#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/55/4075551.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4075551
loop_
_publ_author_name
'Chiong, Hendrich A.'
'Daugulis, Olafs'
_publ_section_title
;
 Monomeric Silver(I) β-Diketiminate Complexes
;
_journal_issue                   17
_journal_name_full               Organometallics
_journal_page_first              4054
_journal_paper_doi               10.1021/om0603621
_journal_volume                  25
_journal_year                    2006
_chemical_formula_moiety         'C23 H11 N2 F18 Ag, 0.5 C6 H6'
_chemical_formula_sum            'C26 H14 Ag F18 N2'
_chemical_formula_weight         804.26
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           13
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yac'
_symmetry_space_group_name_H-M   'P 1 2/n 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 91.367(1)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   22.3715(13)
_cell_length_b                   10.3286(6)
_cell_length_c                   25.7565(15)
_cell_measurement_reflns_used    6713
_cell_measurement_temperature    223(2)
_cell_measurement_theta_max      23.56
_cell_measurement_theta_min      1.19
_cell_volume                     5949.8(6)
_computing_cell_refinement       'Bruker SAINT software (Bruker, 1999)'
_computing_data_collection       'Siemens SMART software (Siemens, 1996)'
_computing_data_reduction        'Bruker SAINT software (Bruker, 1999)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      223(2)
_diffrn_detector_area_resol_mean 1K
_diffrn_measured_fraction_theta_full 0.994
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Siemens SMART CCD'
_diffrn_measurement_method       CCD
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0365
_diffrn_reflns_av_sigmaI/netI    0.0201
_diffrn_reflns_limit_h_max       25
_diffrn_reflns_limit_h_min       -25
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_k_min       0
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_number            27577
_diffrn_reflns_theta_full        23.56
_diffrn_reflns_theta_max         23.56
_diffrn_reflns_theta_min         1.19
_diffrn_standards_decay_%        0.0
_exptl_absorpt_coefficient_mu    0.811
_exptl_absorpt_correction_T_max  0.9578
_exptl_absorpt_correction_T_min  0.7436
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            'Bright yellow'
_exptl_crystal_density_diffrn    1.796
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Block
_exptl_crystal_F_000             3144
_exptl_crystal_size_max          0.50
_exptl_crystal_size_mid          0.40
_exptl_crystal_size_min          0.20
_refine_diff_density_max         0.944
_refine_diff_density_min         -0.701
_refine_diff_density_rms         0.114
_refine_ls_extinction_coef       0.00019(6)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.147
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     653
_refine_ls_number_reflns         8829
_refine_ls_number_restraints     40
_refine_ls_restrained_S_all      1.148
_refine_ls_R_factor_all          0.0858
_refine_ls_R_factor_gt           0.0623
_refine_ls_shift/su_max          0.300
_refine_ls_shift/su_mean         0.032
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0421P)²+50.6251P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1416
_refine_ls_wR_factor_ref         0.1666
_reflns_number_gt                6598
_reflns_number_total             9392
_reflns_threshold_expression     >4sigma(I)
_cod_data_source_file            om0603621si20060425_100200.cif
_cod_data_source_block           k911
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.1 from
2010-06-29.

'_exptl_absorpt_correction_type' value 'Empirical'
changed to 'empirical' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      P2/n
_cod_original_formula_sum        'C26 H14 N2 F18 Ag'
_cod_database_code               4075551
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, y, -z+1/2'
'-x, -y, -z'
'x-1/2, -y, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ag1 Ag 0.75704(2) 0.63935(6) 0.61499(2) 0.04066(19) Uani 1 1 d . . .
Ag2 Ag 0.61892(3) 0.84808(6) 0.33475(2) 0.0438(2) Uani 1 1 d . . .
C6 C 0.5849(3) 0.4353(8) 0.6580(3) 0.042(2) Uiso 0.50 1 d PGD A 1
F1 F 0.5775(5) 0.3343(8) 0.6886(4) 0.051(2) Uiso 0.50 1 d PG A 1
F2 F 0.5601(6) 0.5340(8) 0.6819(5) 0.051(2) Uiso 0.50 1 d PG A 1
F3 F 0.5517(5) 0.4136(12) 0.6158(3) 0.051(2) Uiso 0.50 1 d PG A 1
C7 C 0.7761(4) 0.2115(7) 0.6529(4) 0.045(3) Uiso 0.50 1 d PGD A 1
F4 F 0.8273(4) 0.2130(13) 0.6795(4) 0.071(2) Uiso 0.50 1 d PG A 1
F5 F 0.7406(4) 0.1334(14) 0.6785(4) 0.071(2) Uiso 0.50 1 d PG A 1
F6 F 0.7869(5) 0.1533(11) 0.6084(3) 0.071(2) Uiso 0.50 1 d PG A 1
C14 C 0.5752(3) 1.0112(6) 0.6414(3) 0.046(2) Uiso 0.50 1 d PGD A 1
F7 F 0.5215(3) 1.0637(13) 0.6373(5) 0.0499(19) Uiso 0.50 1 d PG A 1
F8 F 0.5878(6) 1.0045(11) 0.6917(3) 0.0499(19) Uiso 0.50 1 d PG A 1
F9 F 0.6126(4) 1.0964(11) 0.6221(4) 0.0499(19) Uiso 0.50 1 d PG A 1
C15 C 0.5110(4) 0.7172(8) 0.4963(3) 0.044(2) Uiso 0.40 1 d PGD A 1
F10 F 0.4595(5) 0.6624(11) 0.5072(5) 0.0419(18) Uiso 0.40 1 d PG A 1
F11 F 0.4973(6) 0.8240(7) 0.4704(4) 0.0419(18) Uiso 0.40 1 d PG A 1
F12 F 0.5371(5) 0.6397(11) 0.4629(5) 0.0419(18) Uiso 0.40 1 d PG A 1
C22 C 1.0006(4) 0.5150(9) 0.6592(4) 0.066(3) Uiso 0.40 1 d PGD A 1
F13 F 0.9997(8) 0.6422(10) 0.6542(8) 0.074(2) Uiso 0.40 1 d PG A 1
F14 F 0.9961(7) 0.4921(19) 0.7094(4) 0.074(2) Uiso 0.40 1 d PG A 1
F15 F 1.0547(5) 0.4776(19) 0.6466(6) 0.074(2) Uiso 0.40 1 d PG A 1
C23 C 0.9293(8) 0.3071(16) 0.4962(4) 0.092(5) Uiso 0.37 1 d PGD A 1
F16 F 0.8945(8) 0.359(2) 0.4597(9) 0.119(5) Uiso 0.37 1 d PG A 1
F17 F 0.9845(7) 0.320(2) 0.4797(10) 0.119(5) Uiso 0.37 1 d PG A 1
F18 F 0.9177(10) 0.1818(16) 0.4958(9) 0.119(5) Uiso 0.37 1 d PG A 1
C6' C 0.5886(4) 0.4522(13) 0.6709(5) 0.042(2) Uiso 0.30 1 d PGD A 2
F1' F 0.5839(10) 0.3502(13) 0.7014(7) 0.049(3) Uiso 0.30 1 d PG A 2
F2' F 0.5725(7) 0.5525(12) 0.6991(6) 0.049(3) Uiso 0.30 1 d PG A 2
F3' F 0.5469(7) 0.4387(15) 0.6341(5) 0.049(3) Uiso 0.30 1 d PG A 2
C7' C 0.7737(7) 0.2223(10) 0.6724(6) 0.045(3) Uiso 0.25 1 d PGD A 2
F4' F 0.8277(8) 0.232(3) 0.6939(8) 0.057(4) Uiso 0.25 1 d PG A 2
F5' F 0.7411(8) 0.161(2) 0.7067(7) 0.057(4) Uiso 0.25 1 d PG A 2
F6' F 0.7787(9) 0.1428(19) 0.6326(6) 0.057(4) Uiso 0.25 1 d PG A 2
C14' C 0.5772(8) 1.0078(12) 0.6439(6) 0.046(2) Uiso 0.25 1 d PGD A 2
F7' F 0.5344(8) 1.089(2) 0.6292(9) 0.078(6) Uiso 0.25 1 d PG A 2
F8' F 0.5693(10) 0.987(3) 0.6938(7) 0.078(6) Uiso 0.25 1 d PG A 2
F9' F 0.6279(7) 1.072(2) 0.6406(9) 0.078(6) Uiso 0.25 1 d PG A 2
C15' C 0.5064(5) 0.7278(12) 0.4986(4) 0.044(2) Uiso 0.30 1 d PGD A 2
F10' F 0.4680(7) 0.6314(13) 0.5019(7) 0.062(3) Uiso 0.30 1 d PG A 2
F11' F 0.4743(7) 0.8306(11) 0.4856(7) 0.062(3) Uiso 0.30 1 d PG A 2
F12' F 0.5399(6) 0.7019(18) 0.4584(6) 0.062(3) Uiso 0.30 1 d PG A 2
C22' C 1.0013(5) 0.5152(14) 0.6593(5) 0.066(3) Uiso 0.30 1 d PGD A 2
F13' F 1.0275(13) 0.613(2) 0.6357(8) 0.092(4) Uiso 0.30 1 d PG A 2
F14' F 0.9852(9) 0.561(3) 0.7048(8) 0.092(4) Uiso 0.30 1 d PG A 2
F15' F 1.0435(11) 0.4286(17) 0.6690(11) 0.092(4) Uiso 0.30 1 d PG A 2
C23' C 0.9350(7) 0.2725(15) 0.5037(5) 0.092(5) Uiso 0.31 1 d PGD A 2
F16' F 0.9703(9) 0.3429(18) 0.4746(10) 0.095(4) Uiso 0.31 1 d PG A 2
F17' F 0.9644(9) 0.1641(18) 0.5134(8) 0.095(4) Uiso 0.31 1 d PG A 2
F18' F 0.8885(7) 0.241(2) 0.4738(8) 0.095(4) Uiso 0.31 1 d PG A 2
C6" C 0.5862(5) 0.4382(19) 0.6630(8) 0.042(2) Uiso 0.20 1 d PGD A 3
F1" F 0.5806(14) 0.369(2) 0.7056(9) 0.055(5) Uiso 0.20 1 d PG A 3
F2" F 0.5550(14) 0.5448(17) 0.6704(11) 0.055(5) Uiso 0.20 1 d PG A 3
F3" F 0.5579(12) 0.374(2) 0.6256(9) 0.055(5) Uiso 0.20 1 d PG A 3
C7" C 0.7816(6) 0.2265(11) 0.6703(5) 0.045(3) Uiso 0.25 1 d PGD A 3
F4" F 0.8222(7) 0.2483(19) 0.7073(6) 0.043(3) Uiso 0.25 1 d PG A 3
F5" F 0.7432(7) 0.144(2) 0.6903(7) 0.043(3) Uiso 0.25 1 d PG A 3
F6" F 0.8091(7) 0.1630(16) 0.6334(5) 0.043(3) Uiso 0.25 1 d PG A 3
C14" C 0.5773(6) 1.0150(9) 0.6413(5) 0.046(2) Uiso 0.25 1 d PGD A 3
F7" F 0.5230(5) 1.048(2) 0.6553(7) 0.050(4) Uiso 0.25 1 d PG A 3
F8" F 0.6111(7) 1.0221(18) 0.6839(6) 0.050(4) Uiso 0.25 1 d PG A 3
F9" F 0.5957(8) 1.1081(19) 0.6104(6) 0.050(4) Uiso 0.25 1 d PG A 3
C15" C 0.5181(6) 0.7182(13) 0.4918(4) 0.044(2) Uiso 0.30 1 d PGD A 3
F10" F 0.4595(6) 0.7136(18) 0.4964(7) 0.067(4) Uiso 0.30 1 d PG A 3
F11" F 0.5283(8) 0.8113(13) 0.4581(7) 0.067(4) Uiso 0.30 1 d PG A 3
F12" F 0.5336(8) 0.6089(13) 0.4692(8) 0.067(4) Uiso 0.30 1 d PG A 3
C22" C 0.9985(5) 0.5230(12) 0.6601(4) 0.066(3) Uiso 0.30 1 d PGD A 3
F13" F 0.9838(7) 0.6328(16) 0.6828(10) 0.071(3) Uiso 0.30 1 d PG A 3
F14" F 1.0134(10) 0.4428(16) 0.6982(8) 0.071(3) Uiso 0.30 1 d PG A 3
F15" F 1.0480(8) 0.546(3) 0.6349(6) 0.071(3) Uiso 0.30 1 d PG A 3
C23" C 0.9206(7) 0.2703(15) 0.5011(4) 0.092(5) Uiso 0.32 1 d PGD A 3
F16" F 0.9127(10) 0.3511(18) 0.4618(9) 0.093(4) Uiso 0.32 1 d PG A 3
F17" F 0.9747(6) 0.221(2) 0.4961(8) 0.093(4) Uiso 0.32 1 d PG A 3
F18" F 0.8828(8) 0.1739(18) 0.4930(8) 0.093(4) Uiso 0.32 1 d PG A 3
C29 C 0.6748(4) 1.0506(9) 0.4843(3) 0.040(2) Uiso 0.50 1 d PGD B 1
F19 F 0.7331(4) 1.0677(12) 0.4893(5) 0.049(3) Uiso 0.50 1 d PG B 1
F20 F 0.6503(7) 1.1508(11) 0.5073(6) 0.049(3) Uiso 0.50 1 d PG B 1
F21 F 0.6620(5) 0.9483(11) 0.5127(5) 0.049(3) Uiso 0.50 1 d PG B 1
C30 C 0.5896(9) 1.2843(11) 0.3370(6) 0.037(2) Uiso 0.25 1 d PGD B 1
F22 F 0.5624(12) 1.341(3) 0.3758(6) 0.052(5) Uiso 0.25 1 d PG B 1
F23 F 0.6372(8) 1.356(2) 0.3281(8) 0.052(5) Uiso 0.25 1 d PG B 1
F24 F 0.5538(9) 1.297(2) 0.2959(6) 0.052(5) Uiso 0.25 1 d PG B 1
C37 C 0.7053(3) 0.4711(6) 0.4686(3) 0.044(2) Uiso 0.45 1 d PGD B 1
F25 F 0.7213(5) 0.4379(11) 0.5164(3) 0.0575(18) Uiso 0.45 1 d PG B 1
F26 F 0.6466(3) 0.4585(12) 0.4658(4) 0.0575(18) Uiso 0.45 1 d PG B 1
F27 F 0.7272(5) 0.3813(10) 0.4379(4) 0.0575(18) Uiso 0.45 1 d PG B 1
C38 C 0.8741(4) 0.7856(12) 0.4441(5) 0.064(3) Uiso 0.35 1 d PGD B 1
F28 F 0.8860(8) 0.9108(10) 0.4446(7) 0.079(4) Uiso 0.35 1 d PG B 1
F29 F 0.9057(9) 0.7355(15) 0.4830(6) 0.079(4) Uiso 0.35 1 d PG B 1
F30 F 0.8972(8) 0.7393(15) 0.4012(5) 0.079(4) Uiso 0.35 1 d PG B 1
C45 C 0.4883(3) 1.0068(9) 0.1544(3) 0.069(3) Uiso 0.50 1 d PGD B 1
F31 F 0.4825(6) 0.8800(8) 0.1580(6) 0.076(2) Uiso 0.50 1 d PG B 1
F32 F 0.4397(6) 1.0562(12) 0.1748(5) 0.076(2) Uiso 0.50 1 d PG B 1
F33 F 0.4852(6) 1.0344(16) 0.1044(3) 0.076(2) Uiso 0.50 1 d PG B 1
C46 C 0.6877(3) 1.2186(8) 0.1507(3) 0.056(2) Uiso 0.50 1 d PGD B 1
F34 F 0.6905(6) 1.1760(11) 0.1025(4) 0.076(2) Uiso 0.50 1 d PG B 1
F35 F 0.6806(5) 1.3452(8) 0.1471(5) 0.076(2) Uiso 0.50 1 d PG B 1
F36 F 0.7413(4) 1.2000(13) 0.1721(4) 0.076(2) Uiso 0.50 1 d PG B 1
C29' C 0.6812(7) 1.0656(17) 0.4822(4) 0.040(2) Uiso 0.25 1 d PGD B 2
F19' F 0.7388(8) 1.093(3) 0.4810(9) 0.047(5) Uiso 0.25 1 d PG B 2
F20' F 0.6553(11) 1.1697(19) 0.5010(10) 0.047(5) Uiso 0.25 1 d PG B 2
F21' F 0.6755(11) 0.9740(17) 0.5174(8) 0.047(5) Uiso 0.25 1 d PG B 2
C30' C 0.5926(6) 1.2862(8) 0.3373(4) 0.037(2) Uiso 0.30 1 d PGD B 2
F22' F 0.5799(6) 1.3619(16) 0.3768(4) 0.035(3) Uiso 0.30 1 d PG B 2
F23' F 0.6360(7) 1.3452(18) 0.3127(7) 0.035(3) Uiso 0.30 1 d PG B 2
F24' F 0.5454(8) 1.2889(19) 0.3056(6) 0.035(3) Uiso 0.30 1 d PG B 2
C37' C 0.7100(6) 0.4658(9) 0.4597(6) 0.044(2) Uiso 0.25 1 d PGD B 2
F25' F 0.7479(7) 0.396(2) 0.4879(8) 0.066(3) Uiso 0.25 1 d PG B 2
F26' F 0.6584(7) 0.458(2) 0.4834(7) 0.066(3) Uiso 0.25 1 d PG B 2
F27' F 0.7025(9) 0.404(2) 0.4151(5) 0.066(3) Uiso 0.25 1 d PG B 2
C38' C 0.8731(4) 0.7881(13) 0.4559(5) 0.064(3) Uiso 0.35 1 d PGD B 2
F28' F 0.8840(8) 0.8927(13) 0.4840(6) 0.075(4) Uiso 0.35 1 d PG B 2
F29' F 0.9033(9) 0.6937(13) 0.4790(7) 0.075(4) Uiso 0.35 1 d PG B 2
F30' F 0.8987(8) 0.8075(16) 0.4109(5) 0.075(4) Uiso 0.35 1 d PG B 2
C45' C 0.4859(5) 1.0163(17) 0.1534(6) 0.069(3) Uiso 0.25 1 d PGD B 2
F31' F 0.4903(10) 0.8993(19) 0.1332(10) 0.080(5) Uiso 0.25 1 d PG B 2
F32' F 0.4385(11) 1.013(2) 0.1829(8) 0.080(5) Uiso 0.25 1 d PG B 2
F33' F 0.4722(11) 1.095(2) 0.1144(9) 0.080(5) Uiso 0.25 1 d PG B 2
C46' C 0.6875(5) 1.2324(12) 0.1535(5) 0.056(2) Uiso 0.25 1 d PGD B 2
F34' F 0.7126(8) 1.1603(14) 0.1178(7) 0.054(3) Uiso 0.25 1 d PG B 2
F35' F 0.6659(7) 1.3348(15) 0.1288(7) 0.054(3) Uiso 0.25 1 d PG B 2
F36' F 0.7315(8) 1.2748(19) 0.1841(5) 0.054(3) Uiso 0.25 1 d PG B 2
C29" C 0.6727(7) 1.0469(14) 0.4845(4) 0.040(2) Uiso 0.25 1 d PGD B 3
F19" F 0.7254(6) 1.103(2) 0.4896(9) 0.042(4) Uiso 0.25 1 d PG B 3
F20" F 0.6343(7) 1.1261(16) 0.5062(8) 0.042(4) Uiso 0.25 1 d PG B 3
F21" F 0.6751(11) 0.9424(15) 0.5139(10) 0.042(4) Uiso 0.25 1 d PG B 3
C30" C 0.5779(4) 1.2734(8) 0.3362(3) 0.037(2) Uiso 0.45 1 d PGD B 3
F22" F 0.5649(7) 1.3477(19) 0.3760(4) 0.048(3) Uiso 0.45 1 d PG B 3
F23" F 0.6153(4) 1.3412(11) 0.3081(4) 0.048(3) Uiso 0.45 1 d PG B 3
F24" F 0.5282(4) 1.2622(11) 0.3079(4) 0.048(3) Uiso 0.45 1 d PG B 3
C37" C 0.7088(5) 0.4723(8) 0.4708(4) 0.044(2) Uiso 0.30 1 d PGD B 3
F25" F 0.6956(7) 0.4608(15) 0.5202(4) 0.053(3) Uiso 0.30 1 d PG B 3
F26" F 0.6598(6) 0.4393(16) 0.4444(5) 0.053(3) Uiso 0.30 1 d PG B 3
F27" F 0.7488(5) 0.3818(14) 0.4614(6) 0.053(3) Uiso 0.30 1 d PG B 3
C38" C 0.8729(4) 0.7836(13) 0.4389(6) 0.064(3) Uiso 0.30 1 d PGD B 3
F28" F 0.8864(9) 0.8925(13) 0.4632(7) 0.059(4) Uiso 0.30 1 d PG B 3
F29" F 0.9073(8) 0.6939(13) 0.4606(6) 0.059(4) Uiso 0.30 1 d PG B 3
F30" F 0.8914(8) 0.7974(18) 0.3909(5) 0.059(4) Uiso 0.30 1 d PG B 3
C45" C 0.4888(6) 0.9958(17) 0.1551(6) 0.069(3) Uiso 0.25 1 d PGD B 3
F31" F 0.4658(12) 0.8907(19) 0.1759(9) 0.082(6) Uiso 0.25 1 d PG B 3
F32" F 0.4469(12) 1.0854(17) 0.1577(10) 0.082(6) Uiso 0.25 1 d PG B 3
F33" F 0.4950(11) 0.970(3) 0.1053(7) 0.082(6) Uiso 0.25 1 d PG B 3
C46" C 0.6918(5) 1.2059(14) 0.1526(6) 0.056(2) Uiso 0.25 1 d PGD B 3
F34" F 0.6811(9) 1.226(2) 0.1026(6) 0.071(4) Uiso 0.25 1 d PG B 3
F35" F 0.7094(10) 1.3185(17) 0.1718(8) 0.071(4) Uiso 0.25 1 d PG B 3
F36" F 0.7387(8) 1.1285(17) 0.1557(8) 0.071(4) Uiso 0.25 1 d PG B 3
N1 N 0.6641(3) 0.5775(6) 0.6255(2) 0.0371(14) Uani 1 1 d . A .
N2 N 0.7859(3) 0.4392(6) 0.6292(3) 0.0394(15) Uani 1 1 d . A .
N3 N 0.6648(3) 0.9119(6) 0.4071(3) 0.0400(15) Uani 1 1 d . B .
N4 N 0.6076(3) 1.0544(6) 0.3153(2) 0.0390(15) Uani 1 1 d . B .
C1 C 0.7684(8) 0.849(2) 0.6036(9) 0.057(6) Uiso 0.50 1 d PD C 1
H1A H 0.7526 0.8842 0.5708 0.068 Uiso 0.50 1 calc PR C 1
H1B H 0.7603 0.9038 0.6337 0.068 Uiso 0.50 1 calc PR C 1
C2 C 0.8251(8) 0.794(2) 0.6023(9) 0.048(6) Uiso 0.50 1 d PD C 1
H2A H 0.8524 0.8133 0.6316 0.058 Uiso 0.50 1 calc PR C 1
H2B H 0.8446 0.7937 0.5686 0.058 Uiso 0.50 1 calc PR C 1
C24 C 0.5924(11) 0.643(2) 0.3205(8) 0.052(6) Uiso 0.50 1 d PD D 1
H24A H 0.6248 0.5828 0.3129 0.062 Uiso 0.50 1 calc PR D 1
H24B H 0.5628 0.6070 0.3439 0.062 Uiso 0.50 1 calc PR D 1
C25 C 0.5705(13) 0.715(2) 0.2796(8) 0.055(7) Uiso 0.50 1 d PD D 1
H25A H 0.5269 0.7245 0.2771 0.066 Uiso 0.50 1 calc PR D 1
H25B H 0.5890 0.7002 0.2461 0.066 Uiso 0.50 1 calc PR D 1
C1' C 0.7820(7) 0.8365(17) 0.5856(7) 0.041(4) Uiso 0.50 1 d PD C 2
H1'A H 0.7706 0.8562 0.5495 0.049 Uiso 0.50 1 calc PR C 2
H1'B H 0.7762 0.9093 0.6093 0.049 Uiso 0.50 1 calc PR C 2
C2' C 0.8341(9) 0.764(2) 0.5933(9) 0.053(6) Uiso 0.50 1 d PD C 2
H2'A H 0.8609 0.7920 0.6218 0.063 Uiso 0.50 1 calc PR C 2
H2'B H 0.8553 0.7390 0.5620 0.063 Uiso 0.50 1 calc PR C 2
C24' C 0.6119(12) 0.642(2) 0.3246(8) 0.059(7) Uiso 0.50 1 d PD D 2
H24C H 0.6494 0.5957 0.3186 0.070 Uiso 0.50 1 calc PR D 2
H24D H 0.5858 0.5963 0.3485 0.070 Uiso 0.50 1 calc PR D 2
C25' C 0.5845(14) 0.696(3) 0.2817(10) 0.071(10) Uiso 0.50 1 d PD D 2
H25C H 0.5409 0.6867 0.2787 0.086 Uiso 0.50 1 calc PR D 2
H25D H 0.6048 0.6860 0.2487 0.086 Uiso 0.50 1 calc PR D 2
C3 C 0.6499(3) 0.4656(7) 0.6473(3) 0.0403(18) Uani 1 1 d D . .
C4 C 0.6900(4) 0.3647(8) 0.6597(3) 0.048(2) Uani 1 1 d . A .
H4 H 0.6732 0.2962 0.6784 0.058 Uiso 1 1 calc R . .
C5 C 0.7514(3) 0.3486(6) 0.6489(3) 0.045(2) Uani 1 1 d D . .
C8 C 0.6209(3) 0.6691(7) 0.6081(3) 0.0348(17) Uani 1 1 d . . .
C9 C 0.6170(3) 0.7885(8) 0.6327(3) 0.0415(19) Uani 1 1 d . A .
H9 H 0.6412 0.8053 0.6623 0.050 Uiso 1 1 calc R . .
C10 C 0.5783(3) 0.8826(6) 0.6145(3) 0.0378(18) Uani 1 1 d D . .
C11 C 0.5438(3) 0.8616(8) 0.5699(3) 0.0423(19) Uani 1 1 d . A .
H11 H 0.5179 0.9264 0.5570 0.051 Uiso 1 1 calc R . .
C12 C 0.5479(3) 0.7447(8) 0.5447(2) 0.0386(18) Uani 1 1 d D . .
C13 C 0.5858(3) 0.6476(7) 0.5632(3) 0.0379(17) Uani 1 1 d . A .
H13 H 0.5879 0.5680 0.5457 0.045 Uiso 1 1 calc R . .
C16 C 0.8460(3) 0.4159(7) 0.6145(3) 0.0402(18) Uani 1 1 d . . .
C17 C 0.8925(3) 0.4689(8) 0.6435(3) 0.0437(19) Uani 1 1 d . A .
H17 H 0.8846 0.5116 0.6748 0.052 Uiso 1 1 calc R . .
C18 C 0.9504(3) 0.4596(8) 0.6267(3) 0.051(2) Uani 1 1 d D . .
C19 C 0.9628(4) 0.3989(11) 0.5804(4) 0.067(3) Uani 1 1 d . A .
H19 H 1.0023 0.3929 0.5691 0.080 Uiso 1 1 calc R . .
C20 C 0.9165(4) 0.3475(11) 0.5512(3) 0.070(3) Uani 1 1 d D . .
C21 C 0.8585(4) 0.3558(9) 0.5682(4) 0.060(3) Uani 1 1 d . A .
H21 H 0.8272 0.3201 0.5479 0.072 Uiso 1 1 calc R . .
C26 C 0.6547(3) 1.0279(7) 0.4283(2) 0.0368(18) Uani 1 1 d D . .
C27 C 0.6237(3) 1.1298(7) 0.4042(3) 0.0390(18) Uani 1 1 d . B .
H27 H 0.6125 1.1975 0.4263 0.047 Uiso 1 1 calc R . .
C28 C 0.6067(3) 1.1459(6) 0.3513(3) 0.0364(17) Uani 1 1 d D . .
C31 C 0.7068(3) 0.8225(7) 0.4281(3) 0.0369(17) Uani 1 1 d . . .
C32 C 0.6881(3) 0.6980(7) 0.4398(3) 0.0384(18) Uani 1 1 d . B .
H32 H 0.6473 0.6771 0.4375 0.046 Uiso 1 1 calc R . .
C33 C 0.7288(3) 0.6048(6) 0.4549(3) 0.0422(19) Uani 1 1 d D . .
C34 C 0.7891(4) 0.6303(8) 0.4578(3) 0.049(2) Uani 1 1 d . B .
H34 H 0.8166 0.5654 0.4674 0.059 Uiso 1 1 calc R . .
C35 C 0.8081(2) 0.7539(8) 0.4463(3) 0.048(2) Uani 1 1 d D . .
C36 C 0.7674(3) 0.8501(8) 0.4307(3) 0.0445(19) Uani 1 1 d . B .
H36 H 0.7811 0.9331 0.4220 0.053 Uiso 1 1 calc R . .
C39 C 0.6002(3) 1.0816(7) 0.2614(3) 0.0344(17) Uani 1 1 d . . .
C40 C 0.5495(4) 1.0367(8) 0.2345(3) 0.045(2) Uani 1 1 d . B .
H40 H 0.5190 0.9948 0.2525 0.054 Uiso 1 1 calc R . .
C41 C 0.5440(3) 1.0537(8) 0.1813(3) 0.046(2) Uani 1 1 d D . .
C42 C 0.5886(4) 1.1126(8) 0.1540(3) 0.050(2) Uani 1 1 d . B .
H42 H 0.5849 1.1236 0.1178 0.060 Uiso 1 1 calc R . .
C43 C 0.6392(3) 1.1554(8) 0.1810(3) 0.046(2) Uani 1 1 d D . .
C44 C 0.6451(3) 1.1402(7) 0.2339(3) 0.0405(18) Uani 1 1 d . B .
H44 H 0.6798 1.1697 0.2514 0.049 Uiso 1 1 calc R . .
C47 C 0.7044(10) 0.847(3) 0.7591(16) 0.040(6) Uiso 0.25 1 d PG . 1
H47 H 0.6796 0.9215 0.7640 0.048 Uiso 0.25 1 d PG . 1
C48 C 0.680(2) 0.723(4) 0.7622(15) 0.040(6) Uiso 0.25 1 d PG . 1
H48 H 0.6384 0.7128 0.7693 0.048 Uiso 0.25 1 d PG . 1
C49 C 0.716(4) 0.615(2) 0.755(2) 0.040(6) Uiso 0.25 1 d PG . 1
H49 H 0.6991 0.5301 0.7574 0.048 Uiso 0.25 1 d PG . 1
C50 C 0.776(3) 0.631(2) 0.745(2) 0.040(6) Uiso 0.25 1 d PG . 1
H50 H 0.8011 0.5561 0.7401 0.048 Uiso 0.25 1 d PG . 1
C51 C 0.8006(18) 0.754(4) 0.7418(16) 0.040(6) Uiso 0.25 1 d PG . 1
H51 H 0.8423 0.7648 0.7348 0.048 Uiso 0.25 1 d PG . 1
C52 C 0.7647(10) 0.8622(19) 0.7489(16) 0.040(6) Uiso 0.25 1 d PG . 1
H52 H 0.7816 0.9475 0.7467 0.048 Uiso 0.25 1 d PG . 1
C47' C 0.725(3) 0.846(3) 0.7491(18) 0.060(8) Uiso 0.25 1 d PG . 2
H47' H 0.6973 0.9175 0.7511 0.072 Uiso 0.25 1 d PG . 2
C48' C 0.7039(17) 0.720(5) 0.7559(19) 0.060(8) Uiso 0.25 1 d PG . 2
H48' H 0.6625 0.7050 0.7626 0.072 Uiso 0.25 1 d PG . 2
C49' C 0.7433(17) 0.617(2) 0.7531(18) 0.060(8) Uiso 0.25 1 d PG . 2
H49' H 0.7291 0.5297 0.7578 0.072 Uiso 0.25 1 d PG . 2
C50' C 0.8033(15) 0.639(3) 0.7435(14) 0.060(8) Uiso 0.25 1 d PG . 2
H50' H 0.8306 0.5670 0.7415 0.072 Uiso 0.25 1 d PG . 2
C51' C 0.824(2) 0.764(5) 0.7367(16) 0.060(8) Uiso 0.25 1 d PG . 2
H51' H 0.8654 0.7795 0.7301 0.072 Uiso 0.25 1 d PG . 2
C52' C 0.785(3) 0.868(2) 0.7395(19) 0.060(8) Uiso 0.25 1 d PG . 2
H52' H 0.7988 0.9547 0.7349 0.072 Uiso 0.25 1 d PG . 2
C53 C 0.758(2) 0.857(3) 0.245(2) 0.075(9) Uiso 0.25 1 d PG . 1
H53 H 0.7548 0.9495 0.2415 0.090 Uiso 0.25 1 d PG . 1
C54 C 0.788(2) 0.805(5) 0.2880(17) 0.075(9) Uiso 0.25 1 d PG . 1
H54 H 0.8052 0.8604 0.3141 0.090 Uiso 0.25 1 d PG . 1
C55 C 0.7928(19) 0.671(6) 0.2932(19) 0.075(9) Uiso 0.25 1 d PG . 1
H55 H 0.8134 0.6347 0.3229 0.090 Uiso 0.25 1 d PG . 1
C56 C 0.768(2) 0.590(2) 0.255(3) 0.075(9) Uiso 0.25 1 d PG . 1
H56 H 0.7712 0.4978 0.2591 0.090 Uiso 0.25 1 d PG . 1
C57 C 0.738(2) 0.643(6) 0.212(2) 0.075(9) Uiso 0.25 1 d PG . 1
H57 H 0.7207 0.5869 0.1864 0.090 Uiso 0.25 1 d PG . 1
C58 C 0.733(2) 0.776(6) 0.2073(15) 0.075(9) Uiso 0.25 1 d PG . 1
H58 H 0.7125 0.8126 0.1776 0.090 Uiso 0.25 1 d PG . 1
C53' C 0.742(3) 0.852(3) 0.2391(16) 0.069(10) Uiso 0.25 1 d PG . 2
H53' H 0.7409 0.9423 0.2297 0.083 Uiso 0.25 1 d PG . 2
C54' C 0.769(3) 0.815(4) 0.2862(13) 0.069(10) Uiso 0.25 1 d PG . 2
H54' H 0.7850 0.8791 0.3095 0.083 Uiso 0.25 1 d PG . 2
C55' C 0.771(3) 0.685(4) 0.2997(13) 0.069(10) Uiso 0.25 1 d PG . 2
H55' H 0.7890 0.6590 0.3323 0.083 Uiso 0.25 1 d PG . 2
C56' C 0.747(3) 0.592(3) 0.266(2) 0.069(10) Uiso 0.25 1 d PG . 2
H56' H 0.7489 0.5020 0.2754 0.083 Uiso 0.25 1 d PG . 2
C57' C 0.721(3) 0.629(4) 0.2189(18) 0.069(10) Uiso 0.25 1 d PG . 2
H57' H 0.7047 0.5652 0.1956 0.083 Uiso 0.25 1 d PG . 2
C58' C 0.719(2) 0.760(5) 0.2054(11) 0.069(10) Uiso 0.25 1 d PG . 2
H58' H 0.7007 0.7853 0.1728 0.083 Uiso 0.25 1 d PG . 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
N2 Ag1 C1 156.2(5) . .
N2 Ag1 N1 88.9(2) . .
C1 Ag1 N1 114.5(5) . .
N2 Ag1 C2' 111.1(6) . .
C1 Ag1 C2' 46.1(8) . .
N1 Ag1 C2' 159.4(5) . .
N2 Ag1 C2 119.9(5) . .
C1 Ag1 C2 36.6(5) . .
N1 Ag1 C2 151.1(5) . .
C2' Ag1 C2 11.2(8) . .
N2 Ag1 C1' 146.6(5) . .
C1 Ag1 C1' 14.8(6) . .
N1 Ag1 C1' 123.2(4) . .
C2' Ag1 C1' 36.2(5) . .
C2 Ag1 C1' 29.4(6) . .
C24' Ag2 N4 157.3(6) . .
C24' Ag2 N3 115.5(6) . .
N4 Ag2 N3 87.2(2) . .
C24' Ag2 C25' 36.6(6) . .
N4 Ag2 C25' 120.8(6) . .
N3 Ag2 C25' 152.0(6) . .
C24' Ag2 C24 11.5(8) . .
N4 Ag2 C24 148.7(5) . .
N3 Ag2 C24 122.7(5) . .
C25' Ag2 C24 30.0(9) . .
C24' Ag2 C25 44.0(9) . .
N4 Ag2 C25 113.6(6) . .
N3 Ag2 C25 158.1(6) . .
C25' Ag2 C25 9.6(11) . .
C24 Ag2 C25 35.7(6) . .
F2 C6 F1 105.8 . .
F2 C6 F3 106.3 . .
F1 C6 F3 106.3 . .
F2 C6 C3 109.9(8) . .
F1 C6 C3 113.8(7) . .
F3 C6 C3 114.1(8) . .
F4 C7 F5 105.8 . .
F4 C7 F6 106.3 . .
F5 C7 F6 106.3 . .
F4 C7 C5 109.5(8) . .
F5 C7 C5 112.3(9) . .
F6 C7 C5 116.0(8) . .
F8 C14 F9 106.3 . .
F8 C14 F7 105.8 . .
F9 C14 F7 106.3 . .
F8 C14 C10 113.3(8) . .
F9 C14 C10 112.3(8) . .
F7 C14 C10 112.2(8) . .
F10 C15 F12 106.3 . .
F10 C15 F11 105.8 . .
F12 C15 F11 106.3 . .
F10 C15 C12 111.6(9) . .
F12 C15 C12 114.3(9) . .
F11 C15 C12 112.1(8) . .
F15 C22 F14 106.3 . .
F15 C22 F13 106.3 . .
F14 C22 F13 105.8 . .
F15 C22 C18 115.5(10) . .
F14 C22 C18 113.9(10) . .
F13 C22 C18 108.4(10) . .
F16 C23 F18 106.3 . .
F16 C23 F17 105.8 . .
F18 C23 F17 106.3 . .
F16 C23 C20 115.6(17) . .
F18 C23 C20 103.6(15) . .
F17 C23 C20 118.2(17) . .
F1' C6' F2' 105.8 . .
F1' C6' F3' 106.3 . .
F2' C6' F3' 106.3 . .
F1' C6' C3 113.3(13) . .
F2' C6' C3 114.2(11) . .
F3' C6' C3 110.5(10) . .
F6' C7' F5' 106.3 . .
F6' C7' F4' 106.3 . .
F5' C7' F4' 105.8 . .
F6' C7' C5 104.9(13) . .
F5' C7' C5 119.8(15) . .
F4' C7' C5 112.9(17) . .
F7' C14' F8' 105.8 . .
F7' C14' F9' 106.3 . .
F8' C14' F9' 106.3 . .
F7' C14' C10 114.9(17) . .
F8' C14' C10 110.7(17) . .
F9' C14' C10 112.3(16) . .
F11' C15' F12' 106.3 . .
F11' C15' F10' 105.8 . .
F12' C15' F10' 106.3 . .
F11' C15' C12 115.4(11) . .
F12' C15' C12 107.0(11) . .
F10' C15' C12 115.3(12) . .
F14' C22' F15' 106.3 . .
F14' C22' F13' 105.8 . .
F15' C22' F13' 106.3 . .
F14' C22' C18 114.2(14) . .
F15' C22' C18 111.9(14) . .
F13' C22' C18 111.8(14) . .
F17' C23' F16' 105.8 . .
F17' C23' F18' 106.3 . .
F16' C23' F18' 106.3 . .
F17' C23' C20 115.2(15) . .
F16' C23' C20 110.9(16) . .
F18' C23' C20 111.8(14) . .
F2" C6" F3" 106.3 . .
F2" C6" F1" 105.8 . .
F3" C6" F1" 106.3 . .
F2" C6" C3 113(2) . .
F3" C6" C3 109.7(18) . .
F1" C6" C3 116(2) . .
F6" C7" F5" 106.3 . .
F6" C7" F4" 106.3 . .
F5" C7" F4" 105.8 . .
F6" C7" C5 111.1(11) . .
F5" C7" C5 112.6(15) . .
F4" C7" C5 114.3(14) . .
F7" C14" F8" 105.8 . .
F7" C14" F9" 106.3 . .
F8" C14" F9" 106.3 . .
F7" C14" C10 111.9(13) . .
F8" C14" C10 114.3(12) . .
F9" C14" C10 111.7(13) . .
F11" C15" F12" 106.3 . .
F11" C15" F10" 105.8 . .
F12" C15" F10" 106.3 . .
F11" C15" C12 112.2(11) . .
F12" C15" C12 115.7(13) . .
F10" C15" C12 109.9(12) . .
F15" C22" F13" 106.3 . .
F15" C22" F14" 106.3 . .
F13" C22" F14" 105.8 . .
F15" C22" C18 113.1(12) . .
F13" C22" C18 116.3(12) . .
F14" C22" C18 108.3(12) . .
F17" C23" F18" 106.3 . .
F17" C23" F16" 105.8 . .
F18" C23" F16" 106.3 . .
F17" C23" C20 111.0(14) . .
F18" C23" C20 118.6(14) . .
F16" C23" C20 108.0(16) . .
F20 C29 F21 106.3 . .
F20 C29 F19 105.8 . .
F21 C29 F19 106.3 . .
F20 C29 C26 115.5(9) . .
F21 C29 C26 109.8(9) . .
F19 C29 C26 112.6(9) . .
F24 C30 F23 106.3 . .
F24 C30 F22 106.3 . .
F23 C30 F22 105.8 . .
F24 C30 C28 115.7(17) . .
F23 C30 C28 111.7(16) . .
F22 C30 C28 110.5(19) . .
F26 C37 F27 106.3 . .
F26 C37 F25 105.8 . .
F27 C37 F25 106.3 . .
F26 C37 C33 115.2(8) . .
F27 C37 C33 111.3(7) . .
F25 C37 C33 111.4(8) . .
F29 C38 F28 105.8 . .
F29 C38 F30 106.3 . .
F28 C38 F30 106.3 . .
F29 C38 C35 113.1(12) . .
F28 C38 C35 114.1(12) . .
F30 C38 C35 110.8(12) . .
F31 C45 F33 106.3 . .
F31 C45 F32 105.8 . .
F33 C45 F32 106.3 . .
F31 C45 C41 111.8(9) . .
F33 C45 C41 113.9(9) . .
F32 C45 C41 112.2(10) . .
F35 C46 F36 106.3 . .
F35 C46 F34 105.8 . .
F36 C46 F34 106.3 . .
F35 C46 C43 112.4(8) . .
F36 C46 C43 112.4(8) . .
F34 C46 C43 113.2(8) . .
F20' C29' F21' 106.3 . .
F20' C29' F19' 105.8 . .
F21' C29' F19' 106.3 . .
F20' C29' C26 111.9(16) . .
F21' C29' C26 113.3(15) . .
F19' C29' C26 112.8(15) . .
F24' C30' F23' 106.3 . .
F24' C30' F22' 106.3 . .
F23' C30' F22' 105.8 . .
F24' C30' C28 108.9(12) . .
F23' C30' C28 113.7(12) . .
F22' C30' C28 115.3(10) . .
F26' C37' F27' 106.3 . .
F26' C37' F25' 105.8 . .
F27' C37' F25' 106.3 . .
F26' C37' C33 110.1(14) . .
F27' C37' C33 114.8(13) . .
F25' C37' C33 113.0(13) . .
F30' C38' F28' 106.3 . .
F30' C38' F29' 106.3 . .
F28' C38' F29' 105.8 . .
F30' C38' C35 109.0(11) . .
F28' C38' C35 116.4(12) . .
F29' C38' C35 112.4(13) . .
F32' C45' F33' 106.3 . .
F32' C45' F31' 105.8 . .
F33' C45' F31' 106.3 . .
F32' C45' C41 115.1(17) . .
F33' C45' C41 112.5(16) . .
F31' C45' C41 110.3(16) . .
F34' C46' F35' 105.8 . .
F34' C46' F36' 106.3 . .
F35' C46' F36' 106.3 . .
F34' C46' C43 110.3(12) . .
F35' C46' C43 112.7(12) . .
F36' C46' C43 114.9(12) . .
F19" C29" F21" 106.3 . .
F19" C29" F20" 105.8 . .
F21" C29" F20" 106.3 . .
F19" C29" C26 111.8(14) . .
F21" C29" C26 116.9(15) . .
F20" C29" C26 109.1(13) . .
F24" C30" F22" 106.3 . .
F24" C30" F23" 106.3 . .
F22" C30" F23" 105.8 . .
F24" C30" C28 114.4(8) . .
F22" C30" C28 114.0(10) . .
F23" C30" C28 109.4(8) . .
F25" C37" F27" 106.3 . .
F25" C37" F26" 105.8 . .
F27" C37" F26" 106.3 . .
F25" C37" C33 114.9(10) . .
F27" C37" C33 112.8(10) . .
F26" C37" C33 110.2(10) . .
F30" C38" F28" 106.3 . .
F30" C38" F29" 106.3 . .
F28" C38" F29" 105.8 . .
F30" C38" C35 117.8(12) . .
F28" C38" C35 108.9(13) . .
F29" C38" C35 111.0(12) . .
F33" C45" F32" 106.3 . .
F33" C45" F31" 106.3 . .
F32" C45" F31" 105.8 . .
F33" C45" C41 114.1(16) . .
F32" C45" C41 105.8(17) . .
F31" C45" C41 117.7(17) . .
F34" C46" F36" 106.3 . .
F34" C46" F35" 105.8 . .
F36" C46" F35" 106.3 . .
F34" C46" C43 113.9(14) . .
F36" C46" C43 113.2(13) . .
F35" C46" C43 110.8(14) . .
C3 N1 C8 123.2(6) . .
C3 N1 Ag1 122.8(4) . .
C8 N1 Ag1 114.0(5) . .
C5 N2 C16 123.0(6) . .
C5 N2 Ag1 123.9(5) . .
C16 N2 Ag1 113.0(5) . .
C26 N3 C31 123.0(6) . .
C26 N3 Ag2 122.2(4) . .
C31 N3 Ag2 114.8(5) . .
C28 N4 C39 122.6(6) . .
C28 N4 Ag2 122.4(5) . .
C39 N4 Ag2 115.0(5) . .
C2 C1 Ag1 73.2(12) . .
C1 C2 Ag1 70.3(12) . .
C25 C24 Ag2 72.7(14) . .
C24 C25 Ag2 71.6(14) . .
C2' C1' Ag1 71.3(11) . .
C1' C2' Ag1 72.4(11) . .
C25' C24' Ag2 74.0(16) . .
C24' C25' Ag2 69.5(16) . .
N1 C3 C4 125.8(6) . .
N1 C3 C6" 120.7(9) . .
C4 C3 C6" 113.5(9) . .
N1 C3 C6' 118.4(7) . .
C4 C3 C6' 114.7(8) . .
C6" C3 C6' 9.6(11) . .
N1 C3 C6 119.7(6) . .
C4 C3 C6 114.5(7) . .
C6" C3 C6 5.1(10) . .
C6' C3 C6 14.5(6) . .
C3 C4 C5 131.1(7) . .
N2 C5 C4 124.8(6) . .
N2 C5 C7' 124.8(9) . .
C4 C5 C7' 109.5(9) . .
N2 C5 C7 118.0(7) . .
C4 C5 C7 116.6(7) . .
C7' C5 C7 19.7(7) . .
N2 C5 C7" 117.7(8) . .
C4 C5 C7" 116.6(8) . .
C7' C5 C7" 7.2(9) . .
C7 C5 C7" 18.4(6) . .
C9 C8 C13 118.5(7) . .
C9 C8 N1 119.9(7) . .
C13 C8 N1 121.3(7) . .
C10 C9 C8 121.1(7) . .
C9 C10 C11 120.4(6) . .
C9 C10 C14' 117.0(9) . .
C11 C10 C14' 122.6(9) . .
C9 C10 C14 120.2(7) . .
C11 C10 C14 119.4(6) . .
C14' C10 C14 3.2(9) . .
C9 C10 C14" 119.4(8) . .
C11 C10 C14" 120.0(8) . .
C14' C10 C14" 3.6(8) . .
C14 C10 C14" 2.0(7) . .
C12 C11 C10 119.1(7) . .
C11 C12 C13 121.3(6) . .
C11 C12 C15' 115.3(8) . .
C13 C12 C15' 123.3(8) . .
C11 C12 C15 121.0(7) . .
C13 C12 C15 117.8(7) . .
C15' C12 C15 6.2(6) . .
C11 C12 C15" 123.1(8) . .
C13 C12 C15" 115.2(8) . .
C15' C12 C15" 12.6(6) . .
C15 C12 C15" 7.4(7) . .
C12 C13 C8 119.6(7) . .
C21 C16 C17 118.8(8) . .
C21 C16 N2 121.1(7) . .
C17 C16 N2 119.5(7) . .
C18 C17 C16 120.3(8) . .
C19 C18 C17 120.7(7) . .
C19 C18 C22 119.5(8) . .
C17 C18 C22 119.7(8) . .
C19 C18 C22' 119.2(9) . .
C17 C18 C22' 120.1(9) . .
C22 C18 C22' 0.3(8) . .
C19 C18 C22" 122.3(8) . .
C17 C18 C22" 117.0(8) . .
C22 C18 C22" 3.7(6) . .
C22' C18 C22" 4.0(7) . .
C20 C19 C18 119.0(8) . .
C19 C20 C21 120.3(7) . .
C19 C20 C23 117.6(10) . .
C21 C20 C23 120.9(10) . .
C19 C20 C23' 115.1(9) . .
C21 C20 C23' 124.3(10) . .
C23 C20 C23' 16.1(9) . .
C19 C20 C23" 127.4(9) . .
C21 C20 C23" 112.1(9) . .
C23 C20 C23" 16.9(10) . .
C23' C20 C23" 12.4(8) . .
C20 C21 C16 120.8(8) . .
N3 C26 C27 125.4(6) . .
N3 C26 C29" 117.8(8) . .
C27 C26 C29" 116.6(8) . .
N3 C26 C29 118.5(7) . .
C27 C26 C29 116.0(7) . .
C29" C26 C29 2.3(9) . .
N3 C26 C29' 121.8(9) . .
C27 C26 C29' 112.7(9) . .
C29" C26 C29' 10.4(10) . .
C29 C26 C29' 8.1(9) . .
C26 C27 C28 129.5(7) . .
N4 C28 C27 125.5(6) . .
N4 C28 C30" 117.1(7) . .
C27 C28 C30" 116.9(7) . .
N4 C28 C30 120.7(8) . .
C27 C28 C30 113.8(8) . .
C30" C28 C30 10.8(9) . .
N4 C28 C30' 121.4(7) . .
C27 C28 C30' 112.8(7) . .
C30" C28 C30' 13.4(6) . .
C30 C28 C30' 2.6(12) . .
C36 C31 C32 118.6(7) . .
C36 C31 N3 121.6(7) . .
C32 C31 N3 119.2(7) . .
C33 C32 C31 120.7(7) . .
C32 C33 C34 121.6(6) . .
C32 C33 C37" 121.0(7) . .
C34 C33 C37" 117.4(7) . .
C32 C33 C37' 120.5(8) . .
C34 C33 C37' 117.2(8) . .
C37" C33 C37' 11.3(7) . .
C32 C33 C37 118.1(7) . .
C34 C33 C37 120.4(7) . .
C37" C33 C37 3.5(5) . .
C37' C33 C37 9.8(7) . .
C33 C34 C35 118.2(7) . .
C34 C35 C36 121.0(6) . .
C34 C35 C38" 121.4(8) . .
C36 C35 C38" 116.4(8) . .
C34 C35 C38' 118.8(8) . .
C36 C35 C38' 119.9(8) . .
C38" C35 C38' 16.8(8) . .
C34 C35 C38 120.9(8) . .
C36 C35 C38 117.7(8) . .
C38" C35 C38 5.2(8) . .
C38' C35 C38 11.6(8) . .
C31 C36 C35 119.9(7) . .
C40 C39 C44 118.9(7) . .
C40 C39 N4 119.7(7) . .
C44 C39 N4 121.1(7) . .
C39 C40 C41 120.2(7) . .
C42 C41 C40 120.8(6) . .
C42 C41 C45 121.0(7) . .
C40 C41 C45 118.2(7) . .
C42 C41 C45" 122.7(9) . .
C40 C41 C45" 116.3(9) . .
C45 C41 C45" 4.3(9) . .
C42 C41 C45' 119.6(9) . .
C40 C41 C45' 119.4(9) . .
C45 C41 C45' 4.2(8) . .
C45" C41 C45' 8.5(9) . .
C41 C42 C43 118.6(7) . .
C44 C43 C42 121.3(6) . .
C44 C43 C46" 117.8(9) . .
C42 C43 C46" 120.6(9) . .
C44 C43 C46 120.7(7) . .
C42 C43 C46 118.1(7) . .
C46" C43 C46 6.4(7) . .
C44 C43 C46' 117.7(8) . .
C42 C43 C46' 120.8(8) . .
C46" C43 C46' 11.0(7) . .
C46 C43 C46' 5.9(6) . .
C43 C44 C39 120.2(7) . .
C52 C47 C51 108(6) 2_656 2_656
C52 C47 C52 8(4) 2_656 .
C51 C47 C52 103(5) 2_656 .
C52 C47 C48 125.6(11) 2_656 .
C51 C47 C48 17(5) 2_656 .
C52 C47 C48 120.0 . .
C51 C48 C50 79(9) 2_656 2_656
C51 C48 C49 89(5) 2_656 .
C50 C48 C49 10(4) 2_656 .
C51 C48 C47 31(5) 2_656 .
C50 C48 C47 110(4) 2_656 .
C49 C48 C47 120.0 . .
C51 C48 C52 13(4) 2_656 2_656
C50 C48 C52 92(5) 2_656 2_656
C49 C48 C52 101.8(11) . 2_656
C47 C48 C52 18.3(12) . 2_656
C50 C49 C48 84(10) 2_656 .
C50 C49 C50 37(10) 2_656 .
C48 C49 C50 120.0 . .
C50 C49 C51 62(10) 2_656 2_656
C48 C49 C51 22(3) . 2_656
C50 C49 C51 98(3) . 2_656
C50 C49 C49 43(10) 2_656 2_656
C48 C49 C49 126.53(17) . 2_656
C50 C49 C49 6.6(8) . 2_656
C51 C49 C49 105(3) 2_656 2_656
C49 C50 C50 137(10) 2_656 2_656
C49 C50 C48 87(10) 2_656 2_656
C50 C50 C48 136(3) 2_656 2_656
C49 C50 C51 109(10) 2_656 .
C50 C50 C51 113.39(16) 2_656 .
C48 C50 C51 23(3) 2_656 .
C49 C50 C49 130(10) 2_656 .
C50 C50 C49 6.7(10) 2_656 .
C48 C50 C49 143(3) 2_656 .
C51 C50 C49 120.0 . .
C48 C51 C47 132(9) 2_656 2_656
C48 C51 C52 162(6) 2_656 .
C47 C51 C52 30(3) 2_656 .
C48 C51 C50 78(6) 2_656 .
C47 C51 C50 150(3) 2_656 .
C52 C51 C50 120.0 . .
C48 C51 C49 69.5(12) 2_656 2_656
C47 C51 C49 159(8) 2_656 2_656
C52 C51 C49 129(6) . 2_656
C50 C51 C49 9(6) . 2_656
C48 C51 C52 176(10) 2_656 2_656
C47 C51 C52 47(2) 2_656 2_656
C52 C51 C52 16.7(8) . 2_656
C50 C51 C52 103.4(8) . 2_656
C49 C51 C52 112(6) 2_656 2_656
C52 C52 C47 163(7) 2_656 2_656
C52 C52 C47 9(5) 2_656 .
C47 C52 C47 160(4) 2_656 .
C52 C52 C51 126.2(8) 2_656 .
C47 C52 C51 41(5) 2_656 .
C47 C52 C51 120.0 . .
C52 C52 C51 37.1(19) 2_656 2_656
C47 C52 C51 130(3) 2_656 2_656
C47 C52 C51 30.4(16) . 2_656
C51 C52 C51 89.6(15) . 2_656
C52 C52 C48 131.2(18) 2_656 2_656
C47 C52 C48 36(3) 2_656 2_656
C47 C52 C48 125(2) . 2_656
C51 C52 C48 5(2) . 2_656
C51 C52 C48 94.7(7) 2_656 2_656
C52' C47' C47' 118(10) 2_656 2_656
C52' C47' C52' 121(10) 2_656 .
C47' C47' C52' 16(3) 2_656 .
C52' C47' C48' 104(10) 2_656 .
C47' C47' C48' 109.2(18) 2_656 .
C52' C47' C48' 120.0 . .
C52' C47' C51' 76(10) 2_656 2_656
C47' C47' C51' 139(4) 2_656 2_656
C52' C47' C51' 152(2) . 2_656
C48' C47' C51' 33(2) . 2_656
C51' C48' C50' 114(7) 2_656 2_656
C51' C48' C49' 162(6) 2_656 .
C50' C48' C49' 51(4) 2_656 .
C51' C48' C47' 76(4) 2_656 .
C50' C48' C47' 169(5) 2_656 .
C49' C48' C47' 120.0 . .
C51' C48' C52' 63(2) 2_656 2_656
C50' C48' C52' 174(10) 2_656 2_656
C49' C48' C52' 131(6) . 2_656
C47' C48' C52' 15(5) . 2_656
C51' C48' C49' 172(7) 2_656 2_656
C50' C48' C49' 59(3) 2_656 2_656
C49' C48' C49' 10(2) . 2_656
C47' C48' C49' 110.8(17) . 2_656
C52' C48' C49' 123(6) 2_656 2_656
C49' C49' C50' 154(10) 2_656 2_656
C49' C49' C50' 20(10) 2_656 .
C50' C49' C50' 157.6(18) 2_656 .
C49' C49' C48' 126(5) 2_656 .
C50' C49' C48' 38.1(8) 2_656 .
C50' C49' C48' 120.0 . .
C49' C49' C48' 44(5) 2_656 2_656
C50' C49' C48' 125.9(15) 2_656 2_656
C50' C49' C48' 32.1(18) . 2_656
C48' C49' C48' 87.9(18) . 2_656
C48' C50' C49' 91(5) 2_656 2_656
C48' C50' C49' 88(5) 2_656 .
C49' C50' C49' 6(4) 2_656 .
C48' C50' C51' 32(5) 2_656 .
C49' C50' C51' 122.3(10) 2_656 .
C49' C50' C51' 120.0 . .
C48' C51' C52' 86(3) 2_656 .
C48' C51' C50' 34(3) 2_656 .
C52' C51' C50' 120.0 . .
C48' C51' C47' 71(5) 2_656 2_656
C52' C51' C47' 17(3) . 2_656
C50' C51' C47' 105(2) . 2_656
C47' C52' C51' 86(10) 2_656 .
C47' C52' C47' 46(10) 2_656 .
C51' C52' C47' 120.0 . .
C47' C52' C48' 60(10) 2_656 2_656
C51' C52' C48' 31(3) . 2_656
C47' C52' C48' 89(3) . 2_656
C47' C52' C52' 46(10) 2_656 2_656
C51' C52' C52' 128.2(7) . 2_656
C47' C52' C52' 13(2) . 2_656
C48' C52' C52' 98(3) 2_656 2_656
C53 C53 C54 86(10) 2_655 .
C53 C53 C58 95(10) 2_655 .
C54 C53 C58 120.0 . .
C53 C53 C54 76(10) 2_655 2_655
C54 C53 C54 131(2) . 2_655
C58 C53 C54 23(3) . 2_655
C53 C53 C58 68(10) 2_655 2_655
C54 C53 C58 22(3) . 2_655
C58 C53 C58 106(2) . 2_655
C54 C53 C58 111(3) 2_655 2_655
C58 C54 C53 89(8) 2_655 .
C58 C54 C55 62(5) 2_655 .
C53 C54 C55 120.0 . .
C58 C54 C53 75(8) 2_655 2_655
C53 C54 C53 18(4) . 2_655
C55 C54 C53 119(2) . 2_655
C58 C54 C57 41(3) 2_655 2_655
C53 C54 C57 102(3) . 2_655
C55 C54 C57 24(3) . 2_655
C53 C54 C57 97(3) 2_655 2_655
C57 C55 C58 85(6) 2_655 2_655
C57 C55 C56 44(7) 2_655 .
C58 C55 C56 110(4) 2_655 .
C57 C55 C54 107(3) 2_655 .
C58 C55 C54 24(4) 2_655 .
C56 C55 C54 120.0 . .
C57 C55 C56 29(5) 2_655 2_655
C58 C55 C56 93(4) 2_655 2_655
C56 C55 C56 20(2) . 2_655
C54 C55 C56 107.6(15) . 2_655
C56 C56 C57 98(10) 2_655 2_655
C56 C56 C55 127(7) 2_655 .
C57 C56 C55 32(5) 2_655 .
C56 C56 C57 45(9) 2_655 .
C57 C56 C57 112(4) 2_655 .
C55 C56 C57 120.0 . .
C56 C56 C55 34(6) 2_655 2_655
C57 C56 C55 101(4) 2_655 2_655
C55 C56 C55 116.2(13) . 2_655
C57 C56 C55 15(4) . 2_655
C55 C57 C56 104(10) 2_655 2_655
C55 C57 C56 136(9) 2_655 .
C56 C57 C56 37(6) 2_655 .
C55 C57 C58 62(3) 2_655 .
C56 C57 C58 127(5) 2_655 .
C56 C57 C58 120.0 . .
C55 C57 C54 49(3) 2_655 2_655
C56 C57 C54 118(6) 2_655 2_655
C56 C57 C54 122(3) . 2_655
C58 C57 C54 16(3) . 2_655
C55 C57 C57 114(9) 2_655 2_655
C56 C57 C57 40(6) 2_655 2_655
C56 C57 C57 27.7(14) . 2_655
C58 C57 C57 96.45(13) . 2_655
C54 C57 C57 95(3) 2_655 2_655
C54 C58 C55 94(10) 2_655 2_655
C54 C58 C57 123(6) 2_655 .
C55 C58 C57 33(4) 2_655 .
C54 C58 C53 82(8) 2_655 .
C55 C58 C53 136(5) 2_655 .
C57 C58 C53 120.0 . .
C54 C58 C53 68(7) 2_655 2_655
C55 C58 C53 124(6) 2_655 2_655
C57 C58 C53 118(3) . 2_655
C53 C58 C53 17(3) . 2_655
C53' C53' C54' 149(6) 2_655 2_655
C53' C53' C58' 136.4(17) 2_655 .
C54' C53' C58' 17(4) 2_655 .
C53' C53' C54' 17(4) 2_655 .
C54' C53' C54' 134(2) 2_655 .
C58' C53' C54' 120.0 . .
C53' C53' C58' 30.1(15) 2_655 2_655
C54' C53' C58' 119.9(19) 2_655 2_655
C58' C53' C58' 106.3(9) . 2_655
C54' C53' C58' 14.9(12) . 2_655
C53' C53' C55' 120(2) 2_655 2_655
C54' C53' C55' 30(2) 2_655 2_655
C58' C53' C55' 18(3) . 2_655
C54' C53' C55' 104(2) . 2_655
C58' C53' C55' 90.0(16) 2_655 2_655
C58' C54' C53' 143(9) 2_655 2_655
C58' C54' C55' 23(9) 2_655 .
C53' C54' C55' 133.4(18) 2_655 .
C58' C54' C53' 133(4) 2_655 .
C53' C54' C53' 14(3) 2_655 .
C55' C54' C53' 120.0 . .
C58' C54' C57' 29(3) 2_655 2_655
C53' C54' C57' 118(4) 2_655 2_655
C55' C54' C57' 19(3) . 2_655
C53' C54' C57' 105(3) . 2_655
C58' C54' C54' 117(4) 2_655 2_655
C53' C54' C54' 29.3(19) 2_655 2_655
C55' C54' C54' 104.0(2) . 2_655
C53' C54' C54' 16.2(3) . 2_655
C57' C54' C54' 89(3) 2_655 2_655
C58' C55' C57' 122(10) 2_655 2_655
C58' C55' C56' 131(3) 2_655 .
C57' C55' C56' 36(9) 2_655 .
C58' C55' C54' 19(7) 2_655 .
C57' C55' C54' 125(5) 2_655 .
C56' C55' C54' 120.0 . .
C58' C55' C53' 32(4) 2_655 2_655
C57' C55' C53' 111(5) 2_655 2_655
C56' C55' C53' 103.5(14) . 2_655
C54' C55' C53' 16.6(14) . 2_655
C58' C55' C56' 112(4) 2_655 2_655
C57' C55' C56' 32(6) 2_655 2_655
C56' C55' C56' 21(2) . 2_655
C54' C55' C56' 104.4(16) . 2_655
C53' C55' C56' 88.1(19) 2_655 2_655
C57' C56' C56' 107(10) 2_655 2_655
C57' C56' C55' 30(5) 2_655 .
C56' C56' C55' 123(5) 2_655 .
C57' C56' C57' 125(5) 2_655 .
C56' C56' C57' 38(8) 2_655 .
C55' C56' C57' 120.0 . .
C57' C56' C58' 35(2) 2_655 2_655
C56' C56' C58' 107(5) 2_655 2_655
C55' C56' C58' 17.7(14) . 2_655
C57' C56' C58' 103.1(12) . 2_655
C57' C56' C55' 108(4) 2_655 2_655
C56' C56' C55' 36(4) 2_655 2_655
C55' C56' C55' 105.5(14) . 2_655
C57' C56' C55' 17(2) . 2_655
C58' C56' C55' 88.0(12) 2_655 2_655
C55' C57' C56' 114(10) 2_655 2_655
C55' C57' C58' 30(5) 2_655 .
C56' C57' C58' 124(4) 2_655 .
C55' C57' C56' 131(7) 2_655 .
C56' C57' C56' 35(6) 2_655 .
C58' C57' C56' 120.0 . .
C55' C57' C54' 36(4) 2_655 2_655
C56' C57' C54' 111(6) 2_655 2_655
C58' C57' C54' 13.7(17) . 2_655
C56' C57' C54' 106.6(15) . 2_655
C55' C57' C57' 110(8) 2_655 2_655
C56' C57' C57' 34(5) 2_655 2_655
C58' C57' C57' 102.5(4) . 2_655
C56' C57' C57' 20.9(19) . 2_655
C54' C57' C57' 88.8(19) 2_655 2_655
C54' C58' C55' 138(10) 2_655 2_655
C54' C58' C57' 137(4) 2_655 .
C55' C58' C57' 28(5) 2_655 .
C54' C58' C53' 20(6) 2_655 .
C55' C58' C53' 130(7) 2_655 .
C57' C58' C53' 120.0 . .
C54' C58' C53' 32(3) 2_655 2_655
C55' C58' C53' 118(7) 2_655 2_655
C57' C58' C53' 106.5(13) . 2_655
C53' C58' C53' 13.6(12) . 2_655
C54' C58' C56' 117(7) 2_655 2_655
C55' C58' C56' 31(3) 2_655 2_655
C57' C58' C56' 21(3) . 2_655
C53' C58' C56' 103(3) . 2_655
C53' C58' C56' 90(3) 2_655 2_655
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 N2 2.193(6) .
Ag1 C1 2.20(2) .
Ag1 N1 2.198(6) .
Ag1 C2' 2.23(2) .
Ag1 C2 2.24(2) .
Ag1 C1' 2.249(17) .
Ag2 C24' 2.15(2) .
Ag2 N4 2.202(6) .
Ag2 N3 2.206(6) .
Ag2 C25' 2.21(3) .
Ag2 C24 2.23(2) .
Ag2 C25 2.24(3) .
C6 F2 1.3199 .
C6 F1 1.3199 .
C6 F3 1.3202 .
C6 C3 1.520(8) .
C7 F4 1.3199 .
C7 F5 1.3201 .
C7 F6 1.3202 .
C7 C5 1.524(8) .
C14 F8 1.3198 .
C14 F9 1.3200 .
C14 F7 1.3201 .
C14 C10 1.501(8) .
C15 F10 1.3198 .
C15 F12 1.3201 .
C15 F11 1.3202 .
C15 C12 1.507(8) .
C22 F15 1.3198 .
C22 F14 1.3200 .
C22 F13 1.3202 .
C22 C18 1.498(8) .
C23 F16 1.3197 .
C23 F18 1.3198 .
C23 F17 1.3202 .
C23 C20 1.512(9) .
C6' F1' 1.3198 .
C6' F2' 1.3199 .
C6' F3' 1.3202 .
C6' C3 1.521(9) .
C7' F6' 1.3198 .
C7' F5' 1.3200 .
C7' F4' 1.3202 .
C7' C5 1.519(9) .
C14' F7' 1.3201 .
C14' F8' 1.3202 .
C14' F9' 1.3202 .
C14' C10 1.499(9) .
C15' F11' 1.3197 .
C15' F12' 1.3197 .
C15' F10' 1.3198 .
C15' C12 1.501(8) .
C22' F14' 1.3199 .
C22' F15' 1.3199 .
C22' F13' 1.3200 .
C22' C18 1.512(9) .
C23' F17' 1.3199 .
C23' F16' 1.3201 .
C23' F18' 1.3203 .
C23' C20 1.514(9) .
C6" F2" 1.3196 .
C6" F3" 1.3200 .
C6" F1" 1.3202 .
C6" C3 1.518(10) .
C7" F6" 1.3198 .
C7" F5" 1.3200 .
C7" F4" 1.3200 .
C7" C5 1.529(9) .
C14" F7" 1.3198 .
C14" F8" 1.3201 .
C14" F9" 1.3202 .
C14" C10 1.533(9) .
C15" F11" 1.3200 .
C15" F12" 1.3200 .
C15" F10" 1.3201 .
C15" C12 1.527(9) .
C22" F15" 1.3199 .
C22" F13" 1.3199 .
C22" F14" 1.3200 .
C22" C18 1.511(9) .
C23" F17" 1.3199 .
C23" F18" 1.3200 .
C23" F16" 1.3201 .
C23" C20 1.521(9) .
C29 F20 1.3199 .
C29 F21 1.3199 .
C29 F19 1.3201 .
C29 C26 1.518(8) .
C30 F24 1.3197 .
C30 F23 1.3200 .
C30 F22 1.3200 .
C30 C28 1.522(10) .
C37 F26 1.3199 .
C37 F27 1.3199 .
C37 F25 1.3201 .
C37 C33 1.522(8) .
C38 F29 1.3198 .
C38 F28 1.3199 .
C38 F30 1.3204 .
C38 C35 1.514(9) .
C45 F31 1.3199 .
C45 F33 1.3200 .
C45 F32 1.3203 .
C45 C41 1.492(8) .
C46 F35 1.3200 .
C46 F36 1.3201 .
C46 F34 1.3201 .
C46 C43 1.501(8) .
C29' F20' 1.3198 .
C29' F21' 1.3199 .
C29' F19' 1.3200 .
C29' C26 1.545(9) .
C30' F24' 1.3196 .
C30' F23' 1.3199 .
C30' F22' 1.3202 .
C30' C28 1.524(9) .
C37' F26' 1.3198 .
C37' F27' 1.3200 .
C37' F25' 1.3200 .
C37' C33 1.503(9) .
C38' F30' 1.3199 .
C38' F28' 1.3200 .
C38' F29' 1.3201 .
C38' C35 1.512(9) .
C45' F32' 1.3199 .
C45' F33' 1.3200 .
C45' F31' 1.3201 .
C45' C41 1.520(9) .
C46' F34' 1.3198 .
C46' F35' 1.3199 .
C46' F36' 1.3200 .
C46' C43 1.529(9) .
C29" F19" 1.3198 .
C29" F21" 1.3199 .
C29" F20" 1.3204 .
C29" C26 1.505(9) .
C30" F24" 1.3197 .
C30" F22" 1.3200 .
C30" F23" 1.3200 .
C30" C28 1.512(9) .
C37" F25" 1.3199 .
C37" F27" 1.3199 .
C37" F26" 1.3201 .
C37" C33 1.500(8) .
C38" F30" 1.3199 .
C38" F28" 1.3199 .
C38" F29" 1.3200 .
C38" C35 1.499(9) .
C45" F33" 1.3198 .
C45" F32" 1.3203 .
C45" F31" 1.3203 .
C45" C41 1.516(9) .
C46" F34" 1.3199 .
C46" F36" 1.3199 .
C46" F35" 1.3200 .
C46" C43 1.495(9) .
N1 C3 1.327(9) .
N1 C8 1.416(9) .
N2 C5 1.322(10) .
N2 C16 1.427(9) .
N3 C26 1.338(9) .
N3 C31 1.415(9) .
N4 C28 1.324(9) .
N4 C39 1.422(9) .
C1 C2 1.392(19) .
C24 C25 1.368(19) .
C1' C2' 1.395(18) .
C24' C25' 1.369(19) .
C3 C4 1.406(11) .
C4 C5 1.417(11) .
C8 C9 1.390(11) .
C8 C13 1.400(10) .
C9 C10 1.377(10) .
C10 C11 1.385(11) .
C11 C12 1.375(11) .
C12 C13 1.390(10) .
C16 C21 1.380(12) .
C16 C17 1.378(11) .
C17 C18 1.379(11) .
C18 C19 1.381(12) .
C19 C20 1.372(13) .
C20 C21 1.381(12) .
C26 C27 1.398(10) .
C27 C28 1.417(10) .
C31 C36 1.385(11) .
C31 C32 1.388(10) .
C32 C33 1.374(10) .
C33 C34 1.374(11) .
C34 C35 1.380(11) .
C35 C36 1.400(11) .
C39 C40 1.393(11) .
C39 C44 1.384(10) .
C40 C41 1.385(11) .
C41 C42 1.376(11) .
C42 C43 1.386(11) .
C43 C44 1.375(11) .
C47 C52 0.74(5) 2_656
C47 C51 0.964(9) 2_656
C47 C52 1.3898 .
C47 C48 1.3901 .
C48 C51 0.55(7) 2_656
C48 C50 1.38(11) 2_656
C48 C49 1.3898 .
C48 C52 1.92(3) 2_656
C49 C50 0.24(11) 2_656
C49 C50 1.3902 .
C49 C51 1.48(2) 2_656
C49 C49 1.55(16) 2_656
C50 C49 0.24(12) 2_656
C50 C50 1.21(15) 2_656
C50 C48 1.38(7) 2_656
C50 C51 1.3899 .
C51 C48 0.55(8) 2_656
C51 C47 0.96(6) 2_656
C51 C52 1.3899 .
C51 C49 1.48(4) 2_656
C51 C52 1.86(4) 2_656
C52 C52 0.66(4) 2_656
C52 C47 0.74(5) 2_656
C52 C51 1.86(7) 2_656
C52 C48 1.92(6) 2_656
C47' C52' 0.42(12) 2_656
C47' C47' 1.14(14) 2_656
C47' C52' 1.3900 .
C47' C48' 1.3901 .
C47' C51' 1.43(8) 2_656
C48' C51' 0.80(8) 2_656
C48' C50' 0.859(13) 2_656
C48' C49' 1.3900 .
C48' C52' 1.55(2) 2_656
C48' C49' 1.61(5) 2_656
C49' C49' 0.34(7) 2_656
C49' C50' 1.07(7) 2_656
C49' C50' 1.3898 .
C49' C48' 1.61(6) 2_656
C50' C48' 0.859(14) 2_656
C50' C49' 1.07(7) 2_656
C50' C51' 1.3899 .
C51' C48' 0.80(6) 2_656
C51' C52' 1.3898 .
C51' C47' 1.43(13) 2_656
C52' C47' 0.42(9) 2_656
C52' C48' 1.551(12) 2_656
C52' C52' 1.65(16) 2_656
C53 C53 0.45(8) 2_655
C53 C54 1.3898 .
C53 C58 1.3901 .
C53 C54 1.43(9) 2_655
C53 C58 1.49(6) 2_655
C54 C58 0.57(7) 2_655
C54 C55 1.3901 .
C54 C53 1.43(13) 2_655
C54 C57 1.77(3) 2_655
C55 C57 0.76(8) 2_655
C55 C58 1.23(4) 2_655
C55 C56 1.3898 .
C55 C56 2.01(12) 2_655
C56 C56 0.84(10) 2_655
C56 C57 1.00(9) 2_655
C56 C57 1.3901 .
C56 C55 2.01(7) 2_655
C57 C55 0.76(8) 2_655
C57 C56 1.00(13) 2_655
C57 C58 1.3901 .
C57 C54 1.77(3) 2_655
C57 C57 1.99(11) 2_655
C58 C54 0.57(9) 2_655
C58 C55 1.23(5) 2_655
C58 C53 1.49(11) 2_655
C53' C53' 0.65(6) 2_655
C53' C54' 0.79(4) 2_655
C53' C58' 1.3900 .
C53' C54' 1.3901 .
C53' C58' 1.91(5) 2_655
C53' C55' 2.02(4) 2_655
C54' C58' 0.67(4) 2_655
C54' C53' 0.79(6) 2_655
C54' C55' 1.3900 .
C54' C57' 1.937(16) 2_655
C54' C54' 2.02(5) 2_655
C55' C58' 0.82(4) 2_655
C55' C57' 0.77(6) 2_655
C55' C56' 1.3899 .
C55' C53' 2.02(5) 2_655
C55' C56' 1.98(10) 2_655
C56' C57' 0.89(11) 2_655
C56' C56' 0.84(10) 2_655
C56' C57' 1.3901 .
C56' C58' 2.02(4) 2_655
C56' C55' 1.98(6) 2_655
C57' C55' 0.77(4) 2_655
C57' C56' 0.89(12) 2_655
C57' C58' 1.3899 .
C57' C54' 1.937(16) 2_655
C57' C57' 2.03(12) 2_655
C58' C54' 0.67(4) 2_655
C58' C55' 0.82(3) 2_655
C58' C53' 1.91(5) 2_655
C58' C56' 2.02(7) 2_655
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
N2 Ag1 N1 C3 15.8(6) . .
C1 Ag1 N1 C3 -159.9(8) . .
C2' Ag1 N1 C3 -177.4(19) . .
C2 Ag1 N1 C3 -159.3(13) . .
C1' Ag1 N1 C3 -173.6(8) . .
N2 Ag1 N1 C8 -165.8(5) . .
C1 Ag1 N1 C8 18.5(9) . .
C2' Ag1 N1 C8 1(2) . .
C2 Ag1 N1 C8 19.1(14) . .
C1' Ag1 N1 C8 4.8(8) . .
C1 Ag1 N2 C5 156.4(16) . .
N1 Ag1 N2 C5 -13.9(6) . .
C2' Ag1 N2 C5 171.1(9) . .
C2 Ag1 N2 C5 163.4(9) . .
C1' Ag1 N2 C5 -179.4(10) . .
C1 Ag1 N2 C16 -24.1(17) . .
N1 Ag1 N2 C16 165.7(5) . .
C2' Ag1 N2 C16 -9.4(9) . .
C2 Ag1 N2 C16 -17.0(9) . .
C1' Ag1 N2 C16 0.1(11) . .
C24' Ag2 N3 C26 -155.3(9) . .
N4 Ag2 N3 C26 24.9(6) . .
C25' Ag2 N3 C26 -154.8(18) . .
C24 Ag2 N3 C26 -145.0(9) . .
C25 Ag2 N3 C26 -137(2) . .
C24' Ag2 N3 C31 26.4(9) . .
N4 Ag2 N3 C31 -153.3(5) . .
C25' Ag2 N3 C31 27.0(19) . .
C24 Ag2 N3 C31 36.8(9) . .
C25 Ag2 N3 C31 45(2) . .
C24' Ag2 N4 C28 155.3(18) . .
N3 Ag2 N4 C28 -25.3(6) . .
C25' Ag2 N4 C28 154.6(11) . .
C24 Ag2 N4 C28 138.2(12) . .
C25 Ag2 N4 C28 147.5(9) . .
C24' Ag2 N4 C39 -23.4(19) . .
N3 Ag2 N4 C39 156.1(5) . .
C25' Ag2 N4 C39 -24.1(11) . .
C24 Ag2 N4 C39 -40.4(13) . .
C25 Ag2 N4 C39 -31.2(10) . .
N2 Ag1 C1 C2 10(2) . .
N1 Ag1 C1 C2 179.5(12) . .
C2' Ag1 C1 C2 -8.9(16) . .
C1' Ag1 C1 C2 -51(3) . .
N2 Ag1 C2 C1 -175.3(11) . .
N1 Ag1 C2 C1 -1(2) . .
C2' Ag1 C2 C1 145(5) . .
C1' Ag1 C2 C1 24.1(14) . .
C24' Ag2 C24 C25 -131(5) . .
N4 Ag2 C24 C25 15(2) . .
N3 Ag2 C24 C25 174.9(14) . .
C25' Ag2 C24 C25 -14(2) . .
C24' Ag2 C25 C24 12.5(16) . .
N4 Ag2 C25 C24 -171.8(13) . .
N3 Ag2 C25 C24 -12(3) . .
C25' Ag2 C25 C24 48(6) . .
N2 Ag1 C1' C2' -15.1(18) . .
C1 Ag1 C1' C2' 125(3) . .
N1 Ag1 C1' C2' -177.7(12) . .
C2 Ag1 C1' C2' 16.4(18) . .
N2 Ag1 C2' C1' 171.2(11) . .
C1 Ag1 C2' C1' -17.0(12) . .
N1 Ag1 C2' C1' 5(3) . .
C2 Ag1 C2' C1' -46(4) . .
N4 Ag2 C24' C25' -1(3) . .
N3 Ag2 C24' C25' 179.6(16) . .
C24 Ag2 C24' C25' 49(4) . .
C25 Ag2 C24' C25' 9(2) . .
N4 Ag2 C25' C24' 179.5(14) . .
N3 Ag2 C25' C24' -1(3) . .
C24 Ag2 C25' C24' -17.5(18) . .
C25 Ag2 C25' C24' -138(8) . .
C8 N1 C3 C4 172.1(8) . .
Ag1 N1 C3 C4 -9.6(11) . .
C8 N1 C3 C6" -9.9(14) . .
Ag1 N1 C3 C6" 168.3(10) . .
C8 N1 C3 C6' -20.7(12) . .
Ag1 N1 C3 C6' 157.6(7) . .
C8 N1 C3 C6 -4.2(11) . .
Ag1 N1 C3 C6 174.1(5) . .
F2" C6" C3 N1 -23.1(17) . .
F3" C6" C3 N1 95.2(14) . .
F1" C6" C3 N1 -144.8(13) . .
F2" C6" C3 C4 155.1(12) . .
F3" C6" C3 C4 -86.6(14) . .
F1" C6" C3 C4 33.4(16) . .
F2" C6" C3 C6' 56(5) . .
F3" C6" C3 C6' 174(6) . .
F1" C6" C3 C6' -66(6) . .
F2" C6" C3 C6 -103(10) . .
F3" C6" C3 C6 15(10) . .
F1" C6" C3 C6 135(11) . .
F1' C6' C3 N1 -165.5(8) . .
F2' C6' C3 N1 -44.4(11) . .
F3' C6' C3 N1 75.4(11) . .
F1' C6' C3 C4 3.1(11) . .
F2' C6' C3 C4 124.2(9) . .
F3' C6' C3 C4 -116.0(9) . .
F1' C6' C3 C6" 88(6) . .
F2' C6' C3 C6" -151(6) . .
F3' C6' C3 C6" -31(5) . .
F1' C6' C3 C6 95(3) . .
F2' C6' C3 C6 -143(3) . .
F3' C6' C3 C6 -24(2) . .
F2 C6 C3 N1 -49.0(9) . .
F1 C6 C3 N1 -167.5(7) . .
F3 C6 C3 N1 70.3(9) . .
F2 C6 C3 C4 134.3(8) . .
F1 C6 C3 C4 15.8(10) . .
F3 C6 C3 C4 -106.4(8) . .
F2 C6 C3 C6" 54(10) . .
F1 C6 C3 C6" -65(10) . .
F3 C6 C3 C6" 173(10) . .
F2 C6 C3 C6' 40(2) . .
F1 C6 C3 C6' -79(3) . .
F3 C6 C3 C6' 159(3) . .
N1 C3 C4 C5 -6.6(15) . .
C6" C3 C4 C5 175.4(12) . .
C6' C3 C4 C5 -174.2(9) . .
C6 C3 C4 C5 169.9(9) . .
C16 N2 C5 C4 -174.3(8) . .
Ag1 N2 C5 C4 5.2(12) . .
C16 N2 C5 C7' 17.8(14) . .
Ag1 N2 C5 C7' -162.7(8) . .
C16 N2 C5 C7 -3.8(12) . .
Ag1 N2 C5 C7 175.6(5) . .
C16 N2 C5 C7" 17.0(12) . .
Ag1 N2 C5 C7" -163.5(7) . .
C3 C4 C5 N2 9.2(15) . .
C3 C4 C5 C7' 178.7(10) . .
C3 C4 C5 C7 -161.4(9) . .
C3 C4 C5 C7" 178.0(10) . .
F6' C7' C5 N2 -85.2(12) . .
F5' C7' C5 N2 155.6(11) . .
F4' C7' C5 N2 30.1(14) . .
F6' C7' C5 C4 105.3(11) . .
F5' C7' C5 C4 -13.8(14) . .
F4' C7' C5 C4 -139.4(10) . .
F6' C7' C5 C7 -10(2) . .
F5' C7' C5 C7 -129(3) . .
F4' C7' C5 C7 106(2) . .
F6' C7' C5 C7" -79(7) . .
F5' C7' C5 C7" 161(8) . .
F4' C7' C5 C7" 36(7) . .
F4 C7 C5 N2 55.4(9) . .
F5 C7 C5 N2 172.6(7) . .
F6 C7 C5 N2 -64.8(9) . .
F4 C7 C5 C4 -133.4(7) . .
F5 C7 C5 C4 -16.2(10) . .
F6 C7 C5 C4 106.4(8) . .
F4 C7 C5 C7' -60(2) . .
F5 C7 C5 C7' 57(2) . .
F6 C7 C5 C7' 179(3) . .
F4 C7 C5 C7" -39(2) . .
F5 C7 C5 C7" 79(2) . .
F6 C7 C5 C7" -159(2) . .
F6" C7" C5 N2 -62.7(13) . .
F5" C7" C5 N2 178.2(9) . .
F4" C7" C5 N2 57.5(12) . .
F6" C7" C5 C4 127.7(10) . .
F5" C7" C5 C4 8.6(12) . .
F4" C7" C5 C4 -112.1(11) . .
F6" C7" C5 C7' 123(8) . .
F5" C7" C5 C7' 4(7) . .
F4" C7" C5 C7' -117(7) . .
F6" C7" C5 C7 33.1(18) . .
F5" C7" C5 C7 -86(2) . .
F4" C7" C5 C7 153(3) . .
C3 N1 C8 C9 113.5(8) . .
Ag1 N1 C8 C9 -64.9(8) . .
C3 N1 C8 C13 -73.2(10) . .
Ag1 N1 C8 C13 108.4(7) . .
C13 C8 C9 C10 2.0(11) . .
N1 C8 C9 C10 175.5(7) . .
C8 C9 C10 C11 -2.4(12) . .
C8 C9 C10 C14' 179.7(10) . .
C8 C9 C10 C14 -179.5(7) . .
C8 C9 C10 C14" -177.4(8) . .
F7' C14' C10 C9 -171.8(11) . .
F8' C14' C10 C9 -52.1(14) . .
F9' C14' C10 C9 66.5(14) . .
F7' C14' C10 C11 10.3(16) . .
F8' C14' C10 C11 130.0(12) . .
F9' C14' C10 C11 -111.4(13) . .
F7' C14' C10 C14 21(15) . .
F8' C14' C10 C14 140(16) . .
F9' C14' C10 C14 -101(16) . .
F7' C14' C10 C14" 55(12) . .
F8' C14' C10 C14" 175(13) . .
F9' C14' C10 C14" -67(13) . .
F8 C14 C10 C9 -30.0(10) . .
F9 C14 C10 C9 90.6(9) . .
F7 C14 C10 C9 -149.7(8) . .
F8 C14 C10 C11 152.9(8) . .
F9 C14 C10 C11 -86.6(9) . .
F7 C14 C10 C11 33.1(10) . .
F8 C14 C10 C14' -17(15) . .
F9 C14 C10 C14' 103(16) . .
F7 C14 C10 C14' -137(16) . .
F8 C14 C10 C14" -99(19) . .
F9 C14 C10 C14" 22(19) . .
F7 C14 C10 C14" 141(20) . .
F7" C14" C10 C9 -126.5(10) . .
F8" C14" C10 C9 -6.2(13) . .
F9" C14" C10 C9 114.5(10) . .
F7" C14" C10 C11 58.5(12) . .
F8" C14" C10 C11 178.8(10) . .
F9" C14" C10 C11 -60.5(12) . .
F7" C14" C10 C14' -78(13) . .
F8" C14" C10 C14' 42(13) . .
F9" C14" C10 C14' 163(13) . .
F7" C14" C10 C14 -14(19) . .
F8" C14" C10 C14 106(19) . .
F9" C14" C10 C14 -133(20) . .
C9 C10 C11 C12 1.3(11) . .
C14' C10 C11 C12 179.1(10) . .
C14 C10 C11 C12 178.4(7) . .
C14" C10 C11 C12 176.2(8) . .
C10 C11 C12 C13 0.2(11) . .
C10 C11 C12 C15' 176.6(8) . .
C10 C11 C12 C15 179.7(7) . .
C10 C11 C12 C15" -171.9(8) . .
F11' C15' C12 C11 4.8(12) . .
F12' C15' C12 C11 122.9(9) . .
F10' C15' C12 C11 -119.1(10) . .
F11' C15' C12 C13 -178.8(9) . .
F12' C15' C12 C13 -60.7(11) . .
F10' C15' C12 C13 57.3(12) . .
F11' C15' C12 C15 -151(7) . .
F12' C15' C12 C15 -33(6) . .
F10' C15' C12 C15 85(6) . .
F11' C15' C12 C15" -126(3) . .
F12' C15' C12 C15" -8(3) . .
F10' C15' C12 C15" 110(3) . .
F10 C15 C12 C11 -91.3(9) . .
F12 C15 C12 C11 148.1(8) . .
F11 C15 C12 C11 27.2(10) . .
F10 C15 C12 C13 88.2(9) . .
F12 C15 C12 C13 -32.3(10) . .
F11 C15 C12 C13 -153.3(8) . .
F10 C15 C12 C15' -65(6) . .
F12 C15 C12 C15' 174(6) . .
F11 C15 C12 C15' 53(6) . .
F10 C15 C12 C15" 160(5) . .
F12 C15 C12 C15" 40(5) . .
F11 C15 C12 C15" -81(5) . .
F11" C15" C12 C11 47.8(12) . .
F12" C15" C12 C11 170.1(9) . .
F10" C15" C12 C11 -69.6(11) . .
F11" C15" C12 C13 -124.7(10) . .
F12" C15" C12 C13 -2.5(12) . .
F10" C15" C12 C13 117.9(10) . .
F11" C15" C12 C15' 103(3) . .
F12" C15" C12 C15' -135(3) . .
F10" C15" C12 C15' -14(3) . .
F11" C15" C12 C15 124(5) . .
F12" C15" C12 C15 -114(5) . .
F10" C15" C12 C15 6(5) . .
C11 C12 C13 C8 -0.5(11) . .
C15' C12 C13 C8 -176.7(8) . .
C15 C12 C13 C8 180.0(7) . .
C15" C12 C13 C8 172.2(8) . .
C9 C8 C13 C12 -0.6(11) . .
N1 C8 C13 C12 -174.0(7) . .
C5 N2 C16 C21 79.1(11) . .
Ag1 N2 C16 C21 -100.4(8) . .
C5 N2 C16 C17 -109.6(9) . .
Ag1 N2 C16 C17 70.9(8) . .
C21 C16 C17 C18 -1.2(13) . .
N2 C16 C17 C18 -172.7(8) . .
C16 C17 C18 C19 1.0(14) . .
C16 C17 C18 C22 -178.6(8) . .
C16 C17 C18 C22' -178.6(10) . .
C16 C17 C18 C22" 178.6(9) . .
F15 C22 C18 C19 -14.0(15) . .
F14 C22 C18 C19 -137.4(13) . .
F13 C22 C18 C19 105.1(13) . .
F15 C22 C18 C17 165.6(12) . .
F14 C22 C18 C17 42.1(14) . .
F13 C22 C18 C17 -75.3(14) . .
F15 C22 C18 C22' -13(100) . .
F14 C22 C18 C22' -136(100) . .
F13 C22 C18 C22' 106(100) . .
F15 C22 C18 C22" -152(10) . .
F14 C22 C18 C22" 84(10) . .
F13 C22 C18 C22" -33(10) . .
F14' C22' C18 C19 -174.2(16) . .
F15' C22' C18 C19 -53.4(19) . .
F13' C22' C18 C19 65.7(19) . .
F14' C22' C18 C17 5.3(18) . .
F15' C22' C18 C17 126.1(17) . .
F13' C22' C18 C17 -114.7(17) . .
F14' C22' C18 C22 7(100) . .
F15' C22' C18 C22 128(100) . .
F13' C22' C18 C22 -113(100) . .
F14' C22' C18 C22" 44(11) . .
F15' C22' C18 C22" 165(11) . .
F13' C22' C18 C22" -76(11) . .
F15" C22" C18 C19 17.9(17) . .
F13" C22" C18 C19 141.3(15) . .
F14" C22" C18 C19 -99.7(16) . .
F15" C22" C18 C17 -159.7(13) . .
F13" C22" C18 C17 -36.3(17) . .
F14" C22" C18 C17 82.6(15) . .
F15" C22" C18 C22 61(10) . .
F13" C22" C18 C22 -175(10) . .
F14" C22" C18 C22 -57(10) . .
F15" C22" C18 C22' 58(11) . .
F13" C22" C18 C22' -179(100) . .
F14" C22" C18 C22' -60(11) . .
C17 C18 C19 C20 -0.1(15) . .
C22 C18 C19 C20 179.4(10) . .
C22' C18 C19 C20 179.4(11) . .
C22" C18 C19 C20 -177.6(10) . .
C18 C19 C20 C21 -0.4(17) . .
C18 C19 C20 C23 167.6(11) . .
C18 C19 C20 C23' -174.7(11) . .
C18 C19 C20 C23" -176.0(12) . .
F16 C23 C20 C19 -125.0(13) . .
F18 C23 C20 C19 119.1(13) . .
F17 C23 C20 C19 1.9(17) . .
F16 C23 C20 C21 42.9(17) . .
F18 C23 C20 C21 -73.0(15) . .
F17 C23 C20 C21 169.8(12) . .
F16 C23 C20 C23' 150(4) . .
F18 C23 C20 C23' 34(3) . .
F17 C23 C20 C23' -83(4) . .
F16 C23 C20 C23" 106(4) . .
F18 C23 C20 C23" -10(3) . .
F17 C23 C20 C23" -128(4) . .
F17' C23' C20 C19 66.9(16) . .
F16' C23' C20 C19 -53.2(15) . .
F18' C23' C20 C19 -171.6(12) . .
F17' C23' C20 C21 -107.1(14) . .
F16' C23' C20 C21 132.8(13) . .
F18' C23' C20 C21 14.4(18) . .
F17' C23' C20 C23 170(4) . .
F16' C23' C20 C23 50(4) . .
F18' C23' C20 C23 -69(3) . .
F17' C23' C20 C23" -118(5) . .
F16' C23' C20 C23" 122(5) . .
F18' C23' C20 C23" 3(4) . .
F17" C23" C20 C19 19.9(18) . .
F18" C23" C20 C19 143.5(14) . .
F16" C23" C20 C19 -95.6(15) . .
F17" C23" C20 C21 -155.9(11) . .
F18" C23" C20 C21 -32.4(16) . .
F16" C23" C20 C21 88.5(13) . .
F17" C23" C20 C23 79(3) . .
F18" C23" C20 C23 -157(4) . .
F16" C23" C20 C23 -36(3) . .
F17" C23" C20 C23' 14(4) . .
F18" C23" C20 C23' 138(5) . .
F16" C23" C20 C23' -101(4) . .
C19 C20 C21 C16 0.2(17) . .
C23 C20 C21 C16 -167.4(11) . .
C23' C20 C21 C16 173.8(12) . .
C23" C20 C21 C16 176.4(10) . .
C17 C16 C21 C20 0.7(14) . .
N2 C16 C21 C20 172.0(9) . .
C31 N3 C26 C27 166.0(7) . .
Ag2 N3 C26 C27 -12.0(10) . .
C31 N3 C26 C29" -20.3(12) . .
Ag2 N3 C26 C29" 161.6(8) . .
C31 N3 C26 C29 -17.9(11) . .
Ag2 N3 C26 C29 164.1(6) . .
C31 N3 C26 C29' -9.3(13) . .
Ag2 N3 C26 C29' 172.7(9) . .
F19" C29" C26 N3 97.3(11) . .
F21" C29" C26 N3 -25.5(13) . .
F20" C29" C26 N3 -146.0(10) . .
F19" C29" C26 C27 -88.5(12) . .
F21" C29" C26 C27 148.7(10) . .
F20" C29" C26 C27 28.2(13) . .
F19" C29" C26 C29 -12(18) . .
F21" C29" C26 C29 -135(19) . .
F20" C29" C26 C29 105(19) . .
F19" C29" C26 C29' -18(5) . .
F21" C29" C26 C29' -141(5) . .
F20" C29" C26 C29' 98(5) . .
F20 C29 C26 N3 -162.6(8) . .
F21 C29 C26 N3 -42.4(9) . .
F19 C29 C26 N3 75.8(10) . .
F20 C29 C26 C27 13.9(10) . .
F21 C29 C26 C27 134.1(7) . .
F19 C29 C26 C27 -107.8(8) . .
F20 C29 C26 C29" -91(19) . .
F21 C29 C26 C29" 29(19) . .
F19 C29 C26 C29" 148(19) . .
F20 C29 C26 C29' 81(6) . .
F21 C29 C26 C29' -159(7) . .
F19 C29 C26 C29' -41(6) . .
F20' C29' C26 N3 -165.4(11) . .
F21' C29' C26 N3 -45.3(14) . .
F19' C29' C26 N3 75.5(15) . .
F20' C29' C26 C27 18.7(13) . .
F21' C29' C26 C27 138.8(11) . .
F19' C29' C26 C27 -100.4(14) . .
F20' C29' C26 C29" -96(5) . .
F21' C29' C26 C29" 24(5) . .
F19' C29' C26 C29" 145(5) . .
F20' C29' C26 C29 -97(7) . .
F21' C29' C26 C29 23(6) . .
F19' C29' C26 C29 143(7) . .
N3 C26 C27 C28 -13.6(13) . .
C29" C26 C27 C28 172.7(10) . .
C29 C26 C27 C28 170.2(8) . .
C29' C26 C27 C28 162.1(10) . .
C39 N4 C28 C27 -168.6(7) . .
Ag2 N4 C28 C27 12.8(10) . .
C39 N4 C28 C30" 19.4(10) . .
Ag2 N4 C28 C30" -159.2(5) . .
C39 N4 C28 C30 7.7(14) . .
Ag2 N4 C28 C30 -170.8(10) . .
C39 N4 C28 C30' 4.7(12) . .
Ag2 N4 C28 C30' -173.8(7) . .
C26 C27 C28 N4 13.2(13) . .
C26 C27 C28 C30" -174.8(8) . .
C26 C27 C28 C30 -163.3(11) . .
C26 C27 C28 C30' -160.6(9) . .
F24" C30" C28 N4 41.2(9) . .
F22" C30" C28 N4 163.9(7) . .
F23" C30" C28 N4 -77.9(9) . .
F24" C30" C28 C27 -131.5(7) . .
F22" C30" C28 C27 -8.8(9) . .
F23" C30" C28 C27 109.4(8) . .
F24" C30" C28 C30 153(4) . .
F22" C30" C28 C30 -84(4) . .
F23" C30" C28 C30 34(4) . .
F24" C30" C28 C30' 153(3) . .
F22" C30" C28 C30' -84(3) . .
F23" C30" C28 C30' 34(3) . .
F24 C30 C28 N4 27.2(16) . .
F23 C30 C28 N4 -94.6(13) . .
F22 C30 C28 N4 148.0(11) . .
F24 C30 C28 C27 -156.1(11) . .
F23 C30 C28 C27 82.2(13) . .
F22 C30 C28 C27 -35.3(12) . .
F24 C30 C28 C30" -47(4) . .
F23 C30 C28 C30" -168(5) . .
F22 C30 C28 C30" 74(4) . .
F24 C30 C28 C30' 134(18) . .
F23 C30 C28 C30' 12(17) . .
F22 C30 C28 C30' -105(18) . .
F24' C30' C28 N4 46.2(10) . .
F23' C30' C28 N4 -72.1(11) . .
F22' C30' C28 N4 165.5(9) . .
F24' C30' C28 C27 -139.7(9) . .
F23' C30' C28 C27 102.0(10) . .
F22' C30' C28 C27 -20.4(13) . .
F24' C30' C28 C30" -29(3) . .
F23' C30' C28 C30" -147(3) . .
F22' C30' C28 C30" 90(3) . .
F24' C30' C28 C30 -29(18) . .
F23' C30' C28 C30 -147(18) . .
F22' C30' C28 C30 91(18) . .
C26 N3 C31 C36 -64.0(10) . .
Ag2 N3 C31 C36 114.2(7) . .
C26 N3 C31 C32 125.1(8) . .
Ag2 N3 C31 C32 -56.7(8) . .
C36 C31 C32 C33 1.5(12) . .
N3 C31 C32 C33 172.7(7) . .
C31 C32 C33 C34 -1.3(13) . .
C31 C32 C33 C37" 176.1(8) . .
C31 C32 C33 C37' -170.7(9) . .
C31 C32 C33 C37 178.3(7) . .
F25" C37" C33 C32 -86.7(11) . .
F27" C37" C33 C32 151.2(9) . .
F26" C37" C33 C32 32.6(11) . .
F25" C37" C33 C34 90.9(10) . .
F27" C37" C33 C34 -31.2(11) . .
F26" C37" C33 C34 -149.8(9) . .
F25" C37" C33 C37' -177(4) . .
F27" C37" C33 C37' 61(4) . .
F26" C37" C33 C37' -58(4) . .
F25" C37" C33 C37 -120(9) . .
F27" C37" C33 C37 118(9) . .
F26" C37" C33 C37 -1(9) . .
F26' C37' C33 C32 -43.8(13) . .
F27' C37' C33 C32 76.1(13) . .
F25' C37' C33 C32 -161.9(10) . .
F26' C37' C33 C34 146.3(10) . .
F27' C37' C33 C34 -93.8(12) . .
F25' C37' C33 C34 28.3(13) . .
F26' C37' C33 C37" 52(4) . .
F27' C37' C33 C37" 172(4) . .
F25' C37' C33 C37" -66(4) . .
F26' C37' C33 C37 35(4) . .
F27' C37' C33 C37 155(4) . .
F25' C37' C33 C37 -83(4) . .
F26 C37 C33 C32 -1.5(10) . .
F27 C37 C33 C32 119.6(8) . .
F25 C37 C33 C32 -122.0(8) . .
F26 C37 C33 C34 178.2(8) . .
F27 C37 C33 C34 -60.7(10) . .
F25 C37 C33 C34 57.7(10) . .
F26 C37 C33 C37" 146(9) . .
F27 C37 C33 C37" -93(9) . .
F25 C37 C33 C37" 26(9) . .
F26 C37 C33 C37' -108(4) . .
F27 C37 C33 C37' 13(4) . .
F25 C37 C33 C37' 131(4) . .
C32 C33 C34 C35 1.3(13) . .
C37" C33 C34 C35 -176.2(8) . .
C37' C33 C34 C35 171.1(9) . .
C37 C33 C34 C35 -178.3(8) . .
C33 C34 C35 C36 -1.6(13) . .
C33 C34 C35 C38" -168.4(9) . .
C33 C34 C35 C38' 172.3(9) . .
C33 C34 C35 C38 -174.5(9) . .
F30" C38" C35 C34 102.5(12) . .
F28" C38" C35 C34 -136.4(11) . .
F29" C38" C35 C34 -20.4(14) . .
F30" C38" C35 C36 -64.9(12) . .
F28" C38" C35 C36 56.1(11) . .
F29" C38" C35 C36 172.2(9) . .
F30" C38" C35 C38' -171(4) . .
F28" C38" C35 C38' -50(3) . .
F29" C38" C35 C38' 66(3) . .
F30" C38" C35 C38 -171(9) . .
F28" C38" C35 C38 -50(8) . .
F29" C38" C35 C38 66(8) . .
F30' C38' C35 C34 112.3(10) . .
F28' C38' C35 C34 -127.6(10) . .
F29' C38' C35 C34 -5.3(12) . .
F30' C38' C35 C36 -73.7(11) . .
F28' C38' C35 C36 46.4(13) . .
F29' C38' C35 C36 168.6(9) . .
F30' C38' C35 C38" 9(3) . .
F28' C38' C35 C38" 129(3) . .
F29' C38' C35 C38" -109(3) . .
F30' C38' C35 C38 8(3) . .
F28' C38' C35 C38 129(4) . .
F29' C38' C35 C38 -109(4) . .
F29 C38 C35 C34 -44.2(12) . .
F28 C38 C35 C34 -165.2(10) . .
F30 C38 C35 C34 75.0(12) . .
F29 C38 C35 C36 142.6(10) . .
F28 C38 C35 C36 21.7(13) . .
F30 C38 C35 C36 -98.2(11) . .
F29 C38 C35 C38" -141(8) . .
F28 C38 C35 C38" 98(8) . .
F30 C38 C35 C38" -22(8) . .
F29 C38 C35 C38' 39(4) . .
F28 C38 C35 C38' -82(4) . .
F30 C38 C35 C38' 158(4) . .
C32 C31 C36 C35 -1.8(12) . .
N3 C31 C36 C35 -172.8(7) . .
C34 C35 C36 C31 1.8(13) . .
C38" C35 C36 C31 169.3(9) . .
C38' C35 C36 C31 -172.0(9) . .
C38 C35 C36 C31 175.0(9) . .
C28 N4 C39 C40 -113.5(8) . .
Ag2 N4 C39 C40 65.1(8) . .
C28 N4 C39 C44 73.3(10) . .
Ag2 N4 C39 C44 -108.1(7) . .
C44 C39 C40 C41 -1.6(11) . .
N4 C39 C40 C41 -174.9(7) . .
C39 C40 C41 C42 1.2(13) . .
C39 C40 C41 C45 -178.5(7) . .
C39 C40 C41 C45" 177.1(10) . .
C39 C40 C41 C45' -173.9(10) . .
F31 C45 C41 C42 116.7(10) . .
F33 C45 C41 C42 -3.9(12) . .
F32 C45 C41 C42 -124.7(10) . .
F31 C45 C41 C40 -63.6(11) . .
F33 C45 C41 C40 175.9(9) . .
F32 C45 C41 C40 55.1(11) . .
F31 C45 C41 C45" 2(11) . .
F33 C45 C41 C45" -118(11) . .
F32 C45 C41 C45" 121(11) . .
F31 C45 C41 C45' -172(11) . .
F33 C45 C41 C45' 68(11) . .
F32 C45 C41 C45' -53(11) . .
F33" C45" C41 C42 19.9(18) . .
F32" C45" C41 C42 -96.6(15) . .
F31" C45" C41 C42 145.5(14) . .
F33" C45" C41 C40 -155.8(13) . .
F32" C45" C41 C40 87.6(15) . .
F31" C45" C41 C40 -30.2(18) . .
F33" C45" C41 C45 88(11) . .
F32" C45" C41 C45 -29(10) . .
F31" C45" C41 C45 -146(11) . .
F33" C45" C41 C45' 91(6) . .
F32" C45" C41 C45' -26(5) . .
F31" C45" C41 C45' -143(6) . .
F32' C45' C41 C42 -152.6(13) . .
F33' C45' C41 C42 -30.6(16) . .
F31' C45' C41 C42 87.9(15) . .
F32' C45' C41 C40 22.6(17) . .
F33' C45' C41 C40 144.6(13) . .
F31' C45' C41 C40 -96.9(15) . .
F32' C45' C41 C45 97(11) . .
F33' C45' C41 C45 -141(12) . .
F31' C45' C41 C45 -23(11) . .
F32' C45' C41 C45" 94(6) . .
F33' C45' C41 C45" -144(6) . .
F31' C45' C41 C45" -26(5) . .
C40 C41 C42 C43 -0.4(13) . .
C45 C41 C42 C43 179.4(8) . .
C45" C41 C42 C43 -175.9(11) . .
C45' C41 C42 C43 174.8(10) . .
C41 C42 C43 C44 -0.2(13) . .
C41 C42 C43 C46" 172.9(10) . .
C41 C42 C43 C46 179.6(8) . .
C41 C42 C43 C46' -174.3(9) . .
F34" C46" C43 C44 -175.6(10) . .
F36" C46" C43 C44 62.9(14) . .
F35" C46" C43 C44 -56.4(13) . .
F34" C46" C43 C42 11.2(15) . .
F36" C46" C43 C42 -110.4(12) . .
F35" C46" C43 C42 130.3(12) . .
F34" C46" C43 C46 -57(6) . .
F36" C46" C43 C46 -179(100) . .
F35" C46" C43 C46 62(6) . .
F34" C46" C43 C46' -83(4) . .
F36" C46" C43 C46' 155(4) . .
F35" C46" C43 C46' 36(4) . .
F35 C46 C43 C44 -89.8(9) . .
F36 C46 C43 C44 30.0(10) . .
F34 C46 C43 C44 150.4(8) . .
F35 C46 C43 C42 90.4(9) . .
F36 C46 C43 C42 -149.8(8) . .
F34 C46 C43 C42 -29.3(10) . .
F35 C46 C43 C46" -155(7) . .
F36 C46 C43 C46" -35(6) . .
F34 C46 C43 C46" 86(7) . .
F35 C46 C43 C46' -28(6) . .
F36 C46 C43 C46' 92(6) . .
F34 C46 C43 C46' -148(6) . .
F34' C46' C43 C44 121.5(10) . .
F35' C46' C43 C44 -120.6(10) . .
F36' C46' C43 C44 1.4(13) . .
F34' C46' C43 C42 -64.2(12) . .
F35' C46' C43 C42 53.8(13) . .
F36' C46' C43 C42 175.8(10) . .
F34' C46' C43 C46" 28(4) . .
F35' C46' C43 C46" 146(4) . .
F36' C46' C43 C46" -92(4) . .
F34' C46' C43 C46 0(6) . .
F35' C46' C43 C46 118(6) . .
F36' C46' C43 C46 -120(6) . .
C42 C43 C44 C39 -0.2(12) . .
C46" C43 C44 C39 -173.4(9) . .
C46 C43 C44 C39 -179.9(7) . .
C46' C43 C44 C39 174.2(8) . .
C40 C39 C44 C43 1.0(11) . .
N4 C39 C44 C43 174.3(7) . .
C52 C47 C48 C51 2(11) 2_656 2_656
C52 C47 C48 C51 -5(11) . 2_656
C52 C47 C48 C50 8(10) 2_656 2_656
C51 C47 C48 C50 6(9) 2_656 2_656
C52 C47 C48 C50 1(4) . 2_656
C52 C47 C48 C49 7(7) 2_656 .
C51 C47 C48 C49 5(11) 2_656 .
C52 C47 C48 C49 0.0 . .
C51 C47 C48 C52 -2(11) 2_656 2_656
C52 C47 C48 C52 -7(7) . 2_656
C51 C48 C49 C50 9(20) 2_656 2_656
C47 C48 C49 C50 6(23) . 2_656
C52 C48 C49 C50 8(24) 2_656 2_656
C51 C48 C49 C50 3(6) 2_656 .
C50 C48 C49 C50 -6(23) 2_656 .
C47 C48 C49 C50 0.0 . .
C52 C48 C49 C50 2(2) 2_656 .
C50 C48 C49 C51 -9(20) 2_656 2_656
C47 C48 C49 C51 -3(6) . 2_656
C52 C48 C49 C51 -1(5) 2_656 2_656
C51 C48 C49 C49 4(7) 2_656 2_656
C50 C48 C49 C49 -5(19) 2_656 2_656
C47 C48 C49 C49 1(5) . 2_656
C52 C48 C49 C49 4(7) 2_656 2_656
C50 C49 C50 C49 159(74) 2_656 2_656
C48 C49 C50 C49 170(38) . 2_656
C51 C49 C50 C49 171(38) 2_656 2_656
C48 C49 C50 C50 11(39) . 2_656
C51 C49 C50 C50 12(38) 2_656 2_656
C49 C49 C50 C50 -159(74) 2_656 2_656
C50 C49 C50 C48 -11(36) 2_656 2_656
C48 C49 C50 C48 -1(7) . 2_656
C51 C49 C50 C48 0(7) 2_656 2_656
C49 C49 C50 C48 -171(43) 2_656 2_656
C50 C49 C50 C51 -11(39) 2_656 .
C48 C49 C50 C51 0.0 . .
C51 C49 C50 C51 1(2) 2_656 .
C49 C49 C50 C51 -170(38) 2_656 .
C49 C50 C51 C48 10(22) 2_656 2_656
C50 C50 C51 C48 -180(14) 2_656 2_656
C49 C50 C51 C48 -179(11) . 2_656
C49 C50 C51 C47 -179(100) 2_656 2_656
C50 C50 C51 C47 -9(11) 2_656 2_656
C48 C50 C51 C47 171(16) 2_656 2_656
C49 C50 C51 C47 -8(9) . 2_656
C49 C50 C51 C52 -172(30) 2_656 .
C50 C50 C51 C52 -1(5) 2_656 .
C48 C50 C51 C52 179(11) 2_656 .
C49 C50 C51 C52 0.0 . .
C50 C50 C51 C49 170(34) 2_656 2_656
C48 C50 C51 C49 -10(22) 2_656 2_656
C49 C50 C51 C49 172(30) . 2_656
C49 C50 C51 C52 -174(29) 2_656 2_656
C50 C50 C51 C52 -4(6) 2_656 2_656
C48 C50 C51 C52 176(11) 2_656 2_656
C49 C50 C51 C52 -2(3) . 2_656
C51 C47 C52 C52 135(36) 2_656 2_656
C48 C47 C52 C52 136(34) . 2_656
C52 C47 C52 C47 -121(52) 2_656 2_656
C51 C47 C52 C47 13(17) 2_656 2_656
C48 C47 C52 C47 15(18) . 2_656
C52 C47 C52 C51 -136(34) 2_656 .
C51 C47 C52 C51 -2(4) 2_656 .
C48 C47 C52 C51 0.0 . .
C52 C47 C52 C51 -135(36) 2_656 2_656
C48 C47 C52 C51 2(4) . 2_656
C52 C47 C52 C48 -136(35) 2_656 2_656
C51 C47 C52 C48 -1(5) 2_656 2_656
C48 C47 C52 C48 0(4) . 2_656
C48 C51 C52 C52 168(36) 2_656 2_656
C47 C51 C52 C52 165(16) 2_656 2_656
C50 C51 C52 C52 -8(9) . 2_656
C49 C51 C52 C52 -9(12) 2_656 2_656
C48 C51 C52 C47 3(33) 2_656 2_656
C50 C51 C52 C47 -172(8) . 2_656
C49 C51 C52 C47 -174(9) 2_656 2_656
C52 C51 C52 C47 -165(16) 2_656 2_656
C48 C51 C52 C47 176(35) 2_656 .
C47 C51 C52 C47 172(8) 2_656 .
C50 C51 C52 C47 0.0 . .
C49 C51 C52 C47 -2(6) 2_656 .
C52 C51 C52 C47 8(9) 2_656 .
C48 C51 C52 C51 175(35) 2_656 2_656
C47 C51 C52 C51 172(9) 2_656 2_656
C50 C51 C52 C51 -0.8(18) . 2_656
C49 C51 C52 C51 -2(6) 2_656 2_656
C52 C51 C52 C51 7(8) 2_656 2_656
C47 C51 C52 C48 -3(33) 2_656 2_656
C50 C51 C52 C48 -176(35) . 2_656
C49 C51 C52 C48 -177(100) 2_656 2_656
C52 C51 C52 C48 -168(36) 2_656 2_656
C52' C47' C48' C51' 32(13) 2_656 2_656
C47' C47' C48' C51' 159(12) 2_656 2_656
C52' C47' C48' C51' 172(9) . 2_656
C52' C47' C48' C50' -167(51) 2_656 2_656
C47' C47' C48' C50' -40(44) 2_656 2_656
C52' C47' C48' C50' -27(44) . 2_656
C51' C47' C48' C50' 161(52) 2_656 2_656
C52' C47' C48' C49' -139(16) 2_656 .
C47' C47' C48' C49' -13(5) 2_656 .
C52' C47' C48' C49' 0.0 . .
C51' C47' C48' C49' -172(9) 2_656 .
C47' C47' C48' C52' 127(17) 2_656 2_656
C52' C47' C48' C52' 139(16) . 2_656
C51' C47' C48' C52' -32(13) 2_656 2_656
C52' C47' C48' C49' -143(16) 2_656 2_656
C47' C47' C48' C49' -17(6) 2_656 2_656
C52' C47' C48' C49' -4(3) . 2_656
C51' C47' C48' C49' -176(11) 2_656 2_656
C51' C48' C49' C49' -175(38) 2_656 2_656
C50' C48' C49' C49' 151(27) 2_656 2_656
C47' C48' C49' C49' -22(17) . 2_656
C52' C48' C49' C49' -36(18) 2_656 2_656
C51' C48' C49' C50' 34(18) 2_656 2_656
C47' C48' C49' C50' -174(11) . 2_656
C52' C48' C49' C50' 173(13) 2_656 2_656
C49' C48' C49' C50' -151(27) 2_656 2_656
C51' C48' C49' C50' -152(27) 2_656 .
C50' C48' C49' C50' 174(11) 2_656 .
C47' C48' C49' C50' 0.0 . .
C52' C48' C49' C50' -13(5) 2_656 .
C49' C48' C49' C50' 22(17) 2_656 .
C51' C48' C49' C48' -151(26) 2_656 2_656
C50' C48' C49' C48' 175(11) 2_656 2_656
C47' C48' C49' C48' 1.7(19) . 2_656
C52' C48' C49' C48' -11(5) 2_656 2_656
C49' C48' C49' C48' 24(17) 2_656 2_656
C49' C49' C50' C48' 117(23) 2_656 2_656
C50' C49' C50' C48' 13(18) 2_656 2_656
C48' C49' C50' C48' 3(4) . 2_656
C50' C49' C50' C49' -103(37) 2_656 2_656
C48' C49' C50' C49' -113(21) . 2_656
C48' C49' C50' C49' -117(23) 2_656 2_656
C49' C49' C50' C51' 113(22) 2_656 .
C50' C49' C50' C51' 10(17) 2_656 .
C48' C49' C50' C51' 0.0 . .
C48' C49' C50' C51' -3(4) 2_656 .
C49' C50' C51' C48' 13(7) 2_656 2_656
C49' C50' C51' C48' 6(7) . 2_656
C48' C50' C51' C52' -6(7) 2_656 .
C49' C50' C51' C52' 7(5) 2_656 .
C49' C50' C51' C52' 0.0 . .
C48' C50' C51' C47' 4(6) 2_656 2_656
C49' C50' C51' C47' 16(6) 2_656 2_656
C49' C50' C51' C47' 10(3) . 2_656
C48' C51' C52' C47' 30(9) 2_656 2_656
C50' C51' C52' C47' 34(9) . 2_656
C48' C51' C52' C47' -3(4) 2_656 .
C50' C51' C52' C47' 0.0 . .
C47' C51' C52' C47' -34(9) 2_656 .
C50' C51' C52' C48' 3(4) . 2_656
C47' C51' C52' C48' -30(9) 2_656 2_656
C48' C51' C52' C52' 8(5) 2_656 2_656
C50' C51' C52' C52' 12(4) . 2_656
C47' C51' C52' C52' -22(6) 2_656 2_656
C52' C47' C52' C47' 83(21) 2_656 2_656
C48' C47' C52' C47' -50(13) . 2_656
C51' C47' C52' C47' -40(13) 2_656 2_656
C52' C47' C52' C51' 133(11) 2_656 .
C47' C47' C52' C51' 50(13) 2_656 .
C48' C47' C52' C51' 0.0 . .
C51' C47' C52' C51' 10(10) 2_656 .
C52' C47' C52' C48' 131(12) 2_656 2_656
C47' C47' C52' C48' 48(12) 2_656 2_656
C48' C47' C52' C48' -1.8(19) . 2_656
C51' C47' C52' C48' 8(11) 2_656 2_656
C47' C47' C52' C52' -83(21) 2_656 2_656
C48' C47' C52' C52' -133(11) . 2_656
C51' C47' C52' C52' -123(21) 2_656 2_656
C53 C53 C54 C58 36(7) 2_655 2_655
C58 C53 C54 C58 -57(4) . 2_655
C54 C53 C54 C58 -31(6) 2_655 2_655
C53 C53 C54 C55 93(7) 2_655 .
C58 C53 C54 C55 0.0 . .
C54 C53 C54 C55 25(5) 2_655 .
C58 C53 C54 C55 57(4) 2_655 .
C58 C53 C54 C53 -93(7) . 2_655
C54 C53 C54 C53 -67(8) 2_655 2_655
C58 C53 C54 C53 -36(7) 2_655 2_655
C53 C53 C54 C57 75(8) 2_655 2_655
C58 C53 C54 C57 -18(3) . 2_655
C54 C53 C54 C57 8(6) 2_655 2_655
C58 C53 C54 C57 39(4) 2_655 2_655
C58 C54 C55 C57 24(12) 2_655 2_655
C53 C54 C55 C57 -47(9) . 2_655
C53 C54 C55 C57 -26(11) 2_655 2_655
C53 C54 C55 C58 -71(8) . 2_655
C53 C54 C55 C58 -50(6) 2_655 2_655
C57 C54 C55 C58 -24(12) 2_655 2_655
C58 C54 C55 C56 71(8) 2_655 .
C53 C54 C55 C56 0.0 . .
C53 C54 C55 C56 21(4) 2_655 .
C57 C54 C55 C56 47(9) 2_655 .
C58 C54 C55 C56 55(9) 2_655 2_655
C53 C54 C55 C56 -17(4) . 2_655
C53 C54 C55 C56 4(6) 2_655 2_655
C57 C54 C55 C56 30(6) 2_655 2_655
C57 C55 C56 C56 30(5) 2_655 2_655
C58 C55 C56 C56 -30(10) 2_655 2_655
C54 C55 C56 C56 -54(10) . 2_655
C58 C55 C56 C57 -60(7) 2_655 2_655
C54 C55 C56 C57 -84(7) . 2_655
C56 C55 C56 C57 -30(5) 2_655 2_655
C57 C55 C56 C57 84(7) 2_655 .
C58 C55 C56 C57 24(3) 2_655 .
C54 C55 C56 C57 0.0 . .
C56 C55 C56 C57 54(10) 2_655 .
C57 C55 C56 C55 67(6) 2_655 2_655
C58 C55 C56 C55 8(5) 2_655 2_655
C54 C55 C56 C55 -17(4) . 2_655
C56 C55 C56 C55 38(7) 2_655 2_655
C56 C56 C57 C55 34(8) 2_655 2_655
C57 C56 C57 C55 -45(5) 2_655 2_655
C55 C56 C57 C55 -80(3) . 2_655
C57 C56 C57 C56 -79(11) 2_655 2_655
C55 C56 C57 C56 -114(8) . 2_655
C55 C56 C57 C56 -34(8) 2_655 2_655
C56 C56 C57 C58 114(8) 2_655 .
C57 C56 C57 C58 35(5) 2_655 .
C55 C56 C57 C58 0.0 . .
C55 C56 C57 C58 80(3) 2_655 .
C56 C56 C57 C54 96(10) 2_655 2_655
C57 C56 C57 C54 17(6) 2_655 2_655
C55 C56 C57 C54 -18(4) . 2_655
C55 C56 C57 C54 62(4) 2_655 2_655
C56 C56 C57 C57 79(11) 2_655 2_655
C55 C56 C57 C57 -35(5) . 2_655
C55 C56 C57 C57 45(5) 2_655 2_655
C55 C57 C58 C54 28(15) 2_655 2_655
C56 C57 C58 C54 -58(16) 2_655 2_655
C56 C57 C58 C54 -101(12) . 2_655
C57 C57 C58 C54 -86(12) 2_655 2_655
C56 C57 C58 C55 -86(12) 2_655 2_655
C56 C57 C58 C55 -130(10) . 2_655
C54 C57 C58 C55 -28(15) 2_655 2_655
C57 C57 C58 C55 -114(11) 2_655 2_655
C55 C57 C58 C53 130(10) 2_655 .
C56 C57 C58 C53 44(7) 2_655 .
C56 C57 C58 C53 0.0 . .
C54 C57 C58 C53 101(12) 2_655 .
C57 C57 C58 C53 15(3) 2_655 .
C55 C57 C58 C53 110(12) 2_655 2_655
C56 C57 C58 C53 24(8) 2_655 2_655
C56 C57 C58 C53 -20(4) . 2_655
C54 C57 C58 C53 81(12) 2_655 2_655
C57 C57 C58 C53 -4(4) 2_655 2_655
C53 C53 C58 C54 36(10) 2_655 2_655
C54 C53 C58 C54 124(8) . 2_655
C58 C53 C58 C54 105(8) 2_655 2_655
C53 C53 C58 C55 -51(12) 2_655 2_655
C54 C53 C58 C55 37(6) . 2_655
C54 C53 C58 C55 -87(13) 2_655 2_655
C58 C53 C58 C55 18(7) 2_655 2_655
C53 C53 C58 C57 -88(12) 2_655 .
C54 C53 C58 C57 0.0 . .
C54 C53 C58 C57 -124(8) 2_655 .
C58 C53 C58 C57 -19(3) 2_655 .
C54 C53 C58 C53 88(11) . 2_655
C54 C53 C58 C53 -36(10) 2_655 2_655
C58 C53 C58 C53 68(10) 2_655 2_655
C53' C53' C54' C58' -143(48) 2_655 2_655
C54' C53' C54' C58' 13(12) 2_655 2_655
C58' C53' C54' C58' 24(14) . 2_655
C55' C53' C54' C58' 15(13) 2_655 2_655
C54' C53' C54' C53' 156(47) 2_655 2_655
C58' C53' C54' C53' 167(36) . 2_655
C58' C53' C54' C53' 143(48) 2_655 2_655
C55' C53' C54' C53' 157(38) 2_655 2_655
C53' C53' C54' C55' -167(36) 2_655 .
C54' C53' C54' C55' -11(12) 2_655 .
C58' C53' C54' C55' 0.0 . .
C58' C53' C54' C55' -24(14) 2_655 .
C55' C53' C54' C55' -10(3) 2_655 .
C53' C53' C54' C57' -154(38) 2_655 2_655
C54' C53' C54' C57' 2(11) 2_655 2_655
C58' C53' C54' C57' 13(4) . 2_655
C58' C53' C54' C57' -11(11) 2_655 2_655
C55' C53' C54' C57' 3(3) 2_655 2_655
C53' C53' C54' C54' -156(47) 2_655 2_655
C58' C53' C54' C54' 11(12) . 2_655
C58' C53' C54' C54' -13(12) 2_655 2_655
C55' C53' C54' C54' 1(10) 2_655 2_655
C53' C54' C55' C58' 126(26) 2_655 2_655
C53' C54' C55' C58' 131(16) . 2_655
C57' C54' C55' C58' 88(24) 2_655 2_655
C54' C54' C55' C58' 128(18) 2_655 2_655
C58' C54' C55' C57' -88(24) 2_655 2_655
C53' C54' C55' C57' 38(11) 2_655 2_655
C53' C54' C55' C57' 42(12) . 2_655
C54' C54' C55' C57' 39(10) 2_655 2_655
C58' C54' C55' C56' -131(16) 2_655 .
C53' C54' C55' C56' -4(13) 2_655 .
C53' C54' C55' C56' 0.0 . .
C57' C54' C55' C56' -42(12) 2_655 .
C54' C54' C55' C56' -3(3) 2_655 .
C58' C54' C55' C53' -126(26) 2_655 2_655
C53' C54' C55' C53' 4(13) . 2_655
C57' C54' C55' C53' -38(11) 2_655 2_655
C54' C54' C55' C53' 1(10) 2_655 2_655
C58' C54' C55' C56' -116(17) 2_655 2_655
C53' C54' C55' C56' 10(12) 2_655 2_655
C53' C54' C55' C56' 15(3) . 2_655
C57' C54' C55' C56' -28(9) 2_655 2_655
C54' C54' C55' C56' 12(3) 2_655 2_655
C58' C55' C56' C57' 90(15) 2_655 2_655
C54' C55' C56' C57' 109(9) . 2_655
C53' C55' C56' C57' 108(9) 2_655 2_655
C56' C55' C56' C57' 65(10) 2_655 2_655
C58' C55' C56' C56' 25(9) 2_655 2_655
C57' C55' C56' C56' -65(10) 2_655 2_655
C54' C55' C56' C56' 44(9) . 2_655
C53' C55' C56' C56' 43(8) 2_655 2_655
C58' C55' C56' C57' -19(11) 2_655 .
C57' C55' C56' C57' -109(9) 2_655 .
C54' C55' C56' C57' 0.0 . .
C53' C55' C56' C57' -1(4) 2_655 .
C56' C55' C56' C57' -44(9) 2_655 .
C57' C55' C56' C58' -90(15) 2_655 2_655
C54' C55' C56' C58' 19(11) . 2_655
C53' C55' C56' C58' 18(9) 2_655 2_655
C56' C55' C56' C58' -25(9) 2_655 2_655
C58' C55' C56' C55' -9(10) 2_655 2_655
C57' C55' C56' C55' -99(9) 2_655 2_655
C54' C55' C56' C55' 10(3) . 2_655
C53' C55' C56' C55' 9(3) 2_655 2_655
C56' C55' C56' C55' -34(7) 2_655 2_655
C57' C56' C57' C55' -1(8) 2_655 2_655
C56' C56' C57' C55' -73(13) 2_655 2_655
C55' C56' C57' C55' 34(7) . 2_655
C58' C56' C57' C55' 29(7) 2_655 2_655
C57' C56' C57' C56' 71(12) 2_655 2_655
C55' C56' C57' C56' 107(7) . 2_655
C58' C56' C57' C56' 101(9) 2_655 2_655
C55' C56' C57' C56' 73(13) 2_655 2_655
C57' C56' C57' C58' -36(7) 2_655 .
C56' C56' C57' C58' -107(7) 2_655 .
C55' C56' C57' C58' 0.0 . .
C58' C56' C57' C58' -6(4) 2_655 .
C55' C56' C57' C58' -34(7) 2_655 .
C57' C56' C57' C54' -33(7) 2_655 2_655
C56' C56' C57' C54' -104(9) 2_655 2_655
C55' C56' C57' C54' 3(4) . 2_655
C58' C56' C57' C54' -3(3) 2_655 2_655
C55' C56' C57' C54' -31(5) 2_655 2_655
C56' C56' C57' C57' -71(12) 2_655 2_655
C55' C56' C57' C57' 36(7) . 2_655
C58' C56' C57' C57' 30(4) 2_655 2_655
C55' C56' C57' C57' 1(8) 2_655 2_655
C55' C57' C58' C54' -107(27) 2_655 2_655
C56' C57' C58' C54' -28(17) 2_655 2_655
C56' C57' C58' C54' 13(14) . 2_655
C57' C57' C58' C54' 1(14) 2_655 2_655
C56' C57' C58' C55' 79(15) 2_655 2_655
C56' C57' C58' C55' 120(15) . 2_655
C54' C57' C58' C55' 107(27) 2_655 2_655
C57' C57' C58' C55' 108(17) 2_655 2_655
C55' C57' C58' C53' -120(15) 2_655 .
C56' C57' C58' C53' -42(7) 2_655 .
C56' C57' C58' C53' 0.0 . .
C54' C57' C58' C53' -13(14) 2_655 .
C57' C57' C58' C53' -12(3) 2_655 .
C55' C57' C58' C53' -119(18) 2_655 2_655
C56' C57' C58' C53' -40(9) 2_655 2_655
C56' C57' C58' C53' 1(4) . 2_655
C54' C57' C58' C53' -12(11) 2_655 2_655
C57' C57' C58' C53' -11(4) 2_655 2_655
C55' C57' C58' C56' -79(15) 2_655 2_655
C56' C57' C58' C56' 42(7) . 2_655
C54' C57' C58' C56' 28(17) 2_655 2_655
C57' C57' C58' C56' 29(6) 2_655 2_655
C53' C53' C58' C54' -147(41) 2_655 2_655
C54' C53' C58' C54' -152(26) . 2_655
C58' C53' C58' C54' -146(28) 2_655 2_655
C55' C53' C58' C54' -120(31) 2_655 2_655
C53' C53' C58' C55' -27(14) 2_655 2_655
C54' C53' C58' C55' 120(31) 2_655 2_655
C54' C53' C58' C55' -32(7) . 2_655
C58' C53' C58' C55' -26(7) 2_655 2_655
C53' C53' C58' C57' 6(16) 2_655 .
C54' C53' C58' C57' 152(26) 2_655 .
C54' C53' C58' C57' 0.0 . .
C58' C53' C58' C57' 6(4) 2_655 .
C55' C53' C58' C57' 32(7) 2_655 .
C54' C53' C58' C53' 147(41) 2_655 2_655
C54' C53' C58' C53' -6(16) . 2_655
C58' C53' C58' C53' 1(13) 2_655 2_655
C55' C53' C58' C53' 27(14) 2_655 2_655
C53' C53' C58' C56' -9(16) 2_655 2_655
C54' C53' C58' C56' 138(27) 2_655 2_655
C54' C53' C58' C56' -14(3) . 2_655
C58' C53' C58' C56' -8(4) 2_655 2_655
C55' C53' C58' C56' 18(5) 2_655 2_655
