#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/46/4074617.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4074617
loop_
_publ_author_name
'Yin, Gang-Qiang'
'Wei, Qiao-Hua'
'Zhang, Li-Yi'
'Chen, Zhong-Ning'
_publ_section_title
;
 Luminescent PtII−MI(M = Cu, Ag, Au) Heteronuclear Alkynyl
 Complexes Prepared by Reaction of [Pt(C⋮CR)4]2-with
 [M2(dppm)2]2+(dppm = Bis(diphenylphosphino)methane)
;
_journal_issue                   3
_journal_name_full               Organometallics
_journal_page_first              580
_journal_paper_doi               10.1021/om050620e
_journal_volume                  25
_journal_year                    2006
_chemical_formula_sum            'C33 H36 Cl2 Cu F6 N P2 Pt0.5 Sb Si'
_chemical_formula_weight         1004.39
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 104.5260(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   14.9699(4)
_cell_length_b                   15.0645(4)
_cell_length_c                   18.2548(4)
_cell_measurement_reflns_used    6678
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      25.19
_cell_measurement_theta_min      1.78
_cell_volume                     3985.12(17)
_computing_cell_refinement       'Siemens SMART & SAINT'
_computing_data_collection       'Siemens SMART'
_computing_data_reduction        'Siemens XPREP'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'Siemens SHELXTL'
_computing_structure_solution    'Siemens SHELXTL'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.985
_diffrn_measured_fraction_theta_max 0.985
_diffrn_measurement_device_type  'Siemens SMART CCD'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0329
_diffrn_reflns_av_sigmaI/netI    0.0441
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -8
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            13190
_diffrn_reflns_theta_full        25.19
_diffrn_reflns_theta_max         25.19
_diffrn_reflns_theta_min         1.78
_diffrn_standards_decay_%        none
_diffrn_standards_interval_count none
_diffrn_standards_interval_time  none
_diffrn_standards_number         none
_exptl_absorpt_coefficient_mu    3.254
_exptl_absorpt_correction_T_max  1.0000
_exptl_absorpt_correction_T_min  .5547
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   'SADABS (Sheldrick, 1996)'
_exptl_crystal_colour            'pale yellow'
_exptl_crystal_density_diffrn    1.674
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1968
_exptl_crystal_size_max          .56
_exptl_crystal_size_mid          .50
_exptl_crystal_size_min          .40
_refine_diff_density_max         1.444
_refine_diff_density_min         -2.590
_refine_diff_density_rms         0.161
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.167
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     421
_refine_ls_number_reflns         7056
_refine_ls_number_restraints     6
_refine_ls_restrained_S_all      1.167
_refine_ls_R_factor_all          0.1001
_refine_ls_R_factor_gt           0.0701
_refine_ls_shift/su_max          0.076
_refine_ls_shift/su_mean         0.002
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0651P)²+38.5007P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1701
_refine_ls_wR_factor_ref         0.1962
_reflns_number_gt                5346
_reflns_number_total             7056
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om050620esi20051124_094200.cif
_cod_data_source_block           Compoumd_12
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      P2(1)/c
_cod_original_formula_sum        'C33 H36 Cl2 Cu F6 N P2 Pt0.50 Sb Si'
_cod_database_code               4074617
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt Pt 0.0000 0.0000 0.5000 0.04016(18) Uani 1 2 d S . .
Cu Cu 0.19366(10) 0.02259(10) 0.65037(9) 0.0624(4) Uani 1 1 d . . .
Sb Sb 0.66996(11) 0.55929(10) 0.26921(9) 0.1271(6) Uani 1 1 d . . .
P1 P 0.0748(2) 0.04234(19) 0.70397(16) 0.0495(7) Uani 1 1 d . . .
P2 P -0.01906(19) -0.09833(17) 0.59173(14) 0.0432(6) Uani 1 1 d . . .
Si Si 0.3378(3) -0.0487(3) 0.5408(3) 0.0778(11) Uani 1 1 d . . .
F1 F 0.7781(9) 0.5259(11) 0.2471(11) 0.189(7) Uani 1 1 d . . .
F2 F 0.5654(16) 0.5903(19) 0.2899(13) 0.300(13) Uani 1 1 d . . .
F3 F 0.7179(17) 0.5342(13) 0.3623(8) 0.246(10) Uani 1 1 d . . .
F4 F 0.6304(12) 0.4488(11) 0.2522(10) 0.209(7) Uani 1 1 d . . .
F5 F 0.7146(15) 0.6712(10) 0.2826(12) 0.244(9) Uani 1 1 d . . .
F6 F 0.6196(11) 0.5877(13) 0.1692(8) 0.214(8) Uani 1 1 d . . .
N1 N 0.3092(9) 0.0724(11) 0.7113(8) 0.100(4) Uani 1 1 d . . .
C1 C -0.0210(8) -0.0382(7) 0.6773(6) 0.051(3) Uani 1 1 d . . .
H1A H -0.0168 -0.0802 0.7183 0.061 Uiso 1 1 calc R . .
H1B H -0.0792 -0.0069 0.6698 0.061 Uiso 1 1 calc R . .
C11 C 0.1368(7) -0.0143(7) 0.5358(6) 0.048(2) Uani 1 1 d . . .
C12 C 0.2206(8) -0.0233(8) 0.5512(7) 0.058(3) Uani 1 1 d . . .
C13 C 0.4077(12) 0.0531(13) 0.5497(12) 0.115(6) Uani 1 1 d . . .
H13A H 0.3788 0.0944 0.5109 0.173 Uiso 1 1 calc R . .
H13B H 0.4683 0.0387 0.5443 0.173 Uiso 1 1 calc R . .
H13C H 0.4126 0.0793 0.5985 0.173 Uiso 1 1 calc R . .
C14 C 0.3895(12) -0.1321(14) 0.6127(14) 0.148(9) Uani 1 1 d . . .
H14A H 0.3978 -0.1068 0.6623 0.222 Uiso 1 1 calc R . .
H14B H 0.4482 -0.1503 0.6057 0.222 Uiso 1 1 calc R . .
H14C H 0.3494 -0.1826 0.6078 0.222 Uiso 1 1 calc R . .
C15 C 0.3220(12) -0.0964(16) 0.4460(11) 0.135(8) Uani 1 1 d . . .
H15A H 0.2954 -0.0527 0.4086 0.202 Uiso 1 1 calc R . .
H15B H 0.2816 -0.1468 0.4407 0.202 Uiso 1 1 calc R . .
H15C H 0.3807 -0.1148 0.4390 0.202 Uiso 1 1 calc R . .
C16 C 0.3721(13) 0.1115(14) 0.7430(12) 0.113(6) Uani 1 1 d . . .
C17 C 0.4529(13) 0.1630(18) 0.7826(15) 0.181(12) Uani 1 1 d . . .
H17A H 0.4875 0.1808 0.7472 0.272 Uiso 1 1 calc R . .
H17B H 0.4912 0.1272 0.8216 0.272 Uiso 1 1 calc R . .
H17C H 0.4330 0.2148 0.8047 0.272 Uiso 1 1 calc R . .
C21 C 0.0254(8) 0.1508(7) 0.6755(6) 0.053(3) Uani 1 1 d . . .
C22 C -0.0654(10) 0.1690(9) 0.6471(7) 0.072(4) Uani 1 1 d . . .
H22A H -0.1084 0.1234 0.6421 0.086 Uiso 1 1 calc R . .
C23 C -0.0954(12) 0.2549(10) 0.6250(9) 0.087(4) Uani 1 1 d . . .
H23A H -0.1580 0.2662 0.6064 0.105 Uiso 1 1 calc R . .
C24 C -0.0340(13) 0.3212(9) 0.6306(7) 0.079(4) Uani 1 1 d . . .
H24A H -0.0544 0.3781 0.6149 0.095 Uiso 1 1 calc R . .
C25 C 0.0565(13) 0.3060(8) 0.6588(8) 0.078(4) Uani 1 1 d . . .
H25A H 0.0985 0.3524 0.6630 0.094 Uiso 1 1 calc R . .
C26 C 0.0878(10) 0.2200(8) 0.6821(7) 0.068(3) Uani 1 1 d . . .
H26A H 0.1504 0.2096 0.7020 0.081 Uiso 1 1 calc R . .
C31 C 0.0964(9) 0.0439(7) 0.8063(6) 0.057(3) Uani 1 1 d . . .
C32 C 0.1782(11) 0.0103(10) 0.8493(8) 0.083(4) Uani 1 1 d . . .
H32A H 0.2217 -0.0113 0.8253 0.099 Uiso 1 1 calc R . .
C33 C 0.1973(14) 0.0078(12) 0.9274(9) 0.100(6) Uani 1 1 d . . .
H33A H 0.2541 -0.0128 0.9557 0.120 Uiso 1 1 calc R . .
C34 C 0.1315(17) 0.0360(11) 0.9624(8) 0.106(7) Uani 1 1 d . . .
H34A H 0.1423 0.0326 1.0148 0.128 Uiso 1 1 calc R . .
C35 C 0.0519(16) 0.0684(10) 0.9209(9) 0.103(6) Uani 1 1 d . . .
H35A H 0.0078 0.0883 0.9451 0.124 Uiso 1 1 calc R . .
C36 C 0.0332(12) 0.0731(9) 0.8427(8) 0.086(5) Uani 1 1 d . . .
H36A H -0.0227 0.0963 0.8151 0.103 Uiso 1 1 calc R . .
C41 C 0.0728(8) -0.1802(7) 0.6193(7) 0.057(3) Uani 1 1 d . . .
C42 C 0.0962(11) -0.2276(9) 0.5627(8) 0.084(4) Uani 1 1 d . . .
H42A H 0.0664 -0.2165 0.5124 0.101 Uiso 1 1 calc R . .
C43 C 0.1629(14) -0.2908(11) 0.5801(13) 0.112(6) Uani 1 1 d . . .
H43A H 0.1760 -0.3238 0.5410 0.134 Uiso 1 1 calc R . .
C44 C 0.2100(14) -0.3072(13) 0.6505(15) 0.117(7) Uani 1 1 d . . .
H44A H 0.2577 -0.3484 0.6604 0.140 Uiso 1 1 calc R . .
C45 C 0.1873(13) -0.2630(14) 0.7074(12) 0.122(7) Uani 1 1 d . . .
H45A H 0.2176 -0.2760 0.7572 0.147 Uiso 1 1 calc R . .
C46 C 0.1187(11) -0.1977(11) 0.6921(9) 0.093(5) Uani 1 1 d . . .
H46A H 0.1046 -0.1663 0.7317 0.112 Uiso 1 1 calc R . .
C51 C -0.1221(8) -0.1646(7) 0.5689(6) 0.054(3) Uani 1 1 d . . .
C52 C -0.1513(10) -0.2023(9) 0.4981(7) 0.073(4) Uani 1 1 d . . .
H52A H -0.1178 -0.1910 0.4625 0.087 Uiso 1 1 calc R . .
C53 C -0.2266(11) -0.2550(9) 0.4782(10) 0.088(5) Uani 1 1 d . . .
H53A H -0.2445 -0.2797 0.4301 0.105 Uiso 1 1 calc R . .
C54 C -0.2759(12) -0.2713(11) 0.5303(13) 0.105(6) Uani 1 1 d . . .
H54A H -0.3277 -0.3077 0.5174 0.127 Uiso 1 1 calc R . .
C55 C -0.2514(13) -0.2359(13) 0.5990(12) 0.111(6) Uani 1 1 d . . .
H55A H -0.2868 -0.2473 0.6332 0.134 Uiso 1 1 calc R . .
C56 C -0.1738(11) -0.1824(10) 0.6209(9) 0.090(5) Uani 1 1 d . . .
H56A H -0.1567 -0.1587 0.6694 0.108 Uiso 1 1 calc R . .
Cl1 Cl 0.633(2) 0.353(3) 0.642(2) 0.424(15) Uiso 0.48(2) 1 d PD A 1
Cl2 Cl 0.515(3) 0.431(3) 0.5107(19) 0.424(15) Uiso 0.48(2) 1 d PD . 1
Cl1' Cl 0.597(3) 0.295(3) 0.6568(18) 0.424(15) Uiso 0.52 1 d PD A 2
Cl2' Cl 0.567(3) 0.343(3) 0.5047(18) 0.424(15) Uiso 0.52 1 d PD A 2
C01 C 0.5195(18) 0.352(3) 0.5834(19) 0.40(3) Uiso 1 1 d D . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C11 Pt C11 180.000(1) . 3_556
C11 Pt P2 90.2(3) . 3_556
C11 Pt P2 89.8(3) 3_556 3_556
C11 Pt P2 89.8(3) . .
C11 Pt P2 90.2(3) 3_556 .
P2 Pt P2 180.0 3_556 .
N1 Cu C12 106.7(5) . .
N1 Cu C11 137.6(5) . .
C12 Cu C11 33.9(4) . .
N1 Cu P1 112.6(4) . .
C12 Cu P1 140.5(3) . .
C11 Cu P1 107.2(3) . .
F3 Sb F2 91.1(11) . .
F3 Sb F4 90.3(9) . .
F2 Sb F4 90.7(12) . .
F3 Sb F5 91.3(10) . .
F2 Sb F5 92.4(12) . .
F4 Sb F5 176.5(10) . .
F3 Sb F1 89.1(10) . .
F2 Sb F1 179.4(12) . .
F4 Sb F1 88.7(8) . .
F5 Sb F1 88.2(9) . .
F3 Sb F6 179.1(10) . .
F2 Sb F6 89.2(9) . .
F4 Sb F6 90.5(9) . .
F5 Sb F6 87.8(9) . .
F1 Sb F6 90.6(8) . .
C31 P1 C21 103.7(5) . .
C31 P1 C1 101.9(5) . .
C21 P1 C1 106.4(5) . .
C31 P1 Cu 119.5(4) . .
C21 P1 Cu 107.7(4) . .
C1 P1 Cu 116.3(3) . .
C51 P2 C1 106.2(5) . .
C51 P2 C41 103.5(5) . .
C1 P2 C41 105.9(5) . .
C51 P2 Pt 116.4(4) . .
C1 P2 Pt 109.7(4) . .
C41 P2 Pt 114.4(4) . .
C15 Si C14 109.8(11) . .
C15 Si C13 110.2(9) . .
C14 Si C13 112.2(10) . .
C15 Si C12 106.1(7) . .
C14 Si C12 107.9(8) . .
C13 Si C12 110.6(7) . .
C16 N1 Cu 171.4(18) . .
P2 C1 P1 112.1(6) . .
P2 C1 H1A 109.2 . .
P1 C1 H1A 109.2 . .
P2 C1 H1B 109.2 . .
P1 C1 H1B 109.2 . .
H1A C1 H1B 107.9 . .
C12 C11 Pt 174.3(10) . .
C12 C11 Cu 70.6(7) . .
Pt C11 Cu 114.8(5) . .
C11 C12 Si 160.7(11) . .
C11 C12 Cu 75.5(8) . .
Si C12 Cu 123.8(6) . .
Si C13 H13A 109.5 . .
Si C13 H13B 109.5 . .
H13A C13 H13B 109.5 . .
Si C13 H13C 109.5 . .
H13A C13 H13C 109.5 . .
H13B C13 H13C 109.5 . .
Si C14 H14A 109.5 . .
Si C14 H14B 109.5 . .
H14A C14 H14B 109.5 . .
Si C14 H14C 109.5 . .
H14A C14 H14C 109.5 . .
H14B C14 H14C 109.5 . .
Si C15 H15A 109.5 . .
Si C15 H15B 109.5 . .
H15A C15 H15B 109.5 . .
Si C15 H15C 109.5 . .
H15A C15 H15C 109.5 . .
H15B C15 H15C 109.5 . .
N1 C16 C17 179(3) . .
C16 C17 H17A 109.5 . .
C16 C17 H17B 109.5 . .
H17A C17 H17B 109.5 . .
C16 C17 H17C 109.5 . .
H17A C17 H17C 109.5 . .
H17B C17 H17C 109.5 . .
C22 C21 C26 118.1(12) . .
C22 C21 P1 126.1(10) . .
C26 C21 P1 115.8(9) . .
C21 C22 C23 121.1(14) . .
C21 C22 H22A 119.5 . .
C23 C22 H22A 119.5 . .
C24 C23 C22 120.3(15) . .
C24 C23 H23A 119.9 . .
C22 C23 H23A 119.9 . .
C25 C24 C23 120.4(13) . .
C25 C24 H24A 119.8 . .
C23 C24 H24A 119.8 . .
C24 C25 C26 120.1(14) . .
C24 C25 H25A 120.0 . .
C26 C25 H25A 120.0 . .
C21 C26 C25 120.0(13) . .
C21 C26 H26A 120.0 . .
C25 C26 H26A 120.0 . .
C36 C31 C32 118.0(12) . .
C36 C31 P1 122.8(10) . .
C32 C31 P1 119.1(10) . .
C31 C32 C33 121.5(17) . .
C31 C32 H32A 119.2 . .
C33 C32 H32A 119.2 . .
C34 C33 C32 119.1(18) . .
C34 C33 H33A 120.5 . .
C32 C33 H33A 120.5 . .
C35 C34 C33 119.5(15) . .
C35 C34 H34A 120.2 . .
C33 C34 H34A 120.2 . .
C34 C35 C36 121.6(18) . .
C34 C35 H35A 119.2 . .
C36 C35 H35A 119.2 . .
C31 C36 C35 120.1(15) . .
C31 C36 H36A 119.9 . .
C35 C36 H36A 119.9 . .
C46 C41 C42 118.2(13) . .
C46 C41 P2 124.3(11) . .
C42 C41 P2 117.5(10) . .
C43 C42 C41 120.0(15) . .
C43 C42 H42A 120.0 . .
C41 C42 H42A 120.0 . .
C44 C43 C42 122.6(17) . .
C44 C43 H43A 118.7 . .
C42 C43 H43A 118.7 . .
C43 C44 C45 118.7(17) . .
C43 C44 H44A 120.6 . .
C45 C44 H44A 120.6 . .
C44 C45 C46 120.6(17) . .
C44 C45 H45A 119.7 . .
C46 C45 H45A 119.7 . .
C41 C46 C45 119.7(16) . .
C41 C46 H46A 120.1 . .
C45 C46 H46A 120.1 . .
C52 C51 C56 117.4(12) . .
C52 C51 P2 119.8(9) . .
C56 C51 P2 122.7(10) . .
C53 C52 C51 122.6(14) . .
C53 C52 H52A 118.7 . .
C51 C52 H52A 118.7 . .
C52 C53 C54 118.7(15) . .
C52 C53 H53A 120.7 . .
C54 C53 H53A 120.7 . .
C55 C54 C53 121.1(15) . .
C55 C54 H54A 119.4 . .
C53 C54 H54A 119.4 . .
C54 C55 C56 121.2(17) . .
C54 C55 H55A 119.4 . .
C56 C55 H55A 119.4 . .
C55 C56 C51 119.0(15) . .
C55 C56 H56A 120.5 . .
C51 C56 H56A 120.5 . .
C01 Cl2 Cl2 139(4) . 3_666
Cl2' C01 Cl1' 104.9(19) . .
Cl2' C01 Cl2 52.1(19) . .
Cl1' C01 Cl2 143(2) . .
Cl2' C01 Cl1 89(2) . .
Cl1' C01 Cl1 36(2) . .
Cl2 C01 Cl1 107.7(11) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pt C11 1.999(10) .
Pt C11 1.999(10) 3_556
Pt P2 2.306(2) 3_556
Pt P2 2.306(2) .
Cu N1 1.956(14) .
Cu C12 2.070(12) .
Cu C11 2.124(11) .
Cu P1 2.255(3) .
Sb F3 1.712(14) .
Sb F2 1.763(18) .
Sb F4 1.768(15) .
Sb F5 1.808(16) .
Sb F1 1.835(14) .
Sb F6 1.842(14) .
P1 C31 1.814(11) .
P1 C21 1.816(12) .
P1 C1 1.848(12) .
P2 C51 1.796(12) .
P2 C1 1.812(10) .
P2 C41 1.822(11) .
Si C15 1.833(17) .
Si C14 1.841(19) .
Si C13 1.841(17) .
Si C12 1.851(12) .
N1 C16 1.14(2) .
C1 H1A 0.9700 .
C1 H1B 0.9700 .
C11 C12 1.224(15) .
C13 H13A 0.9600 .
C13 H13B 0.9600 .
C13 H13C 0.9600 .
C14 H14A 0.9600 .
C14 H14B 0.9600 .
C14 H14C 0.9600 .
C15 H15A 0.9600 .
C15 H15B 0.9600 .
C15 H15C 0.9600 .
C16 C17 1.47(3) .
C17 H17A 0.9600 .
C17 H17B 0.9600 .
C17 H17C 0.9600 .
C21 C22 1.355(17) .
C21 C26 1.384(17) .
C22 C23 1.395(19) .
C22 H22A 0.9300 .
C23 C24 1.34(2) .
C23 H23A 0.9300 .
C24 C25 1.34(2) .
C24 H24A 0.9300 .
C25 C26 1.407(18) .
C25 H25A 0.9300 .
C26 H26A 0.9300 .
C31 C36 1.358(18) .
C31 C32 1.376(18) .
C32 C33 1.38(2) .
C32 H32A 0.9300 .
C33 C34 1.37(3) .
C33 H33A 0.9300 .
C34 C35 1.33(3) .
C34 H34A 0.9300 .
C35 C36 1.387(19) .
C35 H35A 0.9300 .
C36 H36A 0.9300 .
C41 C46 1.360(18) .
C41 C42 1.373(16) .
C42 C43 1.36(2) .
C42 H42A 0.9300 .
C43 C44 1.32(3) .
C43 H43A 0.9300 .
C44 C45 1.35(3) .
C44 H44A 0.9300 .
C45 C46 1.40(2) .
C45 H45A 0.9300 .
C46 H46A 0.9300 .
C51 C52 1.380(16) .
C51 C56 1.392(17) .
C52 C53 1.353(18) .
C52 H52A 0.9300 .
C53 C54 1.36(2) .
C53 H53A 0.9300 .
C54 C55 1.33(2) .
C54 H54A 0.9300 .
C55 C56 1.39(2) .
C55 H55A 0.9300 .
C56 H56A 0.9300 .
Cl1 C01 1.765(5) .
Cl2 C01 1.765(5) .
Cl2 Cl2 2.15(8) 3_666
Cl1' C01 1.764(5) .
Cl2' C01 1.764(5) .
