#------------------------------------------------------------------------------
#$Date: 2016-03-21 10:23:07 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178648 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/59/4075960.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4075960
loop_
_publ_author_name
'Wei, Qiao-Hua'
'Zhang, Li-Yi'
'Yin, Gang-Qiang'
'Shi, Lin-Xi'
'Chen, Zhong-Ning'
_publ_section_title
;
 Luminescent Au6Ag13Cage Compounds of Arylacetylides, Metastable
 Intermediates to Au5Ag8Complexes of {1,2,3-C6(C6H4R-4)3}3-(R = H, CH3,
 But)
;
_journal_issue                   16
_journal_name_full               Organometallics
_journal_page_first              3818
_journal_paper_doi               10.1021/om050363d
_journal_volume                  24
_journal_year                    2005
_chemical_formula_sum
'C67 H56.67 Ag4.33 Au2 Cl0 F10 N0 O P2 Sb1.67'
_chemical_formula_weight         2194.02
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           148
_symmetry_cell_setting           rhombohedral
_symmetry_space_group_name_Hall  '-R 3'
_symmetry_space_group_name_H-M   'R -3 :H'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            18
_cell_length_a                   25.140(4)
_cell_length_b                   25.140(4)
_cell_length_c                   59.228(12)
_cell_measurement_temperature    293(2)
_cell_volume                     32418(10)
_computing_cell_refinement       'Bruker XSCANS'
_computing_data_collection       'Bruker XSCANS'
_computing_data_reduction        'Bruker SHELXTL'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.944
_diffrn_measured_fraction_theta_max 0.944
_diffrn_measurement_device_type  'Bruker P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.80000
_diffrn_reflns_av_R_equivalents  0.0000
_diffrn_reflns_av_sigmaI/netI    0.0291
_diffrn_reflns_limit_h_max       27
_diffrn_reflns_limit_h_min       0
_diffrn_reflns_limit_k_max       0
_diffrn_reflns_limit_k_min       -23
_diffrn_reflns_limit_l_max       65
_diffrn_reflns_limit_l_min       -66
_diffrn_reflns_number            10106
_diffrn_reflns_theta_full        26.69
_diffrn_reflns_theta_max         26.69
_diffrn_reflns_theta_min         1.12
_exptl_absorpt_coefficient_mu    5.932
_exptl_absorpt_correction_type   none
_exptl_crystal_density_diffrn    2.023
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             18600
_refine_diff_density_max         2.379
_refine_diff_density_min         -2.220
_refine_diff_density_rms         0.307
_refine_ls_extinction_coef       0.00027(2)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.083
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     461
_refine_ls_number_reflns         10106
_refine_ls_number_restraints     400
_refine_ls_restrained_S_all      1.064
_refine_ls_R_factor_all          0.1232
_refine_ls_R_factor_gt           0.0975
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.2350P)²+78.5000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.3007
_refine_ls_wR_factor_ref         0.3291
_reflns_number_gt                6731
_reflns_number_total             10106
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om050363dsi20050509_062135.cif
_cod_data_source_block           compound_2a(SbF6)5
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Rhombohedral' changed to
'rhombohedral' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        32418(9)
_cod_original_sg_symbol_H-M      R-3
_cod_database_code               4075960
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'x+2/3, y+1/3, z+1/3'
'-y+2/3, x-y+1/3, z+1/3'
'-x+y+2/3, -x+1/3, z+1/3'
'x+1/3, y+2/3, z+2/3'
'-y+1/3, x-y+2/3, z+2/3'
'-x+y+1/3, -x+2/3, z+2/3'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'-x+2/3, -y+1/3, -z+1/3'
'y+2/3, -x+y+1/3, -z+1/3'
'x-y+2/3, x+1/3, -z+1/3'
'-x+1/3, -y+2/3, -z+2/3'
'y+1/3, -x+y+2/3, -z+2/3'
'x-y+1/3, x+2/3, -z+2/3'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Au1 Au 0.72683(3) 0.23465(3) 0.048007(13) 0.0991(4) Uani 1 1 d D
Au2 Au 0.83160(4) 0.40179(4) 0.052155(15) 0.1126(4) Uani 1 1 d D
Ag1 Ag 0.84273(6) 0.31404(6) 0.02271(2) 0.0940(5) Uani 1 1 d .
Ag2 Ag 0.64992(6) 0.25716(6) 0.00922(2) 0.0975(5) Uani 1 1 d D
Ag3 Ag 0.65636(7) 0.25963(7) 0.08953(3) 0.1049(5) Uani 1 1 d D
Ag4 Ag 0.83859(7) 0.30634(8) 0.07696(3) 0.1104(5) Uani 1 1 d .
Ag5 Ag 0.6667 0.3333 0.04949(9) 0.215(2) Uani 1 3 d S
P1 P 0.92553(19) 0.2920(2) 0.02360(8) 0.0879(12) Uani 1 1 d .
P2 P 0.9227(3) 0.2871(3) 0.07541(9) 0.1137(16) Uani 1 1 d .
C11 C 0.8416(8) 0.4100(8) 0.0183(3) 0.133(10) Uani 1 1 d D
C12 C 0.8625(7) 0.4248(9) -0.0013(3) 0.097(5) Uani 1 1 d D
C13 C 0.8897(7) 0.4427(8) -0.0230(2) 0.111(6) Uiso 1 1 d GD
C14 C 0.9515(7) 0.4611(9) -0.0253(3) 0.148(8) Uiso 1 1 d GD
C15 C 0.9813(7) 0.4857(9) -0.0457(3) 0.181(11) Uiso 1 1 d GD
C16 C 0.9492(10) 0.4918(9) -0.0637(2) 0.185(12) Uiso 1 1 d GD
C17 C 0.8874(10) 0.4734(12) -0.0613(3) 0.25(2) Uiso 1 1 d GD
C18 C 0.8576(7) 0.4489(11) -0.0410(3) 0.27(2) Uiso 1 1 d GD
C19 C 0.9821(16) 0.5198(19) -0.0858(4) 0.30(3) Uiso 1 1 d D
C21 C 0.8354(9) 0.3982(9) 0.0863(3) 0.117(7) Uani 1 1 d D
C22 C 0.8481(11) 0.4053(12) 0.1069(3) 0.133(8) Uani 1 1 d D
C23 C 0.8619(11) 0.4160(11) 0.1307(3) 0.157(9) Uiso 1 1 d GD
C24 C 0.9199(11) 0.4614(12) 0.1376(4) 0.27(2) Uiso 1 1 d GD
C25 C 0.9358(12) 0.4670(13) 0.1603(4) 0.32(3) Uiso 1 1 d GD
C26 C 0.8938(14) 0.4272(13) 0.1761(3) 0.222(15) Uiso 1 1 d GD
C27 C 0.8358(13) 0.3818(15) 0.1692(3) 0.400 Uiso 1 1 d GD
C28 C 0.8199(10) 0.3762(14) 0.1465(4) 0.400 Uiso 1 1 d GD
C29 C 0.9128(16) 0.4309(16) 0.2008(3) 0.210(14) Uiso 1 1 d D
C31 C 0.7352(8) 0.2368(7) 0.0148(3) 0.112(7) Uani 1 1 d D
C32 C 0.7480(9) 0.2376(10) -0.0056(3) 0.107(6) Uani 1 1 d D
C33 C 0.7660(9) 0.2389(10) -0.0288(3) 0.152(9) Uiso 1 1 d GD
C34 C 0.7702(12) 0.1898(9) -0.0375(4) 0.209(14) Uiso 1 1 d GD
C35 C 0.7974(13) 0.1950(12) -0.0584(4) 0.27(2) Uiso 1 1 d GD
C36 C 0.8204(12) 0.2492(14) -0.0706(3) 0.32(3) Uiso 1 1 d GD
C37 C 0.8161(13) 0.2983(11) -0.0620(4) 0.30(3) Uiso 1 1 d GD
C38 C 0.7889(12) 0.2932(9) -0.0410(4) 0.211(14) Uiso 1 1 d GD
C39 C 0.8490(19) 0.254(2) -0.0937(4) 0.29(2) Uiso 1 1 d D
C41 C 0.7294(8) 0.2257(9) 0.0809(3) 0.117(7) Uani 1 1 d D
C42 C 0.7365(9) 0.2156(10) 0.1008(3) 0.113(6) Uani 1 1 d D
C43 C 0.7464(13) 0.2068(12) 0.1239(3) 0.190(12) Uiso 1 1 d GD
C44 C 0.7867(14) 0.2585(11) 0.1363(5) 0.39(4) Uiso 1 1 d GD
C45 C 0.7970(15) 0.2530(15) 0.1590(4) 0.30(3) Uiso 1 1 d GD
C46 C 0.7671(15) 0.1957(18) 0.1694(3) 0.27(2) Uiso 1 1 d GD
C47 C 0.7268(17) 0.1440(14) 0.1570(5) 0.39(4) Uiso 1 1 d GD
C48 C 0.7165(16) 0.1496(11) 0.1343(5) 0.47(5) Uiso 1 1 d GD
C49 C 0.779(2) 0.192(3) 0.1943(4) 0.400 Uiso 1 1 d D
C51 C 0.6667 0.3333 -0.0135(3) 0.078(6) Uani 1 3 d SD
C52 C 0.6667 0.3333 -0.0347(3) 0.130(12) Uani 1 3 d SD
C53 C 0.6667 0.3333 -0.0589(3) 0.129(12) Uiso 1 3 d SGD
C54 C 0.678(3) 0.292(2) -0.0707(4) 0.13(2) Uiso 0.33 1 d PGD
C55 C 0.678(3) 0.292(2) -0.0942(4) 0.19(4) Uiso 0.33 1 d PGD
C56 C 0.6667(16) 0.3335(16) -0.1058(3) 0.33(5) Uiso 1 3 d SGD
C57 C 0.656(3) 0.375(3) -0.0940(4) 0.22(5) Uiso 0.33 1 d PGD
C58 C 0.656(3) 0.375(2) -0.0705(4) 0.14(2) Uiso 0.33 1 d PGD
C59 C 0.6667 0.3333 -0.1315(4) 0.23(3) Uiso 1 3 d SD
C61 C 0.6667 0.3333 0.1131(4) 0.120(12) Uani 1 3 d SD
C62 C 0.6667 0.3333 0.1344(3) 0.128(13) Uani 1 3 d SD
C63 C 0.6667 0.3333 0.1586(4) 0.19(2) Uiso 1 3 d SGD
C64 C 0.706(2) 0.319(3) 0.1704(4) 0.22(5) Uiso 0.33 1 d PGD
C65 C 0.706(3) 0.320(4) 0.1938(4) 0.28(7) Uiso 0.33 1 d PGD
C66 C 0.6668(16) 0.3335(16) 0.2056(4) 0.19(2) Uiso 1 3 d SGD
C67 C 0.628(2) 0.348(3) 0.1938(4) 0.14(2) Uiso 0.33 1 d PGD
C68 C 0.628(2) 0.348(3) 0.1704(4) 0.119(18) Uiso 0.33 1 d PGD
C69 C 0.6667 0.3333 0.2312(4) 0.400 Uiso 1 3 d SD
C101 C 0.9710(8) 0.3178(10) 0.0496(3) 0.113(6) Uani 1 1 d .
C111 C 0.9053(7) 0.2112(7) 0.0196(3) 0.086(4) Uani 1 1 d .
C112 C 0.8436(9) 0.1680(8) 0.0193(4) 0.117(6) Uani 1 1 d .
C113 C 0.8330(14) 0.1100(12) 0.0164(4) 0.145(8) Uani 1 1 d .
C114 C 0.8755(15) 0.0921(12) 0.0159(4) 0.135(8) Uani 1 1 d .
C115 C 0.9341(11) 0.1359(10) 0.0167(4) 0.116(6) Uani 1 1 d .
C116 C 0.9483(9) 0.1943(9) 0.0191(3) 0.106(5) Uani 1 1 d .
C121 C 0.9795(7) 0.3316(8) 0.0013(3) 0.087(4) Uani 1 1 d .
C122 C 1.0337(8) 0.3860(9) 0.0041(5) 0.124(7) Uani 1 1 d .
C123 C 1.0698(12) 0.4107(12) -0.0111(6) 0.147(9) Uani 1 1 d .
C124 C 1.0576(12) 0.3926(13) -0.0356(6) 0.154(10) Uani 1 1 d .
C125 C 0.9980(13) 0.3339(15) -0.0395(5) 0.154(9) Uani 1 1 d .
C126 C 0.9626(8) 0.3052(10) -0.0199(4) 0.117(6) Uani 1 1 d .
C131 C 0.9033(11) 0.2075(8) 0.0775(3) 0.136(7) Uiso 1 1 d G
C132 C 0.9490(8) 0.1918(13) 0.0770(4) 0.203(13) Uiso 1 1 d G
C133 C 0.9335(15) 0.1305(15) 0.0785(5) 0.28(2) Uiso 1 1 d G
C134 C 0.8723(18) 0.0850(10) 0.0804(5) 0.227(16) Uiso 1 1 d G
C135 C 0.8265(11) 0.1007(10) 0.0808(5) 0.37(4) Uiso 1 1 d G
C136 C 0.8420(9) 0.1619(12) 0.0793(4) 0.167(10) Uiso 1 1 d G
C141 C 0.9788(16) 0.3207(13) 0.0998(5) 0.227(9) Uiso 1 1 d G
C142 C 0.9576(12) 0.3397(16) 0.1180(7) 0.227(9) Uiso 1 1 d G
C143 C 0.996(2) 0.3678(19) 0.1364(6) 0.53(7) Uiso 1 1 d G
C144 C 1.0549(18) 0.3768(17) 0.1367(6) 0.33(3) Uiso 1 1 d G
C145 C 1.0761(11) 0.3578(15) 0.1184(7) 0.227(9) Uiso 1 1 d G
C146 C 1.0380(18) 0.3298(15) 0.1000(5) 0.227(9) Uiso 1 1 d G
Sb1 Sb 0.9613(3) 1.3203(4) -0.11920(9) 0.310(4) Uani 0.67 1 d PD
Sb2 Sb 0.7845(4) -0.0947(3) 0.06246(13) 0.316(4) Uani 0.67 1 d PD
Sb3 Sb 1.0000 0.0000 0.0340(2) 0.368(5) Uani 1 3 d SD
F11 F 0.9116(10) 1.3402(12) -0.1023(4) 0.36(3) Uiso 0.67 1 d PD
F12 F 0.8944(8) 1.2674(10) -0.1367(4) 0.36(3) Uiso 0.67 1 d PD
F13 F 1.0112(10) 1.3006(12) -0.1360(4) 0.31(2) Uiso 0.67 1 d PD
F14 F 1.0284(8) 1.3732(9) -0.1017(3) 0.214(11) Uiso 0.67 1 d PD
F15 F 0.9445(12) 1.2566(9) -0.0994(4) 0.35(3) Uiso 0.67 1 d PD
F16 F 0.9783(11) 1.3842(9) -0.1388(4) 0.274(17) Uiso 0.67 1 d PD
F21 F 0.7257(17) -0.090(2) 0.0448(8) 0.42(3) Uiso 0.67 1 d PD
F22 F 0.7240(17) -0.1587(17) 0.0792(8) 0.44(4) Uiso 0.67 1 d PD
F23 F 0.8434(18) -0.096(2) 0.0807(8) 0.48(4) Uiso 0.67 1 d PD
F24 F 0.8450(18) -0.0309(19) 0.0457(8) 0.555 Uiso 0.67 1 d PD
F25 F 0.788(3) -0.150(2) 0.0424(8) 0.560 Uiso 0.67 1 d PD
F26 F 0.782(2) -0.037(2) 0.0813(8) 0.500 Uiso 0.67 1 d PD
F31 F 0.992(3) 0.050(2) 0.0553(6) 0.45(3) Uiso 1 1 d D
F32 F 1.024(4) 0.0447(13) 0.0074(3) 0.39(3) Uiso 1 1 d D
O1 O 0.873(2) 1.430(2) -0.1635(7) 0.34(2) Uiso 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Sb Sb -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Au Au -2.0133 8.8022 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C41 Au1 C31 168.6(8) . .
C41 Au1 Ag1 119.8(5) . .
C31 Au1 Ag1 55.0(5) . .
C41 Au1 Ag4 55.1(5) . .
C31 Au1 Ag4 119.8(5) . .
Ag1 Au1 Ag4 65.02(5) . .
C41 Au1 Ag2 141.4(6) . .
C31 Au1 Ag2 49.7(5) . .
Ag1 Au1 Ag2 89.75(4) . .
Ag4 Au1 Ag2 139.77(5) . .
C41 Au1 Ag3 47.9(6) . .
C31 Au1 Ag3 143.5(5) . .
Ag1 Au1 Ag3 133.69(4) . .
Ag4 Au1 Ag3 83.65(4) . .
Ag2 Au1 Ag3 94.13(4) . .
C11 Au2 C21 171.3(8) . .
C11 Au2 Ag4 122.2(5) . .
C21 Au2 Ag4 55.4(5) . .
C11 Au2 Ag1 55.4(5) . .
C21 Au2 Ag1 122.3(5) . .
Ag4 Au2 Ag1 67.04(5) . .
C11 Au2 Ag3 139.0(5) . 2_655
C21 Au2 Ag3 49.2(5) . 2_655
Ag4 Au2 Ag3 87.39(5) . 2_655
Ag1 Au2 Ag3 136.90(5) . 2_655
C11 Au2 Ag2 44.8(5) . 2_655
C21 Au2 Ag2 143.8(5) . 2_655
Ag4 Au2 Ag2 130.59(5) . 2_655
Ag1 Au2 Ag2 78.84(4) . 2_655
Ag3 Au2 Ag2 94.87(5) 2_655 2_655
P1 Ag1 C11 132.0(4) . .
P1 Ag1 C31 123.9(4) . .
C11 Ag1 C31 102.1(6) . .
P1 Ag1 Au2 125.36(12) . .
C11 Ag1 Au2 42.9(5) . .
C31 Ag1 Au2 103.1(4) . .
P1 Ag1 Au1 120.17(13) . .
C11 Ag1 Au1 103.0(4) . .
C31 Ag1 Au1 41.1(5) . .
Au2 Ag1 Au1 77.06(4) . .
P1 Ag1 Ag4 88.29(12) . .
C11 Ag1 Ag4 98.6(5) . .
C31 Ag1 Ag4 98.7(5) . .
Au2 Ag1 Ag4 55.88(4) . .
Au1 Ag1 Ag4 57.78(4) . .
C51 Ag2 C11 137.9(5) . 3_665
C51 Ag2 C31 117.1(5) . .
C11 Ag2 C31 98.0(6) 3_665 .
C51 Ag2 Ag5 91.5(4) . .
C11 Ag2 Ag5 105.4(5) 3_665 .
C31 Ag2 Ag5 99.7(4) . .
C51 Ag2 Ag2 46.7(3) . 2_655
C11 Ag2 Ag2 164.3(5) 3_665 2_655
C31 Ag2 Ag2 88.4(4) . 2_655
Ag5 Ag2 Ag2 59.27(6) . 2_655
C51 Ag2 Ag2 46.7(3) . 3_665
C11 Ag2 Ag2 110.9(4) 3_665 3_665
C31 Ag2 Ag2 147.6(4) . 3_665
Ag5 Ag2 Ag2 59.27(6) . 3_665
Ag2 Ag2 Ag2 60.0 2_655 3_665
C51 Ag2 Au1 135.7(2) . .
C11 Ag2 Au1 86.2(5) 3_665 .
C31 Ag2 Au1 37.6(5) . .
Ag5 Ag2 Au1 68.63(6) . .
Ag2 Ag2 Au1 90.28(5) 2_655 .
Ag2 Ag2 Au1 127.67(3) 3_665 .
C51 Ag2 Au2 147.4(2) . 3_665
C11 Ag2 Au2 37.0(5) 3_665 3_665
C31 Ag2 Au2 93.0(4) . 3_665
Ag5 Ag2 Au2 70.08(7) . 3_665
Ag2 Ag2 Au2 128.76(3) 2_655 3_665
Ag2 Ag2 Au2 101.05(5) 3_665 3_665
Au1 Ag2 Au2 63.25(3) . 3_665
C61 Ag3 C21 122.1(6) . 3_665
C61 Ag3 C41 128.9(5) . .
C21 Ag3 C41 99.9(7) 3_665 .
C61 Ag3 Ag5 92.6(5) . .
C21 Ag3 Ag5 107.4(4) 3_665 .
C41 Ag3 Ag5 101.9(4) . .
C61 Ag3 Ag3 47.6(3) . 2_655
C21 Ag3 Ag3 157.7(5) 3_665 2_655
C41 Ag3 Ag3 100.4(4) . 2_655
Ag5 Ag3 Ag3 59.21(6) . 2_655
C61 Ag3 Ag3 47.6(3) . 3_665
C21 Ag3 Ag3 98.1(5) 3_665 3_665
C41 Ag3 Ag3 157.3(4) . 3_665
Ag5 Ag3 Ag3 59.21(6) . 3_665
Ag3 Ag3 Ag3 60.0 2_655 3_665
C61 Ag3 Au2 143.0(2) . 3_665
C21 Ag3 Au2 40.1(5) 3_665 3_665
C41 Ag3 Au2 87.8(5) . 3_665
Ag5 Ag3 Au2 72.73(7) . 3_665
Ag3 Ag3 Au2 131.94(3) 2_655 3_665
Ag3 Ag3 Au2 97.26(6) 3_665 3_665
C61 Ag3 Au1 141.4(3) . .
C21 Ag3 Au1 96.0(5) 3_665 .
C41 Ag3 Au1 36.7(5) . .
Ag5 Ag3 Au1 68.21(7) . .
Ag3 Ag3 Au1 94.74(5) 2_655 .
Ag3 Ag3 Au1 127.41(3) 3_665 .
Au2 Ag3 Au1 64.67(4) 3_665 .
P2 Ag4 C21 131.0(5) . .
P2 Ag4 C41 124.6(5) . .
C21 Ag4 C41 102.1(7) . .
P2 Ag4 Au2 125.02(17) . .
C21 Ag4 Au2 43.7(5) . .
C41 Ag4 Au2 103.0(4) . .
P2 Ag4 Au1 120.83(15) . .
C21 Ag4 Au1 103.6(5) . .
C41 Ag4 Au1 40.6(5) . .
Au2 Ag4 Au1 77.36(4) . .
P2 Ag4 Ag1 88.20(14) . .
C21 Ag4 Ag1 100.7(5) . .
C41 Ag4 Ag1 97.5(5) . .
Au2 Ag4 Ag1 57.07(4) . .
Au1 Ag4 Ag1 57.20(4) . .
Ag3 Ag5 Ag3 61.57(12) . 2_655
Ag3 Ag5 Ag3 61.57(12) . 3_665
Ag3 Ag5 Ag3 61.57(12) 2_655 3_665
Ag3 Ag5 Ag2 107.68(4) . .
Ag3 Ag5 Ag2 148.17(4) 2_655 .
Ag3 Ag5 Ag2 143.18(4) 3_665 .
Ag3 Ag5 Ag2 143.18(4) . 2_655
Ag3 Ag5 Ag2 107.68(4) 2_655 2_655
Ag3 Ag5 Ag2 148.16(4) 3_665 2_655
Ag2 Ag5 Ag2 61.46(11) . 2_655
Ag3 Ag5 Ag2 148.17(4) . 3_665
Ag3 Ag5 Ag2 143.18(4) 2_655 3_665
Ag3 Ag5 Ag2 107.68(4) 3_665 3_665
Ag2 Ag5 Ag2 61.46(11) . 3_665
Ag2 Ag5 Ag2 61.46(11) 2_655 3_665
C121 P1 C101 105.0(9) . .
C121 P1 C111 103.5(8) . .
C101 P1 C111 106.0(9) . .
C121 P1 Ag1 110.9(5) . .
C101 P1 Ag1 113.3(7) . .
C111 P1 Ag1 117.1(5) . .
C131 P2 C101 105.8(10) . .
C131 P2 C141 99.9(12) . .
C101 P2 C141 104.8(13) . .
C131 P2 Ag4 116.3(8) . .
C101 P2 Ag4 113.9(7) . .
C141 P2 Ag4 114.6(13) . .
C12 C11 Au2 164.5(17) . .
C12 C11 Ag2 95.2(13) . 2_655
Au2 C11 Ag2 98.2(7) . 2_655
C12 C11 Ag1 100.5(15) . .
Au2 C11 Ag1 81.7(6) . .
Ag2 C11 Ag1 112.0(7) 2_655 .
C11 C12 C13 176.7(17) . .
C14 C13 C18 120.0 . .
C14 C13 C12 118.5(12) . .
C18 C13 C12 121.0(12) . .
C13 C14 C15 120.0 . .
C14 C15 C16 120.0 . .
C15 C16 C17 120.0 . .
C15 C16 C19 120.0(7) . .
C17 C16 C19 120.0(7) . .
C18 C17 C16 120.0 . .
C17 C18 C13 120.0 . .
C22 C21 Au2 169(2) . .
C22 C21 Ag3 96.0(15) . 2_655
Au2 C21 Ag3 90.7(7) . 2_655
C22 C21 Ag4 103.4(16) . .
Au2 C21 Ag4 80.8(6) . .
Ag3 C21 Ag4 121.2(8) 2_655 .
C21 C22 C23 177(3) . .
C24 C23 C28 120.0 . .
C24 C23 C22 119.8(15) . .
C28 C23 C22 119.8(15) . .
C23 C24 C25 120.0 . .
C26 C25 C24 120.0 . .
C25 C26 C27 120.0 . .
C25 C26 C29 119.8(18) . .
C27 C26 C29 120.1(18) . .
C28 C27 C26 120.0 . .
C27 C28 C23 120.0 . .
C32 C31 Au1 171.0(15) . .
C32 C31 Ag1 89.9(13) . .
Au1 C31 Ag1 83.9(6) . .
C32 C31 Ag2 96.2(13) . .
Au1 C31 Ag2 92.7(7) . .
Ag1 C31 Ag2 126.0(7) . .
C31 C32 C33 177(2) . .
C34 C33 C38 120.0 . .
C34 C33 C32 119.6(14) . .
C38 C33 C32 119.4(14) . .
C35 C34 C33 120.0 . .
C34 C35 C36 120.0 . .
C35 C36 C37 120.0 . .
C35 C36 C39 119.3(18) . .
C37 C36 C39 120.7(18) . .
C38 C37 C36 120.0 . .
C37 C38 C33 120.0 . .
C42 C41 Au1 169.7(19) . .
C42 C41 Ag3 94.7(15) . .
Au1 C41 Ag3 95.5(7) . .
C42 C41 Ag4 92.4(14) . .
Au1 C41 Ag4 84.3(7) . .
Ag3 C41 Ag4 117.0(8) . .
C41 C42 C43 177(2) . .
C44 C43 C48 120.0 . .
C44 C43 C42 117.5(16) . .
C48 C43 C42 122.5(16) . .
C43 C44 C45 120.0 . .
C44 C45 C46 120.0 . .
C45 C46 C47 120.0 . .
C45 C46 C49 118.4(19) . .
C47 C46 C49 121.6(19) . .
C48 C47 C46 120.0 . .
C47 C48 C43 120.0 . .
C52 C51 Ag2 127.7(4) . .
C52 C51 Ag2 127.7(4) . 2_655
Ag2 C51 Ag2 86.5(6) . 2_655
C52 C51 Ag2 127.7(4) . 3_665
Ag2 C51 Ag2 86.5(6) . 3_665
Ag2 C51 Ag2 86.5(6) 2_655 3_665
C51 C52 C53 180.000(1) . .
C58 C53 C54 51.4(10) 3_665 2_655
C58 C53 C54 51(4) 3_665 .
C54 C53 C54 97(4) 2_655 .
C58 C53 C58 97(4) 3_665 .
C54 C53 C58 51(4) 2_655 .
C54 C53 C58 120.0 . .
C58 C53 C58 97.47(11) 3_665 2_655
C54 C53 C58 120(3) 2_655 2_655
C54 C53 C58 51(4) . 2_655
C58 C53 C58 97(4) . 2_655
C58 C53 C54 120(3) 3_665 3_665
C54 C53 C54 96.89(11) 2_655 3_665
C54 C53 C54 97(4) . 3_665
C58 C53 C54 51(4) . 3_665
C58 C53 C54 51.2(9) 2_655 3_665
C58 C53 C52 119.8(13) 3_665 .
C54 C53 C52 120.2(14) 2_655 .
C54 C53 C52 120.2(7) . .
C58 C53 C52 119.8(7) . .
C58 C53 C52 119.8(13) 2_655 .
C54 C53 C52 120.2(14) 3_665 .
C58 C54 C58 120.4(13) 3_665 2_655
C58 C54 C53 64(4) 3_665 .
C58 C54 C53 64(4) 2_655 .
C58 C54 C55 90.29(6) 3_665 .
C58 C54 C55 90.4 2_655 .
C53 C54 C55 120.0 . .
C58 C54 C57 49.4(18) 3_665 3_665
C58 C54 C57 110.0(17) 2_655 3_665
C53 C54 C57 96(4) . 3_665
C55 C54 C57 40.9(17) . 3_665
C58 C54 C57 110.0(18) 3_665 2_655
C58 C54 C57 49.2(17) 2_655 2_655
C53 C54 C57 96(4) . 2_655
C55 C54 C57 41.2(17) . 2_655
C57 C54 C57 69.8(16) 3_665 2_655
C57 C55 C57 121(4) 3_665 2_655
C57 C55 C54 89.7 3_665 .
C57 C55 C54 89.61(5) 2_655 .
C57 C55 C56 65(5) 3_665 .
C57 C55 C56 65(5) 2_655 .
C54 C55 C56 120.2 . .
C57 C55 C58 49.0(14) 3_665 3_665
C57 C55 C58 109.3(17) 2_655 3_665
C54 C55 C58 40.7(15) . 3_665
C56 C55 C58 96(3) . 3_665
C57 C55 C58 109.4(17) 3_665 2_655
C57 C55 C58 48.8(14) 2_655 2_655
C54 C55 C58 40.8(15) . 2_655
C56 C55 C58 96(3) . 2_655
C58 C55 C58 69.0(5) 3_665 2_655
C55 C56 C55 97.3(3) 2_655 3_665
C55 C56 C57 51(4) 2_655 .
C55 C56 C57 52(4) 3_665 .
C55 C56 C55 97(4) 2_655 .
C55 C56 C55 97(4) 3_665 .
C57 C56 C55 120.0 . .
C55 C56 C57 52(3) 2_655 3_665
C55 C56 C57 120(3) 3_665 3_665
C57 C56 C57 97(4) . 3_665
C55 C56 C57 51(4) . 3_665
C55 C56 C57 120(3) 2_655 2_655
C55 C56 C57 51(3) 3_665 2_655
C57 C56 C57 97(4) . 2_655
C55 C56 C57 51(4) . 2_655
C57 C56 C57 97.1(3) 3_665 2_655
C55 C56 C59 120(3) 2_655 .
C55 C56 C59 120(3) 3_665 .
C57 C56 C59 120.2(19) . .
C55 C56 C59 119.8(19) . .
C57 C56 C59 120(3) 3_665 .
C57 C56 C59 120(3) 2_655 .
C55 C57 C55 119(4) 2_655 3_665
C55 C57 C56 64(4) 2_655 .
C55 C57 C56 63(4) 3_665 .
C55 C57 C58 90.4 2_655 .
C55 C57 C58 90.28(6) 3_665 .
C56 C57 C58 119.8 . .
C55 C57 C54 49.4(16) 2_655 2_655
C55 C57 C54 108.8(17) 3_665 2_655
C56 C57 C54 95(3) . 2_655
C58 C57 C54 41.0(15) . 2_655
C55 C57 C54 108.9(17) 2_655 3_665
C55 C57 C54 49.2(15) 3_665 3_665
C56 C57 C54 95(3) . 3_665
C58 C57 C54 41.1(15) . 3_665
C54 C57 C54 69.1(5) 2_655 3_665
C54 C58 C54 119.5(14) 2_655 3_665
C54 C58 C57 89.62(5) 2_655 .
C54 C58 C57 89.7 3_665 .
C54 C58 C53 64(4) 2_655 .
C54 C58 C53 64(4) 3_665 .
C57 C58 C53 120.0 . .
C54 C58 C55 49.0(19) 2_655 2_655
C54 C58 C55 108.2(18) 3_665 2_655
C57 C58 C55 40.6(19) . 2_655
C53 C58 C55 95(4) . 2_655
C54 C58 C55 108.3(18) 2_655 3_665
C54 C58 C55 48.8(18) 3_665 3_665
C57 C58 C55 40.9(19) . 3_665
C53 C58 C55 95(4) . 3_665
C55 C58 C55 68.3(16) 2_655 3_665
C62 C61 Ag3 128.8(5) . .
C62 C61 Ag3 128.8(5) . 2_655
Ag3 C61 Ag3 84.9(7) . 2_655
C62 C61 Ag3 128.8(5) . 3_665
Ag3 C61 Ag3 84.9(7) . 3_665
Ag3 C61 Ag3 84.9(7) 2_655 3_665
C61 C62 C63 180.000(2) . .
C64 C63 C68 51.6(10) 2_655 3_665
C64 C63 C64 97(4) 2_655 .
C68 C63 C64 51(4) 3_665 .
C64 C63 C68 51(4) 2_655 .
C68 C63 C68 97(4) 3_665 .
C64 C63 C68 120.0 . .
C64 C63 C64 97.19(11) 2_655 3_665
C68 C63 C64 120(2) 3_665 3_665
C64 C63 C64 97(4) . 3_665
C68 C63 C64 52(4) . 3_665
C64 C63 C68 120(2) 2_655 2_655
C68 C63 C68 97.18(11) 3_665 2_655
C64 C63 C68 52(4) . 2_655
C68 C63 C68 97(4) . 2_655
C64 C63 C68 51.1(10) 3_665 2_655
C64 C63 C62 120.0(12) 2_655 .
C68 C63 C62 120.0(15) 3_665 .
C64 C63 C62 120.0(7) . .
C68 C63 C62 120.0(7) . .
C64 C63 C62 120.0(12) 3_665 .
C68 C63 C62 120.0(15) 2_655 .
C68 C64 C68 120.0(14) 3_665 2_655
C68 C64 C63 64(4) 3_665 .
C68 C64 C63 64(4) 2_655 .
C68 C64 C65 89.9 3_665 .
C68 C64 C65 90.1 2_655 .
C63 C64 C65 120.0 . .
C68 C64 C67 49(2) 3_665 3_665
C68 C64 C67 109.1(18) 2_655 3_665
C63 C64 C67 96(4) . 3_665
C65 C64 C67 41(2) . 3_665
C68 C64 C67 109.1(18) 3_665 2_655
C68 C64 C67 49(2) 2_655 2_655
C63 C64 C67 95(4) . 2_655
C65 C64 C67 41(2) . 2_655
C67 C64 C67 69.1(16) 3_665 2_655
C67 C65 C67 120(4) 3_665 2_655
C67 C65 C64 90.1 3_665 .
C67 C65 C64 89.9 2_655 .
C67 C65 C66 64(5) 3_665 .
C67 C65 C66 64(4) 2_655 .
C64 C65 C66 120.0 . .
C67 C65 C68 49.3(16) 3_665 3_665
C67 C65 C68 109.0(17) 2_655 3_665
C64 C65 C68 40.8(16) . 3_665
C66 C65 C68 96(4) . 3_665
C67 C65 C68 109.2(17) 3_665 2_655
C67 C65 C68 48.9(16) 2_655 2_655
C64 C65 C68 41.0(16) . 2_655
C66 C65 C68 95(3) . 2_655
C68 C65 C68 69.1(5) 3_665 2_655
C67 C66 C65 52(3) 3_665 2_655
C67 C66 C65 51(5) 3_665 .
C65 C66 C65 97(4) 2_655 .
C67 C66 C67 97(5) 3_665 .
C65 C66 C67 51(4) 2_655 .
C65 C66 C67 120.0 . .
C67 C66 C67 97.2(3) 3_665 2_655
C65 C66 C67 120(3) 2_655 2_655
C65 C66 C67 52(5) . 2_655
C67 C66 C67 97(5) . 2_655
C67 C66 C65 120(2) 3_665 3_665
C65 C66 C65 97.2(3) 2_655 3_665
C65 C66 C65 97(4) . 3_665
C67 C66 C65 52(4) . 3_665
C67 C66 C65 51(3) 2_655 3_665
C67 C66 C69 120(3) 3_665 .
C65 C66 C69 120(3) 2_655 .
C65 C66 C69 120.0(19) . .
C67 C66 C69 120.0(19) . .
C67 C66 C69 120(3) 2_655 .
C65 C66 C69 120(3) 3_665 .
C65 C67 C65 120(4) 2_655 3_665
C65 C67 C68 90.1 2_655 .
C65 C67 C68 89.9 3_665 .
C65 C67 C66 64(5) 2_655 .
C65 C67 C66 64(4) 3_665 .
C68 C67 C66 120.0 . .
C65 C67 C64 49.3(14) 2_655 2_655
C65 C67 C64 109.0(17) 3_665 2_655
C68 C67 C64 40.8(14) . 2_655
C66 C67 C64 96(3) . 2_655
C65 C67 C64 109.2(17) 2_655 3_665
C65 C67 C64 48.9(13) 3_665 3_665
C68 C67 C64 41.0(13) . 3_665
C66 C67 C64 95(3) . 3_665
C64 C67 C64 69.1(5) 2_655 3_665
C64 C68 C64 120.0(13) 2_655 3_665
C64 C68 C67 89.9 2_655 .
C64 C68 C67 90.1 3_665 .
C64 C68 C63 64(4) 2_655 .
C64 C68 C63 64(4) 3_665 .
C67 C68 C63 120.0 . .
C64 C68 C65 49.3(15) 2_655 2_655
C64 C68 C65 109.1(17) 3_665 2_655
C67 C68 C65 40.6(15) . 2_655
C63 C68 C65 96(3) . 2_655
C64 C68 C65 109.2(17) 2_655 3_665
C64 C68 C65 48.9(15) 3_665 3_665
C67 C68 C65 41.2(15) . 3_665
C63 C68 C65 95(3) . 3_665
C65 C68 C65 69.1(16) 2_655 3_665
P1 C101 P2 112.5(10) . .
C116 C111 C112 121.1(17) . .
C116 C111 P1 121.8(14) . .
C112 C111 P1 116.8(13) . .
C113 C112 C111 113(2) . .
C114 C113 C112 127(3) . .
C115 C114 C113 117(2) . .
C114 C115 C116 120(2) . .
C115 C116 C111 122(2) . .
C122 C121 C126 120.1(18) . .
C122 C121 P1 124.0(16) . .
C126 C121 P1 115.9(13) . .
C123 C122 C121 122(2) . .
C122 C123 C124 125(2) . .
C123 C124 C125 113(2) . .
C126 C125 C124 116(2) . .
C121 C126 C125 122(2) . .
C132 C131 C136 120.0 . .
C132 C131 P2 120.6(17) . .
C136 C131 P2 119.4(17) . .
C131 C132 C133 120.0 . .
C134 C133 C132 120.0 . .
C133 C134 C135 120.0 . .
C136 C135 C134 120.0 . .
C135 C136 C131 120.0 . .
C142 C141 C146 120.0 . .
C142 C141 P2 115(3) . .
C146 C141 P2 125(3) . .
C143 C142 C141 120.0 . .
C144 C143 C142 120.0 . .
C143 C144 C145 120.0 . .
C146 C145 C144 120.0 . .
C145 C146 C141 120.0 . .
F12 Sb1 F16 90.2(4) . .
F12 Sb1 F11 90.3(4) . .
F16 Sb1 F11 89.9(4) . .
F12 Sb1 F13 90.0(4) . .
F16 Sb1 F13 90.1(4) . .
F11 Sb1 F13 179.7(6) . .
F12 Sb1 F15 90.1(4) . .
F16 Sb1 F15 179.7(7) . .
F11 Sb1 F15 90.0(4) . .
F13 Sb1 F15 90.0(4) . .
F12 Sb1 F14 179.8(6) . .
F16 Sb1 F14 89.8(4) . .
F11 Sb1 F14 89.9(4) . .
F13 Sb1 F14 89.9(4) . .
F15 Sb1 F14 89.9(4) . .
F23 Sb2 F22 89.3(14) . .
F23 Sb2 F25 91.4(15) . .
F22 Sb2 F25 90.9(15) . .
F23 Sb2 F26 90.3(15) . .
F22 Sb2 F26 91.3(15) . .
F25 Sb2 F26 177.2(17) . .
F23 Sb2 F24 90.7(15) . .
F22 Sb2 F24 179.8(19) . .
F25 Sb2 F24 88.9(15) . .
F26 Sb2 F24 88.9(14) . .
F23 Sb2 F21 177.6(17) . .
F22 Sb2 F21 91.2(14) . .
F25 Sb2 F21 90.9(15) . .
F26 Sb2 F21 87.3(14) . .
F24 Sb2 F21 88.8(14) . .
F32 Sb3 F32 54.2(17) 3_765 2_645
F32 Sb3 F32 54.2(17) 3_765 .
F32 Sb3 F32 54.2(17) 2_645 .
F32 Sb3 F31 106(2) 3_765 3_765
F32 Sb3 F31 160(3) 2_645 3_765
F32 Sb3 F31 121(3) . 3_765
F32 Sb3 F31 121(3) 3_765 2_645
F32 Sb3 F31 106(2) 2_645 2_645
F32 Sb3 F31 160(3) . 2_645
F31 Sb3 F31 79(2) 3_765 2_645
F32 Sb3 F31 160(3) 3_765 .
F32 Sb3 F31 121(3) 2_645 .
F32 Sb3 F31 106(2) . .
F31 Sb3 F31 79(2) 3_765 .
F31 Sb3 F31 79(2) 2_645 .
F32 F32 F32 80.3(17) 11_665 12_545
F32 F32 F32 49.8(9) 11_665 3_765
F32 F32 F32 90.00(2) 12_545 3_765
F32 F32 F32 90.000(19) 11_665 2_645
F32 F32 F32 49.8(9) 12_545 2_645
F32 F32 F32 60.000(8) 3_765 2_645
F32 F32 Sb3 111.8(12) 11_665 .
F32 F32 Sb3 111.8(12) 12_545 .
F32 F32 Sb3 62.9(8) 3_765 .
F32 F32 Sb3 62.9(9) 2_645 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Au1 C41 1.96(2) .
Au1 C31 1.97(2) .
Au1 Ag1 2.9838(16) .
Au1 Ag4 3.0033(18) .
Au1 Ag2 3.2297(17) .
Au1 Ag3 3.2703(18) .
Au2 C11 2.02(2) .
Au2 C21 2.026(19) .
Au2 Ag4 2.8930(19) .
Au2 Ag1 2.9332(16) .
Au2 Ag3 3.1441(17) 2_655
Au2 Ag2 3.3152(17) 2_655
Ag1 P1 2.407(4) .
Ag1 C11 2.440(17) .
Ag1 C31 2.459(16) .
Ag1 Ag4 3.218(2) .
Ag2 C51 2.202(12) .
Ag2 C11 2.359(18) 3_665
Ag2 C31 2.465(16) .
Ag2 Ag5 2.954(5) .
Ag2 Ag2 3.019(2) 2_655
Ag2 Ag2 3.019(2) 3_665
Ag2 Au2 3.3152(17) 3_665
Ag3 C61 2.230(14) .
Ag3 C21 2.380(19) 3_665
Ag3 C41 2.44(2) .
Ag3 Ag5 2.940(5) .
Ag3 Ag3 3.010(3) 2_655
Ag3 Ag3 3.010(3) 3_665
Ag3 Au2 3.1441(17) 3_665
Ag4 P2 2.395(5) .
Ag4 C21 2.413(18) .
Ag4 C41 2.476(18) .
Ag5 Ag3 2.940(5) 2_655
Ag5 Ag3 2.940(5) 3_665
Ag5 Ag2 2.954(5) 2_655
Ag5 Ag2 2.954(5) 3_665
P1 C121 1.798(17) .
P1 C101 1.831(19) .
P1 C111 1.847(16) .
P2 C131 1.812(18) .
P2 C101 1.86(2) .
P2 C141 1.89(2) .
C11 C12 1.251(19) .
C11 Ag2 2.359(18) 2_655
C12 C13 1.420(16) .
C13 C14 1.3900 .
C13 C18 1.3900 .
C14 C15 1.3900 .
C15 C16 1.3900 .
C16 C17 1.3900 .
C16 C19 1.521(5) .
C17 C18 1.3900 .
C21 C22 1.253(19) .
C21 Ag3 2.380(19) 2_655
C22 C23 1.445(17) .
C23 C24 1.3900 .
C23 C28 1.3900 .
C24 C25 1.3900 .
C25 C26 1.3900 .
C26 C27 1.3900 .
C26 C29 1.526(5) .
C27 C28 1.3900 .
C31 C32 1.250(18) .
C32 C33 1.442(17) .
C33 C34 1.3900 .
C33 C38 1.3900 .
C34 C35 1.3900 .
C35 C36 1.3900 .
C36 C37 1.3900 .
C36 C39 1.521(5) .
C37 C38 1.3900 .
C41 C42 1.238(19) .
C42 C43 1.432(17) .
C43 C44 1.3900 .
C43 C48 1.3900 .
C44 C45 1.3900 .
C45 C46 1.3900 .
C46 C47 1.3900 .
C46 C49 1.520(5) .
C47 C48 1.3900 .
C51 C52 1.254(19) .
C51 Ag2 2.202(12) 2_655
C51 Ag2 2.202(12) 3_665
C52 C53 1.434(18) .
C53 C58 1.39(6) 3_665
C53 C54 1.39(5) 2_655
C53 C54 1.3900 .
C53 C58 1.3900 .
C53 C58 1.39(6) 2_655
C53 C54 1.39(5) 3_665
C54 C58 1.20(6) 3_665
C54 C58 1.21(6) 2_655
C54 C55 1.3900 .
C54 C57 1.83(5) 3_665
C54 C57 1.84(5) 2_655
C55 C57 1.20(7) 3_665
C55 C57 1.21(7) 2_655
C55 C56 1.3830 .
C55 C58 1.84(4) 3_665
C55 C58 1.85(4) 2_655
C56 C55 1.38(6) 2_655
C56 C55 1.38(6) 3_665
C56 C57 1.3970 .
C56 C57 1.40(7) 3_665
C56 C57 1.40(7) 2_655
C56 C59 1.520(5) .
C57 C55 1.20(8) 2_655
C57 C55 1.21(8) 3_665
C57 C58 1.3900 .
C57 C54 1.83(4) 2_655
C57 C54 1.84(4) 3_665
C58 C54 1.20(6) 2_655
C58 C54 1.21(6) 3_665
C58 C55 1.84(5) 2_655
C58 C55 1.85(5) 3_665
C61 C62 1.257(19) .
C61 Ag3 2.230(14) 2_655
C61 Ag3 2.230(14) 3_665
C62 C63 1.438(18) .
C63 C64 1.39(6) 2_655
C63 C68 1.39(5) 3_665
C63 C64 1.3900 .
C63 C68 1.3900 .
C63 C64 1.39(6) 3_665
C63 C68 1.39(5) 2_655
C64 C68 1.20(7) 3_665
C64 C68 1.21(7) 2_655
C64 C65 1.3900 .
C64 C67 1.83(6) 3_665
C64 C67 1.84(6) 2_655
C65 C67 1.19(9) 3_665
C65 C67 1.21(9) 2_655
C65 C66 1.3902 .
C65 C68 1.83(4) 3_665
C65 C68 1.84(4) 2_655
C66 C67 1.39(6) 3_665
C66 C65 1.39(7) 2_655
C66 C67 1.3898 .
C66 C67 1.39(6) 2_655
C66 C65 1.39(7) 3_665
C66 C69 1.521(5) .
C67 C65 1.19(6) 2_655
C67 C65 1.21(6) 3_665
C67 C68 1.3900 .
C67 C64 1.83(4) 2_655
C67 C64 1.84(4) 3_665
C68 C64 1.20(6) 2_655
C68 C64 1.21(6) 3_665
C68 C65 1.83(4) 2_655
C68 C65 1.84(4) 3_665
C111 C116 1.35(2) .
C111 C112 1.38(2) .
C112 C113 1.35(3) .
C113 C114 1.35(4) .
C114 C115 1.33(3) .
C115 C116 1.33(3) .
C121 C122 1.38(2) .
C121 C126 1.38(3) .
C122 C123 1.20(3) .
C123 C124 1.51(4) .
C124 C125 1.51(4) .
C125 C126 1.42(3) .
C131 C132 1.3900 .
C131 C136 1.3900 .
C132 C133 1.3900 .
C133 C134 1.3900 .
C134 C135 1.3900 .
C135 C136 1.3900 .
C141 C142 1.3900 .
C141 C146 1.3900 .
C142 C143 1.3900 .
C143 C144 1.3900 .
C144 C145 1.3900 .
C145 C146 1.3900 .
Sb1 F12 1.852(8) .
Sb1 F16 1.853(8) .
Sb1 F11 1.854(8) .
Sb1 F13 1.854(8) .
Sb1 F15 1.855(8) .
Sb1 F14 1.857(8) .
Sb2 F23 1.849(10) .
Sb2 F22 1.852(10) .
Sb2 F25 1.853(10) .
Sb2 F26 1.855(10) .
Sb2 F24 1.855(10) .
Sb2 F21 1.857(10) .
Sb3 F32 1.853(10) 3_765
Sb3 F32 1.853(10) 2_645
Sb3 F32 1.853(10) .
Sb3 F31 1.864(10) 3_765
Sb3 F31 1.864(10) 2_645
Sb3 F31 1.864(10) .
F32 F32 1.31(4) 11_665
F32 F32 1.31(4) 12_545
F32 F32 1.69(5) 3_765
F32 F32 1.69(5) 2_645
