.9500 .
C38A C39A 1.476(18) .
C38A H38D 0.9800 .
C38A H38E 0.9800 .
C38A H38F 0.9800 .
C39A C40A 1.3900 .
C39A C44A 1.3900 .
C40A C41A 1.3900 .
C40A H40A 0.9500 .
C41A C42A 1.3900 .
C41A H41A 0.9500 .
C42A C43A 1.3900 .
C42A H42A 0.9500 .
C43A C44A 1.3900 .
C43A H43A 0.9500 .
C44A H44A 0.9500 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
F5 Cr2 F2 Cr1 105.4(3) . .
F4 Cr2 F2 Cr1 10.7(3) . .
C12 Cr2 F2 Cr1 -99.8(3) . .
C11 Cr2 F2 Cr1 -137.8(3) . .
C13 Cr2 F2 Cr1 -81.3(3) . .
C14 Cr2 F2 Cr1 -129.8(3) . .
C15 Cr2 F2 Cr1 -161.3(3) . .
F1 Cr1 F2 Cr2 86.1(3) . .
F3 Cr1 F2 Cr2 -9.4(3) . .
C1 Cr1 F2 Cr2 -173.0(3) . .
C5 Cr1 F2 Cr2 -177.7(2) . .
C2 Cr1 F2 Cr2 -138.3(3) . .
C3 Cr1 F2 Cr2 -107.1(3) . .
C4 Cr1 F2 Cr2 -111.6(3) . .
F1 Cr1 F3 Cr3 77.2(6) . .
F2 Cr1 F3 Cr3 168.9(5) . .
C1 Cr1 F3 Cr3 -54.2(7) . .
C5 Cr1 F3 Cr3 -19.9(6) . .
C2 Cr1 F3 Cr3 -100.6(6) . .
C3 Cr1 F3 Cr3 -80.9(6) . .
C4 Cr1 F3 Cr3 -43.3(6) . .
F7 Cr3 F3 Cr1 72.2(5) . .
F6 Cr3 F3 Cr1 165.3(5) . .
C22 Cr3 F3 Cr1 -56.5(7) . .
C23 Cr3 F3 Cr1 -24.4(6) . .
C24 Cr3 F3 Cr1 -47.5(6) . .
C21 Cr3 F3 Cr1 -103.3(6) . .
C25 Cr3 F3 Cr1 -84.5(6) . .
F2 Cr2 F4 Cr4 109.37(17) . 2_775
F5 Cr2 F4 Cr4 18.58(18) . 2_775
C12 Cr2 F4 Cr4 -153.33(18) . 2_775
C11 Cr2 F4 Cr4 -151.7(2) . 2_775
C13 Cr2 F4 Cr4 -120.87(19) . 2_775
C14 Cr2 F4 Cr4 -86.6(2) . 2_775
C15 Cr2 F4 Cr4 -82.0(3) . 2_775
F8 Cr4 F5 Cr2 143.15(17) . .
F6 Cr4 F5 Cr2 -122.70(17) 2_775 .
F4 Cr4 F5 Cr2 -20.8(13) 2_775 .
F9 Cr4 F5 Cr2 48.39(17) . .
F9 Cr4 F5 Cr2 -30.53(16) 2_775 .
F2 Cr2 F5 Cr4 -107.11(17) . .
F4 Cr2 F5 Cr4 -14.87(17) . .
C12 Cr2 F5 Cr4 147.6(3) . .
C11 Cr2 F5 Cr4 159.38(17) . .
C13 Cr2 F5 Cr4 80.7(2) . .
C14 Cr2 F5 Cr4 93.33(19) . .
C15 Cr2 F5 Cr4 129.66(19) . .
F7 Cr3 F6 Cr4 109.8(2) . 2_775
F3 Cr3 F6 Cr4 15.0(2) . 2_775
C22 Cr3 F6 Cr4 -148.3(2) . 2_775
C23 Cr3 F6 Cr4 -151.9(2) . 2_775
C24 Cr3 F6 Cr4 -86.4(3) . 2_775
C21 Cr3 F6 Cr4 -113.8(3) . 2_775
C25 Cr3 F6 Cr4 -82.6(3) . 2_775
F8 Cr4 F9 Cr4 -179.88(10) . 2_775
F6 Cr4 F9 Cr4 2.7(6) 2_775 2_775
F4 Cr4 F9 Cr4 88.16(10) 2_775 2_775
F5 Cr4 F9 Cr4 -87.39(10) . 2_775
F9 Cr4 F9 Cr4 0.000(2) 2_775 2_775
F1 Cr1 C1 C5 -81.3(2) . .
F3 Cr1 C1 C5 49.4(4) . .
F2 Cr1 C1 C5 -175.3(2) . .
C2 Cr1 C1 C5 116.3(3) . .
C3 Cr1 C1 C5 79.5(2) . .
C4 Cr1 C1 C5 37.1(2) . .
F1 Cr1 C1 C2 162.4(2) . .
F3 Cr1 C1 C2 -67.0(4) . .
F2 Cr1 C1 C2 68.4(2) . .
C5 Cr1 C1 C2 -116.3(3) . .
C3 Cr1 C1 C2 -36.8(2) . .
C4 Cr1 C1 C2 -79.2(2) . .
F1 Cr1 C1 C6 39.2(4) . .
F3 Cr1 C1 C6 169.8(3) . .
F2 Cr1 C1 C6 -54.9(4) . .
C5 Cr1 C1 C6 120.4(5) . .
C2 Cr1 C1 C6 -123.2(5) . .
C3 Cr1 C1 C6 -160.1(4) . .
C4 Cr1 C1 C6 157.5(4) . .
C5 C1 C2 C3 -1.8(5) . .
C6 C1 C2 C3 176.9(4) . .
Cr1 C1 C2 C3 61.6(3) . .
C5 C1 C2 C7 -179.2(4) . .
C6 C1 C2 C7 -0.5(7) . .
Cr1 C1 C2 C7 -115.7(4) . .
C5 C1 C2 Cr1 -63.4(3) . .
C6 C1 C2 Cr1 115.3(4) . .
F1 Cr1 C2 C3 -143.3(2) . .
F3 Cr1 C2 C3 33.6(3) . .
F2 Cr1 C2 C3 126.4(2) . .
C1 Cr1 C2 C3 -118.1(3) . .
C5 Cr1 C2 C3 -79.8(2) . .
C4 Cr1 C2 C3 -37.7(2) . .
F1 Cr1 C2 C1 -25.2(3) . .
F3 Cr1 C2 C1 151.7(2) . .
F2 Cr1 C2 C1 -115.6(2) . .
C5 Cr1 C2 C1 38.2(2) . .
C3 Cr1 C2 C1 118.1(3) . .
C4 Cr1 C2 C1 80.4(2) . .
F1 Cr1 C2 C7 94.5(4) . .
F3 Cr1 C2 C7 -88.6(4) . .
F2 Cr1 C2 C7 4.2(4) . .
C1 Cr1 C2 C7 119.7(5) . .
C5 Cr1 C2 C7 158.0(4) . .
C3 Cr1 C2 C7 -122.2(5) . .
C4 Cr1 C2 C7 -159.9(4) . .
C1 C2 C3 C4 1.6(5) . .
C7 C2 C3 C4 179.0(4) . .
Cr1 C2 C3 C4 62.3(3) . .
C1 C2 C3 C8 -176.0(4) . .
C7 C2 C3 C8 1.3(7) . .
Cr1 C2 C3 C8 -115.4(4) . .
C1 C2 C3 Cr1 -60.6(3) . .
C7 C2 C3 Cr1 116.7(4) . .
F1 Cr1 C3 C2 88.2(4) . .
F3 Cr1 C3 C2 -154.3(2) . .
F2 Cr1 C3 C2 -58.8(3) . .
C1 Cr1 C3 C2 37.4(2) . .
C5 Cr1 C3 C2 80.2(3) . .
C4 Cr1 C3 C2 117.2(4) . .
F1 Cr1 C3 C4 -29.0(5) . .
F3 Cr1 C3 C4 88.4(2) . .
F2 Cr1 C3 C4 -176.0(2) . .
C1 Cr1 C3 C4 -79.9(3) . .
C5 Cr1 C3 C4 -37.0(2) . .
C2 Cr1 C3 C4 -117.2(4) . .
F1 Cr1 C3 C8 -149.3(3) . .
F3 Cr1 C3 C8 -31.8(3) . .
F2 Cr1 C3 C8 63.7(4) . .
C1 Cr1 C3 C8 159.9(4) . .
C5 Cr1 C3 C8 -157.3(4) . .
C2 Cr1 C3 C8 122.5(4) . .
C4 Cr1 C3 C8 -120.3(4) . .
C2 C3 C4 C5 -0.9(5) . .
C8 C3 C4 C5 176.8(4) . .
Cr1 C3 C4 C5 61.4(3) . .
C2 C3 C4 C9 179.7(4) . .
C8 C3 C4 C9 -2.6(7) . .
Cr1 C3 C4 C9 -118.0(4) . .
C2 C3 C4 Cr1 -62.2(3) . .
C8 C3 C4 Cr1 115.5(4) . .
F1 Cr1 C4 C5 48.6(3) . .
F3 Cr1 C4 C5 147.2(2) . .
F2 Cr1 C4 C5 -110.9(3) . .
C1 Cr1 C4 C5 -37.7(2) . .
C2 Cr1 C4 C5 -80.5(3) . .
C3 Cr1 C4 C5 -117.9(4) . .
F1 Cr1 C4 C3 166.5(2) . .
F3 Cr1 C4 C3 -95.0(2) . .
F2 Cr1 C4 C3 6.9(4) . .
C1 Cr1 C4 C3 80.1(3) . .
C5 Cr1 C4 C3 117.9(4) . .
C2 Cr1 C4 C3 37.4(2) . .
F1 Cr1 C4 C9 -73.5(4) . .
F3 Cr1 C4 C9 25.1(3) . .
F2 Cr1 C4 C9 127.0(3) . .
C1 Cr1 C4 C9 -159.8(4) . .
C5 Cr1 C4 C9 -122.1(5) . .
C2 Cr1 C4 C9 157.4(4) . .
C3 Cr1 C4 C9 120.0(5) . .
C3 C4 C5 C1 -0.2(5) . .
C9 C4 C5 C1 179.2(4) . .
Cr1 C4 C5 C1 61.4(3) . .
C3 C4 C5 C10 -178.8(4) . .
C9 C4 C5 C10 0.6(7) . .
Cr1 C4 C5 C10 -117.1(4) . .
C3 C4 C5 Cr1 -61.7(3) . .
C9 C4 C5 Cr1 117.7(4) . .
C2 C1 C5 C4 1.2(5) . .
C6 C1 C5 C4 -177.5(4) . .
Cr1 C1 C5 C4 -62.5(3) . .
C2 C1 C5 C10 179.8(4) . .
C6 C1 C5 C10 1.1(7) . .
Cr1 C1 C5 C10 116.1(4) . .
C2 C1 C5 Cr1 63.7(3) . .
C6 C1 C5 Cr1 -115.0(4) . .
F1 Cr1 C5 C4 -139.3(2) . .
F3 Cr1 C5 C4 -40.8(3) . .
F2 Cr1 C5 C4 124.9(2) . .
C1 Cr1 C5 C4 117.5(3) . .
C2 Cr1 C5 C4 79.4(3) . .
C3 Cr1 C5 C4 37.3(2) . .
F1 Cr1 C5 C1 103.1(2) . .
F3 Cr1 C5 C1 -158.4(2) . .
F2 Cr1 C5 C1 7.4(3) . .
C2 Cr1 C5 C1 -38.1(2) . .
C3 Cr1 C5 C1 -80.2(3) . .
C4 Cr1 C5 C1 -117.5(3) . .
F1 Cr1 C5 C10 -16.9(3) . .
F3 Cr1 C5 C10 81.6(4) . .
F2 Cr1 C5 C10 -112.7(3) . .
C1 Cr1 C5 C10 -120.1(4) . .
C2 Cr1 C5 C10 -158.2(4) . .
C3 Cr1 C5 C10 159.7(4) . .
C4 Cr1 C5 C10 122.4(5) . .
F2 Cr2 C11 C15 -146.6(3) . .
F5 Cr2 C11 C15 -54.5(3) . .
F4 Cr2 C11 C15 114.6(3) . .
C12 Cr2 C11 C15 117.1(4) . .
C13 Cr2 C11 C15 79.5(3) . .
C14 Cr2 C11 C15 37.1(3) . .
F2 Cr2 C11 C12 96.2(2) . .
F5 Cr2 C11 C12 -171.6(2) . .
F4 Cr2 C11 C12 -2.5(4) . .
C13 Cr2 C11 C12 -37.7(2) . .
C14 Cr2 C11 C12 -80.1(3) . .
C15 Cr2 C11 C12 -117.1(4) . .
F2 Cr2 C11 C16 -23.1(4) . .
F5 Cr2 C11 C16 69.0(4) . .
F4 Cr2 C11 C16 -121.9(4) . .
C12 Cr2 C11 C16 -119.4(5) . .
C13 Cr2 C11 C16 -157.0(4) . .
C14 Cr2 C11 C16 160.6(4) . .
C15 Cr2 C11 C16 123.5(5) . .
C15 C11 C12 C13 -0.2(4) . .
C16 C11 C12 C13 179.0(4) . .
Cr2 C11 C12 C13 63.0(3) . .
C15 C11 C12 C17 178.3(3) . .
C16 C11 C12 C17 -2.6(6) . .
Cr2 C11 C12 C17 -118.5(4) . .
C15 C11 C12 Cr2 -63.2(3) . .
C16 C11 C12 Cr2 116.0(4) . .
F2 Cr2 C12 C13 156.3(2) . .
F5 Cr2 C12 C13 -99.7(4) . .
F4 Cr2 C12 C13 61.7(3) . .
C11 Cr2 C12 C13 -116.9(3) . .
C14 Cr2 C12 C13 -37.1(2) . .
C15 Cr2 C12 C13 -79.4(3) . .
F2 Cr2 C12 C11 -86.8(2) . .
F5 Cr2 C12 C11 17.2(4) . .
F4 Cr2 C12 C11 178.6(2) . .
C13 Cr2 C12 C11 116.9(3) . .
C14 Cr2 C12 C11 79.7(3) . .
C15 Cr2 C12 C11 37.4(2) . .
F2 Cr2 C12 C17 32.8(4) . .
F5 Cr2 C12 C17 136.9(4) . .
F4 Cr2 C12 C17 -61.8(4) . .
C11 Cr2 C12 C17 119.7(5) . .
C13 Cr2 C12 C17 -123.5(5) . .
C14 Cr2 C12 C17 -160.6(5) . .
C15 Cr2 C12 C17 157.1(5) . .
C11 C12 C13 C14 -1.0(4) . .
C17 C12 C13 C14 -179.4(4) . .
Cr2 C12 C13 C14 61.8(3) . .
C11 C12 C13 C18 -177.5(4) . .
C17 C12 C13 C18 4.1(6) . .
Cr2 C12 C13 C18 -114.7(4) . .
C11 C12 C13 Cr2 -62.8(3) . .
C17 C12 C13 Cr2 118.8(4) . .
F2 Cr2 C13 C12 -31.3(3) . .
F5 Cr2 C13 C12 138.5(2) . .
F4 Cr2 C13 C12 -124.2(2) . .
C11 Cr2 C13 C12 38.1(2) . .
C14 Cr2 C13 C12 118.1(4) . .
C15 Cr2 C13 C12 80.4(3) . .
F2 Cr2 C13 C14 -149.4(2) . .
F5 Cr2 C13 C14 20.4(3) . .
F4 Cr2 C13 C14 117.7(2) . .
C12 Cr2 C13 C14 -118.1(4) . .
C11 Cr2 C13 C14 -80.0(3) . .
C15 Cr2 C13 C14 -37.7(2) . .
F2 Cr2 C13 C18 90.5(4) . .
F5 Cr2 C13 C18 -99.7(4) . .
F4 Cr2 C13 C18 -2.4(4) . .
C12 Cr2 C13 C18 121.8(5) . .
C11 Cr2 C13 C18 159.9(4) . .
C14 Cr2 C13 C18 -120.1(5) . .
C15 Cr2 C13 C18 -157.7(4) . .
C12 C13 C14 C15 1.8(4) . .
C18 C13 C14 C15 178.4(3) . .
Cr2 C13 C14 C15 63.1(3) . .
C12 C13 C14 C19 178.5(4) . .
C18 C13 C14 C19 -4.8(6) . .
Cr2 C13 C14 C19 -120.2(4) . .
C12 C13 C14 Cr2 -61.3(3) . .
C18 C13 C14 Cr2 115.3(4) . .
F2 Cr2 C14 C13 71.0(4) . .
F5 Cr2 C14 C13 -166.5(2) . .
F4 Cr2 C14 C13 -67.5(2) . .
C12 Cr2 C14 C13 37.1(2) . .
C11 Cr2 C14 C13 79.9(3) . .
C15 Cr2 C14 C13 117.0(3) . .
F2 Cr2 C14 C15 -46.0(5) . .
F5 Cr2 C14 C15 76.5(2) . .
F4 Cr2 C14 C15 175.5(2) . .
C12 Cr2 C14 C15 -79.9(3) . .
C11 Cr2 C14 C15 -37.1(2) . .
C13 Cr2 C14 C15 -117.0(3) . .
F2 Cr2 C14 C19 -167.4(3) . .
F5 Cr2 C14 C19 -44.9(4) . .
F4 Cr2 C14 C19 54.1(4) . .
C12 Cr2 C14 C19 158.7(5) . .
C11 Cr2 C14 C19 -158.5(5) . .
C13 Cr2 C14 C19 121.6(5) . .
C15 Cr2 C14 C19 -121.5(5) . .
C12 C11 C15 C14 1.2(4) . .
C16 C11 C15 C14 -177.9(4) . .
Cr2 C11 C15 C14 -60.7(3) . .
C12 C11 C15 C20 -180.0(4) . .
C16 C11 C15 C20 0.9(7) . .
Cr2 C11 C15 C20 118.1(4) . .
C12 C11 C15 Cr2 61.9(3) . .
C16 C11 C15 Cr2 -117.2(4) . .
C13 C14 C15 C11 -1.8(4) . .
C19 C14 C15 C11 -178.7(4) . .
Cr2 C14 C15 C11 60.5(3) . .
C13 C14 C15 C20 179.3(4) . .
C19 C14 C15 C20 2.5(6) . .
Cr2 C14 C15 C20 -118.4(4) . .
C13 C14 C15 Cr2 -62.3(3) . .
C19 C14 C15 Cr2 120.9(4) . .
F2 Cr2 C15 C11 41.0(3) . .
F5 Cr2 C15 C11 133.3(3) . .
F4 Cr2 C15 C11 -125.4(3) . .
C12 Cr2 C15 C11 -37.9(3) . .
C13 Cr2 C15 C11 -80.4(3) . .
C14 Cr2 C15 C11 -118.1(4) . .
F2 Cr2 C15 C14 159.2(2) . .
F5 Cr2 C15 C14 -108.6(2) . .
F4 Cr2 C15 C14 -7.3(4) . .
C12 Cr2 C15 C14 80.2(3) . .
C11 Cr2 C15 C14 118.1(4) . .
C13 Cr2 C15 C14 37.8(2) . .
F2 Cr2 C15 C20 -81.1(4) . .
F5 Cr2 C15 C20 11.2(4) . .
F4 Cr2 C15 C20 112.5(4) . .
C12 Cr2 C15 C20 -160.0(4) . .
C11 Cr2 C15 C20 -122.1(5) . .
C13 Cr2 C15 C20 157.5(4) . .
C14 Cr2 C15 C20 119.8(5) . .
F7 Cr3 C21 C25 -141.5(2) . .
F3 Cr3 C21 C25 32.0(3) . .
F6 Cr3 C21 C25 126.2(3) . .
C22 Cr3 C21 C25 -118.1(4) . .
C23 Cr3 C21 C25 -79.6(3) . .
C24 Cr3 C21 C25 -37.2(2) . .
F7 Cr3 C21 C22 -23.5(4) . .
F3 Cr3 C21 C22 150.0(3) . .
F6 Cr3 C21 C22 -115.8(3) . .
C23 Cr3 C21 C22 38.5(3) . .
C24 Cr3 C21 C22 80.9(3) . .
C25 Cr3 C21 C22 118.1(4) . .
F7 Cr3 C21 C26 97.0(6) . .
F3 Cr3 C21 C26 -89.5(6) . .
F6 Cr3 C21 C26 4.7(6) . .
C22 Cr3 C21 C26 120.4(7) . .
C23 Cr3 C21 C26 158.9(7) . .
C24 Cr3 C21 C26 -158.7(7) . .
C25 Cr3 C21 C26 -121.5(7) . .
C25 C21 C22 C23 -2.5(5) . .
C26 C21 C22 C23 178.3(5) . .
Cr3 C21 C22 C23 -64.2(3) . .
C25 C21 C22 C27 175.4(5) . .
C26 C21 C22 C27 -3.9(8) . .
Cr3 C21 C22 C27 113.6(5) . .
C25 C21 C22 Cr3 61.8(3) . .
C26 C21 C22 Cr3 -117.5(5) . .
F7 Cr3 C22 C23 -80.7(3) . .
F3 Cr3 C22 C23 47.0(6) . .
F6 Cr3 C22 C23 -176.3(2) . .
C24 Cr3 C22 C23 36.8(2) . .
C21 Cr3 C22 C23 115.5(4) . .
C25 Cr3 C22 C23 78.6(3) . .
F7 Cr3 C22 C21 163.8(3) . .
F3 Cr3 C22 C21 -68.5(5) . .
F6 Cr3 C22 C21 68.2(3) . .
C23 Cr3 C22 C21 -115.5(4) . .
C24 Cr3 C22 C21 -78.7(3) . .
C25 Cr3 C22 C21 -36.9(3) . .
F7 Cr3 C22 C27 39.8(6) . .
F3 Cr3 C22 C27 167.5(5) . .
F6 Cr3 C22 C27 -55.8(6) . .
C23 Cr3 C22 C27 120.5(7) . .
C24 Cr3 C22 C27 157.3(6) . .
C21 Cr3 C22 C27 -124.0(7) . .
C25 Cr3 C22 C27 -160.9(6) . .
C21 C22 C23 C24 2.7(5) . .
C27 C22 C23 C24 -175.2(4) . .
Cr3 C22 C23 C24 -61.7(3) . .
C21 C22 C23 C28 179.0(4) . .
C27 C22 C23 C28 1.1(8) . .
Cr3 C22 C23 C28 114.5(5) . .
C21 C22 C23 Cr3 64.5(3) . .
C27 C22 C23 Cr3 -113.5(5) . .
F7 Cr3 C23 C22 103.9(3) . .
F3 Cr3 C23 C22 -158.6(3) . .
F6 Cr3 C23 C22 5.7(4) . .
C24 Cr3 C23 C22 -118.3(4) . .
C21 Cr3 C23 C22 -38.6(3) . .
C25 Cr3 C23 C22 -80.9(3) . .
F7 Cr3 C23 C24 -137.8(3) . .
F3 Cr3 C23 C24 -40.3(3) . .
F6 Cr3 C23 C24 124.1(3) . .
C22 Cr3 C23 C24 118.3(4) . .
C21 Cr3 C23 C24 79.8(3) . .
C25 Cr3 C23 C24 37.4(3) . .
F7 Cr3 C23 C28 -16.3(5) . .
F3 Cr3 C23 C28 81.2(4) . .
F6 Cr3 C23 C28 -114.5(5) . .
C22 Cr3 C23 C28 -120.2(5) . .
C24 Cr3 C23 C28 121.5(6) . .
C21 Cr3 C23 C28 -158.8(5) . .
C25 Cr3 C23 C28 158.9(5) . .
C22 C23 C24 C25 -1.9(5) . .
C28 C23 C24 C25 -178.2(4) . .
Cr3 C23 C24 C25 -62.8(3) . .
C22 C23 C24 C29 179.7(4) . .
C28 C23 C24 C29 3.5(7) . .
Cr3 C23 C24 C29 118.8(5) . .
C22 C23 C24 Cr3 60.9(3) . .
C28 C23 C24 Cr3 -115.3(5) . .
F7 Cr3 C24 C25 167.3(2) . .
F3 Cr3 C24 C25 -95.8(3) . .
F6 Cr3 C24 C25 6.0(4) . .
C22 Cr3 C24 C25 80.0(3) . .
C23 Cr3 C24 C25 117.0(4) . .
C21 Cr3 C24 C25 37.3(3) . .
F7 Cr3 C24 C23 50.3(3) . .
F3 Cr3 C24 C23 147.2(3) . .
F6 Cr3 C24 C23 -111.0(3) . .
C22 Cr3 C24 C23 -37.0(3) . .
C21 Cr3 C24 C23 -79.6(3) . .
C25 Cr3 C24 C23 -117.0(4) . .
F7 Cr3 C24 C29 -71.1(5) . .
F3 Cr3 C24 C29 25.8(4) . .
F6 Cr3 C24 C29 127.6(4) . .
C22 Cr3 C24 C29 -158.4(5) . .
C23 Cr3 C24 C29 -121.4(6) . .
C21 Cr3 C24 C29 159.0(5) . .
C25 Cr3 C24 C29 121.6(5) . .
C23 C24 C25 C21 0.4(5) . .
C29 C24 C25 C21 178.7(4) . .
Cr3 C24 C25 C21 -62.0(3) . .
C23 C24 C25 C30 178.0(4) . .
C29 C24 C25 C30 -3.7(7) . .
Cr3 C24 C25 C30 115.6(5) . .
C23 C24 C25 Cr3 62.4(3) . .
C29 C24 C25 Cr3 -119.3(4) . .
C22 C21 C25 C24 1.3(5) . .
C26 C21 C25 C24 -179.5(5) . .
Cr3 C21 C25 C24 61.9(3) . .
C22 C21 C25 C30 -176.3(4) . .
C26 C21 C25 C30 3.0(8) . .
Cr3 C21 C25 C30 -115.6(5) . .
C22 C21 C25 Cr3 -60.7(3) . .
C26 C21 C25 Cr3 118.6(5) . .
F7 Cr3 C25 C24 -26.5(5) . .
F3 Cr3 C25 C24 87.0(3) . .
F6 Cr3 C25 C24 -176.5(2) . .
C22 Cr3 C25 C24 -80.3(3) . .
C23 Cr3 C25 C24 -37.7(3) . .
C21 Cr3 C25 C24 -117.5(4) . .
F7 Cr3 C25 C21 91.0(5) . .
F3 Cr3 C25 C21 -155.5(3) . .
F6 Cr3 C25 C21 -58.9(3) . .
C22 Cr3 C25 C21 37.3(3) . .
C23 Cr3 C25 C21 79.8(3) . .
C24 Cr3 C25 C21 117.5(4) . .
F7 Cr3 C25 C30 -147.3(5) . .
F3 Cr3 C25 C30 -33.8(5) . .
F6 Cr3 C25 C30 62.7(6) . .
C22 Cr3 C25 C30 159.0(6) . .
C23 Cr3 C25 C30 -158.5(6) . .
C24 Cr3 C25 C30 -120.8(7) . .
C21 Cr3 C25 C30 121.7(6) . .
C37 C32 C33 C34 0.0 . .
C31 C32 C33 C34 177.6(12) . .
C32 C33 C34 C35 0.0 . .
C33 C34 C35 C36 0.0 . .
C34 C35 C36 C37 0.0 . .
C35 C36 C37 C32 0.0 . .
C33 C32 C37 C36 0.0 . .
C31 C32 C37 C36 -177.5(12) . .
C37A C32A C33A C34A 0.0 . .
C31A C32A C33A C34A -176.5(14) . .
C32A C33A C34A C35A 0.0 . .
C33A C34A C35A C36A 0.0 . .
C34A C35A C36A C37A 0.0 . .
C35A C36A C37A C32A 0.0 . .
C33A C32A C37A C36A 0.0 . .
C31A C32A C37A C36A 175.8(16) . .
C44 C39 C40 C41 0.0 . .
C38 C39 C40 C41 178.7(9) . .
C39 C40 C41 C42 0.0 . .
C40 C41 C42 C43 0.0 . .
C41 C42 C43 C44 0.0 . .
C42 C43 C44 C39 0.0 . .
C40 C39 C44 C43 0.0 . .
C38 C39 C44 C43 -178.7(9) . .
C44A C39A C40A C41A 0.0 . .
C38A C39A C40A C41A -177.7(10) . .
C39A C40A C41A C42A 0.0 . .
C40A C41A C42A C43A 0.0 . .
C41A C42A C43A C44A 0.0 . .
C42A C43A C44A C39A 0.0 . .
C40A C39A C44A C43A 0.0 . .
C38A C39A C44A C43A 177.7(10) . .
