#------------------------------------------------------------------------------
#$Date: 2021-04-16 11:46:56 +0300 (Fri, 16 Apr 2021) $
#$Revision: 264242 $
#$URL: file:///home/coder/svn-repositories/cod/cif/4/07/64/4076451.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4076451
loop_
_publ_author_name
'Lohan, Manja'
'Milde, Bianca'
'Heider, Silvio'
'Speck, J. Matthäus'
'Krauße, Sabrina'
'Schaarschmidt, Dieter'
'Rüffer, Tobias'
'Lang, Heinrich'
_publ_section_title
;
 Synthesis, Electrochemistry, Spectroelectrochemistry, and Solid-State
 Structures of Palladium Biferrocenylphosphines and Their Use in C,C
 Cross-Coupling Reactions
;
_journal_issue                   6
_journal_name_full               Organometallics
_journal_page_first              2310
_journal_paper_doi               10.1021/om201220w
_journal_volume                  31
_journal_year                    2012
_chemical_formula_moiety         'C56 H46 Cl2 Fe4 O4 P2 Pd, 2/3(C H Cl3)'
_chemical_formula_sum            'C57.33333 H47.33333 Cl5.33333 Fe4 O4 P2 Pd'
_chemical_formula_weight         1381.09
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                103.956(3)
_cell_angle_beta                 92.056(3)
_cell_angle_gamma                103.990(3)
_cell_formula_units_Z            3
_cell_length_a                   10.7582(4)
_cell_length_b                   15.1506(5)
_cell_length_c                   26.4251(9)
_cell_measurement_reflns_used    15096
_cell_measurement_temperature    105
_cell_measurement_theta_max      28.7082
_cell_measurement_theta_min      2.9833
_cell_volume                     4035.6(3)
_computing_cell_refinement
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.46 (release 27-08-2009 CrysAlis171 .NET)
(compiled Aug 27 2009,17:19:36)
;
_computing_data_collection
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.46 (release 27-08-2009 CrysAlis171 .NET)
(compiled Aug 27 2009,17:19:36)
;
_computing_data_reduction
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.46 (release 27-08-2009 CrysAlis171 .NET)
(compiled Aug 27 2009,17:19:36)
;
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      105
_diffrn_measured_fraction_theta_full 0.995
_diffrn_measured_fraction_theta_max 0.995
_diffrn_measurement_device_type  'Oxford Gemini S'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0372
_diffrn_reflns_av_sigmaI/netI    0.0631
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_number            33156
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         26.00
_diffrn_reflns_theta_min         2.98
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 50
_diffrn_standards_interval_time  10
_diffrn_standards_number         2
_exptl_absorpt_coefficient_mu    1.752
_exptl_absorpt_correction_T_max  1.00000
_exptl_absorpt_correction_T_min  0.65526
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
CrysAlisPro, Oxford Diffraction Ltd.,
Version 1.171.33.46 (release 27-08-2009 CrysAlis171 .NET)
(compiled Aug 27 2009,17:19:36)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    1.705
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2082
_exptl_crystal_size_max          0.35
_exptl_crystal_size_mid          0.15
_exptl_crystal_size_min          0.08
_refine_diff_density_max         3.463
_refine_diff_density_min         -1.313
_refine_diff_density_rms         0.184
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.080
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     997
_refine_ls_number_reflns         15792
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.080
_refine_ls_R_factor_all          0.1026
_refine_ls_R_factor_gt           0.0689
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0914P)²+35.2423P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1981
_refine_ls_wR_factor_ref         0.2079
_reflns_number_gt                10531
_reflns_number_total             15792
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om201220w_si_001.cif
_cod_data_source_block           exp_072
_cod_depositor_comments
;

2021-04-11
Z value and formula fixed to values more according to usual
chemical conventions.                 miguel
;
_cod_original_formula_sum            'C172 H142 Cl16 Fe12 O12 P6 Pd3'
_cod_original_formula_weight         4143.28
_cod_original_formula_moiety         '3(C56 H46 Cl2 Fe4 O4 P2 Pd), 2(C H Cl3)'
_cod_original_formula_units_Z            1
_cod_original_cell_volume        4035.6(2)
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4076451
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
C1 C 0.6011(7) -0.0788(5) 0.6617(3) 0.0189(16) Uani 1 1 d .
C2 C 0.7038(7) -0.1035(6) 0.6318(3) 0.0188(16) Uani 1 1 d .
H2 H 0.7671 -0.0628 0.6193 0.023 Uiso 1 1 calc R
C3 C 0.6899(8) -0.1999(6) 0.6254(3) 0.0235(18) Uani 1 1 d .
H3 H 0.7430 -0.2342 0.6075 0.028 Uiso 1 1 calc R
C4 C 0.5834(9) -0.2367(6) 0.6500(3) 0.0242(18) Uani 1 1 d .
H4 H 0.5553 -0.2991 0.6514 0.029 Uiso 1 1 calc R
C5 C 0.5246(8) -0.1627(5) 0.6728(3) 0.0205(17) Uani 1 1 d .
H5 H 0.4520 -0.1679 0.6910 0.025 Uiso 1 1 calc R
C6 C 0.4178(8) -0.1262(7) 0.5493(3) 0.029(2) Uani 1 1 d .
H6 H 0.4005 -0.0674 0.5587 0.035 Uiso 1 1 calc R
C7 C 0.5243(8) -0.1473(6) 0.5221(3) 0.0271(19) Uani 1 1 d .
H7 H 0.5885 -0.1052 0.5109 0.033 Uiso 1 1 calc R
C8 C 0.5125(8) -0.2458(5) 0.5156(3) 0.0198(17) Uani 1 1 d .
C9 C 0.4030(8) -0.2835(6) 0.5388(3) 0.0245(18) Uani 1 1 d .
H9 H 0.3742 -0.3457 0.5404 0.029 Uiso 1 1 calc R
C10 C 0.3439(8) -0.2091(7) 0.5595(3) 0.033(2) Uani 1 1 d .
H10 H 0.2695 -0.2147 0.5767 0.040 Uiso 1 1 calc R
C11 C 0.6027(8) -0.2976(6) 0.4908(3) 0.0231(18) Uani 1 1 d .
C12 C 0.6957(8) -0.2675(6) 0.4572(3) 0.0217(17) Uani 1 1 d .
H12 H 0.7115 -0.2104 0.4482 0.026 Uiso 1 1 calc R
C13 C 0.7594(9) -0.3385(6) 0.4399(3) 0.029(2) Uani 1 1 d .
H13 H 0.8245 -0.3363 0.4176 0.035 Uiso 1 1 calc R
C14 C 0.7075(11) -0.4138(7) 0.4621(4) 0.039(2) Uani 1 1 d .
H14 H 0.7326 -0.4696 0.4574 0.047 Uiso 1 1 calc R
C15 C 0.6103(9) -0.3884(6) 0.4928(3) 0.032(2) Uani 1 1 d .
H15 H 0.5594 -0.4257 0.5114 0.038 Uiso 1 1 calc R
C16 C 0.3778(9) -0.4063(7) 0.3930(4) 0.037(2) Uani 1 1 d .
H16 H 0.3171 -0.3863 0.4139 0.045 Uiso 1 1 calc R
C17 C 0.4579(9) -0.3535(6) 0.3636(3) 0.031(2) Uani 1 1 d .
H17 H 0.4585 -0.2930 0.3614 0.037 Uiso 1 1 calc R
C18 C 0.5374(8) -0.4096(6) 0.3380(3) 0.0229(18) Uani 1 1 d .
H18 H 0.6001 -0.3917 0.3165 0.027 Uiso 1 1 calc R
C19 C 0.5049(9) -0.4968(6) 0.3508(3) 0.030(2) Uani 1 1 d .
H19 H 0.5415 -0.5468 0.3390 0.036 Uiso 1 1 calc R
C20 C 0.4059(9) -0.4947(7) 0.3852(4) 0.036(2) Uani 1 1 d .
H20 H 0.3667 -0.5431 0.3999 0.043 Uiso 1 1 calc R
C21 C 0.6658(7) 0.1020(6) 0.6399(3) 0.0214(17) Uani 1 1 d .
C22 C 0.7496(8) 0.1870(6) 0.6553(4) 0.030(2) Uani 1 1 d .
H22 H 0.7737 0.2237 0.6895 0.037 Uiso 1 1 calc R
C23 C 0.7947(9) 0.2104(7) 0.6087(4) 0.037(2) Uani 1 1 d .
H23 H 0.8549 0.2645 0.6066 0.045 Uiso 1 1 calc R
C24 C 0.7324(8) 0.1383(7) 0.5691(4) 0.036(2) Uani 1 1 d .
H24 H 0.7420 0.1356 0.5339 0.043 Uiso 1 1 calc R
C25 C 0.6530(7) 0.0886(5) 0.7421(3) 0.0195(17) Uani 1 1 d .
C26 C 0.7244(8) 0.0578(6) 0.7743(3) 0.0236(18) Uani 1 1 d .
H26 H 0.7455 0.0003 0.7669 0.028 Uiso 1 1 calc R
C27 C 0.7604(8) 0.1301(7) 0.8214(3) 0.034(2) Uani 1 1 d .
H27 H 0.8098 0.1296 0.8509 0.041 Uiso 1 1 calc R
C28 C 0.7091(10) 0.2000(7) 0.8152(3) 0.038(2) Uani 1 1 d .
H28 H 0.7181 0.2565 0.8404 0.045 Uiso 1 1 calc R
C29 C 0.1136(7) 0.1582(5) 0.6959(3) 0.0174(16) Uani 1 1 d .
C30 C 0.1824(8) 0.2369(5) 0.6776(3) 0.0215(17) Uani 1 1 d .
H30 H 0.2467 0.2373 0.6550 0.026 Uiso 1 1 calc R
C31 C 0.1313(8) 0.3147(5) 0.7015(3) 0.0202(17) Uani 1 1 d .
H31 H 0.1561 0.3749 0.6965 0.024 Uiso 1 1 calc R
C32 C 0.0372(8) 0.2842(6) 0.7337(3) 0.0228(18) Uani 1 1 d .
H32 H -0.0082 0.3222 0.7541 0.027 Uiso 1 1 calc R
C33 C 0.0220(7) 0.1887(6) 0.7306(3) 0.0197(17) Uani 1 1 d .
H33 H -0.0356 0.1519 0.7474 0.024 Uiso 1 1 calc R
C34 C 0.3494(8) 0.2242(6) 0.7935(3) 0.0216(17) Uani 1 1 d .
H34 H 0.3775 0.1704 0.7804 0.026 Uiso 1 1 calc R
C35 C 0.4003(8) 0.3130(6) 0.7841(3) 0.0235(18) Uani 1 1 d .
H35 H 0.4676 0.3278 0.7640 0.028 Uiso 1 1 calc R
C36 C 0.3303(8) 0.3767(6) 0.8110(3) 0.0213(17) Uani 1 1 d .
H36 H 0.3431 0.4397 0.8111 0.026 Uiso 1 1 calc R
C37 C 0.2374(7) 0.3251(5) 0.8375(3) 0.0178(16) Uani 1 1 d .
C38 C 0.2474(8) 0.2302(5) 0.8264(3) 0.0223(18) Uani 1 1 d .
H38 H 0.1972 0.1815 0.8382 0.027 Uiso 1 1 calc R
C39 C 0.1429(8) 0.3602(5) 0.8695(3) 0.0230(18) Uani 1 1 d .
C40 C 0.1346(8) 0.4563(6) 0.8869(3) 0.0231(18) Uani 1 1 d .
H40 H 0.1872 0.5080 0.8784 0.028 Uiso 1 1 calc R
C41 C 0.0323(8) 0.4582(6) 0.9193(3) 0.0253(19) Uani 1 1 d .
H41 H 0.0058 0.5115 0.9351 0.030 Uiso 1 1 calc R
C42 C -0.0233(8) 0.3652(6) 0.9236(4) 0.029(2) Uani 1 1 d .
H42 H -0.0914 0.3473 0.9429 0.035 Uiso 1 1 calc R
C43 C 0.0436(8) 0.3053(6) 0.8934(3) 0.0242(18) Uani 1 1 d .
H43 H 0.0267 0.2407 0.8895 0.029 Uiso 1 1 calc R
C44 C 0.3423(9) 0.3876(7) 0.9685(4) 0.035(2) Uani 1 1 d .
H44 H 0.3959 0.3637 0.9451 0.042 Uiso 1 1 calc R
C45 C 0.3423(10) 0.4832(7) 0.9857(4) 0.040(2) Uani 1 1 d .
H45 H 0.3951 0.5329 0.9755 0.047 Uiso 1 1 calc R
C46 C 0.2482(10) 0.4901(7) 1.0211(4) 0.040(2) Uani 1 1 d .
H46 H 0.2281 0.5452 1.0385 0.049 Uiso 1 1 calc R
C47 C 0.1897(11) 0.3984(7) 1.0255(4) 0.041(3) Uani 1 1 d .
H47 H 0.1243 0.3827 1.0463 0.050 Uiso 1 1 calc R
C48 C 0.2484(10) 0.3342(7) 0.9924(4) 0.036(2) Uani 1 1 d .
H48 H 0.2282 0.2693 0.9876 0.043 Uiso 1 1 calc R
C49 C 0.0523(8) -0.0158(6) 0.6168(3) 0.0222(18) Uani 1 1 d .
C50 C -0.0183(8) 0.0153(7) 0.5844(3) 0.0279(19) Uani 1 1 d .
H50 H -0.0329 0.0747 0.5900 0.033 Uiso 1 1 calc R
C51 C -0.0645(9) -0.0626(7) 0.5402(4) 0.038(2) Uani 1 1 d .
H51 H -0.1163 -0.0641 0.5109 0.045 Uiso 1 1 calc R
C52 C -0.0201(10) -0.1330(8) 0.5486(4) 0.044(3) Uani 1 1 d .
H52 H -0.0365 -0.1925 0.5255 0.053 Uiso 1 1 calc R
C53 C 0.0475(7) -0.0183(6) 0.7216(3) 0.0189(16) Uani 1 1 d .
C54 C -0.0351(8) -0.1045(6) 0.7121(3) 0.0217(17) Uani 1 1 d .
H54 H -0.0620 -0.1472 0.6795 0.026 Uiso 1 1 calc R
C55 C -0.0729(9) -0.1173(6) 0.7614(3) 0.0275(19) Uani 1 1 d .
H55 H -0.1285 -0.1702 0.7675 0.033 Uiso 1 1 calc R
C56 C -0.0124(8) -0.0378(6) 0.7973(3) 0.0243(18) Uani 1 1 d .
H56 H -0.0217 -0.0262 0.8330 0.029 Uiso 1 1 calc R
C57 C -0.2381(7) 0.1251(5) 0.0213(3) 0.0151(15) Uani 1 1 d .
C58 C -0.1652(8) 0.2078(5) 0.0080(3) 0.0211(17) Uani 1 1 d .
H58 H -0.0972 0.2116 -0.0128 0.025 Uiso 1 1 calc R
C59 C -0.2189(8) 0.2840(6) 0.0335(3) 0.0203(17) Uani 1 1 d .
H59 H -0.1928 0.3459 0.0312 0.024 Uiso 1 1 calc R
C60 C -0.3178(8) 0.2484(5) 0.0627(3) 0.0188(17) Uani 1 1 d .
H60 H -0.3655 0.2839 0.0835 0.023 Uiso 1 1 calc R
C61 C -0.3332(7) 0.1512(5) 0.0555(3) 0.0172(16) Uani 1 1 d .
H61 H -0.3929 0.1112 0.0699 0.021 Uiso 1 1 calc R
C62 C -0.0195(7) 0.1754(6) 0.1232(3) 0.0195(17) Uani 1 1 d .
H62 H 0.0032 0.1196 0.1095 0.023 Uiso 1 1 calc R
C63 C 0.0412(8) 0.2634(6) 0.1156(3) 0.0229(18) Uani 1 1 d .
H63 H 0.1117 0.2759 0.0966 0.027 Uiso 1 1 calc R
C64 C -0.0237(8) 0.3313(6) 0.1420(3) 0.0193(17) Uani 1 1 d .
H64 H -0.0046 0.3947 0.1424 0.023 Uiso 1 1 calc R
C65 C -0.1229(8) 0.2829(5) 0.1674(3) 0.0188(17) Uani 1 1 d .
C66 C -0.1208(8) 0.1850(5) 0.1550(3) 0.0170(16) Uani 1 1 d .
H66 H -0.1758 0.1372 0.1660 0.020 Uiso 1 1 calc R
C67 C -0.2169(8) 0.3212(5) 0.1974(3) 0.0216(17) Uani 1 1 d .
C68 C -0.2187(9) 0.4185(6) 0.2141(3) 0.0255(19) Uani 1 1 d .
H68 H -0.1581 0.4695 0.2084 0.031 Uiso 1 1 calc R
C69 C -0.3308(10) 0.4224(6) 0.2413(3) 0.034(2) Uani 1 1 d .
H69 H -0.3559 0.4769 0.2559 0.041 Uiso 1 1 calc R
C70 C -0.3967(9) 0.3309(6) 0.2423(3) 0.0271(19) Uani 1 1 d .
H70 H -0.4731 0.3144 0.2572 0.033 Uiso 1 1 calc R
C71 C -0.3265(8) 0.2676(6) 0.2165(3) 0.0236(18) Uani 1 1 d .
H71 H -0.3476 0.2029 0.2125 0.028 Uiso 1 1 calc R
C72 C -0.0495(9) 0.3407(7) 0.3065(3) 0.033(2) Uani 1 1 d .
H72 H 0.0088 0.3144 0.2870 0.040 Uiso 1 1 calc R
C73 C -0.0455(10) 0.4367(7) 0.3225(4) 0.044(3) Uani 1 1 d .
H73 H 0.0169 0.4852 0.3153 0.053 Uiso 1 1 calc R
C74 C -0.1534(10) 0.4478(6) 0.3517(3) 0.038(2) Uani 1 1 d .
H74 H -0.1737 0.5041 0.3667 0.046 Uiso 1 1 calc R
C75 C -0.2221(9) 0.3571(7) 0.3530(3) 0.033(2) Uani 1 1 d .
H75 H -0.2970 0.3428 0.3692 0.040 Uiso 1 1 calc R
C76 C -0.1592(9) 0.2913(7) 0.3259(3) 0.033(2) Uani 1 1 d .
H76 H -0.1851 0.2265 0.3214 0.039 Uiso 1 1 calc R
C77 C -0.2965(7) -0.0414(5) -0.0614(3) 0.0174(16) Uani 1 1 d .
C78 C -0.3660(8) -0.0078(6) -0.0927(3) 0.0214(17) Uani 1 1 d .
H78 H -0.3870 0.0497 -0.0843 0.026 Uiso 1 1 calc R
C79 C -0.4003(9) -0.0785(7) -0.1408(3) 0.031(2) Uani 1 1 d .
H79 H -0.4474 -0.0760 -0.1704 0.038 Uiso 1 1 calc R
C80 C -0.3514(10) -0.1500(7) -0.1353(3) 0.039(2) Uani 1 1 d .
H80 H -0.3609 -0.2060 -0.1609 0.046 Uiso 1 1 calc R
C81 C -0.3093(7) -0.0561(5) 0.0412(3) 0.0155(15) Uani 1 1 d .
C82 C -0.3976(8) -0.1395(6) 0.0278(3) 0.0234(18) Uani 1 1 d .
H82 H -0.4275 -0.1763 -0.0060 0.028 Uiso 1 1 calc R
C83 C -0.4360(8) -0.1603(6) 0.0749(3) 0.0267(19) Uani 1 1 d .
H83 H -0.4964 -0.2135 0.0783 0.032 Uiso 1 1 calc R
C84 C -0.3682(8) -0.0886(6) 0.1138(3) 0.0235(18) Uani 1 1 d .
H84 H -0.3749 -0.0843 0.1493 0.028 Uiso 1 1 calc R
C85 C 0.3167(14) 0.4786(9) 0.2230(6) 0.073(4) Uani 1 1 d .
H85 H 0.3993 0.5110 0.2439 0.088 Uiso 1 1 calc R
C86 C -0.007(2) 0.451(2) 0.4661(9) 0.169(12) Uani 1 1 d .
H86 H -0.0781 0.4435 0.4398 0.203 Uiso 1 1 calc R
O1 O 0.6527(6) 0.0692(4) 0.5864(2) 0.0306(14) Uani 1 1 d .
O2 O 0.6417(6) 0.1767(4) 0.7667(2) 0.0336(15) Uani 1 1 d .
O3 O 0.0528(7) -0.1060(4) 0.5956(2) 0.0360(16) Uani 1 1 d .
O4 O 0.0651(5) 0.0237(4) 0.7741(2) 0.0212(12) Uani 1 1 d .
O5 O -0.2863(6) -0.1288(4) -0.0871(2) 0.0316(15) Uani 1 1 d .
O6 O -0.2885(5) -0.0230(4) 0.0947(2) 0.0212(12) Uani 1 1 d .
Fe1 Fe 0.52835(11) -0.17821(8) 0.59352(4) 0.0193(3) Uani 1 1 d .
Fe2 Fe 0.56724(12) -0.38865(8) 0.41721(4) 0.0223(3) Uani 1 1 d .
Fe3 Fe 0.20724(11) 0.26438(8) 0.75819(4) 0.0176(3) Uani 1 1 d .
Fe4 Fe 0.16825(12) 0.40609(8) 0.94943(5) 0.0223(3) Uani 1 1 d .
Fe5 Fe -0.15035(10) 0.22477(7) 0.08763(4) 0.0151(2) Uani 1 1 d .
Fe6 Fe -0.21255(12) 0.36458(8) 0.27767(4) 0.0224(3) Uani 1 1 d .
Pd1 Pd 0.35422(6) 0.03564(4) 0.67847(2) 0.01591(15) Uani 1 1 d .
Pd2 Pd 0.0000 0.0000 0.0000 0.01367(19) Uani 1 2 d S
P1 P 0.56830(19) 0.03424(14) 0.67826(7) 0.0155(4) Uani 1 1 d .
P2 P 0.14275(19) 0.04229(14) 0.67977(7) 0.0153(4) Uani 1 1 d .
P3 P -0.21063(19) 0.01019(13) 0.00235(7) 0.0137(4) Uani 1 1 d .
Cl1 Cl 0.3622(2) 0.10013(14) 0.60811(8) 0.0244(4) Uani 1 1 d .
Cl2 Cl 0.34350(18) -0.03301(13) 0.74787(7) 0.0195(4) Uani 1 1 d .
Cl3 Cl 0.01803(19) 0.08072(13) -0.06408(7) 0.0200(4) Uani 1 1 d .
Cl4 Cl 0.2553(3) 0.3762(2) 0.24258(15) 0.0707(9) Uani 1 1 d .
Cl5 Cl 0.2165(4) 0.5544(3) 0.2359(2) 0.0984(14) Uani 1 1 d .
Cl6 Cl 0.3472(4) 0.4518(4) 0.15814(16) 0.1056(16) Uani 1 1 d .
Cl7 Cl 0.0916(9) 0.3768(7) 0.4338(3) 0.210(4) Uani 1 1 d .
Cl8 Cl 0.0773(4) 0.5744(4) 0.48169(19) 0.1089(17) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe Fe 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pd Pd -0.9988 1.0072 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C5 C1 C2 108.2(7) . .
C5 C1 P1 125.6(6) . .
C2 C1 P1 126.1(6) . .
C5 C1 Fe1 70.1(4) . .
C2 C1 Fe1 69.2(4) . .
P1 C1 Fe1 123.4(4) . .
C3 C2 C1 107.2(7) . .
C3 C2 Fe1 69.8(5) . .
C1 C2 Fe1 69.1(4) . .
C3 C2 H2 126.4 . .
C1 C2 H2 126.4 . .
Fe1 C2 H2 126.2 . .
C2 C3 C4 109.4(7) . .
C2 C3 Fe1 69.9(5) . .
C4 C3 Fe1 70.4(5) . .
C2 C3 H3 125.3 . .
C4 C3 H3 125.3 . .
Fe1 C3 H3 126.0 . .
C3 C4 C5 109.1(7) . .
C3 C4 Fe1 69.4(5) . .
C5 C4 Fe1 69.7(5) . .
C3 C4 H4 125.4 . .
C5 C4 H4 125.4 . .
Fe1 C4 H4 127.0 . .
C4 C5 C1 106.0(7) . .
C4 C5 Fe1 69.3(4) . .
C1 C5 Fe1 68.7(4) . .
C4 C5 H5 127.0 . .
C1 C5 H5 127.0 . .
Fe1 C5 H5 126.5 . .
C10 C6 C7 108.6(8) . .
C10 C6 Fe1 69.8(5) . .
C7 C6 Fe1 69.6(5) . .
C10 C6 H6 125.7 . .
C7 C6 H6 125.7 . .
Fe1 C6 H6 126.5 . .
C8 C7 C6 106.7(8) . .
C8 C7 Fe1 69.3(5) . .
C6 C7 Fe1 69.4(5) . .
C8 C7 H7 126.6 . .
C6 C7 H7 126.6 . .
Fe1 C7 H7 126.2 . .
C9 C8 C7 108.7(7) . .
C9 C8 C11 125.8(7) . .
C7 C8 C11 125.5(7) . .
C9 C8 Fe1 69.6(4) . .
C7 C8 Fe1 69.7(4) . .
C11 C8 Fe1 124.8(6) . .
C8 C9 C10 107.9(8) . .
C8 C9 Fe1 70.1(5) . .
C10 C9 Fe1 69.7(5) . .
C8 C9 H9 126.1 . .
C10 C9 H9 126.1 . .
Fe1 C9 H9 125.7 . .
C6 C10 C9 108.1(8) . .
C6 C10 Fe1 70.0(5) . .
C9 C10 Fe1 69.3(5) . .
C6 C10 H10 125.9 . .
C9 C10 H10 125.9 . .
Fe1 C10 H10 126.3 . .
C15 C11 C12 106.4(7) . .
C15 C11 C8 127.3(8) . .
C12 C11 C8 126.2(7) . .
C15 C11 Fe2 68.9(5) . .
C12 C11 Fe2 68.6(4) . .
C8 C11 Fe2 124.6(6) . .
C13 C12 C11 108.8(7) . .
C13 C12 Fe2 69.9(5) . .
C11 C12 Fe2 70.5(5) . .
C13 C12 H12 125.6 . .
C11 C12 H12 125.6 . .
Fe2 C12 H12 125.5 . .
C12 C13 C14 108.2(8) . .
C12 C13 Fe2 69.6(5) . .
C14 C13 Fe2 70.3(6) . .
C12 C13 H13 125.9 . .
C14 C13 H13 125.9 . .
Fe2 C13 H13 125.8 . .
C13 C14 C15 107.2(8) . .
C13 C14 Fe2 69.3(5) . .
C15 C14 Fe2 69.1(6) . .
C13 C14 H14 126.4 . .
C15 C14 H14 126.4 . .
Fe2 C14 H14 126.8 . .
C11 C15 C14 109.3(8) . .
C11 C15 Fe2 70.7(5) . .
C14 C15 Fe2 70.2(5) . .
C11 C15 H15 125.3 . .
C14 C15 H15 125.3 . .
Fe2 C15 H15 125.3 . .
C20 C16 C17 108.3(8) . .
C20 C16 Fe2 69.9(6) . .
C17 C16 Fe2 70.1(5) . .
C20 C16 H16 125.9 . .
C17 C16 H16 125.9 . .
Fe2 C16 H16 125.8 . .
C16 C17 C18 107.6(8) . .
C16 C17 Fe2 69.6(5) . .
C18 C17 Fe2 69.2(5) . .
C16 C17 H17 126.2 . .
C18 C17 H17 126.2 . .
Fe2 C17 H17 126.6 . .
C19 C18 C17 108.3(7) . .
C19 C18 Fe2 70.3(5) . .
C17 C18 Fe2 70.2(5) . .
C19 C18 H18 125.8 . .
C17 C18 H18 125.8 . .
Fe2 C18 H18 125.3 . .
C18 C19 C20 107.7(8) . .
C18 C19 Fe2 69.4(5) . .
C20 C19 Fe2 69.6(5) . .
C18 C19 H19 126.1 . .
C20 C19 H19 126.1 . .
Fe2 C19 H19 126.4 . .
C16 C20 C19 108.0(8) . .
C16 C20 Fe2 69.8(5) . .
C19 C20 Fe2 69.7(5) . .
C16 C20 H20 126.0 . .
C19 C20 H20 126.0 . .
Fe2 C20 H20 126.1 . .
C22 C21 O1 110.8(7) . .
C22 C21 P1 129.6(7) . .
O1 C21 P1 119.4(6) . .
C21 C22 C23 106.6(9) . .
C21 C22 H22 126.7 . .
C23 C22 H22 126.7 . .
C24 C23 C22 105.7(8) . .
C24 C23 H23 127.1 . .
C22 C23 H23 127.1 . .
C23 C24 O1 111.8(8) . .
C23 C24 H24 124.1 . .
O1 C24 H24 124.1 . .
C26 C25 O2 109.9(7) . .
C26 C25 P1 132.5(6) . .
O2 C25 P1 117.5(6) . .
C25 C26 C27 106.7(8) . .
C25 C26 H26 126.6 . .
C27 C26 H26 126.6 . .
C28 C27 C26 106.6(8) . .
C28 C27 H27 126.7 . .
C26 C27 H27 126.7 . .
C27 C28 O2 110.9(8) . .
C27 C28 H28 124.6 . .
O2 C28 H28 124.6 . .
C30 C29 C33 108.6(7) . .
C30 C29 P2 125.0(6) . .
C33 C29 P2 126.3(6) . .
C30 C29 Fe3 70.5(4) . .
C33 C29 Fe3 69.8(4) . .
P2 C29 Fe3 123.8(4) . .
C31 C30 C29 106.0(7) . .
C31 C30 Fe3 69.6(4) . .
C29 C30 Fe3 68.3(4) . .
C31 C30 H30 127.0 . .
C29 C30 H30 127.0 . .
Fe3 C30 H30 126.6 . .
C32 C31 C30 108.5(7) . .
C32 C31 Fe3 68.7(5) . .
C30 C31 Fe3 69.6(5) . .
C32 C31 H31 125.7 . .
C30 C31 H31 125.7 . .
Fe3 C31 H31 127.6 . .
C33 C32 C31 110.2(7) . .
C33 C32 Fe3 70.7(5) . .
C31 C32 Fe3 71.1(5) . .
C33 C32 H32 124.9 . .
C31 C32 H32 124.9 . .
Fe3 C32 H32 124.9 . .
C32 C33 C29 106.6(7) . .
C32 C33 Fe3 69.3(5) . .
C29 C33 Fe3 68.5(4) . .
C32 C33 H33 126.7 . .
C29 C33 H33 126.7 . .
Fe3 C33 H33 127.1 . .
C35 C34 C38 108.9(7) . .
C35 C34 Fe3 70.3(5) . .
C38 C34 Fe3 69.6(5) . .
C35 C34 H34 125.6 . .
C38 C34 H34 125.6 . .
Fe3 C34 H34 126.1 . .
C34 C35 C36 108.2(7) . .
C34 C35 Fe3 69.6(5) . .
C36 C35 Fe3 69.5(4) . .
C34 C35 H35 125.9 . .
C36 C35 H35 125.9 . .
Fe3 C35 H35 126.6 . .
C37 C36 C35 107.1(7) . .
C37 C36 Fe3 69.6(4) . .
C35 C36 Fe3 69.7(4) . .
C37 C36 H36 126.4 . .
C35 C36 H36 126.4 . .
Fe3 C36 H36 125.8 . .
C36 C37 C38 108.8(7) . .
C36 C37 C39 127.0(7) . .
C38 C37 C39 124.2(7) . .
C36 C37 Fe3 69.7(4) . .
C38 C37 Fe3 69.5(4) . .
C39 C37 Fe3 125.1(6) . .
C37 C38 C34 107.0(7) . .
C37 C38 Fe3 69.8(4) . .
C34 C38 Fe3 69.6(5) . .
C37 C38 H38 126.5 . .
C34 C38 H38 126.5 . .
Fe3 C38 H38 125.7 . .
C40 C39 C43 106.0(7) . .
C40 C39 C37 127.5(7) . .
C43 C39 C37 126.3(7) . .
C40 C39 Fe4 68.9(5) . .
C43 C39 Fe4 68.4(5) . .
C37 C39 Fe4 124.0(6) . .
C41 C40 C39 108.1(7) . .
C41 C40 Fe4 70.0(5) . .
C39 C40 Fe4 69.6(5) . .
C41 C40 H40 125.9 . .
C39 C40 H40 125.9 . .
Fe4 C40 H40 126.0 . .
C40 C41 C42 109.0(7) . .
C40 C41 Fe4 69.3(5) . .
C42 C41 Fe4 69.6(5) . .
C40 C41 H41 125.5 . .
C42 C41 H41 125.5 . .
Fe4 C41 H41 127.3 . .
C43 C42 C41 107.5(7) . .
C43 C42 Fe4 69.0(5) . .
C41 C42 Fe4 69.6(5) . .
C43 C42 H42 126.3 . .
C41 C42 H42 126.3 . .
Fe4 C42 H42 126.7 . .
C42 C43 C39 109.4(7) . .
C42 C43 Fe4 70.5(5) . .
C39 C43 Fe4 69.8(5) . .
C42 C43 H43 125.3 . .
C39 C43 H43 125.3 . .
Fe4 C43 H43 126.0 . .
C48 C44 C45 109.0(9) . .
C48 C44 Fe4 70.8(5) . .
C45 C44 Fe4 69.3(5) . .
C48 C44 H44 125.5 . .
C45 C44 H44 125.5 . .
Fe4 C44 H44 126.0 . .
C46 C45 C44 107.9(9) . .
C46 C45 Fe4 70.4(6) . .
C44 C45 Fe4 69.8(5) . .
C46 C45 H45 126.0 . .
C44 C45 H45 126.0 . .
Fe4 C45 H45 125.3 . .
C45 C46 C47 107.9(9) . .
C45 C46 Fe4 69.0(5) . .
C47 C46 Fe4 70.3(6) . .
C45 C46 H46 126.1 . .
C47 C46 H46 126.1 . .
Fe4 C46 H46 126.3 . .
C46 C47 C48 108.2(9) . .
C46 C47 Fe4 69.2(5) . .
C48 C47 Fe4 69.7(5) . .
C46 C47 H47 125.9 . .
C48 C47 H47 125.9 . .
Fe4 C47 H47 126.8 . .
C44 C48 C47 107.0(9) . .
C44 C48 Fe4 68.8(5) . .
C47 C48 Fe4 69.6(5) . .
C44 C48 H48 126.5 . .
C47 C48 H48 126.5 . .
Fe4 C48 H48 126.6 . .
O3 C49 C50 110.9(7) . .
O3 C49 P2 117.5(6) . .
C50 C49 P2 131.6(7) . .
C49 C50 C51 105.1(9) . .
C49 C50 H50 127.4 . .
C51 C50 H50 127.4 . .
C52 C51 C50 107.2(9) . .
C52 C51 H51 126.4 . .
C50 C51 H51 126.4 . .
C51 C52 O3 110.6(9) . .
C51 C52 H52 124.7 . .
O3 C52 H52 124.7 . .
C54 C53 O4 110.0(7) . .
C54 C53 P2 132.2(6) . .
O4 C53 P2 117.6(6) . .
C53 C54 C55 106.8(7) . .
C53 C54 H54 126.6 . .
C55 C54 H54 126.6 . .
C56 C55 C54 106.4(7) . .
C56 C55 H55 126.8 . .
C54 C55 H55 126.8 . .
C55 C56 O4 110.4(7) . .
C55 C56 H56 124.8 . .
O4 C56 H56 124.8 . .
C58 C57 C61 108.6(6) . .
C58 C57 P3 126.0(6) . .
C61 C57 P3 125.3(6) . .
C58 C57 Fe5 69.9(4) . .
C61 C57 Fe5 69.5(4) . .
P3 C57 Fe5 123.6(4) . .
C57 C58 C59 106.2(7) . .
C57 C58 Fe5 69.0(4) . .
C59 C58 Fe5 69.8(4) . .
C57 C58 H58 126.9 . .
C59 C58 H58 126.9 . .
Fe5 C58 H58 125.9 . .
C60 C59 C58 108.5(7) . .
C60 C59 Fe5 68.8(4) . .
C58 C59 Fe5 69.0(4) . .
C60 C59 H59 125.8 . .
C58 C59 H59 125.8 . .
Fe5 C59 H59 128.0 . .
C61 C60 C59 109.7(7) . .
C61 C60 Fe5 70.3(4) . .
C59 C60 Fe5 70.8(5) . .
C61 C60 H60 125.2 . .
C59 C60 H60 125.2 . .
Fe5 C60 H60 125.3 . .
C60 C61 C57 107.0(7) . .
C60 C61 Fe5 69.4(4) . .
C57 C61 Fe5 68.9(4) . .
C60 C61 H61 126.5 . .
C57 C61 H61 126.5 . .
Fe5 C61 H61 126.8 . .
C63 C62 C66 109.2(7) . .
C63 C62 Fe5 70.6(5) . .
C66 C62 Fe5 70.1(4) . .
C63 C62 H62 125.4 . .
C66 C62 H62 125.4 . .
Fe5 C62 H62 125.5 . .
C62 C63 C64 108.6(7) . .
C62 C63 Fe5 69.5(4) . .
C64 C63 Fe5 69.2(4) . .
C62 C63 H63 125.7 . .
C64 C63 H63 125.7 . .
Fe5 C63 H63 127.2 . .
C65 C64 C63 107.0(7) . .
C65 C64 Fe5 70.0(4) . .
C63 C64 Fe5 69.8(4) . .
C65 C64 H64 126.5 . .
C63 C64 H64 126.5 . .
Fe5 C64 H64 125.3 . .
C64 C65 C66 107.9(7) . .
C64 C65 C67 127.4(7) . .
C66 C65 C67 124.6(7) . .
C64 C65 Fe5 69.3(4) . .
C66 C65 Fe5 69.1(4) . .
C67 C65 Fe5 123.8(6) . .
C62 C66 C65 107.3(7) . .
C62 C66 Fe5 69.5(4) . .
C65 C66 Fe5 69.7(4) . .
C62 C66 H66 126.4 . .
C65 C66 H66 126.4 . .
Fe5 C66 H66 126.0 . .
C68 C67 C71 107.1(7) . .
C68 C67 C65 127.1(8) . .
C71 C67 C65 125.8(7) . .
C68 C67 Fe6 68.9(4) . .
C71 C67 Fe6 68.3(4) . .
C65 C67 Fe6 127.6(6) . .
C69 C68 C67 107.4(8) . .
C69 C68 Fe6 69.4(5) . .
C67 C68 Fe6 70.1(5) . .
C69 C68 H68 126.3 . .
C67 C68 H68 126.3 . .
Fe6 C68 H68 125.8 . .
C70 C69 C68 109.1(8) . .
C70 C69 Fe6 70.3(5) . .
C68 C69 Fe6 69.5(5) . .
C70 C69 H69 125.5 . .
C68 C69 H69 125.5 . .
Fe6 C69 H69 126.3 . .
C69 C70 C71 108.2(8) . .
C69 C70 Fe6 69.5(6) . .
C71 C70 Fe6 68.7(5) . .
C69 C70 H70 125.9 . .
C71 C70 H70 125.9 . .
Fe6 C70 H70 127.4 . .
C70 C71 C67 108.2(7) . .
C70 C71 Fe6 70.4(5) . .
C67 C71 Fe6 70.4(4) . .
C70 C71 H71 125.9 . .
C67 C71 H71 125.9 . .
Fe6 C71 H71 124.8 . .
C73 C72 C76 107.2(8) . .
C73 C72 Fe6 69.5(6) . .
C76 C72 Fe6 69.5(5) . .
C73 C72 H72 126.4 . .
C76 C72 H72 126.4 . .
Fe6 C72 H72 126.2 . .
C72 C73 C74 109.0(8) . .
C72 C73 Fe6 70.1(5) . .
C74 C73 Fe6 69.8(6) . .
C72 C73 H73 125.5 . .
C74 C73 H73 125.5 . .
Fe6 C73 H73 126.2 . .
C75 C74 C73 106.5(8) . .
C75 C74 Fe6 69.3(5) . .
C73 C74 Fe6 68.8(5) . .
C75 C74 H74 126.8 . .
C73 C74 H74 126.8 . .
Fe6 C74 H74 126.7 . .
C74 C75 C76 109.0(8) . .
C74 C75 Fe6 70.2(5) . .
C76 C75 Fe6 69.9(5) . .
C74 C75 H75 125.5 . .
C76 C75 H75 125.5 . .
Fe6 C75 H75 125.9 . .
C75 C76 C72 108.3(8) . .
C75 C76 Fe6 69.5(5) . .
C72 C76 Fe6 69.6(5) . .
C75 C76 H76 125.8 . .
C72 C76 H76 125.8 . .
Fe6 C76 H76 126.6 . .
C78 C77 O5 110.3(7) . .
C78 C77 P3 132.3(6) . .
O5 C77 P3 117.2(6) . .
C77 C78 C79 106.0(8) . .
C77 C78 H78 127.0 . .
C79 C78 H78 127.0 . .
C80 C79 C78 106.7(8) . .
C80 C79 H79 126.6 . .
C78 C79 H79 126.6 . .
C79 C80 O5 110.5(8) . .
C79 C80 H80 124.7 . .
O5 C80 H80 124.7 . .
C82 C81 O6 110.4(7) . .
C82 C81 P3 131.5(6) . .
O6 C81 P3 117.9(5) . .
C81 C82 C83 106.6(7) . .
C81 C82 H82 126.7 . .
C83 C82 H82 126.7 . .
C84 C83 C82 106.4(8) . .
C84 C83 H83 126.8 . .
C82 C83 H83 126.8 . .
C83 C84 O6 111.1(7) . .
C83 C84 H84 124.5 . .
O6 C84 H84 124.5 . .
Cl6 C85 Cl4 110.5(8) . .
Cl6 C85 Cl5 112.8(9) . .
Cl4 C85 Cl5 111.3(8) . .
Cl6 C85 H85 107.3 . .
Cl4 C85 H85 107.3 . .
Cl5 C85 H85 107.3 . .
Cl8 C86 Cl8 109.9(13) 2_566 .
Cl8 C86 Cl7 117.9(18) 2_566 .
Cl8 C86 Cl7 111.7(15) . .
Cl8 C86 H86 105.4 2_566 .
Cl8 C86 H86 105.4 . .
Cl7 C86 H86 105.4 . .
C24 O1 C21 105.1(7) . .
C28 O2 C25 105.9(7) . .
C49 O3 C52 106.1(8) . .
C53 O4 C56 106.4(6) . .
C80 O5 C77 106.4(7) . .
C84 O6 C81 105.5(6) . .
C3 Fe1 C1 68.6(3) . .
C3 Fe1 C2 40.2(3) . .
C1 Fe1 C2 41.7(3) . .
C3 Fe1 C9 120.9(3) . .
C1 Fe1 C9 160.8(3) . .
C2 Fe1 C9 155.8(3) . .
C3 Fe1 C10 158.5(4) . .
C1 Fe1 C10 124.9(3) . .
C2 Fe1 C10 160.9(4) . .
C9 Fe1 C10 41.0(4) . .
C3 Fe1 C8 105.3(3) . .
C1 Fe1 C8 158.1(3) . .
C2 Fe1 C8 120.2(3) . .
C9 Fe1 C8 40.4(3) . .
C10 Fe1 C8 68.3(3) . .
C3 Fe1 C4 40.2(3) . .
C1 Fe1 C4 68.4(3) . .
C2 Fe1 C4 68.1(3) . .
C9 Fe1 C4 107.2(3) . .
C10 Fe1 C4 124.2(4) . .
C8 Fe1 C4 121.3(3) . .
C3 Fe1 C6 158.5(4) . .
C1 Fe1 C6 109.2(3) . .
C2 Fe1 C6 123.8(4) . .
C9 Fe1 C6 68.4(4) . .
C10 Fe1 C6 40.2(4) . .
C8 Fe1 C6 68.4(3) . .
C4 Fe1 C6 160.7(4) . .
C3 Fe1 C7 120.9(3) . .
C1 Fe1 C7 122.8(3) . .
C2 Fe1 C7 105.7(3) . .
C9 Fe1 C7 68.7(3) . .
C10 Fe1 C7 68.6(4) . .
C8 Fe1 C7 41.0(3) . .
C4 Fe1 C7 156.8(3) . .
C6 Fe1 C7 41.0(3) . .
C3 Fe1 C5 68.9(3) . .
C1 Fe1 C5 41.2(3) . .
C2 Fe1 C5 69.8(3) . .
C9 Fe1 C5 123.3(3) . .
C10 Fe1 C5 109.0(3) . .
C8 Fe1 C5 158.2(3) . .
C4 Fe1 C5 41.0(3) . .
C6 Fe1 C5 124.5(3) . .
C7 Fe1 C5 160.1(3) . .
C12 Fe2 C15 68.0(3) . .
C12 Fe2 C13 40.5(3) . .
C15 Fe2 C13 68.1(4) . .
C12 Fe2 C18 116.7(3) . .
C15 Fe2 C18 169.7(3) . .
C13 Fe2 C18 109.0(3) . .
C12 Fe2 C16 127.4(4) . .
C15 Fe2 C16 117.2(4) . .
C13 Fe2 C16 166.0(4) . .
C18 Fe2 C16 68.2(4) . .
C12 Fe2 C14 68.1(4) . .
C15 Fe2 C14 40.6(4) . .
C13 Fe2 C14 40.5(4) . .
C18 Fe2 C14 130.8(4) . .
C16 Fe2 C14 151.4(4) . .
C12 Fe2 C20 166.1(4) . .
C15 Fe2 C20 109.7(4) . .
C13 Fe2 C20 152.7(4) . .
C18 Fe2 C20 68.1(3) . .
C16 Fe2 C20 40.3(4) . .
C14 Fe2 C20 119.7(4) . .
C12 Fe2 C19 150.8(3) . .
C15 Fe2 C19 131.6(4) . .
C13 Fe2 C19 119.2(4) . .
C18 Fe2 C19 40.3(3) . .
C16 Fe2 C19 68.1(4) . .
C14 Fe2 C19 110.9(4) . .
C20 Fe2 C19 40.7(3) . .
C12 Fe2 C17 106.6(3) . .
C15 Fe2 C17 148.9(4) . .
C13 Fe2 C17 128.7(4) . .
C18 Fe2 C17 40.7(3) . .
C16 Fe2 C17 40.4(4) . .
C14 Fe2 C17 168.0(4) . .
C20 Fe2 C17 67.9(4) . .
C19 Fe2 C17 68.0(4) . .
C12 Fe2 C11 40.8(3) . .
C15 Fe2 C11 40.4(3) . .
C13 Fe2 C11 68.5(3) . .
C18 Fe2 C11 149.0(3) . .
C16 Fe2 C11 106.5(4) . .
C14 Fe2 C11 68.4(4) . .
C20 Fe2 C11 128.6(3) . .
C19 Fe2 C11 168.2(3) . .
C17 Fe2 C11 115.2(3) . .
C32 Fe3 C29 68.4(3) . .
C32 Fe3 C34 165.3(3) . .
C29 Fe3 C34 109.7(3) . .
C32 Fe3 C33 40.0(3) . .
C29 Fe3 C33 41.6(3) . .
C34 Fe3 C33 128.9(3) . .
C32 Fe3 C38 126.1(3) . .
C29 Fe3 C38 117.7(3) . .
C34 Fe3 C38 40.8(3) . .
C33 Fe3 C38 106.1(3) . .
C32 Fe3 C37 106.0(3) . .
C29 Fe3 C37 150.4(3) . .
C34 Fe3 C37 68.1(3) . .
C33 Fe3 C37 115.3(3) . .
C38 Fe3 C37 40.7(3) . .
C32 Fe3 C36 116.6(3) . .
C29 Fe3 C36 168.3(3) . .
C34 Fe3 C36 68.3(3) . .
C33 Fe3 C36 148.6(3) . .
C38 Fe3 C36 68.9(3) . .
C37 Fe3 C36 40.6(3) . .
C32 Fe3 C35 151.8(3) . .
C29 Fe3 C35 130.4(3) . .
C34 Fe3 C35 40.1(3) . .
C33 Fe3 C35 168.0(3) . .
C38 Fe3 C35 68.4(3) . .
C37 Fe3 C35 68.1(3) . .
C36 Fe3 C35 40.8(3) . .
C32 Fe3 C30 68.8(3) . .
C29 Fe3 C30 41.3(3) . .
C34 Fe3 C30 120.1(3) . .
C33 Fe3 C30 69.7(3) . .
C38 Fe3 C30 152.8(3) . .
C37 Fe3 C30 166.0(3) . .
C36 Fe3 C30 128.9(3) . .
C35 Fe3 C30 110.0(3) . .
C32 Fe3 C31 40.3(3) . .
C29 Fe3 C31 68.3(3) . .
C34 Fe3 C31 153.8(3) . .
C33 Fe3 C31 68.1(3) . .
C38 Fe3 C31 164.3(3) . .
C37 Fe3 C31 127.1(3) . .
C36 Fe3 C31 108.0(3) . .
C35 Fe3 C31 120.0(3) . .
C30 Fe3 C31 40.8(3) . .
C45 Fe4 C44 40.9(4) . .
C45 Fe4 C43 156.0(4) . .
C44 Fe4 C43 119.5(4) . .
C45 Fe4 C40 107.1(4) . .
C44 Fe4 C40 122.0(4) . .
C43 Fe4 C40 69.4(3) . .
C45 Fe4 C46 40.7(4) . .
C44 Fe4 C46 68.3(4) . .
C43 Fe4 C46 160.5(4) . .
C40 Fe4 C46 123.5(4) . .
C45 Fe4 C41 125.3(4) . .
C44 Fe4 C41 160.1(4) . .
C43 Fe4 C41 68.4(3) . .
C40 Fe4 C41 40.7(3) . .
C46 Fe4 C41 110.7(4) . .
C45 Fe4 C39 119.9(4) . .
C44 Fe4 C39 103.9(4) . .
C43 Fe4 C39 41.8(3) . .
C40 Fe4 C39 41.5(3) . .
C46 Fe4 C39 157.5(4) . .
C41 Fe4 C39 69.1(3) . .
C45 Fe4 C42 162.2(4) . .
C44 Fe4 C42 156.0(4) . .
C43 Fe4 C42 40.5(3) . .
C40 Fe4 C42 69.2(4) . .
C46 Fe4 C42 125.9(4) . .
C41 Fe4 C42 40.8(3) . .
C39 Fe4 C42 69.6(4) . .
C45 Fe4 C47 68.3(5) . .
C44 Fe4 C47 67.9(4) . .
C43 Fe4 C47 122.9(4) . .
C40 Fe4 C47 160.2(4) . .
C46 Fe4 C47 40.5(4) . .
C41 Fe4 C47 125.2(4) . .
C39 Fe4 C47 157.9(4) . .
C42 Fe4 C47 109.0(4) . .
C45 Fe4 C48 68.6(4) . .
C44 Fe4 C48 40.3(4) . .
C43 Fe4 C48 105.1(4) . .
C40 Fe4 C48 157.4(4) . .
C46 Fe4 C48 68.6(4) . .
C41 Fe4 C48 159.3(4) . .
C39 Fe4 C48 119.9(4) . .
C42 Fe4 C48 121.6(4) . .
C47 Fe4 C48 40.7(4) . .
C60 Fe5 C57 68.6(3) . .
C60 Fe5 C62 162.8(3) . .
C57 Fe5 C62 109.0(3) . .
C60 Fe5 C61 40.3(3) . .
C57 Fe5 C61 41.6(3) . .
C62 Fe5 C61 126.7(3) . .
C60 Fe5 C64 118.3(3) . .
C57 Fe5 C64 164.8(3) . .
C62 Fe5 C64 68.5(3) . .
C61 Fe5 C64 151.9(3) . .
C60 Fe5 C66 124.7(3) . .
C57 Fe5 C66 119.5(3) . .
C62 Fe5 C66 40.4(3) . .
C61 Fe5 C66 106.3(3) . .
C64 Fe5 C66 69.0(3) . .
C60 Fe5 C58 69.2(3) . .
C57 Fe5 C58 41.1(3) . .
C62 Fe5 C58 121.0(3) . .
C61 Fe5 C58 69.8(3) . .
C64 Fe5 C58 126.2(3) . .
C66 Fe5 C58 154.8(3) . .
C60 Fe5 C63 154.6(3) . .
C57 Fe5 C63 127.7(3) . .
C62 Fe5 C63 39.9(3) . .
C61 Fe5 C63 164.7(3) . .
C64 Fe5 C63 41.0(3) . .
C66 Fe5 C63 67.9(3) . .
C58 Fe5 C63 109.1(3) . .
C60 Fe5 C65 105.9(3) . .
C57 Fe5 C65 153.7(3) . .
C62 Fe5 C65 68.3(3) . .
C61 Fe5 C65 117.5(3) . .
C64 Fe5 C65 40.7(3) . .
C66 Fe5 C65 41.2(3) . .
C58 Fe5 C65 163.1(3) . .
C63 Fe5 C65 68.1(3) . .
C60 Fe5 C59 40.3(3) . .
C57 Fe5 C59 68.5(3) . .
C62 Fe5 C59 156.1(3) . .
C61 Fe5 C59 68.2(3) . .
C64 Fe5 C59 107.4(3) . .
C66 Fe5 C59 162.2(3) . .
C58 Fe5 C59 41.2(3) . .
C63 Fe5 C59 121.6(3) . .
C65 Fe5 C59 124.9(3) . .
C73 Fe6 C75 68.4(4) . .
C73 Fe6 C71 156.2(4) . .
C75 Fe6 C71 123.3(4) . .
C73 Fe6 C76 68.1(4) . .
C75 Fe6 C76 40.6(4) . .
C71 Fe6 C76 106.2(4) . .
C73 Fe6 C72 40.4(4) . .
C75 Fe6 C72 68.8(4) . .
C71 Fe6 C72 120.2(4) . .
C76 Fe6 C72 40.9(4) . .
C73 Fe6 C74 41.4(4) . .
C75 Fe6 C74 40.4(4) . .
C71 Fe6 C74 160.1(4) . .
C76 Fe6 C74 68.5(4) . .
C72 Fe6 C74 69.2(4) . .
C73 Fe6 C69 125.4(4) . .
C75 Fe6 C69 123.1(4) . .
C71 Fe6 C69 68.5(4) . .
C76 Fe6 C69 157.9(4) . .
C72 Fe6 C69 160.6(4) . .
C74 Fe6 C69 108.8(4) . .
C73 Fe6 C68 107.3(4) . .
C75 Fe6 C68 158.5(4) . .
C71 Fe6 C68 69.4(3) . .
C76 Fe6 C68 159.3(3) . .
C72 Fe6 C68 122.5(4) . .
C74 Fe6 C68 122.4(4) . .
C69 Fe6 C68 41.0(3) . .
C73 Fe6 C70 161.8(4) . .
C75 Fe6 C70 108.4(4) . .
C71 Fe6 C70 40.8(3) . .
C76 Fe6 C70 122.0(4) . .
C72 Fe6 C70 156.9(4) . .
C74 Fe6 C70 124.5(4) . .
C69 Fe6 C70 40.1(4) . .
C68 Fe6 C70 68.7(3) . .
C73 Fe6 C67 120.7(4) . .
C75 Fe6 C67 159.5(4) . .
C71 Fe6 C67 41.3(3) . .
C76 Fe6 C67 122.4(3) . .
C72 Fe6 C67 105.5(3) . .
C74 Fe6 C67 157.8(4) . .
C69 Fe6 C67 68.7(3) . .
C68 Fe6 C67 41.1(3) . .
C70 Fe6 C67 68.8(3) . .
Cl1 Pd1 P2 87.18(7) . .
Cl1 Pd1 P1 92.28(7) . .
P2 Pd1 P1 178.13(8) . .
Cl1 Pd1 Cl2 178.52(8) . .
P2 Pd1 Cl2 92.53(7) . .
P1 Pd1 Cl2 88.05(7) . .
Cl3 Pd2 Cl3 180.00(7) 2 .
Cl3 Pd2 P3 87.70(7) 2 2
Cl3 Pd2 P3 92.30(7) . 2
Cl3 Pd2 P3 92.30(7) 2 .
Cl3 Pd2 P3 87.70(7) . .
P3 Pd2 P3 180.0 2 .
C1 P1 C25 103.5(4) . .
C1 P1 C21 105.8(4) . .
C25 P1 C21 100.5(4) . .
C1 P1 Pd1 116.5(3) . .
C25 P1 Pd1 111.1(3) . .
C21 P1 Pd1 117.4(3) . .
C53 P2 C49 101.1(4) . .
C53 P2 C29 104.2(4) . .
C49 P2 C29 104.4(4) . .
C53 P2 Pd1 116.9(3) . .
C49 P2 Pd1 111.5(3) . .
C29 P2 Pd1 116.9(3) . .
C57 P3 C77 104.4(4) . .
C57 P3 C81 104.8(3) . .
C77 P3 C81 101.4(3) . .
C57 P3 Pd2 117.8(3) . .
C77 P3 Pd2 110.0(2) . .
C81 P3 Pd2 116.6(2) . .
C86 Cl8 C86 70.1(13) 2_566 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
C1 C5 1.439(11) .
C1 C2 1.449(10) .
C1 P1 1.787(8) .
C1 Fe1 2.036(8) .
C2 C3 1.400(11) .
C2 Fe1 2.037(8) .
C2 H2 0.9300 .
C3 C4 1.403(12) .
C3 Fe1 2.035(8) .
C3 H3 0.9300 .
C4 C5 1.437(11) .
C4 Fe1 2.048(8) .
C4 H4 0.9300 .
C5 Fe1 2.054(8) .
C5 H5 0.9300 .
C6 C10 1.407(14) .
C6 C7 1.435(12) .
C6 Fe1 2.049(9) .
C6 H6 0.9300 .
C7 C8 1.434(12) .
C7 Fe1 2.052(9) .
C7 H7 0.9300 .
C8 C9 1.410(11) .
C8 C11 1.467(11) .
C8 Fe1 2.046(8) .
C9 C10 1.431(12) .
C9 Fe1 2.040(8) .
C9 H9 0.9300 .
C10 Fe1 2.046(9) .
C10 H10 0.9300 .
C11 C15 1.412(12) .
C11 C12 1.427(11) .
C11 Fe2 2.057(8) .
C12 C13 1.407(12) .
C12 Fe2 2.032(8) .
C12 H12 0.9300 .
C13 C14 1.412(13) .
C13 Fe2 2.035(9) .
C13 H13 0.9300 .
C14 C15 1.417(14) .
C14 Fe2 2.049(10) .
C14 H14 0.9300 .
C15 Fe2 2.034(9) .
C15 H15 0.9300 .
C16 C20 1.412(14) .
C16 C17 1.415(13) .
C16 Fe2 2.048(10) .
C16 H16 0.9300 .
C17 C18 1.424(12) .
C17 Fe2 2.054(9) .
C17 H17 0.9300 .
C18 C19 1.409(12) .
C18 Fe2 2.041(8) .
C18 H18 0.9300 .
C19 C20 1.425(12) .
C19 Fe2 2.052(9) .
C19 H19 0.9300 .
C20 Fe2 2.050(9) .
C20 H20 0.9300 .
C21 C22 1.341(12) .
C21 O1 1.372(10) .
C21 P1 1.800(8) .
C22 C23 1.428(13) .
C22 H22 0.9300 .
C23 C24 1.336(14) .
C23 H23 0.9300 .
C24 O1 1.366(10) .
C24 H24 0.9300 .
C25 C26 1.363(11) .
C25 O2 1.372(9) .
C25 P1 1.791(8) .
C26 C27 1.415(12) .
C26 H26 0.9300 .
C27 C28 1.346(14) .
C27 H27 0.9300 .
C28 O2 1.371(11) .
C28 H28 0.9300 .
C29 C30 1.443(11) .
C29 C33 1.451(10) .
C29 P2 1.810(8) .
C29 Fe3 2.033(8) .
C30 C31 1.438(11) .
C30 Fe3 2.063(8) .
C30 H30 0.9300 .
C31 C32 1.411(11) .
C31 Fe3 2.064(8) .
C31 H31 0.9300 .
C32 C33 1.398(11) .
C32 Fe3 2.032(8) .
C32 H32 0.9300 .
C33 Fe3 2.051(8) .
C33 H33 0.9300 .
C34 C35 1.410(12) .
C34 C38 1.430(12) .
C34 Fe3 2.050(8) .
C34 H34 0.9300 .
C35 C36 1.436(11) .
C35 Fe3 2.059(8) .
C35 H35 0.9300 .
C36 C37 1.428(11) .
C36 Fe3 2.057(8) .
C36 H36 0.9300 .
C37 C38 1.429(11) .
C37 C39 1.461(11) .
C37 Fe3 2.055(7) .
C38 Fe3 2.051(8) .
C38 H38 0.9300 .
C39 C40 1.443(11) .
C39 C43 1.450(12) .
C39 Fe4 2.043(8) .
C40 C41 1.419(12) .
C40 Fe4 2.033(8) .
C40 H40 0.9300 .
C41 C42 1.426(12) .
C41 Fe4 2.043(8) .
C41 H41 0.9300 .
C42 C43 1.409(12) .
C42 Fe4 2.043(9) .
C42 H42 0.9300 .
C43 Fe4 2.024(8) .
C43 H43 0.9300 .
C44 C48 1.404(14) .
C44 C45 1.411(14) .
C44 Fe4 2.023(9) .
C44 H44 0.9300 .
C45 C46 1.407(14) .
C45 Fe4 2.016(10) .
C45 H45 0.9300 .
C46 C47 1.415(15) .
C46 Fe4 2.034(9) .
C46 H46 0.9300 .
C47 C48 1.426(13) .
C47 Fe4 2.049(9) .
C47 H47 0.9300 .
C48 Fe4 2.050(9) .
C48 H48 0.9300 .
C49 O3 1.347(10) .
C49 C50 1.361(12) .
C49 P2 1.804(8) .
C50 C51 1.418(13) .
C50 H50 0.9300 .
C51 C52 1.330(15) .
C51 H51 0.9300 .
C52 O3 1.364(11) .
C52 H52 0.9300 .
C53 C54 1.350(11) .
C53 O4 1.365(9) .
C53 P2 1.797(8) .
C54 C55 1.422(11) .
C54 H54 0.9300 .
C55 C56 1.342(12) .
C55 H55 0.9300 .
C56 O4 1.370(9) .
C56 H56 0.9300 .
C57 C58 1.437(11) .
C57 C61 1.453(10) .
C57 P3 1.790(8) .
C57 Fe5 2.040(7) .
C58 C59 1.448(11) .
C58 Fe5 2.052(8) .
C58 H58 0.9300 .
C59 C60 1.414(11) .
C59 Fe5 2.063(8) .
C59 H59 0.9300 .
C60 C61 1.406(11) .
C60 Fe5 2.037(8) .
C60 H60 0.9300 .
C61 Fe5 2.049(7) .
C61 H61 0.9300 .
C62 C63 1.401(12) .
C62 C66 1.414(11) .
C62 Fe5 2.044(8) .
C62 H62 0.9300 .
C63 C64 1.438(11) .
C63 Fe5 2.058(8) .
C63 H63 0.9300 .
C64 C65 1.428(11) .
C64 Fe5 2.050(7) .
C64 H64 0.9300 .
C65 C66 1.445(10) .
C65 C67 1.452(11) .
C65 Fe5 2.059(7) .
C66 Fe5 2.051(8) .
C66 H66 0.9300 .
C67 C68 1.438(11) .
C67 C71 1.442(12) .
C67 Fe6 2.058(8) .
C68 C69 1.432(12) .
C68 Fe6 2.042(8) .
C68 H68 0.9300 .
C69 C70 1.404(13) .
C69 Fe6 2.041(10) .
C69 H69 0.9300 .
C70 C71 1.424(11) .
C70 Fe6 2.052(9) .
C70 H70 0.9300 .
C71 Fe6 2.029(8) .
C71 H71 0.9300 .
C72 C73 1.402(14) .
C72 C76 1.420(13) .
C72 Fe6 2.033(10) .
C72 H72 0.9300 .
C73 C74 1.438(14) .
C73 Fe6 2.025(10) .
C73 H73 0.9300 .
C74 C75 1.404(13) .
C74 Fe6 2.038(8) .
C74 H74 0.9300 .
C75 C76 1.407(13) .
C75 Fe6 2.026(9) .
C75 H75 0.9300 .
C76 Fe6 2.031(10) .
C76 H76 0.9300 .
C77 C78 1.357(11) .
C77 O5 1.367(9) .
C77 P3 1.791(8) .
C78 C79 1.421(12) .
C78 H78 0.9300 .
C79 C80 1.348(14) .
C79 H79 0.9300 .
C80 O5 1.358(10) .
C80 H80 0.9300 .
C81 C82 1.342(11) .
C81 O6 1.371(9) .
C81 P3 1.804(8) .
C82 C83 1.407(12) .
C82 H82 0.9300 .
C83 C84 1.340(12) .
C83 H83 0.9300 .
C84 O6 1.356(9) .
C84 H84 0.9300 .
C85 Cl6 1.725(15) .
C85 Cl4 1.740(14) .
C85 Cl5 1.742(16) .
C85 H85 0.9800 .
C86 Cl8 1.68(3) 2_566
C86 Cl8 1.81(3) .
C86 Cl7 1.82(2) .
C86 H86 0.9800 .
Pd1 Cl1 2.295(2) .
Pd1 P2 2.303(2) .
Pd1 P1 2.309(2) .
Pd1 Cl2 2.3099(19) .
Pd2 Cl3 2.3041(18) 2
Pd2 Cl3 2.3041(18) .
Pd2 P3 2.3102(19) 2
Pd2 P3 2.3102(19) .
Cl8 C86 1.68(3) 2_566
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C5 C1 C2 C3 -0.3(9) . .
P1 C1 C2 C3 -176.6(6) . .
Fe1 C1 C2 C3 -59.7(5) . .
C5 C1 C2 Fe1 59.4(5) . .
P1 C1 C2 Fe1 -116.9(6) . .
C1 C2 C3 C4 -0.2(9) . .
Fe1 C2 C3 C4 -59.5(6) . .
C1 C2 C3 Fe1 59.2(5) . .
C2 C3 C4 C5 0.7(10) . .
Fe1 C3 C4 C5 -58.5(6) . .
C2 C3 C4 Fe1 59.2(6) . .
C3 C4 C5 C1 -0.9(9) . .
Fe1 C4 C5 C1 -59.2(5) . .
C3 C4 C5 Fe1 58.3(6) . .
C2 C1 C5 C4 0.7(9) . .
P1 C1 C5 C4 177.0(6) . .
Fe1 C1 C5 C4 59.6(5) . .
C2 C1 C5 Fe1 -58.9(5) . .
P1 C1 C5 Fe1 117.5(6) . .
C10 C6 C7 C8 0.5(9) . .
Fe1 C6 C7 C8 59.5(6) . .
C10 C6 C7 Fe1 -59.1(6) . .
C6 C7 C8 C9 -0.8(9) . .
Fe1 C7 C8 C9 58.9(6) . .
C6 C7 C8 C11 -178.5(8) . .
Fe1 C7 C8 C11 -118.9(8) . .
C6 C7 C8 Fe1 -59.6(6) . .
C7 C8 C9 C10 0.8(9) . .
C11 C8 C9 C10 178.5(8) . .
Fe1 C8 C9 C10 59.7(5) . .
C7 C8 C9 Fe1 -58.9(6) . .
C11 C8 C9 Fe1 118.8(8) . .
C7 C6 C10 C9 0.0(9) . .
Fe1 C6 C10 C9 -59.0(6) . .
C7 C6 C10 Fe1 59.0(6) . .
C8 C9 C10 C6 -0.5(9) . .
Fe1 C9 C10 C6 59.4(6) . .
C8 C9 C10 Fe1 -59.9(6) . .
C9 C8 C11 C15 -11.3(14) . .
C7 C8 C11 C15 166.1(8) . .
Fe1 C8 C11 C15 77.4(10) . .
C9 C8 C11 C12 164.8(8) . .
C7 C8 C11 C12 -17.8(13) . .
Fe1 C8 C11 C12 -106.5(9) . .
C9 C8 C11 Fe2 77.3(10) . .
C7 C8 C11 Fe2 -105.3(9) . .
Fe1 C8 C11 Fe2 166.0(4) . .
C15 C11 C12 C13 -0.8(9) . .
C8 C11 C12 C13 -177.6(8) . .
Fe2 C11 C12 C13 -59.6(6) . .
C15 C11 C12 Fe2 58.8(6) . .
C8 C11 C12 Fe2 -117.9(8) . .
C11 C12 C13 C14 0.1(10) . .
Fe2 C12 C13 C14 -59.9(7) . .
C11 C12 C13 Fe2 60.1(6) . .
C12 C13 C14 C15 0.6(11) . .
Fe2 C13 C14 C15 -58.9(7) . .
C12 C13 C14 Fe2 59.5(6) . .
C12 C11 C15 C14 1.2(10) . .
C8 C11 C15 C14 177.9(8) . .
Fe2 C11 C15 C14 59.8(7) . .
C12 C11 C15 Fe2 -58.6(6) . .
C8 C11 C15 Fe2 118.1(9) . .
C13 C14 C15 C11 -1.1(11) . .
Fe2 C14 C15 C11 -60.1(6) . .
C13 C14 C15 Fe2 59.0(7) . .
C20 C16 C17 C18 -0.8(10) . .
Fe2 C16 C17 C18 58.9(6) . .
C20 C16 C17 Fe2 -59.7(7) . .
C16 C17 C18 C19 1.0(10) . .
Fe2 C17 C18 C19 60.1(6) . .
C16 C17 C18 Fe2 -59.2(6) . .
C17 C18 C19 C20 -0.8(10) . .
Fe2 C18 C19 C20 59.3(6) . .
C17 C18 C19 Fe2 -60.1(6) . .
C17 C16 C20 C19 0.3(11) . .
Fe2 C16 C20 C19 -59.5(7) . .
C17 C16 C20 Fe2 59.8(6) . .
C18 C19 C20 C16 0.3(11) . .
Fe2 C19 C20 C16 59.5(6) . .
C18 C19 C20 Fe2 -59.2(6) . .
O1 C21 C22 C23 -0.7(10) . .
P1 C21 C22 C23 -176.5(7) . .
C21 C22 C23 C24 1.3(11) . .
C22 C23 C24 O1 -1.4(11) . .
O2 C25 C26 C27 -0.4(9) . .
P1 C25 C26 C27 -176.2(7) . .
C25 C26 C27 C28 0.2(10) . .
C26 C27 C28 O2 0.1(11) . .
C33 C29 C30 C31 -0.1(9) . .
P2 C29 C30 C31 -177.9(6) . .
Fe3 C29 C30 C31 -59.7(5) . .
C33 C29 C30 Fe3 59.7(5) . .
P2 C29 C30 Fe3 -118.2(6) . .
C29 C30 C31 C32 1.1(9) . .
Fe3 C30 C31 C32 -57.7(6) . .
C29 C30 C31 Fe3 58.8(5) . .
C30 C31 C32 C33 -1.8(9) . .
Fe3 C31 C32 C33 -60.1(6) . .
C30 C31 C32 Fe3 58.2(6) . .
C31 C32 C33 C29 1.8(9) . .
Fe3 C32 C33 C29 -58.6(5) . .
C31 C32 C33 Fe3 60.3(6) . .
C30 C29 C33 C32 -1.0(9) . .
P2 C29 C33 C32 176.8(6) . .
Fe3 C29 C33 C32 59.0(5) . .
C30 C29 C33 Fe3 -60.1(5) . .
P2 C29 C33 Fe3 117.8(6) . .
C38 C34 C35 C36 -0.2(9) . .
Fe3 C34 C35 C36 58.9(5) . .
C38 C34 C35 Fe3 -59.1(6) . .
C34 C35 C36 C37 0.9(9) . .
Fe3 C35 C36 C37 59.8(5) . .
C34 C35 C36 Fe3 -59.0(6) . .
C35 C36 C37 C38 -1.2(9) . .
Fe3 C36 C37 C38 58.6(5) . .
C35 C36 C37 C39 -179.2(7) . .
Fe3 C36 C37 C39 -119.3(8) . .
C35 C36 C37 Fe3 -59.9(5) . .
C36 C37 C38 C34 1.1(9) . .
C39 C37 C38 C34 179.1(7) . .
Fe3 C37 C38 C34 59.9(5) . .
C36 C37 C38 Fe3 -58.8(5) . .
C39 C37 C38 Fe3 119.2(8) . .
C35 C34 C38 C37 -0.6(9) . .
Fe3 C34 C38 C37 -60.1(5) . .
C35 C34 C38 Fe3 59.5(6) . .
C36 C37 C39 C40 -9.1(13) . .
C38 C37 C39 C40 173.2(8) . .
Fe3 C37 C39 C40 -99.1(9) . .
C36 C37 C39 C43 175.7(8) . .
C38 C37 C39 C43 -1.9(13) . .
Fe3 C37 C39 C43 85.7(10) . .
C36 C37 C39 Fe4 -97.4(9) . .
C38 C37 C39 Fe4 84.9(9) . .
Fe3 C37 C39 Fe4 172.6(4) . .
C43 C39 C40 C41 -1.1(9) . .
C37 C39 C40 C41 -177.0(8) . .
Fe4 C39 C40 C41 -59.7(6) . .
C43 C39 C40 Fe4 58.6(5) . .
C37 C39 C40 Fe4 -117.4(8) . .
C39 C40 C41 C42 1.1(10) . .
Fe4 C40 C41 C42 -58.3(6) . .
C39 C40 C41 Fe4 59.4(6) . .
C40 C41 C42 C43 -0.7(10) . .
Fe4 C41 C42 C43 -58.8(6) . .
C40 C41 C42 Fe4 58.1(6) . .
C41 C42 C43 C39 0.0(10) . .
Fe4 C42 C43 C39 -59.1(6) . .
C41 C42 C43 Fe4 59.2(6) . .
C40 C39 C43 C42 0.6(9) . .
C37 C39 C43 C42 176.7(8) . .
Fe4 C39 C43 C42 59.5(6) . .
C40 C39 C43 Fe4 -58.9(5) . .
C37 C39 C43 Fe4 117.1(8) . .
C48 C44 C45 C46 0.5(11) . .
Fe4 C44 C45 C46 60.4(7) . .
C48 C44 C45 Fe4 -59.9(7) . .
C44 C45 C46 C47 -0.3(11) . .
Fe4 C45 C46 C47 59.7(7) . .
C44 C45 C46 Fe4 -60.0(7) . .
C45 C46 C47 C48 0.0(12) . .
Fe4 C46 C47 C48 58.9(7) . .
C45 C46 C47 Fe4 -58.9(7) . .
C45 C44 C48 C47 -0.5(11) . .
Fe4 C44 C48 C47 -59.4(7) . .
C45 C44 C48 Fe4 58.9(7) . .
C46 C47 C48 C44 0.3(11) . .
Fe4 C47 C48 C44 58.9(7) . .
C46 C47 C48 Fe4 -58.6(7) . .
O3 C49 C50 C51 0.3(9) . .
P2 C49 C50 C51 179.1(7) . .
C49 C50 C51 C52 -0.1(10) . .
C50 C51 C52 O3 0.0(11) . .
O4 C53 C54 C55 0.7(9) . .
P2 C53 C54 C55 174.7(7) . .
C53 C54 C55 C56 0.8(9) . .
C54 C55 C56 O4 -2.0(10) . .
C61 C57 C58 C59 -1.3(8) . .
P3 C57 C58 C59 -177.8(6) . .
Fe5 C57 C58 C59 -60.2(5) . .
C61 C57 C58 Fe5 58.9(5) . .
P3 C57 C58 Fe5 -117.6(6) . .
C57 C58 C59 C60 2.0(9) . .
Fe5 C58 C59 C60 -57.6(5) . .
C57 C58 C59 Fe5 59.6(5) . .
C58 C59 C60 C61 -2.1(9) . .
Fe5 C59 C60 C61 -59.8(5) . .
C58 C59 C60 Fe5 57.7(5) . .
C59 C60 C61 C57 1.3(9) . .
Fe5 C60 C61 C57 -58.8(5) . .
C59 C60 C61 Fe5 60.1(6) . .
C58 C57 C61 C60 0.0(8) . .
P3 C57 C61 C60 176.6(6) . .
Fe5 C57 C61 C60 59.2(5) . .
C58 C57 C61 Fe5 -59.1(5) . .
P3 C57 C61 Fe5 117.4(6) . .
C66 C62 C63 C64 -1.4(9) . .
Fe5 C62 C63 C64 58.3(5) . .
C66 C62 C63 Fe5 -59.7(5) . .
C62 C63 C64 C65 1.9(9) . .
Fe5 C63 C64 C65 60.4(5) . .
C62 C63 C64 Fe5 -58.5(5) . .
C63 C64 C65 C66 -1.8(8) . .
Fe5 C64 C65 C66 58.5(5) . .
C63 C64 C65 C67 -177.6(7) . .
Fe5 C64 C65 C67 -117.4(8) . .
C63 C64 C65 Fe5 -60.3(5) . .
C63 C62 C66 C65 0.2(9) . .
Fe5 C62 C66 C65 -59.7(5) . .
C63 C62 C66 Fe5 60.0(5) . .
C64 C65 C66 C62 1.0(8) . .
C67 C65 C66 C62 177.0(7) . .
Fe5 C65 C66 C62 59.6(5) . .
C64 C65 C66 Fe5 -58.6(5) . .
C67 C65 C66 Fe5 117.4(8) . .
C64 C65 C67 C68 -9.6(14) . .
C66 C65 C67 C68 175.2(8) . .
Fe5 C65 C67 C68 -98.2(9) . .
C64 C65 C67 C71 170.9(8) . .
C66 C65 C67 C71 -4.3(13) . .
Fe5 C65 C67 C71 82.2(10) . .
C64 C65 C67 Fe6 -100.3(9) . .
C66 C65 C67 Fe6 84.5(9) . .
Fe5 C65 C67 Fe6 171.0(4) . .
C71 C67 C68 C69 -1.9(10) . .
C65 C67 C68 C69 178.5(8) . .
Fe6 C67 C68 C69 -59.7(6) . .
C71 C67 C68 Fe6 57.7(6) . .
C65 C67 C68 Fe6 -121.9(8) . .
C67 C68 C69 C70 0.7(10) . .
Fe6 C68 C69 C70 -59.4(6) . .
C67 C68 C69 Fe6 60.1(6) . .
C68 C69 C70 C71 0.8(10) . .
Fe6 C69 C70 C71 -58.0(6) . .
C68 C69 C70 Fe6 58.9(7) . .
C69 C70 C71 C67 -2.1(10) . .
Fe6 C70 C71 C67 -60.6(6) . .
C69 C70 C71 Fe6 58.5(6) . .
C68 C67 C71 C70 2.5(10) . .
C65 C67 C71 C70 -177.9(8) . .
Fe6 C67 C71 C70 60.6(6) . .
C68 C67 C71 Fe6 -58.1(6) . .
C65 C67 C71 Fe6 121.5(8) . .
C76 C72 C73 C74 -0.4(11) . .
Fe6 C72 C73 C74 59.1(7) . .
C76 C72 C73 Fe6 -59.5(6) . .
C72 C73 C74 C75 0.0(11) . .
Fe6 C73 C74 C75 59.4(7) . .
C72 C73 C74 Fe6 -59.3(7) . .
C73 C74 C75 C76 0.3(11) . .
Fe6 C74 C75 C76 59.3(7) . .
C73 C74 C75 Fe6 -59.0(7) . .
C74 C75 C76 C72 -0.6(11) . .
Fe6 C75 C76 C72 59.0(7) . .
C74 C75 C76 Fe6 -59.5(7) . .
C73 C72 C76 C75 0.6(11) . .
Fe6 C72 C76 C75 -58.9(7) . .
C73 C72 C76 Fe6 59.5(7) . .
O5 C77 C78 C79 -0.4(9) . .
P3 C77 C78 C79 174.5(6) . .
C77 C78 C79 C80 0.9(10) . .
C78 C79 C80 O5 -1.0(11) . .
O6 C81 C82 C83 0.6(9) . .
P3 C81 C82 C83 175.0(6) . .
C81 C82 C83 C84 -0.3(9) . .
C82 C83 C84 O6 -0.1(9) . .
C23 C24 O1 C21 1.1(10) . .
C22 C21 O1 C24 -0.2(9) . .
P1 C21 O1 C24 176.2(6) . .
C27 C28 O2 C25 -0.4(10) . .
C26 C25 O2 C28 0.5(9) . .
P1 C25 O2 C28 177.0(6) . .
C50 C49 O3 C52 -0.3(10) . .
P2 C49 O3 C52 -179.3(6) . .
C51 C52 O3 C49 0.2(10) . .
C54 C53 O4 C56 -1.8(8) . .
P2 C53 O4 C56 -176.8(5) . .
C55 C56 O4 C53 2.4(9) . .
C79 C80 O5 C77 0.8(10) . .
C78 C77 O5 C80 -0.2(9) . .
P3 C77 O5 C80 -176.0(6) . .
C83 C84 O6 C81 0.4(9) . .
C82 C81 O6 C84 -0.6(8) . .
P3 C81 O6 C84 -175.9(5) . .
C2 C3 Fe1 C1 -38.9(5) . .
C4 C3 Fe1 C1 81.5(5) . .
C4 C3 Fe1 C2 120.4(7) . .
C2 C3 Fe1 C9 159.7(5) . .
C4 C3 Fe1 C9 -79.9(5) . .
C2 C3 Fe1 C10 -171.8(8) . .
C4 C3 Fe1 C10 -51.4(11) . .
C2 C3 Fe1 C8 118.9(5) . .
C4 C3 Fe1 C8 -120.7(5) . .
C2 C3 Fe1 C4 -120.4(7) . .
C2 C3 Fe1 C6 49.3(11) . .
C4 C3 Fe1 C6 169.7(8) . .
C2 C3 Fe1 C7 77.4(6) . .
C4 C3 Fe1 C7 -162.2(5) . .
C2 C3 Fe1 C5 -83.2(5) . .
C4 C3 Fe1 C5 37.2(5) . .
C5 C1 Fe1 C3 -82.0(5) . .
C2 C1 Fe1 C3 37.5(5) . .
P1 C1 Fe1 C3 157.8(6) . .
C5 C1 Fe1 C2 -119.6(7) . .
P1 C1 Fe1 C2 120.3(7) . .
C5 C1 Fe1 C9 41.6(12) . .
C2 C1 Fe1 C9 161.1(10) . .
P1 C1 Fe1 C9 -78.6(12) . .
C5 C1 Fe1 C10 78.8(6) . .
C2 C1 Fe1 C10 -161.6(5) . .
P1 C1 Fe1 C10 -41.3(7) . .
C5 C1 Fe1 C8 -159.5(8) . .
C2 C1 Fe1 C8 -40.0(11) . .
P1 C1 Fe1 C8 80.3(10) . .
C5 C1 Fe1 C4 -38.7(5) . .
C2 C1 Fe1 C4 80.9(5) . .
P1 C1 Fe1 C4 -158.8(6) . .
C5 C1 Fe1 C6 120.8(5) . .
C2 C1 Fe1 C6 -119.6(5) . .
P1 C1 Fe1 C6 0.7(6) . .
C5 C1 Fe1 C7 164.2(5) . .
C2 C1 Fe1 C7 -76.3(5) . .
P1 C1 Fe1 C7 44.1(6) . .
C2 C1 Fe1 C5 119.6(7) . .
P1 C1 Fe1 C5 -120.1(7) . .
C1 C2 Fe1 C3 -118.5(7) . .
C3 C2 Fe1 C1 118.5(7) . .
C3 C2 Fe1 C9 -46.5(10) . .
C1 C2 Fe1 C9 -165.0(8) . .
C3 C2 Fe1 C10 170.8(10) . .
C1 C2 Fe1 C10 52.2(12) . .
C3 C2 Fe1 C8 -77.6(5) . .
C1 C2 Fe1 C8 163.9(5) . .
C3 C2 Fe1 C4 36.9(5) . .
C1 C2 Fe1 C4 -81.7(5) . .
C3 C2 Fe1 C6 -160.5(5) . .
C1 C2 Fe1 C6 81.0(5) . .
C3 C2 Fe1 C7 -119.5(5) . .
C1 C2 Fe1 C7 121.9(5) . .
C3 C2 Fe1 C5 80.9(5) . .
C1 C2 Fe1 C5 -37.6(4) . .
C8 C9 Fe1 C3 -76.7(6) . .
C10 C9 Fe1 C3 164.5(5) . .
C8 C9 Fe1 C1 168.0(9) . .
C10 C9 Fe1 C1 49.2(12) . .
C8 C9 Fe1 C2 -43.6(10) . .
C10 C9 Fe1 C2 -162.4(8) . .
C8 C9 Fe1 C10 118.8(7) . .
C10 C9 Fe1 C8 -118.8(7) . .
C8 C9 Fe1 C4 -118.3(5) . .
C10 C9 Fe1 C4 122.8(6) . .
C8 C9 Fe1 C6 81.6(5) . .
C10 C9 Fe1 C6 -37.2(5) . .
C8 C9 Fe1 C7 37.5(5) . .
C10 C9 Fe1 C7 -81.4(6) . .
C8 C9 Fe1 C5 -160.5(5) . .
C10 C9 Fe1 C5 80.7(6) . .
C6 C10 Fe1 C3 -158.1(8) . .
C9 C10 Fe1 C3 -38.7(11) . .
C6 C10 Fe1 C1 78.2(6) . .
C9 C10 Fe1 C1 -162.4(5) . .
C6 C10 Fe1 C2 38.3(12) . .
C9 C10 Fe1 C2 157.8(9) . .
C6 C10 Fe1 C9 -119.4(7) . .
C6 C10 Fe1 C8 -81.8(5) . .
C9 C10 Fe1 C8 37.6(5) . .
C6 C10 Fe1 C4 164.3(5) . .
C9 C10 Fe1 C4 -76.2(6) . .
C9 C10 Fe1 C6 119.4(7) . .
C6 C10 Fe1 C7 -37.6(5) . .
C9 C10 Fe1 C7 81.8(5) . .
C6 C10 Fe1 C5 121.3(5) . .
C9 C10 Fe1 C5 -119.3(5) . .
C9 C8 Fe1 C3 120.1(5) . .
C7 C8 Fe1 C3 -119.8(5) . .
C11 C8 Fe1 C3 0.0(7) . .
C9 C8 Fe1 C1 -169.5(8) . .
C7 C8 Fe1 C1 -49.4(11) . .
C11 C8 Fe1 C1 70.4(11) . .
C9 C8 Fe1 C2 160.9(5) . .
C7 C8 Fe1 C2 -79.0(6) . .
C11 C8 Fe1 C2 40.8(8) . .
C7 C8 Fe1 C9 120.1(7) . .
C11 C8 Fe1 C9 -120.1(9) . .
C9 C8 Fe1 C10 -38.2(5) . .
C7 C8 Fe1 C10 81.9(6) . .
C11 C8 Fe1 C10 -158.3(8) . .
C9 C8 Fe1 C4 79.6(6) . .
C7 C8 Fe1 C4 -160.3(5) . .
C11 C8 Fe1 C4 -40.5(8) . .
C9 C8 Fe1 C6 -81.6(6) . .
C7 C8 Fe1 C6 38.5(5) . .
C11 C8 Fe1 C6 158.3(8) . .
C9 C8 Fe1 C7 -120.1(7) . .
C11 C8 Fe1 C7 119.8(9) . .
C9 C8 Fe1 C5 48.8(11) . .
C7 C8 Fe1 C5 168.9(8) . .
C11 C8 Fe1 C5 -71.3(12) . .
C5 C4 Fe1 C3 120.8(7) . .
C3 C4 Fe1 C1 -81.9(5) . .
C5 C4 Fe1 C1 38.9(5) . .
C3 C4 Fe1 C2 -36.9(5) . .
C5 C4 Fe1 C2 83.9(5) . .
C3 C4 Fe1 C9 117.9(5) . .
C5 C4 Fe1 C9 -121.4(5) . .
C3 C4 Fe1 C10 159.7(5) . .
C5 C4 Fe1 C10 -79.5(6) . .
C3 C4 Fe1 C8 76.1(6) . .
C5 C4 Fe1 C8 -163.2(5) . .
C3 C4 Fe1 C6 -168.6(9) . .
C5 C4 Fe1 C6 -47.8(12) . .
C3 C4 Fe1 C7 41.9(11) . .
C5 C4 Fe1 C7 162.7(8) . .
C3 C4 Fe1 C5 -120.8(7) . .
C10 C6 Fe1 C3 158.1(8) . .
C7 C6 Fe1 C3 38.1(11) . .
C10 C6 Fe1 C1 -121.8(5) . .
C7 C6 Fe1 C1 118.2(5) . .
C10 C6 Fe1 C2 -165.9(5) . .
C7 C6 Fe1 C2 74.2(6) . .
C10 C6 Fe1 C9 37.9(5) . .
C7 C6 Fe1 C9 -82.0(5) . .
C7 C6 Fe1 C10 -120.0(7) . .
C10 C6 Fe1 C8 81.5(5) . .
C7 C6 Fe1 C8 -38.5(5) . .
C10 C6 Fe1 C4 -42.3(12) . .
C7 C6 Fe1 C4 -162.3(9) . .
C10 C6 Fe1 C7 120.0(7) . .
C10 C6 Fe1 C5 -78.5(6) . .
C7 C6 Fe1 C5 161.6(5) . .
C8 C7 Fe1 C3 77.2(6) . .
C6 C7 Fe1 C3 -164.7(5) . .
C8 C7 Fe1 C1 160.3(5) . .
C6 C7 Fe1 C1 -81.7(6) . .
C8 C7 Fe1 C2 118.1(5) . .
C6 C7 Fe1 C2 -123.8(5) . .
C8 C7 Fe1 C9 -37.0(5) . .
C6 C7 Fe1 C9 81.1(6) . .
C8 C7 Fe1 C10 -81.1(5) . .
C6 C7 Fe1 C10 36.9(5) . .
C6 C7 Fe1 C8 118.0(7) . .
C8 C7 Fe1 C4 47.1(11) . .
C6 C7 Fe1 C4 165.2(8) . .
C8 C7 Fe1 C6 -118.0(7) . .
C8 C7 Fe1 C5 -167.9(9) . .
C6 C7 Fe1 C5 -49.9(12) . .
C4 C5 Fe1 C3 -36.5(5) . .
C1 C5 Fe1 C3 81.2(5) . .
C4 C5 Fe1 C1 -117.6(7) . .
C4 C5 Fe1 C2 -79.5(5) . .
C1 C5 Fe1 C2 38.1(5) . .
C4 C5 Fe1 C9 77.5(6) . .
C1 C5 Fe1 C9 -164.9(5) . .
C4 C5 Fe1 C10 120.7(5) . .
C1 C5 Fe1 C10 -121.7(5) . .
C4 C5 Fe1 C8 41.8(11) . .
C1 C5 Fe1 C8 159.4(8) . .
C1 C5 Fe1 C4 117.6(7) . .
C4 C5 Fe1 C6 162.7(5) . .
C1 C5 Fe1 C6 -79.7(6) . .
C4 C5 Fe1 C7 -159.9(9) . .
C1 C5 Fe1 C7 -42.3(12) . .
C13 C12 Fe2 C15 81.6(5) . .
C11 C12 Fe2 C15 -37.9(5) . .
C11 C12 Fe2 C13 -119.5(7) . .
C13 C12 Fe2 C18 -88.3(5) . .
C11 C12 Fe2 C18 152.2(5) . .
C13 C12 Fe2 C16 -170.3(5) . .
C11 C12 Fe2 C16 70.2(6) . .
C13 C12 Fe2 C14 37.6(5) . .
C11 C12 Fe2 C14 -81.9(5) . .
C13 C12 Fe2 C20 164.6(14) . .
C11 C12 Fe2 C20 45.0(17) . .
C13 C12 Fe2 C19 -56.3(9) . .
C11 C12 Fe2 C19 -175.8(7) . .
C13 C12 Fe2 C17 -130.9(5) . .
C11 C12 Fe2 C17 109.6(5) . .
C13 C12 Fe2 C11 119.5(7) . .
C11 C15 Fe2 C12 38.4(5) . .
C14 C15 Fe2 C12 -81.6(6) . .
C11 C15 Fe2 C13 82.2(6) . .
C14 C15 Fe2 C13 -37.8(6) . .
C11 C15 Fe2 C18 157.4(18) . .
C14 C15 Fe2 C18 38(2) . .
C11 C15 Fe2 C16 -83.6(6) . .
C14 C15 Fe2 C16 156.5(6) . .
C11 C15 Fe2 C14 119.9(8) . .
C11 C15 Fe2 C20 -127.0(6) . .
C14 C15 Fe2 C20 113.1(6) . .
C11 C15 Fe2 C19 -167.6(5) . .
C14 C15 Fe2 C19 72.5(7) . .
C11 C15 Fe2 C17 -47.4(9) . .
C14 C15 Fe2 C17 -167.4(7) . .
C14 C15 Fe2 C11 -119.9(8) . .
C14 C13 Fe2 C12 119.2(7) . .
C12 C13 Fe2 C15 -81.3(5) . .
C14 C13 Fe2 C15 37.9(5) . .
C12 C13 Fe2 C18 109.3(5) . .
C14 C13 Fe2 C18 -131.5(5) . .
C12 C13 Fe2 C16 33.7(17) . .
C14 C13 Fe2 C16 152.9(14) . .
C12 C13 Fe2 C14 -119.2(7) . .
C12 C13 Fe2 C20 -172.0(7) . .
C14 C13 Fe2 C20 -52.8(10) . .
C12 C13 Fe2 C19 152.2(5) . .
C14 C13 Fe2 C19 -88.6(6) . .
C12 C13 Fe2 C17 68.1(6) . .
C14 C13 Fe2 C17 -172.7(5) . .
C12 C13 Fe2 C11 -37.7(5) . .
C14 C13 Fe2 C11 81.5(6) . .
C19 C18 Fe2 C12 156.4(5) . .
C17 C18 Fe2 C12 -84.6(6) . .
C19 C18 Fe2 C15 42(2) . .
C17 C18 Fe2 C15 160.5(19) . .
C19 C18 Fe2 C13 113.1(5) . .
C17 C18 Fe2 C13 -127.9(5) . .
C19 C18 Fe2 C16 -81.5(6) . .
C17 C18 Fe2 C16 37.5(5) . .
C19 C18 Fe2 C14 73.1(7) . .
C17 C18 Fe2 C14 -167.9(6) . .
C19 C18 Fe2 C20 -37.9(5) . .
C17 C18 Fe2 C20 81.1(6) . .
C17 C18 Fe2 C19 119.0(7) . .
C19 C18 Fe2 C17 -119.0(7) . .
C19 C18 Fe2 C11 -167.3(6) . .
C17 C18 Fe2 C11 -48.3(9) . .
C20 C16 Fe2 C12 -170.9(5) . .
C17 C16 Fe2 C12 69.9(6) . .
C20 C16 Fe2 C15 -88.9(6) . .
C17 C16 Fe2 C15 151.9(5) . .
C20 C16 Fe2 C13 162.1(13) . .
C17 C16 Fe2 C13 42.9(17) . .
C20 C16 Fe2 C18 81.4(6) . .
C17 C16 Fe2 C18 -37.8(5) . .
C20 C16 Fe2 C14 -56.0(10) . .
C17 C16 Fe2 C14 -175.2(7) . .
C17 C16 Fe2 C20 -119.2(8) . .
C20 C16 Fe2 C19 37.8(5) . .
C17 C16 Fe2 C19 -81.4(6) . .
C20 C16 Fe2 C17 119.2(8) . .
C20 C16 Fe2 C11 -131.0(5) . .
C17 C16 Fe2 C11 109.8(5) . .
C13 C14 Fe2 C12 -37.7(5) . .
C15 C14 Fe2 C12 81.3(6) . .
C13 C14 Fe2 C15 -118.9(8) . .
C15 C14 Fe2 C13 118.9(8) . .
C13 C14 Fe2 C18 69.4(7) . .
C15 C14 Fe2 C18 -171.7(5) . .
C13 C14 Fe2 C16 -166.7(7) . .
C15 C14 Fe2 C16 -47.8(10) . .
C13 C14 Fe2 C20 155.1(5) . .
C15 C14 Fe2 C20 -86.0(6) . .
C13 C14 Fe2 C19 110.9(6) . .
C15 C14 Fe2 C19 -130.2(6) . .
C13 C14 Fe2 C17 28(2) . .
C15 C14 Fe2 C17 147.2(16) . .
C13 C14 Fe2 C11 -81.8(6) . .
C15 C14 Fe2 C11 37.1(5) . .
C16 C20 Fe2 C12 31.4(18) . .
C19 C20 Fe2 C12 150.6(13) . .
C16 C20 Fe2 C15 109.2(6) . .
C19 C20 Fe2 C15 -131.7(6) . .
C16 C20 Fe2 C13 -170.7(7) . .
C19 C20 Fe2 C13 -51.5(10) . .
C16 C20 Fe2 C18 -81.7(6) . .
C19 C20 Fe2 C18 37.5(5) . .
C19 C20 Fe2 C16 119.2(8) . .
C16 C20 Fe2 C14 152.8(6) . .
C19 C20 Fe2 C14 -88.0(6) . .
C16 C20 Fe2 C19 -119.2(8) . .
C16 C20 Fe2 C17 -37.6(6) . .
C19 C20 Fe2 C17 81.6(6) . .
C16 C20 Fe2 C11 67.7(7) . .
C19 C20 Fe2 C11 -173.1(5) . .
C18 C19 Fe2 C12 -47.0(9) . .
C20 C19 Fe2 C12 -166.1(7) . .
C18 C19 Fe2 C15 -170.8(5) . .
C20 C19 Fe2 C15 70.1(7) . .
C18 C19 Fe2 C13 -85.2(6) . .
C20 C19 Fe2 C13 155.7(6) . .
C20 C19 Fe2 C18 -119.1(8) . .
C18 C19 Fe2 C16 81.6(6) . .
C20 C19 Fe2 C16 -37.5(6) . .
C18 C19 Fe2 C14 -129.2(5) . .
C20 C19 Fe2 C14 111.7(6) . .
C18 C19 Fe2 C20 119.1(8) . .
C18 C19 Fe2 C17 37.9(5) . .
C20 C19 Fe2 C17 -81.1(6) . .
C18 C19 Fe2 C11 146.5(16) . .
C20 C19 Fe2 C11 27(2) . .
C16 C17 Fe2 C12 -128.9(5) . .
C18 C17 Fe2 C12 111.9(5) . .
C16 C17 Fe2 C15 -54.2(9) . .
C18 C17 Fe2 C15 -173.3(6) . .
C16 C17 Fe2 C13 -167.9(5) . .
C18 C17 Fe2 C13 73.0(6) . .
C16 C17 Fe2 C18 119.2(7) . .
C18 C17 Fe2 C16 -119.2(7) . .
C16 C17 Fe2 C14 169.0(16) . .
C18 C17 Fe2 C14 49.8(19) . .
C16 C17 Fe2 C20 37.6(5) . .
C18 C17 Fe2 C20 -81.6(5) . .
C16 C17 Fe2 C19 81.6(6) . .
C18 C17 Fe2 C19 -37.6(5) . .
C16 C17 Fe2 C11 -86.0(6) . .
C18 C17 Fe2 C11 154.8(5) . .
C15 C11 Fe2 C12 -118.4(7) . .
C8 C11 Fe2 C12 120.0(9) . .
C12 C11 Fe2 C15 118.4(7) . .
C8 C11 Fe2 C15 -121.6(9) . .
C15 C11 Fe2 C13 -81.0(6) . .
C12 C11 Fe2 C13 37.4(5) . .
C8 C11 Fe2 C13 157.4(8) . .
C15 C11 Fe2 C18 -172.3(6) . .
C12 C11 Fe2 C18 -53.9(9) . .
C8 C11 Fe2 C18 66.1(10) . .
C15 C11 Fe2 C16 112.8(6) . .
C12 C11 Fe2 C16 -128.8(5) . .
C8 C11 Fe2 C16 -8.8(8) . .
C15 C11 Fe2 C14 -37.4(6) . .
C12 C11 Fe2 C14 81.0(6) . .
C8 C11 Fe2 C14 -158.9(8) . .
C15 C11 Fe2 C20 74.1(7) . .
C12 C11 Fe2 C20 -167.5(5) . .
C8 C11 Fe2 C20 -47.4(9) . .
C15 C11 Fe2 C19 52(2) . .
C12 C11 Fe2 C19 170.0(16) . .
C8 C11 Fe2 C19 -70(2) . .
C15 C11 Fe2 C17 155.1(6) . .
C12 C11 Fe2 C17 -86.5(6) . .
C8 C11 Fe2 C17 33.6(8) . .
C33 C32 Fe3 C29 38.9(5) . .
C31 C32 Fe3 C29 -81.5(5) . .
C33 C32 Fe3 C34 -46.4(15) . .
C31 C32 Fe3 C34 -166.9(11) . .
C31 C32 Fe3 C33 -120.4(7) . .
C33 C32 Fe3 C38 -70.5(6) . .
C31 C32 Fe3 C38 169.1(4) . .
C33 C32 Fe3 C37 -110.4(5) . .
C31 C32 Fe3 C37 129.2(5) . .
C33 C32 Fe3 C36 -152.7(5) . .
C31 C32 Fe3 C36 86.9(5) . .
C33 C32 Fe3 C35 176.2(6) . .
C31 C32 Fe3 C35 55.8(9) . .
C33 C32 Fe3 C30 83.3(5) . .
C31 C32 Fe3 C30 -37.1(4) . .
C33 C32 Fe3 C31 120.4(7) . .
C30 C29 Fe3 C32 82.0(5) . .
C33 C29 Fe3 C32 -37.4(5) . .
P2 C29 Fe3 C32 -158.3(6) . .
C30 C29 Fe3 C34 -113.6(5) . .
C33 C29 Fe3 C34 127.0(5) . .
P2 C29 Fe3 C34 6.1(6) . .
C30 C29 Fe3 C33 119.4(6) . .
P2 C29 Fe3 C33 -120.9(7) . .
C30 C29 Fe3 C38 -157.5(5) . .
C33 C29 Fe3 C38 83.1(5) . .
P2 C29 Fe3 C38 -37.8(6) . .
C30 C29 Fe3 C37 166.4(6) . .
C33 C29 Fe3 C37 47.0(8) . .
P2 C29 Fe3 C37 -73.9(8) . .
C30 C29 Fe3 C36 -35.5(18) . .
C33 C29 Fe3 C36 -154.9(15) . .
P2 C29 Fe3 C36 84.2(17) . .
C30 C29 Fe3 C35 -73.2(6) . .
C33 C29 Fe3 C35 167.4(5) . .
P2 C29 Fe3 C35 46.5(7) . .
C33 C29 Fe3 C30 -119.4(6) . .
P2 C29 Fe3 C30 119.7(7) . .
C30 C29 Fe3 C31 38.5(5) . .
C33 C29 Fe3 C31 -80.9(5) . .
P2 C29 Fe3 C31 158.2(6) . .
C35 C34 Fe3 C32 -150.2(12) . .
C38 C34 Fe3 C32 -30.2(15) . .
C35 C34 Fe3 C29 130.0(5) . .
C38 C34 Fe3 C29 -110.0(5) . .
C35 C34 Fe3 C33 173.0(5) . .
C38 C34 Fe3 C33 -67.0(6) . .
C35 C34 Fe3 C38 -120.0(6) . .
C35 C34 Fe3 C37 -81.6(5) . .
C38 C34 Fe3 C37 38.4(4) . .
C35 C34 Fe3 C36 -37.7(5) . .
C38 C34 Fe3 C36 82.3(5) . .
C38 C34 Fe3 C35 120.0(6) . .
C35 C34 Fe3 C30 85.7(5) . .
C38 C34 Fe3 C30 -154.3(4) . .
C35 C34 Fe3 C31 49.3(9) . .
C38 C34 Fe3 C31 169.3(6) . .
C29 C33 Fe3 C32 118.5(7) . .
C32 C33 Fe3 C29 -118.5(7) . .
C32 C33 Fe3 C34 166.4(5) . .
C29 C33 Fe3 C34 -75.1(6) . .
C32 C33 Fe3 C38 127.6(5) . .
C29 C33 Fe3 C38 -113.9(5) . .
C32 C33 Fe3 C37 85.0(5) . .
C29 C33 Fe3 C37 -156.5(4) . .
C32 C33 Fe3 C36 51.9(8) . .
C29 C33 Fe3 C36 170.5(6) . .
C32 C33 Fe3 C35 -171.4(14) . .
C29 C33 Fe3 C35 -52.9(17) . .
C32 C33 Fe3 C30 -80.8(5) . .
C29 C33 Fe3 C30 37.8(4) . .
C32 C33 Fe3 C31 -36.9(5) . .
C29 C33 Fe3 C31 81.6(5) . .
C37 C38 Fe3 C32 -71.1(6) . .
C34 C38 Fe3 C32 170.9(5) . .
C37 C38 Fe3 C29 -153.6(4) . .
C34 C38 Fe3 C29 88.5(5) . .
C37 C38 Fe3 C34 118.0(7) . .
C37 C38 Fe3 C33 -110.2(5) . .
C34 C38 Fe3 C33 131.8(5) . .
C34 C38 Fe3 C37 -118.0(7) . .
C37 C38 Fe3 C36 37.1(5) . .
C34 C38 Fe3 C36 -80.9(5) . .
C37 C38 Fe3 C35 81.1(5) . .
C34 C38 Fe3 C35 -36.9(5) . .
C37 C38 Fe3 C30 173.0(7) . .
C34 C38 Fe3 C30 55.0(9) . .
C37 C38 Fe3 C31 -44.4(14) . .
C34 C38 Fe3 C31 -162.4(11) . .
C36 C37 Fe3 C32 -112.4(5) . .
C38 C37 Fe3 C32 127.3(5) . .
C39 C37 Fe3 C32 9.3(7) . .
C36 C37 Fe3 C29 173.3(6) . .
C38 C37 Fe3 C29 53.0(8) . .
C39 C37 Fe3 C29 -65.0(10) . .
C36 C37 Fe3 C34 81.8(5) . .
C38 C37 Fe3 C34 -38.5(5) . .
C39 C37 Fe3 C34 -156.5(8) . .
C36 C37 Fe3 C33 -154.2(5) . .
C38 C37 Fe3 C33 85.5(5) . .
C39 C37 Fe3 C33 -32.5(8) . .
C36 C37 Fe3 C38 120.3(7) . .
C39 C37 Fe3 C38 -118.0(9) . .
C38 C37 Fe3 C36 -120.3(7) . .
C39 C37 Fe3 C36 121.7(9) . .
C36 C37 Fe3 C35 38.4(5) . .
C38 C37 Fe3 C35 -81.9(5) . .
C39 C37 Fe3 C35 160.1(8) . .
C36 C37 Fe3 C30 -46.4(15) . .
C38 C37 Fe3 C30 -166.7(12) . .
C39 C37 Fe3 C30 75.3(15) . .
C36 C37 Fe3 C31 -73.5(6) . .
C38 C37 Fe3 C31 166.2(5) . .
C39 C37 Fe3 C31 48.2(8) . .
C37 C36 Fe3 C32 83.7(5) . .
C35 C36 Fe3 C32 -158.1(5) . .
C37 C36 Fe3 C29 -163.6(14) . .
C35 C36 Fe3 C29 -45.4(18) . .
C37 C36 Fe3 C34 -81.2(5) . .
C35 C36 Fe3 C34 37.0(5) . .
C37 C36 Fe3 C33 49.2(8) . .
C35 C36 Fe3 C33 167.4(6) . .
C37 C36 Fe3 C38 -37.2(5) . .
C35 C36 Fe3 C38 81.0(5) . .
C35 C36 Fe3 C37 118.2(7) . .
C37 C36 Fe3 C35 -118.2(7) . .
C37 C36 Fe3 C30 167.0(5) . .
C35 C36 Fe3 C30 -74.9(6) . .
C37 C36 Fe3 C31 126.5(5) . .
C35 C36 Fe3 C31 -115.4(5) . .
C34 C35 Fe3 C32 164.6(6) . .
C36 C35 Fe3 C32 44.8(9) . .
C34 C35 Fe3 C29 -71.2(6) . .
C36 C35 Fe3 C29 169.1(5) . .
C36 C35 Fe3 C34 -119.7(7) . .
C34 C35 Fe3 C33 -27.1(17) . .
C36 C35 Fe3 C33 -146.9(14) . .
C34 C35 Fe3 C38 37.5(5) . .
C36 C35 Fe3 C38 -82.2(5) . .
C34 C35 Fe3 C37 81.5(5) . .
C36 C35 Fe3 C37 -38.2(5) . .
C34 C35 Fe3 C36 119.7(7) . .
C34 C35 Fe3 C30 -113.4(5) . .
C36 C35 Fe3 C30 126.9(5) . .
C34 C35 Fe3 C31 -157.3(5) . .
C36 C35 Fe3 C31 83.0(5) . .
C31 C30 Fe3 C32 36.6(5) . .
C29 C30 Fe3 C32 -81.1(5) . .
C31 C30 Fe3 C29 117.7(7) . .
C31 C30 Fe3 C34 -156.3(5) . .
C29 C30 Fe3 C34 86.0(5) . .
C31 C30 Fe3 C33 79.6(5) . .
C29 C30 Fe3 C33 -38.1(4) . .
C31 C30 Fe3 C38 165.4(7) . .
C29 C30 Fe3 C38 47.7(9) . .
C31 C30 Fe3 C37 -33.7(15) . .
C29 C30 Fe3 C37 -151.4(12) . .
C31 C30 Fe3 C36 -71.0(6) . .
C29 C30 Fe3 C36 171.3(5) . .
C31 C30 Fe3 C35 -113.2(5) . .
C29 C30 Fe3 C35 129.1(5) . .
C29 C30 Fe3 C31 -117.7(7) . .
C30 C31 Fe3 C32 -120.7(7) . .
C32 C31 Fe3 C29 81.7(5) . .
C30 C31 Fe3 C29 -38.9(5) . .
C32 C31 Fe3 C34 172.5(7) . .
C30 C31 Fe3 C34 51.9(9) . .
C32 C31 Fe3 C33 36.7(5) . .
C30 C31 Fe3 C33 -83.9(5) . .
C32 C31 Fe3 C38 -34.2(14) . .
C30 C31 Fe3 C38 -154.8(11) . .
C32 C31 Fe3 C37 -69.1(6) . .
C30 C31 Fe3 C37 170.3(5) . .
C32 C31 Fe3 C36 -110.1(5) . .
C30 C31 Fe3 C36 129.3(5) . .
C32 C31 Fe3 C35 -153.1(5) . .
C30 C31 Fe3 C35 86.2(5) . .
C32 C31 Fe3 C30 120.7(7) . .
C46 C45 Fe4 C44 -118.6(9) . .
C46 C45 Fe4 C43 -160.4(8) . .
C44 C45 Fe4 C43 -41.9(12) . .
C46 C45 Fe4 C40 121.9(6) . .
C44 C45 Fe4 C40 -119.5(6) . .
C44 C45 Fe4 C46 118.6(9) . .
C46 C45 Fe4 C41 80.8(7) . .
C44 C45 Fe4 C41 -160.6(6) . .
C46 C45 Fe4 C39 165.2(6) . .
C44 C45 Fe4 C39 -76.2(7) . .
C46 C45 Fe4 C42 46.8(16) . .
C44 C45 Fe4 C42 165.4(12) . .
C46 C45 Fe4 C47 -37.7(6) . .
C44 C45 Fe4 C47 80.9(6) . .
C46 C45 Fe4 C48 -81.6(7) . .
C44 C45 Fe4 C48 37.0(6) . .
C48 C44 Fe4 C45 120.0(8) . .
C48 C44 Fe4 C43 -78.1(6) . .
C45 C44 Fe4 C43 161.9(6) . .
C48 C44 Fe4 C40 -161.1(5) . .
C45 C44 Fe4 C40 78.8(7) . .
C48 C44 Fe4 C46 82.0(6) . .
C45 C44 Fe4 C46 -38.0(6) . .
C48 C44 Fe4 C41 173.1(9) . .
C45 C44 Fe4 C41 53.1(13) . .
C48 C44 Fe4 C39 -120.2(5) . .
C45 C44 Fe4 C39 119.8(6) . .
C48 C44 Fe4 C42 -49.1(12) . .
C45 C44 Fe4 C42 -169.1(9) . .
C48 C44 Fe4 C47 38.2(6) . .
C45 C44 Fe4 C47 -81.8(7) . .
C45 C44 Fe4 C48 -120.0(8) . .
C42 C43 Fe4 C45 -167.6(9) . .
C39 C43 Fe4 C45 -47.2(11) . .
C42 C43 Fe4 C44 162.3(6) . .
C39 C43 Fe4 C44 -77.4(6) . .
C42 C43 Fe4 C40 -81.7(5) . .
C39 C43 Fe4 C40 38.6(5) . .
C42 C43 Fe4 C46 53.2(13) . .
C39 C43 Fe4 C46 173.5(10) . .
C42 C43 Fe4 C41 -37.9(5) . .
C39 C43 Fe4 C41 82.4(5) . .
C42 C43 Fe4 C39 -120.3(7) . .
C39 C43 Fe4 C42 120.3(7) . .
C42 C43 Fe4 C47 80.8(6) . .
C39 C43 Fe4 C47 -158.8(5) . .
C42 C43 Fe4 C48 121.3(6) . .
C39 C43 Fe4 C48 -118.3(5) . .
C41 C40 Fe4 C45 -124.7(5) . .
C39 C40 Fe4 C45 116.0(5) . .
C41 C40 Fe4 C44 -166.9(5) . .
C39 C40 Fe4 C44 73.8(6) . .
C41 C40 Fe4 C43 80.3(5) . .
C39 C40 Fe4 C43 -38.9(5) . .
C41 C40 Fe4 C46 -83.2(6) . .
C39 C40 Fe4 C46 157.6(5) . .
C39 C40 Fe4 C41 -119.2(7) . .
C41 C40 Fe4 C39 119.2(7) . .
C41 C40 Fe4 C42 36.9(5) . .
C39 C40 Fe4 C42 -82.4(5) . .
C41 C40 Fe4 C47 -51.7(14) . .
C39 C40 Fe4 C47 -170.9(11) . .
C41 C40 Fe4 C48 160.0(9) . .
C39 C40 Fe4 C48 40.8(12) . .
C47 C46 Fe4 C45 -119.2(9) . .
C45 C46 Fe4 C44 38.2(6) . .
C47 C46 Fe4 C44 -80.9(6) . .
C45 C46 Fe4 C43 156.0(10) . .
C47 C46 Fe4 C43 36.8(14) . .
C45 C46 Fe4 C40 -76.7(7) . .
C47 C46 Fe4 C40 164.2(6) . .
C45 C46 Fe4 C41 -120.5(6) . .
C47 C46 Fe4 C41 120.3(6) . .
C45 C46 Fe4 C39 -35.3(13) . .
C47 C46 Fe4 C39 -154.5(9) . .
C45 C46 Fe4 C42 -164.0(6) . .
C47 C46 Fe4 C42 76.8(7) . .
C45 C46 Fe4 C47 119.2(9) . .
C45 C46 Fe4 C48 81.7(7) . .
C47 C46 Fe4 C48 -37.5(6) . .
C40 C41 Fe4 C45 74.3(6) . .
C42 C41 Fe4 C45 -164.9(5) . .
C40 C41 Fe4 C44 34.4(12) . .
C42 C41 Fe4 C44 155.3(10) . .
C40 C41 Fe4 C43 -83.2(5) . .
C42 C41 Fe4 C43 37.7(5) . .
C42 C41 Fe4 C40 120.9(7) . .
C40 C41 Fe4 C46 117.7(5) . .
C42 C41 Fe4 C46 -121.4(6) . .
C40 C41 Fe4 C39 -38.2(5) . .
C42 C41 Fe4 C39 82.7(5) . .
C40 C41 Fe4 C42 -120.9(7) . .
C40 C41 Fe4 C47 161.0(6) . .
C42 C41 Fe4 C47 -78.1(7) . .
C40 C41 Fe4 C48 -158.2(9) . .
C42 C41 Fe4 C48 -37.4(12) . .
C40 C39 Fe4 C45 -82.0(6) . .
C43 C39 Fe4 C45 159.9(5) . .
C37 C39 Fe4 C45 39.8(8) . .
C40 C39 Fe4 C44 -122.9(5) . .
C43 C39 Fe4 C44 119.0(5) . .
C37 C39 Fe4 C44 -1.1(8) . .
C40 C39 Fe4 C43 118.1(7) . .
C37 C39 Fe4 C43 -120.1(9) . .
C43 C39 Fe4 C40 -118.1(7) . .
C37 C39 Fe4 C40 121.8(9) . .
C40 C39 Fe4 C46 -56.3(11) . .
C43 C39 Fe4 C46 -174.4(9) . .
C37 C39 Fe4 C46 65.5(12) . .
C40 C39 Fe4 C41 37.6(5) . .
C43 C39 Fe4 C41 -80.5(5) . .
C37 C39 Fe4 C41 159.4(7) . .
C40 C39 Fe4 C42 81.3(5) . .
C43 C39 Fe4 C42 -36.7(5) . .
C37 C39 Fe4 C42 -156.9(7) . .
C40 C39 Fe4 C47 171.8(10) . .
C43 C39 Fe4 C47 53.7(12) . .
C37 C39 Fe4 C47 -66.4(13) . .
C40 C39 Fe4 C48 -163.2(5) . .
C43 C39 Fe4 C48 78.8(6) . .
C37 C39 Fe4 C48 -41.3(8) . .
C43 C42 Fe4 C45 163.4(12) . .
C41 C42 Fe4 C45 44.3(15) . .
C43 C42 Fe4 C44 -40.5(12) . .
C41 C42 Fe4 C44 -159.6(9) . .
C41 C42 Fe4 C43 -119.1(7) . .
C43 C42 Fe4 C40 82.3(5) . .
C41 C42 Fe4 C40 -36.8(5) . .
C43 C42 Fe4 C46 -160.7(5) . .
C41 C42 Fe4 C46 80.2(7) . .
C43 C42 Fe4 C41 119.1(7) . .
C43 C42 Fe4 C39 37.8(5) . .
C41 C42 Fe4 C39 -81.2(5) . .
C43 C42 Fe4 C47 -118.7(5) . .
C41 C42 Fe4 C47 122.2(6) . .
C43 C42 Fe4 C48 -75.5(6) . .
C41 C42 Fe4 C48 165.4(5) . .
C46 C47 Fe4 C45 37.8(6) . .
C48 C47 Fe4 C45 -82.1(7) . .
C46 C47 Fe4 C44 82.0(7) . .
C48 C47 Fe4 C44 -37.8(6) . .
C46 C47 Fe4 C43 -166.2(6) . .
C48 C47 Fe4 C43 74.0(7) . .
C46 C47 Fe4 C40 -42.1(15) . .
C48 C47 Fe4 C40 -162.0(10) . .
C48 C47 Fe4 C46 -119.8(9) . .
C46 C47 Fe4 C41 -80.9(7) . .
C48 C47 Fe4 C41 159.3(6) . .
C46 C47 Fe4 C39 154.0(9) . .
C48 C47 Fe4 C39 34.2(14) . .
C46 C47 Fe4 C42 -123.5(6) . .
C48 C47 Fe4 C42 116.7(6) . .
C46 C47 Fe4 C48 119.8(9) . .
C44 C48 Fe4 C45 -37.5(6) . .
C47 C48 Fe4 C45 81.1(7) . .
C47 C48 Fe4 C44 118.6(9) . .
C44 C48 Fe4 C43 118.2(6) . .
C47 C48 Fe4 C43 -123.3(7) . .
C44 C48 Fe4 C40 45.6(12) . .
C47 C48 Fe4 C40 164.2(9) . .
C44 C48 Fe4 C46 -81.3(6) . .
C47 C48 Fe4 C46 37.3(7) . .
C44 C48 Fe4 C41 -173.4(9) . .
C47 C48 Fe4 C41 -54.8(13) . .
C44 C48 Fe4 C39 75.6(6) . .
C47 C48 Fe4 C39 -165.9(6) . .
C44 C48 Fe4 C42 158.8(5) . .
C47 C48 Fe4 C42 -82.6(7) . .
C44 C48 Fe4 C47 -118.6(9) . .
C61 C60 Fe5 C57 38.8(4) . .
C59 C60 Fe5 C57 -81.5(5) . .
C61 C60 Fe5 C62 -46.5(12) . .
C59 C60 Fe5 C62 -166.7(9) . .
C59 C60 Fe5 C61 -120.2(6) . .
C61 C60 Fe5 C64 -156.1(4) . .
C59 C60 Fe5 C64 83.7(5) . .
C61 C60 Fe5 C66 -73.1(5) . .
C59 C60 Fe5 C66 166.7(4) . .
C61 C60 Fe5 C58 83.0(5) . .
C59 C60 Fe5 C58 -37.2(4) . .
C61 C60 Fe5 C63 173.8(6) . .
C59 C60 Fe5 C63 53.6(9) . .
C61 C60 Fe5 C65 -114.1(5) . .
C59 C60 Fe5 C65 125.7(5) . .
C61 C60 Fe5 C59 120.2(6) . .
C58 C57 Fe5 C60 82.4(5) . .
C61 C57 Fe5 C60 -37.5(4) . .
P3 C57 Fe5 C60 -157.0(5) . .
C58 C57 Fe5 C62 -115.7(5) . .
C61 C57 Fe5 C62 124.3(5) . .
P3 C57 Fe5 C62 4.8(6) . .
C58 C57 Fe5 C61 120.0(6) . .
P3 C57 Fe5 C61 -119.5(7) . .
C58 C57 Fe5 C64 -37.8(14) . .
C61 C57 Fe5 C64 -157.8(11) . .
P3 C57 Fe5 C64 82.7(13) . .
C58 C57 Fe5 C66 -158.8(5) . .
C61 C57 Fe5 C66 81.3(5) . .
P3 C57 Fe5 C66 -38.2(6) . .
C61 C57 Fe5 C58 -120.0(6) . .
P3 C57 Fe5 C58 120.6(7) . .
C58 C57 Fe5 C63 -75.1(6) . .
C61 C57 Fe5 C63 165.0(5) . .
P3 C57 Fe5 C63 45.5(6) . .
C58 C57 Fe5 C65 165.0(7) . .
C61 C57 Fe5 C65 45.1(9) . .
P3 C57 Fe5 C65 -74.4(8) . .
C58 C57 Fe5 C59 39.0(5) . .
C61 C57 Fe5 C59 -81.0(5) . .
P3 C57 Fe5 C59 159.5(6) . .
C63 C62 Fe5 C60 -154.4(9) . .
C66 C62 Fe5 C60 -34.6(12) . .
C63 C62 Fe5 C57 126.6(5) . .
C66 C62 Fe5 C57 -113.5(5) . .
C63 C62 Fe5 C61 169.8(4) . .
C66 C62 Fe5 C61 -70.3(5) . .
C63 C62 Fe5 C64 -37.4(4) . .
C66 C62 Fe5 C64 82.4(5) . .
C63 C62 Fe5 C66 -119.9(6) . .
C63 C62 Fe5 C58 82.9(5) . .
C66 C62 Fe5 C58 -157.3(4) . .
C66 C62 Fe5 C63 119.9(6) . .
C63 C62 Fe5 C65 -81.3(5) . .
C66 C62 Fe5 C65 38.5(4) . .
C63 C62 Fe5 C59 47.1(9) . .
C66 C62 Fe5 C59 167.0(7) . .
C57 C61 Fe5 C60 118.7(6) . .
C60 C61 Fe5 C57 -118.7(6) . .
C60 C61 Fe5 C62 164.5(4) . .
C57 C61 Fe5 C62 -76.9(5) . .
C60 C61 Fe5 C64 49.2(9) . .
C57 C61 Fe5 C64 167.9(6) . .
C60 C61 Fe5 C66 125.0(5) . .
C57 C61 Fe5 C66 -116.4(4) . .
C60 C61 Fe5 C58 -81.3(5) . .
C57 C61 Fe5 C58 37.4(4) . .
C60 C61 Fe5 C63 -169.9(11) . .
C57 C61 Fe5 C63 -51.3(13) . .
C60 C61 Fe5 C65 82.1(5) . .
C57 C61 Fe5 C65 -159.3(4) . .
C60 C61 Fe5 C59 -37.0(4) . .
C57 C61 Fe5 C59 81.6(5) . .
C65 C64 Fe5 C60 81.3(5) . .
C63 C64 Fe5 C60 -160.9(5) . .
C65 C64 Fe5 C57 -164.7(11) . .
C63 C64 Fe5 C57 -46.9(14) . .
C65 C64 Fe5 C62 -81.3(5) . .
C63 C64 Fe5 C62 36.5(5) . .
C65 C64 Fe5 C61 47.5(9) . .
C63 C64 Fe5 C61 165.3(6) . .
C65 C64 Fe5 C66 -37.8(5) . .
C63 C64 Fe5 C66 80.0(5) . .
C65 C64 Fe5 C58 165.3(5) . .
C63 C64 Fe5 C58 -76.9(6) . .
C65 C64 Fe5 C63 -117.8(7) . .
C63 C64 Fe5 C65 117.8(7) . .
C65 C64 Fe5 C59 123.7(5) . .
C63 C64 Fe5 C59 -118.5(5) . .
C62 C66 Fe5 C60 168.2(4) . .
C65 C66 Fe5 C60 -73.3(5) . .
C62 C66 Fe5 C57 85.0(5) . .
C65 C66 Fe5 C57 -156.6(4) . .
C65 C66 Fe5 C62 118.4(7) . .
C62 C66 Fe5 C61 128.1(5) . .
C65 C66 Fe5 C61 -113.4(5) . .
C62 C66 Fe5 C64 -81.1(5) . .
C65 C66 Fe5 C64 37.3(5) . .
C62 C66 Fe5 C58 51.0(9) . .
C65 C66 Fe5 C58 169.5(7) . .
C62 C66 Fe5 C63 -36.9(5) . .
C65 C66 Fe5 C63 81.5(5) . .
C62 C66 Fe5 C65 -118.4(7) . .
C62 C66 Fe5 C59 -162.7(10) . .
C65 C66 Fe5 C59 -44.2(12) . .
C57 C58 Fe5 C60 -80.9(5) . .
C59 C58 Fe5 C60 36.5(5) . .
C59 C58 Fe5 C57 117.4(7) . .
C57 C58 Fe5 C62 83.6(5) . .
C59 C58 Fe5 C62 -158.9(5) . .
C57 C58 Fe5 C61 -37.8(4) . .
C59 C58 Fe5 C61 79.6(5) . .
C57 C58 Fe5 C64 168.5(4) . .
C59 C58 Fe5 C64 -74.1(6) . .
C57 C58 Fe5 C66 47.6(9) . .
C59 C58 Fe5 C66 165.1(7) . .
C57 C58 Fe5 C63 126.0(5) . .
C59 C58 Fe5 C63 -116.6(5) . .
C57 C58 Fe5 C65 -156.8(10) . .
C59 C58 Fe5 C65 -39.4(13) . .
C57 C58 Fe5 C59 -117.4(7) . .
C62 C63 Fe5 C60 162.7(7) . .
C64 C63 Fe5 C60 42.3(9) . .
C62 C63 Fe5 C57 -73.6(5) . .
C64 C63 Fe5 C57 166.0(4) . .
C64 C63 Fe5 C62 -120.4(6) . .
C62 C63 Fe5 C61 -32.6(14) . .
C64 C63 Fe5 C61 -153.0(11) . .
C62 C63 Fe5 C64 120.4(6) . .
C62 C63 Fe5 C66 37.4(4) . .
C64 C63 Fe5 C66 -83.0(5) . .
C62 C63 Fe5 C58 -115.8(5) . .
C64 C63 Fe5 C58 123.8(5) . .
C62 C63 Fe5 C65 82.0(5) . .
C64 C63 Fe5 C65 -38.4(4) . .
C62 C63 Fe5 C59 -159.6(4) . .
C64 C63 Fe5 C59 80.0(5) . .
C64 C65 Fe5 C60 -115.2(5) . .
C66 C65 Fe5 C60 125.1(5) . .
C67 C65 Fe5 C60 6.6(7) . .
C64 C65 Fe5 C57 171.0(6) . .
C66 C65 Fe5 C57 51.3(9) . .
C67 C65 Fe5 C57 -67.1(10) . .
C64 C65 Fe5 C62 81.9(5) . .
C66 C65 Fe5 C62 -37.8(5) . .
C67 C65 Fe5 C62 -156.2(8) . .
C64 C65 Fe5 C61 -156.9(5) . .
C66 C65 Fe5 C61 83.3(5) . .
C67 C65 Fe5 C61 -35.1(8) . .
C66 C65 Fe5 C64 -119.7(7) . .
C67 C65 Fe5 C64 121.9(9) . .
C64 C65 Fe5 C66 119.7(7) . .
C67 C65 Fe5 C66 -118.4(8) . .
C64 C65 Fe5 C58 -44.7(13) . .
C66 C65 Fe5 C58 -164.4(10) . .
C67 C65 Fe5 C58 77.1(13) . .
C64 C65 Fe5 C63 38.7(5) . .
C66 C65 Fe5 C63 -81.0(5) . .
C67 C65 Fe5 C63 160.6(8) . .
C64 C65 Fe5 C59 -75.4(6) . .
C66 C65 Fe5 C59 164.9(5) . .
C67 C65 Fe5 C59 46.5(8) . .
C58 C59 Fe5 C60 -120.8(7) . .
C60 C59 Fe5 C57 81.9(5) . .
C58 C59 Fe5 C57 -38.9(5) . .
C60 C59 Fe5 C62 170.4(7) . .
C58 C59 Fe5 C62 49.5(10) . .
C60 C59 Fe5 C61 37.0(4) . .
C58 C59 Fe5 C61 -83.8(5) . .
C60 C59 Fe5 C64 -113.5(5) . .
C58 C59 Fe5 C64 125.6(5) . .
C60 C59 Fe5 C66 -38.2(12) . .
C58 C59 Fe5 C66 -159.0(9) . .
C60 C59 Fe5 C58 120.8(7) . .
C60 C59 Fe5 C63 -156.1(4) . .
C58 C59 Fe5 C63 83.1(5) . .
C60 C59 Fe5 C65 -72.2(5) . .
C58 C59 Fe5 C65 167.0(5) . .
C72 C73 Fe6 C75 82.2(6) . .
C74 C73 Fe6 C75 -38.0(6) . .
C72 C73 Fe6 C71 -42.1(11) . .
C74 C73 Fe6 C71 -162.3(8) . .
C72 C73 Fe6 C76 38.3(5) . .
C74 C73 Fe6 C76 -81.8(6) . .
C74 C73 Fe6 C72 -120.1(8) . .
C72 C73 Fe6 C74 120.1(8) . .
C72 C73 Fe6 C69 -161.8(5) . .
C74 C73 Fe6 C69 78.1(7) . .
C72 C73 Fe6 C68 -120.2(5) . .
C74 C73 Fe6 C68 119.7(6) . .
C72 C73 Fe6 C70 165.4(10) . .
C74 C73 Fe6 C70 45.3(14) . .
C72 C73 Fe6 C67 -77.3(6) . .
C74 C73 Fe6 C67 162.5(5) . .
C74 C75 Fe6 C73 38.9(6) . .
C76 C75 Fe6 C73 -81.1(6) . .
C74 C75 Fe6 C71 -164.6(6) . .
C76 C75 Fe6 C71 75.4(6) . .
C74 C75 Fe6 C76 120.0(8) . .
C74 C75 Fe6 C72 82.4(7) . .
C76 C75 Fe6 C72 -37.5(6) . .
C76 C75 Fe6 C74 -120.0(8) . .
C74 C75 Fe6 C69 -80.2(7) . .
C76 C75 Fe6 C69 159.9(5) . .
C74 C75 Fe6 C68 -43.6(13) . .
C76 C75 Fe6 C68 -163.6(9) . .
C74 C75 Fe6 C70 -122.0(6) . .
C76 C75 Fe6 C70 118.0(6) . .
C74 C75 Fe6 C67 159.6(10) . .
C76 C75 Fe6 C67 39.6(13) . .
C70 C71 Fe6 C73 -167.2(9) . .
C67 C71 Fe6 C73 -48.6(11) . .
C70 C71 Fe6 C75 79.5(6) . .
C67 C71 Fe6 C75 -162.0(5) . .
C70 C71 Fe6 C76 120.5(5) . .
C67 C71 Fe6 C76 -121.0(5) . .
C70 C71 Fe6 C72 162.6(5) . .
C67 C71 Fe6 C72 -78.8(6) . .
C70 C71 Fe6 C74 49.1(13) . .
C67 C71 Fe6 C74 167.7(11) . .
C70 C71 Fe6 C69 -36.8(5) . .
C67 C71 Fe6 C69 81.8(5) . .
C70 C71 Fe6 C68 -80.9(5) . .
C67 C71 Fe6 C68 37.6(5) . .
C67 C71 Fe6 C70 118.6(7) . .
C70 C71 Fe6 C67 -118.6(7) . .
C75 C76 Fe6 C73 81.9(6) . .
C72 C76 Fe6 C73 -37.9(6) . .
C72 C76 Fe6 C75 -119.8(8) . .
C75 C76 Fe6 C71 -122.6(6) . .
C72 C76 Fe6 C71 117.6(5) . .
C75 C76 Fe6 C72 119.8(8) . .
C75 C76 Fe6 C74 37.2(6) . .
C72 C76 Fe6 C74 -82.7(6) . .
C75 C76 Fe6 C69 -50.0(12) . .
C72 C76 Fe6 C69 -169.8(9) . .
C75 C76 Fe6 C68 163.0(9) . .
C72 C76 Fe6 C68 43.2(12) . .
C75 C76 Fe6 C70 -80.9(6) . .
C72 C76 Fe6 C70 159.2(5) . .
C75 C76 Fe6 C67 -164.7(5) . .
C72 C76 Fe6 C67 75.5(6) . .
C76 C72 Fe6 C73 118.5(8) . .
C73 C72 Fe6 C75 -81.2(6) . .
C76 C72 Fe6 C75 37.3(5) . .
C73 C72 Fe6 C71 161.7(5) . .
C76 C72 Fe6 C71 -79.8(6) . .
C73 C72 Fe6 C76 -118.5(8) . .
C73 C72 Fe6 C74 -37.8(6) . .
C76 C72 Fe6 C74 80.7(6) . .
C73 C72 Fe6 C69 49.9(13) . .
C76 C72 Fe6 C69 168.4(9) . .
C73 C72 Fe6 C68 78.2(6) . .
C76 C72 Fe6 C68 -163.3(5) . .
C73 C72 Fe6 C70 -168.4(8) . .
C76 C72 Fe6 C70 -49.9(11) . .
C73 C72 Fe6 C67 119.5(5) . .
C76 C72 Fe6 C67 -122.0(5) . .
C75 C74 Fe6 C73 -118.2(9) . .
C73 C74 Fe6 C75 118.2(9) . .
C75 C74 Fe6 C71 40.7(14) . .
C73 C74 Fe6 C71 158.8(10) . .
C75 C74 Fe6 C76 -37.3(6) . .
C73 C74 Fe6 C76 80.9(7) . .
C75 C74 Fe6 C72 -81.3(6) . .
C73 C74 Fe6 C72 36.9(6) . .
C75 C74 Fe6 C69 119.3(6) . .
C73 C74 Fe6 C69 -122.6(6) . .
C75 C74 Fe6 C68 162.6(5) . .
C73 C74 Fe6 C68 -79.3(7) . .
C75 C74 Fe6 C70 77.5(7) . .
C73 C74 Fe6 C70 -164.3(6) . .
C75 C74 Fe6 C67 -161.2(9) . .
C73 C74 Fe6 C67 -43.0(13) . .
C70 C69 Fe6 C73 -164.7(5) . .
C68 C69 Fe6 C73 75.0(6) . .
C70 C69 Fe6 C75 -79.1(6) . .
C68 C69 Fe6 C75 160.6(5) . .
C70 C69 Fe6 C71 37.4(5) . .
C68 C69 Fe6 C71 -82.9(5) . .
C70 C69 Fe6 C76 -42.6(11) . .
C68 C69 Fe6 C76 -162.9(8) . .
C70 C69 Fe6 C72 157.8(10) . .
C68 C69 Fe6 C72 37.5(13) . .
C70 C69 Fe6 C74 -121.6(5) . .
C68 C69 Fe6 C74 118.1(5) . .
C70 C69 Fe6 C68 120.3(7) . .
C68 C69 Fe6 C70 -120.3(7) . .
C70 C69 Fe6 C67 82.0(5) . .
C68 C69 Fe6 C67 -38.3(5) . .
C69 C68 Fe6 C73 -124.4(6) . .
C67 C68 Fe6 C73 117.2(6) . .
C69 C68 Fe6 C75 -49.5(12) . .
C67 C68 Fe6 C75 -167.9(9) . .
C69 C68 Fe6 C71 80.5(5) . .
C67 C68 Fe6 C71 -37.9(5) . .
C69 C68 Fe6 C76 161.8(9) . .
C67 C68 Fe6 C76 43.4(12) . .
C69 C68 Fe6 C72 -166.1(5) . .
C67 C68 Fe6 C72 75.5(6) . .
C69 C68 Fe6 C74 -81.5(7) . .
C67 C68 Fe6 C74 160.1(5) . .
C67 C68 Fe6 C69 -118.4(7) . .
C69 C68 Fe6 C70 36.7(5) . .
C67 C68 Fe6 C70 -81.7(5) . .
C69 C68 Fe6 C67 118.4(7) . .
C69 C70 Fe6 C73 43.3(13) . .
C71 C70 Fe6 C73 163.4(11) . .
C69 C70 Fe6 C75 119.9(5) . .
C71 C70 Fe6 C75 -120.0(5) . .
C69 C70 Fe6 C71 -120.2(7) . .
C69 C70 Fe6 C76 162.5(5) . .
C71 C70 Fe6 C76 -77.4(6) . .
C69 C70 Fe6 C72 -161.3(8) . .
C71 C70 Fe6 C72 -41.2(11) . .
C69 C70 Fe6 C74 78.0(6) . .
C71 C70 Fe6 C74 -161.8(5) . .
C71 C70 Fe6 C69 120.2(7) . .
C69 C70 Fe6 C68 -37.5(5) . .
C71 C70 Fe6 C68 82.7(5) . .
C69 C70 Fe6 C67 -81.7(5) . .
C71 C70 Fe6 C67 38.5(5) . .
C68 C67 Fe6 C73 -81.1(6) . .
C71 C67 Fe6 C73 159.3(6) . .
C65 C67 Fe6 C73 40.2(9) . .
C68 C67 Fe6 C75 167.3(10) . .
C71 C67 Fe6 C75 47.8(12) . .
C65 C67 Fe6 C75 -71.4(14) . .
C68 C67 Fe6 C71 119.5(7) . .
C65 C67 Fe6 C71 -119.2(9) . .
C68 C67 Fe6 C76 -163.2(5) . .
C71 C67 Fe6 C76 77.2(6) . .
C65 C67 Fe6 C76 -42.0(9) . .
C68 C67 Fe6 C72 -122.1(5) . .
C71 C67 Fe6 C72 118.3(5) . .
C65 C67 Fe6 C72 -0.8(8) . .
C68 C67 Fe6 C74 -49.4(12) . .
C71 C67 Fe6 C74 -168.9(10) . .
C65 C67 Fe6 C74 71.9(13) . .
C68 C67 Fe6 C69 38.3(5) . .
C71 C67 Fe6 C69 -81.2(5) . .
C65 C67 Fe6 C69 159.6(8) . .
C71 C67 Fe6 C68 -119.5(7) . .
C65 C67 Fe6 C68 121.3(9) . .
C68 C67 Fe6 C70 81.5(5) . .
C71 C67 Fe6 C70 -38.0(5) . .
C65 C67 Fe6 C70 -157.2(8) . .
C5 C1 P1 C25 90.3(7) . .
C2 C1 P1 C25 -94.0(7) . .
Fe1 C1 P1 C25 178.6(4) . .
C5 C1 P1 C21 -164.5(7) . .
C2 C1 P1 C21 11.2(8) . .
Fe1 C1 P1 C21 -76.2(5) . .
C5 C1 P1 Pd1 -31.9(8) . .
C2 C1 P1 Pd1 143.8(6) . .
Fe1 C1 P1 Pd1 56.4(5) . .
C26 C25 P1 C1 -1.8(9) . .
O2 C25 P1 C1 -177.3(6) . .
C26 C25 P1 C21 -111.0(8) . .
O2 C25 P1 C21 73.4(7) . .
C26 C25 P1 Pd1 124.0(7) . .
O2 C25 P1 Pd1 -51.6(6) . .
C22 C21 P1 C1 -127.2(8) . .
O1 C21 P1 C1 57.2(7) . .
C22 C21 P1 C25 -19.8(9) . .
O1 C21 P1 C25 164.6(6) . .
C22 C21 P1 Pd1 100.7(8) . .
O1 C21 P1 Pd1 -74.8(7) . .
Cl1 Pd1 P1 C1 -113.2(3) . .
P2 Pd1 P1 C1 174(32) . .
Cl2 Pd1 P1 C1 65.4(3) . .
Cl1 Pd1 P1 C25 128.7(3) . .
P2 Pd1 P1 C25 56(2) . .
Cl2 Pd1 P1 C25 -52.7(3) . .
Cl1 Pd1 P1 C21 13.8(3) . .
P2 Pd1 P1 C21 -59(2) . .
Cl2 Pd1 P1 C21 -167.6(3) . .
C54 C53 P2 C49 24.5(9) . .
O4 C53 P2 C49 -161.8(6) . .
C54 C53 P2 C29 132.7(8) . .
O4 C53 P2 C29 -53.7(6) . .
C54 C53 P2 Pd1 -96.6(8) . .
O4 C53 P2 Pd1 77.0(6) . .
O3 C49 P2 C53 -69.8(7) . .
C50 C49 P2 C53 111.4(8) . .
O3 C49 P2 C29 -177.8(6) . .
C50 C49 P2 C29 3.4(9) . .
O3 C49 P2 Pd1 55.1(6) . .
C50 C49 P2 Pd1 -123.7(8) . .
C30 C29 P2 C53 171.2(7) . .
C33 C29 P2 C53 -6.2(8) . .
Fe3 C29 P2 C53 82.5(5) . .
C30 C29 P2 C49 -83.1(7) . .
C33 C29 P2 C49 99.4(7) . .
Fe3 C29 P2 C49 -171.9(4) . .
C30 C29 P2 Pd1 40.6(7) . .
C33 C29 P2 Pd1 -136.9(6) . .
Fe3 C29 P2 Pd1 -48.2(5) . .
Cl1 Pd1 P2 C53 169.5(3) . .
P1 Pd1 P2 C53 -117(2) . .
Cl2 Pd1 P2 C53 -9.0(3) . .
Cl1 Pd1 P2 C49 54.0(3) . .
P1 Pd1 P2 C49 127(2) . .
Cl2 Pd1 P2 C49 -124.5(3) . .
Cl1 Pd1 P2 C29 -66.0(3) . .
P1 Pd1 P2 C29 7(2) . .
Cl2 Pd1 P2 C29 115.5(3) . .
C58 C57 P3 C77 -85.1(7) . .
C61 C57 P3 C77 98.9(7) . .
Fe5 C57 P3 C77 -173.6(4) . .
C58 C57 P3 C81 168.7(7) . .
C61 C57 P3 C81 -7.2(7) . .
Fe5 C57 P3 C81 80.2(5) . .
C58 C57 P3 Pd2 37.1(7) . .
C61 C57 P3 Pd2 -138.8(6) . .
Fe5 C57 P3 Pd2 -51.3(5) . .
C78 C77 P3 C57 1.8(9) . .
O5 C77 P3 C57 176.4(6) . .
C78 C77 P3 C81 110.5(8) . .
O5 C77 P3 C81 -74.9(6) . .
C78 C77 P3 Pd2 -125.5(7) . .
O5 C77 P3 Pd2 49.1(6) . .
C82 C81 P3 C57 127.7(8) . .
O6 C81 P3 C57 -58.1(6) . .
C82 C81 P3 C77 19.3(8) . .
O6 C81 P3 C77 -166.5(6) . .
C82 C81 P3 Pd2 -100.0(8) . .
O6 C81 P3 Pd2 74.1(6) . .
Cl3 Pd2 P3 C57 117.7(3) 2 .
Cl3 Pd2 P3 C57 -62.3(3) . .
P3 Pd2 P3 C57 -46(16) 2 .
Cl3 Pd2 P3 C77 -122.9(3) 2 .
Cl3 Pd2 P3 C77 57.1(3) . .
P3 Pd2 P3 C77 74(16) 2 .
Cl3 Pd2 P3 C81 -8.3(3) 2 .
Cl3 Pd2 P3 C81 171.7(3) . .
P3 Pd2 P3 C81 -172(16) 2 .
Cl8 C86 Cl8 C86 0.000(3) 2_566 2_566
Cl7 C86 Cl8 C86 -133(2) . 2_566
