#------------------------------------------------------------------------------
#$Date: 2016-03-21 09:55:35 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178630 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/41/4074124.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4074124
loop_
_publ_author_name
'Buchowicz, Włodzimierz'
'Jerzykiewicz, Lucjan B.'
'Krasińska, Anna'
'Losi, Serena'
'Pietrzykowski, Antoni'
'Zanello, Piero'
_publ_section_title
;
 ansa-Nickelocenes by the Ring-Closing Metathesis Route: 
 Syntheses, X-ray Crystal Structures, and Physical Properties
;
_journal_issue                   21
_journal_name_full               Organometallics
_journal_page_first              5076
_journal_paper_doi               10.1021/om060423v
_journal_volume                  25
_journal_year                    2006
_chemical_formula_moiety         'C32 H36 Ni2'
_chemical_formula_sum            'C32 H36 Ni2'
_chemical_formula_weight         538.03
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 108.05(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   16.487(5)
_cell_length_b                   7.617(4)
_cell_length_c                   10.600(4)
_cell_measurement_reflns_used    6082
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      27
_cell_measurement_theta_min      3
_cell_volume                     1265.7(9)
_computing_cell_refinement       'Oxford Diffraion software, CrystAlis 1.171'
_computing_data_collection       'Oxford Diffraion software, CrystAlis 1.171'
_computing_data_reduction        'Oxford Diffraion software, CrystAlis 1.171'
_computing_molecular_graphics    'SHELXTL-NT V5.1, Bruker AXS 1999'
_computing_publication_material  'SHELXTL-NT V5.1, Bruker AXS 1999'
_computing_structure_refinement  'SHELXTL-NT V5.1, Bruker AXS 1999'
_computing_structure_solution    'SHELXTL-NT V5.1, Bruker AXS 1999'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.997
_diffrn_measured_fraction_theta_max 0.997
_diffrn_measurement_device_type  'Kuma CCD-KM4 automatic diffractometer'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0394
_diffrn_reflns_av_sigmaI/netI    0.0426
_diffrn_reflns_limit_h_max       21
_diffrn_reflns_limit_h_min       -21
_diffrn_reflns_limit_k_max       9
_diffrn_reflns_limit_k_min       -9
_diffrn_reflns_limit_l_max       13
_diffrn_reflns_limit_l_min       -10
_diffrn_reflns_number            7704
_diffrn_reflns_theta_full        26.98
_diffrn_reflns_theta_max         26.98
_diffrn_reflns_theta_min         3.35
_exptl_absorpt_coefficient_mu    1.506
_exptl_absorpt_correction_T_max  0.832
_exptl_absorpt_correction_T_min  0.658
_exptl_absorpt_correction_type   analytical
_exptl_absorpt_process_details
;
Oxford Diffraion software, CrystAlis 1.171
;
_exptl_crystal_colour            brown
_exptl_crystal_density_diffrn    1.412
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             568
_exptl_crystal_size_max          0.324
_exptl_crystal_size_mid          0.207
_exptl_crystal_size_min          0.098
_refine_diff_density_max         0.613
_refine_diff_density_min         -0.463
_refine_diff_density_rms         0.094
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.222
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     154
_refine_ls_number_reflns         2761
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.222
_refine_ls_R_factor_all          0.0507
_refine_ls_R_factor_gt           0.0400
_refine_ls_shift/su_max          0.025
_refine_ls_shift/su_mean         0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0085P)²+4.0339P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1005
_refine_ls_wR_factor_ref         0.1026
_reflns_number_gt                2296
_reflns_number_total             2761
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om060423vsi20060516_101700.cif
_cod_data_source_block           compond_6
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      'P 21/c'
_cod_database_code               4074124
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ni1 Ni 0.34186(3) 0.47973(5) 0.05580(4) 0.01337(13) Uani 1 1 d .
C11 C 0.2617(2) 0.7005(4) -0.0532(3) 0.0158(7) Uani 1 1 d .
C12 C 0.2767(2) 0.5788(5) -0.1457(3) 0.0183(7) Uani 1 1 d .
H12A H 0.2317 0.5150 -0.2160 0.022 Uiso 1 1 calc R
C13 C 0.3660(2) 0.5663(5) -0.1238(3) 0.0175(7) Uani 1 1 d .
H13A H 0.3944 0.4962 -0.1779 0.021 Uiso 1 1 calc R
C14 C 0.4075(2) 0.6804(5) -0.0169(3) 0.0173(7) Uani 1 1 d .
H14A H 0.4700 0.7059 0.0166 0.021 Uiso 1 1 calc R
C15 C 0.3431(2) 0.7618(4) 0.0270(3) 0.0161(7) Uani 1 1 d .
H15A H 0.3531 0.8523 0.0985 0.019 Uiso 1 1 calc R
C16 C 0.1763(2) 0.7566(5) -0.0411(4) 0.0194(8) Uani 1 1 d .
H16A H 0.1752 0.8864 -0.0360 0.023 Uiso 1 1 calc R
H16B H 0.1710 0.7098 0.0431 0.023 Uiso 1 1 calc R
C17 C 0.0995(2) 0.6963(5) -0.1547(4) 0.0222(8) Uani 1 1 d .
H17A H 0.1037 0.7446 -0.2392 0.027 Uiso 1 1 calc R
H17B H 0.1001 0.5667 -0.1607 0.027 Uiso 1 1 calc R
C18 C 0.0166(2) 0.7545(5) -0.1362(4) 0.0221(8) Uani 1 1 d .
H18A H 0.0074 0.8770 -0.1309 0.027 Uiso 1 1 calc R
C19 C -0.0442(2) 0.6470(5) -0.1267(4) 0.0215(8) Uani 1 1 d .
H19A H -0.0349 0.5250 -0.1350 0.026 Uiso 1 1 calc R
C20 C -0.1265(2) 0.6988(5) -0.1039(4) 0.0238(8) Uani 1 1 d .
H20A H -0.1296 0.8283 -0.0996 0.029 Uiso 1 1 calc R
H20B H -0.1278 0.6509 -0.0177 0.029 Uiso 1 1 calc R
C21 C -0.2039(2) 0.6307(5) -0.2145(4) 0.0192(8) Uani 1 1 d .
H21A H -0.2048 0.6874 -0.2989 0.023 Uiso 1 1 calc R
H21B H -0.1970 0.5029 -0.2245 0.023 Uiso 1 1 calc R
C22 C -0.2882(2) 0.6625(5) -0.1921(3) 0.0170(7) Uani 1 1 d .
C23 C -0.3065(2) 0.7823(4) -0.1014(3) 0.0170(7) Uani 1 1 d .
H23A H -0.2660 0.8533 -0.0390 0.020 Uiso 1 1 calc R
C24 C -0.3958(2) 0.7778(5) -0.1200(3) 0.0184(7) Uani 1 1 d .
H24A H -0.4251 0.8457 -0.0727 0.022 Uiso 1 1 calc R
C25 C -0.4331(2) 0.6549(5) -0.2209(4) 0.0203(8) Uani 1 1 d .
H25A H -0.4919 0.6251 -0.2531 0.024 Uiso 1 1 calc R
C26 C -0.3673(2) 0.5837(5) -0.2657(3) 0.0184(7) Uani 1 1 d .
H26A H -0.3747 0.4979 -0.3334 0.022 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C14 Ni1 C13 38.54(13) . .
C14 Ni1 C15 38.56(13) . .
C13 Ni1 C15 64.06(13) . .
C14 Ni1 C24 123.46(14) . 3_565
C13 Ni1 C24 112.40(14) . 3_565
C15 Ni1 C24 156.38(14) . 3_565
C14 Ni1 C23 158.70(13) . 3_565
C13 Ni1 C23 127.57(13) . 3_565
C15 Ni1 C23 162.57(13) . 3_565
C24 Ni1 C23 38.22(14) 3_565 3_565
C14 Ni1 C25 108.89(14) . 3_565
C13 Ni1 C25 125.47(14) . 3_565
C15 Ni1 C25 123.01(14) . 3_565
C24 Ni1 C25 37.83(13) 3_565 3_565
C23 Ni1 C25 63.61(14) 3_565 3_565
C14 Ni1 C26 124.26(14) . 3_565
C13 Ni1 C26 158.82(14) . 3_565
C15 Ni1 C26 110.77(13) . 3_565
C24 Ni1 C26 63.34(14) 3_565 3_565
C23 Ni1 C26 63.34(13) 3_565 3_565
C25 Ni1 C26 37.97(14) 3_565 3_565
C14 Ni1 C22 159.36(13) . 3_565
C13 Ni1 C22 161.58(13) . 3_565
C15 Ni1 C22 127.07(13) . 3_565
C24 Ni1 C22 63.84(13) 3_565 3_565
C23 Ni1 C22 38.01(13) 3_565 3_565
C25 Ni1 C22 63.83(14) 3_565 3_565
C26 Ni1 C22 38.01(13) 3_565 3_565
C14 Ni1 C12 63.73(14) . .
C13 Ni1 C12 37.92(13) . .
C15 Ni1 C12 63.13(13) . .
C24 Ni1 C12 129.87(13) 3_565 .
C23 Ni1 C12 116.46(14) 3_565 .
C25 Ni1 C12 161.24(14) 3_565 .
C26 Ni1 C12 160.63(14) 3_565 .
C22 Ni1 C12 129.08(14) 3_565 .
C14 Ni1 C11 63.93(13) . .
C13 Ni1 C11 63.58(13) . .
C15 Ni1 C11 37.79(13) . .
C24 Ni1 C11 164.31(13) 3_565 .
C23 Ni1 C11 130.63(13) 3_565 .
C25 Ni1 C11 157.37(13) 3_565 .
C26 Ni1 C11 126.20(13) 3_565 .
C22 Ni1 C11 114.69(13) 3_565 .
C12 Ni1 C11 37.51(13) . .
C12 C11 C15 107.0(3) . .
C12 C11 C16 127.3(3) . .
C15 C11 C16 125.8(3) . .
C12 C11 Ni1 70.4(2) . .
C15 C11 Ni1 68.97(19) . .
C16 C11 Ni1 125.9(2) . .
C13 C12 C11 108.9(3) . .
C13 C12 Ni1 69.5(2) . .
C11 C12 Ni1 72.1(2) . .
C13 C12 H12A 125.6 . .
C11 C12 H12A 125.6 . .
Ni1 C12 H12A 125.6 . .
C12 C13 C14 107.9(3) . .
C12 C13 Ni1 72.6(2) . .
C14 C13 Ni1 70.10(19) . .
C12 C13 H13A 126.0 . .
C14 C13 H13A 126.0 . .
Ni1 C13 H13A 126.0 . .
C13 C14 C15 107.6(3) . .
C13 C14 Ni1 71.4(2) . .
C15 C14 Ni1 71.6(2) . .
C13 C14 H14A 126.1 . .
C15 C14 H14A 126.1 . .
Ni1 C14 H14A 126.1 . .
C11 C15 C14 108.7(3) . .
C11 C15 Ni1 73.2(2) . .
C14 C15 Ni1 69.85(19) . .
C11 C15 H15A 125.6 . .
C14 C15 H15A 125.6 . .
Ni1 C15 H15A 125.6 . .
C11 C16 C17 114.5(3) . .
C11 C16 H16A 108.6 . .
C17 C16 H16A 108.6 . .
C11 C16 H16B 108.6 . .
C17 C16 H16B 108.6 . .
H16A C16 H16B 107.6 . .
C18 C17 C16 111.9(3) . .
C18 C17 H17A 109.2 . .
C16 C17 H17A 109.2 . .
C18 C17 H17B 109.2 . .
C16 C17 H17B 109.2 . .
H17A C17 H17B 107.9 . .
C19 C18 C17 124.6(4) . .
C19 C18 H18A 117.7 . .
C17 C18 H18A 117.7 . .
C18 C19 C20 126.4(4) . .
C18 C19 H19A 116.8 . .
C20 C19 H19A 116.8 . .
C19 C20 C21 111.6(3) . .
C19 C20 H20A 109.3 . .
C21 C20 H20A 109.3 . .
C19 C20 H20B 109.3 . .
C21 C20 H20B 109.3 . .
H20A C20 H20B 108.0 . .
C22 C21 C20 114.7(3) . .
C22 C21 H21A 108.6 . .
C20 C21 H21A 108.6 . .
C22 C21 H21B 108.6 . .
C20 C21 H21B 108.6 . .
H21A C21 H21B 107.6 . .
C23 C22 C26 106.8(3) . .
C23 C22 C21 127.6(3) . .
C26 C22 C21 125.5(3) . .
C23 C22 Ni1 70.1(2) . 3_565
C26 C22 Ni1 70.5(2) . 3_565
C21 C22 Ni1 127.3(2) . 3_565
C24 C23 C22 108.5(3) . .
C24 C23 Ni1 70.8(2) . 3_565
C22 C23 Ni1 71.9(2) . 3_565
C24 C23 H23A 125.7 . .
C22 C23 H23A 125.7 . .
Ni1 C23 H23A 123.1 3_565 .
C25 C24 C23 108.1(3) . .
C25 C24 Ni1 71.2(2) . 3_565
C23 C24 Ni1 70.9(2) . 3_565
C25 C24 H24A 126.0 . .
C23 C24 H24A 126.0 . .
Ni1 C24 H24A 123.5 3_565 .
C24 C25 C26 107.9(3) . .
C24 C25 Ni1 70.9(2) . 3_565
C26 C25 Ni1 71.3(2) . 3_565
C24 C25 H25A 126.0 . .
C26 C25 H25A 126.0 . .
Ni1 C25 H25A 123.4 3_565 .
C25 C26 C22 108.7(3) . .
C25 C26 Ni1 70.7(2) . 3_565
C22 C26 Ni1 71.5(2) . 3_565
C25 C26 H26A 125.7 . .
C22 C26 H26A 125.7 . .
Ni1 C26 H26A 123.8 3_565 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ni1 C14 2.149(4) .
Ni1 C13 2.165(3) .
Ni1 C15 2.171(4) .
Ni1 C24 2.174(4) 3_565
Ni1 C23 2.175(4) 3_565
Ni1 C25 2.178(4) 3_565
Ni1 C26 2.187(4) 3_565
Ni1 C22 2.199(3) 3_565
Ni1 C12 2.205(4) .
Ni1 C11 2.227(4) .
C11 C12 1.425(5) .
C11 C15 1.425(5) .
C11 C16 1.515(5) .
C12 C13 1.421(5) .
C12 H12A 1.0000 .
C13 C14 1.424(5) .
C13 H13A 1.0000 .
C14 C15 1.427(5) .
C14 H14A 1.0000 .
C15 H15A 1.0000 .
C16 C17 1.523(5) .
C16 H16A 0.9900 .
C16 H16B 0.9900 .
C17 C18 1.506(5) .
C17 H17A 0.9900 .
C17 H17B 0.9900 .
C18 C19 1.323(5) .
C18 H18A 0.9500 .
C19 C20 1.503(5) .
C19 H19A 0.9500 .
C20 C21 1.531(5) .
C20 H20A 0.9900 .
C20 H20B 0.9900 .
C21 C22 1.499(5) .
C21 H21A 0.9900 .
C21 H21B 0.9900 .
C22 C23 1.425(5) .
C22 C26 1.428(5) .
C22 Ni1 2.199(3) 3_565
C23 C24 1.424(5) .
C23 Ni1 2.175(4) 3_565
C23 H23A 0.9500 .
C24 C25 1.411(5) .
C24 Ni1 2.174(4) 3_565
C24 H24A 0.9500 .
C25 C26 1.420(5) .
C25 Ni1 2.178(4) 3_565
C25 H25A 0.9500 .
C26 Ni1 2.187(4) 3_565
C26 H26A 0.9500 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C14 Ni1 C11 C12 80.1(2) . .
C13 Ni1 C11 C12 36.9(2) . .
C15 Ni1 C11 C12 117.9(3) . .
C24 Ni1 C11 C12 -41.8(6) 3_565 .
C23 Ni1 C11 C12 -81.1(3) 3_565 .
C25 Ni1 C11 C12 156.4(3) 3_565 .
C26 Ni1 C11 C12 -165.1(2) 3_565 .
C22 Ni1 C11 C12 -122.7(2) 3_565 .
C14 Ni1 C11 C15 -37.8(2) . .
C13 Ni1 C11 C15 -81.0(2) . .
C24 Ni1 C11 C15 -159.7(4) 3_565 .
C23 Ni1 C11 C15 160.9(2) 3_565 .
C25 Ni1 C11 C15 38.5(4) 3_565 .
C26 Ni1 C11 C15 76.9(2) 3_565 .
C22 Ni1 C11 C15 119.3(2) 3_565 .
C12 Ni1 C11 C15 -117.9(3) . .
C14 Ni1 C11 C16 -157.5(3) . .
C13 Ni1 C11 C16 159.3(3) . .
C15 Ni1 C11 C16 -119.6(4) . .
C24 Ni1 C11 C16 80.6(6) 3_565 .
C23 Ni1 C11 C16 41.3(4) 3_565 .
C25 Ni1 C11 C16 -81.2(5) 3_565 .
C26 Ni1 C11 C16 -42.7(3) 3_565 .
C22 Ni1 C11 C16 -0.3(3) 3_565 .
C12 Ni1 C11 C16 122.4(4) . .
C15 C11 C12 C13 -0.5(4) . .
C16 C11 C12 C13 179.2(3) . .
Ni1 C11 C12 C13 -60.1(2) . .
C15 C11 C12 Ni1 59.5(2) . .
C16 C11 C12 Ni1 -120.8(4) . .
C14 Ni1 C12 C13 38.2(2) . .
C15 Ni1 C12 C13 81.5(2) . .
C24 Ni1 C12 C13 -74.7(3) 3_565 .
C23 Ni1 C12 C13 -118.0(2) 3_565 .
C25 Ni1 C12 C13 -32.5(5) 3_565 .
C26 Ni1 C12 C13 157.5(4) 3_565 .
C22 Ni1 C12 C13 -161.1(2) 3_565 .
C11 Ni1 C12 C13 118.9(3) . .
C14 Ni1 C12 C11 -80.7(2) . .
C13 Ni1 C12 C11 -118.9(3) . .
C15 Ni1 C12 C11 -37.4(2) . .
C24 Ni1 C12 C11 166.4(2) 3_565 .
C23 Ni1 C12 C11 123.1(2) 3_565 .
C25 Ni1 C12 C11 -151.4(4) 3_565 .
C26 Ni1 C12 C11 38.6(5) 3_565 .
C22 Ni1 C12 C11 80.0(2) 3_565 .
C11 C12 C13 C14 0.1(4) . .
Ni1 C12 C13 C14 -61.6(2) . .
C11 C12 C13 Ni1 61.7(2) . .
C14 Ni1 C13 C12 -117.1(3) . .
C15 Ni1 C13 C12 -78.8(2) . .
C24 Ni1 C13 C12 126.8(2) 3_565 .
C23 Ni1 C13 C12 85.8(2) 3_565 .
C25 Ni1 C13 C12 167.8(2) 3_565 .
C26 Ni1 C13 C12 -159.4(3) 3_565 .
C22 Ni1 C13 C12 52.6(5) 3_565 .
C11 Ni1 C13 C12 -36.5(2) . .
C15 Ni1 C13 C14 38.3(2) . .
C24 Ni1 C13 C14 -116.1(2) 3_565 .
C23 Ni1 C13 C14 -157.1(2) 3_565 .
C25 Ni1 C13 C14 -75.1(2) 3_565 .
C26 Ni1 C13 C14 -42.3(5) 3_565 .
C22 Ni1 C13 C14 169.7(4) 3_565 .
C12 Ni1 C13 C14 117.1(3) . .
C11 Ni1 C13 C14 80.6(2) . .
C12 C13 C14 C15 0.3(4) . .
Ni1 C13 C14 C15 -62.8(2) . .
C12 C13 C14 Ni1 63.2(2) . .
C15 Ni1 C14 C13 -116.7(3) . .
C24 Ni1 C14 C13 84.5(2) 3_565 .
C23 Ni1 C14 C13 58.3(4) 3_565 .
C25 Ni1 C14 C13 123.7(2) 3_565 .
C26 Ni1 C14 C13 162.9(2) 3_565 .
C22 Ni1 C14 C13 -170.8(3) 3_565 .
C12 Ni1 C14 C13 -37.6(2) . .
C11 Ni1 C14 C13 -79.6(2) . .
C13 Ni1 C14 C15 116.7(3) . .
C24 Ni1 C14 C15 -158.88(19) 3_565 .
C23 Ni1 C14 C15 174.9(3) 3_565 .
C25 Ni1 C14 C15 -119.6(2) 3_565 .
C26 Ni1 C14 C15 -80.4(2) 3_565 .
C22 Ni1 C14 C15 -54.1(5) 3_565 .
C12 Ni1 C14 C15 79.1(2) . .
C11 Ni1 C14 C15 37.1(2) . .
C12 C11 C15 C14 0.7(4) . .
C16 C11 C15 C14 -179.0(3) . .
Ni1 C11 C15 C14 61.2(2) . .
C12 C11 C15 Ni1 -60.5(2) . .
C16 C11 C15 Ni1 119.8(3) . .
C13 C14 C15 C11 -0.7(4) . .
Ni1 C14 C15 C11 -63.3(2) . .
C13 C14 C15 Ni1 62.7(2) . .
C14 Ni1 C15 C11 117.9(3) . .
C13 Ni1 C15 C11 79.6(2) . .
C24 Ni1 C15 C11 166.5(3) 3_565 .
C23 Ni1 C15 C11 -56.0(5) 3_565 .
C25 Ni1 C15 C11 -163.4(2) 3_565 .
C26 Ni1 C15 C11 -122.8(2) 3_565 .
C22 Ni1 C15 C11 -83.1(2) 3_565 .
C12 Ni1 C15 C11 37.1(2) . .
C13 Ni1 C15 C14 -38.3(2) . .
C24 Ni1 C15 C14 48.6(4) 3_565 .
C23 Ni1 C15 C14 -173.8(4) 3_565 .
C25 Ni1 C15 C14 78.7(2) 3_565 .
C26 Ni1 C15 C14 119.3(2) 3_565 .
C22 Ni1 C15 C14 159.0(2) 3_565 .
C12 Ni1 C15 C14 -80.8(2) . .
C11 Ni1 C15 C14 -117.9(3) . .
C12 C11 C16 C17 -10.2(5) . .
C15 C11 C16 C17 169.4(3) . .
Ni1 C11 C16 C17 -102.0(3) . .
C11 C16 C17 C18 179.4(3) . .
C16 C17 C18 C19 -119.7(4) . .
C17 C18 C19 C20 178.0(3) . .
C18 C19 C20 C21 122.7(4) . .
C19 C20 C21 C22 174.5(3) . .
C20 C21 C22 C23 17.0(5) . .
C20 C21 C22 C26 -167.2(3) . .
C20 C21 C22 Ni1 -75.6(4) . 3_565
C26 C22 C23 C24 -0.4(4) . .
C21 C22 C23 C24 176.0(3) . .
Ni1 C22 C23 C24 -61.7(2) 3_565 .
C26 C22 C23 Ni1 61.3(2) . 3_565
C21 C22 C23 Ni1 -122.3(4) . 3_565
C22 C23 C24 C25 0.5(4) . .
Ni1 C23 C24 C25 -61.9(2) 3_565 .
C22 C23 C24 Ni1 62.4(2) . 3_565
C23 C24 C25 C26 -0.4(4) . .
Ni1 C24 C25 C26 -62.1(2) 3_565 .
C23 C24 C25 Ni1 61.7(2) . 3_565
C24 C25 C26 C22 0.1(4) . .
Ni1 C25 C26 C22 -61.7(2) 3_565 .
C24 C25 C26 Ni1 61.8(2) . 3_565
C23 C22 C26 C25 0.2(4) . .
C21 C22 C26 C25 -176.3(3) . .
Ni1 C22 C26 C25 61.2(2) 3_565 .
C23 C22 C26 Ni1 -61.0(2) . 3_565
C21 C22 C26 Ni1 122.5(3) . 3_565
