#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/63/4076374.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4076374
loop_
_publ_author_name
'Kameo, Hajime'
'Ishii, Sho'
'Nakazawa, Hiroshi'
_publ_section_title
;
 Synthesis and Reactivity of Rhodium Complexes Bearing
 [E(o-C6H4PPh2)3]-Type Tetradentate Ligands (E = Si, Ge, and Sn)
;
_journal_issue                   6
_journal_name_full               Organometallics
_journal_page_first              2212
_journal_paper_doi               10.1021/om2011276
_journal_volume                  31
_journal_year                    2012
_chemical_formula_moiety
'C57 H51 Ge O3 P4 Rh, 0.25(C6 H14), 0.75(C7 H8)'
_chemical_formula_sum            'C63.75 H60.5 Ge O3 P4 Rh'
_chemical_formula_weight         1174.00
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      15
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_cell_angle_alpha                90.00
_cell_angle_beta                 106.5372(15)
_cell_angle_gamma                90.00
_cell_formula_units_Z            16
_cell_length_a                   24.2964(9)
_cell_length_b                   24.2266(7)
_cell_length_c                   39.8765(16)
_cell_measurement_reflns_used    28071
_cell_measurement_temperature    200(2)
_cell_measurement_theta_max      27.4835
_cell_measurement_theta_min      4.0112
_cell_volume                     22501.2(14)
_computing_cell_refinement       CrystalClear
_computing_data_collection       'CrystalClear (Rigaku, 2001)'
_computing_molecular_graphics    'Ortep-3 for Windows (Farrugia, 1997)'
_computing_publication_material  SHELXL97
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      200(2)
_diffrn_detector_area_resol_mean 7.32
_diffrn_measured_fraction_theta_full 0.984
_diffrn_measured_fraction_theta_max 0.984
_diffrn_measurement_details
;
scan:
    Number of images: 1800
               Slice: -80.0000 - 100.0000
         Image width: 0.1000
            Exp time: 15.0000
       Rotation axis: Phi
               Omega: 0.0000
                 Chi: 0.0000
                 Phi: 0.0000
                 XTD: 55.1588
              2theta: 24.8277
scan:
    Number of images: 600
               Slice: -15.0000 - 45.0000
         Image width: 0.1000
            Exp time: 15.0000
       Rotation axis: Omega
               Omega: 0.0000
                 Chi: 90.0000
                 Phi: 0.0000
                 XTD: 55.1588
              2theta: 24.8277
scan:
    Number of images: 600
               Slice: -15.0000 - 45.0000
         Image width: 0.1000
            Exp time: 15.0000
       Rotation axis: Omega
               Omega: 0.0000
                 Chi: 90.0000
                 Phi: 90.0000
                 XTD: 55.1588
              2theta: 24.8277
scan:
    Number of images: 600
               Slice: -15.0000 - 45.0000
         Image width: 0.1000
            Exp time: 15.0000
       Rotation axis: Omega
               Omega: 0.0000
                 Chi: 90.0000
                 Phi: 180.0000
                 XTD: 55.1588
              2theta: 24.8277
scan:
    Number of images: 600
               Slice: -15.0000 - 45.0000
         Image width: 0.1000
            Exp time: 15.0000
       Rotation axis: Omega
               Omega: 0.0000
                 Chi: 90.0000
                 Phi: 270.0000
                 XTD: 55.1588
              2theta: 24.8277

;
_diffrn_measurement_device       'Mercury CCD (2x2 bin mode)'
_diffrn_measurement_device_details 'AFC7: Eulerian 3-circle'
_diffrn_measurement_device_type  'Rigaku/MSC Mercury CCD'
_diffrn_measurement_method       'ω or φ'
_diffrn_radiation_detector       CCD
_diffrn_radiation_monochromator  'Graphite Monochromator'
_diffrn_radiation_source         'Rotating Anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71070
_diffrn_reflns_av_R_equivalents  0.0360
_diffrn_reflns_av_sigmaI/netI    0.0328
_diffrn_reflns_limit_h_max       31
_diffrn_reflns_limit_h_min       -31
_diffrn_reflns_limit_k_max       31
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       51
_diffrn_reflns_limit_l_min       -49
_diffrn_reflns_number            86883
_diffrn_reflns_reduction_process 'Lp corrections applied'
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         4.01
_diffrn_source_current           280.0000
_diffrn_source_power             16.8000
_diffrn_source_voltage           60.0000
_exptl_absorpt_coefficient_mu    0.987
_exptl_absorpt_correction_T_max  0.9710
_exptl_absorpt_correction_T_min  0.6936
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   '(Jacobson, 1998)'
_exptl_crystal_colour            Yellow
_exptl_crystal_density_diffrn    1.386
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       Platelet
_exptl_crystal_F_000             9664
_exptl_crystal_preparation
'mounted on the CryoLoop with Palaton oil and placed in N2 stream at 200(2) K'
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.03
_refine_diff_density_max         1.046
_refine_diff_density_min         -1.348
_refine_diff_density_rms         0.096
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.232
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1195
_refine_ls_number_reflns         25416
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.232
_refine_ls_R_factor_all          0.0695
_refine_ls_R_factor_gt           0.0629
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0415P)²+146.4319P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1385
_refine_ls_wR_factor_ref         0.1415
_reflns_number_gt                23663
_reflns_number_total             25416
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om2011276_si_002.cif
_cod_data_source_block           9
_cod_depositor_comments
;
The following automatic conversions were performed:

'_exptl_absorpt_correction_type' value 'Multi-scan' changed to
'multi-scan' according to
/home/saulius/struct/CIF-dictionaries/cif_core.dic dictionary named
'cif_core.dic' version 2.4.1 from 2010-06-29.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_sg_symbol_H-M      C2/c
_cod_original_formula_sum        'C63.75 H60.50 Ge O3 P4 Rh'
_cod_database_code               4076374
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Rh1 Rh 0.166843(13) 0.162399(12) 0.102502(8) 0.01981(7) Uani 1 1 d . . .
Ge1 Ge 0.118380(18) 0.213248(17) 0.136486(11) 0.02048(9) Uani 1 1 d . . .
P1 P 0.14473(4) 0.23973(4) 0.06692(3) 0.0213(2) Uani 1 1 d . . .
C1 C 0.07976(17) 0.27746(16) 0.10993(11) 0.0229(8) Uani 1 1 d . . .
C2 C 0.04317(19) 0.31376(18) 0.12032(12) 0.0297(9) Uani 1 1 d . . .
H2 H 0.0339 0.3070 0.1415 0.036 Uiso 1 1 calc R . .
C3 C 0.02027(19) 0.35914(18) 0.10057(13) 0.0321(10) Uani 1 1 d . . .
H3 H -0.0049 0.3832 0.1080 0.039 Uiso 1 1 calc R . .
C4 C 0.03405(19) 0.36961(18) 0.06979(13) 0.0318(10) Uani 1 1 d . . .
H4 H 0.0185 0.4010 0.0561 0.038 Uiso 1 1 calc R . .
C5 C 0.0706(2) 0.33427(18) 0.05899(12) 0.0304(9) Uani 1 1 d . . .
H5 H 0.0802 0.3418 0.0380 0.036 Uiso 1 1 calc R . .
C6 C 0.09350(17) 0.28766(17) 0.07875(11) 0.0236(8) Uani 1 1 d . . .
C7 C 0.11418(17) 0.23047(18) 0.01905(10) 0.0245(8) Uani 1 1 d . . .
C8 C 0.10982(19) 0.27286(19) -0.00559(11) 0.0301(9) Uani 1 1 d . . .
H8 H 0.1225 0.3090 0.0022 0.036 Uiso 1 1 calc R . .
C9 C 0.0875(2) 0.2628(2) -0.04094(12) 0.0359(10) Uani 1 1 d . . .
H9 H 0.0846 0.2920 -0.0573 0.043 Uiso 1 1 calc R . .
C10 C 0.0692(2) 0.2104(2) -0.05255(12) 0.0385(11) Uani 1 1 d . . .
H10 H 0.0541 0.2034 -0.0769 0.046 Uiso 1 1 calc R . .
C11 C 0.0730(2) 0.1680(2) -0.02885(12) 0.0371(11) Uani 1 1 d . . .
H11 H 0.0602 0.1320 -0.0368 0.044 Uiso 1 1 calc R . .
C12 C 0.09561(19) 0.17843(19) 0.00677(11) 0.0299(9) Uani 1 1 d . . .
H12 H 0.0984 0.1491 0.0230 0.036 Uiso 1 1 calc R . .
C13 C 0.20303(17) 0.28887(17) 0.06772(11) 0.0245(8) Uani 1 1 d . . .
C14 C 0.21894(19) 0.32821(18) 0.09427(12) 0.0303(9) Uani 1 1 d . . .
H14 H 0.1975 0.3315 0.1107 0.036 Uiso 1 1 calc R . .
C15 C 0.2654(2) 0.36230(19) 0.09690(14) 0.0379(11) Uani 1 1 d . . .
H15 H 0.2762 0.3886 0.1153 0.046 Uiso 1 1 calc R . .
C16 C 0.2966(2) 0.3582(2) 0.07272(15) 0.0406(12) Uani 1 1 d . . .
H16 H 0.3283 0.3820 0.0744 0.049 Uiso 1 1 calc R . .
C17 C 0.2814(2) 0.3198(2) 0.04649(14) 0.0368(11) Uani 1 1 d . . .
H17 H 0.3026 0.3170 0.0299 0.044 Uiso 1 1 calc R . .
C18 C 0.23535(19) 0.28518(19) 0.04401(12) 0.0305(9) Uani 1 1 d . . .
H18 H 0.2255 0.2584 0.0259 0.037 Uiso 1 1 calc R . .
P2 P 0.24094(5) 0.16600(5) 0.15408(3) 0.0246(2) Uani 1 1 d . . .
C19 C 0.17416(18) 0.24010(16) 0.17917(10) 0.0236(8) Uani 1 1 d . . .
C20 C 0.1637(2) 0.27830(17) 0.20281(11) 0.0281(9) Uani 1 1 d . . .
H20 H 0.1260 0.2923 0.1995 0.034 Uiso 1 1 calc R . .
C21 C 0.2080(2) 0.29588(18) 0.23115(11) 0.0345(10) Uani 1 1 d . . .
H21 H 0.2007 0.3224 0.2469 0.041 Uiso 1 1 calc R . .
C22 C 0.2621(2) 0.2753(2) 0.23646(12) 0.0356(10) Uani 1 1 d . . .
H22 H 0.2921 0.2878 0.2559 0.043 Uiso 1 1 calc R . .
C23 C 0.2739(2) 0.2367(2) 0.21401(11) 0.0331(10) Uani 1 1 d . . .
H23 H 0.3116 0.2224 0.2182 0.040 Uiso 1 1 calc R . .
C24 C 0.22963(18) 0.21862(17) 0.18486(11) 0.0257(8) Uani 1 1 d . . .
C25 C 0.31462(18) 0.1837(2) 0.15421(11) 0.0290(9) Uani 1 1 d . . .
C26 C 0.3204(2) 0.2218(2) 0.12938(15) 0.0445(12) Uani 1 1 d . . .
H26 H 0.2871 0.2343 0.1121 0.053 Uiso 1 1 calc R . .
C27 C 0.3733(2) 0.2417(3) 0.12922(19) 0.0599(17) Uani 1 1 d . . .
H27 H 0.3762 0.2684 0.1124 0.072 Uiso 1 1 calc R . .
C28 C 0.4225(2) 0.2228(3) 0.15371(18) 0.0561(16) Uani 1 1 d . . .
H28 H 0.4592 0.2361 0.1535 0.067 Uiso 1 1 calc R . .
C29 C 0.4180(2) 0.1852(3) 0.17790(17) 0.0548(15) Uani 1 1 d . . .
H29 H 0.4517 0.1720 0.1945 0.066 Uiso 1 1 calc R . .
C30 C 0.3646(2) 0.1658(3) 0.17859(14) 0.0456(13) Uani 1 1 d . . .
H30 H 0.3621 0.1399 0.1960 0.055 Uiso 1 1 calc R . .
C31 C 0.2517(2) 0.10460(19) 0.18260(11) 0.0311(9) Uani 1 1 d . . .
C32 C 0.2196(2) 0.0987(2) 0.20616(13) 0.0414(11) Uani 1 1 d . . .
H32 H 0.1943 0.1274 0.2085 0.050 Uiso 1 1 calc R . .
C33 C 0.2240(3) 0.0514(2) 0.22627(16) 0.0565(16) Uani 1 1 d . . .
H33 H 0.2018 0.0480 0.2423 0.068 Uiso 1 1 calc R . .
C34 C 0.2601(3) 0.0095(3) 0.22322(16) 0.0615(17) Uani 1 1 d . . .
H34 H 0.2633 -0.0226 0.2373 0.074 Uiso 1 1 calc R . .
C35 C 0.2918(3) 0.0140(2) 0.19965(16) 0.0550(15) Uani 1 1 d . . .
H35 H 0.3165 -0.0153 0.1973 0.066 Uiso 1 1 calc R . .
C36 C 0.2879(2) 0.0613(2) 0.17917(13) 0.0416(12) Uani 1 1 d . . .
H36 H 0.3097 0.0642 0.1629 0.050 Uiso 1 1 calc R . .
P3 P 0.09255(5) 0.10097(4) 0.09999(3) 0.0230(2) Uani 1 1 d . . .
C37 C 0.06123(17) 0.16654(17) 0.14875(10) 0.0229(8) Uani 1 1 d . . .
C38 C 0.02970(18) 0.18051(18) 0.17175(11) 0.0272(9) Uani 1 1 d . . .
H38 H 0.0353 0.2155 0.1830 0.033 Uiso 1 1 calc R . .
C39 C -0.0099(2) 0.1438(2) 0.17853(12) 0.0332(10) Uani 1 1 d . . .
H39 H -0.0314 0.1537 0.1942 0.040 Uiso 1 1 calc R . .
C40 C -0.0177(2) 0.0931(2) 0.16241(13) 0.0388(11) Uani 1 1 d . . .
H40 H -0.0446 0.0679 0.1671 0.047 Uiso 1 1 calc R . .
C41 C 0.0131(2) 0.0784(2) 0.13950(13) 0.0365(10) Uani 1 1 d . . .
H41 H 0.0072 0.0432 0.1285 0.044 Uiso 1 1 calc R . .
C42 C 0.05276(18) 0.11498(17) 0.13242(11) 0.0252(8) Uani 1 1 d . . .
C43 C 0.1061(2) 0.02609(17) 0.10535(12) 0.0293(9) Uani 1 1 d . . .
C44 C 0.0646(2) -0.01464(19) 0.09340(13) 0.0369(11) Uani 1 1 d . . .
H44 H 0.0262 -0.0042 0.0819 0.044 Uiso 1 1 calc R . .
C45 C 0.0786(3) -0.0702(2) 0.09802(15) 0.0481(13) Uani 1 1 d . . .
H45 H 0.0500 -0.0976 0.0896 0.058 Uiso 1 1 calc R . .
C46 C 0.1340(3) -0.0856(2) 0.11473(17) 0.0569(16) Uani 1 1 d . . .
H46 H 0.1438 -0.1236 0.1178 0.068 Uiso 1 1 calc R . .
C47 C 0.1752(3) -0.0461(2) 0.12694(17) 0.0527(15) Uani 1 1 d . . .
H47 H 0.2135 -0.0569 0.1385 0.063 Uiso 1 1 calc R . .
C48 C 0.1616(2) 0.0094(2) 0.12252(14) 0.0389(11) Uani 1 1 d . . .
H48 H 0.1905 0.0363 0.1313 0.047 Uiso 1 1 calc R . .
C49 C 0.03279(18) 0.10323(16) 0.05990(11) 0.0247(8) Uani 1 1 d . . .
C50 C -0.0088(2) 0.1442(2) 0.05586(12) 0.0341(10) Uani 1 1 d . . .
H50 H -0.0072 0.1688 0.0747 0.041 Uiso 1 1 calc R . .
C51 C -0.0526(2) 0.1500(2) 0.02481(13) 0.0410(12) Uani 1 1 d . . .
H51 H -0.0805 0.1782 0.0227 0.049 Uiso 1 1 calc R . .
C52 C -0.0557(2) 0.1147(2) -0.00293(13) 0.0394(11) Uani 1 1 d . . .
H52 H -0.0859 0.1182 -0.0240 0.047 Uiso 1 1 calc R . .
C53 C -0.0141(2) 0.0741(2) 0.00044(13) 0.0363(10) Uani 1 1 d . . .
H53 H -0.0158 0.0500 -0.0186 0.044 Uiso 1 1 calc R . .
C54 C 0.0296(2) 0.06852(17) 0.03108(11) 0.0297(9) Uani 1 1 d . . .
H54 H 0.0580 0.0409 0.0328 0.036 Uiso 1 1 calc R . .
P4 P 0.21219(5) 0.11097(5) 0.07169(3) 0.0274(2) Uani 1 1 d . . .
O1 O 0.23987(16) 0.13667(19) 0.04305(10) 0.0536(10) Uani 1 1 d . . .
C55 C 0.2962(3) 0.1537(3) 0.04899(18) 0.0585(16) Uani 1 1 d . . .
H55 H 0.3025 0.1874 0.0632 0.088 Uiso 1 1 calc R . .
H55A H 0.3038 0.1611 0.0266 0.088 Uiso 1 1 calc R . .
H55B H 0.3221 0.1247 0.0615 0.088 Uiso 1 1 calc R . .
O2 O 0.26529(15) 0.07679(14) 0.09627(9) 0.0380(8) Uani 1 1 d . . .
C56 C 0.2890(3) 0.0281(2) 0.08567(18) 0.0584(17) Uani 1 1 d . . .
H56 H 0.2620 -0.0026 0.0838 0.088 Uiso 1 1 calc R . .
H56A H 0.3253 0.0190 0.1030 0.088 Uiso 1 1 calc R . .
H56B H 0.2958 0.0344 0.0629 0.088 Uiso 1 1 calc R . .
O3 O 0.17232(16) 0.06539(14) 0.04741(9) 0.0413(8) Uani 1 1 d . . .
C57 C 0.1776(3) 0.0436(3) 0.01499(16) 0.0668(19) Uani 1 1 d . . .
H57 H 0.1642 0.0711 -0.0036 0.100 Uiso 1 1 calc R . .
H57A H 0.1544 0.0101 0.0089 0.100 Uiso 1 1 calc R . .
H57B H 0.2179 0.0347 0.0175 0.100 Uiso 1 1 calc R . .
Rh2 Rh 0.290088(13) 0.125091(12) 0.397770(7) 0.01813(7) Uani 1 1 d . . .
Ge2 Ge 0.223478(18) 0.062472(16) 0.361975(11) 0.02028(9) Uani 1 1 d . . .
P5 P 0.26429(5) 0.17732(4) 0.34703(3) 0.0230(2) Uani 1 1 d . . .
C58 C 0.17930(17) 0.09920(17) 0.31899(10) 0.0231(8) Uani 1 1 d . . .
C59 C 0.13211(19) 0.07759(19) 0.29342(11) 0.0293(9) Uani 1 1 d . . .
H59 H 0.1175 0.0423 0.2968 0.035 Uiso 1 1 calc R . .
C60 C 0.1065(2) 0.1069(2) 0.26332(12) 0.0366(11) Uani 1 1 d . . .
H60 H 0.0743 0.0920 0.2462 0.044 Uiso 1 1 calc R . .
C61 C 0.1281(2) 0.1584(2) 0.25823(12) 0.0399(11) Uani 1 1 d . . .
H61 H 0.1105 0.1786 0.2375 0.048 Uiso 1 1 calc R . .
C62 C 0.1746(2) 0.1803(2) 0.28287(12) 0.0351(10) Uani 1 1 d . . .
H62 H 0.1893 0.2153 0.2790 0.042 Uiso 1 1 calc R . .
C63 C 0.20038(18) 0.15110(17) 0.31369(10) 0.0239(8) Uani 1 1 d . . .
C64 C 0.31518(19) 0.1794(2) 0.32046(11) 0.0315(9) Uani 1 1 d . . .
C65 C 0.3138(2) 0.1373(2) 0.29663(13) 0.0411(11) Uani 1 1 d . . .
H65 H 0.2848 0.1098 0.2930 0.049 Uiso 1 1 calc R . .
C66 C 0.3540(3) 0.1346(3) 0.27811(16) 0.0574(16) Uani 1 1 d . . .
H66 H 0.3524 0.1053 0.2620 0.069 Uiso 1 1 calc R . .
C67 C 0.3959(3) 0.1738(4) 0.28289(17) 0.065(2) Uani 1 1 d . . .
H67 H 0.4232 0.1720 0.2700 0.078 Uiso 1 1 calc R . .
C68 C 0.3986(2) 0.2158(3) 0.30631(16) 0.0581(17) Uani 1 1 d . . .
H68 H 0.4278 0.2431 0.3095 0.070 Uiso 1 1 calc R . .
C69 C 0.3589(2) 0.2188(2) 0.32550(13) 0.0438(12) Uani 1 1 d . . .
H69 H 0.3615 0.2476 0.3420 0.053 Uiso 1 1 calc R . .
C70 C 0.24278(19) 0.25021(17) 0.34791(11) 0.0262(8) Uani 1 1 d . . .
C71 C 0.2520(2) 0.2918(2) 0.32591(12) 0.0393(11) Uani 1 1 d . . .
H71 H 0.2729 0.2837 0.3097 0.047 Uiso 1 1 calc R . .
C72 C 0.2311(3) 0.34450(19) 0.32738(13) 0.0426(12) Uani 1 1 d . . .
H72 H 0.2386 0.3724 0.3125 0.051 Uiso 1 1 calc R . .
C73 C 0.1999(3) 0.3570(2) 0.34990(15) 0.0461(13) Uani 1 1 d . . .
H73 H 0.1853 0.3932 0.3506 0.055 Uiso 1 1 calc R . .
C74 C 0.1898(3) 0.3166(2) 0.37163(17) 0.0512(14) Uani 1 1 d . . .
H74 H 0.1683 0.3250 0.3875 0.061 Uiso 1 1 calc R . .
C75 C 0.2110(2) 0.2640(2) 0.37052(14) 0.0408(12) Uani 1 1 d . . .
H75 H 0.2036 0.2365 0.3857 0.049 Uiso 1 1 calc R . .
P6 P 0.22941(4) 0.11654(4) 0.43312(3) 0.01960(19) Uani 1 1 d . . .
C76 C 0.17238(17) 0.03347(16) 0.38812(11) 0.0237(8) Uani 1 1 d . . .
C77 C 0.13260(19) -0.00934(17) 0.37679(12) 0.0296(9) Uani 1 1 d . . .
H77 H 0.1295 -0.0270 0.3551 0.035 Uiso 1 1 calc R . .
C78 C 0.0977(2) -0.02613(18) 0.39708(13) 0.0339(10) Uani 1 1 d . . .
H78 H 0.0709 -0.0553 0.3893 0.041 Uiso 1 1 calc R . .
C79 C 0.1020(2) -0.0002(2) 0.42864(13) 0.0348(10) Uani 1 1 d . . .
H79 H 0.0781 -0.0116 0.4425 0.042 Uiso 1 1 calc R . .
C80 C 0.1412(2) 0.04222(19) 0.44020(12) 0.0310(9) Uani 1 1 d . . .
H80 H 0.1437 0.0600 0.4618 0.037 Uiso 1 1 calc R . .
C81 C 0.17681(17) 0.05883(16) 0.42011(10) 0.0225(8) Uani 1 1 d . . .
C82 C 0.17941(17) 0.17345(16) 0.43365(10) 0.0217(8) Uani 1 1 d . . .
C83 C 0.12746(19) 0.17761(17) 0.40745(11) 0.0270(8) Uani 1 1 d . . .
H83 H 0.1161 0.1490 0.3906 0.032 Uiso 1 1 calc R . .
C84 C 0.09221(19) 0.22316(18) 0.40587(12) 0.0316(9) Uani 1 1 d . . .
H84 H 0.0570 0.2256 0.3878 0.038 Uiso 1 1 calc R . .
C85 C 0.1078(2) 0.26511(18) 0.43035(13) 0.0322(10) Uani 1 1 d . . .
H85 H 0.0831 0.2958 0.4295 0.039 Uiso 1 1 calc R . .
C86 C 0.1597(2) 0.26171(17) 0.45613(12) 0.0306(9) Uani 1 1 d . . .
H86 H 0.1711 0.2905 0.4728 0.037 Uiso 1 1 calc R . .
C87 C 0.19525(18) 0.21631(17) 0.45768(11) 0.0256(8) Uani 1 1 d . . .
H87 H 0.2309 0.2145 0.4754 0.031 Uiso 1 1 calc R . .
C88 C 0.26031(18) 0.10607(16) 0.48075(10) 0.0235(8) Uani 1 1 d . . .
C89 C 0.2296(2) 0.11143(17) 0.50546(11) 0.0290(9) Uani 1 1 d . . .
H89 H 0.1899 0.1205 0.4978 0.035 Uiso 1 1 calc R . .
C90 C 0.2559(2) 0.10375(18) 0.54074(12) 0.0339(10) Uani 1 1 d . . .
H90 H 0.2341 0.1070 0.5570 0.041 Uiso 1 1 calc R . .
C91 C 0.3138(2) 0.09127(18) 0.55234(12) 0.0356(11) Uani 1 1 d . . .
H91 H 0.3320 0.0865 0.5766 0.043 Uiso 1 1 calc R . .
C92 C 0.3450(2) 0.08578(19) 0.52840(12) 0.0332(10) Uani 1 1 d . . .
H92 H 0.3847 0.0768 0.5363 0.040 Uiso 1 1 calc R . .
C93 C 0.31857(19) 0.09335(17) 0.49303(11) 0.0277(9) Uani 1 1 d . . .
H93 H 0.3405 0.0898 0.4769 0.033 Uiso 1 1 calc R . .
P7 P 0.35209(4) 0.05099(4) 0.40029(3) 0.0225(2) Uani 1 1 d . . .
C94 C 0.26445(19) 0.00039(17) 0.34873(11) 0.0271(9) Uani 1 1 d . . .
C95 C 0.2408(2) -0.04049(19) 0.32448(13) 0.0361(10) Uani 1 1 d . . .
H95 H 0.2014 -0.0383 0.3116 0.043 Uiso 1 1 calc R . .
C96 C 0.2733(3) -0.0841(2) 0.31885(15) 0.0470(13) Uani 1 1 d . . .
H96 H 0.2563 -0.1119 0.3023 0.056 Uiso 1 1 calc R . .
C97 C 0.3300(3) -0.0875(2) 0.33710(16) 0.0511(15) Uani 1 1 d . . .
H97 H 0.3523 -0.1176 0.3331 0.061 Uiso 1 1 calc R . .
C98 C 0.3552(2) -0.0475(2) 0.36138(14) 0.0429(12) Uani 1 1 d . . .
H98 H 0.3947 -0.0503 0.3741 0.052 Uiso 1 1 calc R . .
C99 C 0.32246(19) -0.00290(17) 0.36707(11) 0.0264(8) Uani 1 1 d . . .
C100 C 0.36834(18) 0.00808(17) 0.44026(11) 0.0256(8) Uani 1 1 d . . .
C101 C 0.3289(2) -0.03181(19) 0.44324(13) 0.0344(10) Uani 1 1 d . . .
H101 H 0.2957 -0.0383 0.4242 0.041 Uiso 1 1 calc R . .
C102 C 0.3374(2) -0.0622(2) 0.47372(13) 0.0409(11) Uani 1 1 d . . .
H102 H 0.3098 -0.0890 0.4755 0.049 Uiso 1 1 calc R . .
C103 C 0.3853(2) -0.0539(2) 0.50134(13) 0.0396(11) Uani 1 1 d . . .
H103 H 0.3915 -0.0755 0.5219 0.048 Uiso 1 1 calc R . .
C104 C 0.4244(2) -0.0138(2) 0.49901(12) 0.0355(10) Uani 1 1 d . . .
H104 H 0.4574 -0.0076 0.5182 0.043 Uiso 1 1 calc R . .
C105 C 0.41579(19) 0.01722(18) 0.46883(11) 0.0286(9) Uani 1 1 d . . .
H105 H 0.4426 0.0451 0.4676 0.034 Uiso 1 1 calc R . .
C106 C 0.42462(18) 0.06219(19) 0.39530(11) 0.0285(9) Uani 1 1 d . . .
C107 C 0.4708(2) 0.0260(2) 0.40773(13) 0.0379(11) Uani 1 1 d . . .
H107 H 0.4655 -0.0072 0.4191 0.045 Uiso 1 1 calc R . .
C108 C 0.5242(2) 0.0380(3) 0.40372(16) 0.0493(14) Uani 1 1 d . . .
H108 H 0.5554 0.0135 0.4128 0.059 Uiso 1 1 calc R . .
C109 C 0.5325(2) 0.0857(3) 0.38658(17) 0.0557(16) Uani 1 1 d . . .
H109 H 0.5691 0.0940 0.3838 0.067 Uiso 1 1 calc R . .
C110 C 0.4868(2) 0.1207(3) 0.37358(16) 0.0515(15) Uani 1 1 d . . .
H110 H 0.4920 0.1531 0.3614 0.062 Uiso 1 1 calc R . .
C111 C 0.4336(2) 0.1095(2) 0.37799(13) 0.0379(11) Uani 1 1 d . . .
H111 H 0.4028 0.1345 0.3691 0.046 Uiso 1 1 calc R . .
P8 P 0.35691(5) 0.18288(4) 0.42973(3) 0.0253(2) Uani 1 1 d . . .
O4 O 0.38121(14) 0.22397(14) 0.40564(8) 0.0355(7) Uani 1 1 d . . .
C112 C 0.4348(2) 0.2531(3) 0.41770(17) 0.0527(15) Uani 1 1 d . . .
H112 H 0.4357 0.2738 0.4390 0.079 Uiso 1 1 calc R . .
H113 H 0.4388 0.2788 0.3995 0.079 Uiso 1 1 calc R . .
H114 H 0.4666 0.2266 0.4228 0.079 Uiso 1 1 calc R . .
O5 O 0.34701(17) 0.22449(13) 0.45886(9) 0.0412(8) Uani 1 1 d . . .
C113 C 0.3189(3) 0.2757(2) 0.44974(16) 0.0464(13) Uani 1 1 d . . .
H115 H 0.3395 0.2978 0.4366 0.070 Uiso 1 1 calc R . .
H116 H 0.3183 0.2956 0.4710 0.070 Uiso 1 1 calc R . .
H117 H 0.2794 0.2694 0.4353 0.070 Uiso 1 1 calc R . .
O6 O 0.41236(15) 0.15225(14) 0.45402(9) 0.0393(8) Uani 1 1 d . . .
C114 C 0.4501(3) 0.1719(3) 0.48672(15) 0.0591(17) Uani 1 1 d . . .
H118 H 0.4474 0.2122 0.4877 0.089 Uiso 1 1 calc R . .
H119 H 0.4897 0.1613 0.4884 0.089 Uiso 1 1 calc R . .
H120 H 0.4387 0.1556 0.5062 0.089 Uiso 1 1 calc R . .
C115 C 0.4727 0.3653 0.3334 0.200 Uiso 0.50 1 d P . .
C116 C 0.5451 0.3612 0.3279 0.200 Uiso 0.50 1 d P . .
C117 C 0.6015 0.3581 0.3019 0.200 Uiso 0.50 1 d P . .
C118 C 0.6011 0.3933 0.2664 0.200 Uiso 0.50 1 d P . .
C119 C 0.6288 0.4020 0.2320 0.200 Uiso 0.50 1 d P . .
C120 C 0.6014 0.4475 0.2057 0.200 Uiso 0.50 1 d P . .
C121 C -0.0269 0.5065 0.1908 0.100 Uiso 0.50 1 d P A 1
C122 C 0.0317 0.5055 0.1943 0.100 Uiso 0.50 1 d P A 1
C123 C 0.0703 0.5252 0.2248 0.100 Uiso 0.50 1 d P A 1
C124 C 0.0503 0.5458 0.2517 0.100 Uiso 0.50 1 d P . 1
C125 C -0.0083 0.5468 0.2481 0.100 Uiso 0.50 1 d P . 1
C126 C -0.0469 0.5272 0.2176 0.100 Uiso 0.50 1 d P . 1
C127 C -0.0768 0.4795 0.1673 0.100 Uiso 0.50 1 d P A 1
C128 C 0.0399 0.3444 0.2274 0.100 Uiso 0.50 1 d P B 2
C129 C -0.0111 0.3430 0.2005 0.100 Uiso 0.50 1 d P B 2
C130 C -0.0529 0.3042 0.2009 0.100 Uiso 0.50 1 d P . 2
C131 C -0.0438 0.2667 0.2284 0.100 Uiso 0.50 1 d P . 2
C132 C 0.0072 0.2681 0.2553 0.100 Uiso 0.50 1 d P . 2
C133 C 0.0490 0.3069 0.2548 0.101 Uiso 0.50 1 d P . 2
C134 C 0.0845 0.3938 0.2312 0.100 Uiso 0.50 1 d P B 2
C135 C 0.0615 0.3862 0.2266 0.100 Uiso 0.50 1 d P C 3
C136 C 0.0126 0.4022 0.2006 0.100 Uiso 0.50 1 d P C 3
C137 C 0.0129 0.4508 0.1821 0.100 Uiso 0.50 1 d P C 3
C138 C 0.0620 0.4833 0.1896 0.100 Uiso 0.50 1 d P C 3
C139 C 0.1108 0.4673 0.2156 0.100 Uiso 0.50 1 d P C 3
C140 C 0.1106 0.4187 0.2341 0.100 Uiso 0.50 1 d P C 3
C141 C 0.0588 0.3461 0.2392 0.100 Uiso 0.50 1 d P C 3
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Rh Rh -1.1178 0.9187 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
P4 Rh1 P2 97.37(4) . .
P4 Rh1 P1 100.24(4) . .
P2 Rh1 P1 119.92(4) . .
P4 Rh1 P3 96.73(4) . .
P2 Rh1 P3 117.44(4) . .
P1 Rh1 P3 116.75(4) . .
P4 Rh1 Ge1 177.47(3) . .
P2 Rh1 Ge1 81.96(3) . .
P1 Rh1 Ge1 82.19(3) . .
P3 Rh1 Ge1 81.46(3) . .
C37 Ge1 C19 109.82(16) . .
C37 Ge1 C1 109.18(17) . .
C19 Ge1 C1 108.14(16) . .
C37 Ge1 Rh1 110.15(12) . .
C19 Ge1 Rh1 109.56(12) . .
C1 Ge1 Rh1 109.96(12) . .
C13 P1 C7 100.15(19) . .
C13 P1 C6 99.14(18) . .
C7 P1 C6 103.65(18) . .
C13 P1 Rh1 117.91(13) . .
C7 P1 Rh1 119.16(14) . .
C6 P1 Rh1 113.87(14) . .
C2 C1 C6 119.1(4) . .
C2 C1 Ge1 125.9(3) . .
C6 C1 Ge1 114.9(3) . .
C3 C2 C1 121.5(4) . .
C3 C2 H2 119.3 . .
C1 C2 H2 119.3 . .
C2 C3 C4 119.6(4) . .
C2 C3 H3 120.2 . .
C4 C3 H3 120.2 . .
C3 C4 C5 120.0(4) . .
C3 C4 H4 120.0 . .
C5 C4 H4 120.0 . .
C4 C5 C6 120.7(4) . .
C4 C5 H5 119.6 . .
C6 C5 H5 119.6 . .
C1 C6 C5 119.1(4) . .
C1 C6 P1 117.5(3) . .
C5 C6 P1 123.3(3) . .
C12 C7 C8 117.9(4) . .
C12 C7 P1 118.0(3) . .
C8 C7 P1 124.1(3) . .
C9 C8 C7 121.0(4) . .
C9 C8 H8 119.5 . .
C7 C8 H8 119.5 . .
C8 C9 C10 120.0(4) . .
C8 C9 H9 120.0 . .
C10 C9 H9 120.0 . .
C11 C10 C9 120.1(4) . .
C11 C10 H10 119.9 . .
C9 C10 H10 119.9 . .
C10 C11 C12 119.5(5) . .
C10 C11 H11 120.2 . .
C12 C11 H11 120.2 . .
C7 C12 C11 121.4(4) . .
C7 C12 H12 119.3 . .
C11 C12 H12 119.3 . .
C18 C13 C14 118.1(4) . .
C18 C13 P1 121.7(3) . .
C14 C13 P1 120.0(3) . .
C15 C14 C13 120.7(4) . .
C15 C14 H14 119.6 . .
C13 C14 H14 119.6 . .
C14 C15 C16 120.1(5) . .
C14 C15 H15 120.0 . .
C16 C15 H15 120.0 . .
C17 C16 C15 119.8(4) . .
C17 C16 H16 120.1 . .
C15 C16 H16 120.1 . .
C16 C17 C18 120.3(5) . .
C16 C17 H17 119.8 . .
C18 C17 H17 119.8 . .
C17 C18 C13 121.0(4) . .
C17 C18 H18 119.5 . .
C13 C18 H18 119.5 . .
C25 P2 C24 99.6(2) . .
C25 P2 C31 102.6(2) . .
C24 P2 C31 99.7(2) . .
C25 P2 Rh1 121.39(14) . .
C24 P2 Rh1 113.05(14) . .
C31 P2 Rh1 117.06(15) . .
C20 C19 C24 119.3(4) . .
C20 C19 Ge1 126.3(3) . .
C24 C19 Ge1 114.4(3) . .
C21 C20 C19 120.3(4) . .
C21 C20 H20 119.9 . .
C19 C20 H20 119.9 . .
C22 C21 C20 120.3(4) . .
C22 C21 H21 119.8 . .
C20 C21 H21 119.8 . .
C21 C22 C23 121.0(4) . .
C21 C22 H22 119.5 . .
C23 C22 H22 119.5 . .
C22 C23 C24 119.7(4) . .
C22 C23 H23 120.2 . .
C24 C23 H23 120.2 . .
C19 C24 C23 119.4(4) . .
C19 C24 P2 117.9(3) . .
C23 C24 P2 122.8(3) . .
C26 C25 C30 117.4(4) . .
C26 C25 P2 116.6(3) . .
C30 C25 P2 125.7(4) . .
C27 C26 C25 121.4(5) . .
C27 C26 H26 119.3 . .
C25 C26 H26 119.3 . .
C26 C27 C28 120.0(6) . .
C26 C27 H27 120.0 . .
C28 C27 H27 120.0 . .
C29 C28 C27 119.7(5) . .
C29 C28 H28 120.2 . .
C27 C28 H28 120.2 . .
C28 C29 C30 120.5(5) . .
C28 C29 H29 119.7 . .
C30 C29 H29 119.7 . .
C29 C30 C25 121.0(5) . .
C29 C30 H30 119.5 . .
C25 C30 H30 119.5 . .
C32 C31 C36 118.6(5) . .
C32 C31 P2 119.4(4) . .
C36 C31 P2 121.8(4) . .
C33 C32 C31 120.8(5) . .
C33 C32 H32 119.6 . .
C31 C32 H32 119.6 . .
C34 C33 C32 120.5(6) . .
C34 C33 H33 119.8 . .
C32 C33 H33 119.8 . .
C33 C34 C35 120.0(5) . .
C33 C34 H34 120.0 . .
C35 C34 H34 120.0 . .
C34 C35 C36 120.3(6) . .
C34 C35 H35 119.9 . .
C36 C35 H35 119.9 . .
C35 C36 C31 120.0(5) . .
C35 C36 H36 120.0 . .
C31 C36 H36 120.0 . .
C49 P3 C43 101.6(2) . .
C49 P3 C42 99.33(19) . .
C43 P3 C42 102.1(2) . .
C49 P3 Rh1 115.66(14) . .
C43 P3 Rh1 121.01(15) . .
C42 P3 Rh1 113.98(13) . .
C38 C37 C42 119.2(4) . .
C38 C37 Ge1 125.9(3) . .
C42 C37 Ge1 114.9(3) . .
C39 C38 C37 120.8(4) . .
C39 C38 H38 119.6 . .
C37 C38 H38 119.6 . .
C40 C39 C38 119.4(4) . .
C40 C39 H39 120.3 . .
C38 C39 H39 120.3 . .
C39 C40 C41 120.7(4) . .
C39 C40 H40 119.6 . .
C41 C40 H40 119.6 . .
C40 C41 C42 120.3(4) . .
C40 C41 H41 119.8 . .
C42 C41 H41 119.8 . .
C37 C42 C41 119.5(4) . .
C37 C42 P3 116.9(3) . .
C41 C42 P3 123.5(3) . .
C48 C43 C44 117.9(4) . .
C48 C43 P3 117.4(3) . .
C44 C43 P3 124.7(4) . .
C45 C44 C43 121.0(5) . .
C45 C44 H44 119.5 . .
C43 C44 H44 119.5 . .
C46 C45 C44 119.8(5) . .
C46 C45 H45 120.1 . .
C44 C45 H45 120.1 . .
C47 C46 C45 119.9(5) . .
C47 C46 H46 120.0 . .
C45 C46 H46 120.0 . .
C46 C47 C48 120.6(5) . .
C46 C47 H47 119.7 . .
C48 C47 H47 119.7 . .
C47 C48 C43 120.7(5) . .
C47 C48 H48 119.7 . .
C43 C48 H48 119.7 . .
C50 C49 C54 117.5(4) . .
C50 C49 P3 119.5(3) . .
C54 C49 P3 122.7(3) . .
C51 C50 C49 121.4(4) . .
C51 C50 H50 119.3 . .
C49 C50 H50 119.3 . .
C52 C51 C50 120.2(5) . .
C52 C51 H51 119.9 . .
C50 C51 H51 119.9 . .
C51 C52 C53 119.2(5) . .
C51 C52 H52 120.4 . .
C53 C52 H52 120.4 . .
C54 C53 C52 120.8(4) . .
C54 C53 H53 119.6 . .
C52 C53 H53 119.6 . .
C53 C54 C49 120.9(4) . .
C53 C54 H54 119.6 . .
C49 C54 H54 119.6 . .
O3 P4 O1 98.1(2) . .
O3 P4 O2 104.81(19) . .
O1 P4 O2 102.0(2) . .
O3 P4 Rh1 114.01(14) . .
O1 P4 Rh1 122.92(18) . .
O2 P4 Rh1 112.66(13) . .
C55 O1 P4 126.0(4) . .
O1 C55 H55 109.5 . .
O1 C55 H55A 109.5 . .
H55 C55 H55A 109.5 . .
O1 C55 H55B 109.5 . .
H55 C55 H55B 109.5 . .
H55A C55 H55B 109.5 . .
C56 O2 P4 124.4(4) . .
O2 C56 H56 109.5 . .
O2 C56 H56A 109.5 . .
H56 C56 H56A 109.5 . .
O2 C56 H56B 109.5 . .
H56 C56 H56B 109.5 . .
H56A C56 H56B 109.5 . .
C57 O3 P4 127.2(4) . .
O3 C57 H57 109.5 . .
O3 C57 H57A 109.5 . .
H57 C57 H57A 109.5 . .
O3 C57 H57B 109.5 . .
H57 C57 H57B 109.5 . .
H57A C57 H57B 109.5 . .
P8 Rh2 P5 97.32(4) . .
P8 Rh2 P6 101.10(4) . .
P5 Rh2 P6 121.23(4) . .
P8 Rh2 P7 95.85(4) . .
P5 Rh2 P7 118.03(4) . .
P6 Rh2 P7 114.85(4) . .
P8 Rh2 Ge2 176.44(3) . .
P5 Rh2 Ge2 81.68(3) . .
P6 Rh2 Ge2 82.30(3) . .
P7 Rh2 Ge2 81.68(3) . .
C94 Ge2 C58 107.88(17) . .
C94 Ge2 C76 108.37(17) . .
C58 Ge2 C76 110.82(17) . .
C94 Ge2 Rh2 109.94(13) . .
C58 Ge2 Rh2 110.22(12) . .
C76 Ge2 Rh2 109.57(12) . .
C64 P5 C70 103.0(2) . .
C64 P5 C63 99.2(2) . .
C70 P5 C63 99.11(19) . .
C64 P5 Rh2 117.27(14) . .
C70 P5 Rh2 120.93(14) . .
C63 P5 Rh2 113.85(13) . .
C63 C58 C59 119.1(4) . .
C63 C58 Ge2 114.1(3) . .
C59 C58 Ge2 126.8(3) . .
C60 C59 C58 120.9(4) . .
C60 C59 H59 119.5 . .
C58 C59 H59 119.5 . .
C59 C60 C61 119.5(4) . .
C59 C60 H60 120.2 . .
C61 C60 H60 120.2 . .
C62 C61 C60 120.6(4) . .
C62 C61 H61 119.7 . .
C60 C61 H61 119.7 . .
C61 C62 C63 120.2(5) . .
C61 C62 H62 119.9 . .
C63 C62 H62 119.9 . .
C58 C63 C62 119.7(4) . .
C58 C63 P5 118.1(3) . .
C62 C63 P5 122.2(3) . .
C65 C64 C69 118.0(5) . .
C65 C64 P5 118.9(4) . .
C69 C64 P5 122.9(4) . .
C66 C65 C64 121.1(6) . .
C66 C65 H65 119.5 . .
C64 C65 H65 119.5 . .
C67 C66 C65 120.3(6) . .
C67 C66 H66 119.9 . .
C65 C66 H66 119.9 . .
C66 C67 C68 120.1(6) . .
C66 C67 H67 119.9 . .
C68 C67 H67 119.9 . .
C67 C68 C69 120.4(6) . .
C67 C68 H68 119.8 . .
C69 C68 H68 119.8 . .
C68 C69 C64 120.1(6) . .
C68 C69 H69 119.9 . .
C64 C69 H69 119.9 . .
C75 C70 C71 117.1(4) . .
C75 C70 P5 117.2(3) . .
C71 C70 P5 125.6(4) . .
C72 C71 C70 120.9(5) . .
C72 C71 H71 119.5 . .
C70 C71 H71 119.5 . .
C73 C72 C71 120.8(5) . .
C73 C72 H72 119.6 . .
C71 C72 H72 119.6 . .
C72 C73 C74 119.3(5) . .
C72 C73 H73 120.4 . .
C74 C73 H73 120.4 . .
C73 C74 C75 120.2(5) . .
C73 C74 H74 119.9 . .
C75 C74 H74 119.9 . .
C74 C75 C70 121.7(5) . .
C74 C75 H75 119.2 . .
C70 C75 H75 119.2 . .
C82 P6 C88 99.62(18) . .
C82 P6 C81 99.35(18) . .
C88 P6 C81 103.21(18) . .
C82 P6 Rh2 118.38(13) . .
C88 P6 Rh2 119.56(14) . .
C81 P6 Rh2 113.66(13) . .
C81 C76 C77 119.2(4) . .
C81 C76 Ge2 115.6(3) . .
C77 C76 Ge2 125.1(3) . .
C78 C77 C76 120.5(4) . .
C78 C77 H77 119.7 . .
C76 C77 H77 119.7 . .
C79 C78 C77 119.7(4) . .
C79 C78 H78 120.1 . .
C77 C78 H78 120.1 . .
C78 C79 C80 120.4(4) . .
C78 C79 H79 119.8 . .
C80 C79 H79 119.8 . .
C79 C80 C81 120.1(4) . .
C79 C80 H80 119.9 . .
C81 C80 H80 119.9 . .
C76 C81 C80 120.0(4) . .
C76 C81 P6 117.0(3) . .
C80 C81 P6 123.0(3) . .
C87 C82 C83 118.4(4) . .
C87 C82 P6 120.9(3) . .
C83 C82 P6 120.3(3) . .
C84 C83 C82 120.4(4) . .
C84 C83 H83 119.8 . .
C82 C83 H83 119.8 . .
C85 C84 C83 120.7(4) . .
C85 C84 H84 119.6 . .
C83 C84 H84 119.6 . .
C84 C85 C86 119.2(4) . .
C84 C85 H85 120.4 . .
C86 C85 H85 120.4 . .
C85 C86 C87 120.3(4) . .
C85 C86 H86 119.9 . .
C87 C86 H86 119.9 . .
C86 C87 C82 121.0(4) . .
C86 C87 H87 119.5 . .
C82 C87 H87 119.5 . .
C93 C88 C89 117.7(4) . .
C93 C88 P6 117.8(3) . .
C89 C88 P6 124.6(3) . .
C90 C89 C88 121.3(4) . .
C90 C89 H89 119.4 . .
C88 C89 H89 119.4 . .
C89 C90 C91 120.1(4) . .
C89 C90 H90 120.0 . .
C91 C90 H90 120.0 . .
C90 C91 C92 119.7(4) . .
C90 C91 H91 120.2 . .
C92 C91 H91 120.2 . .
C91 C92 C93 120.2(4) . .
C91 C92 H92 119.9 . .
C93 C92 H92 119.9 . .
C92 C93 C88 121.1(4) . .
C92 C93 H93 119.4 . .
C88 C93 H93 119.4 . .
C106 P7 C100 101.49(19) . .
C106 P7 C99 102.4(2) . .
C100 P7 C99 99.45(19) . .
C106 P7 Rh2 120.48(15) . .
C100 P7 Rh2 116.59(13) . .
C99 P7 Rh2 113.43(14) . .
C95 C94 C99 118.8(4) . .
C95 C94 Ge2 126.4(3) . .
C99 C94 Ge2 114.7(3) . .
C96 C95 C94 121.2(5) . .
C96 C95 H95 119.4 . .
C94 C95 H95 119.4 . .
C97 C96 C95 119.8(5) . .
C97 C96 H96 120.1 . .
C95 C96 H96 120.1 . .
C96 C97 C98 120.8(5) . .
C96 C97 H97 119.6 . .
C98 C97 H97 119.6 . .
C97 C98 C99 119.6(5) . .
C97 C98 H98 120.2 . .
C99 C98 H98 120.2 . .
C94 C99 C98 119.8(4) . .
C94 C99 P7 117.6(3) . .
C98 C99 P7 122.5(4) . .
C105 C100 C101 118.2(4) . .
C105 C100 P7 122.8(3) . .
C101 C100 P7 118.8(3) . .
C102 C101 C100 120.7(5) . .
C102 C101 H101 119.7 . .
C100 C101 H101 119.7 . .
C103 C102 C101 120.5(5) . .
C103 C102 H102 119.8 . .
C101 C102 H102 119.8 . .
C102 C103 C104 119.5(4) . .
C102 C103 H103 120.2 . .
C104 C103 H103 120.2 . .
C103 C104 C105 120.3(4) . .
C103 C104 H104 119.9 . .
C105 C104 H104 119.9 . .
C104 C105 C100 120.8(4) . .
C104 C105 H105 119.6 . .
C100 C105 H105 119.6 . .
C111 C106 C107 118.0(4) . .
C111 C106 P7 117.7(3) . .
C107 C106 P7 124.3(4) . .
C108 C107 C106 120.8(5) . .
C108 C107 H107 119.6 . .
C106 C107 H107 119.6 . .
C107 C108 C109 120.3(5) . .
C107 C108 H108 119.8 . .
C109 C108 H108 119.8 . .
C110 C109 C108 119.1(5) . .
C110 C109 H109 120.4 . .
C108 C109 H109 120.4 . .
C109 C110 C111 120.9(5) . .
C109 C110 H110 119.5 . .
C111 C110 H110 119.5 . .
C110 C111 C106 120.8(5) . .
C110 C111 H111 119.6 . .
C106 C111 H111 119.6 . .
O6 P8 O5 97.30(19) . .
O6 P8 O4 105.04(19) . .
O5 P8 O4 101.51(19) . .
O6 P8 Rh2 113.73(13) . .
O5 P8 Rh2 124.65(15) . .
O4 P8 Rh2 112.08(13) . .
C112 O4 P8 123.8(3) . .
O4 C112 H112 109.5 . .
O4 C112 H113 109.5 . .
H112 C112 H113 109.5 . .
O4 C112 H114 109.5 . .
H112 C112 H114 109.5 . .
H113 C112 H114 109.5 . .
C113 O5 P8 121.7(3) . .
O5 C113 H115 109.5 . .
O5 C113 H116 109.5 . .
H115 C113 H116 109.5 . .
O5 C113 H117 109.5 . .
H115 C113 H117 109.5 . .
H116 C113 H117 109.5 . .
C114 O6 P8 127.0(4) . .
O6 C114 H118 109.5 . .
O6 C114 H119 109.5 . .
H118 C114 H119 109.5 . .
O6 C114 H120 109.5 . .
H118 C114 H120 109.5 . .
H119 C114 H120 109.5 . .
C115 C116 C117 155.710(2) . .
C118 C117 C116 127.278(2) . .
C117 C118 C119 147.928(1) . .
C120 C119 C118 116.398(1) . .
C126 C121 C122 119.983(2) . .
C126 C121 C127 104.369(2) . .
C122 C121 C127 134.221(2) . .
C123 C122 C121 120.010(2) . .
C122 C123 C124 119.998(3) . .
C125 C124 C126 71.120(1) 2 2
C125 C124 C123 125.722(1) 2 .
C126 C124 C123 135.660(2) 2 .
C125 C124 C125 6.136(1) 2 .
C126 C124 C125 76.706(1) 2 .
C123 C124 C125 120.000(2) . .
C125 C125 C124 157.534(4) 2 2
C125 C125 C126 135.065(3) 2 .
C124 C125 C126 64.734(2) 2 .
C125 C125 C124 16.336(2) 2 .
C124 C125 C124 173.428(1) 2 .
C126 C125 C124 119.991(2) . .
C125 C125 C126 35.565(2) 2 2
C124 C125 C126 123.425(1) 2 2
C126 C125 C126 142.546(2) . 2
C124 C125 C126 50.004(2) . 2
C124 C126 C121 163.641(1) 2 .
C124 C126 C125 44.133(2) 2 .
C121 C126 C125 120.018(3) . .
C124 C126 C125 53.284(2) 2 2
C121 C126 C125 110.738(3) . 2
C125 C126 C125 9.4 . 2
C129 C128 C133 120.015(2) . .
C129 C128 C134 121.589(1) . .
C133 C128 C134 117.671(2) . .
C128 C129 C130 119.971(2) . .
C129 C130 C131 120.003(2) . .
C129 C130 C133 99.129(1) . 2
C131 C130 C133 43.723(1) . 2
C129 C130 C132 94.694(2) . 2
C131 C130 C132 25.387(1) . 2
C133 C130 C132 43.190(2) 2 2
C132 C131 C133 79.404(2) 2 2
C132 C131 C132 6.375(1) 2 .
C133 C131 C132 76.307(2) 2 .
C132 C131 C130 115.336(2) 2 .
C133 C131 C130 83.683(3) 2 .
C132 C131 C130 119.998(3) . .
C132 C132 C131 160.656(1) 2 2
C132 C132 C133 110.374(3) 2 .
C131 C132 C133 58.840(2) 2 .
C132 C132 C131 12.966(2) 2 .
C131 C132 C131 172.778(1) 2 .
C133 C132 C131 120.013(3) . .
C132 C132 C133 53.907(2) 2 2
C131 C132 C133 139.524(1) 2 2
C133 C132 C133 99.838(3) . 2
C131 C132 C133 46.808(2) . 2
C132 C132 C130 152.434(1) 2 2
C131 C132 C130 39.282(1) 2 2
C133 C132 C130 58.959(3) . 2
C131 C132 C130 147.462(2) . 2
C133 C132 C130 100.713(2) 2 2
C131 C133 C132 41.758(1) 2 .
C131 C133 C128 160.677(2) 2 .
C132 C133 C128 120.000(2) . .
C131 C133 C132 56.882(1) 2 2
C132 C133 C132 15.7 . 2
C128 C133 C132 104.474(2) . 2
C131 C133 C130 52.596(2) 2 2
C132 C133 C130 77.849(1) . 2
C128 C133 C130 140.648(1) . 2
C132 C133 C130 91.748(1) 2 2
C141 C135 C136 115.967(2) . .
C141 C135 C140 123.945(1) . .
C136 C135 C140 120.011(2) . .
C135 C136 C137 119.976(1) . .
C138 C137 C136 120.003(1) . .
C137 C138 C139 120.003(2) . .
C140 C139 C138 119.981(1) . .
C139 C140 C135 120.026(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Rh1 P4 2.2463(11) .
Rh1 P2 2.3175(11) .
Rh1 P1 2.3189(11) .
Rh1 P3 2.3194(11) .
Rh1 Ge1 2.3767(5) .
Ge1 C37 1.958(4) .
Ge1 C19 1.961(4) .
Ge1 C1 1.964(4) .
P1 C13 1.844(4) .
P1 C7 1.855(4) .
P1 C6 1.859(4) .
C1 C2 1.395(6) .
C1 C6 1.398(6) .
C2 C3 1.375(6) .
C2 H2 0.9500 .
C3 C4 1.384(7) .
C3 H3 0.9500 .
C4 C5 1.387(6) .
C4 H4 0.9500 .
C5 C6 1.399(6) .
C5 H5 0.9500 .
C7 C12 1.381(6) .
C7 C8 1.404(6) .
C8 C9 1.380(6) .
C8 H8 0.9500 .
C9 C10 1.382(7) .
C9 H9 0.9500 .
C10 C11 1.381(7) .
C10 H10 0.9500 .
C11 C12 1.393(6) .
C11 H11 0.9500 .
C12 H12 0.9500 .
C13 C18 1.393(6) .
C13 C14 1.395(6) .
C14 C15 1.379(6) .
C14 H14 0.9500 .
C15 C16 1.388(8) .
C15 H15 0.9500 .
C16 C17 1.370(7) .
C16 H16 0.9500 .
C17 C18 1.379(6) .
C17 H17 0.9500 .
C18 H18 0.9500 .
P2 C25 1.839(4) .
P2 C24 1.844(4) .
P2 C31 1.845(5) .
C19 C20 1.395(6) .
C19 C24 1.402(6) .
C20 C21 1.388(6) .
C20 H20 0.9500 .
C21 C22 1.364(7) .
C21 H21 0.9500 .
C22 C23 1.380(7) .
C22 H22 0.9500 .
C23 C24 1.410(6) .
C23 H23 0.9500 .
C25 C26 1.389(7) .
C25 C30 1.390(6) .
C26 C27 1.375(7) .
C26 H26 0.9500 .
C27 C28 1.389(9) .
C27 H27 0.9500 .
C28 C29 1.353(9) .
C28 H28 0.9500 .
C29 C30 1.390(8) .
C29 H29 0.9500 .
C30 H30 0.9500 .
C31 C32 1.390(7) .
C31 C36 1.398(7) .
C32 C33 1.384(7) .
C32 H32 0.9500 .
C33 C34 1.369(9) .
C33 H33 0.9500 .
C34 C35 1.380(9) .
C34 H34 0.9500 .
C35 C36 1.396(8) .
C35 H35 0.9500 .
C36 H36 0.9500 .
P3 C49 1.829(4) .
P3 C43 1.845(4) .
P3 C42 1.853(4) .
C37 C38 1.394(6) .
C37 C42 1.397(6) .
C38 C39 1.393(6) .
C38 H38 0.9500 .
C39 C40 1.374(7) .
C39 H39 0.9500 .
C40 C41 1.382(7) .
C40 H40 0.9500 .
C41 C42 1.397(6) .
C41 H41 0.9500 .
C43 C48 1.388(7) .
C43 C44 1.394(6) .
C44 C45 1.389(7) .
C44 H44 0.9500 .
C45 C46 1.372(9) .
C45 H45 0.9500 .
C46 C47 1.371(8) .
C46 H46 0.9500 .
C47 C48 1.382(7) .
C47 H47 0.9500 .
C48 H48 0.9500 .
C49 C50 1.393(6) .
C49 C54 1.409(6) .
C50 C51 1.391(7) .
C50 H50 0.9500 .
C51 C52 1.382(7) .
C51 H51 0.9500 .
C52 C53 1.389(7) .
C52 H52 0.9500 .
C53 C54 1.379(6) .
C53 H53 0.9500 .
C54 H54 0.9500 .
P4 O3 1.601(3) .
P4 O1 1.607(4) .
P4 O2 1.610(3) .
O1 C55 1.383(7) .
C55 H55 0.9800 .
C55 H55A 0.9800 .
C55 H55B 0.9800 .
O2 C56 1.429(6) .
C56 H56 0.9800 .
C56 H56A 0.9800 .
C56 H56B 0.9800 .
O3 C57 1.436(6) .
C57 H57 0.9800 .
C57 H57A 0.9800 .
C57 H57B 0.9800 .
Rh2 P8 2.2456(11) .
Rh2 P5 2.3163(10) .
Rh2 P6 2.3208(10) .
Rh2 P7 2.3272(10) .
Rh2 Ge2 2.3755(5) .
Ge2 C94 1.957(4) .
Ge2 C58 1.958(4) .
Ge2 C76 1.964(4) .
P5 C64 1.844(5) .
P5 C70 1.845(4) .
P5 C63 1.846(4) .
C58 C63 1.396(6) .
C58 C59 1.401(6) .
C59 C60 1.380(6) .
C59 H59 0.9500 .
C60 C61 1.391(7) .
C60 H60 0.9500 .
C61 C62 1.376(7) .
C61 H61 0.9500 .
C62 C63 1.401(6) .
C62 H62 0.9500 .
C64 C65 1.389(7) .
C64 C69 1.398(7) .
C65 C66 1.383(7) .
C65 H65 0.9500 .
C66 C67 1.366(10) .
C66 H66 0.9500 .
C67 C68 1.370(10) .
C67 H67 0.9500 .
C68 C69 1.394(8) .
C68 H68 0.9500 .
C69 H69 0.9500 .
C70 C75 1.384(7) .
C70 C71 1.395(6) .
C71 C72 1.382(7) .
C71 H71 0.9500 .
C72 C73 1.364(8) .
C72 H72 0.9500 .
C73 C74 1.374(8) .
C73 H73 0.9500 .
C74 C75 1.381(7) .
C74 H74 0.9500 .
C75 H75 0.9500 .
P6 C82 1.842(4) .
P6 C88 1.850(4) .
P6 C81 1.865(4) .
C76 C81 1.392(6) .
C76 C77 1.402(6) .
C77 C78 1.390(7) .
C77 H77 0.9500 .
C78 C79 1.383(7) .
C78 H78 0.9500 .
C79 C80 1.387(6) .
C79 H79 0.9500 .
C80 C81 1.396(6) .
C80 H80 0.9500 .
C82 C87 1.391(6) .
C82 C83 1.395(6) .
C83 C84 1.387(6) .
C83 H83 0.9500 .
C84 C85 1.385(7) .
C84 H84 0.9500 .
C85 C86 1.386(7) .
C85 H85 0.9500 .
C86 C87 1.388(6) .
C86 H86 0.9500 .
C87 H87 0.9500 .
C88 C93 1.394(6) .
C88 C89 1.402(6) .
C89 C90 1.382(6) .
C89 H89 0.9500 .
C90 C91 1.384(7) .
C90 H90 0.9500 .
C91 C92 1.385(7) .
C91 H91 0.9500 .
C92 C93 1.386(6) .
C92 H92 0.9500 .
C93 H93 0.9500 .
P7 C106 1.849(5) .
P7 C100 1.849(4) .
P7 C99 1.853(4) .
C94 C95 1.389(6) .
C94 C99 1.393(6) .
C95 C96 1.377(7) .
C95 H95 0.9500 .
C96 C97 1.364(8) .
C96 H96 0.9500 .
C97 C98 1.383(7) .
C97 H97 0.9500 .
C98 C99 1.398(6) .
C98 H98 0.9500 .
C100 C105 1.389(6) .
C100 C101 1.390(6) .
C101 C102 1.386(7) .
C101 H101 0.9500 .
C102 C103 1.371(7) .
C102 H102 0.9500 .
C103 C104 1.380(7) .
C103 H103 0.9500 .
C104 C105 1.384(6) .
C104 H104 0.9500 .
C105 H105 0.9500 .
C106 C111 1.386(6) .
C106 C107 1.399(6) .
C107 C108 1.382(7) .
C107 H107 0.9500 .
C108 C109 1.384(8) .
C108 H108 0.9500 .
C109 C110 1.376(8) .
C109 H109 0.9500 .
C110 C111 1.381(7) .
C110 H110 0.9500 .
C111 H111 0.9500 .
P8 O6 1.600(3) .
P8 O5 1.607(3) .
P8 O4 1.608(3) .
O4 C112 1.439(6) .
C112 H112 0.9800 .
C112 H113 0.9800 .
C112 H114 0.9800 .
O5 C113 1.414(6) .
C113 H115 0.9800 .
C113 H116 0.9800 .
C113 H117 0.9800 .
O6 C114 1.445(6) .
C114 H118 0.9800 .
C114 H119 0.9800 .
C114 H120 0.9800 .
C115 C116 1.8344 .
C116 C117 1.9432 .
C117 C118 1.6477 .
C118 C119 1.7070 .
C119 C120 1.5352 .
C121 C126 1.3898 .
C121 C122 1.3902 .
C121 C127 1.4593 .
C122 C123 1.3899 .
C123 C124 1.3900 .
C124 C125 1.0229 2
C124 C126 1.3284 2
C124 C125 1.3901 .
C125 C125 0.3887 2
C125 C124 1.0229 2
C125 C126 1.3900 .
C125 C126 1.6876 2
C126 C124 1.3284 2
C126 C125 1.6877 2
C128 C129 1.3901 .
C128 C133 1.3902 .
C128 C134 1.5923 .
C129 C130 1.3903 .
C130 C131 1.3904 .
C130 C133 1.7397 2
C130 C132 1.9850 2
C131 C132 0.9416 2
C131 C133 1.2097 2
C131 C132 1.3898 .
C132 C132 0.4659 2
C132 C131 0.9416 2
C132 C133 1.3897 .
C132 C133 1.6122 2
C132 C130 1.9849 2
C133 C131 1.2098 2
C133 C132 1.6122 2
C133 C130 1.7397 2
C135 C141 1.1031 .
C135 C136 1.3897 .
C135 C140 1.3900 .
C136 C137 1.3903 .
C137 C138 1.3901 .
C138 C139 1.3901 .
C139 C140 1.3896 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
P4 Rh1 Ge1 C37 -32.4(8) . .
P2 Rh1 Ge1 C37 -107.22(13) . .
P1 Rh1 Ge1 C37 130.92(13) . .
P3 Rh1 Ge1 C37 12.24(13) . .
P4 Rh1 Ge1 C19 88.5(8) . .
P2 Rh1 Ge1 C19 13.68(13) . .
P1 Rh1 Ge1 C19 -108.17(13) . .
P3 Rh1 Ge1 C19 133.15(13) . .
P4 Rh1 Ge1 C1 -152.7(8) . .
P2 Rh1 Ge1 C1 132.41(12) . .
P1 Rh1 Ge1 C1 10.55(12) . .
P3 Rh1 Ge1 C1 -108.13(12) . .
P4 Rh1 P1 C13 -76.05(16) . .
P2 Rh1 P1 C13 28.68(16) . .
P3 Rh1 P1 C13 -179.02(16) . .
Ge1 Rh1 P1 C13 104.69(16) . .
P4 Rh1 P1 C7 45.55(15) . .
P2 Rh1 P1 C7 150.28(15) . .
P3 Rh1 P1 C7 -57.42(16) . .
Ge1 Rh1 P1 C7 -133.71(15) . .
P4 Rh1 P1 C6 168.41(14) . .
P2 Rh1 P1 C6 -86.86(14) . .
P3 Rh1 P1 C6 65.44(14) . .
Ge1 Rh1 P1 C6 -10.85(14) . .
C37 Ge1 C1 C2 53.1(4) . .
C19 Ge1 C1 C2 -66.4(4) . .
Rh1 Ge1 C1 C2 174.0(3) . .
C37 Ge1 C1 C6 -130.1(3) . .
C19 Ge1 C1 C6 110.5(3) . .
Rh1 Ge1 C1 C6 -9.1(3) . .
C6 C1 C2 C3 0.2(6) . .
Ge1 C1 C2 C3 176.9(3) . .
C1 C2 C3 C4 -0.6(7) . .
C2 C3 C4 C5 0.2(7) . .
C3 C4 C5 C6 0.5(7) . .
C2 C1 C6 C5 0.6(6) . .
Ge1 C1 C6 C5 -176.5(3) . .
C2 C1 C6 P1 177.6(3) . .
Ge1 C1 C6 P1 0.5(4) . .
C4 C5 C6 C1 -0.9(6) . .
C4 C5 C6 P1 -177.7(3) . .
C13 P1 C6 C1 -117.3(3) . .
C7 P1 C6 C1 139.8(3) . .
Rh1 P1 C6 C1 8.8(4) . .
C13 P1 C6 C5 59.5(4) . .
C7 P1 C6 C5 -43.3(4) . .
Rh1 P1 C6 C5 -174.3(3) . .
C13 P1 C7 C12 142.0(3) . .
C6 P1 C7 C12 -115.9(3) . .
Rh1 P1 C7 C12 11.9(4) . .
C13 P1 C7 C8 -36.6(4) . .
C6 P1 C7 C8 65.5(4) . .
Rh1 P1 C7 C8 -166.8(3) . .
C12 C7 C8 C9 0.3(6) . .
P1 C7 C8 C9 178.9(3) . .
C7 C8 C9 C10 -0.3(7) . .
C8 C9 C10 C11 0.4(7) . .
C9 C10 C11 C12 -0.5(7) . .
C8 C7 C12 C11 -0.3(7) . .
P1 C7 C12 C11 -179.0(4) . .
C10 C11 C12 C7 0.4(7) . .
C7 P1 C13 C18 -37.9(4) . .
C6 P1 C13 C18 -143.6(4) . .
Rh1 P1 C13 C18 93.1(4) . .
C7 P1 C13 C14 147.5(3) . .
C6 P1 C13 C14 41.7(4) . .
Rh1 P1 C13 C14 -81.6(4) . .
C18 C13 C14 C15 -0.1(7) . .
P1 C13 C14 C15 174.7(4) . .
C13 C14 C15 C16 0.8(7) . .
C14 C15 C16 C17 -0.8(8) . .
C15 C16 C17 C18 -0.1(8) . .
C16 C17 C18 C13 0.8(7) . .
C14 C13 C18 C17 -0.7(7) . .
P1 C13 C18 C17 -175.4(4) . .
P4 Rh1 P2 C25 48.17(18) . .
P1 Rh1 P2 C25 -58.16(18) . .
P3 Rh1 P2 C25 149.73(18) . .
Ge1 Rh1 P2 C25 -134.29(18) . .
P4 Rh1 P2 C24 166.31(15) . .
P1 Rh1 P2 C24 59.98(15) . .
P3 Rh1 P2 C24 -92.13(15) . .
Ge1 Rh1 P2 C24 -16.16(15) . .
P4 Rh1 P2 C31 -78.62(17) . .
P1 Rh1 P2 C31 175.05(17) . .
P3 Rh1 P2 C31 22.94(18) . .
Ge1 Rh1 P2 C31 98.92(17) . .
C37 Ge1 C19 C20 -69.5(4) . .
C1 Ge1 C19 C20 49.5(4) . .
Rh1 Ge1 C19 C20 169.4(3) . .
C37 Ge1 C19 C24 112.1(3) . .
C1 Ge1 C19 C24 -128.8(3) . .
Rh1 Ge1 C19 C24 -9.0(3) . .
C24 C19 C20 C21 1.7(6) . .
Ge1 C19 C20 C21 -176.6(3) . .
C19 C20 C21 C22 -1.0(7) . .
C20 C21 C22 C23 -0.2(7) . .
C21 C22 C23 C24 0.8(7) . .
C20 C19 C24 C23 -1.1(6) . .
Ge1 C19 C24 C23 177.4(3) . .
C20 C19 C24 P2 177.4(3) . .
Ge1 C19 C24 P2 -4.1(4) . .
C22 C23 C24 C19 -0.1(7) . .
C22 C23 C24 P2 -178.5(4) . .
C25 P2 C24 C19 146.4(3) . .
C31 P2 C24 C19 -108.9(3) . .
Rh1 P2 C24 C19 16.2(4) . .
C25 P2 C24 C23 -35.2(4) . .
C31 P2 C24 C23 69.5(4) . .
Rh1 P2 C24 C23 -165.4(3) . .
C24 P2 C25 C26 -90.3(4) . .
C31 P2 C25 C26 167.3(4) . .
Rh1 P2 C25 C26 34.3(5) . .
C24 P2 C25 C30 84.2(5) . .
C31 P2 C25 C30 -18.2(5) . .
Rh1 P2 C25 C30 -151.2(4) . .
C30 C25 C26 C27 -1.1(8) . .
P2 C25 C26 C27 173.9(5) . .
C25 C26 C27 C28 1.6(10) . .
C26 C27 C28 C29 -0.8(11) . .
C27 C28 C29 C30 -0.5(10) . .
C28 C29 C30 C25 1.1(10) . .
C26 C25 C30 C29 -0.3(8) . .
P2 C25 C30 C29 -174.7(5) . .
C25 P2 C31 C32 139.8(4) . .
C24 P2 C31 C32 37.6(4) . .
Rh1 P2 C31 C32 -84.7(4) . .
C25 P2 C31 C36 -45.9(4) . .
C24 P2 C31 C36 -148.1(4) . .
Rh1 P2 C31 C36 89.7(4) . .
C36 C31 C32 C33 1.2(8) . .
P2 C31 C32 C33 175.8(5) . .
C31 C32 C33 C34 -0.2(10) . .
C32 C33 C34 C35 -0.8(11) . .
C33 C34 C35 C36 0.8(10) . .
C34 C35 C36 C31 0.2(9) . .
C32 C31 C36 C35 -1.2(8) . .
P2 C31 C36 C35 -175.6(4) . .
P4 Rh1 P3 C49 -82.23(15) . .
P2 Rh1 P3 C49 175.84(15) . .
P1 Rh1 P3 C49 22.84(16) . .
Ge1 Rh1 P3 C49 99.56(15) . .
P4 Rh1 P3 C43 41.13(17) . .
P2 Rh1 P3 C43 -60.81(18) . .
P1 Rh1 P3 C43 146.19(17) . .
Ge1 Rh1 P3 C43 -137.08(17) . .
P4 Rh1 P3 C42 163.53(15) . .
P2 Rh1 P3 C42 61.60(16) . .
P1 Rh1 P3 C42 -91.40(15) . .
Ge1 Rh1 P3 C42 -14.68(15) . .
C19 Ge1 C37 C38 51.3(4) . .
C1 Ge1 C37 C38 -67.1(4) . .
Rh1 Ge1 C37 C38 172.0(3) . .
C19 Ge1 C37 C42 -128.6(3) . .
C1 Ge1 C37 C42 113.0(3) . .
Rh1 Ge1 C37 C42 -7.9(3) . .
C42 C37 C38 C39 -0.1(6) . .
Ge1 C37 C38 C39 -180.0(3) . .
C37 C38 C39 C40 0.3(7) . .
C38 C39 C40 C41 -0.3(8) . .
C39 C40 C41 C42 0.1(8) . .
C38 C37 C42 C41 -0.2(6) . .
Ge1 C37 C42 C41 179.7(3) . .
C38 C37 C42 P3 176.1(3) . .
Ge1 C37 C42 P3 -4.0(4) . .
C40 C41 C42 C37 0.2(7) . .
C40 C41 C42 P3 -175.9(4) . .
C49 P3 C42 C37 -108.7(3) . .
C43 P3 C42 C37 147.1(3) . .
Rh1 P3 C42 C37 14.9(4) . .
C49 P3 C42 C41 67.4(4) . .
C43 P3 C42 C41 -36.7(4) . .
Rh1 P3 C42 C41 -169.0(4) . .
C49 P3 C43 C48 151.6(4) . .
C42 P3 C43 C48 -106.0(4) . .
Rh1 P3 C43 C48 21.9(4) . .
C49 P3 C43 C44 -28.3(5) . .
C42 P3 C43 C44 74.0(4) . .
Rh1 P3 C43 C44 -158.1(4) . .
C48 C43 C44 C45 -1.0(8) . .
P3 C43 C44 C45 178.9(4) . .
C43 C44 C45 C46 0.3(9) . .
C44 C45 C46 C47 0.3(10) . .
C45 C46 C47 C48 -0.1(10) . .
C46 C47 C48 C43 -0.6(10) . .
C44 C43 C48 C47 1.2(8) . .
P3 C43 C48 C47 -178.8(5) . .
C43 P3 C49 C50 146.9(4) . .
C42 P3 C49 C50 42.4(4) . .
Rh1 P3 C49 C50 -80.0(4) . .
C43 P3 C49 C54 -39.6(4) . .
C42 P3 C49 C54 -144.2(4) . .
Rh1 P3 C49 C54 93.4(4) . .
C54 C49 C50 C51 1.5(7) . .
P3 C49 C50 C51 175.2(4) . .
C49 C50 C51 C52 -0.1(8) . .
C50 C51 C52 C53 -0.9(8) . .
C51 C52 C53 C54 0.5(8) . .
C52 C53 C54 C49 1.0(7) . .
C50 C49 C54 C53 -1.9(7) . .
P3 C49 C54 C53 -175.5(4) . .
P2 Rh1 P4 O3 140.04(16) . .
P1 Rh1 P4 O3 -97.66(16) . .
P3 Rh1 P4 O3 21.14(16) . .
Ge1 Rh1 P4 O3 65.5(8) . .
P2 Rh1 P4 O1 -101.78(19) . .
P1 Rh1 P4 O1 20.52(19) . .
P3 Rh1 P4 O1 139.32(18) . .
Ge1 Rh1 P4 O1 -176(25) . .
P2 Rh1 P4 O2 20.74(16) . .
P1 Rh1 P4 O2 143.04(16) . .
P3 Rh1 P4 O2 -98.15(16) . .
Ge1 Rh1 P4 O2 -53.8(8) . .
O3 P4 O1 C55 -141.3(5) . .
O2 P4 O1 C55 -34.2(6) . .
Rh1 P4 O1 C55 93.1(5) . .
O3 P4 O2 C56 33.1(5) . .
O1 P4 O2 C56 -68.8(5) . .
Rh1 P4 O2 C56 157.6(4) . .
O1 P4 O3 C57 19.0(5) . .
O2 P4 O3 C57 -85.7(5) . .
Rh1 P4 O3 C57 150.6(4) . .
P8 Rh2 Ge2 C94 32.7(6) . .
P5 Rh2 Ge2 C94 106.57(14) . .
P6 Rh2 Ge2 C94 -130.16(14) . .
P7 Rh2 Ge2 C94 -13.52(14) . .
P8 Rh2 Ge2 C58 -86.1(6) . .
P5 Rh2 Ge2 C58 -12.23(13) . .
P6 Rh2 Ge2 C58 111.04(13) . .
P7 Rh2 Ge2 C58 -132.32(13) . .
P8 Rh2 Ge2 C76 151.7(5) . .
P5 Rh2 Ge2 C76 -134.43(12) . .
P6 Rh2 Ge2 C76 -11.16(12) . .
P7 Rh2 Ge2 C76 105.48(12) . .
P8 Rh2 P5 C64 73.91(18) . .
P6 Rh2 P5 C64 -178.33(18) . .
P7 Rh2 P5 C64 -26.73(19) . .
Ge2 Rh2 P5 C64 -102.64(18) . .
P8 Rh2 P5 C70 -53.16(17) . .
P6 Rh2 P5 C70 54.60(17) . .
P7 Rh2 P5 C70 -153.80(17) . .
Ge2 Rh2 P5 C70 130.29(17) . .
P8 Rh2 P5 C63 -170.97(15) . .
P6 Rh2 P5 C63 -63.22(15) . .
P7 Rh2 P5 C63 88.38(15) . .
Ge2 Rh2 P5 C63 12.48(15) . .
C94 Ge2 C58 C63 -109.4(3) . .
C76 Ge2 C58 C63 132.1(3) . .
Rh2 Ge2 C58 C63 10.6(3) . .
C94 Ge2 C58 C59 67.4(4) . .
C76 Ge2 C58 C59 -51.1(4) . .
Rh2 Ge2 C58 C59 -172.6(3) . .
C63 C58 C59 C60 0.0(6) . .
Ge2 C58 C59 C60 -176.7(4) . .
C58 C59 C60 C61 0.4(7) . .
C59 C60 C61 C62 0.0(8) . .
C60 C61 C62 C63 -0.8(8) . .
C59 C58 C63 C62 -0.8(6) . .
Ge2 C58 C63 C62 176.3(3) . .
C59 C58 C63 P5 -177.7(3) . .
Ge2 C58 C63 P5 -0.7(4) . .
C61 C62 C63 C58 1.2(7) . .
C61 C62 C63 P5 178.0(4) . .
C64 P5 C63 C58 115.3(3) . .
C70 P5 C63 C58 -139.9(3) . .
Rh2 P5 C63 C58 -10.1(4) . .
C64 P5 C63 C62 -61.6(4) . .
C70 P5 C63 C62 43.3(4) . .
Rh2 P5 C63 C62 173.0(3) . .
C70 P5 C64 C65 -140.3(4) . .
C63 P5 C64 C65 -38.7(4) . .
Rh2 P5 C64 C65 84.3(4) . .
C70 P5 C64 C69 46.0(4) . .
C63 P5 C64 C69 147.6(4) . .
Rh2 P5 C64 C69 -89.4(4) . .
C69 C64 C65 C66 -0.8(8) . .
P5 C64 C65 C66 -174.8(4) . .
C64 C65 C66 C67 -0.3(9) . .
C65 C66 C67 C68 0.6(10) . .
C66 C67 C68 C69 0.2(10) . .
C67 C68 C69 C64 -1.3(9) . .
C65 C64 C69 C68 1.5(7) . .
P5 C64 C69 C68 175.3(4) . .
C64 P5 C70 C75 -170.3(4) . .
C63 P5 C70 C75 88.0(4) . .
Rh2 P5 C70 C75 -37.0(4) . .
C64 P5 C70 C71 14.9(5) . .
C63 P5 C70 C71 -86.9(4) . .
Rh2 P5 C70 C71 148.2(4) . .
C75 C70 C71 C72 1.3(8) . .
P5 C70 C71 C72 176.1(4) . .
C70 C71 C72 C73 -1.4(9) . .
C71 C72 C73 C74 0.8(9) . .
C72 C73 C74 C75 -0.2(10) . .
C73 C74 C75 C70 0.2(10) . .
C71 C70 C75 C74 -0.7(8) . .
P5 C70 C75 C74 -176.0(5) . .
P8 Rh2 P6 C82 77.14(15) . .
P5 Rh2 P6 C82 -28.57(16) . .
P7 Rh2 P6 C82 178.99(15) . .
Ge2 Rh2 P6 C82 -103.93(15) . .
P8 Rh2 P6 C88 -44.51(15) . .
P5 Rh2 P6 C88 -150.22(15) . .
P7 Rh2 P6 C88 57.34(15) . .
Ge2 Rh2 P6 C88 134.42(15) . .
P8 Rh2 P6 C81 -166.87(14) . .
P5 Rh2 P6 C81 87.42(14) . .
P7 Rh2 P6 C81 -65.02(14) . .
Ge2 Rh2 P6 C81 12.06(14) . .
C94 Ge2 C76 C81 128.9(3) . .
C58 Ge2 C76 C81 -112.9(3) . .
Rh2 Ge2 C76 C81 9.0(3) . .
C94 Ge2 C76 C77 -51.8(4) . .
C58 Ge2 C76 C77 66.4(4) . .
Rh2 Ge2 C76 C77 -171.8(3) . .
C81 C76 C77 C78 0.4(6) . .
Ge2 C76 C77 C78 -178.8(3) . .
C76 C77 C78 C79 0.3(7) . .
C77 C78 C79 C80 -0.2(7) . .
C78 C79 C80 C81 -0.5(7) . .
C77 C76 C81 C80 -1.1(6) . .
Ge2 C76 C81 C80 178.2(3) . .
C77 C76 C81 P6 -178.6(3) . .
Ge2 C76 C81 P6 0.7(4) . .
C79 C80 C81 C76 1.2(6) . .
C79 C80 C81 P6 178.5(3) . .
C82 P6 C81 C76 116.2(3) . .
C88 P6 C81 C76 -141.5(3) . .
Rh2 P6 C81 C76 -10.5(3) . .
C82 P6 C81 C80 -61.2(4) . .
C88 P6 C81 C80 41.0(4) . .
Rh2 P6 C81 C80 172.0(3) . .
C88 P6 C82 C87 40.6(4) . .
C81 P6 C82 C87 145.9(3) . .
Rh2 P6 C82 C87 -90.7(3) . .
C88 P6 C82 C83 -146.7(3) . .
C81 P6 C82 C83 -41.4(4) . .
Rh2 P6 C82 C83 82.0(3) . .
C87 C82 C83 C84 -1.0(6) . .
P6 C82 C83 C84 -173.9(3) . .
C82 C83 C84 C85 -0.4(7) . .
C83 C84 C85 C86 1.4(7) . .
C84 C85 C86 C87 -1.1(7) . .
C85 C86 C87 C82 -0.3(7) . .
C83 C82 C87 C86 1.3(6) . .
P6 C82 C87 C86 174.1(3) . .
C82 P6 C88 C93 -142.3(3) . .
C81 P6 C88 C93 115.6(3) . .
Rh2 P6 C88 C93 -11.8(4) . .
C82 P6 C88 C89 35.9(4) . .
C81 P6 C88 C89 -66.1(4) . .
Rh2 P6 C88 C89 166.5(3) . .
C93 C88 C89 C90 -0.8(6) . .
P6 C88 C89 C90 -179.0(3) . .
C88 C89 C90 C91 0.9(7) . .
C89 C90 C91 C92 -0.9(7) . .
C90 C91 C92 C93 0.7(7) . .
C91 C92 C93 C88 -0.6(7) . .
C89 C88 C93 C92 0.6(6) . .
P6 C88 C93 C92 179.0(3) . .
P8 Rh2 P7 C106 -41.78(17) . .
P5 Rh2 P7 C106 59.74(17) . .
P6 Rh2 P7 C106 -146.89(16) . .
Ge2 Rh2 P7 C106 135.64(16) . .
P8 Rh2 P7 C100 81.80(16) . .
P5 Rh2 P7 C100 -176.68(16) . .
P6 Rh2 P7 C100 -23.31(16) . .
Ge2 Rh2 P7 C100 -100.78(16) . .
P8 Rh2 P7 C99 -163.55(16) . .
P5 Rh2 P7 C99 -62.04(16) . .
P6 Rh2 P7 C99 91.34(16) . .
Ge2 Rh2 P7 C99 13.87(16) . .
C58 Ge2 C94 C95 -50.9(5) . .
C76 Ge2 C94 C95 69.1(5) . .
Rh2 Ge2 C94 C95 -171.1(4) . .
C58 Ge2 C94 C99 131.9(3) . .
C76 Ge2 C94 C99 -108.0(3) . .
Rh2 Ge2 C94 C99 11.7(4) . .
C99 C94 C95 C96 1.1(8) . .
Ge2 C94 C95 C96 -176.0(4) . .
C94 C95 C96 C97 -0.5(9) . .
C95 C96 C97 C98 0.2(10) . .
C96 C97 C98 C99 -0.6(10) . .
C95 C94 C99 C98 -1.4(7) . .
Ge2 C94 C99 C98 176.0(4) . .
C95 C94 C99 P7 -178.0(4) . .
Ge2 C94 C99 P7 -0.6(5) . .
C97 C98 C99 C94 1.2(8) . .
C97 C98 C99 P7 177.6(5) . .
C106 P7 C99 C94 -142.7(4) . .
C100 P7 C99 C94 113.2(4) . .
Rh2 P7 C99 C94 -11.3(4) . .
C106 P7 C99 C98 40.8(5) . .
C100 P7 C99 C98 -63.3(5) . .
Rh2 P7 C99 C98 172.2(4) . .
C106 P7 C100 C105 39.4(4) . .
C99 P7 C100 C105 144.2(4) . .
Rh2 P7 C100 C105 -93.5(4) . .
C106 P7 C100 C101 -146.6(4) . .
C99 P7 C100 C101 -41.8(4) . .
Rh2 P7 C100 C101 80.5(4) . .
C105 C100 C101 C102 -1.1(7) . .
P7 C100 C101 C102 -175.4(4) . .
C100 C101 C102 C103 -0.8(8) . .
C101 C102 C103 C104 1.8(8) . .
C102 C103 C104 C105 -0.8(8) . .
C103 C104 C105 C100 -1.1(7) . .
C101 C100 C105 C104 2.1(7) . .
P7 C100 C105 C104 176.1(3) . .
C100 P7 C106 C111 -153.4(4) . .
C99 P7 C106 C111 104.1(4) . .
Rh2 P7 C106 C111 -22.9(4) . .
C100 P7 C106 C107 26.8(4) . .
C99 P7 C106 C107 -75.7(4) . .
Rh2 P7 C106 C107 157.3(4) . .
C111 C106 C107 C108 1.8(8) . .
P7 C106 C107 C108 -178.4(4) . .
C106 C107 C108 C109 -1.4(9) . .
C107 C108 C109 C110 -0.1(10) . .
C108 C109 C110 C111 1.2(10) . .
C109 C110 C111 C106 -0.8(10) . .
C107 C106 C111 C110 -0.7(8) . .
P7 C106 C111 C110 179.4(5) . .
P5 Rh2 P8 O6 -140.68(16) . .
P6 Rh2 P8 O6 95.40(16) . .
P7 Rh2 P8 O6 -21.38(16) . .
Ge2 Rh2 P8 O6 -67.3(6) . .
P5 Rh2 P8 O5 101.11(17) . .
P6 Rh2 P8 O5 -22.80(17) . .
P7 Rh2 P8 O5 -139.59(16) . .
Ge2 Rh2 P8 O5 174.5(5) . .
P5 Rh2 P8 O4 -21.72(15) . .
P6 Rh2 P8 O4 -145.63(15) . .
P7 Rh2 P8 O4 97.59(15) . .
Ge2 Rh2 P8 O4 51.7(6) . .
O6 P8 O4 C112 -36.5(5) . .
O5 P8 O4 C112 64.4(5) . .
Rh2 P8 O4 C112 -160.5(4) . .
O6 P8 O5 C113 154.0(4) . .
O4 P8 O5 C113 46.9(4) . .
Rh2 P8 O5 C113 -80.5(4) . .
O5 P8 O6 C114 -19.0(5) . .
O4 P8 O6 C114 85.0(5) . .
Rh2 P8 O6 C114 -152.1(4) . .
C115 C116 C117 C118 40.336(2) . .
C116 C117 C118 C119 -167.3 . .
C117 C118 C119 C120 176.680(1) . .
C126 C121 C122 C123 0.0 . .
C127 C121 C122 C123 -164.0 . .
C121 C122 C123 C124 0.0 . .
C122 C123 C124 C125 2.6 . 2
C122 C123 C124 C126 102.168(2) . 2
C122 C123 C124 C125 0.0 . .
C126 C124 C125 C125 24.118(2) 2 2
C123 C124 C125 C125 159.529(1) . 2
C125 C124 C125 C124 -24.802(5) 2 2
C126 C124 C125 C124 -0.684(4) 2 2
C123 C124 C125 C124 134.727(5) . 2
C125 C124 C125 C126 -159.5 2 .
C126 C124 C125 C126 -135.415(2) 2 .
C123 C124 C125 C126 0.0 . .
C125 C124 C125 C126 -24.118(2) 2 2
C123 C124 C125 C126 135.411(2) . 2
C122 C121 C126 C124 -12.972(2) . 2
C127 C121 C126 C124 155.263(3) . 2
C122 C121 C126 C125 0.0 . .
C127 C121 C126 C125 168.186(2) . .
C122 C121 C126 C125 -1.432(1) . 2
C127 C121 C126 C125 166.803(1) . 2
C125 C125 C126 C124 166.838(2) 2 2
C124 C125 C126 C124 174.8 . 2
C126 C125 C126 C124 112.676(1) 2 2
C125 C125 C126 C121 -7.972(1) 2 .
C124 C125 C126 C121 -174.8 2 .
C124 C125 C126 C121 0.0 . .
C126 C125 C126 C121 -62.134(1) 2 .
C124 C125 C126 C125 -166.838(2) 2 2
C124 C125 C126 C125 8.004(1) . 2
C126 C125 C126 C125 -54.2 2 2
C133 C128 C129 C130 0.0 . .
C134 C128 C129 C130 -170.0 . .
C128 C129 C130 C131 0.0 . .
C128 C129 C130 C133 41.182(1) . 2
C128 C129 C130 C132 -2.1 . 2
C129 C130 C131 C132 -4.897(1) . 2
C133 C130 C131 C132 -75.101(2) 2 2
C129 C130 C131 C133 70.204(2) . 2
C132 C130 C131 C133 75.101(2) 2 2
C129 C130 C131 C132 0.0 . .
C133 C130 C131 C132 -70.190(2) 2 .
C132 C130 C131 C132 4.9 2 .
C133 C131 C132 C132 -118.434(2) 2 2
C130 C131 C132 C132 -44.183(4) . 2
C132 C131 C132 C131 -34.571(4) 2 2
C133 C131 C132 C131 -153.005(5) 2 2
C130 C131 C132 C131 -78.754(7) . 2
C132 C131 C132 C133 44.196(4) 2 .
C133 C131 C132 C133 -74.238(3) 2 .
C130 C131 C132 C133 0.013(1) . .
C132 C131 C132 C133 118.434(2) 2 2
C130 C131 C132 C133 74.251(3) . 2
C132 C131 C132 C130 122.556(3) 2 2
C133 C131 C132 C130 4.1 2 2
C130 C131 C132 C130 78.373(3) . 2
C132 C132 C133 C131 -162.110(2) 2 2
C131 C132 C133 C131 -171.7 . 2
C133 C132 C133 C131 142.877(2) 2 2
C130 C132 C133 C131 46.226(1) 2 2
C132 C132 C133 C128 9.568(2) 2 .
C131 C132 C133 C128 171.678(1) 2 .
C131 C132 C133 C128 0.0 . .
C133 C132 C133 C128 -45.4 2 .
C130 C132 C133 C128 -142.096(2) 2 .
C131 C132 C133 C132 162.1 2 2
C131 C132 C133 C132 -9.6 . 2
C133 C132 C133 C132 -55.013(1) 2 2
C130 C132 C133 C132 -151.664(1) 2 2
C132 C132 C133 C130 151.664(1) 2 2
C131 C132 C133 C130 -46.226(1) 2 2
C131 C132 C133 C130 142.059(2) . 2
C133 C132 C133 C130 96.651(1) 2 2
C129 C128 C133 C131 16.971(2) . 2
C134 C128 C133 C131 -172.626(1) . 2
C129 C128 C133 C132 0.035(1) . .
C134 C128 C133 C132 170.4 . .
C129 C128 C133 C132 2.7 . 2
C134 C128 C133 C132 173.103(2) . 2
C129 C128 C133 C130 -108.675(2) . 2
C134 C128 C133 C130 61.728(3) . 2
C141 C135 C136 C137 -176.9 . .
C140 C135 C136 C137 -0.013(1) . .
C135 C136 C137 C138 0.000(1) . .
C136 C137 C138 C139 0.0 . .
C137 C138 C139 C140 0.027(1) . .
C138 C139 C140 C135 -0.040(1) . .
C141 C135 C140 C139 176.7 . .
C136 C135 C140 C139 0.0 . .
