#------------------------------------------------------------------------------
#$Date: 2016-03-21 09:25:51 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178623 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/34/4073495.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4073495
loop_
_publ_author_name
'McGlacken, Gerard P.'
'O'Brien, Ciara T.'
'Whitwood, Adrian C.'
'Fairlamb, Ian J. S.'
_publ_section_title
;
 Chiral Mono- and Bis-annelated Cyclopentadienyl Ligands Derived from
 Tartaric Acid:  Synthesis of [(η5-Cyclopentadienyl)RuCl(cod)] and
 [(η5-Cyclopentadienyl)(η6-benzene)Ru]PF6Derivatives
;
_journal_issue                   15
_journal_name_full               Organometallics
_journal_page_first              3722
_journal_paper_doi               10.1021/om700393b
_journal_volume                  26
_journal_year                    2007
_chemical_absolute_configuration ad
_chemical_formula_moiety         '2(C18 H21 O2 Ru), C H2 Cl2, 2(F6 P)'
_chemical_formula_sum            'C37 H44 Cl2 F12 O4 P2 Ru2'
_chemical_formula_weight         1115.70
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           3
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'P 2y'
_symmetry_space_group_name_H-M   'P 1 2 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 110.3650(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   23.2056(11)
_cell_length_b                   8.1184(4)
_cell_length_c                   23.2436(11)
_cell_measurement_reflns_used    8909
_cell_measurement_temperature    115(2)
_cell_measurement_theta_max      28.19
_cell_measurement_theta_min      2.51
_cell_volume                     4105.2(3)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      115(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0290
_diffrn_reflns_av_sigmaI/netI    0.0478
_diffrn_reflns_limit_h_max       30
_diffrn_reflns_limit_h_min       -30
_diffrn_reflns_limit_k_max       10
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            42845
_diffrn_reflns_theta_full        28.30
_diffrn_reflns_theta_max         28.30
_diffrn_reflns_theta_min         0.93
_exptl_absorpt_coefficient_mu    1.038
_exptl_absorpt_correction_T_max  0.94
_exptl_absorpt_correction_T_min  0.811
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS v2.03; (Sheldrick)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.805
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       needle
_exptl_crystal_F_000             2232
_exptl_crystal_size_max          0.20
_exptl_crystal_size_mid          0.13
_exptl_crystal_size_min          0.06
_refine_diff_density_max         1.532
_refine_diff_density_min         -0.592
_refine_diff_density_rms         0.117
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.05(4)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.029
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1082
_refine_ls_number_reflns         20334
_refine_ls_number_restraints     1
_refine_ls_restrained_S_all      1.029
_refine_ls_R_factor_all          0.0710
_refine_ls_R_factor_gt           0.0493
_refine_ls_shift/su_max          0.013
_refine_ls_shift/su_mean         0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0505P)²+9.3495P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1157
_refine_ls_wR_factor_ref         0.1264
_reflns_number_gt                15022
_reflns_number_total             20334
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om700393b-file005.cif
_cod_data_source_block           ijf0501m
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      P2
_cod_database_code               4073495
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.2392(4) 0.1856(10) 0.9832(4) 0.0188(16) Uani 1 1 d .
H1 H 0.2403 0.0687 0.9850 0.023 Uiso 1 1 calc R
C2 C 0.1820(4) 0.2701(10) 0.9656(4) 0.0214(19) Uani 1 1 d .
H2 H 0.1448 0.2094 0.9551 0.026 Uiso 1 1 calc R
C3 C 0.1805(4) 0.4454(10) 0.9638(4) 0.0195(18) Uani 1 1 d .
H3 H 0.1424 0.5023 0.9528 0.023 Uiso 1 1 calc R
C4 C 0.2368(4) 0.5349(10) 0.9786(4) 0.0227(19) Uani 1 1 d .
H4 H 0.2362 0.6517 0.9762 0.027 Uiso 1 1 calc R
C5 C 0.2940(4) 0.4487(9) 0.9970(4) 0.0229(19) Uani 1 1 d .
H5 H 0.3317 0.5075 1.0086 0.027 Uiso 1 1 calc R
C6 C 0.2936(4) 0.2749(9) 0.9977(4) 0.0193(17) Uani 1 1 d .
H6 H 0.3315 0.2173 1.0083 0.023 Uiso 1 1 calc R
C7 C 0.2326(3) 0.1933(9) 0.8282(3) 0.0179(14) Uani 1 1 d .
C8 C 0.1787(4) 0.2749(11) 0.8129(4) 0.033(2) Uani 1 1 d .
H8 H 0.1400 0.2209 0.8016 0.039 Uiso 1 1 calc R
C9 C 0.1849(5) 0.4440(11) 0.8153(4) 0.036(2) Uani 1 1 d .
H9 H 0.1532 0.5241 0.8070 0.043 Uiso 1 1 calc R
C10 C 0.2537(3) 0.4743(10) 0.8340(3) 0.0229(16) Uani 1 1 d .
H10 H 0.2742 0.5775 0.8398 0.027 Uiso 1 1 calc R
C11 C 0.2812(3) 0.3106(7) 0.8410(3) 0.0152(13) Uani 1 1 d .
C12 C 0.3469(3) 0.2710(9) 0.8559(3) 0.0207(15) Uani 1 1 d .
H12A H 0.3729 0.3415 0.8898 0.025 Uiso 1 1 calc R
H12B H 0.3594 0.2876 0.8197 0.025 Uiso 1 1 calc R
C13 C 0.3533(3) 0.0899(7) 0.8752(3) 0.0258(13) Uani 1 1 d .
H13 H 0.3492 0.0755 0.9163 0.031 Uiso 1 1 calc R
C14 C 0.3064(3) -0.0112(9) 0.8271(3) 0.0298(14) Uani 1 1 d .
H14 H 0.3065 0.0194 0.7855 0.036 Uiso 1 1 calc R
C15 C 0.2423(3) 0.0095(9) 0.8296(3) 0.0251(15) Uani 1 1 d .
H15A H 0.2113 -0.0440 0.7939 0.030 Uiso 1 1 calc R
H15B H 0.2397 -0.0387 0.8677 0.030 Uiso 1 1 calc R
C16 C 0.3980(3) -0.1563(12) 0.8633(3) 0.0220(14) Uani 1 1 d .
C17 C 0.4189(4) -0.1953(18) 0.8121(4) 0.089(5) Uani 1 1 d .
H17A H 0.3887 -0.1548 0.7737 0.133 Uiso 1 1 calc R
H17B H 0.4232 -0.3149 0.8095 0.133 Uiso 1 1 calc R
H17C H 0.4587 -0.1423 0.8188 0.133 Uiso 1 1 calc R
C18 C 0.4251(4) -0.2509(11) 0.9222(4) 0.039(2) Uani 1 1 d .
H18A H 0.4700 -0.2486 0.9352 0.059 Uiso 1 1 calc R
H18B H 0.4108 -0.3653 0.9158 0.059 Uiso 1 1 calc R
H18C H 0.4121 -0.2005 0.9540 0.059 Uiso 1 1 calc R
O1 O 0.4097(2) 0.0190(7) 0.8742(3) 0.0317(13) Uani 1 1 d .
O2 O 0.3313(2) -0.1714(8) 0.84289(19) 0.0259(11) Uani 1 1 d .
Ru1 Ru 0.23226(2) 0.35268(7) 0.905930(19) 0.01623(11) Uani 1 1 d .
C19 C 0.2059(4) 0.4354(9) 0.5046(4) 0.0218(18) Uani 1 1 d .
H19 H 0.1681 0.4942 0.4916 0.026 Uiso 1 1 calc R
C20 C 0.2069(4) 0.2614(10) 0.5070(4) 0.0208(18) Uani 1 1 d .
H20 H 0.1694 0.2027 0.4981 0.025 Uiso 1 1 calc R
C21 C 0.2617(4) 0.1747(9) 0.5222(4) 0.0217(18) Uani 1 1 d .
H21 H 0.2612 0.0576 0.5217 0.026 Uiso 1 1 calc R
C22 C 0.3181(4) 0.2594(12) 0.5383(4) 0.027(2) Uani 1 1 d .
H22 H 0.3556 0.1997 0.5492 0.032 Uiso 1 1 calc R
C23 C 0.3187(4) 0.4338(11) 0.5381(4) 0.0223(19) Uani 1 1 d .
H23 H 0.3566 0.4911 0.5487 0.027 Uiso 1 1 calc R
C24 C 0.2641(4) 0.5212(10) 0.5226(4) 0.0212(18) Uani 1 1 d .
H24 H 0.2649 0.6381 0.5239 0.025 Uiso 1 1 calc R
C25 C 0.2182(3) 0.3625(11) 0.6615(3) 0.0267(15) Uani 1 1 d .
C26 C 0.2480(5) 0.2172(10) 0.6708(4) 0.037(2) Uani 1 1 d .
H26 H 0.2286 0.1125 0.6662 0.044 Uiso 1 1 calc R
C27 C 0.3098(4) 0.2412(8) 0.6877(3) 0.0177(14) Uani 1 1 d .
H27 H 0.3397 0.1562 0.6965 0.021 Uiso 1 1 calc R
C28 C 0.3227(3) 0.4142(9) 0.6903(3) 0.0178(15) Uani 1 1 d .
H28 H 0.3616 0.4664 0.7001 0.021 Uiso 1 1 calc R
C29 C 0.2625(4) 0.4916(9) 0.6744(4) 0.030(2) Uani 1 1 d .
C30 C 0.2552(3) 0.6817(9) 0.6763(3) 0.0255(16) Uani 1 1 d .
H30A H 0.2658 0.7211 0.7190 0.031 Uiso 1 1 calc R
H30B H 0.2817 0.7384 0.6571 0.031 Uiso 1 1 calc R
C31 C 0.1884(3) 0.7108(7) 0.6402(3) 0.0256(13) Uani 1 1 d .
H31 H 0.1801 0.6954 0.5953 0.031 Uiso 1 1 calc R
C32 C 0.1468(3) 0.6012(7) 0.6612(3) 0.0260(13) Uani 1 1 d .
H32 H 0.1587 0.6093 0.7068 0.031 Uiso 1 1 calc R
C33 C 0.1493(3) 0.4184(10) 0.6429(4) 0.0312(18) Uani 1 1 d .
H33A H 0.1283 0.4054 0.5981 0.037 Uiso 1 1 calc R
H33B H 0.1278 0.3487 0.6640 0.037 Uiso 1 1 calc R
C34 C 0.1006(3) 0.8502(10) 0.6353(2) 0.0165(11) Uani 1 1 d .
C35 C 0.0812(3) 0.9245(7) 0.6862(3) 0.0199(13) Uani 1 1 d .
H35A H 0.1011 0.8639 0.7245 0.030 Uiso 1 1 calc R
H35B H 0.0365 0.9168 0.6747 0.030 Uiso 1 1 calc R
H35C H 0.0937 1.0404 0.6921 0.030 Uiso 1 1 calc R
C36 C 0.0668(4) 0.9213(12) 0.5739(3) 0.042(2) Uani 1 1 d .
H36A H 0.0746 1.0401 0.5745 0.063 Uiso 1 1 calc R
H36B H 0.0226 0.9021 0.5634 0.063 Uiso 1 1 calc R
H36C H 0.0807 0.8687 0.5431 0.063 Uiso 1 1 calc R
O3 O 0.16672(19) 0.8667(7) 0.65124(19) 0.0246(10) Uani 1 1 d .
O4 O 0.0880(2) 0.6770(7) 0.6326(2) 0.0261(11) Uani 1 1 d .
Ru2 Ru 0.26717(2) 0.34854(6) 0.597020(19) 0.01418(10) Uani 1 1 d .
C37 C 0.0180(4) 0.5328(10) 0.2625(4) 0.0228(19) Uani 1 1 d .
H37 H 0.0170 0.6498 0.2624 0.027 Uiso 1 1 calc R
C38 C 0.0350(4) 0.4433(10) 0.3204(4) 0.0171(16) Uani 1 1 d .
H38 H 0.0458 0.4983 0.3588 0.021 Uiso 1 1 calc R
C39 C 0.0345(4) 0.2727(11) 0.3159(4) 0.026(2) Uani 1 1 d .
H39 H 0.0451 0.2114 0.3530 0.031 Uiso 1 1 calc R
C40 C 0.0198(4) 0.1853(10) 0.2617(4) 0.0222(18) Uani 1 1 d .
H40 H 0.0207 0.0683 0.2619 0.027 Uiso 1 1 calc R
C41 C 0.0034(4) 0.2733(9) 0.2064(4) 0.0206(18) Uani 1 1 d .
H41 H -0.0075 0.2163 0.1684 0.025 Uiso 1 1 calc R
C42 C 0.0032(4) 0.4473(10) 0.2075(4) 0.0236(19) Uani 1 1 d .
H42 H -0.0073 0.5067 0.1700 0.028 Uiso 1 1 calc R
C43 C 0.1720(4) 0.5130(10) 0.2655(4) 0.030(2) Uani 1 1 d .
C44 C 0.1887(4) 0.4289(9) 0.3246(4) 0.0232(18) Uani 1 1 d .
H44 H 0.2001 0.4795 0.3638 0.028 Uiso 1 1 calc R
C45 C 0.1844(4) 0.2550(9) 0.3121(4) 0.0235(18) Uani 1 1 d .
H45 H 0.1921 0.1693 0.3416 0.028 Uiso 1 1 calc R
C46 C 0.1671(4) 0.2349(11) 0.2486(4) 0.040(3) Uani 1 1 d .
H46 H 0.1606 0.1325 0.2276 0.048 Uiso 1 1 calc R
C47 C 0.1605(3) 0.3948(12) 0.2203(3) 0.032(2) Uani 1 1 d .
C48 C 0.1443(3) 0.4412(8) 0.1533(3) 0.0169(13) Uani 1 1 d .
H48A H 0.1801 0.4240 0.1402 0.020 Uiso 1 1 calc R
H48B H 0.1099 0.3721 0.1273 0.020 Uiso 1 1 calc R
C49 C 0.1257(3) 0.6212(7) 0.1467(3) 0.0231(12) Uani 1 1 d .
H49 H 0.0846 0.6355 0.1511 0.028 Uiso 1 1 calc R
C50 C 0.1741(3) 0.7246(7) 0.1944(3) 0.0245(12) Uani 1 1 d .
H50 H 0.2157 0.6952 0.1940 0.029 Uiso 1 1 calc R
C51 C 0.1727(3) 0.6999(10) 0.2580(3) 0.0276(16) Uani 1 1 d .
H51A H 0.1356 0.7505 0.2620 0.033 Uiso 1 1 calc R
H51B H 0.2096 0.7488 0.2890 0.033 Uiso 1 1 calc R
C52 C 0.1371(3) 0.8665(11) 0.1023(3) 0.0213(14) Uani 1 1 d .
C53 C 0.1875(4) 0.9162(14) 0.0801(4) 0.050(3) Uani 1 1 d .
H53A H 0.1989 1.0309 0.0917 0.075 Uiso 1 1 calc R
H53B H 0.1735 0.9056 0.0354 0.075 Uiso 1 1 calc R
H53C H 0.2232 0.8449 0.0987 0.075 Uiso 1 1 calc R
C54 C 0.0784(4) 0.9638(11) 0.0753(4) 0.040(2) Uani 1 1 d .
H54A H 0.0475 0.9216 0.0915 0.060 Uiso 1 1 calc R
H54B H 0.0632 0.9529 0.0305 0.060 Uiso 1 1 calc R
H54C H 0.0865 1.0802 0.0865 0.060 Uiso 1 1 calc R
O5 O 0.1260(2) 0.6939(7) 0.0907(2) 0.0301(12) Uani 1 1 d .
O6 O 0.1580(2) 0.8846(7) 0.16911(19) 0.0272(12) Uani 1 1 d .
Ru3 Ru 0.09427(2) 0.36347(5) 0.267538(19) 0.01451(13) Uani 1 1 d .
C55 C 0.4957(4) 0.2578(9) 0.2943(4) 0.0169(16) Uani 1 1 d .
H55 H 0.5075 0.1991 0.3320 0.020 Uiso 1 1 calc R
C56 C 0.4945(4) 0.4322(10) 0.2940(4) 0.0240(19) Uani 1 1 d .
H56 H 0.5045 0.4908 0.3316 0.029 Uiso 1 1 calc R
C57 C 0.4784(4) 0.5202(10) 0.2373(4) 0.0223(19) Uani 1 1 d .
H57 H 0.4781 0.6372 0.2376 0.027 Uiso 1 1 calc R
C58 C 0.4627(4) 0.4334(11) 0.1800(4) 0.0191(17) Uani 1 1 d .
H58 H 0.4523 0.4891 0.1417 0.023 Uiso 1 1 calc R
C59 C 0.4638(4) 0.2558(11) 0.1843(4) 0.024(2) Uani 1 1 d .
H59 H 0.4530 0.1943 0.1473 0.029 Uiso 1 1 calc R
C60 C 0.4792(4) 0.1716(9) 0.2378(4) 0.0208(18) Uani 1 1 d .
H60 H 0.4790 0.0546 0.2375 0.025 Uiso 1 1 calc R
C61 C 0.3389(3) 0.3177(9) 0.2817(3) 0.0194(15) Uani 1 1 d .
C62 C 0.3316(3) 0.4769(9) 0.2536(3) 0.0205(16) Uani 1 1 d .
H62 H 0.3377 0.5805 0.2738 0.025 Uiso 1 1 calc R
C63 C 0.3133(4) 0.4489(11) 0.1882(5) 0.033(2) Uani 1 1 d .
H63 H 0.3046 0.5311 0.1572 0.040 Uiso 1 1 calc R
C64 C 0.3107(4) 0.2790(12) 0.1789(4) 0.031(2) Uani 1 1 d .
H64 H 0.3007 0.2274 0.1400 0.037 Uiso 1 1 calc R
C65 C 0.3243(3) 0.1977(10) 0.2325(3) 0.0204(16) Uani 1 1 d .
C66 C 0.3237(4) 0.0121(9) 0.2442(3) 0.0250(16) Uani 1 1 d .
H66A H 0.2810 -0.0278 0.2339 0.030 Uiso 1 1 calc R
H66B H 0.3431 -0.0485 0.2187 0.030 Uiso 1 1 calc R
C67 C 0.3597(3) -0.0137(7) 0.3116(3) 0.0229(12) Uani 1 1 d .
H67 H 0.4047 0.0010 0.3201 0.028 Uiso 1 1 calc R
C68 C 0.3387(3) 0.0963(7) 0.3518(3) 0.0228(12) Uani 1 1 d .
H68 H 0.2929 0.0889 0.3393 0.027 Uiso 1 1 calc R
C69 C 0.3575(4) 0.2815(10) 0.3500(3) 0.0302(18) Uani 1 1 d .
H69A H 0.3352 0.3537 0.3695 0.036 Uiso 1 1 calc R
H69B H 0.4023 0.2967 0.3711 0.036 Uiso 1 1 calc R
C70 C 0.3643(3) -0.1560(11) 0.3985(2) 0.0176(12) Uani 1 1 d .
C71 C 0.3135(3) -0.2282(10) 0.4175(3) 0.0263(16) Uani 1 1 d .
H71A H 0.2747 -0.1722 0.3953 0.039 Uiso 1 1 calc R
H71B H 0.3235 -0.2131 0.4618 0.039 Uiso 1 1 calc R
H71C H 0.3094 -0.3460 0.4078 0.039 Uiso 1 1 calc R
C72 C 0.4267(4) -0.2195(12) 0.4333(4) 0.045(2) Uani 1 1 d .
H72A H 0.4276 -0.3390 0.4279 0.068 Uiso 1 1 calc R
H72B H 0.4371 -0.1942 0.4770 0.068 Uiso 1 1 calc R
H72C H 0.4567 -0.1671 0.4181 0.068 Uiso 1 1 calc R
O7 O 0.3481(2) -0.1676(8) 0.33318(18) 0.0235(10) Uani 1 1 d .
O8 O 0.3660(2) 0.0213(7) 0.4107(2) 0.0281(12) Uani 1 1 d .
Ru4 Ru 0.40394(2) 0.34557(6) 0.232560(19) 0.01536(14) Uani 1 1 d .
F1 F 0.15192(16) 0.8633(8) 0.91995(17) 0.0342(10) Uani 1 1 d .
F2 F 0.0650(3) 0.7288(7) 0.9164(3) 0.0416(15) Uani 1 1 d .
F3 F 0.0975(3) 0.7205(7) 0.8361(3) 0.0407(15) Uani 1 1 d .
F4 F 0.0974(2) 0.9946(6) 0.8328(2) 0.0289(12) Uani 1 1 d .
F5 F 0.0652(3) 1.0085(7) 0.9133(3) 0.0375(14) Uani 1 1 d .
F6 F 0.01137(16) 0.8561(8) 0.82995(16) 0.0291(9) Uani 1 1 d .
P1 P 0.08154(7) 0.8608(3) 0.87503(7) 0.0185(3) Uani 1 1 d .
F7 F 0.4019(3) 0.7064(7) 0.6678(3) 0.0335(13) Uani 1 1 d .
F8 F 0.48855(15) 0.8394(8) 0.67232(16) 0.0267(9) Uani 1 1 d .
F9 F 0.4027(3) 0.9886(6) 0.6650(2) 0.0328(13) Uani 1 1 d .
F10 F 0.34890(16) 0.8411(7) 0.58003(16) 0.0315(9) Uani 1 1 d .
F11 F 0.4349(2) 0.6989(5) 0.5870(2) 0.0264(11) Uani 1 1 d .
F12 F 0.4357(3) 0.9775(6) 0.5846(3) 0.0345(13) Uani 1 1 d .
P2 P 0.41870(7) 0.8422(3) 0.62582(7) 0.0162(3) Uani 1 1 d .
F13 F 0.17088(16) 0.8484(7) 0.48836(14) 0.0271(9) Uani 1 1 d .
F14 F 0.0816(3) 0.7258(6) 0.4341(3) 0.0410(15) Uani 1 1 d .
F15 F 0.0882(2) 1.0025(6) 0.4341(2) 0.0294(12) Uani 1 1 d .
F16 F 0.1700(3) 0.9816(6) 0.4025(3) 0.0361(13) Uani 1 1 d .
F17 F 0.1633(3) 0.7061(6) 0.4027(2) 0.0318(12) Uani 1 1 d .
F18 F 0.08095(17) 0.8582(7) 0.34830(15) 0.0338(10) Uani 1 1 d .
P3 P 0.12597(7) 0.8535(3) 0.41852(6) 0.0171(3) Uani 1 1 d .
F19 F 0.41947(18) 0.8430(8) 0.15201(16) 0.0370(11) Uani 1 1 d .
F20 F 0.4100(2) 0.6983(6) 0.0656(2) 0.0322(12) Uani 1 1 d .
F21 F 0.3287(2) 0.7256(6) 0.0963(2) 0.0301(12) Uani 1 1 d .
F22 F 0.3392(2) 1.0052(6) 0.0980(2) 0.0298(12) Uani 1 1 d .
F23 F 0.4202(3) 0.9793(7) 0.0658(3) 0.0382(13) Uani 1 1 d .
F24 F 0.33005(17) 0.8604(8) 0.01144(14) 0.0301(10) Uani 1 1 d .
P4 P 0.37529(7) 0.8524(3) 0.08185(6) 0.0184(3) Uani 1 1 d .
C73A C 0.0000 0.4964(15) 1.0000 0.010(3) Uiso 0.718(17) 2 d SP
H73A H -0.0345 0.5675 0.9757 0.012 Uiso 0.359(9) 1 calc PR
H73B H 0.0345 0.5675 1.0243 0.012 Uiso 0.359(9) 1 calc PR
C73B C 0.0000 0.229(4) 1.0000 0.042(10) Uani 0.282(17) 2 d SP
H73C H 0.0346 0.1578 1.0243 0.050 Uiso 0.141(9) 1 calc PR
H73D H -0.0346 0.1578 0.9757 0.050 Uiso 0.141(9) 1 calc PR
Cl1 Cl 0.02348(8) 0.3648(3) 0.95036(7) 0.0327(4) Uani 1 1 d .
C74A C 0.0000 0.4808(17) 0.5000 0.019(3) Uani 0.742(17) 2 d SP
H74A H 0.0256 0.5522 0.5337 0.023 Uiso 0.371(9) 1 calc PR
H74B H -0.0256 0.5522 0.4663 0.023 Uiso 0.371(9) 1 calc PR
C74B C 0.0000 0.208(4) 0.5000 0.028(9) Uani 0.258(17) 2 d SP
H74C H -0.0258 0.1378 0.4660 0.033 Uiso 0.129(9) 1 calc PR
H74D H 0.0258 0.1378 0.5340 0.033 Uiso 0.129(9) 1 calc PR
Cl2 Cl 0.04734(7) 0.3540(3) 0.47360(7) 0.0307(4) Uani 1 1 d .
C75 C 0.5000 0.2190(14) 0.5000 0.032(3) Uani 1 2 d S
H75A H 0.4662 0.1476 0.4744 0.038 Uiso 0.50 1 calc PR
H75B H 0.5338 0.1476 0.5256 0.038 Uiso 0.50 1 calc PR
Cl3 Cl 0.47341(8) 0.3453(3) 0.54728(7) 0.0320(4) Uani 1 1 d .
C76 C 0.5000 0.2186(14) 0.0000 0.029(2) Uani 1 2 d S
H76A H 0.4752 0.1473 -0.0342 0.035 Uiso 0.50 1 calc PR
H76B H 0.5248 0.1473 0.0342 0.035 Uiso 0.50 1 calc PR
Cl4 Cl 0.45101(7) 0.3478(4) 0.02446(7) 0.0348(4) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ru Ru -1.2594 0.8363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C6 C1 C2 119.7(8) . .
C6 C1 Ru1 71.4(5) . .
C2 C1 Ru1 71.0(5) . .
C6 C1 H1 120.2 . .
C2 C1 H1 120.2 . .
Ru1 C1 H1 130.0 . .
C1 C2 C3 120.1(9) . .
C1 C2 Ru1 71.5(5) . .
C3 C2 Ru1 71.9(6) . .
C1 C2 H2 119.9 . .
C3 C2 H2 119.9 . .
Ru1 C2 H2 129.0 . .
C2 C3 C4 119.3(9) . .
C2 C3 Ru1 70.5(6) . .
C4 C3 Ru1 71.1(4) . .
C2 C3 H3 120.3 . .
C4 C3 H3 120.3 . .
Ru1 C3 H3 130.5 . .
C5 C4 C3 120.0(7) . .
C5 C4 Ru1 72.2(4) . .
C3 C4 Ru1 71.3(4) . .
C5 C4 H4 120.0 . .
C3 C4 H4 120.0 . .
Ru1 C4 H4 128.7 . .
C6 C5 C4 119.0(9) . .
C6 C5 Ru1 70.0(6) . .
C4 C5 Ru1 70.5(5) . .
C6 C5 H5 120.5 . .
C4 C5 H5 120.5 . .
Ru1 C5 H5 131.7 . .
C1 C6 C5 121.9(9) . .
C1 C6 Ru1 71.9(5) . .
C5 C6 Ru1 73.0(6) . .
C1 C6 H6 119.1 . .
C5 C6 H6 119.1 . .
Ru1 C6 H6 128.4 . .
C8 C7 C11 108.8(7) . .
C8 C7 C15 127.5(7) . .
C11 C7 C15 123.7(6) . .
C8 C7 Ru1 70.3(5) . .
C11 C7 Ru1 70.6(4) . .
C15 C7 Ru1 126.9(5) . .
C7 C8 C9 113.7(9) . .
C7 C8 Ru1 74.0(5) . .
C9 C8 Ru1 69.9(6) . .
C7 C8 H8 123.1 . .
C9 C8 H8 123.1 . .
Ru1 C8 H8 124.5 . .
C8 C9 C10 104.9(8) . .
C8 C9 Ru1 72.9(6) . .
C10 C9 Ru1 69.3(4) . .
C8 C9 H9 127.5 . .
C10 C9 H9 127.5 . .
Ru1 C9 H9 122.1 . .
C11 C10 C9 105.1(7) . .
C11 C10 Ru1 72.8(4) . .
C9 C10 Ru1 69.1(4) . .
C11 C10 H10 127.5 . .
C9 C10 H10 127.5 . .
Ru1 C10 H10 122.4 . .
C7 C11 C10 107.5(6) . .
C7 C11 C12 125.5(6) . .
C10 C11 C12 126.9(6) . .
C7 C11 Ru1 71.8(4) . .
C10 C11 Ru1 68.0(4) . .
C12 C11 Ru1 127.4(4) . .
C11 C12 C13 105.3(5) . .
C11 C12 H12A 110.7 . .
C13 C12 H12A 110.7 . .
C11 C12 H12B 110.7 . .
C13 C12 H12B 110.7 . .
H12A C12 H12B 108.8 . .
O1 C13 C14 101.4(5) . .
O1 C13 C12 112.1(5) . .
C14 C13 C12 109.6(5) . .
O1 C13 H13 111.1 . .
C14 C13 H13 111.1 . .
C12 C13 H13 111.1 . .
O2 C14 C13 100.6(5) . .
O2 C14 C15 114.0(6) . .
C13 C14 C15 112.2(5) . .
O2 C14 H14 109.9 . .
C13 C14 H14 109.9 . .
C15 C14 H14 109.9 . .
C7 C15 C14 104.4(6) . .
C7 C15 H15A 110.9 . .
C14 C15 H15A 110.9 . .
C7 C15 H15B 110.9 . .
C14 C15 H15B 110.9 . .
H15A C15 H15B 108.9 . .
O1 C16 O2 104.5(6) . .
O1 C16 C17 105.0(8) . .
O2 C16 C17 109.3(6) . .
O1 C16 C18 110.4(6) . .
O2 C16 C18 108.2(6) . .
C17 C16 C18 118.5(8) . .
C16 C17 H17A 109.5 . .
C16 C17 H17B 109.5 . .
H17A C17 H17B 109.5 . .
C16 C17 H17C 109.5 . .
H17A C17 H17C 109.5 . .
H17B C17 H17C 109.5 . .
C16 C18 H18A 109.5 . .
C16 C18 H18B 109.5 . .
H18A C18 H18B 109.5 . .
C16 C18 H18C 109.5 . .
H18A C18 H18C 109.5 . .
H18B C18 H18C 109.5 . .
C13 O1 C16 106.3(5) . .
C14 O2 C16 107.3(6) . .
C9 Ru1 C10 41.6(3) . .
C9 Ru1 C8 37.2(3) . .
C10 Ru1 C8 64.3(3) . .
C9 Ru1 C2 121.5(3) . .
C10 Ru1 C2 161.4(3) . .
C8 Ru1 C2 107.0(3) . .
C9 Ru1 C6 171.3(3) . .
C10 Ru1 C6 129.8(3) . .
C8 Ru1 C6 146.1(3) . .
C2 Ru1 C6 67.0(3) . .
C9 Ru1 C11 65.9(3) . .
C10 Ru1 C11 39.1(3) . .
C8 Ru1 C11 61.9(3) . .
C2 Ru1 C11 153.3(3) . .
C6 Ru1 C11 107.7(3) . .
C9 Ru1 C1 151.5(4) . .
C10 Ru1 C1 160.9(3) . .
C8 Ru1 C1 118.9(3) . .
C2 Ru1 C1 37.6(3) . .
C6 Ru1 C1 36.7(3) . .
C11 Ru1 C1 123.4(3) . .
C9 Ru1 C4 113.0(3) . .
C10 Ru1 C4 108.9(3) . .
C8 Ru1 C4 143.9(3) . .
C2 Ru1 C4 67.6(3) . .
C6 Ru1 C4 67.1(3) . .
C11 Ru1 C4 136.3(3) . .
C1 Ru1 C4 79.6(2) . .
C9 Ru1 C3 106.1(3) . .
C10 Ru1 C3 129.5(3) . .
C8 Ru1 C3 117.1(3) . .
C2 Ru1 C3 37.5(2) . .
C6 Ru1 C3 79.3(3) . .
C11 Ru1 C3 168.6(3) . .
C1 Ru1 C3 67.6(3) . .
C4 Ru1 C3 37.5(3) . .
C9 Ru1 C7 63.1(3) . .
C10 Ru1 C7 64.3(3) . .
C8 Ru1 C7 35.7(3) . .
C2 Ru1 C7 119.1(3) . .
C6 Ru1 C7 115.8(3) . .
C11 Ru1 C7 37.5(2) . .
C1 Ru1 C7 106.5(3) . .
C4 Ru1 C7 173.1(3) . .
C3 Ru1 C7 147.5(3) . .
C9 Ru1 C5 138.5(3) . .
C10 Ru1 C5 109.3(3) . .
C8 Ru1 C5 173.6(3) . .
C2 Ru1 C5 79.4(3) . .
C6 Ru1 C5 37.0(2) . .
C11 Ru1 C5 112.8(3) . .
C1 Ru1 C5 66.7(3) . .
C4 Ru1 C5 37.3(3) . .
C3 Ru1 C5 67.3(3) . .
C7 Ru1 C5 141.9(3) . .
C20 C19 C24 117.9(9) . .
C20 C19 Ru2 69.6(6) . .
C24 C19 Ru2 69.9(5) . .
C20 C19 H19 121.0 . .
C24 C19 H19 121.0 . .
Ru2 C19 H19 132.3 . .
C21 C20 C19 121.2(9) . .
C21 C20 Ru2 72.4(5) . .
C19 C20 Ru2 73.2(6) . .
C21 C20 H20 119.4 . .
C19 C20 H20 119.4 . .
Ru2 C20 H20 127.0 . .
C20 C21 C22 120.3(8) . .
C20 C21 Ru2 70.9(5) . .
C22 C21 Ru2 71.6(5) . .
C20 C21 H21 119.9 . .
C22 C21 H21 119.9 . .
Ru2 C21 H21 130.2 . .
C21 C22 C23 119.7(9) . .
C21 C22 Ru2 71.2(5) . .
C23 C22 Ru2 71.5(6) . .
C21 C22 H22 120.1 . .
C23 C22 H22 120.1 . .
Ru2 C22 H22 129.6 . .
C24 C23 C22 120.3(10) . .
C24 C23 Ru2 71.4(4) . .
C22 C23 Ru2 71.3(6) . .
C24 C23 H23 119.9 . .
C22 C23 H23 119.8 . .
Ru2 C23 H23 130.1 . .
C23 C24 C19 120.4(7) . .
C23 C24 Ru2 72.2(5) . .
C19 C24 Ru2 72.2(4) . .
C23 C24 H24 119.8 . .
C19 C24 H24 119.8 . .
Ru2 C24 H24 128.0 . .
C26 C25 C29 108.6(6) . .
C26 C25 C33 135.5(8) . .
C29 C25 C33 115.9(7) . .
C26 C25 Ru2 72.8(4) . .
C29 C25 Ru2 70.8(4) . .
C33 C25 Ru2 123.4(4) . .
C25 C26 C27 110.5(7) . .
C25 C26 Ru2 71.4(4) . .
C27 C26 Ru2 71.1(4) . .
C25 C26 H26 124.8 . .
C27 C26 H26 124.8 . .
Ru2 C26 H26 124.4 . .
C26 C27 C28 109.7(7) . .
C26 C27 Ru2 72.6(4) . .
C28 C27 Ru2 70.5(4) . .
C26 C27 H27 125.2 . .
C28 C27 H27 125.2 . .
Ru2 C27 H27 123.4 . .
C27 C28 C29 104.1(7) . .
C27 C28 Ru2 71.0(5) . .
C29 C28 Ru2 70.6(4) . .
C27 C28 H28 127.9 . .
C29 C28 H28 127.9 . .
Ru2 C28 H28 122.3 . .
C25 C29 C28 107.1(6) . .
C25 C29 C30 131.1(8) . .
C28 C29 C30 121.7(8) . .
C25 C29 Ru2 70.9(4) . .
C28 C29 Ru2 70.2(4) . .
C30 C29 Ru2 126.2(5) . .
C31 C30 C29 104.0(6) . .
C31 C30 H30A 110.9 . .
C29 C30 H30A 110.9 . .
C31 C30 H30B 110.9 . .
C29 C30 H30B 110.9 . .
H30A C30 H30B 109.0 . .
O3 C31 C30 113.7(5) . .
O3 C31 C32 99.2(5) . .
C30 C31 C32 112.2(5) . .
O3 C31 H31 110.4 . .
C30 C31 H31 110.4 . .
C32 C31 H31 110.4 . .
O4 C32 C31 102.1(5) . .
O4 C32 C33 113.8(5) . .
C31 C32 C33 112.8(5) . .
O4 C32 H32 109.3 . .
C31 C32 H32 109.3 . .
C33 C32 H32 109.3 . .
C32 C33 C25 109.4(6) . .
C32 C33 H33A 109.8 . .
C25 C33 H33A 109.8 . .
C32 C33 H33B 109.8 . .
C25 C33 H33B 109.8 . .
H33A C33 H33B 108.2 . .
O4 C34 O3 106.5(6) . .
O4 C34 C36 107.8(6) . .
O3 C34 C36 111.5(5) . .
O4 C34 C35 108.1(5) . .
O3 C34 C35 109.6(5) . .
C36 C34 C35 113.0(6) . .
C34 C35 H35A 109.5 . .
C34 C35 H35B 109.5 . .
H35A C35 H35B 109.5 . .
C34 C35 H35C 109.5 . .
H35A C35 H35C 109.5 . .
H35B C35 H35C 109.5 . .
C34 C36 H36A 109.5 . .
C34 C36 H36B 109.5 . .
H36A C36 H36B 109.5 . .
C34 C36 H36C 109.5 . .
H36A C36 H36C 109.5 . .
H36B C36 H36C 109.5 . .
C31 O3 C34 106.3(6) . .
C32 O4 C34 104.6(5) . .
C28 Ru2 C29 39.2(3) . .
C28 Ru2 C27 38.5(3) . .
C29 Ru2 C27 63.2(3) . .
C28 Ru2 C25 64.5(2) . .
C29 Ru2 C25 38.2(3) . .
C27 Ru2 C25 61.5(3) . .
C28 Ru2 C20 173.9(3) . .
C29 Ru2 C20 139.8(3) . .
C27 Ru2 C20 136.1(3) . .
C25 Ru2 C20 111.2(3) . .
C28 Ru2 C26 63.2(3) . .
C29 Ru2 C26 62.0(3) . .
C27 Ru2 C26 36.3(3) . .
C25 Ru2 C26 35.9(3) . .
C20 Ru2 C26 110.7(3) . .
C28 Ru2 C24 118.2(3) . .
C29 Ru2 C24 108.1(3) . .
C27 Ru2 C24 153.3(3) . .
C25 Ru2 C24 128.6(3) . .
C20 Ru2 C24 67.7(3) . .
C26 Ru2 C24 164.0(3) . .
C28 Ru2 C21 142.7(3) . .
C29 Ru2 C21 170.6(3) . .
C27 Ru2 C21 112.9(3) . .
C25 Ru2 C21 132.5(3) . .
C20 Ru2 C21 36.8(3) . .
C26 Ru2 C21 109.5(3) . .
C24 Ru2 C21 79.1(2) . .
C28 Ru2 C22 116.0(3) . .
C29 Ru2 C22 151.0(4) . .
C27 Ru2 C22 107.9(3) . .
C25 Ru2 C22 163.7(3) . .
C20 Ru2 C22 66.8(3) . .
C26 Ru2 C22 128.3(4) . .
C24 Ru2 C22 66.6(3) . .
C21 Ru2 C22 37.1(3) . .
C28 Ru2 C23 106.3(3) . .
C29 Ru2 C23 122.4(3) . .
C27 Ru2 C23 124.2(3) . .
C25 Ru2 C23 158.7(3) . .
C20 Ru2 C23 79.2(3) . .
C26 Ru2 C23 159.1(4) . .
C24 Ru2 C23 36.5(3) . .
C21 Ru2 C23 67.0(3) . .
C22 Ru2 C23 37.3(2) . .
C28 Ru2 C19 147.2(3) . .
C29 Ru2 C19 115.3(3) . .
C27 Ru2 C19 168.3(3) . .
C25 Ru2 C19 109.6(3) . .
C20 Ru2 C19 37.2(2) . .
C26 Ru2 C19 132.0(4) . .
C24 Ru2 C19 38.0(3) . .
C21 Ru2 C19 66.6(3) . .
C22 Ru2 C19 79.0(3) . .
C23 Ru2 C19 66.9(3) . .
C42 C37 C38 120.1(7) . .
C42 C37 Ru3 71.1(5) . .
C38 C37 Ru3 71.7(5) . .
C42 C37 H37 120.0 . .
C38 C37 H37 120.0 . .
Ru3 C37 H37 129.7 . .
C39 C38 C37 115.9(9) . .
C39 C38 Ru3 70.2(6) . .
C37 C38 Ru3 70.0(4) . .
C39 C38 H38 122.1 . .
C37 C38 H38 122.1 . .
Ru3 C38 H38 129.9 . .
C40 C39 C38 124.9(9) . .
C40 C39 Ru3 72.8(5) . .
C38 C39 Ru3 73.3(6) . .
C40 C39 H39 117.5 . .
C38 C39 H39 117.5 . .
Ru3 C39 H39 129.1 . .
C39 C40 C41 118.5(7) . .
C39 C40 Ru3 70.7(5) . .
C41 C40 Ru3 71.4(5) . .
C39 C40 H40 120.8 . .
C41 C40 H40 120.8 . .
Ru3 C40 H40 129.4 . .
C40 C41 C42 119.6(9) . .
C40 C41 Ru3 71.7(5) . .
C42 C41 Ru3 70.6(6) . .
C40 C41 H41 120.2 . .
C42 C41 H41 120.2 . .
Ru3 C41 H41 130.0 . .
C37 C42 C41 121.0(9) . .
C37 C42 Ru3 72.2(5) . .
C41 C42 Ru3 72.1(6) . .
C37 C42 H42 119.5 . .
C41 C42 H42 119.5 . .
Ru3 C42 H42 128.5 . .
C47 C43 C44 107.9(7) . .
C47 C43 C51 127.7(7) . .
C44 C43 C51 124.2(8) . .
C47 C43 Ru3 71.8(5) . .
C44 C43 Ru3 70.8(4) . .
C51 C43 Ru3 126.6(6) . .
C45 C44 C43 107.0(8) . .
C45 C44 Ru3 69.9(6) . .
C43 C44 Ru3 70.3(5) . .
C45 C44 H44 126.5 . .
C43 C44 H44 126.5 . .
Ru3 C44 H44 124.9 . .
C46 C45 C44 107.6(8) . .
C46 C45 Ru3 70.6(5) . .
C44 C45 Ru3 71.6(5) . .
C46 C45 H45 126.2 . .
C44 C45 H45 126.2 . .
Ru3 C45 H45 123.2 . .
C45 C46 C47 108.9(7) . .
C45 C46 Ru3 71.8(4) . .
C47 C46 Ru3 72.0(5) . .
C45 C46 H46 125.6 . .
C47 C46 H46 125.6 . .
Ru3 C46 H46 122.3 . .
C43 C47 C46 108.6(6) . .
C43 C47 C48 121.5(7) . .
C46 C47 C48 130.0(7) . .
C43 C47 Ru3 71.5(4) . .
C46 C47 Ru3 69.3(4) . .
C48 C47 Ru3 125.2(5) . .
C49 C48 C47 107.6(6) . .
C49 C48 H48A 110.2 . .
C47 C48 H48A 110.2 . .
C49 C48 H48B 110.2 . .
C47 C48 H48B 110.2 . .
H48A C48 H48B 108.5 . .
O5 C49 C48 113.4(5) . .
O5 C49 C50 101.5(5) . .
C48 C49 C50 110.3(5) . .
O5 C49 H49 110.4 . .
C48 C49 H49 110.4 . .
C50 C49 H49 110.4 . .
O6 C50 C51 115.9(5) . .
O6 C50 C49 100.4(5) . .
C51 C50 C49 112.3(5) . .
O6 C50 H50 109.3 . .
C51 C50 H50 109.3 . .
C49 C50 H50 109.3 . .
C50 C51 C43 104.5(6) . .
C50 C51 H51A 110.9 . .
C43 C51 H51A 110.8 . .
C50 C51 H51B 110.9 . .
C43 C51 H51B 110.8 . .
H51A C51 H51B 108.9 . .
O5 C52 O6 105.6(6) . .
O5 C52 C53 108.2(7) . .
O6 C52 C53 109.3(6) . .
O5 C52 C54 110.9(6) . .
O6 C52 C54 107.7(6) . .
C53 C52 C54 114.7(7) . .
C52 C53 H53A 109.5 . .
C52 C53 H53B 109.5 . .
H53A C53 H53B 109.5 . .
C52 C53 H53C 109.5 . .
H53A C53 H53C 109.5 . .
H53B C53 H53C 109.5 . .
C52 C54 H54A 109.5 . .
C52 C54 H54B 109.5 . .
H54A C54 H54B 109.5 . .
C52 C54 H54C 109.5 . .
H54A C54 H54C 109.5 . .
H54B C54 H54C 109.5 . .
C49 O5 C52 106.8(5) . .
C50 O6 C52 106.9(6) . .
C46 Ru3 C45 37.6(3) . .
C46 Ru3 C43 63.5(3) . .
C45 Ru3 C43 64.6(3) . .
C46 Ru3 C47 38.6(3) . .
C45 Ru3 C47 63.8(3) . .
C43 Ru3 C47 36.7(3) . .
C46 Ru3 C39 128.4(4) . .
C45 Ru3 C39 107.2(3) . .
C43 Ru3 C39 150.4(4) . .
C47 Ru3 C39 166.8(3) . .
C46 Ru3 C44 63.4(3) . .
C45 Ru3 C44 38.4(2) . .
C43 Ru3 C44 38.9(3) . .
C47 Ru3 C44 63.1(3) . .
C39 Ru3 C44 116.6(3) . .
C46 Ru3 C42 132.0(3) . .
C45 Ru3 C42 169.3(3) . .
C43 Ru3 C42 115.6(3) . .
C47 Ru3 C42 109.5(3) . .
C39 Ru3 C42 77.9(3) . .
C44 Ru3 C42 147.8(3) . .
C46 Ru3 C37 163.5(4) . .
C45 Ru3 C37 153.8(3) . .
C43 Ru3 C37 107.7(3) . .
C47 Ru3 C37 126.1(3) . .
C39 Ru3 C37 66.4(3) . .
C44 Ru3 C37 119.6(3) . .
C42 Ru3 C37 36.7(3) . .
C46 Ru3 C41 110.3(3) . .
C45 Ru3 C41 135.7(3) . .
C43 Ru3 C41 140.9(3) . .
C47 Ru3 C41 113.2(3) . .
C39 Ru3 C41 65.7(3) . .
C44 Ru3 C41 173.6(3) . .
C42 Ru3 C41 37.3(2) . .
C37 Ru3 C41 66.8(3) . .
C46 Ru3 C40 108.7(3) . .
C45 Ru3 C40 111.4(3) . .
C43 Ru3 C40 171.7(3) . .
C47 Ru3 C40 135.3(3) . .
C39 Ru3 C40 36.5(3) . .
C44 Ru3 C40 141.8(3) . .
C42 Ru3 C40 66.8(3) . .
C37 Ru3 C40 79.1(2) . .
C41 Ru3 C40 36.8(3) . .
C46 Ru3 C38 158.1(4) . .
C45 Ru3 C38 122.0(3) . .
C43 Ru3 C38 121.4(3) . .
C47 Ru3 C38 156.1(3) . .
C39 Ru3 C38 36.5(2) . .
C44 Ru3 C38 105.9(3) . .
C42 Ru3 C38 67.6(3) . .
C37 Ru3 C38 38.3(3) . .
C41 Ru3 C38 79.5(3) . .
C40 Ru3 C38 66.9(3) . .
C56 C55 C60 119.3(9) . .
C56 C55 Ru4 70.4(6) . .
C60 C55 Ru4 70.9(5) . .
C56 C55 H55 120.3 . .
C60 C55 H55 120.3 . .
Ru4 C55 H55 131.1 . .
C55 C56 C57 120.2(9) . .
C55 C56 Ru4 72.4(6) . .
C57 C56 Ru4 71.2(5) . .
C55 C56 H56 119.9 . .
C57 C56 H56 119.9 . .
Ru4 C56 H56 128.8 . .
C56 C57 C58 120.7(8) . .
C56 C57 Ru4 71.0(5) . .
C58 C57 Ru4 72.4(5) . .
C56 C57 H57 119.7 . .
C58 C57 H57 119.7 . .
Ru4 C57 H57 129.4 . .
C57 C58 C59 115.5(9) . .
C57 C58 Ru4 69.9(4) . .
C59 C58 Ru4 69.1(6) . .
C57 C58 H58 122.2 . .
C59 C58 H58 122.2 . .
Ru4 C58 H58 131.1 . .
C60 C59 C58 124.1(9) . .
C60 C59 Ru4 73.1(5) . .
C58 C59 Ru4 72.9(6) . .
C60 C59 H59 117.9 . .
C58 C59 H59 117.9 . .
Ru4 C59 H59 128.6 . .
C59 C60 C55 120.1(7) . .
C59 C60 Ru4 71.1(5) . .
C55 C60 Ru4 72.0(5) . .
C59 C60 H60 120.0 . .
C55 C60 H60 120.0 . .
Ru4 C60 H60 129.4 . .
C62 C61 C65 106.7(6) . .
C62 C61 C69 126.6(6) . .
C65 C61 C69 126.7(7) . .
C62 C61 Ru4 70.3(4) . .
C65 C61 Ru4 70.9(4) . .
C69 C61 Ru4 124.4(5) . .
C61 C62 C63 106.4(7) . .
C61 C62 Ru4 71.6(4) . .
C63 C62 Ru4 69.9(5) . .
C61 C62 H62 126.8 . .
C63 C62 H62 126.8 . .
Ru4 C62 H62 123.5 . .
C64 C63 C62 107.4(9) . .
C64 C63 Ru4 70.9(6) . .
C62 C63 Ru4 71.2(5) . .
C64 C63 H63 126.3 . .
C62 C63 H63 126.3 . .
Ru4 C63 H63 123.2 . .
C65 C64 C63 111.0(9) . .
C65 C64 Ru4 73.9(5) . .
C63 C64 Ru4 71.5(6) . .
C65 C64 H64 124.5 . .
C63 C64 H64 124.5 . .
Ru4 C64 H64 121.7 . .
C64 C65 C61 108.4(7) . .
C64 C65 C66 129.3(7) . .
C61 C65 C66 122.3(7) . .
C64 C65 Ru4 70.1(5) . .
C61 C65 Ru4 70.6(4) . .
C66 C65 Ru4 126.5(5) . .
C67 C66 C65 106.5(6) . .
C67 C66 H66A 110.4 . .
C65 C66 H66A 110.4 . .
C67 C66 H66B 110.4 . .
C65 C66 H66B 110.4 . .
H66A C66 H66B 108.6 . .
O7 C67 C68 99.4(5) . .
O7 C67 C66 112.8(5) . .
C68 C67 C66 112.6(5) . .
O7 C67 H67 110.5 . .
C68 C67 H67 110.5 . .
C66 C67 H67 110.5 . .
O8 C68 C67 102.3(5) . .
O8 C68 C69 113.5(5) . .
C67 C68 C69 113.7(5) . .
O8 C68 H68 109.0 . .
C67 C68 H68 109.0 . .
C69 C68 H68 109.0 . .
C61 C69 C68 103.4(6) . .
C61 C69 H69A 111.1 . .
C68 C69 H69A 111.1 . .
C61 C69 H69B 111.1 . .
C68 C69 H69B 111.1 . .
H69A C69 H69B 109.0 . .
O7 C70 O8 104.4(6) . .
O7 C70 C72 113.7(5) . .
O8 C70 C72 106.3(6) . .
O7 C70 C71 109.8(5) . .
O8 C70 C71 107.1(5) . .
C72 C70 C71 114.7(7) . .
C70 C71 H71A 109.5 . .
C70 C71 H71B 109.5 . .
H71A C71 H71B 109.5 . .
C70 C71 H71C 109.5 . .
H71A C71 H71C 109.5 . .
H71B C71 H71C 109.5 . .
C70 C72 H72A 109.5 . .
C70 C72 H72B 109.5 . .
H72A C72 H72B 109.5 . .
C70 C72 H72C 109.5 . .
H72A C72 H72C 109.5 . .
H72B C72 H72C 109.5 . .
C67 O7 C70 107.9(6) . .
C68 O8 C70 105.1(5) . .
C64 Ru4 C63 37.6(3) . .
C64 Ru4 C62 63.7(3) . .
C63 Ru4 C62 38.9(3) . .
C64 Ru4 C59 107.9(3) . .
C63 Ru4 C59 124.7(4) . .
C62 Ru4 C59 161.9(3) . .
C64 Ru4 C61 62.8(3) . .
C63 Ru4 C61 63.8(3) . .
C62 Ru4 C61 38.2(3) . .
C59 Ru4 C61 154.6(3) . .
C64 Ru4 C65 36.0(3) . .
C63 Ru4 C65 62.3(3) . .
C62 Ru4 C65 63.7(3) . .
C59 Ru4 C65 120.0(3) . .
C61 Ru4 C65 38.5(2) . .
C64 Ru4 C56 173.1(3) . .
C63 Ru4 C56 137.3(3) . .
C62 Ru4 C56 109.5(3) . .
C59 Ru4 C56 78.8(3) . .
C61 Ru4 C56 111.6(3) . .
C65 Ru4 C56 141.7(3) . .
C64 Ru4 C57 143.2(3) . .
C63 Ru4 C57 112.9(3) . .
C62 Ru4 C57 108.9(3) . .
C59 Ru4 C57 67.3(3) . .
C61 Ru4 C57 135.0(3) . .
C65 Ru4 C57 172.5(3) . .
C56 Ru4 C57 37.8(3) . .
C64 Ru4 C60 119.0(3) . .
C63 Ru4 C60 152.9(3) . .
C62 Ru4 C60 162.1(3) . .
C59 Ru4 C60 35.8(3) . .
C61 Ru4 C60 125.2(3) . .
C65 Ru4 C60 107.3(3) . .
C56 Ru4 C60 67.2(3) . .
C57 Ru4 C60 79.5(2) . .
C64 Ru4 C55 146.4(3) . .
C63 Ru4 C55 169.3(3) . .
C62 Ru4 C55 130.4(3) . .
C59 Ru4 C55 65.8(3) . .
C61 Ru4 C55 107.9(3) . .
C65 Ru4 C55 116.1(3) . .
C56 Ru4 C55 37.2(2) . .
C57 Ru4 C55 67.5(3) . .
C60 Ru4 C55 37.2(3) . .
C64 Ru4 C58 116.3(3) . .
C63 Ru4 C58 106.9(3) . .
C62 Ru4 C58 128.9(3) . .
C59 Ru4 C58 38.0(2) . .
C61 Ru4 C58 167.0(3) . .
C65 Ru4 C58 147.4(3) . .
C56 Ru4 C58 68.2(3) . .
C57 Ru4 C58 37.7(3) . .
C60 Ru4 C58 67.4(3) . .
C55 Ru4 C58 80.0(3) . .
F2 P1 F3 90.8(3) . .
F2 P1 F4 179.3(3) . .
F3 P1 F4 89.3(2) . .
F2 P1 F6 88.6(3) . .
F3 P1 F6 89.8(3) . .
F4 P1 F6 90.8(3) . .
F2 P1 F1 91.1(3) . .
F3 P1 F1 89.6(3) . .
F4 P1 F1 89.5(3) . .
F6 P1 F1 179.3(4) . .
F2 P1 F5 90.9(3) . .
F3 P1 F5 178.2(3) . .
F4 P1 F5 89.0(3) . .
F6 P1 F5 89.9(3) . .
F1 P1 F5 90.8(3) . .
F12 P2 F11 90.4(2) . .
F12 P2 F10 90.5(3) . .
F11 P2 F10 90.2(3) . .
F12 P2 F8 90.7(3) . .
F11 P2 F8 89.4(3) . .
F10 P2 F8 178.7(3) . .
F12 P2 F7 179.6(4) . .
F11 P2 F7 89.8(3) . .
F10 P2 F7 89.8(3) . .
F8 P2 F7 89.0(3) . .
F12 P2 F9 89.2(3) . .
F11 P2 F9 179.5(3) . .
F10 P2 F9 90.1(3) . .
F8 P2 F9 90.4(3) . .
F7 P2 F9 90.6(2) . .
F14 P3 F16 179.6(4) . .
F14 P3 F17 90.6(3) . .
F16 P3 F17 89.6(2) . .
F14 P3 F13 89.9(3) . .
F16 P3 F13 90.5(3) . .
F17 P3 F13 90.0(3) . .
F14 P3 F18 90.2(3) . .
F16 P3 F18 89.5(3) . .
F17 P3 F18 89.8(3) . .
F13 P3 F18 179.8(3) . .
F14 P3 F15 89.5(2) . .
F16 P3 F15 90.3(3) . .
F17 P3 F15 179.7(3) . .
F13 P3 F15 90.3(3) . .
F18 P3 F15 89.9(3) . .
F19 P4 F23 91.7(3) . .
F19 P4 F20 90.4(3) . .
F23 P4 F20 91.5(2) . .
F19 P4 F24 179.2(3) . .
F23 P4 F24 89.1(3) . .
F20 P4 F24 89.7(3) . .
F19 P4 F21 89.8(3) . .
F23 P4 F21 178.5(3) . .
F20 P4 F21 88.8(3) . .
F24 P4 F21 89.5(3) . .
F19 P4 F22 90.0(3) . .
F23 P4 F22 89.5(3) . .
F20 P4 F22 178.9(3) . .
F24 P4 F22 89.9(3) . .
F21 P4 F22 90.1(2) . .
Cl1 C73A Cl1 106.8(7) . 2_557
Cl1 C73A H73A 110.4 . .
Cl1 C73A H73A 110.4 2_557 .
Cl1 C73A H73B 110.4 . .
Cl1 C73A H73B 110.4 2_557 .
H73A C73A H73B 108.6 . .
Cl1 C73B Cl1 104.9(17) . 2_557
Cl1 C73B H73C 110.8 . .
Cl1 C73B H73C 110.8 2_557 .
Cl1 C73B H73D 110.8 . .
Cl1 C73B H73D 110.8 2_557 .
H73C C73B H73D 108.8 . .
C73A Cl1 C73B 74.2(9) . .
Cl2 C74A Cl2 108.6(8) 2_556 .
Cl2 C74A H74A 110.0 2_556 .
Cl2 C74A H74A 110.0 . .
Cl2 C74A H74B 110.0 2_556 .
Cl2 C74A H74B 110.0 . .
H74A C74A H74B 108.3 . .
Cl2 C74B Cl2 100.9(15) 2_556 .
Cl2 C74B H74C 111.6 2_556 .
Cl2 C74B H74C 111.6 . .
Cl2 C74B H74D 111.6 2_556 .
Cl2 C74B H74D 111.6 . .
H74C C74B H74D 109.4 . .
C74A Cl2 C74B 75.2(8) . .
Cl3 C75 Cl3 108.9(6) . 2_656
Cl3 C75 H75A 109.9 . .
Cl3 C75 H75A 109.9 2_656 .
Cl3 C75 H75B 109.9 . .
Cl3 C75 H75B 109.9 2_656 .
H75A C75 H75B 108.3 . .
Cl4 C76 Cl4 107.8(6) . 2_655
Cl4 C76 H76A 110.2 . .
Cl4 C76 H76A 110.2 2_655 .
Cl4 C76 H76B 110.2 . .
Cl4 C76 H76B 110.2 2_655 .
H76A C76 H76B 108.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 C6 1.390(11) .
C1 C2 1.422(11) .
C1 Ru1 2.211(8) .
C1 H1 0.9500 .
C2 C3 1.424(9) .
C2 Ru1 2.204(9) .
C2 H2 0.9500 .
C3 C4 1.428(12) .
C3 Ru1 2.223(8) .
C3 H3 0.9500 .
C4 C5 1.428(12) .
C4 Ru1 2.220(8) .
C4 H4 0.9500 .
C5 C6 1.411(9) .
C5 Ru1 2.242(8) .
C5 H5 0.9500 .
C6 Ru1 2.204(8) .
C6 H6 0.9500 .
C7 C8 1.350(11) .
C7 C11 1.426(9) .
C7 C15 1.508(10) .
C7 Ru1 2.225(7) .
C8 C9 1.380(11) .
C8 Ru1 2.179(8) .
C8 H8 0.9500 .
C9 C10 1.521(12) .
C9 Ru1 2.142(9) .
C9 H9 0.9500 .
C10 C11 1.460(10) .
C10 Ru1 2.144(7) .
C10 H10 0.9500 .
C11 C12 1.477(9) .
C11 Ru1 2.210(6) .
C12 C13 1.529(9) .
C12 H12A 0.9900 .
C12 H12B 0.9900 .
C13 O1 1.436(7) .
C13 C14 1.503(9) .
C13 H13 1.0000 .
C14 O2 1.418(9) .
C14 C15 1.518(9) .
C14 H14 1.0000 .
C15 H15A 0.9900 .
C15 H15B 0.9900 .
C16 O1 1.454(11) .
C16 O2 1.459(7) .
C16 C17 1.467(9) .
C16 C18 1.504(10) .
C17 H17A 0.9800 .
C17 H17B 0.9800 .
C17 H17C 0.9800 .
C18 H18A 0.9800 .
C18 H18B 0.9800 .
C18 H18C 0.9800 .
C19 C20 1.414(9) .
C19 C24 1.446(12) .
C19 Ru2 2.238(8) .
C19 H19 0.9500 .
C20 C21 1.388(11) .
C20 Ru2 2.190(9) .
C20 H20 0.9500 .
C21 C22 1.409(12) .
C21 Ru2 2.210(8) .
C21 H21 0.9500 .
C22 C23 1.416(10) .
C22 Ru2 2.215(10) .
C22 H22 0.9500 .
C23 C24 1.385(12) .
C23 Ru2 2.218(8) .
C23 H23 0.9500 .
C24 Ru2 2.207(8) .
C24 H24 0.9500 .
C25 C26 1.346(12) .
C25 C29 1.425(11) .
C25 C33 1.572(9) .
C25 Ru2 2.176(6) .
C26 C27 1.363(12) .
C26 Ru2 2.193(7) .
C26 H26 0.9500 .
C27 C28 1.433(9) .
C27 Ru2 2.175(7) .
C27 H27 0.9500 .
C28 C29 1.457(10) .
C28 Ru2 2.168(7) .
C28 H28 0.9500 .
C29 C30 1.555(10) .
C29 Ru2 2.175(8) .
C30 C31 1.502(10) .
C30 H30A 0.9900 .
C30 H30B 0.9900 .
C31 O3 1.418(8) .
C31 C32 1.513(8) .
C31 H31 1.0000 .
C32 O4 1.433(7) .
C32 C33 1.550(10) .
C32 H32 1.0000 .
C33 H33A 0.9900 .
C33 H33B 0.9900 .
C34 O4 1.433(10) .
C34 O3 1.453(7) .
C34 C36 1.487(9) .
C34 C35 1.529(8) .
C35 H35A 0.9800 .
C35 H35B 0.9800 .
C35 H35C 0.9800 .
C36 H36A 0.9800 .
C36 H36B 0.9800 .
C36 H36C 0.9800 .
C37 C42 1.389(12) .
C37 C38 1.457(11) .
C37 Ru3 2.212(8) .
C37 H37 0.9500 .
C38 C39 1.389(9) .
C38 Ru3 2.235(9) .
C38 H38 0.9500 .
C39 C40 1.382(12) .
C39 Ru3 2.194(9) .
C39 H39 0.9500 .
C40 C41 1.403(11) .
C40 Ru3 2.221(8) .
C40 H40 0.9500 .
C41 C42 1.412(9) .
C41 Ru3 2.217(9) .
C41 H41 0.9500 .
C42 Ru3 2.197(9) .
C42 H42 0.9500 .
C43 C47 1.378(12) .
C43 C44 1.460(11) .
C43 C51 1.528(11) .
C43 Ru3 2.188(8) .
C44 C45 1.438(9) .
C44 Ru3 2.194(9) .
C44 H44 0.9500 .
C45 C46 1.397(12) .
C45 Ru3 2.172(8) .
C45 H45 0.9500 .
C46 C47 1.439(12) .
C46 Ru3 2.157(8) .
C46 H46 0.9500 .
C47 C48 1.518(8) .
C47 Ru3 2.192(6) .
C48 C49 1.516(9) .
C48 H48A 0.9900 .
C48 H48B 0.9900 .
C49 O5 1.433(7) .
C49 C50 1.525(8) .
C49 H49 1.0000 .
C50 O6 1.421(8) .
C50 C51 1.501(9) .
C50 H50 1.0000 .
C51 H51A 0.9900 .
C51 H51B 0.9900 .
C52 O5 1.433(11) .
C52 O6 1.465(7) .
C52 C53 1.488(9) .
C52 C54 1.510(10) .
C53 H53A 0.9800 .
C53 H53B 0.9800 .
C53 H53C 0.9800 .
C54 H54A 0.9800 .
C54 H54B 0.9800 .
C54 H54C 0.9800 .
C55 C56 1.416(9) .
C55 C60 1.418(11) .
C55 Ru4 2.231(8) .
C55 H55 0.9500 .
C56 C57 1.429(12) .
C56 Ru4 2.205(9) .
C56 H56 0.9500 .
C57 C58 1.439(11) .
C57 Ru4 2.208(8) .
C57 H57 0.9500 .
C58 C59 1.445(9) .
C58 Ru4 2.242(9) .
C58 H58 0.9500 .
C59 C60 1.353(12) .
C59 Ru4 2.191(9) .
C59 H59 0.9500 .
C60 Ru4 2.216(8) .
C60 H60 0.9500 .
C61 C62 1.433(10) .
C61 C65 1.450(8) .
C61 C69 1.521(9) .
C61 Ru4 2.199(6) .
C62 C63 1.447(12) .
C62 Ru4 2.182(7) .
C62 H62 0.9500 .
C63 C64 1.394(11) .
C63 Ru4 2.164(10) .
C63 H63 0.9500 .
C64 C65 1.346(11) .
C64 Ru4 2.157(9) .
C64 H64 0.9500 .
C65 C66 1.531(10) .
C65 Ru4 2.204(8) .
C66 C67 1.512(9) .
C66 H66A 0.9900 .
C66 H66B 0.9900 .
C67 O7 1.407(8) .
C67 C68 1.492(8) .
C67 H67 1.0000 .
C68 O8 1.428(7) .
C68 C69 1.571(9) .
C68 H68 1.0000 .
C69 H69A 0.9900 .
C69 H69B 0.9900 .
C70 O7 1.435(6) .
C70 O8 1.465(10) .
C70 C72 1.483(10) .
C70 C71 1.514(8) .
C71 H71A 0.9800 .
C71 H71B 0.9800 .
C71 H71C 0.9800 .
C72 H72A 0.9800 .
C72 H72B 0.9800 .
C72 H72C 0.9800 .
F1 P1 1.603(4) .
F2 P1 1.574(5) .
F3 P1 1.577(5) .
F4 P1 1.591(5) .
F5 P1 1.614(5) .
F6 P1 1.601(4) .
F7 P2 1.608(5) .
F8 P2 1.605(4) .
F9 P2 1.617(5) .
F10 P2 1.599(4) .
F11 P2 1.595(5) .
F12 P2 1.595(5) .
F13 P3 1.595(3) .
F14 P3 1.589(5) .
F15 P3 1.607(5) .
F16 P3 1.590(5) .
F17 P3 1.593(5) .
F18 P3 1.603(4) .
F19 P4 1.598(4) .
F20 P4 1.603(5) .
F21 P4 1.610(5) .
F22 P4 1.613(5) .
F23 P4 1.599(5) .
F24 P4 1.609(4) .
C73A Cl1 1.791(8) .
C73A Cl1 1.791(8) 2_557
C73A H73A 0.9900 .
C73A H73B 0.9900 .
C73B Cl1 1.81(2) .
C73B Cl1 1.81(2) 2_557
C73B H73C 0.9900 .
C73B H73D 0.9900 .
C74A Cl2 1.764(8) 2_556
C74A Cl2 1.764(8) .
C74A H74A 0.9900 .
C74A H74B 0.9900 .
C74B Cl2 1.86(2) 2_556
C74B Cl2 1.86(2) .
C74B H74C 0.9900 .
C74B H74D 0.9900 .
C75 Cl3 1.764(7) .
C75 Cl3 1.764(7) 2_656
C75 H75A 0.9900 .
C75 H75B 0.9900 .
C76 Cl4 1.779(7) .
C76 Cl4 1.779(7) 2_655
C76 H76A 0.9900 .
C76 H76B 0.9900 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
C6 C1 C2 C3 -0.9(14) .
Ru1 C1 C2 C3 -55.1(9) .
C6 C1 C2 Ru1 54.2(7) .
C1 C2 C3 C4 1.2(15) .
Ru1 C2 C3 C4 -53.7(8) .
C1 C2 C3 Ru1 54.9(8) .
C2 C3 C4 C5 -2.0(13) .
Ru1 C3 C4 C5 -55.4(7) .
C2 C3 C4 Ru1 53.4(9) .
C3 C4 C5 C6 2.6(14) .
Ru1 C4 C5 C6 -52.4(9) .
C3 C4 C5 Ru1 55.0(7) .
C2 C1 C6 C5 1.6(14) .
Ru1 C1 C6 C5 55.5(9) .
C2 C1 C6 Ru1 -54.0(7) .
C4 C5 C6 C1 -2.4(16) .
Ru1 C5 C6 C1 -55.1(9) .
C4 C5 C6 Ru1 52.6(8) .
C11 C7 C8 C9 -1.5(11) .
C15 C7 C8 C9 -179.2(8) .
Ru1 C7 C8 C9 58.9(8) .
C11 C7 C8 Ru1 -60.4(5) .
C15 C7 C8 Ru1 121.9(8) .
C7 C8 C9 C10 1.1(12) .
Ru1 C8 C9 C10 62.3(5) .
C7 C8 C9 Ru1 -61.2(7) .
C8 C9 C10 C11 -0.2(9) .
Ru1 C9 C10 C11 64.6(5) .
C8 C9 C10 Ru1 -64.8(7) .
C8 C7 C11 C10 1.3(8) .
C15 C7 C11 C10 179.1(7) .
Ru1 C7 C11 C10 -58.9(4) .
C8 C7 C11 C12 -176.3(6) .
C15 C7 C11 C12 1.5(11) .
Ru1 C7 C11 C12 123.5(6) .
C8 C7 C11 Ru1 60.2(6) .
C15 C7 C11 Ru1 -122.0(7) .
C9 C10 C11 C7 -0.7(7) .
Ru1 C10 C11 C7 61.4(4) .
C9 C10 C11 C12 176.9(6) .
Ru1 C10 C11 C12 -121.1(6) .
C9 C10 C11 Ru1 -62.0(5) .
C7 C11 C12 C13 -18.2(8) .
C10 C11 C12 C13 164.6(6) .
Ru1 C11 C12 C13 75.5(6) .
C11 C12 C13 O1 163.2(5) .
C11 C12 C13 C14 51.4(6) .
O1 C13 C14 O2 44.3(6) .
C12 C13 C14 O2 162.9(5) .
O1 C13 C14 C15 165.9(6) .
C12 C13 C14 C15 -75.5(7) .
C8 C7 C15 C14 160.5(7) .
C11 C7 C15 C14 -16.9(9) .
Ru1 C7 C15 C14 -107.0(6) .
O2 C14 C15 C7 165.4(6) .
C13 C14 C15 C7 51.9(7) .
C14 C13 O1 C16 -36.0(6) .
C12 C13 O1 C16 -152.9(5) .
O2 C16 O1 C13 14.2(6) .
C17 C16 O1 C13 129.3(6) .
C18 C16 O1 C13 -101.9(6) .
C13 C14 O2 C16 -36.5(6) .
C15 C14 O2 C16 -156.8(5) .
O1 C16 O2 C14 15.0(6) .
C17 C16 O2 C14 -97.0(9) .
C18 C16 O2 C14 132.6(7) .
C8 C9 Ru1 C10 113.9(8) .
C10 C9 Ru1 C8 -113.9(8) .
C8 C9 Ru1 C2 -76.1(7) .
C10 C9 Ru1 C2 170.0(4) .
C8 C9 Ru1 C11 74.7(6) .
C10 C9 Ru1 C11 -39.1(4) .
C8 C9 Ru1 C1 -41.3(10) .
C10 C9 Ru1 C1 -155.2(6) .
C8 C9 Ru1 C4 -153.1(6) .
C10 C9 Ru1 C4 93.0(5) .
C8 C9 Ru1 C3 -113.9(6) .
C10 C9 Ru1 C3 132.3(4) .
C8 C9 Ru1 C7 33.1(6) .
C10 C9 Ru1 C7 -80.8(5) .
C8 C9 Ru1 C5 172.4(5) .
C10 C9 Ru1 C5 58.6(6) .
C11 C10 Ru1 C9 -114.1(6) .
C11 C10 Ru1 C8 -76.3(5) .
C9 C10 Ru1 C8 37.9(5) .
C11 C10 Ru1 C2 -141.9(9) .
C9 C10 Ru1 C2 -27.7(11) .
C11 C10 Ru1 C6 66.7(5) .
C9 C10 Ru1 C6 -179.1(4) .
C9 C10 Ru1 C11 114.1(6) .
C11 C10 Ru1 C1 28.2(11) .
C9 C10 Ru1 C1 142.4(9) .
C11 C10 Ru1 C4 142.3(4) .
C9 C10 Ru1 C4 -103.6(5) .
C11 C10 Ru1 C3 178.7(4) .
C9 C10 Ru1 C3 -67.2(6) .
C11 C10 Ru1 C7 -36.5(4) .
C9 C10 Ru1 C7 77.6(5) .
C11 C10 Ru1 C5 102.7(4) .
C9 C10 Ru1 C5 -143.2(5) .
C7 C8 Ru1 C9 123.4(9) .
C7 C8 Ru1 C10 81.1(5) .
C9 C8 Ru1 C10 -42.3(6) .
C7 C8 Ru1 C2 -116.6(5) .
C9 C8 Ru1 C2 120.0(6) .
C7 C8 Ru1 C6 -42.8(8) .
C9 C8 Ru1 C6 -166.2(5) .
C7 C8 Ru1 C11 37.1(4) .
C9 C8 Ru1 C11 -86.4(6) .
C7 C8 Ru1 C1 -77.6(5) .
C9 C8 Ru1 C1 158.9(6) .
C7 C8 Ru1 C4 168.3(5) .
C9 C8 Ru1 C4 44.9(9) .
C7 C8 Ru1 C3 -155.7(4) .
C9 C8 Ru1 C3 80.8(7) .
C9 C8 Ru1 C7 -123.4(9) .
C1 C2 Ru1 C9 153.5(5) .
C3 C2 Ru1 C9 -74.8(7) .
C1 C2 Ru1 C10 174.7(8) .
C3 C2 Ru1 C10 -53.6(13) .
C1 C2 Ru1 C8 115.6(5) .
C3 C2 Ru1 C8 -112.7(6) .
C1 C2 Ru1 C6 -28.9(5) .
C3 C2 Ru1 C6 102.9(7) .
C1 C2 Ru1 C11 54.9(8) .
C3 C2 Ru1 C11 -173.4(5) .
C3 C2 Ru1 C1 131.8(9) .
C1 C2 Ru1 C4 -102.5(5) .
C3 C2 Ru1 C4 29.3(6) .
C1 C2 Ru1 C3 -131.8(9) .
C1 C2 Ru1 C7 78.9(6) .
C3 C2 Ru1 C7 -149.3(6) .
C1 C2 Ru1 C5 -65.4(5) .
C3 C2 Ru1 C5 66.3(6) .
C1 C6 Ru1 C10 -160.0(4) .
C5 C6 Ru1 C10 67.1(7) .
C1 C6 Ru1 C8 -56.8(8) .
C5 C6 Ru1 C8 170.3(5) .
C1 C6 Ru1 C2 29.5(5) .
C5 C6 Ru1 C2 -103.4(7) .
C1 C6 Ru1 C11 -122.5(5) .
C5 C6 Ru1 C11 104.6(6) .
C5 C6 Ru1 C1 -132.9(8) .
C1 C6 Ru1 C4 103.9(5) .
C5 C6 Ru1 C4 -29.0(6) .
C1 C6 Ru1 C3 66.7(5) .
C5 C6 Ru1 C3 -66.2(6) .
C1 C6 Ru1 C7 -82.9(5) .
C5 C6 Ru1 C7 144.2(6) .
C1 C6 Ru1 C5 132.9(8) .
C7 C11 Ru1 C9 -76.7(5) .
C10 C11 Ru1 C9 41.6(5) .
C12 C11 Ru1 C9 162.0(7) .
C7 C11 Ru1 C10 -118.3(6) .
C12 C11 Ru1 C10 120.5(7) .
C7 C11 Ru1 C8 -35.3(4) .
C10 C11 Ru1 C8 83.0(5) .
C12 C11 Ru1 C8 -156.5(7) .
C7 C11 Ru1 C2 35.8(8) .
C10 C11 Ru1 C2 154.0(6) .
C12 C11 Ru1 C2 -85.5(8) .
C7 C11 Ru1 C6 109.6(4) .
C10 C11 Ru1 C6 -132.2(4) .
C12 C11 Ru1 C6 -11.7(6) .
C7 C11 Ru1 C1 72.5(5) .
C10 C11 Ru1 C1 -169.3(4) .
C12 C11 Ru1 C1 -48.8(7) .
C7 C11 Ru1 C4 -175.3(4) .
C10 C11 Ru1 C4 -57.0(6) .
C12 C11 Ru1 C4 63.4(7) .
C7 C11 Ru1 C3 -123.4(14) .
C10 C11 Ru1 C3 -5.1(17) .
C12 C11 Ru1 C3 115.4(15) .
C10 C11 Ru1 C7 118.3(6) .
C12 C11 Ru1 C7 -121.3(7) .
C7 C11 Ru1 C5 148.8(4) .
C10 C11 Ru1 C5 -93.0(5) .
C12 C11 Ru1 C5 27.5(6) .
C6 C1 Ru1 C9 174.9(6) .
C2 C1 Ru1 C9 -53.1(8) .
C6 C1 Ru1 C10 53.2(11) .
C2 C1 Ru1 C10 -174.8(8) .
C6 C1 Ru1 C8 147.8(5) .
C2 C1 Ru1 C8 -80.2(6) .
C6 C1 Ru1 C2 -132.0(7) .
C2 C1 Ru1 C6 132.0(7) .
C6 C1 Ru1 C11 74.1(5) .
C2 C1 Ru1 C11 -153.9(5) .
C6 C1 Ru1 C4 -65.4(5) .
C2 C1 Ru1 C4 66.6(5) .
C6 C1 Ru1 C3 -102.6(5) .
C2 C1 Ru1 C3 29.4(5) .
C6 C1 Ru1 C7 111.4(5) .
C2 C1 Ru1 C7 -116.6(5) .
C6 C1 Ru1 C5 -28.7(5) .
C2 C1 Ru1 C5 103.3(6) .
C5 C4 Ru1 C9 -141.8(5) .
C3 C4 Ru1 C9 86.7(6) .
C5 C4 Ru1 C10 -97.3(5) .
C3 C4 Ru1 C10 131.2(5) .
C5 C4 Ru1 C8 -169.4(5) .
C3 C4 Ru1 C8 59.1(7) .
C5 C4 Ru1 C2 102.2(5) .
C3 C4 Ru1 C2 -29.3(5) .
C5 C4 Ru1 C6 28.8(5) .
C3 C4 Ru1 C6 -102.7(5) .
C5 C4 Ru1 C11 -63.3(6) .
C3 C4 Ru1 C11 165.2(4) .
C5 C4 Ru1 C1 65.0(5) .
C3 C4 Ru1 C1 -66.5(5) .
C5 C4 Ru1 C3 131.5(7) .
C3 C4 Ru1 C5 -131.5(7) .
C2 C3 Ru1 C9 121.1(6) .
C4 C3 Ru1 C9 -106.9(5) .
C2 C3 Ru1 C10 160.6(5) .
C4 C3 Ru1 C10 -67.4(6) .
C2 C3 Ru1 C8 82.6(7) .
C4 C3 Ru1 C8 -145.3(5) .
C4 C3 Ru1 C2 132.0(9) .
C2 C3 Ru1 C6 -65.9(6) .
C4 C3 Ru1 C6 66.2(5) .
C2 C3 Ru1 C11 164.8(12) .
C4 C3 Ru1 C11 -63.2(17) .
C2 C3 Ru1 C1 -29.5(6) .
C4 C3 Ru1 C1 102.6(5) .
C2 C3 Ru1 C4 -132.0(9) .
C2 C3 Ru1 C7 56.1(9) .
C4 C3 Ru1 C7 -171.8(5) .
C2 C3 Ru1 C5 -102.6(7) .
C4 C3 Ru1 C5 29.5(5) .
C8 C7 Ru1 C9 -34.5(6) .
C11 C7 Ru1 C9 84.7(5) .
C15 C7 Ru1 C9 -157.1(7) .
C8 C7 Ru1 C10 -81.1(5) .
C11 C7 Ru1 C10 38.1(4) .
C15 C7 Ru1 C10 156.2(7) .
C11 C7 Ru1 C8 119.2(7) .
C15 C7 Ru1 C8 -122.7(8) .
C8 C7 Ru1 C2 78.3(6) .
C11 C7 Ru1 C2 -162.5(4) .
C15 C7 Ru1 C2 -44.3(7) .
C8 C7 Ru1 C6 155.1(5) .
C11 C7 Ru1 C6 -85.7(5) .
C15 C7 Ru1 C6 32.5(7) .
C8 C7 Ru1 C11 -119.2(7) .
C15 C7 Ru1 C11 118.1(8) .
C8 C7 Ru1 C1 116.9(5) .
C11 C7 Ru1 C1 -123.9(4) .
C15 C7 Ru1 C1 -5.7(7) .
C11 C7 Ru1 C3 162.1(5) .
C15 C7 Ru1 C3 -79.7(8) .
C8 C7 Ru1 C5 -170.0(5) .
C11 C7 Ru1 C5 -50.8(6) .
C15 C7 Ru1 C5 67.3(8) .
C6 C5 Ru1 C9 -168.3(5) .
C4 C5 Ru1 C9 59.3(7) .
C6 C5 Ru1 C10 -131.4(6) .
C4 C5 Ru1 C10 96.1(5) .
C6 C5 Ru1 C2 65.6(6) .
C4 C5 Ru1 C2 -66.9(5) .
C4 C5 Ru1 C6 -132.5(9) .
C6 C5 Ru1 C11 -89.5(6) .
C4 C5 Ru1 C11 138.0(5) .
C6 C5 Ru1 C1 28.5(5) .
C4 C5 Ru1 C1 -104.0(5) .
C6 C5 Ru1 C4 132.5(9) .
C6 C5 Ru1 C3 102.8(6) .
C4 C5 Ru1 C3 -29.6(5) .
C6 C5 Ru1 C7 -58.7(8) .
C4 C5 Ru1 C7 168.8(5) .
C24 C19 C20 C21 -4.3(16) .
Ru2 C19 C20 C21 -56.5(9) .
C24 C19 C20 Ru2 52.2(8) .
C19 C20 C21 C22 2.9(14) .
Ru2 C20 C21 C22 -53.9(8) .
C19 C20 C21 Ru2 56.9(9) .
C20 C21 C22 C23 -0.9(15) .
Ru2 C21 C22 C23 -54.5(9) .
C20 C21 C22 Ru2 53.6(7) .
C21 C22 C23 C24 0.5(16) .
Ru2 C22 C23 C24 -53.9(8) .
C21 C22 C23 Ru2 54.4(9) .
C22 C23 C24 C19 -1.9(14) .
Ru2 C23 C24 C19 -55.8(7) .
C22 C23 C24 Ru2 53.9(9) .
C20 C19 C24 C23 3.8(13) .
Ru2 C19 C24 C23 55.8(7) .
C20 C19 C24 Ru2 -52.0(8) .
C29 C25 C26 C27 -1.5(8) .
C33 C25 C26 C27 -179.0(7) .
Ru2 C25 C26 C27 60.6(5) .
C29 C25 C26 Ru2 -62.1(5) .
C33 C25 C26 Ru2 120.4(8) .
C25 C26 C27 C28 0.3(9) .
Ru2 C26 C27 C28 61.0(6) .
C25 C26 C27 Ru2 -60.8(5) .
C26 C27 C28 C29 1.1(9) .
Ru2 C27 C28 C29 63.4(5) .
C26 C27 C28 Ru2 -62.3(6) .
C26 C25 C29 C28 2.2(7) .
C33 C25 C29 C28 -179.8(6) .
Ru2 C25 C29 C28 -61.2(5) .
C26 C25 C29 C30 -174.7(8) .
C33 C25 C29 C30 3.2(11) .
Ru2 C25 C29 C30 121.9(8) .
C26 C25 C29 Ru2 63.4(5) .
C33 C25 C29 Ru2 -118.6(5) .
C27 C28 C29 C25 -1.9(8) .
Ru2 C28 C29 C25 61.7(5) .
C27 C28 C29 C30 175.3(7) .
Ru2 C28 C29 C30 -121.0(7) .
C27 C28 C29 Ru2 -63.6(5) .
C25 C29 C30 C31 -19.3(10) .
C28 C29 C30 C31 164.1(6) .
Ru2 C29 C30 C31 76.5(8) .
C29 C30 C31 O3 161.5(5) .
C29 C30 C31 C32 49.9(7) .
O3 C31 C32 O4 45.7(6) .
C30 C31 C32 O4 166.1(5) .
O3 C31 C32 C33 168.3(5) .
C30 C31 C32 C33 -71.4(7) .
O4 C32 C33 C25 164.6(5) .
C31 C32 C33 C25 48.9(8) .
C26 C25 C33 C32 160.8(8) .
C29 C25 C33 C32 -16.5(8) .
Ru2 C25 C33 C32 -99.8(7) .
C30 C31 O3 C34 -156.7(5) .
C32 C31 O3 C34 -37.4(6) .
O4 C34 O3 C31 16.3(6) .
C36 C34 O3 C31 -101.1(7) .
C35 C34 O3 C31 133.0(6) .
C31 C32 O4 C34 -36.6(6) .
C33 C32 O4 C34 -158.4(5) .
O3 C34 O4 C32 13.8(6) .
C36 C34 O4 C32 133.6(5) .
C35 C34 O4 C32 -104.0(5) .
C27 C28 Ru2 C29 113.2(7) .
C29 C28 Ru2 C27 -113.2(7) .
C27 C28 Ru2 C25 75.6(5) .
C29 C28 Ru2 C25 -37.6(4) .
C27 C28 Ru2 C26 35.5(5) .
C29 C28 Ru2 C26 -77.7(5) .
C27 C28 Ru2 C24 -162.5(5) .
C29 C28 Ru2 C24 84.3(5) .
C27 C28 Ru2 C21 -51.9(7) .
C29 C28 Ru2 C21 -165.1(5) .
C27 C28 Ru2 C22 -86.3(5) .
C29 C28 Ru2 C22 160.5(5) .
C27 C28 Ru2 C23 -125.1(5) .
C29 C28 Ru2 C23 121.7(5) .
C27 C28 Ru2 C19 162.4(5) .
C29 C28 Ru2 C19 49.2(7) .
C25 C29 Ru2 C28 -117.1(6) .
C30 C29 Ru2 C28 115.4(9) .
C25 C29 Ru2 C27 -77.2(4) .
C28 C29 Ru2 C27 39.9(4) .
C30 C29 Ru2 C27 155.3(9) .
C28 C29 Ru2 C25 117.1(6) .
C30 C29 Ru2 C25 -127.6(10) .
C25 C29 Ru2 C20 53.5(6) .
C28 C29 Ru2 C20 170.6(5) .
C30 C29 Ru2 C20 -74.0(9) .
C25 C29 Ru2 C26 -36.1(4) .
C28 C29 Ru2 C26 81.0(5) .
C30 C29 Ru2 C26 -163.6(9) .
C25 C29 Ru2 C24 130.2(4) .
C28 C29 Ru2 C24 -112.7(4) .
C30 C29 Ru2 C24 2.7(8) .
C25 C29 Ru2 C22 -155.4(6) .
C28 C29 Ru2 C22 -38.4(8) .
C30 C29 Ru2 C22 77.0(10) .
C25 C29 Ru2 C23 167.6(4) .
C28 C29 Ru2 C23 -75.3(5) .
C30 C29 Ru2 C23 40.1(9) .
C25 C29 Ru2 C19 89.9(5) .
C28 C29 Ru2 C19 -153.0(4) .
C30 C29 Ru2 C19 -37.6(9) .
C26 C27 Ru2 C28 119.1(7) .
C26 C27 Ru2 C29 78.5(5) .
C28 C27 Ru2 C29 -40.6(5) .
C26 C27 Ru2 C25 35.1(5) .
C28 C27 Ru2 C25 -84.0(5) .
C26 C27 Ru2 C20 -56.6(7) .
C28 C27 Ru2 C20 -175.7(4) .
C28 C27 Ru2 C26 -119.1(7) .
C26 C27 Ru2 C24 155.2(7) .
C28 C27 Ru2 C24 36.1(9) .
C26 C27 Ru2 C21 -92.1(5) .
C28 C27 Ru2 C21 148.9(4) .
C26 C27 Ru2 C22 -131.4(5) .
C28 C27 Ru2 C22 109.5(5) .
C26 C27 Ru2 C23 -169.0(5) .
C28 C27 Ru2 C23 71.9(6) .
C26 C27 Ru2 C19 -7.0(16) .
C28 C27 Ru2 C19 -126.0(12) .
C26 C25 Ru2 C28 -78.9(5) .
C29 C25 Ru2 C28 38.6(4) .
C33 C25 Ru2 C28 147.5(8) .
C26 C25 Ru2 C29 -117.5(6) .
C33 C25 Ru2 C29 108.9(9) .
C26 C25 Ru2 C27 -35.6(5) .
C29 C25 Ru2 C27 81.9(4) .
C33 C25 Ru2 C27 -169.2(8) .
C26 C25 Ru2 C20 96.4(5) .
C29 C25 Ru2 C20 -146.1(4) .
C33 C25 Ru2 C20 -37.2(8) .
C29 C25 Ru2 C26 117.5(6) .
C33 C25 Ru2 C26 -133.6(9) .
C26 C25 Ru2 C24 174.3(5) .
C29 C25 Ru2 C24 -68.3(5) .
C33 C25 Ru2 C24 40.6(8) .
C26 C25 Ru2 C21 60.4(6) .
C29 C25 Ru2 C21 177.9(5) .
C33 C25 Ru2 C21 -73.2(8) .
C26 C25 Ru2 C22 16.6(12) .
C29 C25 Ru2 C22 134.1(10) .
C33 C25 Ru2 C22 -117.0(11) .
C26 C25 Ru2 C23 -147.3(8) .
C29 C25 Ru2 C23 -29.8(9) .
C33 C25 Ru2 C23 79.1(10) .
C26 C25 Ru2 C19 136.2(5) .
C29 C25 Ru2 C19 -106.4(4) .
C33 C25 Ru2 C19 2.5(8) .
C21 C20 Ru2 C29 -165.9(5) .
C19 C20 Ru2 C29 62.5(8) .
C21 C20 Ru2 C27 -63.2(6) .
C19 C20 Ru2 C27 165.2(5) .
C21 C20 Ru2 C25 -133.6(5) .
C19 C20 Ru2 C25 94.8(7) .
C21 C20 Ru2 C26 -95.1(5) .
C19 C20 Ru2 C26 133.3(6) .
C21 C20 Ru2 C24 102.0(5) .
C19 C20 Ru2 C24 -29.6(6) .
C19 C20 Ru2 C21 -131.6(9) .
C21 C20 Ru2 C22 28.9(5) .
C19 C20 Ru2 C22 -102.7(7) .
C21 C20 Ru2 C23 65.7(5) .
C19 C20 Ru2 C23 -65.8(6) .
C21 C20 Ru2 C19 131.6(9) .
C25 C26 Ru2 C28 82.8(5) .
C27 C26 Ru2 C28 -37.6(5) .
C25 C26 Ru2 C29 38.4(4) .
C27 C26 Ru2 C29 -81.9(5) .
C25 C26 Ru2 C27 120.4(7) .
C27 C26 Ru2 C25 -120.4(7) .
C25 C26 Ru2 C20 -97.9(5) .
C27 C26 Ru2 C20 141.7(5) .
C25 C26 Ru2 C24 -16.5(14) .
C27 C26 Ru2 C24 -136.9(11) .
C25 C26 Ru2 C21 -137.1(5) .
C27 C26 Ru2 C21 102.5(5) .
C25 C26 Ru2 C22 -174.1(5) .
C27 C26 Ru2 C22 65.5(6) .
C25 C26 Ru2 C23 146.6(8) .
C27 C26 Ru2 C23 26.2(11) .
C25 C26 Ru2 C19 -61.5(6) .
C27 C26 Ru2 C19 178.1(4) .
C23 C24 Ru2 C28 79.0(5) .
C19 C24 Ru2 C28 -149.6(4) .
C23 C24 Ru2 C29 120.4(5) .
C19 C24 Ru2 C29 -108.2(5) .
C23 C24 Ru2 C27 54.3(9) .
C19 C24 Ru2 C27 -174.2(6) .
C23 C24 Ru2 C25 157.6(5) .
C19 C24 Ru2 C25 -70.9(5) .
C23 C24 Ru2 C20 -102.4(6) .
C19 C24 Ru2 C20 29.1(5) .
C23 C24 Ru2 C26 169.9(11) .
C19 C24 Ru2 C26 -58.6(13) .
C23 C24 Ru2 C21 -65.8(5) .
C19 C24 Ru2 C21 65.7(5) .
C23 C24 Ru2 C22 -29.1(6) .
C19 C24 Ru2 C22 102.4(5) .
C19 C24 Ru2 C23 131.4(7) .
C23 C24 Ru2 C19 -131.4(7) .
C20 C21 Ru2 C28 169.9(5) .
C22 C21 Ru2 C28 -57.5(7) .
C20 C21 Ru2 C27 137.8(5) .
C22 C21 Ru2 C27 -89.6(5) .
C20 C21 Ru2 C25 66.1(6) .
C22 C21 Ru2 C25 -161.2(5) .
C22 C21 Ru2 C20 132.7(7) .
C20 C21 Ru2 C26 98.8(5) .
C22 C21 Ru2 C26 -128.5(5) .
C20 C21 Ru2 C24 -67.2(5) .
C22 C21 Ru2 C24 65.5(5) .
C20 C21 Ru2 C22 -132.7(7) .
C20 C21 Ru2 C23 -103.3(5) .
C22 C21 Ru2 C23 29.4(5) .
C20 C21 Ru2 C19 -29.5(5) .
C22 C21 Ru2 C19 103.1(6) .
C21 C22 Ru2 C28 145.4(5) .
C23 C22 Ru2 C28 -82.8(7) .
C21 C22 Ru2 C29 171.3(6) .
C23 C22 Ru2 C29 -56.9(10) .
C21 C22 Ru2 C27 104.6(5) .
C23 C22 Ru2 C27 -123.6(6) .
C21 C22 Ru2 C25 57.8(12) .
C23 C22 Ru2 C25 -170.4(7) .
C21 C22 Ru2 C20 -28.6(5) .
C23 C22 Ru2 C20 103.2(7) .
C21 C22 Ru2 C26 70.1(6) .
C23 C22 Ru2 C26 -158.1(6) .
C21 C22 Ru2 C24 -103.3(5) .
C23 C22 Ru2 C24 28.5(6) .
C23 C22 Ru2 C21 131.8(9) .
C21 C22 Ru2 C23 -131.8(9) .
C21 C22 Ru2 C19 -65.6(5) .
C23 C22 Ru2 C19 66.2(6) .
C24 C23 Ru2 C28 -115.7(5) .
C22 C23 Ru2 C28 111.7(6) .
C24 C23 Ru2 C29 -76.2(6) .
C22 C23 Ru2 C29 151.2(6) .
C24 C23 Ru2 C27 -153.8(5) .
C22 C23 Ru2 C27 73.6(7) .
C24 C23 Ru2 C25 -54.8(10) .
C22 C23 Ru2 C25 172.6(5) .
C24 C23 Ru2 C20 66.9(5) .
C22 C23 Ru2 C20 -65.6(6) .
C24 C23 Ru2 C26 -172.2(8) .
C22 C23 Ru2 C26 55.2(12) .
C22 C23 Ru2 C24 -132.6(9) .
C24 C23 Ru2 C21 103.3(5) .
C22 C23 Ru2 C21 -29.3(6) .
C24 C23 Ru2 C22 132.6(9) .
C24 C23 Ru2 C19 30.1(5) .
C22 C23 Ru2 C19 -102.5(7) .
C20 C19 Ru2 C28 -172.6(5) .
C24 C19 Ru2 C28 55.4(7) .
C20 C19 Ru2 C29 -140.7(6) .
C24 C19 Ru2 C29 87.3(5) .
C20 C19 Ru2 C27 -60.9(16) .
C24 C19 Ru2 C27 167.1(12) .
C20 C19 Ru2 C25 -99.6(6) .
C24 C19 Ru2 C25 128.4(5) .
C24 C19 Ru2 C20 -132.0(9) .
C20 C19 Ru2 C26 -66.5(8) .
C24 C19 Ru2 C26 161.5(5) .
C20 C19 Ru2 C24 132.0(9) .
C20 C19 Ru2 C21 29.2(6) .
C24 C19 Ru2 C21 -102.8(4) .
C20 C19 Ru2 C22 66.0(6) .
C24 C19 Ru2 C22 -66.0(5) .
C20 C19 Ru2 C23 103.0(7) .
C24 C19 Ru2 C23 -29.0(5) .
C42 C37 C38 C39 -0.6(13) .
Ru3 C37 C38 C39 -54.7(9) .
C42 C37 C38 Ru3 54.1(7) .
C37 C38 C39 C40 0.5(17) .
Ru3 C38 C39 C40 -54.1(10) .
C37 C38 C39 Ru3 54.7(8) .
C38 C39 C40 C41 -0.6(16) .
Ru3 C39 C40 C41 -55.0(7) .
C38 C39 C40 Ru3 54.4(10) .
C39 C40 C41 C42 0.9(15) .
Ru3 C40 C41 C42 -53.8(9) .
C39 C40 C41 Ru3 54.6(7) .
C38 C37 C42 C41 0.9(14) .
Ru3 C37 C42 C41 55.3(10) .
C38 C37 C42 Ru3 -54.4(7) .
C40 C41 C42 C37 -1.0(17) .
Ru3 C41 C42 C37 -55.4(9) .
C40 C41 C42 Ru3 54.3(9) .
C47 C43 C44 C45 -2.0(10) .
C51 C43 C44 C45 -177.7(8) .
Ru3 C43 C44 C45 60.6(7) .
C47 C43 C44 Ru3 -62.6(6) .
C51 C43 C44 Ru3 121.7(8) .
C43 C44 C45 C46 0.9(11) .
Ru3 C44 C45 C46 61.8(6) .
C43 C44 C45 Ru3 -60.9(6) .
C44 C45 C46 C47 0.4(10) .
Ru3 C45 C46 C47 62.9(6) .
C44 C45 C46 Ru3 -62.5(7) .
C44 C43 C47 C46 2.2(9) .
C51 C43 C47 C46 177.7(8) .
Ru3 C43 C47 C46 -59.7(5) .
C44 C43 C47 C48 -177.6(6) .
C51 C43 C47 C48 -2.1(13) .
Ru3 C43 C47 C48 120.5(6) .
C44 C43 C47 Ru3 61.9(6) .
C51 C43 C47 Ru3 -122.6(9) .
C45 C46 C47 C43 -1.7(9) .
Ru3 C46 C47 C43 61.0(5) .
C45 C46 C47 C48 178.2(7) .
Ru3 C46 C47 C48 -119.1(8) .
C45 C46 C47 Ru3 -62.7(6) .
C43 C47 C48 C49 -16.3(9) .
C46 C47 C48 C49 163.9(7) .
Ru3 C47 C48 C49 72.3(8) .
C47 C48 C49 O5 163.4(5) .
C47 C48 C49 C50 50.3(7) .
O5 C49 C50 O6 42.9(6) .
C48 C49 C50 O6 163.4(5) .
O5 C49 C50 C51 166.7(6) .
C48 C49 C50 C51 -72.8(7) .
O6 C50 C51 C43 163.2(6) .
C49 C50 C51 C43 48.5(8) .
C47 C43 C51 C50 -13.7(11) .
C44 C43 C51 C50 161.1(7) .
Ru3 C43 C51 C50 -108.4(7) .
C48 C49 O5 C52 -152.9(5) .
C50 C49 O5 C52 -34.7(6) .
O6 C52 O5 C49 13.4(6) .
C53 C52 O5 C49 130.3(6) .
C54 C52 O5 C49 -103.0(6) .
C51 C50 O6 C52 -156.8(5) .
C49 C50 O6 C52 -35.5(6) .
O5 C52 O6 C50 15.3(6) .
C53 C52 O6 C50 -100.9(8) .
C54 C52 O6 C50 133.8(7) .
C47 C46 Ru3 C45 -117.7(7) .
C45 C46 Ru3 C43 82.0(5) .
C47 C46 Ru3 C43 -35.7(4) .
C45 C46 Ru3 C47 117.7(7) .
C45 C46 Ru3 C39 -65.7(6) .
C47 C46 Ru3 C39 176.6(5) .
C45 C46 Ru3 C44 38.3(5) .
C47 C46 Ru3 C44 -79.4(5) .
C45 C46 Ru3 C42 -176.4(5) .
C47 C46 Ru3 C42 65.9(6) .
C45 C46 Ru3 C37 143.0(11) .
C47 C46 Ru3 C37 25.3(13) .
C45 C46 Ru3 C41 -140.2(5) .
C47 C46 Ru3 C41 102.1(5) .
C45 C46 Ru3 C40 -101.1(5) .
C47 C46 Ru3 C40 141.2(5) .
C45 C46 Ru3 C38 -26.6(11) .
C47 C46 Ru3 C38 -144.3(8) .
C44 C45 Ru3 C46 117.0(8) .
C46 C45 Ru3 C43 -78.9(6) .
C44 C45 Ru3 C43 38.1(5) .
C46 C45 Ru3 C47 -38.0(5) .
C44 C45 Ru3 C47 79.0(6) .
C46 C45 Ru3 C39 131.6(5) .
C44 C45 Ru3 C39 -111.4(6) .
C46 C45 Ru3 C44 -117.0(8) .
C46 C45 Ru3 C42 14.7(18) .
C44 C45 Ru3 C42 131.8(15) .
C46 C45 Ru3 C37 -157.2(7) .
C44 C45 Ru3 C37 -40.2(10) .
C46 C45 Ru3 C41 59.1(7) .
C44 C45 Ru3 C41 176.1(5) .
C46 C45 Ru3 C40 93.2(5) .
C44 C45 Ru3 C40 -149.8(5) .
C46 C45 Ru3 C38 168.6(5) .
C44 C45 Ru3 C38 -74.4(6) .
C47 C43 Ru3 C46 37.6(5) .
C44 C43 Ru3 C46 -79.7(5) .
C51 C43 Ru3 C46 161.5(9) .
C47 C43 Ru3 C45 79.6(5) .
C44 C43 Ru3 C45 -37.6(5) .
C51 C43 Ru3 C45 -156.5(9) .
C44 C43 Ru3 C47 -117.3(7) .
C51 C43 Ru3 C47 123.9(9) .
C47 C43 Ru3 C39 159.5(6) .
C44 C43 Ru3 C39 42.2(9) .
C51 C43 Ru3 C39 -76.6(10) .
C47 C43 Ru3 C44 117.3(7) .
C51 C43 Ru3 C44 -118.9(10) .
C47 C43 Ru3 C42 -88.6(5) .
C44 C43 Ru3 C42 154.2(5) .
C51 C43 Ru3 C42 35.3(8) .
C47 C43 Ru3 C37 -127.3(5) .
C44 C43 Ru3 C37 115.4(5) .
C51 C43 Ru3 C37 -3.5(8) .
C47 C43 Ru3 C41 -52.5(7) .
C44 C43 Ru3 C41 -169.8(4) .
C51 C43 Ru3 C41 71.3(9) .
C47 C43 Ru3 C38 -166.9(4) .
C44 C43 Ru3 C38 75.8(5) .
C51 C43 Ru3 C38 -43.0(8) .
C43 C47 Ru3 C46 -119.0(6) .
C48 C47 Ru3 C46 125.0(10) .
C43 C47 Ru3 C45 -81.9(5) .
C46 C47 Ru3 C45 37.1(5) .
C48 C47 Ru3 C45 162.1(8) .
C46 C47 Ru3 C43 119.0(6) .
C48 C47 Ru3 C43 -116.0(9) .
C43 C47 Ru3 C39 -130.8(14) .
C46 C47 Ru3 C39 -11.8(16) .
C48 C47 Ru3 C39 113.3(13) .
C43 C47 Ru3 C44 -38.8(4) .
C46 C47 Ru3 C44 80.2(5) .
C48 C47 Ru3 C44 -154.7(8) .
C43 C47 Ru3 C42 107.0(5) .
C46 C47 Ru3 C42 -134.0(5) .
C48 C47 Ru3 C42 -8.9(8) .
C43 C47 Ru3 C37 69.6(6) .
C46 C47 Ru3 C37 -171.4(5) .
C48 C47 Ru3 C37 -46.3(9) .
C43 C47 Ru3 C41 147.0(5) .
C46 C47 Ru3 C41 -94.0(5) .
C48 C47 Ru3 C41 31.1(8) .
C43 C47 Ru3 C40 -176.6(5) .
C46 C47 Ru3 C40 -57.6(6) .
C48 C47 Ru3 C40 67.4(8) .
C43 C47 Ru3 C38 28.5(9) .
C46 C47 Ru3 C38 147.5(7) .
C48 C47 Ru3 C38 -87.5(10) .
C40 C39 Ru3 C46 -67.4(6) .
C38 C39 Ru3 C46 156.7(6) .
C40 C39 Ru3 C45 -103.0(5) .
C38 C39 Ru3 C45 121.1(6) .
C40 C39 Ru3 C43 -171.5(6) .
C38 C39 Ru3 C43 52.5(10) .
C40 C39 Ru3 C47 -58.0(16) .
C38 C39 Ru3 C47 166.1(11) .
C40 C39 Ru3 C44 -143.4(5) .
C38 C39 Ru3 C44 80.7(7) .
C40 C39 Ru3 C42 67.3(5) .
C38 C39 Ru3 C42 -68.7(6) .
C40 C39 Ru3 C37 104.1(5) .
C38 C39 Ru3 C37 -31.9(6) .
C40 C39 Ru3 C41 30.0(5) .
C38 C39 Ru3 C41 -105.9(7) .
C38 C39 Ru3 C40 -135.9(9) .
C40 C39 Ru3 C38 135.9(9) .
C45 C44 Ru3 C46 -37.5(5) .
C43 C44 Ru3 C46 80.0(6) .
C43 C44 Ru3 C45 117.5(8) .
C45 C44 Ru3 C43 -117.5(8) .
C45 C44 Ru3 C47 -81.0(6) .
C43 C44 Ru3 C47 36.5(5) .
C45 C44 Ru3 C39 84.3(6) .
C43 C44 Ru3 C39 -158.2(5) .
C45 C44 Ru3 C42 -165.0(5) .
C43 C44 Ru3 C42 -47.5(8) .
C45 C44 Ru3 C37 160.9(5) .
C43 C44 Ru3 C37 -81.6(6) .
C45 C44 Ru3 C40 49.2(8) .
C43 C44 Ru3 C40 166.7(5) .
C45 C44 Ru3 C38 121.9(6) .
C43 C44 Ru3 C38 -120.6(5) .
C37 C42 Ru3 C46 -162.0(5) .
C41 C42 Ru3 C46 65.8(8) .
C37 C42 Ru3 C45 -174.1(14) .
C41 C42 Ru3 C45 53.7(19) .
C37 C42 Ru3 C43 -85.5(6) .
C41 C42 Ru3 C43 142.3(6) .
C37 C42 Ru3 C47 -124.8(5) .
C41 C42 Ru3 C47 103.0(6) .
C37 C42 Ru3 C39 66.6(5) .
C41 C42 Ru3 C39 -65.6(6) .
C37 C42 Ru3 C44 -54.6(8) .
C41 C42 Ru3 C44 173.2(5) .
C41 C42 Ru3 C37 -132.2(9) .
C37 C42 Ru3 C41 132.2(9) .
C37 C42 Ru3 C40 103.2(5) .
C41 C42 Ru3 C40 -29.0(6) .
C37 C42 Ru3 C38 29.7(5) .
C41 C42 Ru3 C38 -102.5(7) .
C42 C37 Ru3 C46 54.0(13) .
C38 C37 Ru3 C46 -173.8(10) .
C42 C37 Ru3 C45 177.5(6) .
C38 C37 Ru3 C45 -50.3(9) .
C42 C37 Ru3 C43 109.3(5) .
C38 C37 Ru3 C43 -118.5(5) .
C42 C37 Ru3 C47 73.3(6) .
C38 C37 Ru3 C47 -154.5(5) .
C42 C37 Ru3 C39 -101.7(6) .
C38 C37 Ru3 C39 30.5(5) .
C42 C37 Ru3 C44 150.0(5) .
C38 C37 Ru3 C44 -77.8(5) .
C38 C37 Ru3 C42 132.2(7) .
C42 C37 Ru3 C41 -29.2(5) .
C38 C37 Ru3 C41 103.0(5) .
C42 C37 Ru3 C40 -65.7(5) .
C38 C37 Ru3 C40 66.5(5) .
C42 C37 Ru3 C38 -132.2(7) .
C40 C41 Ru3 C46 94.3(5) .
C42 C41 Ru3 C46 -133.7(6) .
C40 C41 Ru3 C45 60.4(6) .
C42 C41 Ru3 C45 -167.7(5) .
C40 C41 Ru3 C43 167.0(5) .
C42 C41 Ru3 C43 -61.1(8) .
C40 C41 Ru3 C47 135.9(5) .
C42 C41 Ru3 C47 -92.1(6) .
C40 C41 Ru3 C39 -29.7(5) .
C42 C41 Ru3 C39 102.3(7) .
C40 C41 Ru3 C42 -132.0(9) .
C40 C41 Ru3 C37 -103.1(5) .
C42 C41 Ru3 C37 28.8(6) .
C42 C41 Ru3 C40 132.0(9) .
C40 C41 Ru3 C38 -65.3(5) .
C42 C41 Ru3 C38 66.7(6) .
C39 C40 Ru3 C46 130.2(6) .
C41 C40 Ru3 C46 -99.2(5) .
C39 C40 Ru3 C45 90.1(6) .
C41 C40 Ru3 C45 -139.3(5) .
C39 C40 Ru3 C47 164.0(5) .
C41 C40 Ru3 C47 -65.4(6) .
C41 C40 Ru3 C39 130.6(8) .
C39 C40 Ru3 C44 59.8(7) .
C41 C40 Ru3 C44 -169.7(5) .
C39 C40 Ru3 C42 -101.2(6) .
C41 C40 Ru3 C42 29.4(5) .
C39 C40 Ru3 C37 -64.8(5) .
C41 C40 Ru3 C37 65.7(5) .
C39 C40 Ru3 C41 -130.6(8) .
C39 C40 Ru3 C38 -26.7(5) .
C41 C40 Ru3 C38 103.8(5) .
C39 C38 Ru3 C46 -56.1(12) .
C37 C38 Ru3 C46 175.3(7) .
C39 C38 Ru3 C45 -74.9(7) .
C37 C38 Ru3 C45 156.4(5) .
C39 C38 Ru3 C43 -152.7(6) .
C37 C38 Ru3 C43 78.6(6) .
C39 C38 Ru3 C47 -172.2(6) .
C37 C38 Ru3 C47 59.1(9) .
C37 C38 Ru3 C39 -128.6(9) .
C39 C38 Ru3 C44 -113.4(6) .
C37 C38 Ru3 C44 117.9(5) .
C39 C38 Ru3 C42 100.0(7) .
C37 C38 Ru3 C42 -28.6(5) .
C39 C38 Ru3 C37 128.6(9) .
C39 C38 Ru3 C41 63.0(6) .
C37 C38 Ru3 C41 -65.6(5) .
C39 C38 Ru3 C40 26.7(6) .
C37 C38 Ru3 C40 -101.9(5) .
C60 C55 C56 C57 -1.7(16) .
Ru4 C55 C56 C57 -54.8(8) .
C60 C55 C56 Ru4 53.2(8) .
C55 C56 C57 C58 0.6(14) .
Ru4 C56 C57 C58 -54.8(7) .
C55 C56 C57 Ru4 55.4(9) .
C56 C57 C58 C59 0.7(13) .
Ru4 C57 C58 C59 -53.4(9) .
C56 C57 C58 Ru4 54.2(7) .
C57 C58 C59 C60 -1.0(17) .
Ru4 C58 C59 C60 -54.8(10) .
C57 C58 C59 Ru4 53.8(8) .
C58 C59 C60 C55 -0.1(15) .
Ru4 C59 C60 C55 -54.8(7) .
C58 C59 C60 Ru4 54.7(10) .
C56 C55 C60 C59 1.4(14) .
Ru4 C55 C60 C59 54.4(8) .
C56 C55 C60 Ru4 -53.0(9) .
C65 C61 C62 C63 -0.4(8) .
C69 C61 C62 C63 -179.7(7) .
Ru4 C61 C62 C63 61.5(5) .
C65 C61 C62 Ru4 -62.0(4) .
C69 C61 C62 Ru4 118.8(7) .
C61 C62 C63 C64 -0.6(10) .
Ru4 C62 C63 C64 62.1(8) .
C61 C62 C63 Ru4 -62.7(5) .
C62 C63 C64 C65 1.5(12) .
Ru4 C63 C64 C65 63.8(7) .
C62 C63 C64 Ru4 -62.3(6) .
C63 C64 C65 C61 -1.8(11) .
Ru4 C64 C65 C61 60.5(5) .
C63 C64 C65 C66 176.3(9) .
Ru4 C64 C65 C66 -121.4(8) .
C63 C64 C65 Ru4 -62.3(8) .
C62 C61 C65 C64 1.4(8) .
C69 C61 C65 C64 -179.4(7) .
Ru4 C61 C65 C64 -60.2(6) .
C62 C61 C65 C66 -176.9(7) .
C69 C61 C65 C66 2.3(11) .
Ru4 C61 C65 C66 121.6(7) .
C62 C61 C65 Ru4 61.5(4) .
C69 C61 C65 Ru4 -119.2(7) .
C64 C65 C66 C67 164.0(8) .
C61 C65 C66 C67 -18.1(9) .
Ru4 C65 C66 C67 70.7(7) .
C65 C66 C67 O7 162.1(5) .
C65 C66 C67 C68 50.6(7) .
O7 C67 C68 O8 45.2(6) .
C66 C67 C68 O8 164.9(5) .
O7 C67 C68 C69 168.0(5) .
C66 C67 C68 C69 -72.3(7) .
C62 C61 C69 C68 163.4(6) .
C65 C61 C69 C68 -15.6(9) .
Ru4 C61 C69 C68 -106.6(6) .
O8 C68 C69 C61 164.4(5) .
C67 C68 C69 C61 48.0(7) .
C68 C67 O7 C70 -39.0(6) .
C66 C67 O7 C70 -158.5(5) .
O8 C70 O7 C67 18.3(6) .
C72 C70 O7 C67 -97.2(8) .
C71 C70 O7 C67 132.8(6) .
C67 C68 O8 C70 -35.1(6) .
C69 C68 O8 C70 -157.9(5) .
O7 C70 O8 C68 11.6(6) .
C72 C70 O8 C68 132.0(5) .
C71 C70 O8 C68 -104.9(5) .
C65 C64 Ru4 C63 -119.4(8) .
C65 C64 Ru4 C62 -80.7(5) .
C63 C64 Ru4 C62 38.7(6) .
C65 C64 Ru4 C59 116.6(5) .
C63 C64 Ru4 C59 -124.0(6) .
C65 C64 Ru4 C61 -37.8(4) .
C63 C64 Ru4 C61 81.6(6) .
C63 C64 Ru4 C65 119.4(8) .
C65 C64 Ru4 C57 -167.5(5) .
C63 C64 Ru4 C57 -48.1(9) .
C65 C64 Ru4 C60 79.3(5) .
C63 C64 Ru4 C60 -161.3(6) .
C65 C64 Ru4 C55 43.6(8) .
C63 C64 Ru4 C55 163.0(5) .
C65 C64 Ru4 C58 156.8(5) .
C63 C64 Ru4 C58 -83.8(7) .
C62 C63 Ru4 C64 116.8(8) .
C64 C63 Ru4 C62 -116.8(8) .
C64 C63 Ru4 C59 73.5(7) .
C62 C63 Ru4 C59 -169.6(4) .
C64 C63 Ru4 C61 -78.6(6) .
C62 C63 Ru4 C61 38.2(4) .
C64 C63 Ru4 C65 -35.3(5) .
C62 C63 Ru4 C65 81.5(5) .
C64 C63 Ru4 C56 -172.8(5) .
C62 C63 Ru4 C56 -56.0(7) .
C64 C63 Ru4 C57 151.0(6) .
C62 C63 Ru4 C57 -92.1(5) .
C64 C63 Ru4 C60 38.0(11) .
C62 C63 Ru4 C60 154.8(6) .
C64 C63 Ru4 C55 -119.1(16) .
C62 C63 Ru4 C55 -2.2(19) .
C64 C63 Ru4 C58 111.3(6) .
C62 C63 Ru4 C58 -131.9(5) .
C61 C62 Ru4 C64 78.7(5) .
C63 C62 Ru4 C64 -37.4(5) .
C61 C62 Ru4 C63 116.1(6) .
C61 C62 Ru4 C59 144.6(9) .
C63 C62 Ru4 C59 28.5(12) .
C63 C62 Ru4 C61 -116.1(6) .
C61 C62 Ru4 C65 38.4(4) .
C63 C62 Ru4 C65 -77.7(5) .
C61 C62 Ru4 C56 -100.5(4) .
C63 C62 Ru4 C56 143.4(5) .
C61 C62 Ru4 C57 -140.6(4) .
C63 C62 Ru4 C57 103.3(5) .
C61 C62 Ru4 C60 -24.7(12) .
C63 C62 Ru4 C60 -140.8(9) .
C61 C62 Ru4 C55 -64.4(5) .
C63 C62 Ru4 C55 179.5(5) .
C61 C62 Ru4 C58 -177.7(4) .
C63 C62 Ru4 C58 66.2(6) .
C60 C59 Ru4 C64 -115.0(5) .
C58 C59 Ru4 C64 110.0(6) .
C60 C59 Ru4 C63 -153.0(5) .
C58 C59 Ru4 C63 72.0(7) .
C60 C59 Ru4 C62 -174.4(9) .
C58 C59 Ru4 C62 50.6(13) .
C60 C59 Ru4 C61 -51.1(9) .
C58 C59 Ru4 C61 173.9(5) .
C60 C59 Ru4 C65 -77.7(6) .
C58 C59 Ru4 C65 147.3(5) .
C60 C59 Ru4 C56 66.3(5) .
C58 C59 Ru4 C56 -68.7(6) .
C60 C59 Ru4 C57 104.0(5) .
C58 C59 Ru4 C57 -30.9(6) .
C58 C59 Ru4 C60 -135.0(9) .
C60 C59 Ru4 C55 29.5(5) .
C58 C59 Ru4 C55 -105.5(7) .
C60 C59 Ru4 C58 135.0(9) .
C62 C61 Ru4 C64 -81.3(5) .
C65 C61 Ru4 C64 35.3(5) .
C69 C61 Ru4 C64 157.2(7) .
C62 C61 Ru4 C63 -38.9(5) .
C65 C61 Ru4 C63 77.6(5) .
C69 C61 Ru4 C63 -160.4(7) .
C65 C61 Ru4 C62 116.6(6) .
C69 C61 Ru4 C62 -121.5(7) .
C62 C61 Ru4 C59 -155.2(7) .
C65 C61 Ru4 C59 -38.7(9) .
C69 C61 Ru4 C59 83.3(8) .
C62 C61 Ru4 C65 -116.6(6) .
C69 C61 Ru4 C65 121.9(8) .
C62 C61 Ru4 C56 94.4(5) .
C65 C61 Ru4 C56 -149.1(4) .
C69 C61 Ru4 C56 -27.1(7) .
C62 C61 Ru4 C57 58.1(6) .
C65 C61 Ru4 C57 174.6(5) .
C69 C61 Ru4 C57 -63.4(8) .
C62 C61 Ru4 C60 171.0(4) .
C65 C61 Ru4 C60 -72.4(5) .
C69 C61 Ru4 C60 49.5(7) .
C62 C61 Ru4 C55 133.8(4) .
C65 C61 Ru4 C55 -109.6(4) .
C69 C61 Ru4 C55 12.3(6) .
C62 C61 Ru4 C58 8.0(13) .
C65 C61 Ru4 C58 124.6(11) .
C69 C61 Ru4 C58 -113.5(12) .
C61 C65 Ru4 C64 -118.9(7) .
C66 C65 Ru4 C64 124.7(8) .
C64 C65 Ru4 C63 36.9(6) .
C61 C65 Ru4 C63 -82.0(5) .
C66 C65 Ru4 C63 161.7(7) .
C64 C65 Ru4 C62 80.8(5) .
C61 C65 Ru4 C62 -38.1(4) .
C66 C65 Ru4 C62 -154.5(7) .
C64 C65 Ru4 C59 -79.1(6) .
C61 C65 Ru4 C59 162.0(4) .
C66 C65 Ru4 C59 45.6(7) .
C64 C65 Ru4 C61 118.9(7) .
C66 C65 Ru4 C61 -116.4(8) .
C64 C65 Ru4 C56 169.3(5) .
C61 C65 Ru4 C56 50.4(7) .
C66 C65 Ru4 C56 -66.0(8) .
C64 C65 Ru4 C60 -115.8(5) .
C61 C65 Ru4 C60 125.3(4) .
C66 C65 Ru4 C60 8.9(7) .
C64 C65 Ru4 C55 -154.9(5) .
C61 C65 Ru4 C55 86.2(5) .
C66 C65 Ru4 C55 -30.2(7) .
C64 C65 Ru4 C58 -40.9(8) .
C61 C65 Ru4 C58 -159.8(5) .
C66 C65 Ru4 C58 83.8(8) .
C55 C56 Ru4 C63 165.7(5) .
C57 C56 Ru4 C63 -62.6(7) .
C55 C56 Ru4 C62 132.2(6) .
C57 C56 Ru4 C62 -96.1(5) .
C55 C56 Ru4 C59 -64.4(6) .
C57 C56 Ru4 C59 67.3(5) .
C55 C56 Ru4 C61 91.4(6) .
C57 C56 Ru4 C61 -136.9(5) .
C55 C56 Ru4 C65 60.4(8) .
C57 C56 Ru4 C65 -167.9(5) .
C55 C56 Ru4 C57 -131.7(9) .
C55 C56 Ru4 C60 -29.0(5) .
C57 C56 Ru4 C60 102.8(5) .
C57 C56 Ru4 C55 131.7(9) .
C55 C56 Ru4 C58 -102.6(6) .
C57 C56 Ru4 C58 29.1(5) .
C56 C57 Ru4 C64 168.8(5) .
C58 C57 Ru4 C64 -58.8(7) .
C56 C57 Ru4 C63 139.2(5) .
C58 C57 Ru4 C63 -88.3(6) .
C56 C57 Ru4 C62 97.6(5) .
C58 C57 Ru4 C62 -129.9(5) .
C56 C57 Ru4 C59 -101.3(6) .
C58 C57 Ru4 C59 31.2(5) .
C56 C57 Ru4 C61 64.0(6) .
C58 C57 Ru4 C61 -163.6(5) .
C58 C57 Ru4 C56 132.5(7) .
C56 C57 Ru4 C60 -66.1(5) .
C58 C57 Ru4 C60 66.4(5) .
C56 C57 Ru4 C55 -29.3(5) .
C58 C57 Ru4 C55 103.2(5) .
C56 C57 Ru4 C58 -132.5(7) .
C59 C60 Ru4 C64 80.3(6) .
C55 C60 Ru4 C64 -147.7(5) .
C59 C60 Ru4 C63 54.9(9) .
C55 C60 Ru4 C63 -173.1(6) .
C59 C60 Ru4 C62 174.3(9) .
C55 C60 Ru4 C62 -53.7(12) .
C55 C60 Ru4 C59 132.0(7) .
C59 C60 Ru4 C61 155.9(5) .
C55 C60 Ru4 C61 -72.1(5) .
C59 C60 Ru4 C65 117.5(5) .
C55 C60 Ru4 C65 -110.5(5) .
C59 C60 Ru4 C56 -103.0(6) .
C55 C60 Ru4 C56 29.0(5) .
C59 C60 Ru4 C57 -65.6(5) .
C55 C60 Ru4 C57 66.4(5) .
C59 C60 Ru4 C55 -132.0(7) .
C59 C60 Ru4 C58 -28.2(5) .
C55 C60 Ru4 C58 103.8(5) .
C56 C55 Ru4 C64 -169.9(5) .
C60 C55 Ru4 C64 57.7(7) .
C56 C55 Ru4 C63 -64.7(18) .
C60 C55 Ru4 C63 162.9(15) .
C56 C55 Ru4 C62 -66.6(7) .
C60 C55 Ru4 C62 161.0(4) .
C56 C55 Ru4 C59 103.9(7) .
C60 C55 Ru4 C59 -28.4(5) .
C56 C55 Ru4 C61 -102.4(6) .
C60 C55 Ru4 C61 125.2(5) .
C56 C55 Ru4 C65 -143.1(6) .
C60 C55 Ru4 C65 84.5(5) .
C60 C55 Ru4 C56 -132.4(8) .
C56 C55 Ru4 C57 29.7(6) .
C60 C55 Ru4 C57 -102.7(4) .
C56 C55 Ru4 C60 132.4(8) .
C56 C55 Ru4 C58 66.9(6) .
C60 C55 Ru4 C58 -65.5(5) .
C57 C58 Ru4 C64 145.1(5) .
C59 C58 Ru4 C64 -85.8(7) .
C57 C58 Ru4 C63 105.7(5) .
C59 C58 Ru4 C63 -125.2(6) .
C57 C58 Ru4 C62 68.8(6) .
C59 C58 Ru4 C62 -162.1(6) .
C57 C58 Ru4 C59 -129.1(9) .
C57 C58 Ru4 C61 62.5(13) .
C59 C58 Ru4 C61 -168.4(9) .
C57 C58 Ru4 C65 170.5(5) .
C59 C58 Ru4 C65 -60.4(9) .
C57 C58 Ru4 C56 -29.1(5) .
C59 C58 Ru4 C56 100.0(7) .
C59 C58 Ru4 C57 129.1(9) .
C57 C58 Ru4 C60 -102.5(5) .
C59 C58 Ru4 C60 26.6(6) .
C57 C58 Ru4 C55 -66.0(5) .
C59 C58 Ru4 C55 63.2(6) .
Cl1 C73A Cl1 C73B 0.000(14) 2_557
Cl1 C73B Cl1 C73A 0.000(15) 2_557
Cl2 C74A Cl2 C74B 0.000(5) 2_556
Cl2 C74B Cl2 C74A 0.000(5) 2_556
