#------------------------------------------------------------------------------
#$Date: 2016-03-21 09:44:23 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178627 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/38/4073856.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4073856
loop_
_publ_author_name
'Xiang, Li'
'Wang, Qiuwen'
'Song, Haibin'
'Zi, Guofu'
_publ_section_title
;
 Synthesis, Structural Characterization, and Reactivity of
 Organolanthanides Derived from a New Chiral Ligand,
 (R)-Bis(pyrrol-2-ylmethyleneamino)-1,1‘-binaphthyl
;
_journal_issue                   22
_journal_name_full               Organometallics
_journal_page_first              5323
_journal_paper_doi               10.1021/om7006826
_journal_volume                  26
_journal_year                    2007
_chemical_absolute_configuration rmad
_chemical_formula_moiety         'C98.67 H69.33 N12 Yb2'
_chemical_formula_sum            'C98.67 H69.33 N12 Yb2'
_chemical_formula_weight         1769.07
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           5
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  'C 2y'
_symmetry_space_group_name_H-M   'C 1 2 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 111.308(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            6
_cell_length_a                   25.536(3)
_cell_length_b                   22.103(2)
_cell_length_c                   25.583(3)
_cell_measurement_reflns_used    15337
_cell_measurement_temperature    113(2)
_cell_measurement_theta_max      27.9
_cell_measurement_theta_min      1.7
_cell_volume                     13453(3)
_computing_cell_refinement       CrystalClear
_computing_data_collection       CrystalClear
_computing_data_reduction        CrystalClear
_computing_publication_material  'CrystalStructure 3.7.0'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      113(2)
_diffrn_detector_area_resol_mean 7.31
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Rigaku Saturn'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  confocal
_diffrn_radiation_source         'rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71070
_diffrn_reflns_av_R_equivalents  0.0645
_diffrn_reflns_av_sigmaI/netI    0.1059
_diffrn_reflns_limit_h_max       33
_diffrn_reflns_limit_h_min       -32
_diffrn_reflns_limit_k_max       28
_diffrn_reflns_limit_k_min       -28
_diffrn_reflns_limit_l_max       33
_diffrn_reflns_limit_l_min       -33
_diffrn_reflns_number            63422
_diffrn_reflns_theta_full        27.87
_diffrn_reflns_theta_max         27.87
_diffrn_reflns_theta_min         1.61
_exptl_absorpt_coefficient_mu    2.124
_exptl_absorpt_correction_T_max  0.8157
_exptl_absorpt_correction_T_min  0.7553
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'Jacobson, R. (1998) Private communication'
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.310
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             5312
_exptl_crystal_size_max          0.14
_exptl_crystal_size_mid          0.12
_exptl_crystal_size_min          0.10
_platon_squeeze_details
;
;
_refine_diff_density_max         1.631
_refine_diff_density_min         -1.306
_refine_diff_density_rms         0.134
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.042(7)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.051
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1512
_refine_ls_number_reflns         31053
_refine_ls_number_restraints     44
_refine_ls_restrained_S_all      1.051
_refine_ls_R_factor_all          0.0696
_refine_ls_R_factor_gt           0.0599
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0372P)²+7.7536P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1203
_refine_ls_wR_factor_ref         0.1275
_reflns_number_gt                27015
_reflns_number_total             31053
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om7006826-file002.cif
_cod_data_source_block           compound7
_cod_database_code               4073856
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Yb1 Yb 0.254231(12) 0.408477(15) 1.011078(12) 0.02449(7) Uani 1 1 d .
Yb2 Yb 0.176756(13) 0.413464(15) 0.822177(12) 0.02351(7) Uani 1 1 d .
Yb3 Yb 1.0000 0.79400(2) 0.5000 0.02447(10) Uani 1 2 d S
Yb4 Yb 1.0000 0.58641(2) 0.5000 0.02290(10) Uani 1 2 d S
N1 N 0.2408(3) 0.3821(3) 1.0976(3) 0.0277(15) Uani 1 1 d .
N2 N 0.3386(3) 0.4298(3) 1.0938(2) 0.0255(14) Uani 1 1 d .
N3 N 0.2108(3) 0.4895(3) 1.0402(3) 0.0274(15) Uani 1 1 d .
N4 N 0.3166(3) 0.3265(3) 1.0287(3) 0.0327(16) Uani 1 1 d .
N5 N 0.1062(3) 0.4703(3) 0.8595(3) 0.0303(15) Uani 1 1 d .
N6 N 0.0990(2) 0.4591(3) 0.7461(2) 0.0224(13) Uani 1 1 d .
N7 N 0.1668(3) 0.3670(3) 0.9021(3) 0.0317(16) Uani 1 1 d .
N8 N 0.2021(3) 0.5102(3) 0.7997(3) 0.0303(16) Uani 1 1 d .
N9 N 0.2698(3) 0.3492(3) 0.8527(3) 0.0255(14) Uani 1 1 d .
N10 N 0.2003(2) 0.3847(3) 0.7414(2) 0.0244(14) Uani 1 1 d .
N11 N 0.2490(3) 0.4490(3) 0.9067(3) 0.0299(15) Uani 1 1 d .
N12 N 0.1311(3) 0.3232(3) 0.7841(3) 0.0284(14) Uani 1 1 d .
N13 N 0.9332(2) 0.7517(3) 0.5432(2) 0.0227(13) Uani 1 1 d .
N14 N 0.9080(3) 0.8276(3) 0.4322(3) 0.0276(15) Uani 1 1 d .
N15 N 1.0358(2) 0.7019(3) 0.5561(2) 0.0226(13) Uani 1 1 d .
N16 N 1.0120(3) 0.8779(3) 0.4480(3) 0.0311(15) Uani 1 1 d .
N17 N 0.9831(3) 0.4951(3) 0.4430(3) 0.0278(15) Uani 1 1 d .
N18 N 1.0800(3) 0.5650(3) 0.4784(2) 0.0266(14) Uani 1 1 d .
C1 C 0.3229(3) 0.3704(4) 1.1828(3) 0.0259(17) Uani 1 1 d .
C2 C 0.2779(3) 0.3427(4) 1.1395(3) 0.0286(17) Uani 1 1 d .
C3 C 0.2739(4) 0.2804(4) 1.1348(3) 0.0308(18) Uani 1 1 d .
H3 H 0.2433 0.2628 1.1053 0.037 Uiso 1 1 calc R
C4 C 0.3127(4) 0.2440(4) 1.1714(3) 0.034(2) Uani 1 1 d .
H4 H 0.3091 0.2013 1.1673 0.041 Uiso 1 1 calc R
C5 C 0.3583(3) 0.2688(4) 1.2156(3) 0.0302(18) Uani 1 1 d .
C6 C 0.3646(3) 0.3326(4) 1.2213(3) 0.0293(18) Uani 1 1 d .
C7 C 0.4124(3) 0.3564(4) 1.2643(3) 0.0339(19) Uani 1 1 d .
H7 H 0.4160 0.3991 1.2690 0.041 Uiso 1 1 calc R
C8 C 0.4537(4) 0.3198(5) 1.2995(3) 0.037(2) Uani 1 1 d .
H8 H 0.4860 0.3367 1.3275 0.045 Uiso 1 1 calc R
C9 C 0.4471(4) 0.2566(5) 1.2931(4) 0.046(2) Uani 1 1 d .
H9 H 0.4753 0.2310 1.3177 0.055 Uiso 1 1 calc R
C10 C 0.4009(4) 0.2305(4) 1.2523(3) 0.038(2) Uani 1 1 d .
H10 H 0.3976 0.1878 1.2488 0.045 Uiso 1 1 calc R
C11 C 0.3295(3) 0.4378(4) 1.1841(3) 0.0282(18) Uani 1 1 d .
C12 C 0.3386(3) 0.4656(4) 1.1397(3) 0.0279(17) Uani 1 1 d .
C13 C 0.3448(4) 0.5308(4) 1.1389(4) 0.042(2) Uani 1 1 d .
H13 H 0.3507 0.5497 1.1082 0.050 Uiso 1 1 calc R
C14 C 0.3422(4) 0.5638(4) 1.1806(4) 0.045(2) Uani 1 1 d .
H14 H 0.3463 0.6064 1.1794 0.054 Uiso 1 1 calc R
C15 C 0.3333(4) 0.5372(4) 1.2282(4) 0.043(2) Uani 1 1 d .
C16 C 0.3241(3) 0.4744(4) 1.2282(3) 0.0296(18) Uani 1 1 d .
C17 C 0.3109(4) 0.4494(4) 1.2728(3) 0.039(2) Uani 1 1 d .
H17 H 0.3041 0.4071 1.2733 0.047 Uiso 1 1 calc R
C18 C 0.3078(4) 0.4852(5) 1.3147(4) 0.044(2) Uani 1 1 d .
H18 H 0.2982 0.4677 1.3440 0.052 Uiso 1 1 calc R
C19 C 0.3185(4) 0.5477(4) 1.3158(4) 0.053(3) Uani 1 1 d .
H19 H 0.3173 0.5723 1.3458 0.063 Uiso 1 1 calc R
C20 C 0.3307(4) 0.5720(5) 1.2723(4) 0.051(3) Uani 1 1 d .
H20 H 0.3375 0.6143 1.2723 0.061 Uiso 1 1 calc R
C21 C 0.2149(4) 0.4229(4) 1.1153(3) 0.036(2) Uani 1 1 d .
H21A H 0.2098 0.4165 1.1498 0.044 Uiso 1 1 calc R
C22 C 0.1940(4) 0.4763(4) 1.0851(3) 0.0311(19) Uani 1 1 d .
C23 C 0.1652(4) 0.5246(4) 1.0954(4) 0.042(2) Uani 1 1 d .
H23 H 0.1498 0.5274 1.1240 0.050 Uiso 1 1 calc R
C24 C 0.1632(4) 0.5681(5) 1.0561(4) 0.052(3) Uani 1 1 d .
H24 H 0.1455 0.6065 1.0521 0.063 Uiso 1 1 calc R
C25 C 0.1911(3) 0.5460(4) 1.0240(3) 0.0301(18) Uani 1 1 d .
H25 H 0.1961 0.5675 0.9939 0.036 Uiso 1 1 calc R
C26 C 0.3769(3) 0.3891(4) 1.1025(3) 0.0306(19) Uani 1 1 d .
H26A H 0.4113 0.3937 1.1333 0.037 Uiso 1 1 calc R
C27 C 0.3691(4) 0.3368(4) 1.0670(3) 0.0310(18) Uani 1 1 d .
C28 C 0.4067(4) 0.2905(4) 1.0696(4) 0.040(2) Uani 1 1 d .
H28 H 0.4450 0.2877 1.0936 0.048 Uiso 1 1 calc R
C29 C 0.3759(4) 0.2496(4) 1.0296(4) 0.044(2) Uani 1 1 d .
H29 H 0.3895 0.2129 1.0199 0.053 Uiso 1 1 calc R
C30 C 0.3204(4) 0.2722(4) 1.0056(3) 0.036(2) Uani 1 1 d .
H30 H 0.2903 0.2523 0.9775 0.043 Uiso 1 1 calc R
C31 C 0.0299(3) 0.5265(4) 0.7897(3) 0.0244(16) Uani 1 1 d .
C32 C 0.0753(3) 0.5251(4) 0.8389(3) 0.0290(18) Uani 1 1 d .
C33 C 0.0948(4) 0.5785(4) 0.8720(3) 0.036(2) Uani 1 1 d .
H33 H 0.1270 0.5766 0.9055 0.043 Uiso 1 1 calc R
C34 C 0.0672(4) 0.6319(4) 0.8555(3) 0.036(2) Uani 1 1 d .
H34 H 0.0803 0.6673 0.8775 0.043 Uiso 1 1 calc R
C35 C 0.0194(3) 0.6350(4) 0.8059(3) 0.0317(18) Uani 1 1 d .
C36 C 0.0025(3) 0.5835(4) 0.7708(3) 0.0249(15) Uani 1 1 d .
C37 C -0.0417(3) 0.5900(4) 0.7178(3) 0.0307(17) Uani 1 1 d .
H37 H -0.0518 0.5566 0.6927 0.037 Uiso 1 1 calc R
C38 C -0.0698(3) 0.6435(4) 0.7024(3) 0.0279(17) Uani 1 1 d .
H38 H -0.1000 0.6467 0.6673 0.034 Uiso 1 1 calc R
C39 C -0.0543(3) 0.6940(5) 0.7385(3) 0.041(2) Uani 1 1 d .
H39 H -0.0745 0.7309 0.7274 0.049 Uiso 1 1 calc R
C40 C -0.0120(3) 0.6911(5) 0.7877(3) 0.040(2) Uani 1 1 d .
H40 H -0.0021 0.7258 0.8112 0.048 Uiso 1 1 calc R
C41 C 0.0080(3) 0.4713(4) 0.7548(3) 0.0287(17) Uani 1 1 d .
C42 C 0.0418(3) 0.4390(3) 0.7322(3) 0.0220(15) Uani 1 1 d .
C43 C 0.0228(4) 0.3876(4) 0.6985(3) 0.036(2) Uani 1 1 d .
H43 H 0.0474 0.3660 0.6849 0.043 Uiso 1 1 calc R
C44 C -0.0315(3) 0.3691(4) 0.6855(3) 0.0318(18) Uani 1 1 d .
H44 H -0.0447 0.3351 0.6615 0.038 Uiso 1 1 calc R
C45 C -0.0687(3) 0.3989(4) 0.7065(3) 0.0307(18) Uani 1 1 d .
C46 C -0.0483(3) 0.4490(4) 0.7428(3) 0.0321(19) Uani 1 1 d .
C47 C -0.0858(4) 0.4763(4) 0.7665(4) 0.044(2) Uani 1 1 d .
H47 H -0.0726 0.5084 0.7926 0.052 Uiso 1 1 calc R
C48 C -0.1417(4) 0.4563(5) 0.7517(4) 0.044(2) Uani 1 1 d .
H48 H -0.1663 0.4752 0.7671 0.053 Uiso 1 1 calc R
C49 C -0.1602(3) 0.4083(6) 0.7142(4) 0.051(2) Uani 1 1 d .
H49 H -0.1981 0.3953 0.7031 0.061 Uiso 1 1 calc R
C50 C -0.1245(4) 0.3790(5) 0.6926(4) 0.051(3) Uani 1 1 d .
H50 H -0.1378 0.3453 0.6683 0.061 Uiso 1 1 calc R
C51 C 0.1098(3) 0.4519(3) 0.9080(3) 0.0263(17) Uani 1 1 d .
H51 H 0.0918 0.4742 0.9284 0.032 Uiso 1 1 calc R
C52 C 0.1404(3) 0.3984(3) 0.9320(3) 0.0253(17) Uani 1 1 d .
C53 C 0.1449(3) 0.3679(4) 0.9814(3) 0.0291(17) Uani 1 1 d .
H53A H 0.1303 0.3803 1.0090 0.035 Uiso 1 1 calc R
C54 C 0.1755(3) 0.3154(4) 0.9816(3) 0.0318(19) Uani 1 1 d .
H54A H 0.1861 0.2851 1.0099 0.038 Uiso 1 1 calc R
C55 C 0.1876(4) 0.3156(4) 0.9324(4) 0.0328(19) Uani 1 1 d .
H55A H 0.2075 0.2846 0.9217 0.039 Uiso 1 1 calc R
C56 C 0.1097(4) 0.5121(4) 0.7319(3) 0.0288(19) Uani 1 1 d .
H56A H 0.0802 0.5341 0.7050 0.035 Uiso 1 1 calc R
C57 C 0.1633(3) 0.5389(4) 0.7545(3) 0.0247(16) Uani 1 1 d .
C58 C 0.1840(3) 0.5935(4) 0.7432(3) 0.0323(19) Uani 1 1 d .
H58 H 0.1646 0.6221 0.7151 0.039 Uiso 1 1 calc R
C59 C 0.2393(3) 0.5976(3) 0.7817(3) 0.0282(17) Uani 1 1 d .
H59 H 0.2654 0.6291 0.7844 0.034 Uiso 1 1 calc R
C60 C 0.2481(3) 0.5463(4) 0.8152(3) 0.0281(18) Uani 1 1 d .
H60 H 0.2823 0.5376 0.8453 0.034 Uiso 1 1 calc R
C61 C 0.2909(3) 0.3027(3) 0.7756(3) 0.0234(16) Uani 1 1 d .
C62 C 0.2802(3) 0.2967(4) 0.8247(3) 0.0264(16) Uani 1 1 d .
C63 C 0.2762(4) 0.2395(4) 0.8473(4) 0.039(2) Uani 1 1 d .
H63 H 0.2689 0.2368 0.8811 0.047 Uiso 1 1 calc R
C64 C 0.2828(4) 0.1868(4) 0.8201(3) 0.0401(19) Uani 1 1 d .
H64 H 0.2818 0.1483 0.8361 0.048 Uiso 1 1 calc R
C65 C 0.2912(3) 0.1913(4) 0.7683(3) 0.0329(17) Uani 1 1 d .
C66 C 0.2943(3) 0.2483(4) 0.7457(4) 0.0321(19) Uani 1 1 d .
C67 C 0.2974(3) 0.2528(4) 0.6915(3) 0.0298(18) Uani 1 1 d .
H67 H 0.2985 0.2915 0.6757 0.036 Uiso 1 1 calc R
C68 C 0.2988(3) 0.2010(4) 0.6619(3) 0.035(2) Uani 1 1 d .
H68 H 0.3004 0.2038 0.6254 0.042 Uiso 1 1 calc R
C69 C 0.2979(4) 0.1436(4) 0.6864(4) 0.039(2) Uani 1 1 d .
H69 H 0.3004 0.1080 0.6667 0.047 Uiso 1 1 calc R
C70 C 0.2936(4) 0.1389(4) 0.7372(4) 0.043(2) Uani 1 1 d .
H70 H 0.2921 0.1000 0.7524 0.052 Uiso 1 1 calc R
C71 C 0.2971(3) 0.3634(3) 0.7540(3) 0.0230(15) Uani 1 1 d .
C72 C 0.2514(3) 0.4023(4) 0.7359(3) 0.0251(16) Uani 1 1 d .
C73 C 0.2554(4) 0.4604(4) 0.7152(3) 0.0328(18) Uani 1 1 d .
H73 H 0.2236 0.4864 0.7034 0.039 Uiso 1 1 calc R
C74 C 0.3054(4) 0.4797(4) 0.7123(3) 0.0338(19) Uani 1 1 d .
H74 H 0.3074 0.5186 0.6973 0.041 Uiso 1 1 calc R
C75 C 0.3551(3) 0.4422(3) 0.7312(3) 0.0259(17) Uani 1 1 d .
C76 C 0.3496(3) 0.3843(4) 0.7528(3) 0.0276(17) Uani 1 1 d .
C77 C 0.3995(3) 0.3474(4) 0.7712(3) 0.0287(17) Uani 1 1 d .
H77 H 0.3980 0.3083 0.7860 0.034 Uiso 1 1 calc R
C78 C 0.4481(4) 0.3671(4) 0.7680(4) 0.040(2) Uani 1 1 d .
H78 H 0.4805 0.3420 0.7810 0.048 Uiso 1 1 calc R
C79 C 0.4515(4) 0.4239(4) 0.7456(4) 0.045(2) Uani 1 1 d .
H79 H 0.4859 0.4365 0.7427 0.053 Uiso 1 1 calc R
C80 C 0.4053(4) 0.4621(4) 0.7277(4) 0.041(2) Uani 1 1 d .
H80 H 0.4080 0.5011 0.7133 0.049 Uiso 1 1 calc R
C81 C 0.3085(3) 0.3660(4) 0.8984(3) 0.0254(16) Uani 1 1 d .
H81 H 0.3425 0.3436 0.9131 0.030 Uiso 1 1 calc R
C82 C 0.3002(3) 0.4194(4) 0.9277(3) 0.0245(16) Uani 1 1 d .
C83 C 0.3381(3) 0.4503(4) 0.9727(3) 0.0283(18) Uani 1 1 d .
H83A H 0.3757 0.4390 0.9942 0.034 Uiso 1 1 calc R
C84 C 0.3091(4) 0.5023(4) 0.9797(3) 0.0336(19) Uani 1 1 d .
H84A H 0.3233 0.5326 1.0076 0.040 Uiso 1 1 calc R
C85 C 0.2563(4) 0.5007(4) 0.9383(3) 0.0293(18) Uani 1 1 d .
H85A H 0.2286 0.5313 0.9324 0.035 Uiso 1 1 calc R
C86 C 0.1770(3) 0.3344(4) 0.7179(3) 0.0279(18) Uani 1 1 d .
H86A H 0.1858 0.3184 0.6876 0.033 Uiso 1 1 calc R
C87 C 0.1391(3) 0.3032(4) 0.7364(3) 0.0286(18) Uani 1 1 d .
C88 C 0.1081(4) 0.2503(4) 0.7171(4) 0.037(2) Uani 1 1 d .
H88 H 0.1065 0.2275 0.6850 0.044 Uiso 1 1 calc R
C89 C 0.0808(4) 0.2371(4) 0.7527(4) 0.044(2) Uani 1 1 d .
H89 H 0.0568 0.2037 0.7505 0.053 Uiso 1 1 calc R
C90 C 0.0953(4) 0.2828(4) 0.7929(4) 0.039(2) Uani 1 1 d .
H90 H 0.0818 0.2853 0.8229 0.047 Uiso 1 1 calc R
C91 C 0.8417(3) 0.8022(3) 0.5003(3) 0.0289(18) Uani 1 1 d .
C92 C 0.8872(3) 0.7862(4) 0.5480(3) 0.0248(16) Uani 1 1 d .
C93 C 0.8926(4) 0.8088(3) 0.6021(3) 0.0307(19) Uani 1 1 d .
H93 H 0.9217 0.7943 0.6347 0.037 Uiso 1 1 calc R
C94 C 0.8561(4) 0.8509(4) 0.6066(3) 0.0346(19) Uani 1 1 d .
H94 H 0.8604 0.8659 0.6427 0.042 Uiso 1 1 calc R
C95 C 0.8125(4) 0.8730(4) 0.5601(3) 0.0347(19) Uani 1 1 d .
C96 C 0.8042(3) 0.8472(4) 0.5061(3) 0.0337(19) Uani 1 1 d .
C97 C 0.7600(4) 0.8684(4) 0.4585(4) 0.044(2) Uani 1 1 d .
H97 H 0.7524 0.8500 0.4230 0.053 Uiso 1 1 calc R
C98 C 0.7264(4) 0.9182(5) 0.4644(4) 0.049(2) Uani 1 1 d .
H98 H 0.6980 0.9348 0.4323 0.059 Uiso 1 1 calc R
C99 C 0.7353(4) 0.9416(5) 0.5161(4) 0.056(3) Uani 1 1 d .
H99 H 0.7114 0.9729 0.5198 0.067 Uiso 1 1 calc R
C100 C 0.7785(4) 0.9208(4) 0.5635(4) 0.044(2) Uani 1 1 d .
H100 H 0.7849 0.9395 0.5988 0.052 Uiso 1 1 calc R
C101 C 0.8309(3) 0.7737(4) 0.4451(3) 0.0291(18) Uani 1 1 d .
C102 C 0.8580(3) 0.7930(4) 0.4107(3) 0.0329(19) Uani 1 1 d .
C103 C 0.8394(4) 0.7725(4) 0.3542(3) 0.038(2) Uani 1 1 d .
H103 H 0.8574 0.7875 0.3302 0.045 Uiso 1 1 calc R
C104 C 0.7973(3) 0.7327(4) 0.3337(3) 0.038(2) Uani 1 1 d .
H104 H 0.7848 0.7216 0.2952 0.045 Uiso 1 1 calc R
C105 C 0.7714(3) 0.7073(4) 0.3684(3) 0.036(2) Uani 1 1 d .
C106 C 0.7869(3) 0.7292(4) 0.4252(3) 0.0340(19) Uani 1 1 d .
C107 C 0.7614(3) 0.7047(4) 0.4600(3) 0.0335(19) Uani 1 1 d .
H107 H 0.7702 0.7201 0.4969 0.040 Uiso 1 1 calc R
C108 C 0.7233(4) 0.6579(5) 0.4408(4) 0.045(2) Uani 1 1 d .
H108 H 0.7065 0.6411 0.4651 0.054 Uiso 1 1 calc R
C109 C 0.7090(4) 0.6344(5) 0.3860(4) 0.052(3) Uani 1 1 d .
H109 H 0.6834 0.6016 0.3741 0.063 Uiso 1 1 calc R
C110 C 0.7313(4) 0.6585(5) 0.3512(4) 0.051(3) Uani 1 1 d .
H110 H 0.7207 0.6431 0.3141 0.061 Uiso 1 1 calc R
C111 C 0.9501(3) 0.7058(3) 0.5746(3) 0.0235(16) Uani 1 1 d .
H111 H 0.9281 0.6910 0.5949 0.028 Uiso 1 1 calc R
C112 C 1.0010(3) 0.6763(3) 0.5800(3) 0.0242(16) Uani 1 1 d .
C113 C 1.0260(3) 0.6243(3) 0.6103(3) 0.0228(15) Uani 1 1 d .
H11A H 1.0110 0.5992 0.6316 0.027 Uiso 1 1 calc R
C114 C 1.0779(3) 0.6164(4) 0.6029(3) 0.0306(18) Uani 1 1 d .
H11B H 1.1042 0.5845 0.6171 0.037 Uiso 1 1 calc R
C115 C 1.0825(3) 0.6657(3) 0.5703(3) 0.0228(16) Uani 1 1 d .
H11C H 1.1138 0.6730 0.5595 0.027 Uiso 1 1 calc R
C116 C 0.9128(4) 0.8744(4) 0.4024(3) 0.036(2) Uani 1 1 d .
H116 H 0.8802 0.8891 0.3732 0.043 Uiso 1 1 calc R
C117 C 0.9631(4) 0.9024(4) 0.4122(3) 0.036(2) Uani 1 1 d .
C118 C 0.9754(4) 0.9575(4) 0.3881(3) 0.042(2) Uani 1 1 d .
H118 H 0.9492 0.9834 0.3617 0.050 Uiso 1 1 calc R
C119 C 1.0321(4) 0.9644(4) 0.4111(4) 0.044(2) Uani 1 1 d .
H119 H 1.0533 0.9963 0.4035 0.053 Uiso 1 1 calc R
C120 C 1.0538(4) 0.9155(4) 0.4483(3) 0.0351(18) Uani 1 1 d .
H120 H 1.0924 0.9099 0.4705 0.042 Uiso 1 1 calc R
C121 C 0.9694(3) 0.3999(4) 0.4826(3) 0.0277(17) Uani 1 1 d .
C122 C 0.9468(3) 0.4468(3) 0.4443(3) 0.0248(16) Uani 1 1 d .
C123 C 0.8896(4) 0.4474(4) 0.4106(3) 0.035(2) Uani 1 1 d .
H123 H 0.8751 0.4786 0.3835 0.042 Uiso 1 1 calc R
C124 C 0.8543(3) 0.4034(5) 0.4163(4) 0.043(2) Uani 1 1 d .
H124 H 0.8157 0.4043 0.3929 0.051 Uiso 1 1 calc R
C125 C 0.8740(4) 0.3572(4) 0.4561(4) 0.043(2) Uani 1 1 d .
C126 C 0.9328(4) 0.3548(4) 0.4901(4) 0.039(2) Uani 1 1 d .
C127 C 0.9531(5) 0.3095(5) 0.5327(5) 0.056(3) Uani 1 1 d .
H127 H 0.9919 0.3070 0.5554 0.067 Uiso 1 1 calc R
C128 C 0.9148(5) 0.2694(5) 0.5399(6) 0.063(3) Uani 1 1 d .
H128 H 0.9280 0.2376 0.5664 0.075 Uiso 1 1 calc R
C129 C 0.8570(5) 0.2742(5) 0.5091(6) 0.067(3) Uani 1 1 d .
H129 H 0.8310 0.2486 0.5171 0.080 Uiso 1 1 calc R
C130 C 0.8392(5) 0.3153(5) 0.4686(6) 0.075(4) Uani 1 1 d .
H130 H 0.8002 0.3164 0.4466 0.090 Uiso 1 1 calc R
C131 C 1.0243(3) 0.4824(4) 0.4253(3) 0.0281(18) Uani 1 1 d .
H13A H 1.0222 0.4466 0.4042 0.034 Uiso 1 1 calc R
C132 C 1.0712(3) 0.5206(4) 0.4369(3) 0.0255(17) Uani 1 1 d .
C133 C 1.1135(4) 0.5210(4) 0.4151(3) 0.034(2) Uani 1 1 d .
H133 H 1.1166 0.4955 0.3864 0.041 Uiso 1 1 calc R
C134 C 1.1505(4) 0.5661(4) 0.4434(4) 0.042(2) Uani 1 1 d .
H134 H 1.1838 0.5778 0.4377 0.051 Uiso 1 1 calc R
C135 C 1.1294(3) 0.5913(4) 0.4820(3) 0.0293(17) Uani 1 1 d .
H135 H 1.1474 0.6229 0.5074 0.035 Uiso 1 1 calc R
C136 C 0.9607(10) 0.1428(14) 0.4269(13) 0.245(14) Uani 1 1 d DU
H13B H 0.9459 0.1757 0.3999 0.368 Uiso 1 1 calc R
H13C H 0.9772 0.1116 0.4104 0.368 Uiso 1 1 calc R
H13D H 0.9896 0.1588 0.4610 0.368 Uiso 1 1 calc R
C137 C 0.9146(5) 0.1162(7) 0.4414(5) 0.152(8) Uani 1 1 d GDU
C138 C 0.9140(5) 0.0567(6) 0.4588(4) 0.091(4) Uani 1 1 d GU
H138 H 0.9457 0.0315 0.4650 0.109 Uiso 1 1 calc R
C139 C 0.8668(7) 0.0342(5) 0.4673(5) 0.162(9) Uani 1 1 d GU
H139 H 0.8664 -0.0064 0.4792 0.194 Uiso 1 1 calc R
C140 C 0.8203(5) 0.0712(7) 0.4583(5) 0.161(9) Uani 1 1 d GU
H140 H 0.7881 0.0558 0.4641 0.194 Uiso 1 1 calc R
C141 C 0.8209(5) 0.1307(7) 0.4409(5) 0.130(6) Uani 1 1 d GU
H141 H 0.7892 0.1559 0.4347 0.156 Uiso 1 1 calc R
C142 C 0.8681(7) 0.1532(5) 0.4324(5) 0.131(7) Uani 1 1 d GU
H142 H 0.8685 0.1938 0.4204 0.158 Uiso 1 1 calc R
C143 C 0.1939(8) 0.1604(5) 0.9634(6) 0.079(4) Uani 1 1 d .
H143 H 0.2167 0.1606 0.9412 0.095 Uiso 1 1 calc R
C144 C 0.1383(9) 0.1626(6) 0.9386(7) 0.096(5) Uani 1 1 d .
H144 H 0.1225 0.1622 0.8987 0.115 Uiso 1 1 calc R
C145 C 0.1026(9) 0.1653(8) 0.9674(11) 0.135(8) Uani 1 1 d .
H145 H 0.0634 0.1713 0.9482 0.162 Uiso 1 1 calc R
C146 C 0.1260(9) 0.1587(8) 1.0289(10) 0.144(9) Uani 1 1 d .
H146 H 0.1032 0.1571 1.0510 0.173 Uiso 1 1 calc R
C147 C 0.1839(9) 0.1551(6) 1.0516(6) 0.097(6) Uani 1 1 d .
H147 H 0.2008 0.1505 1.0912 0.116 Uiso 1 1 calc R
C148 C 0.2192(6) 0.1576(5) 1.0219(6) 0.068(3) Uani 1 1 d .
H148 H 0.2589 0.1575 1.0403 0.082 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Yb Yb -0.3850 5.5486 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N4 Yb1 N3 152.6(2) . .
N4 Yb1 N1 87.2(2) . .
N3 Yb1 N1 70.0(2) . .
N4 Yb1 N2 70.2(2) . .
N3 Yb1 N2 87.0(2) . .
N1 Yb1 N2 68.4(2) . .
N4 Yb1 C53 110.5(2) . .
N3 Yb1 C53 77.9(2) . .
N1 Yb1 C53 73.1(2) . .
N2 Yb1 C53 141.4(2) . .
N4 Yb1 C85 121.3(3) . .
N3 Yb1 C85 77.3(2) . .
N1 Yb1 C85 146.2(2) . .
N2 Yb1 C85 102.3(2) . .
C53 Yb1 C85 108.5(2) . .
N4 Yb1 N11 103.0(2) . .
N3 Yb1 N11 101.3(2) . .
N1 Yb1 N11 168.8(2) . .
N2 Yb1 N11 119.2(2) . .
C53 Yb1 N11 98.6(2) . .
C85 Yb1 N11 28.7(2) . .
N4 Yb1 C84 104.7(3) . .
N3 Yb1 C84 82.5(3) . .
N1 Yb1 C84 134.0(2) . .
N2 Yb1 C84 74.3(2) . .
C53 Yb1 C84 136.7(2) . .
C85 Yb1 C84 28.8(2) . .
N11 Yb1 C84 48.2(2) . .
N4 Yb1 C54 81.6(3) . .
N3 Yb1 C54 105.7(2) . .
N1 Yb1 C54 75.0(2) . .
N2 Yb1 C54 134.2(2) . .
C53 Yb1 C54 29.2(2) . .
C85 Yb1 C54 123.3(2) . .
N11 Yb1 C54 101.6(2) . .
C84 Yb1 C54 149.8(2) . .
N4 Yb1 C82 76.6(2) . .
N3 Yb1 C82 123.4(2) . .
N1 Yb1 C82 162.4(2) . .
N2 Yb1 C82 99.3(2) . .
C53 Yb1 C82 118.8(2) . .
C85 Yb1 C82 46.3(2) . .
N11 Yb1 C82 28.75(19) . .
C84 Yb1 C82 47.1(2) . .
C54 Yb1 C82 108.6(2) . .
N4 Yb1 C83 76.7(2) . .
N3 Yb1 C83 111.4(2) . .
N1 Yb1 C83 140.6(2) . .
N2 Yb1 C83 72.4(2) . .
C53 Yb1 C83 146.2(2) . .
C85 Yb1 C83 47.4(2) . .
N11 Yb1 C83 48.3(2) . .
C84 Yb1 C83 29.3(2) . .
C54 Yb1 C83 135.6(2) . .
C82 Yb1 C83 28.6(2) . .
N4 Yb1 C52 121.1(2) . .
N3 Yb1 C52 79.1(2) . .
N1 Yb1 C52 100.4(2) . .
N2 Yb1 C52 164.6(2) . .
C53 Yb1 C52 28.6(2) . .
C85 Yb1 C52 81.1(2) . .
N11 Yb1 C52 70.5(2) . .
C84 Yb1 C52 109.9(2) . .
C54 Yb1 C52 46.2(2) . .
C82 Yb1 C52 93.9(2) . .
C83 Yb1 C52 118.8(2) . .
N12 Yb2 N8 144.1(2) . .
N12 Yb2 N7 78.3(2) . .
N8 Yb2 N7 136.3(2) . .
N12 Yb2 N11 139.1(2) . .
N8 Yb2 N11 74.6(2) . .
N7 Yb2 N11 69.9(2) . .
N12 Yb2 N6 83.3(2) . .
N8 Yb2 N6 69.3(2) . .
N7 Yb2 N6 123.6(2) . .
N11 Yb2 N6 135.9(2) . .
N12 Yb2 N10 70.3(2) . .
N8 Yb2 N10 81.7(2) . .
N7 Yb2 N10 138.7(2) . .
N11 Yb2 N10 120.1(2) . .
N6 Yb2 N10 79.1(2) . .
N12 Yb2 N9 85.6(2) . .
N8 Yb2 N9 105.2(2) . .
N7 Yb2 N9 83.1(2) . .
N11 Yb2 N9 66.1(2) . .
N6 Yb2 N9 147.78(19) . .
N10 Yb2 N9 68.68(19) . .
N12 Yb2 N5 104.7(2) . .
N8 Yb2 N5 86.6(2) . .
N7 Yb2 N5 66.1(2) . .
N11 Yb2 N5 85.5(2) . .
N6 Yb2 N5 68.13(19) . .
N10 Yb2 N5 147.23(19) . .
N9 Yb2 N5 144.08(19) . .
N16 Yb3 N16 76.8(3) 2_756 .
N16 Yb3 N15 151.3(2) 2_756 2_756
N16 Yb3 N15 114.6(2) . 2_756
N16 Yb3 N15 114.6(2) 2_756 .
N16 Yb3 N15 151.3(2) . .
N15 Yb3 N15 68.8(3) 2_756 .
N16 Yb3 N14 69.8(2) 2_756 2_756
N16 Yb3 N14 82.8(2) . 2_756
N15 Yb3 N14 135.4(2) 2_756 2_756
N15 Yb3 N14 77.5(2) . 2_756
N16 Yb3 N14 82.8(2) 2_756 .
N16 Yb3 N14 69.8(2) . .
N15 Yb3 N14 77.5(2) 2_756 .
N15 Yb3 N14 135.4(2) . .
N14 Yb3 N14 145.1(3) 2_756 .
N16 Yb3 N13 78.4(2) 2_756 .
N16 Yb3 N13 141.5(2) . .
N15 Yb3 N13 77.4(2) 2_756 .
N15 Yb3 N13 66.8(2) . .
N14 Yb3 N13 115.16(19) 2_756 .
N14 Yb3 N13 78.3(2) . .
N16 Yb3 N13 141.5(2) 2_756 2_756
N16 Yb3 N13 78.4(2) . 2_756
N15 Yb3 N13 66.8(2) 2_756 2_756
N15 Yb3 N13 77.40(19) . 2_756
N14 Yb3 N13 78.3(2) 2_756 2_756
N14 Yb3 N13 115.16(19) . 2_756
N13 Yb3 N13 136.5(3) . 2_756
N16 Yb3 C117 22.9(2) 2_756 2_756
N16 Yb3 C117 75.0(2) . 2_756
N15 Yb3 C117 169.6(2) 2_756 2_756
N15 Yb3 C117 105.0(2) . 2_756
N14 Yb3 C117 46.9(2) 2_756 2_756
N14 Yb3 C117 103.3(2) . 2_756
N13 Yb3 C117 92.6(2) . 2_756
N13 Yb3 C117 120.9(2) 2_756 2_756
N18 Yb4 N18 156.8(3) . 2_756
N18 Yb4 N17 70.9(2) . .
N18 Yb4 N17 89.7(2) 2_756 .
N18 Yb4 N17 89.7(2) . 2_756
N18 Yb4 N17 70.9(2) 2_756 2_756
N17 Yb4 N17 68.0(3) . 2_756
N18 Yb4 C114 102.3(2) . 2_756
N18 Yb4 C114 83.4(2) 2_756 2_756
N17 Yb4 C114 73.6(2) . 2_756
N17 Yb4 C114 133.2(2) 2_756 2_756
N18 Yb4 C114 83.4(2) . .
N18 Yb4 C114 102.3(2) 2_756 .
N17 Yb4 C114 133.2(2) . .
N17 Yb4 C114 73.6(2) 2_756 .
C114 Yb4 C114 152.0(3) 2_756 .
N18 Yb4 C113 74.3(2) . 2_756
N18 Yb4 C113 113.0(2) 2_756 2_756
N17 Yb4 C113 73.6(2) . 2_756
N17 Yb4 C113 141.4(2) 2_756 2_756
C114 Yb4 C113 29.7(2) 2_756 2_756
C114 Yb4 C113 136.3(2) . 2_756
N18 Yb4 C113 113.0(2) . .
N18 Yb4 C113 74.3(2) 2_756 .
N17 Yb4 C113 141.4(2) . .
N17 Yb4 C113 73.6(2) 2_756 .
C114 Yb4 C113 136.3(2) 2_756 .
C114 Yb4 C113 29.7(2) . .
C113 Yb4 C113 145.0(3) 2_756 .
N18 Yb4 C115 76.3(2) . .
N18 Yb4 C115 119.1(2) 2_756 .
N17 Yb4 C115 145.4(2) . .
N17 Yb4 C115 101.8(2) 2_756 .
C114 Yb4 C115 125.0(2) 2_756 .
C114 Yb4 C115 29.1(2) . .
C113 Yb4 C115 107.9(2) 2_756 .
C113 Yb4 C115 47.2(2) . .
N18 Yb4 C115 119.1(2) . 2_756
N18 Yb4 C115 76.3(2) 2_756 2_756
N17 Yb4 C115 101.8(2) . 2_756
N17 Yb4 C115 145.4(2) 2_756 2_756
C114 Yb4 C115 29.1(2) 2_756 2_756
C114 Yb4 C115 125.0(2) . 2_756
C113 Yb4 C115 47.2(2) 2_756 2_756
C113 Yb4 C115 107.9(2) . 2_756
C115 Yb4 C115 103.4(3) . 2_756
N18 Yb4 C112 75.7(2) . 2_756
N18 Yb4 C112 121.9(2) 2_756 2_756
N17 Yb4 C112 101.2(2) . 2_756
N17 Yb4 C112 164.3(2) 2_756 2_756
C114 Yb4 C112 47.7(2) 2_756 2_756
C114 Yb4 C112 109.6(2) . 2_756
C113 Yb4 C112 28.9(2) 2_756 2_756
C113 Yb4 C112 117.1(2) . 2_756
C115 Yb4 C112 80.5(2) . 2_756
C115 Yb4 C112 45.6(2) 2_756 2_756
N18 Yb4 C112 121.9(2) . .
N18 Yb4 C112 75.7(2) 2_756 .
N17 Yb4 C112 164.3(2) . .
N17 Yb4 C112 101.2(2) 2_756 .
C114 Yb4 C112 109.6(2) 2_756 .
C114 Yb4 C112 47.7(2) . .
C113 Yb4 C112 117.1(2) 2_756 .
C113 Yb4 C112 28.9(2) . .
C115 Yb4 C112 45.6(2) . .
C115 Yb4 C112 80.5(2) 2_756 .
C112 Yb4 C112 91.4(3) 2_756 .
C21 N1 C2 116.2(7) . .
C21 N1 Yb1 114.3(5) . .
C2 N1 Yb1 123.5(5) . .
C26 N2 C12 118.4(7) . .
C26 N2 Yb1 112.8(5) . .
C12 N2 Yb1 123.9(5) . .
C25 N3 C22 104.7(7) . .
C25 N3 Yb1 140.0(5) . .
C22 N3 Yb1 114.9(5) . .
C30 N4 C27 104.7(7) . .
C30 N4 Yb1 138.7(6) . .
C27 N4 Yb1 115.5(5) . .
C51 N5 C32 117.4(7) . .
C51 N5 Yb2 112.5(5) . .
C32 N5 Yb2 128.5(5) . .
C56 N6 C42 120.8(6) . .
C56 N6 Yb2 114.1(5) . .
C42 N6 Yb2 121.8(4) . .
C55 N7 C52 105.7(7) . .
C55 N7 Yb2 134.7(6) . .
C52 N7 Yb2 119.1(5) . .
C55 N7 Yb1 73.9(4) . .
C52 N7 Yb1 71.3(4) . .
Yb2 N7 Yb1 112.8(3) . .
C60 N8 C57 105.0(6) . .
C60 N8 Yb2 138.3(5) . .
C57 N8 Yb2 116.3(5) . .
C81 N9 C62 117.8(7) . .
C81 N9 Yb2 115.4(5) . .
C62 N9 Yb2 126.8(4) . .
C86 N10 C72 118.1(7) . .
C86 N10 Yb2 113.7(5) . .
C72 N10 Yb2 122.2(5) . .
C85 N11 C82 105.0(7) . .
C85 N11 Yb2 134.0(5) . .
C82 N11 Yb2 120.2(5) . .
C85 N11 Yb1 75.7(4) . .
C82 N11 Yb1 76.4(4) . .
Yb2 N11 Yb1 120.8(3) . .
C90 N12 C87 105.2(7) . .
C90 N12 Yb2 139.3(6) . .
C87 N12 Yb2 115.5(5) . .
C111 N13 C92 117.9(6) . .
C111 N13 Yb3 116.5(5) . .
C92 N13 Yb3 122.8(5) . .
C116 N14 C102 117.3(7) . .
C116 N14 Yb3 112.2(6) . .
C102 N14 Yb3 127.0(5) . .
C112 N15 C115 106.5(6) . .
C112 N15 Yb3 115.9(4) . .
C115 N15 Yb3 137.6(5) . .
C112 N15 Yb4 73.7(4) . .
C115 N15 Yb4 72.9(4) . .
Yb3 N15 Yb4 116.98(19) . .
C120 N16 C117 106.8(7) . .
C120 N16 Yb3 137.9(5) . .
C117 N16 Yb3 114.5(6) . .
C131 N17 C122 117.2(7) . .
C131 N17 Yb4 113.1(5) . .
C122 N17 Yb4 125.7(5) . .
C135 N18 C132 103.8(6) . .
C135 N18 Yb4 139.6(5) . .
C132 N18 Yb4 113.9(5) . .
C2 C1 C6 118.5(7) . .
C2 C1 C11 120.0(7) . .
C6 C1 C11 121.1(7) . .
C3 C2 C1 120.8(7) . .
C3 C2 N1 122.0(7) . .
C1 C2 N1 116.8(7) . .
C4 C3 C2 121.3(8) . .
C4 C3 H3 119.4 . .
C2 C3 H3 119.4 . .
C3 C4 C5 120.6(8) . .
C3 C4 H4 119.7 . .
C5 C4 H4 119.7 . .
C4 C5 C6 119.9(7) . .
C4 C5 C10 120.6(8) . .
C6 C5 C10 119.3(8) . .
C7 C6 C5 118.9(7) . .
C7 C6 C1 122.3(8) . .
C5 C6 C1 118.8(7) . .
C8 C7 C6 122.0(9) . .
C8 C7 H7 119.0 . .
C6 C7 H7 119.0 . .
C7 C8 C9 118.5(9) . .
C7 C8 H8 120.7 . .
C9 C8 H8 120.7 . .
C10 C9 C8 122.2(9) . .
C10 C9 H9 118.9 . .
C8 C9 H9 118.9 . .
C9 C10 C5 119.1(9) . .
C9 C10 H10 120.4 . .
C5 C10 H10 120.4 . .
C12 C11 C16 119.2(8) . .
C12 C11 C1 118.2(8) . .
C16 C11 C1 122.5(8) . .
C11 C12 N2 119.0(7) . .
C11 C12 C13 120.2(8) . .
N2 C12 C13 120.8(7) . .
C14 C13 C12 120.2(9) . .
C14 C13 H13 119.9 . .
C12 C13 H13 119.9 . .
C13 C14 C15 122.0(9) . .
C13 C14 H14 119.0 . .
C15 C14 H14 119.0 . .
C20 C15 C16 119.2(9) . .
C20 C15 C14 122.0(9) . .
C16 C15 C14 118.7(8) . .
C15 C16 C17 118.5(8) . .
C15 C16 C11 119.5(8) . .
C17 C16 C11 122.1(8) . .
C18 C17 C16 120.4(9) . .
C18 C17 H17 119.8 . .
C16 C17 H17 119.8 . .
C17 C18 C19 121.4(9) . .
C17 C18 H18 119.3 . .
C19 C18 H18 119.3 . .
C20 C19 C18 118.0(9) . .
C20 C19 H19 121.0 . .
C18 C19 H19 121.0 . .
C19 C20 C15 122.4(10) . .
C19 C20 H20 118.8 . .
C15 C20 H20 118.8 . .
N1 C21 C22 122.2(7) . .
N1 C21 H21A 118.9 . .
C22 C21 H21A 118.9 . .
C23 C22 N3 110.0(8) . .
C23 C22 C21 132.0(8) . .
N3 C22 C21 117.3(7) . .
C22 C23 C24 106.4(8) . .
C22 C23 H23 126.8 . .
C24 C23 H23 126.8 . .
C25 C24 C23 107.6(8) . .
C25 C24 H24 126.2 . .
C23 C24 H24 126.2 . .
N3 C25 C24 111.3(8) . .
N3 C25 H25 124.3 . .
C24 C25 H25 124.3 . .
N2 C26 C27 122.1(7) . .
N2 C26 H26A 119.0 . .
C27 C26 H26A 119.0 . .
N4 C27 C28 113.2(8) . .
N4 C27 C26 117.5(7) . .
C28 C27 C26 128.9(8) . .
C29 C28 C27 104.5(8) . .
C29 C28 H28 127.8 . .
C27 C28 H28 127.8 . .
C28 C29 C30 107.6(8) . .
C28 C29 H29 126.2 . .
C30 C29 H29 126.2 . .
N4 C30 C29 110.0(8) . .
N4 C30 H30 125.0 . .
C29 C30 H30 125.0 . .
C32 C31 C36 118.5(7) . .
C32 C31 C41 122.6(7) . .
C36 C31 C41 119.0(6) . .
C31 C32 C33 121.4(7) . .
C31 C32 N5 121.7(7) . .
C33 C32 N5 116.9(7) . .
C34 C33 C32 120.2(7) . .
C34 C33 H33 119.9 . .
C32 C33 H33 119.9 . .
C33 C34 C35 120.2(7) . .
C33 C34 H34 119.9 . .
C35 C34 H34 119.9 . .
C34 C35 C36 119.9(7) . .
C34 C35 C40 121.6(8) . .
C36 C35 C40 118.3(7) . .
C35 C36 C37 118.6(7) . .
C35 C36 C31 119.4(6) . .
C37 C36 C31 122.0(7) . .
C38 C37 C36 120.9(8) . .
C38 C37 H37 119.5 . .
C36 C37 H37 119.5 . .
C37 C38 C39 120.3(7) . .
C37 C38 H38 119.9 . .
C39 C38 H38 119.9 . .
C40 C39 C38 121.2(9) . .
C40 C39 H39 119.4 . .
C38 C39 H39 119.4 . .
C39 C40 C35 120.5(9) . .
C39 C40 H40 119.8 . .
C35 C40 H40 119.8 . .
C42 C41 C46 117.0(7) . .
C42 C41 C31 120.8(7) . .
C46 C41 C31 122.2(7) . .
C41 C42 C43 122.8(7) . .
C41 C42 N6 117.5(7) . .
C43 C42 N6 119.6(7) . .
C44 C43 C42 119.2(8) . .
C44 C43 H43 120.4 . .
C42 C43 H43 120.4 . .
C43 C44 C45 121.9(8) . .
C43 C44 H44 119.0 . .
C45 C44 H44 119.0 . .
C50 C45 C44 121.1(8) . .
C50 C45 C46 120.4(8) . .
C44 C45 C46 118.5(7) . .
C45 C46 C47 117.4(8) . .
C45 C46 C41 120.4(8) . .
C47 C46 C41 122.2(8) . .
C48 C47 C46 121.4(8) . .
C48 C47 H47 119.3 . .
C46 C47 H47 119.3 . .
C49 C48 C47 118.7(9) . .
C49 C48 H48 120.6 . .
C47 C48 H48 120.6 . .
C50 C49 C48 121.5(8) . .
C50 C49 H49 119.2 . .
C48 C49 H49 119.2 . .
C49 C50 C45 120.4(9) . .
C49 C50 H50 119.8 . .
C45 C50 H50 119.8 . .
N5 C51 C52 121.2(7) . .
N5 C51 H51 119.4 . .
C52 C51 H51 119.4 . .
N7 C52 C53 111.2(7) . .
N7 C52 C51 118.7(6) . .
C53 C52 C51 129.9(7) . .
N7 C52 Yb1 81.7(4) . .
C53 C52 Yb1 70.9(4) . .
C51 C52 Yb1 119.5(5) . .
C54 C53 C52 105.5(7) . .
C54 C53 Yb1 76.2(5) . .
C52 C53 Yb1 80.6(5) . .
C54 C53 H53A 127.3 . .
C52 C53 H53A 127.3 . .
Yb1 C53 H53A 109.4 . .
C53 C54 C55 107.4(7) . .
C53 C54 Yb1 74.6(5) . .
C55 C54 Yb1 82.3(5) . .
C53 C54 H54A 126.3 . .
C55 C54 H54A 126.3 . .
Yb1 C54 H54A 109.7 . .
N7 C55 C54 110.2(8) . .
N7 C55 Yb1 79.6(5) . .
C54 C55 Yb1 69.5(5) . .
N7 C55 H55A 124.9 . .
C54 C55 H55A 124.9 . .
Yb1 C55 H55A 117.6 . .
N6 C56 C57 122.9(7) . .
N6 C56 H56A 118.5 . .
C57 C56 H56A 118.5 . .
N8 C57 C58 111.2(7) . .
N8 C57 C56 116.6(7) . .
C58 C57 C56 131.9(7) . .
C57 C58 C59 105.9(7) . .
C57 C58 H58 127.1 . .
C59 C58 H58 127.1 . .
C60 C59 C58 106.0(7) . .
C60 C59 H59 127.0 . .
C58 C59 H59 127.0 . .
N8 C60 C59 111.8(7) . .
N8 C60 H60 124.1 . .
C59 C60 H60 124.1 . .
C62 C61 C66 118.1(7) . .
C62 C61 C71 120.6(7) . .
C66 C61 C71 121.4(7) . .
C61 C62 C63 121.7(7) . .
C61 C62 N9 120.4(7) . .
C63 C62 N9 117.8(7) . .
C64 C63 C62 120.1(8) . .
C64 C63 H63 119.9 . .
C62 C63 H63 119.9 . .
C63 C64 C65 119.5(8) . .
C63 C64 H64 120.2 . .
C65 C64 H64 120.2 . .
C66 C65 C70 118.9(7) . .
C66 C65 C64 119.9(8) . .
C70 C65 C64 121.1(9) . .
C65 C66 C67 119.9(8) . .
C65 C66 C61 120.4(8) . .
C67 C66 C61 119.5(7) . .
C68 C67 C66 119.9(8) . .
C68 C67 H67 120.1 . .
C66 C67 H67 120.1 . .
C67 C68 C69 119.4(7) . .
C67 C68 H68 120.3 . .
C69 C68 H68 120.3 . .
C70 C69 C68 121.1(8) . .
C70 C69 H69 119.5 . .
C68 C69 H69 119.5 . .
C69 C70 C65 120.8(9) . .
C69 C70 H70 119.6 . .
C65 C70 H70 119.6 . .
C72 C71 C76 118.4(7) . .
C72 C71 C61 119.7(7) . .
C76 C71 C61 121.9(7) . .
C71 C72 C73 121.6(7) . .
C71 C72 N10 119.4(7) . .
C73 C72 N10 118.9(7) . .
C74 C73 C72 119.9(8) . .
C74 C73 H73 120.0 . .
C72 C73 H73 120.0 . .
C73 C74 C75 121.6(7) . .
C73 C74 H74 119.2 . .
C75 C74 H74 119.2 . .
C80 C75 C76 122.3(8) . .
C80 C75 C74 121.0(7) . .
C76 C75 C74 116.7(7) . .
C75 C76 C71 121.7(7) . .
C75 C76 C77 115.9(7) . .
C71 C76 C77 122.4(7) . .
C78 C77 C76 121.5(8) . .
C78 C77 H77 119.2 . .
C76 C77 H77 119.2 . .
C77 C78 C79 120.7(9) . .
C77 C78 H78 119.6 . .
C79 C78 H78 119.6 . .
C80 C79 C78 120.8(8) . .
C80 C79 H79 119.6 . .
C78 C79 H79 119.6 . .
C79 C80 C75 118.7(8) . .
C79 C80 H80 120.7 . .
C75 C80 H80 120.7 . .
N9 C81 C82 119.8(7) . .
N9 C81 H81 120.1 . .
C82 C81 H81 120.1 . .
N11 C82 C83 111.5(7) . .
N11 C82 C81 118.5(7) . .
C83 C82 C81 129.7(7) . .
N11 C82 Yb1 74.9(4) . .
C83 C82 Yb1 76.7(5) . .
C81 C82 Yb1 120.3(5) . .
C82 C83 C84 105.4(7) . .
C82 C83 Yb1 74.7(4) . .
C84 C83 Yb1 73.9(5) . .
C82 C83 H83A 127.3 . .
C84 C83 H83A 127.3 . .
Yb1 C83 H83A 116.5 . .
C85 C84 C83 107.0(7) . .
C85 C84 Yb1 75.4(5) . .
C83 C84 Yb1 76.9(5) . .
C85 C84 H84A 126.5 . .
C83 C84 H84A 126.5 . .
Yb1 C84 H84A 113.8 . .
N11 C85 C84 111.0(7) . .
N11 C85 Yb1 75.7(4) . .
C84 C85 Yb1 75.8(5) . .
N11 C85 H85A 124.5 . .
C84 C85 H85A 124.5 . .
Yb1 C85 H85A 115.8 . .
N10 C86 C87 121.3(7) . .
N10 C86 H86A 119.3 . .
C87 C86 H86A 119.3 . .
N12 C87 C88 109.5(8) . .
N12 C87 C86 118.9(7) . .
C88 C87 C86 131.5(8) . .
C89 C88 C87 107.6(8) . .
C89 C88 H88 126.2 . .
C87 C88 H88 126.2 . .
C88 C89 C90 106.0(8) . .
C88 C89 H89 127.0 . .
C90 C89 H89 127.0 . .
N12 C90 C89 111.7(8) . .
N12 C90 H90 124.2 . .
C89 C90 H90 124.2 . .
C92 C91 C96 117.7(7) . .
C92 C91 C101 122.4(7) . .
C96 C91 C101 119.9(7) . .
C91 C92 C93 121.1(7) . .
C91 C92 N13 120.4(7) . .
C93 C92 N13 118.2(6) . .
C94 C93 C92 119.8(7) . .
C94 C93 H93 120.1 . .
C92 C93 H93 120.1 . .
C93 C94 C95 122.1(8) . .
C93 C94 H94 118.9 . .
C95 C94 H94 118.9 . .
C94 C95 C100 122.5(8) . .
C94 C95 C96 118.5(8) . .
C100 C95 C96 118.9(8) . .
C97 C96 C91 120.0(8) . .
C97 C96 C95 119.5(8) . .
C91 C96 C95 120.4(7) . .
C96 C97 C98 119.1(8) . .
C96 C97 H97 120.4 . .
C98 C97 H97 120.4 . .
C99 C98 C97 119.9(9) . .
C99 C98 H98 120.1 . .
C97 C98 H98 120.1 . .
C98 C99 C100 121.5(9) . .
C98 C99 H99 119.2 . .
C100 C99 H99 119.2 . .
C99 C100 C95 120.9(8) . .
C99 C100 H100 119.6 . .
C95 C100 H100 119.6 . .
C102 C101 C106 119.7(7) . .
C102 C101 C91 121.3(8) . .
C106 C101 C91 118.6(7) . .
C101 C102 N14 120.8(7) . .
C101 C102 C103 119.7(8) . .
N14 C102 C103 119.2(8) . .
C104 C103 C102 122.0(9) . .
C104 C103 H103 119.0 . .
C102 C103 H103 119.0 . .
C103 C104 C105 120.8(8) . .
C103 C104 H104 119.6 . .
C105 C104 H104 119.6 . .
C104 C105 C110 123.5(8) . .
C104 C105 C106 118.9(8) . .
C110 C105 C106 117.6(8) . .
C107 C106 C101 121.8(7) . .
C107 C106 C105 119.6(8) . .
C101 C106 C105 118.6(8) . .
C108 C107 C106 119.8(8) . .
C108 C107 H107 120.1 . .
C106 C107 H107 120.1 . .
C107 C108 C109 121.5(9) . .
C107 C108 H108 119.3 . .
C109 C108 H108 119.3 . .
C110 C109 C108 119.9(9) . .
C110 C109 H109 120.1 . .
C108 C109 H109 120.1 . .
C109 C110 C105 121.6(9) . .
C109 C110 H110 119.2 . .
C105 C110 H110 119.2 . .
N13 C111 C112 121.2(7) . .
N13 C111 H111 119.4 . .
C112 C111 H111 119.4 . .
N15 C112 C113 110.3(6) . .
N15 C112 C111 119.2(6) . .
C113 C112 C111 130.4(7) . .
N15 C112 Yb4 78.8(4) . .
C113 C112 Yb4 73.1(4) . .
C111 C112 Yb4 118.9(5) . .
C112 C113 C114 106.6(7) . .
C112 C113 Yb4 78.1(4) . .
C114 C113 Yb4 73.6(4) . .
C112 C113 H11A 126.7 . .
C114 C113 H11A 126.7 . .
Yb4 C113 H11A 114.2 . .
C115 C114 C113 105.6(7) . .
C115 C114 Yb4 78.8(4) . .
C113 C114 Yb4 76.7(4) . .
C115 C114 H11B 127.2 . .
C113 C114 H11B 127.2 . .
Yb4 C114 H11B 110.6 . .
N15 C115 C114 111.0(7) . .
N15 C115 Yb4 79.5(4) . .
C114 C115 Yb4 72.1(4) . .
N15 C115 H11C 124.5 . .
C114 C115 H11C 124.5 . .
Yb4 C115 H11C 115.6 . .
N14 C116 C117 121.9(8) . .
N14 C116 H116 119.0 . .
C117 C116 H116 119.0 . .
N16 C117 C116 121.0(8) . .
N16 C117 C118 109.3(8) . .
C116 C117 C118 129.6(8) . .
C119 C118 C117 105.8(8) . .
C119 C118 H118 127.1 . .
C117 C118 H118 127.1 . .
C118 C119 C120 107.5(8) . .
C118 C119 H119 126.2 . .
C120 C119 H119 126.2 . .
N16 C120 C119 110.5(8) . .
N16 C120 H120 124.8 . .
C119 C120 H120 124.8 . .
C122 C121 C126 119.1(7) . .
C122 C121 C121 119.7(6) . 2_756
C126 C121 C121 121.1(6) . 2_756
C121 C122 C123 120.8(7) . .
C121 C122 N17 117.7(6) . .
C123 C122 N17 121.4(7) . .
C124 C123 C122 120.4(8) . .
C124 C123 H123 119.8 . .
C122 C123 H123 119.8 . .
C123 C124 C125 121.3(8) . .
C123 C124 H124 119.4 . .
C125 C124 H124 119.4 . .
C130 C125 C124 124.0(10) . .
C130 C125 C126 116.6(10) . .
C124 C125 C126 119.2(8) . .
C121 C126 C127 121.1(8) . .
C121 C126 C125 119.0(8) . .
C127 C126 C125 119.8(9) . .
C128 C127 C126 118.1(11) . .
C128 C127 H127 120.9 . .
C126 C127 H127 120.9 . .
C127 C128 C129 121.9(11) . .
C127 C128 H128 119.0 . .
C129 C128 H128 119.0 . .
C130 C129 C128 118.8(10) . .
C130 C129 H129 120.6 . .
C128 C129 H129 120.6 . .
C129 C130 C125 124.5(12) . .
C129 C130 H130 117.7 . .
C125 C130 H130 117.7 . .
N17 C131 C132 121.7(8) . .
N17 C131 H13A 119.2 . .
C132 C131 H13A 119.1 . .
C133 C132 N18 111.5(7) . .
C133 C132 C131 130.5(8) . .
N18 C132 C131 118.0(7) . .
C134 C133 C132 106.1(8) . .
C134 C133 H133 126.9 . .
C132 C133 H133 126.9 . .
C133 C134 C135 107.0(8) . .
C133 C134 H134 126.5 . .
C135 C134 H134 126.5 . .
N18 C135 C134 111.5(8) . .
N18 C135 H135 124.3 . .
C134 C135 H135 124.3 . .
C137 C136 H13B 109.5 . .
C137 C136 H13C 109.5 . .
H13B C136 H13C 109.5 . .
C137 C136 H13D 109.5 . .
H13B C136 H13D 109.5 . .
H13C C136 H13D 109.5 . .
C138 C137 C142 120.0 . .
C138 C137 C136 124.0(17) . .
C142 C137 C136 115.8(17) . .
C137 C138 C139 120.0 . .
C137 C138 H138 120.0 . .
C139 C138 H138 120.0 . .
C140 C139 C138 120.0 . .
C140 C139 H139 120.0 . .
C138 C139 H139 120.0 . .
C139 C140 C141 120.0 . .
C139 C140 H140 120.0 . .
C141 C140 H140 120.0 . .
C140 C141 C142 120.0 . .
C140 C141 H141 120.0 . .
C142 C141 H141 120.0 . .
C141 C142 C137 120.0 . .
C141 C142 H142 120.0 . .
C137 C142 H142 120.0 . .
C144 C143 C148 120.8(16) . .
C144 C143 H143 119.6 . .
C148 C143 H143 119.6 . .
C143 C144 C145 123.3(18) . .
C143 C144 H144 118.4 . .
C145 C144 H144 118.4 . .
C144 C145 C146 119(2) . .
C144 C145 H145 120.6 . .
C146 C145 H145 120.6 . .
C147 C146 C145 114(2) . .
C147 C146 H146 122.8 . .
C145 C146 H146 122.8 . .
C148 C147 C146 125.5(17) . .
C148 C147 H147 117.2 . .
C146 C147 H147 117.2 . .
C147 C148 C143 116.8(14) . .
C147 C148 H148 121.6 . .
C143 C148 H148 121.6 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Yb1 N4 2.347(7) .
Yb1 N3 2.364(6) .
Yb1 N1 2.430(7) .
Yb1 N2 2.456(6) .
Yb1 C53 2.763(8) .
Yb1 C85 2.774(8) .
Yb1 N11 2.774(7) .
Yb1 C84 2.779(8) .
Yb1 C54 2.782(8) .
Yb1 C82 2.793(7) .
Yb1 C83 2.817(8) .
Yb1 C52 2.885(7) .
Yb2 N12 2.337(7) .
Yb2 N8 2.366(7) .
Yb2 N7 2.383(7) .
Yb2 N11 2.407(6) .
Yb2 N6 2.437(5) .
Yb2 N10 2.437(6) .
Yb2 N9 2.631(6) .
Yb2 N5 2.644(7) .
Yb3 N16 2.367(7) 2_756
Yb3 N16 2.367(7) .
Yb3 N15 2.467(6) 2_756
Yb3 N15 2.467(6) .
Yb3 N14 2.473(6) 2_756
Yb3 N14 2.473(6) .
Yb3 N13 2.524(6) .
Yb3 N13 2.524(6) 2_756
Yb3 C117 3.183(8) 2_756
Yb4 N18 2.351(7) .
Yb4 N18 2.351(7) 2_756
Yb4 N17 2.435(7) .
Yb4 N17 2.435(7) 2_756
Yb4 C114 2.743(7) 2_756
Yb4 C114 2.743(7) .
Yb4 C113 2.782(7) 2_756
Yb4 C113 2.782(7) .
Yb4 C115 2.827(7) .
Yb4 C115 2.827(7) 2_756
Yb4 C112 2.845(8) 2_756
Yb4 C112 2.845(8) .
N1 C21 1.294(10) .
N1 C2 1.438(9) .
N2 C26 1.287(9) .
N2 C12 1.414(10) .
N3 C25 1.356(10) .
N3 C22 1.395(10) .
N4 C30 1.356(10) .
N4 C27 1.361(10) .
N5 C51 1.275(9) .
N5 C32 1.437(10) .
N6 C56 1.284(10) .
N6 C42 1.444(9) .
N7 C55 1.369(10) .
N7 C52 1.379(10) .
N8 C60 1.353(10) .
N8 C57 1.375(9) .
N9 C81 1.282(9) .
N9 C62 1.439(9) .
N10 C86 1.301(10) .
N10 C72 1.417(9) .
N11 C85 1.375(10) .
N11 C82 1.383(9) .
N12 C90 1.354(10) .
N12 C87 1.380(10) .
N13 C111 1.267(9) .
N13 C92 1.443(9) .
N14 C116 1.317(10) .
N14 C102 1.417(11) .
N15 C112 1.370(9) .
N15 C115 1.371(9) .
N16 C120 1.351(11) .
N16 C117 1.364(10) .
N17 C131 1.316(10) .
N17 C122 1.423(10) .
N18 C135 1.362(10) .
N18 C132 1.402(10) .
C1 C2 1.413(10) .
C1 C6 1.428(10) .
C1 C11 1.498(11) .
C2 C3 1.384(11) .
C3 C4 1.354(11) .
C3 H3 0.9500 .
C4 C5 1.405(11) .
C4 H4 0.9500 .
C5 C6 1.422(12) .
C5 C10 1.428(11) .
C6 C7 1.415(11) .
C7 C8 1.374(11) .
C7 H7 0.9500 .
C8 C9 1.410(13) .
C8 H8 0.9500 .
C9 C10 1.385(13) .
C9 H9 0.9500 .
C10 H10 0.9500 .
C11 C12 1.385(11) .
C11 C16 1.435(11) .
C12 C13 1.451(12) .
C13 C14 1.314(12) .
C13 H13 0.9500 .
C14 C15 1.440(14) .
C14 H14 0.9500 .
C15 C20 1.389(13) .
C15 C16 1.407(12) .
C16 C17 1.414(12) .
C17 C18 1.360(12) .
C17 H17 0.9500 .
C18 C19 1.406(14) .
C18 H18 0.9500 .
C19 C20 1.370(15) .
C19 H19 0.9500 .
C20 H20 0.9500 .
C21 C22 1.406(12) .
C21 H21A 0.9500 .
C22 C23 1.374(11) .
C23 C24 1.380(13) .
C23 H23 0.9500 .
C24 C25 1.358(12) .
C24 H24 0.9500 .
C25 H25 0.9500 .
C26 C27 1.440(11) .
C26 H26A 0.9500 .
C27 C28 1.386(11) .
C28 C29 1.377(13) .
C28 H28 0.9500 .
C29 C30 1.414(12) .
C29 H29 0.9500 .
C30 H30 0.9500 .
C31 C32 1.368(10) .
C31 C36 1.437(10) .
C31 C41 1.495(11) .
C32 C33 1.431(11) .
C33 C34 1.361(11) .
C33 H33 0.9500 .
C34 C35 1.406(10) .
C34 H34 0.9500 .
C35 C36 1.416(11) .
C35 C40 1.459(11) .
C36 C37 1.421(10) .
C37 C38 1.365(11) .
C37 H37 0.9500 .
C38 C39 1.411(12) .
C38 H38 0.9500 .
C39 C40 1.331(10) .
C39 H39 0.9500 .
C40 H40 0.9500 .
C41 C42 1.396(10) .
C41 C46 1.443(11) .
C42 C43 1.400(10) .
C43 C44 1.366(11) .
C43 H43 0.9500 .
C44 C45 1.412(11) .
C44 H44 0.9500 .
C45 C50 1.409(11) .
C45 C46 1.418(11) .
C46 C47 1.439(12) .
C47 C48 1.407(13) .
C47 H47 0.9500 .
C48 C49 1.395(14) .
C48 H48 0.9500 .
C49 C50 1.385(14) .
C49 H49 0.9500 .
C50 H50 0.9500 .
C51 C52 1.427(10) .
C51 H51 0.9500 .
C52 C53 1.399(10) .
C53 C54 1.398(11) .
C53 H53A 0.9500 .
C54 C55 1.401(12) .
C54 H54A 0.9500 .
C55 H55A 0.9500 .
C56 C57 1.408(11) .
C56 H56A 0.9500 .
C57 C58 1.388(11) .
C58 C59 1.401(10) .
C58 H58 0.9500 .
C59 C60 1.389(10) .
C59 H59 0.9500 .
C60 H60 0.9500 .
C61 C62 1.385(10) .
C61 C66 1.445(11) .
C61 C71 1.483(10) .
C62 C63 1.408(11) .
C63 C64 1.400(12) .
C63 H63 0.9500 .
C64 C65 1.419(11) .
C64 H64 0.9500 .
C65 C66 1.400(12) .
C65 C70 1.418(12) .
C66 C67 1.420(11) .
C67 C68 1.382(11) .
C67 H67 0.9500 .
C68 C69 1.419(13) .
C68 H68 0.9500 .
C69 C70 1.349(13) .
C69 H69 0.9500 .
C70 H70 0.9500 .
C71 C72 1.387(10) .
C71 C76 1.428(10) .
C72 C73 1.407(11) .
C73 C74 1.374(12) .
C73 H73 0.9500 .
C74 C75 1.443(11) .
C74 H74 0.9500 .
C75 C80 1.390(11) .
C75 C76 1.420(10) .
C76 C77 1.440(10) .
C77 C78 1.348(12) .
C77 H77 0.9500 .
C78 C79 1.395(13) .
C78 H78 0.9500 .
C79 C80 1.386(13) .
C79 H79 0.9500 .
C80 H80 0.9500 .
C81 C82 1.455(11) .
C81 H81 0.9500 .
C82 C83 1.385(10) .
C83 C84 1.414(11) .
C83 H83A 0.9500 .
C84 C85 1.380(11) .
C84 H84A 0.9500 .
C85 H85A 0.9500 .
C86 C87 1.403(11) .
C86 H86A 0.9500 .
C87 C88 1.398(11) .
C88 C89 1.365(13) .
C88 H88 0.9500 .
C89 C90 1.392(12) .
C89 H89 0.9500 .
C90 H90 0.9500 .
C91 C92 1.392(10) .
C91 C96 1.425(11) .
C91 C101 1.477(10) .
C92 C93 1.429(10) .
C93 C94 1.352(11) .
C93 H93 0.9500 .
C94 C95 1.388(11) .
C94 H94 0.9500 .
C95 C100 1.390(12) .
C95 C96 1.437(11) .
C96 C97 1.406(10) .
C97 C98 1.437(13) .
C97 H97 0.9500 .
C98 C99 1.359(13) .
C98 H98 0.9500 .
C99 C100 1.389(12) .
C99 H99 0.9500 .
C100 H100 0.9500 .
C101 C102 1.371(11) .
C101 C106 1.440(12) .
C102 C103 1.422(11) .
C103 C104 1.340(12) .
C103 H103 0.9500 .
C104 C105 1.402(12) .
C104 H104 0.9500 .
C105 C110 1.441(12) .
C105 C106 1.444(10) .
C106 C107 1.389(11) .
C107 C108 1.383(12) .
C107 H107 0.9500 .
C108 C109 1.412(12) .
C108 H108 0.9500 .
C109 C110 1.332(13) .
C109 H109 0.9500 .
C110 H110 0.9500 .
C111 C112 1.418(10) .
C111 H111 0.9500 .
C112 C113 1.404(10) .
C113 C114 1.417(11) .
C113 H11A 0.9500 .
C114 C115 1.402(10) .
C114 H11B 0.9500 .
C115 H11C 0.9500 .
C116 C117 1.365(12) .
C116 H116 0.9500 .
C117 C118 1.449(13) .
C118 C119 1.359(13) .
C118 H118 0.9500 .
C119 C120 1.414(12) .
C119 H119 0.9500 .
C120 H120 0.9500 .
C121 C122 1.399(10) .
C121 C126 1.428(11) .
C121 C121 1.489(14) 2_756
C122 C123 1.402(10) .
C123 C124 1.370(12) .
C123 H123 0.9500 .
C124 C125 1.401(13) .
C124 H124 0.9500 .
C125 C130 1.397(14) .
C125 C126 1.436(12) .
C126 C127 1.431(13) .
C127 C128 1.381(14) .
C127 H127 0.9500 .
C128 C129 1.402(15) .
C128 H128 0.9500 .
C129 C130 1.328(16) .
C129 H129 0.9500 .
C130 H130 0.9500 .
C131 C132 1.407(11) .
C131 H13A 0.9500 .
C132 C133 1.385(12) .
C133 C134 1.382(12) .
C133 H133 0.9500 .
C134 C135 1.400(12) .
C134 H134 0.9500 .
C135 H135 0.9500 .
C136 C137 1.479(10) .
C136 H13B 0.9800 .
C136 H13C 0.9800 .
C136 H13D 0.9800 .
C137 C138 1.3900 .
C137 C142 1.3900 .
C138 C139 1.3900 .
C138 H138 0.9500 .
C139 C140 1.3900 .
C139 H139 0.9500 .
C140 C141 1.3900 .
C140 H140 0.9500 .
C141 C142 1.3900 .
C141 H141 0.9500 .
C142 H142 0.9500 .
C143 C144 1.33(2) .
C143 C148 1.399(17) .
C143 H143 0.9500 .
C144 C145 1.37(2) .
C144 H144 0.9500 .
C145 C146 1.47(3) .
C145 H145 0.9500 .
C146 C147 1.38(2) .
C146 H146 0.9500 .
C147 C148 1.376(19) .
C147 H147 0.9500 .
C148 H148 0.9500 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
N4 Yb1 N1 C21 167.7(6) .
N3 Yb1 N1 C21 3.0(5) .
N2 Yb1 N1 C21 97.9(6) .
C53 Yb1 N1 C21 -79.9(6) .
C85 Yb1 N1 C21 18.3(8) .
N11 Yb1 N1 C21 -36.5(13) .
C84 Yb1 N1 C21 59.9(7) .
C54 Yb1 N1 C21 -110.3(6) .
C82 Yb1 N1 C21 145.1(7) .
C83 Yb1 N1 C21 102.6(6) .
C52 Yb1 N1 C21 -71.2(6) .
N4 Yb1 N1 C2 16.0(6) .
N3 Yb1 N1 C2 -148.7(6) .
N2 Yb1 N1 C2 -53.8(6) .
C53 Yb1 N1 C2 128.4(6) .
C85 Yb1 N1 C2 -133.4(6) .
N11 Yb1 N1 C2 171.8(9) .
C84 Yb1 N1 C2 -91.8(6) .
C54 Yb1 N1 C2 98.1(6) .
C82 Yb1 N1 C2 -6.5(11) .
C83 Yb1 N1 C2 -49.1(7) .
C52 Yb1 N1 C2 137.1(6) .
N4 Yb1 N2 C26 6.3(5) .
N3 Yb1 N2 C26 170.9(5) .
N1 Yb1 N2 C26 101.3(6) .
C53 Yb1 N2 C26 104.7(6) .
C85 Yb1 N2 C26 -112.8(5) .
N11 Yb1 N2 C26 -87.8(5) .
C84 Yb1 N2 C26 -106.1(6) .
C54 Yb1 N2 C26 61.9(6) .
C82 Yb1 N2 C26 -65.7(5) .
C83 Yb1 N2 C26 -75.5(5) .
C52 Yb1 N2 C26 145.8(7) .
N4 Yb1 N2 C12 -148.6(6) .
N3 Yb1 N2 C12 16.0(6) .
N1 Yb1 N2 C12 -53.6(6) .
C53 Yb1 N2 C12 -50.2(7) .
C85 Yb1 N2 C12 92.3(6) .
N11 Yb1 N2 C12 117.3(6) .
C84 Yb1 N2 C12 99.0(6) .
C54 Yb1 N2 C12 -93.0(6) .
C82 Yb1 N2 C12 139.4(6) .
C83 Yb1 N2 C12 129.5(6) .
C52 Yb1 N2 C12 -9.1(11) .
N4 Yb1 N3 C25 144.9(8) .
N1 Yb1 N3 C25 180.0(9) .
N2 Yb1 N3 C25 111.9(8) .
C53 Yb1 N3 C25 -103.8(8) .
C85 Yb1 N3 C25 8.6(8) .
N11 Yb1 N3 C25 -7.3(9) .
C84 Yb1 N3 C25 37.4(8) .
C54 Yb1 N3 C25 -112.8(8) .
C82 Yb1 N3 C25 12.8(9) .
C83 Yb1 N3 C25 42.2(9) .
C52 Yb1 N3 C25 -74.6(8) .
N4 Yb1 N3 C22 -43.6(8) .
N1 Yb1 N3 C22 -8.5(5) .
N2 Yb1 N3 C22 -76.5(5) .
C53 Yb1 N3 C22 67.7(5) .
C85 Yb1 N3 C22 -179.8(6) .
N11 Yb1 N3 C22 164.3(5) .
C84 Yb1 N3 C22 -151.1(6) .
C54 Yb1 N3 C22 58.7(6) .
C82 Yb1 N3 C22 -175.7(5) .
C83 Yb1 N3 C22 -146.3(5) .
C52 Yb1 N3 C22 96.9(6) .
N3 Yb1 N4 C30 147.5(8) .
N1 Yb1 N4 C30 114.8(9) .
N2 Yb1 N4 C30 -177.2(9) .
C53 Yb1 N4 C30 44.0(9) .
C85 Yb1 N4 C30 -84.6(9) .
N11 Yb1 N4 C30 -60.6(9) .
C84 Yb1 N4 C30 -110.3(9) .
C54 Yb1 N4 C30 39.5(9) .
C82 Yb1 N4 C30 -72.1(9) .
C83 Yb1 N4 C30 -101.4(9) .
C52 Yb1 N4 C30 14.4(10) .
N3 Yb1 N4 C27 -46.6(9) .
N1 Yb1 N4 C27 -79.4(6) .
N2 Yb1 N4 C27 -11.4(5) .
C53 Yb1 N4 C27 -150.1(6) .
C85 Yb1 N4 C27 81.2(6) .
N11 Yb1 N4 C27 105.3(6) .
C84 Yb1 N4 C27 55.6(6) .
C54 Yb1 N4 C27 -154.6(6) .
C82 Yb1 N4 C27 93.8(6) .
C83 Yb1 N4 C27 64.4(6) .
C52 Yb1 N4 C27 -179.8(5) .
N12 Yb2 N5 C51 82.6(6) .
N8 Yb2 N5 C51 -132.0(6) .
N7 Yb2 N5 C51 12.9(6) .
N11 Yb2 N5 C51 -57.2(6) .
N6 Yb2 N5 C51 159.0(6) .
N10 Yb2 N5 C51 159.0(5) .
N9 Yb2 N5 C51 -20.5(8) .
N12 Yb2 N5 C32 -112.1(6) .
N8 Yb2 N5 C32 33.3(6) .
N7 Yb2 N5 C32 178.1(7) .
N11 Yb2 N5 C32 108.1(6) .
N6 Yb2 N5 C32 -35.8(6) .
N10 Yb2 N5 C32 -35.7(8) .
N9 Yb2 N5 C32 144.8(6) .
N12 Yb2 N6 C56 -156.8(6) .
N8 Yb2 N6 C56 -0.4(5) .
N7 Yb2 N6 C56 132.1(5) .
N11 Yb2 N6 C56 36.8(7) .
N10 Yb2 N6 C56 -85.6(6) .
N9 Yb2 N6 C56 -86.3(7) .
N5 Yb2 N6 C56 94.4(6) .
N12 Yb2 N6 C42 43.6(5) .
N8 Yb2 N6 C42 -160.0(6) .
N7 Yb2 N6 C42 -27.5(6) .
N11 Yb2 N6 C42 -122.8(5) .
N10 Yb2 N6 C42 114.8(5) .
N9 Yb2 N6 C42 114.1(6) .
N5 Yb2 N6 C42 -65.2(5) .
N12 Yb2 N7 C55 64.8(8) .
N8 Yb2 N7 C55 -126.8(7) .
N11 Yb2 N7 C55 -89.1(8) .
N6 Yb2 N7 C55 138.5(7) .
N10 Yb2 N7 C55 24.1(9) .
N9 Yb2 N7 C55 -22.1(8) .
N5 Yb2 N7 C55 176.9(8) .
N12 Yb2 N7 C52 -124.9(6) .
N8 Yb2 N7 C52 43.4(7) .
N11 Yb2 N7 C52 81.2(6) .
N6 Yb2 N7 C52 -51.3(6) .
N10 Yb2 N7 C52 -165.7(5) .
N9 Yb2 N7 C52 148.2(6) .
N5 Yb2 N7 C52 -12.9(5) .
N12 Yb2 N7 Yb1 154.4(3) .
N8 Yb2 N7 Yb1 -37.2(4) .
N11 Yb2 N7 Yb1 0.5(2) .
N6 Yb2 N7 Yb1 -131.9(2) .
N10 Yb2 N7 Yb1 113.7(3) .
N9 Yb2 N7 Yb1 67.6(2) .
N5 Yb2 N7 Yb1 -93.5(3) .
N4 Yb1 N7 C55 32.4(5) .
N3 Yb1 N7 C55 -134.1(5) .
N1 Yb1 N7 C55 -59.5(5) .
N2 Yb1 N7 C55 60.1(11) .
C53 Yb1 N7 C55 -76.9(5) .
C85 Yb1 N7 C55 152.5(5) .
N11 Yb1 N7 C55 131.7(5) .
C84 Yb1 N7 C55 140.2(5) .
C54 Yb1 N7 C55 -36.0(5) .
C82 Yb1 N7 C55 104.9(5) .
C83 Yb1 N7 C55 110.5(5) .
C52 Yb1 N7 C55 -113.3(7) .
N4 Yb1 N7 C52 145.7(4) .
N3 Yb1 N7 C52 -20.8(5) .
N1 Yb1 N7 C52 53.8(5) .
N2 Yb1 N7 C52 173.4(9) .
C53 Yb1 N7 C52 36.4(4) .
C85 Yb1 N7 C52 -94.2(5) .
N11 Yb1 N7 C52 -115.0(5) .
C84 Yb1 N7 C52 -106.5(5) .
C54 Yb1 N7 C52 77.2(5) .
C82 Yb1 N7 C52 -141.8(5) .
C83 Yb1 N7 C52 -136.2(4) .
N4 Yb1 N7 Yb2 -99.9(3) .
N3 Yb1 N7 Yb2 93.6(3) .
N1 Yb1 N7 Yb2 168.3(2) .
N2 Yb1 N7 Yb2 -72.1(10) .
C53 Yb1 N7 Yb2 150.8(4) .
C85 Yb1 N7 Yb2 20.3(3) .
N11 Yb1 N7 Yb2 -0.5(2) .
C84 Yb1 N7 Yb2 8.0(3) .
C54 Yb1 N7 Yb2 -168.3(4) .
C82 Yb1 N7 Yb2 -27.4(3) .
C83 Yb1 N7 Yb2 -21.8(3) .
C52 Yb1 N7 Yb2 114.5(5) .
N12 Yb2 N8 C60 -133.4(8) .
N7 Yb2 N8 C60 66.4(9) .
N11 Yb2 N8 C60 29.7(8) .
N6 Yb2 N8 C60 -176.1(9) .
N10 Yb2 N8 C60 -94.7(8) .
N9 Yb2 N8 C60 -29.6(9) .
N5 Yb2 N8 C60 116.0(8) .
N12 Yb2 N8 C57 38.0(8) .
N7 Yb2 N8 C57 -122.2(6) .
N11 Yb2 N8 C57 -158.9(6) .
N6 Yb2 N8 C57 -4.7(5) .
N10 Yb2 N8 C57 76.7(6) .
N9 Yb2 N8 C57 141.8(6) .
N5 Yb2 N8 C57 -72.6(6) .
N12 Yb2 N9 C81 -147.8(5) .
N8 Yb2 N9 C81 67.0(6) .
N7 Yb2 N9 C81 -69.1(5) .
N11 Yb2 N9 C81 1.9(5) .
N6 Yb2 N9 C81 142.3(5) .
N10 Yb2 N9 C81 141.6(6) .
N5 Yb2 N9 C81 -38.7(7) .
N12 Yb2 N9 C62 29.4(6) .
N8 Yb2 N9 C62 -115.8(6) .
N7 Yb2 N9 C62 108.1(6) .
N11 Yb2 N9 C62 179.1(6) .
N6 Yb2 N9 C62 -40.5(8) .
N10 Yb2 N9 C62 -41.2(6) .
N5 Yb2 N9 C62 138.5(6) .
N12 Yb2 N10 C86 -0.7(5) .
N8 Yb2 N10 C86 -157.8(5) .
N7 Yb2 N10 C86 42.1(6) .
N11 Yb2 N10 C86 135.5(5) .
N6 Yb2 N10 C86 -87.3(5) .
N9 Yb2 N10 C86 92.3(5) .
N5 Yb2 N10 C86 -87.4(6) .
N12 Yb2 N10 C72 -152.9(6) .
N8 Yb2 N10 C72 50.0(5) .
N7 Yb2 N10 C72 -110.2(6) .
N11 Yb2 N10 C72 -16.8(6) .
N6 Yb2 N10 C72 120.4(6) .
N9 Yb2 N10 C72 -60.0(5) .
N5 Yb2 N10 C72 120.3(6) .
N12 Yb2 N11 C85 -141.9(7) .
N8 Yb2 N11 C85 53.2(7) .
N7 Yb2 N11 C85 -100.7(8) .
N6 Yb2 N11 C85 17.3(9) .
N10 Yb2 N11 C85 123.8(7) .
N9 Yb2 N11 C85 168.0(8) .
N5 Yb2 N11 C85 -34.5(7) .
N12 Yb2 N11 C82 49.9(7) .
N8 Yb2 N11 C82 -115.0(6) .
N7 Yb2 N11 C82 91.1(6) .
N6 Yb2 N11 C82 -150.9(5) .
N10 Yb2 N11 C82 -44.4(6) .
N9 Yb2 N11 C82 -0.2(5) .
N5 Yb2 N11 C82 157.2(6) .
N12 Yb2 N11 Yb1 -41.8(5) .
N8 Yb2 N11 Yb1 153.3(3) .
N7 Yb2 N11 Yb1 -0.6(3) .
N6 Yb2 N11 Yb1 117.4(3) .
N10 Yb2 N11 Yb1 -136.1(3) .
N9 Yb2 N11 Yb1 -91.9(3) .
N5 Yb2 N11 Yb1 65.5(3) .
N4 Yb1 N11 C85 -133.5(5) .
N3 Yb1 N11 C85 33.8(5) .
N1 Yb1 N11 C85 71.4(12) .
N2 Yb1 N11 C85 -59.1(5) .
C53 Yb1 N11 C85 113.0(5) .
C84 Yb1 N11 C85 -35.3(5) .
C54 Yb1 N11 C85 142.6(5) .
C82 Yb1 N11 C85 -109.7(7) .
C83 Yb1 N11 C85 -74.9(5) .
C52 Yb1 N11 C85 107.8(5) .
N4 Yb1 N11 C82 -23.8(5) .
N3 Yb1 N11 C82 143.5(4) .
N1 Yb1 N11 C82 -178.9(9) .
N2 Yb1 N11 C82 50.6(5) .
C53 Yb1 N11 C82 -137.3(5) .
C85 Yb1 N11 C82 109.7(7) .
C84 Yb1 N11 C82 74.4(5) .
C54 Yb1 N11 C82 -107.8(5) .
C83 Yb1 N11 C82 34.8(4) .
C52 Yb1 N11 C82 -142.5(5) .
N4 Yb1 N11 Yb2 93.5(3) .
N3 Yb1 N11 Yb2 -99.3(3) .
N1 Yb1 N11 Yb2 -61.7(11) .
N2 Yb1 N11 Yb2 167.9(3) .
C53 Yb1 N11 Yb2 -20.0(3) .
C85 Yb1 N11 Yb2 -133.1(6) .
C84 Yb1 N11 Yb2 -168.3(5) .
C54 Yb1 N11 Yb2 9.5(3) .
C82 Yb1 N11 Yb2 117.3(6) .
C83 Yb1 N11 Yb2 152.1(4) .
C52 Yb1 N11 Yb2 -25.2(3) .
N8 Yb2 N12 C90 -137.9(8) .
N7 Yb2 N12 C90 28.3(8) .
N11 Yb2 N12 C90 67.4(9) .
N6 Yb2 N12 C90 -98.2(8) .
N10 Yb2 N12 C90 -179.0(9) .
N9 Yb2 N12 C90 112.1(8) .
N5 Yb2 N12 C90 -32.9(9) .
N8 Yb2 N12 C87 38.4(7) .
N7 Yb2 N12 C87 -155.4(6) .
N11 Yb2 N12 C87 -116.2(6) .
N6 Yb2 N12 C87 78.2(5) .
N10 Yb2 N12 C87 -2.6(5) .
N9 Yb2 N12 C87 -71.5(5) .
N5 Yb2 N12 C87 143.4(5) .
N16 Yb3 N13 C111 -120.4(5) 2_756
N16 Yb3 N13 C111 -171.1(5) .
N15 Yb3 N13 C111 75.1(5) 2_756
N15 Yb3 N13 C111 3.0(5) .
N14 Yb3 N13 C111 -59.5(6) 2_756
N14 Yb3 N13 C111 154.7(5) .
N13 Yb3 N13 C111 40.3(5) 2_756
C117 Yb3 N13 C111 -102.2(5) 2_756
N16 Yb3 N13 C92 40.2(5) 2_756
N16 Yb3 N13 C92 -10.6(6) .
N15 Yb3 N13 C92 -124.4(5) 2_756
N15 Yb3 N13 C92 163.6(5) .
N14 Yb3 N13 C92 101.1(5) 2_756
N14 Yb3 N13 C92 -44.8(5) .
N13 Yb3 N13 C92 -159.2(5) 2_756
C117 Yb3 N13 C92 58.3(5) 2_756
N16 Yb3 N14 C116 78.4(6) 2_756
N16 Yb3 N14 C116 -0.1(5) .
N15 Yb3 N14 C116 -122.5(6) 2_756
N15 Yb3 N14 C116 -163.6(5) .
N14 Yb3 N14 C116 40.4(5) 2_756
N13 Yb3 N14 C116 158.0(6) .
N13 Yb3 N14 C116 -65.9(6) 2_756
C117 Yb3 N14 C116 68.1(6) 2_756
N16 Yb3 N14 C102 -123.3(6) 2_756
N16 Yb3 N14 C102 158.1(7) .
N15 Yb3 N14 C102 35.7(6) 2_756
N15 Yb3 N14 C102 -5.3(7) .
N14 Yb3 N14 C102 -161.3(6) 2_756
N13 Yb3 N14 C102 -43.8(6) .
N13 Yb3 N14 C102 92.4(6) 2_756
C117 Yb3 N14 C102 -133.6(6) 2_756
N16 Yb3 N15 C112 64.9(5) 2_756
N16 Yb3 N15 C112 173.2(5) .
N15 Yb3 N15 C112 -84.1(5) 2_756
N14 Yb3 N15 C112 125.6(5) 2_756
N14 Yb3 N15 C112 -40.6(6) .
N13 Yb3 N15 C112 0.9(4) .
N13 Yb3 N15 C112 -153.8(5) 2_756
C117 Yb3 N15 C112 87.2(5) 2_756
N16 Yb3 N15 C115 -117.1(6) 2_756
N16 Yb3 N15 C115 -8.8(9) .
N15 Yb3 N15 C115 93.9(7) 2_756
N14 Yb3 N15 C115 -56.5(6) 2_756
N14 Yb3 N15 C115 137.4(6) .
N13 Yb3 N15 C115 178.9(7) .
N13 Yb3 N15 C115 24.2(6) 2_756
C117 Yb3 N15 C115 -94.9(7) 2_756
N16 Yb3 N15 Yb4 149.0(2) 2_756
N16 Yb3 N15 Yb4 -102.7(4) .
N15 Yb3 N15 Yb4 0.0 2_756
N14 Yb3 N15 Yb4 -150.4(3) 2_756
N14 Yb3 N15 Yb4 43.4(4) .
N13 Yb3 N15 Yb4 85.0(2) .
N13 Yb3 N15 Yb4 -69.7(2) 2_756
C117 Yb3 N15 Yb4 171.2(2) 2_756
N18 Yb4 N15 C112 -150.2(4) .
N18 Yb4 N15 C112 18.6(4) 2_756
N17 Yb4 N15 C112 -176.4(9) .
N17 Yb4 N15 C112 -55.9(4) 2_756
C114 Yb4 N15 C112 104.7(4) 2_756
C114 Yb4 N15 C112 -77.3(4) .
C113 Yb4 N15 C112 134.5(4) 2_756
C113 Yb4 N15 C112 -36.5(4) .
C115 Yb4 N15 C112 -113.5(6) .
C115 Yb4 N15 C112 91.7(4) 2_756
C112 Yb4 N15 C112 138.5(3) 2_756
N18 Yb4 N15 C115 -36.6(4) .
N18 Yb4 N15 C115 132.1(4) 2_756
N17 Yb4 N15 C115 -62.9(10) .
N17 Yb4 N15 C115 57.6(5) 2_756
C114 Yb4 N15 C115 -141.7(4) 2_756
C114 Yb4 N15 C115 36.2(4) .
C113 Yb4 N15 C115 -111.9(4) 2_756
C113 Yb4 N15 C115 77.0(4) .
C115 Yb4 N15 C115 -154.7(3) 2_756
C112 Yb4 N15 C115 -108.0(4) 2_756
C112 Yb4 N15 C115 113.5(6) .
N18 Yb4 N15 Yb3 98.6(3) .
N18 Yb4 N15 Yb3 -92.6(3) 2_756
N17 Yb4 N15 Yb3 72.4(10) .
N17 Yb4 N15 Yb3 -167.1(2) 2_756
C114 Yb4 N15 Yb3 -6.5(3) 2_756
C114 Yb4 N15 Yb3 171.5(4) .
C113 Yb4 N15 Yb3 23.3(3) 2_756
C113 Yb4 N15 Yb3 -147.7(4) .
C115 Yb4 N15 Yb3 135.3(5) .
C115 Yb4 N15 Yb3 -19.5(2) 2_756
C112 Yb4 N15 Yb3 27.3(2) 2_756
C112 Yb4 N15 Yb3 -111.2(5) .
N16 Yb3 N16 C120 85.3(8) 2_756
N15 Yb3 N16 C120 -122.6(8) 2_756
N15 Yb3 N16 C120 -32.2(10) .
N14 Yb3 N16 C120 14.5(8) 2_756
N14 Yb3 N16 C120 172.4(9) .
N13 Yb3 N16 C120 136.5(7) .
N13 Yb3 N16 C120 -65.0(8) 2_756
C117 Yb3 N16 C120 61.7(8) 2_756
N16 Yb3 N16 C117 -82.6(6) 2_756
N15 Yb3 N16 C117 69.5(6) 2_756
N15 Yb3 N16 C117 159.9(5) .
N14 Yb3 N16 C117 -153.4(6) 2_756
N14 Yb3 N16 C117 4.5(5) .
N13 Yb3 N16 C117 -31.4(7) .
N13 Yb3 N16 C117 127.1(6) 2_756
C117 Yb3 N16 C117 -106.2(6) 2_756
N18 Yb4 N17 C131 -5.0(5) .
N18 Yb4 N17 C131 -172.1(5) 2_756
N17 Yb4 N17 C131 -102.7(6) 2_756
C114 Yb4 N17 C131 104.7(6) 2_756
C114 Yb4 N17 C131 -65.5(6) .
C113 Yb4 N17 C131 73.7(5) 2_756
C113 Yb4 N17 C131 -108.3(6) .
C115 Yb4 N17 C131 -24.1(7) .
C115 Yb4 N17 C131 112.0(5) 2_756
C112 Yb4 N17 C131 65.4(5) 2_756
C112 Yb4 N17 C131 -151.3(7) .
N18 Yb4 N17 C122 151.6(6) .
N18 Yb4 N17 C122 -15.5(6) 2_756
N17 Yb4 N17 C122 54.0(5) 2_756
C114 Yb4 N17 C122 -98.6(6) 2_756
C114 Yb4 N17 C122 91.2(6) .
C113 Yb4 N17 C122 -129.6(6) 2_756
C113 Yb4 N17 C122 48.4(7) .
C115 Yb4 N17 C122 132.6(5) .
C115 Yb4 N17 C122 -91.4(6) 2_756
C112 Yb4 N17 C122 -137.9(6) 2_756
C112 Yb4 N17 C122 5.4(12) .
N18 Yb4 N18 C135 -156.1(8) 2_756
N17 Yb4 N18 C135 169.4(8) .
N17 Yb4 N18 C135 -123.8(8) 2_756
C114 Yb4 N18 C135 101.9(8) 2_756
C114 Yb4 N18 C135 -50.3(8) .
C113 Yb4 N18 C135 91.7(8) 2_756
C113 Yb4 N18 C135 -51.9(8) .
C115 Yb4 N18 C135 -21.6(7) .
C115 Yb4 N18 C135 76.3(8) 2_756
C112 Yb4 N18 C135 61.9(7) 2_756
C112 Yb4 N18 C135 -20.8(8) .
N18 Yb4 N18 C132 46.4(5) 2_756
N17 Yb4 N18 C132 11.9(5) .
N17 Yb4 N18 C132 78.7(5) 2_756
C114 Yb4 N18 C132 -55.6(5) 2_756
C114 Yb4 N18 C132 152.2(5) .
C113 Yb4 N18 C132 -65.7(5) 2_756
C113 Yb4 N18 C132 150.6(5) .
C115 Yb4 N18 C132 -179.1(5) .
C115 Yb4 N18 C132 -81.2(6) 2_756
C112 Yb4 N18 C132 -95.6(5) 2_756
C112 Yb4 N18 C132 -178.3(5) .
C6 C1 C2 C3 0.8(11) .
C11 C1 C2 C3 174.4(8) .
C6 C1 C2 N1 -172.4(7) .
C11 C1 C2 N1 1.1(11) .
C21 N1 C2 C3 127.1(9) .
Yb1 N1 C2 C3 -81.8(9) .
C21 N1 C2 C1 -59.8(10) .
Yb1 N1 C2 C1 91.4(8) .
C1 C2 C3 C4 0.0(12) .
N1 C2 C3 C4 172.9(8) .
C2 C3 C4 C5 0.2(12) .
C3 C4 C5 C6 -1.4(12) .
C3 C4 C5 C10 -176.5(8) .
C4 C5 C6 C7 -176.7(8) .
C10 C5 C6 C7 -1.5(12) .
C4 C5 C6 C1 2.2(12) .
C10 C5 C6 C1 177.4(7) .
C2 C1 C6 C7 177.0(8) .
C11 C1 C6 C7 3.5(12) .
C2 C1 C6 C5 -1.9(11) .
C11 C1 C6 C5 -175.4(8) .
C5 C6 C7 C8 2.0(12) .
C1 C6 C7 C8 -176.8(8) .
C6 C7 C8 C9 -1.7(13) .
C7 C8 C9 C10 0.9(14) .
C8 C9 C10 C5 -0.4(13) .
C4 C5 C10 C9 175.9(8) .
C6 C5 C10 C9 0.7(12) .
C2 C1 C11 C12 -62.0(11) .
C6 C1 C11 C12 111.4(9) .
C2 C1 C11 C16 115.1(9) .
C6 C1 C11 C16 -71.5(11) .
C16 C11 C12 N2 -174.1(7) .
C1 C11 C12 N2 3.1(11) .
C16 C11 C12 C13 2.2(11) .
C1 C11 C12 C13 179.4(8) .
C26 N2 C12 C11 -64.0(10) .
Yb1 N2 C12 C11 89.6(8) .
C26 N2 C12 C13 119.7(8) .
Yb1 N2 C12 C13 -86.7(8) .
C11 C12 C13 C14 0.7(13) .
N2 C12 C13 C14 176.9(8) .
C12 C13 C14 C15 0.0(14) .
C13 C14 C15 C20 179.9(10) .
C13 C14 C15 C16 -3.6(14) .
C20 C15 C16 C17 1.7(13) .
C14 C15 C16 C17 -174.9(8) .
C20 C15 C16 C11 -177.1(8) .
C14 C15 C16 C11 6.3(12) .
C12 C11 C16 C15 -5.7(11) .
C1 C11 C16 C15 177.2(8) .
C12 C11 C16 C17 175.5(7) .
C1 C11 C16 C17 -1.6(12) .
C15 C16 C17 C18 -0.7(12) .
C11 C16 C17 C18 178.0(8) .
C16 C17 C18 C19 -1.1(13) .
C17 C18 C19 C20 1.8(13) .
C18 C19 C20 C15 -0.7(14) .
C16 C15 C20 C19 -1.0(15) .
C14 C15 C20 C19 175.5(9) .
C2 N1 C21 C22 156.9(8) .
Yb1 N1 C21 C22 3.0(10) .
C25 N3 C22 C23 -0.5(9) .
Yb1 N3 C22 C23 -174.9(6) .
C25 N3 C22 C21 -172.2(7) .
Yb1 N3 C22 C21 13.4(9) .
N1 C21 C22 C23 179.2(10) .
N1 C21 C22 N3 -11.3(12) .
N3 C22 C23 C24 0.9(11) .
C21 C22 C23 C24 171.0(10) .
C22 C23 C24 C25 -0.9(11) .
C22 N3 C25 C24 -0.1(9) .
Yb1 N3 C25 C24 172.0(7) .
C23 C24 C25 N3 0.6(11) .
C12 N2 C26 C27 155.5(7) .
Yb1 N2 C26 C27 -0.9(9) .
C30 N4 C27 C28 -0.4(10) .
Yb1 N4 C27 C28 -170.8(6) .
C30 N4 C27 C26 -174.1(7) .
Yb1 N4 C27 C26 15.5(9) .
N2 C26 C27 N4 -9.9(12) .
N2 C26 C27 C28 177.6(9) .
N4 C27 C28 C29 1.4(11) .
C26 C27 C28 C29 174.2(8) .
C27 C28 C29 C30 -1.7(10) .
C27 N4 C30 C29 -0.7(9) .
Yb1 N4 C30 C29 166.1(7) .
C28 C29 C30 N4 1.6(10) .
C36 C31 C32 C33 1.4(12) .
C41 C31 C32 C33 -178.9(8) .
C36 C31 C32 N5 -177.7(7) .
C41 C31 C32 N5 2.0(12) .
C51 N5 C32 C31 -121.8(9) .
Yb2 N5 C32 C31 73.6(10) .
C51 N5 C32 C33 59.1(11) .
Yb2 N5 C32 C33 -105.6(8) .
C31 C32 C33 C34 1.7(14) .
N5 C32 C33 C34 -179.1(8) .
C32 C33 C34 C35 0.1(14) .
C33 C34 C35 C36 -5.0(13) .
C33 C34 C35 C40 178.4(8) .
C34 C35 C36 C37 -172.5(8) .
C40 C35 C36 C37 4.2(11) .
C34 C35 C36 C31 8.0(12) .
C40 C35 C36 C31 -175.2(7) .
C32 C31 C36 C35 -6.2(11) .
C41 C31 C36 C35 174.1(7) .
C32 C31 C36 C37 174.3(7) .
C41 C31 C36 C37 -5.4(11) .
C35 C36 C37 C38 -4.2(11) .
C31 C36 C37 C38 175.2(7) .
C36 C37 C38 C39 1.7(12) .
C37 C38 C39 C40 0.7(13) .
C38 C39 C40 C35 -0.5(13) .
C34 C35 C40 C39 174.7(9) .
C36 C35 C40 C39 -2.0(13) .
C32 C31 C41 C42 -61.1(11) .
C36 C31 C41 C42 118.6(8) .
C32 C31 C41 C46 119.2(9) .
C36 C31 C41 C46 -61.2(10) .
C46 C41 C42 C43 0.9(11) .
C31 C41 C42 C43 -178.8(7) .
C46 C41 C42 N6 -177.2(6) .
C31 C41 C42 N6 3.0(10) .
C56 N6 C42 C41 -61.9(10) .
Yb2 N6 C42 C41 96.4(7) .
C56 N6 C42 C43 120.0(8) .
Yb2 N6 C42 C43 -81.8(8) .
C41 C42 C43 C44 2.1(11) .
N6 C42 C43 C44 -179.8(7) .
C42 C43 C44 C45 -2.2(12) .
C43 C44 C45 C50 -179.9(8) .
C43 C44 C45 C46 -0.8(12) .
C50 C45 C46 C47 2.9(12) .
C44 C45 C46 C47 -176.2(8) .
C50 C45 C46 C41 -176.9(8) .
C44 C45 C46 C41 4.0(11) .
C42 C41 C46 C45 -4.0(11) .
C31 C41 C46 C45 175.8(7) .
C42 C41 C46 C47 176.2(8) .
C31 C41 C46 C47 -4.1(12) .
C45 C46 C47 C48 -3.6(13) .
C41 C46 C47 C48 176.2(9) .
C46 C47 C48 C49 1.3(15) .
C47 C48 C49 C50 1.9(15) .
C48 C49 C50 C45 -2.6(16) .
C44 C45 C50 C49 179.2(9) .
C46 C45 C50 C49 0.1(14) .
C32 N5 C51 C52 -179.0(7) .
Yb2 N5 C51 C52 -12.0(10) .
C55 N7 C52 C53 0.8(9) .
Yb2 N7 C52 C53 -172.0(5) .
Yb1 N7 C52 C53 -65.7(5) .
C55 N7 C52 C51 -174.3(7) .
Yb2 N7 C52 C51 12.9(9) .
Yb1 N7 C52 C51 119.2(7) .
C55 N7 C52 Yb1 66.5(5) .
Yb2 N7 C52 Yb1 -106.3(4) .
N5 C51 C52 N7 0.7(12) .
N5 C51 C52 C53 -173.3(8) .
N5 C51 C52 Yb1 97.7(8) .
N4 Yb1 C52 N7 -40.5(5) .
N3 Yb1 C52 N7 159.5(5) .
N1 Yb1 C52 N7 -133.5(4) .
N2 Yb1 C52 N7 -175.0(7) .
C53 Yb1 C52 N7 -115.9(7) .
C85 Yb1 C52 N7 80.8(4) .
N11 Yb1 C52 N7 53.2(4) .
C84 Yb1 C52 N7 81.7(5) .
C54 Yb1 C52 N7 -76.1(5) .
C82 Yb1 C52 N7 36.2(4) .
C83 Yb1 C52 N7 50.9(5) .
N4 Yb1 C52 C53 75.4(5) .
N3 Yb1 C52 C53 -84.6(5) .
N1 Yb1 C52 C53 -17.6(5) .
N2 Yb1 C52 C53 -59.0(10) .
C85 Yb1 C52 C53 -163.3(5) .
N11 Yb1 C52 C53 169.2(5) .
C84 Yb1 C52 C53 -162.4(5) .
C54 Yb1 C52 C53 39.8(5) .
C82 Yb1 C52 C53 152.1(5) .
C83 Yb1 C52 C53 166.9(4) .
N4 Yb1 C52 C51 -158.9(5) .
N3 Yb1 C52 C51 41.1(6) .
N1 Yb1 C52 C51 108.2(6) .
N2 Yb1 C52 C51 66.7(10) .
C53 Yb1 C52 C51 125.7(8) .
C85 Yb1 C52 C51 -37.6(6) .
N11 Yb1 C52 C51 -65.1(5) .
C84 Yb1 C52 C51 -36.7(6) .
C54 Yb1 C52 C51 165.6(7) .
C82 Yb1 C52 C51 -82.2(6) .
C83 Yb1 C52 C51 -67.4(6) .
N7 C52 C53 C54 0.0(9) .
C51 C52 C53 C54 174.4(8) .
Yb1 C52 C53 C54 -72.7(5) .
N7 C52 C53 Yb1 72.7(6) .
C51 C52 C53 Yb1 -112.9(8) .
N4 Yb1 C53 C54 -9.2(5) .
N3 Yb1 C53 C54 -161.9(5) .
N1 Yb1 C53 C54 -89.5(5) .
N2 Yb1 C53 C54 -92.8(5) .
C85 Yb1 C53 C54 126.1(5) .
N11 Yb1 C53 C54 98.3(5) .
C84 Yb1 C53 C54 133.1(5) .
C82 Yb1 C53 C54 76.4(5) .
C83 Yb1 C53 C54 87.7(6) .
C52 Yb1 C53 C54 108.6(7) .
N4 Yb1 C53 C52 -117.8(5) .
N3 Yb1 C53 C52 89.4(5) .
N1 Yb1 C53 C52 161.9(5) .
N2 Yb1 C53 C52 158.6(4) .
C85 Yb1 C53 C52 17.4(5) .
N11 Yb1 C53 C52 -10.3(5) .
C84 Yb1 C53 C52 24.5(6) .
C54 Yb1 C53 C52 -108.6(7) .
C82 Yb1 C53 C52 -32.2(5) .
C83 Yb1 C53 C52 -21.0(7) .
C52 C53 C54 C55 -0.7(9) .
Yb1 C53 C54 C55 -76.6(6) .
C52 C53 C54 Yb1 75.9(5) .
N4 Yb1 C54 C53 171.3(5) .
N3 Yb1 C54 C53 18.3(5) .
N1 Yb1 C54 C53 82.0(5) .
N2 Yb1 C54 C53 119.7(5) .
C85 Yb1 C54 C53 -66.6(5) .
N11 Yb1 C54 C53 -87.0(5) .
C84 Yb1 C54 C53 -83.8(7) .
C82 Yb1 C54 C53 -115.9(5) .
C83 Yb1 C54 C53 -127.4(5) .
C52 Yb1 C54 C53 -38.9(4) .
N4 Yb1 C54 C55 -78.2(5) .
N3 Yb1 C54 C55 128.8(5) .
N1 Yb1 C54 C55 -167.5(5) .
N2 Yb1 C54 C55 -129.8(5) .
C53 Yb1 C54 C55 110.5(7) .
C85 Yb1 C54 C55 43.9(6) .
N11 Yb1 C54 C55 23.5(5) .
C84 Yb1 C54 C55 26.7(8) .
C82 Yb1 C54 C55 -5.4(5) .
C83 Yb1 C54 C55 -16.9(6) .
C52 Yb1 C54 C55 71.6(5) .
C52 N7 C55 C54 -1.3(9) .
Yb2 N7 C55 C54 169.9(6) .
Yb1 N7 C55 C54 63.5(6) .
C52 N7 C55 Yb1 -64.7(5) .
Yb2 N7 C55 Yb1 106.4(6) .
C53 C54 C55 N7 1.3(10) .
Yb1 C54 C55 N7 -69.9(6) .
C53 C54 C55 Yb1 71.2(6) .
N4 Yb1 C55 N7 -147.2(5) .
N3 Yb1 C55 N7 54.7(6) .
N1 Yb1 C55 N7 128.7(5) .
N2 Yb1 C55 N7 -161.6(4) .
C53 Yb1 C55 N7 77.2(5) .
C85 Yb1 C55 N7 -27.4(5) .
N11 Yb1 C55 N7 -39.9(5) .
C84 Yb1 C55 N7 -48.0(6) .
C54 Yb1 C55 N7 116.3(7) .
C82 Yb1 C55 N7 -68.9(5) .
C83 Yb1 C55 N7 -76.1(5) .
C52 Yb1 C55 N7 36.7(4) .
N4 Yb1 C55 C54 96.5(5) .
N3 Yb1 C55 C54 -61.6(5) .
N1 Yb1 C55 C54 12.4(5) .
N2 Yb1 C55 C54 82.1(6) .
C53 Yb1 C55 C54 -39.1(5) .
C85 Yb1 C55 C54 -143.7(5) .
N11 Yb1 C55 C54 -156.2(5) .
C84 Yb1 C55 C54 -164.3(5) .
C82 Yb1 C55 C54 174.8(5) .
C83 Yb1 C55 C54 167.6(5) .
C52 Yb1 C55 C54 -79.6(5) .
C42 N6 C56 C57 165.6(7) .
Yb2 N6 C56 C57 5.8(10) .
C60 N8 C57 C58 -2.3(9) .
Yb2 N8 C57 C58 -176.4(5) .
C60 N8 C57 C56 -176.6(7) .
Yb2 N8 C57 C56 9.3(9) .
N6 C56 C57 N8 -10.4(12) .
N6 C56 C57 C58 176.6(8) .
N8 C57 C58 C59 2.6(9) .
C56 C57 C58 C59 175.8(9) .
C57 C58 C59 C60 -1.9(9) .
C57 N8 C60 C59 1.0(9) .
Yb2 N8 C60 C59 173.0(6) .
C58 C59 C60 N8 0.6(9) .
C66 C61 C62 C63 4.0(11) .
C71 C61 C62 C63 -177.7(7) .
C66 C61 C62 N9 -172.6(7) .
C71 C61 C62 N9 5.7(11) .
C81 N9 C62 C61 -107.0(8) .
Yb2 N9 C62 C61 75.9(9) .
C81 N9 C62 C63 76.3(9) .
Yb2 N9 C62 C63 -100.8(7) .
C61 C62 C63 C64 -0.2(12) .
N9 C62 C63 C64 176.5(7) .
C62 C63 C64 C65 -2.8(12) .
C63 C64 C65 C66 1.8(12) .
C63 C64 C65 C70 -174.9(8) .
C70 C65 C66 C67 2.6(11) .
C64 C65 C66 C67 -174.2(7) .
C70 C65 C66 C61 178.8(8) .
C64 C65 C66 C61 2.1(11) .
C62 C61 C66 C65 -4.9(11) .
C71 C61 C66 C65 176.8(7) .
C62 C61 C66 C67 171.3(7) .
C71 C61 C66 C67 -7.0(11) .
C65 C66 C67 C68 -1.7(12) .
C61 C66 C67 C68 -178.0(7) .
C66 C67 C68 C69 -0.8(11) .
C67 C68 C69 C70 2.5(12) .
C68 C69 C70 C65 -1.6(13) .
C66 C65 C70 C69 -1.0(12) .
C64 C65 C70 C69 175.7(8) .
C62 C61 C71 C72 -65.5(10) .
C66 C61 C71 C72 112.7(8) .
C62 C61 C71 C76 112.3(8) .
C66 C61 C71 C76 -69.5(10) .
C76 C71 C72 C73 1.8(10) .
C61 C71 C72 C73 179.7(7) .
C76 C71 C72 N10 -174.2(6) .
C61 C71 C72 N10 3.7(10) .
C86 N10 C72 C71 -57.0(9) .
Yb2 N10 C72 C71 94.1(7) .
C86 N10 C72 C73 126.9(7) .
Yb2 N10 C72 C73 -82.0(7) .
C71 C72 C73 C74 0.5(11) .
N10 C72 C73 C74 176.6(7) .
C72 C73 C74 C75 -1.7(12) .
C73 C74 C75 C80 179.7(8) .
C73 C74 C75 C76 0.4(11) .
C80 C75 C76 C71 -177.3(8) .
C74 C75 C76 C71 2.0(11) .
C80 C75 C76 C77 0.3(11) .
C74 C75 C76 C77 179.6(7) .
C72 C71 C76 C75 -3.1(10) .
C61 C71 C76 C75 179.1(7) .
C72 C71 C76 C77 179.5(7) .
C61 C71 C76 C77 1.6(11) .
C75 C76 C77 C78 0.0(11) .
C71 C76 C77 C78 177.6(7) .
C76 C77 C78 C79 -1.1(13) .
C77 C78 C79 C80 1.8(14) .
C78 C79 C80 C75 -1.5(14) .
C76 C75 C80 C79 0.4(13) .
C74 C75 C80 C79 -178.9(8) .
C62 N9 C81 C82 179.1(7) .
Yb2 N9 C81 C82 -3.4(9) .
C85 N11 C82 C83 2.1(9) .
Yb2 N11 C82 C83 173.3(5) .
Yb1 N11 C82 C83 -68.7(6) .
C85 N11 C82 C81 -172.6(7) .
Yb2 N11 C82 C81 -1.3(9) .
Yb1 N11 C82 C81 116.6(6) .
C85 N11 C82 Yb1 70.8(5) .
Yb2 N11 C82 Yb1 -117.9(4) .
N9 C81 C82 N11 3.3(11) .
N9 C81 C82 C83 -170.2(8) .
N9 C81 C82 Yb1 91.8(7) .
N4 Yb1 C82 N11 156.2(5) .
N3 Yb1 C82 N11 -44.4(5) .
N1 Yb1 C82 N11 179.3(6) .
N2 Yb1 C82 N11 -136.9(4) .
C53 Yb1 C82 N11 49.9(5) .
C85 Yb1 C82 N11 -38.7(4) .
C84 Yb1 C82 N11 -78.6(5) .
C54 Yb1 C82 N11 79.9(5) .
C83 Yb1 C82 N11 -117.0(7) .
C52 Yb1 C82 N11 35.1(5) .
N4 Yb1 C82 C83 -86.8(5) .
N3 Yb1 C82 C83 72.6(5) .
N1 Yb1 C82 C83 -63.7(9) .
N2 Yb1 C82 C83 -19.9(5) .
C53 Yb1 C82 C83 166.9(4) .
C85 Yb1 C82 C83 78.3(5) .
N11 Yb1 C82 C83 117.0(7) .
C84 Yb1 C82 C83 38.4(5) .
C54 Yb1 C82 C83 -163.0(5) .
C52 Yb1 C82 C83 152.1(5) .
N4 Yb1 C82 C81 41.7(5) .
N3 Yb1 C82 C81 -158.9(5) .
N1 Yb1 C82 C81 64.8(10) .
N2 Yb1 C82 C81 108.6(5) .
C53 Yb1 C82 C81 -64.6(6) .
C85 Yb1 C82 C81 -153.2(7) .
N11 Yb1 C82 C81 -114.5(8) .
C84 Yb1 C82 C81 166.9(7) .
C54 Yb1 C82 C81 -34.6(6) .
C83 Yb1 C82 C81 128.5(8) .
C52 Yb1 C82 C81 -79.4(6) .
N11 C82 C83 C84 -0.5(9) .
C81 C82 C83 C84 173.5(8) .
Yb1 C82 C83 C84 -68.0(6) .
N11 C82 C83 Yb1 67.6(6) .
C81 C82 C83 Yb1 -118.5(8) .
N4 Yb1 C83 C82 86.3(5) .
N3 Yb1 C83 C82 -121.2(4) .
N1 Yb1 C83 C82 154.8(4) .
N2 Yb1 C83 C82 159.4(5) .
C53 Yb1 C83 C82 -20.9(7) .
C85 Yb1 C83 C82 -74.1(5) .
N11 Yb1 C83 C82 -35.0(4) .
C84 Yb1 C83 C82 -111.5(7) .
C54 Yb1 C83 C82 23.3(6) .
C52 Yb1 C83 C82 -32.1(5) .
N4 Yb1 C83 C84 -162.3(5) .
N3 Yb1 C83 C84 -9.7(5) .
N1 Yb1 C83 C84 -93.8(5) .
N2 Yb1 C83 C84 -89.2(5) .
C53 Yb1 C83 C84 90.6(6) .
C85 Yb1 C83 C84 37.4(4) .
N11 Yb1 C83 C84 76.4(5) .
C54 Yb1 C83 C84 134.7(5) .
C82 Yb1 C83 C84 111.5(7) .
C52 Yb1 C83 C84 79.3(5) .
C82 C83 C84 C85 -1.4(9) .
Yb1 C83 C84 C85 -70.0(6) .
C82 C83 C84 Yb1 68.7(5) .
N4 Yb1 C84 C85 129.7(5) .
N3 Yb1 C84 C85 -77.3(5) .
N1 Yb1 C84 C85 -129.8(5) .
N2 Yb1 C84 C85 -166.3(5) .
C53 Yb1 C84 C85 -14.0(7) .
N11 Yb1 C84 C85 35.2(4) .
C54 Yb1 C84 C85 31.0(8) .
C82 Yb1 C84 C85 74.4(5) .
C83 Yb1 C84 C85 111.8(7) .
C52 Yb1 C84 C85 -1.8(6) .
N4 Yb1 C84 C83 17.9(5) .
N3 Yb1 C84 C83 170.9(5) .
N1 Yb1 C84 C83 118.4(5) .
N2 Yb1 C84 C83 81.9(4) .
C53 Yb1 C84 C83 -125.8(5) .
C85 Yb1 C84 C83 -111.8(7) .
N11 Yb1 C84 C83 -76.6(5) .
C54 Yb1 C84 C83 -80.8(7) .
C82 Yb1 C84 C83 -37.4(4) .
C52 Yb1 C84 C83 -113.6(4) .
C82 N11 C85 C84 -3.0(9) .
Yb2 N11 C85 C84 -172.4(6) .
Yb1 N11 C85 C84 68.4(6) .
C82 N11 C85 Yb1 -71.3(5) .
Yb2 N11 C85 Yb1 119.2(6) .
C83 C84 C85 N11 2.8(10) .
Yb1 C84 C85 N11 -68.3(6) .
C83 C84 C85 Yb1 71.0(6) .
N4 Yb1 C85 N11 55.9(5) .
N3 Yb1 C85 N11 -146.0(5) .
N1 Yb1 C85 N11 -160.7(4) .
N2 Yb1 C85 N11 130.0(5) .
C53 Yb1 C85 N11 -73.6(5) .
C84 Yb1 C85 N11 116.5(7) .
C54 Yb1 C85 N11 -45.4(6) .
C82 Yb1 C85 N11 38.8(4) .
C83 Yb1 C85 N11 78.4(5) .
C52 Yb1 C85 N11 -65.3(5) .
N4 Yb1 C85 C84 -60.6(6) .
N3 Yb1 C85 C84 97.6(5) .
N1 Yb1 C85 C84 82.9(7) .
N2 Yb1 C85 C84 13.5(5) .
C53 Yb1 C85 C84 169.9(5) .
N11 Yb1 C85 C84 -116.5(7) .
C54 Yb1 C85 C84 -161.9(5) .
C82 Yb1 C85 C84 -77.6(5) .
C83 Yb1 C85 C84 -38.1(5) .
C52 Yb1 C85 C84 178.3(5) .
C72 N10 C86 C87 157.5(7) .
Yb2 N10 C86 C87 4.0(9) .
C90 N12 C87 C88 -0.5(9) .
Yb2 N12 C87 C88 -178.0(5) .
C90 N12 C87 C86 -176.7(7) .
Yb2 N12 C87 C86 5.7(9) .
N10 C86 C87 N12 -6.8(11) .
N10 C86 C87 C88 178.0(8) .
N12 C87 C88 C89 0.0(10) .
C86 C87 C88 C89 175.6(9) .
C87 C88 C89 C90 0.5(10) .
C87 N12 C90 C89 0.8(10) .
Yb2 N12 C90 C89 177.4(6) .
C88 C89 C90 N12 -0.8(11) .
C96 C91 C92 C93 7.2(12) .
C101 C91 C92 C93 -171.9(8) .
C96 C91 C92 N13 -166.0(7) .
C101 C91 C92 N13 14.8(12) .
C111 N13 C92 C91 -131.5(8) .
Yb3 N13 C92 C91 68.1(9) .
C111 N13 C92 C93 55.0(9) .
Yb3 N13 C92 C93 -105.3(7) .
C91 C92 C93 C94 -6.6(12) .
N13 C92 C93 C94 166.8(8) .
C92 C93 C94 C95 0.7(13) .
C93 C94 C95 C100 -172.9(9) .
C93 C94 C95 C96 3.9(13) .
C92 C91 C96 C97 175.2(8) .
C101 C91 C96 C97 -5.7(13) .
C92 C91 C96 C95 -2.4(13) .
C101 C91 C96 C95 176.8(8) .
C94 C95 C96 C97 179.3(9) .
C100 C95 C96 C97 -3.7(13) .
C94 C95 C96 C91 -3.1(13) .
C100 C95 C96 C91 173.9(8) .
C91 C96 C97 C98 -173.4(9) .
C95 C96 C97 C98 4.2(14) .
C96 C97 C98 C99 -4.2(16) .
C97 C98 C99 C100 3.7(17) .
C98 C99 C100 C95 -3.3(17) .
C94 C95 C100 C99 -180.0(10) .
C96 C95 C100 C99 3.1(14) .
C92 C91 C101 C102 -82.6(10) .
C96 C91 C101 C102 98.3(10) .
C92 C91 C101 C106 103.7(9) .
C96 C91 C101 C106 -75.4(10) .
C106 C101 C102 N14 -167.9(7) .
C91 C101 C102 N14 18.4(12) .
C106 C101 C102 C103 5.1(12) .
C91 C101 C102 C103 -168.5(7) .
C116 N14 C102 C101 -136.7(8) .
Yb3 N14 C102 C101 66.0(10) .
C116 N14 C102 C103 50.2(11) .
Yb3 N14 C102 C103 -107.1(8) .
C101 C102 C103 C104 -2.8(13) .
N14 C102 C103 C104 170.4(8) .
C102 C103 C104 C105 -3.0(13) .
C103 C104 C105 C110 -171.3(9) .
C103 C104 C105 C106 6.2(13) .
C102 C101 C106 C107 174.5(8) .
C91 C101 C106 C107 -11.6(11) .
C102 C101 C106 C105 -1.9(11) .
C91 C101 C106 C105 171.9(7) .
C104 C105 C106 C107 179.8(8) .
C110 C105 C106 C107 -2.6(12) .
C104 C105 C106 C101 -3.7(11) .
C110 C105 C106 C101 173.9(7) .
C101 C106 C107 C108 -173.6(8) .
C105 C106 C107 C108 2.8(12) .
C106 C107 C108 C109 -0.7(13) .
C107 C108 C109 C110 -1.5(15) .
C108 C109 C110 C105 1.6(16) .
C104 C105 C110 C109 177.9(10) .
C106 C105 C110 C109 0.5(14) .
C92 N13 C111 C112 -168.3(6) .
Yb3 N13 C111 C112 -6.7(8) .
C115 N15 C112 C113 1.0(8) .
Yb3 N15 C112 C113 179.6(4) .
Yb4 N15 C112 C113 67.1(5) .
C115 N15 C112 C111 177.0(6) .
Yb3 N15 C112 C111 -4.5(8) .
Yb4 N15 C112 C111 -117.0(6) .
C115 N15 C112 Yb4 -66.0(4) .
Yb3 N15 C112 Yb4 112.5(3) .
N13 C111 C112 N15 7.8(10) .
N13 C111 C112 C113 -177.3(7) .
N13 C111 C112 Yb4 -85.3(7) .
N18 Yb4 C112 N15 35.4(4) .
N18 Yb4 C112 N15 -161.2(4) 2_756
N17 Yb4 C112 N15 177.3(7) .
N17 Yb4 C112 N15 132.1(4) 2_756
C114 Yb4 C112 N15 -83.7(4) 2_756
C114 Yb4 C112 N15 76.9(4) .
C113 Yb4 C112 N15 -52.3(4) 2_756
C113 Yb4 C112 N15 115.4(6) .
C115 Yb4 C112 N15 36.5(3) .
C115 Yb4 C112 N15 -83.0(4) 2_756
C112 Yb4 C112 N15 -38.6(3) 2_756
N18 Yb4 C112 C113 -80.0(5) .
N18 Yb4 C112 C113 83.4(4) 2_756
N17 Yb4 C112 C113 61.8(9) .
N17 Yb4 C112 C113 16.6(5) 2_756
C114 Yb4 C112 C113 160.8(4) 2_756
C114 Yb4 C112 C113 -38.6(4) .
C113 Yb4 C112 C113 -167.8(3) 2_756
C115 Yb4 C112 C113 -78.9(4) .
C115 Yb4 C112 C113 161.5(4) 2_756
C112 Yb4 C112 C113 -154.1(5) 2_756
N18 Yb4 C112 C111 152.7(5) .
N18 Yb4 C112 C111 -43.9(5) 2_756
N17 Yb4 C112 C111 -65.4(10) .
N17 Yb4 C112 C111 -110.6(5) 2_756
C114 Yb4 C112 C111 33.6(6) 2_756
C114 Yb4 C112 C111 -165.8(7) .
C113 Yb4 C112 C111 65.0(6) 2_756
C113 Yb4 C112 C111 -127.3(8) .
C115 Yb4 C112 C111 153.8(7) .
C115 Yb4 C112 C111 34.3(5) 2_756
C112 Yb4 C112 C111 78.7(5) 2_756
N15 C112 C113 C114 -2.1(8) .
C111 C112 C113 C114 -177.5(7) .
Yb4 C112 C113 C114 68.6(5) .
N15 C112 C113 Yb4 -70.8(5) .
C111 C112 C113 Yb4 113.9(8) .
N18 Yb4 C113 C112 114.6(4) .
N18 Yb4 C113 C112 -88.8(4) 2_756
N17 Yb4 C113 C112 -157.5(4) .
N17 Yb4 C113 C112 -163.0(5) 2_756
C114 Yb4 C113 C112 -26.6(6) 2_756
C114 Yb4 C113 C112 111.5(6) .
C113 Yb4 C113 C112 19.2(4) 2_756
C115 Yb4 C113 C112 72.8(4) .
C115 Yb4 C113 C112 -19.2(5) 2_756
C112 Yb4 C113 C112 29.4(6) 2_756
N18 Yb4 C113 C114 3.1(5) .
N18 Yb4 C113 C114 159.7(5) 2_756
N17 Yb4 C113 C114 90.9(5) .
N17 Yb4 C113 C114 85.5(5) 2_756
C114 Yb4 C113 C114 -138.1(6) 2_756
C113 Yb4 C113 C114 -92.3(4) 2_756
C115 Yb4 C113 C114 -38.8(4) .
C115 Yb4 C113 C114 -130.7(5) 2_756
C112 Yb4 C113 C114 -82.1(5) 2_756
C112 Yb4 C113 C114 -111.5(6) .
C112 C113 C114 C115 2.3(8) .
Yb4 C113 C114 C115 74.1(5) .
C112 C113 C114 Yb4 -71.8(5) .
N18 Yb4 C114 C115 73.7(5) .
N18 Yb4 C114 C115 -129.2(5) 2_756
N17 Yb4 C114 C115 129.5(5) .
N17 Yb4 C114 C115 165.3(5) 2_756
C114 Yb4 C114 C115 -30.1(4) 2_756
C113 Yb4 C114 C115 14.7(6) 2_756
C113 Yb4 C114 C115 -109.2(7) .
C115 Yb4 C114 C115 -47.4(6) 2_756
C112 Yb4 C114 C115 1.4(5) 2_756
C112 Yb4 C114 C115 -71.8(5) .
N18 Yb4 C114 C113 -177.1(5) .
N18 Yb4 C114 C113 -20.0(5) 2_756
N17 Yb4 C114 C113 -121.3(5) .
N17 Yb4 C114 C113 -85.5(5) 2_756
C114 Yb4 C114 C113 79.1(4) 2_756
C113 Yb4 C114 C113 123.9(6) 2_756
C115 Yb4 C114 C113 109.2(7) .
C115 Yb4 C114 C113 61.8(5) 2_756
C112 Yb4 C114 C113 110.7(5) 2_756
C112 Yb4 C114 C113 37.4(4) .
C112 N15 C115 C114 0.5(8) .
Yb3 N15 C115 C114 -177.6(5) .
Yb4 N15 C115 C114 -66.1(5) .
C112 N15 C115 Yb4 66.6(5) .
Yb3 N15 C115 Yb4 -111.5(5) .
C113 C114 C115 N15 -1.8(8) .
Yb4 C114 C115 N15 70.8(5) .
C113 C114 C115 Yb4 -72.6(5) .
N18 Yb4 C115 N15 142.6(4) .
N18 Yb4 C115 N15 -56.2(4) 2_756
N17 Yb4 C115 N15 161.1(4) .
N17 Yb4 C115 N15 -130.7(4) 2_756
C114 Yb4 C115 N15 47.1(5) 2_756
C114 Yb4 C115 N15 -116.2(7) .
C113 Yb4 C115 N15 74.4(4) 2_756
C113 Yb4 C115 N15 -76.6(4) .
C115 Yb4 C115 N15 25.5(3) 2_756
C112 Yb4 C115 N15 65.1(4) 2_756
C112 Yb4 C115 N15 -36.4(4) .
N18 Yb4 C115 C114 -101.1(5) .
N18 Yb4 C115 C114 60.1(5) 2_756
N17 Yb4 C115 C114 -82.6(6) .
N17 Yb4 C115 C114 -14.4(5) 2_756
C114 Yb4 C115 C114 163.3(3) 2_756
C113 Yb4 C115 C114 -169.4(4) 2_756
C113 Yb4 C115 C114 39.6(4) .
C115 Yb4 C115 C114 141.7(5) 2_756
C112 Yb4 C115 C114 -178.6(5) 2_756
C112 Yb4 C115 C114 79.8(5) .
C102 N14 C116 C117 -165.1(8) .
Yb3 N14 C116 C117 -4.6(10) .
C120 N16 C117 C116 179.4(8) .
Yb3 N16 C117 C116 -9.0(10) .
C120 N16 C117 C118 1.5(9) .
Yb3 N16 C117 C118 173.0(5) .
N14 C116 C117 N16 9.6(13) .
N14 C116 C117 C118 -172.9(8) .
N16 C117 C118 C119 -0.7(10) .
C116 C117 C118 C119 -178.4(9) .
C117 C118 C119 C120 -0.4(10) .
C117 N16 C120 C119 -1.7(9) .
Yb3 N16 C120 C119 -170.2(6) .
C118 C119 C120 N16 1.3(10) .
C126 C121 C122 C123 -4.6(12) .
C121 C121 C122 C123 179.2(8) 2_756
C126 C121 C122 N17 172.1(7) .
C121 C121 C122 N17 -4.1(12) 2_756
C131 N17 C122 C121 67.0(9) .
Yb4 N17 C122 C121 -88.8(8) .
C131 N17 C122 C123 -116.3(8) .
Yb4 N17 C122 C123 87.9(8) .
C121 C122 C123 C124 2.9(13) .
N17 C122 C123 C124 -173.7(8) .
C122 C123 C124 C125 0.6(14) .
C123 C124 C125 C130 172.1(11) .
C123 C124 C125 C126 -2.2(15) .
C122 C121 C126 C127 -173.7(9) .
C121 C121 C126 C127 2.4(13) 2_756
C122 C121 C126 C125 2.9(12) .
C121 C121 C126 C125 179.1(8) 2_756
C130 C125 C126 C121 -174.3(10) .
C124 C125 C126 C121 0.4(14) .
C130 C125 C126 C127 2.4(15) .
C124 C125 C126 C127 177.1(9) .
C121 C126 C127 C128 176.2(9) .
C125 C126 C127 C128 -0.4(15) .
C126 C127 C128 C129 -3.7(18) .
C127 C128 C129 C130 6(2) .
C128 C129 C130 C125 -4(2) .
C124 C125 C130 C129 -174.7(12) .
C126 C125 C130 C129 -0.2(19) .
C122 N17 C131 C132 -161.6(7) .
Yb4 N17 C131 C132 -2.8(9) .
C135 N18 C132 C133 -1.3(9) .
Yb4 N18 C132 C133 163.9(5) .
C135 N18 C132 C131 176.5(7) .
Yb4 N18 C132 C131 -18.3(9) .
N17 C131 C132 C133 -168.1(8) .
N17 C131 C132 N18 14.6(11) .
N18 C132 C133 C134 0.5(9) .
C131 C132 C133 C134 -177.0(8) .
C132 C133 C134 C135 0.5(9) .
C132 N18 C135 C134 1.6(9) .
Yb4 N18 C135 C134 -157.2(6) .
C133 C134 C135 N18 -1.4(9) .
C142 C137 C138 C139 0.0 .
C136 C137 C138 C139 -175.0(18) .
C137 C138 C139 C140 0.0 .
C138 C139 C140 C141 0.0 .
C139 C140 C141 C142 0.0 .
C140 C141 C142 C137 0.0 .
C138 C137 C142 C141 0.0 .
C136 C137 C142 C141 175.4(17) .
C148 C143 C144 C145 3(2) .
C143 C144 C145 C146 -7(2) .
C144 C145 C146 C147 5(2) .
C145 C146 C147 C148 1(2) .
C146 C147 C148 C143 -4(2) .
C144 C143 C148 C147 2.3(17) .
loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
1 0.000 0.072 0.000 1430.9 252.2
2 0.500 -0.143 0.000 1430.9 252.2
3 0.296 0.038 0.396 13.5 2.9
4 0.704 0.038 0.603 13.5 2.7
5 0.155 0.022 0.425 5.6 0.6
6 0.844 0.022 0.575 5.2 0.5
7 0.204 0.538 0.603 13.5 2.7
8 0.796 0.538 0.396 13.5 2.9
9 0.344 0.522 0.575 5.2 0.5
10 0.655 0.522 0.425 5.6 0.6
