#------------------------------------------------------------------------------
#$Date: 2016-03-21 10:45:35 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178666 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/77/4077792.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4077792
loop_
_publ_author_name
'Charmant, Jonathan P. H.'
'Forniés, Juan'
'Gómez, Julio'
'Lalinde, Elena'
'Merino, Rosa I.'
'Moreno, M. Teresa'
'Orpen, A. Guy'
_publ_section_title
;
 Unprecedented Pt−Pt Bonded Trimer
 {[Pt2Cu4(C⋮CPh)8]}3Showing Unusual Near-Infrared Luminescence
;
_journal_issue                   17
_journal_name_full               Organometallics
_journal_page_first              3353
_journal_paper_doi               10.1021/om9902030
_journal_volume                  18
_journal_year                    1999
_chemical_formula_sum            'C194 H120 Cl4 Cu12 Pt6'
_chemical_formula_weight         4525.72
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           126
_symmetry_cell_setting           tetragonal
_symmetry_space_group_name_Hall  '-P 4a 2bc'
_symmetry_space_group_name_H-M   'P 4/n n c :2'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   16.1431(19)
_cell_length_b                   16.1431(19)
_cell_length_c                   32.538(3)
_cell_measurement_reflns_used    427
_cell_measurement_temperature    173(2)
_cell_volume                     8479.4(16)
_computing_cell_refinement       'Siemens SMART'
_computing_data_collection       'Siemens SMART'
_computing_data_reduction        'Siemens SAINT'
_computing_molecular_graphics    'Siemens SHELXTL'
_computing_publication_material  'Siemens SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      173(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_method       'Frames each covering 0.3 deg in ω'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0573
_diffrn_reflns_av_sigmaI/netI    0.0261
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_k_max       20
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -42
_diffrn_reflns_number            50480
_diffrn_reflns_theta_full        27.49
_diffrn_reflns_theta_max         27.49
_diffrn_reflns_theta_min         1.78
_diffrn_standards_decay_%        none
_exptl_absorpt_coefficient_mu    6.509
_exptl_absorpt_correction_T_max  0.264
_exptl_absorpt_correction_T_min  0.403
_exptl_absorpt_correction_type
;
  Empirical using SADABS absorption and area detector correction
software
;
_exptl_crystal_colour            'dark violet'
_exptl_crystal_density_diffrn    1.773
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             4336
_exptl_crystal_size_max          0.5
_exptl_crystal_size_mid          0.4
_exptl_crystal_size_min          0.4
_refine_diff_density_max         1.339
_refine_diff_density_min         -1.623
_refine_diff_density_rms         0.178
_refine_ls_extinction_coef       0.00022(4)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   1.662
_refine_ls_hydrogen_treatment
; 
 All hydrogen atoms except those of the solvent were assigned fixed
isotropic
 displacement parameters and assigned to ideal positions.  The solvent
hydrogens 
 were not located.
;
_refine_ls_matrix_type           full
_refine_ls_number_parameters     364
_refine_ls_number_reflns         4877
_refine_ls_number_restraints     18
_refine_ls_restrained_S_all      1.661
_refine_ls_R_factor_all          0.0777
_refine_ls_R_factor_gt           0.0503
_refine_ls_shift/su_max          0.003
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0500P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1342
_refine_ls_wR_factor_ref         0.1414
_reflns_number_gt                3393
_reflns_number_total             4877
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om9902030.cif
_cod_data_source_block           '[1]3'
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Tetragonal' changed to 'tetragonal'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1715 2011-07-08 13:25:40Z adriana 
;
_cod_original_cell_volume        8479.3(16)
_cod_original_sg_symbol_H-M      P4/nnc
_cod_database_code               4077792
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x+1/2, -y+1/2, z'
'-y+1/2, x, z'
'y, -x+1/2, z'
'-x+1/2, y, -z+1/2'
'x, -y+1/2, -z+1/2'
'y, x, -z+1/2'
'-y+1/2, -x+1/2, -z+1/2'
'-x, -y, -z'
'x-1/2, y-1/2, -z'
'y-1/2, -x, -z'
'-y, x-1/2, -z'
'x-1/2, -y, z-1/2'
'-x, y-1/2, z-1/2'
'-y, -x, z-1/2'
'y-1/2, x-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.2500 0.2500 0.810884(16) 0.02234(16) Uani 1 4 d S . .
Pt2 Pt 0.2500 0.2500 0.902945(16) 0.02388(16) Uani 1 4 d S . .
Pt3 Pt 0.2500 0.2500 1.021110(16) 0.02249(16) Uani 1 4 d S . .
Cu1 Cu 0.38076(5) 0.31163(6) 0.96218(3) 0.0258(2) Uani 1 1 d . . .
Cu2 Cu 0.11724(8) 0.2500 0.7500 0.0340(3) Uani 1 2 d S . .
C1 C 0.2906(6) 0.3677(5) 0.8072(2) 0.0335(19) Uani 1 1 d . . .
C2 C 0.3161(6) 0.4386(5) 0.7997(2) 0.0346(19) Uani 1 1 d . A .
C3 C 0.3544(6) 0.5163(5) 0.7973(3) 0.042(2) Uani 1 1 d . . .
C4 C 0.3106(12) 0.5865(11) 0.8200(6) 0.048(5) Uani 0.50 1 d P A 1
H4 H 0.2606 0.5781 0.8348 0.058 Uiso 0.50 1 calc PR A 1
C4' C 0.3211(17) 0.5798(11) 0.7781(6) 0.063(7) Uani 0.50 1 d P A 2
H4' H 0.2681 0.5741 0.7657 0.076 Uiso 0.50 1 calc PR A 2
C5 C 0.350(2) 0.6662(12) 0.8174(7) 0.090(10) Uani 0.50 1 d P A 1
H5 H 0.3281 0.7130 0.8314 0.108 Uiso 0.50 1 calc PR A 1
C5' C 0.3647(15) 0.6595(13) 0.7757(7) 0.059(6) Uani 0.50 1 d P A 2
H5' H 0.3414 0.7021 0.7592 0.071 Uiso 0.50 1 calc PR A 2
C6 C 0.4253(9) 0.6728(7) 0.7926(4) 0.071(4) Uani 1 1 d . . .
H6 H 0.4619 0.7189 0.7939 0.085 Uiso 1 1 calc R A 1
C7 C 0.4367(14) 0.6127(17) 0.7696(7) 0.067(7) Uani 0.50 1 d P A 1
H7 H 0.4723 0.6227 0.7469 0.080 Uiso 0.50 1 calc PR A 1
C7' C 0.4793(18) 0.6050(18) 0.8119(7) 0.086(9) Uani 0.50 1 d P A 2
H7' H 0.5340 0.6137 0.8218 0.103 Uiso 0.50 1 calc PR A 2
C8 C 0.4072(13) 0.5383(12) 0.7721(6) 0.050(5) Uani 0.50 1 d P A 1
H8 H 0.4275 0.4980 0.7534 0.060 Uiso 0.50 1 calc PR A 1
C8' C 0.4390(12) 0.5304(12) 0.8133(7) 0.051(5) Uani 0.50 1 d P A 2
H8' H 0.4672 0.4847 0.8253 0.062 Uiso 0.50 1 calc PR A 2
C9 C 0.1978(5) 0.3631(5) 0.9017(2) 0.0270(17) Uani 1 1 d . . .
C10 C 0.1671(4) 0.4313(5) 0.9019(2) 0.0275(17) Uani 1 1 d . B .
C11 C 0.1301(5) 0.5098(5) 0.8900(3) 0.0343(19) Uani 1 1 d . . .
C12 C 0.0567(11) 0.5391(11) 0.9071(5) 0.039(4) Uani 0.50 1 d P B 1
H12 H 0.0280 0.5047 0.9261 0.047 Uiso 0.50 1 calc PR B 1
C12' C 0.1352(11) 0.5837(11) 0.9151(6) 0.042(5) Uani 0.50 1 d P B 2
H12' H 0.1689 0.5849 0.9390 0.051 Uiso 0.50 1 calc PR B 2
C13 C 0.0233(14) 0.6156(14) 0.8978(7) 0.056(6) Uani 0.50 1 d P B 1
H13 H -0.0214 0.6383 0.9130 0.067 Uiso 0.50 1 calc PR B 1
C13' C 0.0885(16) 0.6546(11) 0.9032(8) 0.064(7) Uani 0.50 1 d P B 2
H13' H 0.0799 0.6993 0.9217 0.077 Uiso 0.50 1 calc PR B 2
C14 C 0.0575(8) 0.6563(7) 0.8659(4) 0.067(3) Uani 1 1 d . . .
H14 H 0.0296 0.7039 0.8557 0.081 Uiso 1 1 calc R B 1
C15 C 0.1304(18) 0.6333(13) 0.8473(6) 0.067(7) Uani 0.50 1 d P B 1
H15 H 0.1565 0.6675 0.8274 0.081 Uiso 0.50 1 calc PR B 1
C15' C 0.0481(19) 0.5868(14) 0.8399(8) 0.082(8) Uani 0.50 1 d P B 2
H15' H 0.0152 0.5882 0.8157 0.098 Uiso 0.50 1 calc PR B 2
C16 C 0.1653(14) 0.5554(10) 0.8593(5) 0.047(5) Uani 0.50 1 d P B 1
H16 H 0.2135 0.5353 0.8458 0.057 Uiso 0.50 1 calc PR B 1
C16' C 0.0896(12) 0.5178(12) 0.8520(6) 0.045(5) Uani 0.50 1 d P B 2
H16' H 0.0914 0.4721 0.8337 0.054 Uiso 0.50 1 calc PR B 2
C17 C 0.2001(5) 0.3630(5) 1.0222(2) 0.0331(19) Uani 1 1 d . . .
C18 C 0.1672(5) 0.4326(5) 1.0224(2) 0.0329(19) Uani 1 1 d . C .
C19 C 0.1305(4) 0.5113(5) 1.0324(3) 0.0295(17) Uani 1 1 d . . .
C20 C 0.0658(10) 0.5478(10) 1.0076(5) 0.031(4) Uani 0.50 1 d P C 1
H20 H 0.0458 0.5198 0.9839 0.037 Uiso 0.50 1 calc PR C 1
C20' C 0.1308(13) 0.5756(10) 1.0058(6) 0.047(5) Uani 0.50 1 d P C 2
H20' H 0.1617 0.5728 0.9811 0.056 Uiso 0.50 1 calc PR C 2
C21 C 0.0326(13) 0.6255(13) 1.0188(7) 0.042(5) Uani 0.50 1 d P C 1
H21 H -0.0038 0.6546 1.0010 0.050 Uiso 0.50 1 calc PR C 1
C21' C 0.085(2) 0.6458(16) 1.0153(12) 0.104(14) Uani 0.50 1 d P C 2
H21' H 0.0764 0.6873 0.9950 0.125 Uiso 0.50 1 calc PR C 2
C22 C 0.0532(8) 0.6550(8) 1.0536(5) 0.077(4) Uani 1 1 d . . .
H22 H 0.0267 0.7046 1.0622 0.093 Uiso 1 1 calc R C 1
C23 C 0.1172(13) 0.6169(13) 1.0825(6) 0.048(5) Uani 0.50 1 d P C 1
H23 H 0.1299 0.6396 1.1087 0.058 Uiso 0.50 1 calc PR C 1
C23' C 0.0543(15) 0.5933(17) 1.0794(7) 0.063(7) Uani 0.50 1 d P C 2
H23' H 0.0297 0.5999 1.1058 0.075 Uiso 0.50 1 calc PR C 2
C24 C 0.1546(9) 0.5473(8) 1.0675(4) 0.050(5) Uani 0.50 1 d P C 1
H24 H 0.1992 0.5236 1.0825 0.060 Uiso 0.50 1 calc PR C 1
C24' C 0.0902(9) 0.5193(8) 1.0694(4) 0.055(6) Uani 0.50 1 d PR C 2
H24' H 0.0844 0.4738 1.0877 0.066 Uiso 0.50 1 d PR C 2
C25 C 0.7290(9) 0.7487(8) 0.8714(4) 0.27(8) Uani 0.13 1 d PRU . .
C26 C 0.7292(9) 0.7487(8) 0.8312(4) 0.9(3) Uani 0.13 1 d PRU . .
Cl1 Cl 0.6455(9) 0.7120(8) 0.8549(4) 0.401(16) Uani 0.50 1 d PRU . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cu Cu 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C1 Pt1 C1 89.80(3) 4 2
C1 Pt1 C1 173.3(4) 4 3
C1 Pt1 C1 89.80(3) 2 3
C1 Pt1 C1 89.80(3) 4 .
C1 Pt1 C1 173.3(4) 2 .
C1 Pt1 C1 89.80(3) 3 .
C1 Pt1 Cu2 42.9(2) 4 2
C1 Pt1 Cu2 101.5(2) 2 2
C1 Pt1 Cu2 130.8(2) 3 2
C1 Pt1 Cu2 73.8(2) . 2
C1 Pt1 Cu2 73.8(2) 4 3
C1 Pt1 Cu2 42.9(2) 2 3
C1 Pt1 Cu2 101.5(2) 3 3
C1 Pt1 Cu2 130.8(2) . 3
Cu2 Pt1 Cu2 62.56(2) 2 3
C1 Pt1 Cu2 101.5(2) 4 4
C1 Pt1 Cu2 130.8(2) 2 4
C1 Pt1 Cu2 73.8(2) 3 4
C1 Pt1 Cu2 42.9(2) . 4
Cu2 Pt1 Cu2 62.56(2) 2 4
Cu2 Pt1 Cu2 94.50(4) 3 4
C1 Pt1 Cu2 130.8(2) 4 .
C1 Pt1 Cu2 73.8(2) 2 .
C1 Pt1 Cu2 42.9(2) 3 .
C1 Pt1 Cu2 101.5(2) . .
Cu2 Pt1 Cu2 94.50(4) 2 .
Cu2 Pt1 Cu2 62.56(2) 3 .
Cu2 Pt1 Cu2 62.56(2) 4 .
C1 Pt1 Pt2 93.4(2) 4 .
C1 Pt1 Pt2 93.4(2) 2 .
C1 Pt1 Pt2 93.4(2) 3 .
C1 Pt1 Pt2 93.4(2) . .
Cu2 Pt1 Pt2 132.75(2) 2 .
Cu2 Pt1 Pt2 132.75(2) 3 .
Cu2 Pt1 Pt2 132.75(2) 4 .
Cu2 Pt1 Pt2 132.750(19) . .
C1 Pt1 Pt1 86.6(2) 4 8_556
C1 Pt1 Pt1 86.6(2) 2 8_556
C1 Pt1 Pt1 86.6(2) 3 8_556
C1 Pt1 Pt1 86.6(2) . 8_556
Cu2 Pt1 Pt1 47.250(19) 2 8_556
Cu2 Pt1 Pt1 47.25(2) 3 8_556
Cu2 Pt1 Pt1 47.250(19) 4 8_556
Cu2 Pt1 Pt1 47.25(2) . 8_556
Pt2 Pt1 Pt1 180.0 . 8_556
C9 Pt2 C9 89.977(9) 4 2
C9 Pt2 C9 177.7(4) 4 3
C9 Pt2 C9 89.976(11) 2 3
C9 Pt2 C9 89.977(10) 4 .
C9 Pt2 C9 177.7(4) 2 .
C9 Pt2 C9 89.976(9) 3 .
C9 Pt2 Pt1 88.8(2) 4 .
C9 Pt2 Pt1 88.8(2) 2 .
C9 Pt2 Pt1 88.8(2) 3 .
C9 Pt2 Pt1 88.8(2) . .
C9 Pt2 Cu1 40.7(2) 4 .
C9 Pt2 Cu1 91.1(2) 2 .
C9 Pt2 Cu1 141.6(2) 3 .
C9 Pt2 Cu1 90.4(2) . .
Pt1 Pt2 Cu1 129.557(19) . .
C9 Pt2 Cu1 91.1(2) 4 3
C9 Pt2 Cu1 141.6(2) 2 3
C9 Pt2 Cu1 90.4(2) 3 3
C9 Pt2 Cu1 40.7(2) . 3
Pt1 Pt2 Cu1 129.557(19) . 3
Cu1 Pt2 Cu1 66.07(2) . 3
C9 Pt2 Cu1 90.4(2) 4 4
C9 Pt2 Cu1 40.7(2) 2 4
C9 Pt2 Cu1 91.1(2) 3 4
C9 Pt2 Cu1 141.6(2) . 4
Pt1 Pt2 Cu1 129.557(19) . 4
Cu1 Pt2 Cu1 66.07(2) . 4
Cu1 Pt2 Cu1 100.89(4) 3 4
C9 Pt2 Cu1 141.6(2) 4 2
C9 Pt2 Cu1 90.4(2) 2 2
C9 Pt2 Cu1 40.7(2) 3 2
C9 Pt2 Cu1 91.1(2) . 2
Pt1 Pt2 Cu1 129.557(19) . 2
Cu1 Pt2 Cu1 100.89(4) . 2
Cu1 Pt2 Cu1 66.07(2) 3 2
Cu1 Pt2 Cu1 66.07(2) 4 2
C9 Pt2 Pt3 91.2(2) 4 .
C9 Pt2 Pt3 91.2(2) 2 .
C9 Pt2 Pt3 91.2(2) 3 .
C9 Pt2 Pt3 91.2(2) . .
Pt1 Pt2 Pt3 180.0 . .
Cu1 Pt2 Pt3 50.443(19) . .
Cu1 Pt2 Pt3 50.443(18) 3 .
Cu1 Pt2 Pt3 50.443(19) 4 .
Cu1 Pt2 Pt3 50.443(19) 2 .
C17 Pt3 C17 89.983(9) 4 2
C17 Pt3 C17 178.0(4) 4 3
C17 Pt3 C17 89.983(10) 2 3
C17 Pt3 C17 89.983(10) 4 .
C17 Pt3 C17 178.0(4) 2 .
C17 Pt3 C17 89.983(9) 3 .
C17 Pt3 Cu1 141.6(2) 4 2
C17 Pt3 Cu1 89.5(2) 2 2
C17 Pt3 Cu1 40.4(2) 3 2
C17 Pt3 Cu1 91.7(2) . 2
C17 Pt3 Cu1 89.5(2) 4 4
C17 Pt3 Cu1 40.4(2) 2 4
C17 Pt3 Cu1 91.7(2) 3 4
C17 Pt3 Cu1 141.6(2) . 4
Cu1 Pt3 Cu1 66.233(19) 2 4
C17 Pt3 Cu1 40.4(2) 4 .
C17 Pt3 Cu1 91.7(2) 2 .
C17 Pt3 Cu1 141.6(2) 3 .
C17 Pt3 Cu1 89.5(2) . .
Cu1 Pt3 Cu1 101.18(4) 2 .
Cu1 Pt3 Cu1 66.233(19) 4 .
C17 Pt3 Cu1 91.7(2) 4 3
C17 Pt3 Cu1 141.6(2) 2 3
C17 Pt3 Cu1 89.5(2) 3 3
C17 Pt3 Cu1 40.4(2) . 3
Cu1 Pt3 Cu1 66.23(2) 2 3
Cu1 Pt3 Cu1 101.18(4) 4 3
Cu1 Pt3 Cu1 66.233(19) . 3
C17 Pt3 Pt2 91.0(2) 4 .
C17 Pt3 Pt2 91.0(2) 2 .
C17 Pt3 Pt2 91.0(2) 3 .
C17 Pt3 Pt2 91.0(2) . .
Cu1 Pt3 Pt2 50.592(18) 2 .
Cu1 Pt3 Pt2 50.592(18) 4 .
Cu1 Pt3 Pt2 50.592(18) . .
Cu1 Pt3 Pt2 50.592(18) 3 .
C17 Cu1 C9 160.7(3) 4 4
C17 Cu1 C10 165.4(3) 4 4
C9 Cu1 C10 33.6(3) 4 4
C17 Cu1 C18 34.6(3) 4 4
C9 Cu1 C18 164.5(3) 4 4
C10 Cu1 C18 131.0(3) 4 4
C17 Cu1 Pt3 40.7(2) 4 .
C9 Cu1 Pt3 120.1(2) 4 .
C10 Cu1 Pt3 153.6(2) 4 .
C18 Cu1 Pt3 75.3(2) 4 .
C17 Cu1 Pt2 119.6(2) 4 .
C9 Cu1 Pt2 41.1(2) 4 .
C10 Cu1 Pt2 74.7(2) 4 .
C18 Cu1 Pt2 154.3(2) 4 .
Pt3 Cu1 Pt2 78.96(3) . .
C17 Cu1 Cu1 82.0(2) 4 4
C9 Cu1 Cu1 83.1(2) 4 4
C10 Cu1 Cu1 106.1(2) 4 4
C18 Cu1 Cu1 106.3(2) 4 4
Pt3 Cu1 Cu1 56.884(10) . 4
Pt2 Cu1 Cu1 56.963(10) . 4
C17 Cu1 Cu1 84.0(3) 4 3
C9 Cu1 Cu1 83.8(2) 4 3
C10 Cu1 Cu1 107.62(19) 4 3
C18 Cu1 Cu1 108.2(2) 4 3
Pt3 Cu1 Cu1 56.884(10) . 3
Pt2 Cu1 Cu1 56.963(10) . 3
Cu1 Cu1 Cu1 90.0 4 3
C1 Cu2 C1 166.0(5) 3 8_556
C1 Cu2 C2 157.6(3) 3 8_556
C1 Cu2 C2 34.7(3) 8_556 8_556
C1 Cu2 C2 34.7(3) 3 3
C1 Cu2 C2 157.6(3) 8_556 3
C2 Cu2 C2 130.1(4) 8_556 3
C1 Cu2 Pt1 43.5(2) 3 .
C1 Cu2 Pt1 123.1(2) 8_556 .
C2 Cu2 Pt1 145.4(2) 8_556 .
C2 Cu2 Pt1 78.2(2) 3 .
C1 Cu2 Pt1 123.1(2) 3 5_556
C1 Cu2 Pt1 43.5(2) 8_556 5_556
C2 Cu2 Pt1 78.2(2) 8_556 5_556
C2 Cu2 Pt1 145.4(2) 3 5_556
Pt1 Cu2 Pt1 85.50(4) . 5_556
C1 Cu2 Pt1 123.1(2) 3 8_556
C1 Cu2 Pt1 43.5(2) 8_556 8_556
C2 Cu2 Pt1 78.2(2) 8_556 8_556
C2 Cu2 Pt1 145.4(2) 3 8_556
Pt1 Cu2 Pt1 85.50(4) . 8_556
Pt1 Cu2 Pt1 0.000(15) 5_556 8_556
C1 Cu2 Cu2 71.4(3) 3 4
C1 Cu2 Cu2 98.4(2) 8_556 4
C2 Cu2 Cu2 130.6(2) 8_556 4
C2 Cu2 Cu2 86.9(2) 3 4
Pt1 Cu2 Cu2 58.718(11) . 4
Pt1 Cu2 Cu2 58.718(11) 5_556 4
Pt1 Cu2 Cu2 58.718(11) 8_556 4
C1 Cu2 Cu2 98.4(2) 3 3
C1 Cu2 Cu2 71.4(3) 8_556 3
C2 Cu2 Cu2 86.9(2) 8_556 3
C2 Cu2 Cu2 130.6(2) 3 3
Pt1 Cu2 Cu2 58.718(11) . 3
Pt1 Cu2 Cu2 58.718(11) 5_556 3
Pt1 Cu2 Cu2 58.718(11) 8_556 3
Cu2 Cu2 Cu2 90.0 4 3
C2 C1 Cu2 79.2(6) . 4
C2 C1 Pt1 172.0(7) . .
Cu2 C1 Pt1 93.6(3) 4 .
C1 C2 C3 169.6(9) . .
C1 C2 Cu2 66.1(5) . 4
C3 C2 Cu2 123.7(6) . 4
C8 C3 C4' 75.1(15) . .
C8 C3 C2 126.8(12) . .
C4' C3 C2 123.0(12) . .
C8 C3 C8' 63.3(14) . .
C4' C3 C8' 115.1(14) . .
C2 C3 C8' 121.7(11) . .
C8 C3 C4 115.3(12) . .
C4' C3 C4 57.4(12) . .
C2 C3 C4 115.7(10) . .
C8' C3 C4 98.3(11) . .
C5 C4 C3 115.5(16) . .
C3 C4' C5' 121(2) . .
C4 C5 C6 117.7(18) . .
C6 C5' C4' 123(2) . .
C5' C6 C7 71.9(16) . .
C5' C6 C5 62.7(17) . .
C7 C6 C5 113.6(16) . .
C5' C6 C7' 123.3(17) . .
C7 C6 C7' 66.7(16) . .
C5 C6 C7' 101.1(16) . .
C6 C7 C8 129(2) . .
C8' C7' C6 112(2) . .
C3 C8 C7 124(2) . .
C7' C8' C3 124(2) . .
C10 C9 Cu1 80.5(5) . 3
C10 C9 Pt2 178.5(7) . .
Cu1 C9 Pt2 98.1(3) 3 .
C9 C10 C11 164.4(8) . .
C9 C10 Cu1 66.0(5) . 3
C11 C10 Cu1 129.6(6) . 3
C16 C11 C12 117.6(13) . .
C16 C11 C16' 60.0(11) . .
C12 C11 C16' 85.6(12) . .
C16 C11 C12' 86.8(11) . .
C12 C11 C12' 62.8(10) . .
C16' C11 C12' 116.5(13) . .
C16 C11 C10 119.5(11) . .
C12 C11 C10 122.7(11) . .
C16' C11 C10 120.3(11) . .
C12' C11 C10 123.2(10) . .
C13 C12 C11 123.2(17) . .
C13' C12' C11 118.6(18) . .
C14 C13 C12 116.5(18) . .
C14 C13' C12' 118.1(18) . .
C13' C14 C13 55.5(13) . .
C13' C14 C15 94.4(17) . .
C13 C14 C15 124.0(15) . .
C13' C14 C15' 125.2(15) . .
C13 C14 C15' 91.6(17) . .
C15 C14 C15' 67.3(16) . .
C14 C15 C16 117.0(19) . .
C16' C15' C14 115(2) . .
C11 C16 C15 120.6(18) . .
C15' C16' C11 124(2) . .
C18 C17 Cu1 80.5(5) . 3
C18 C17 Pt3 178.4(8) . .
Cu1 C17 Pt3 98.9(3) 3 .
C17 C18 C19 167.2(8) . .
C17 C18 Cu1 64.9(5) . 3
C19 C18 Cu1 127.9(6) . 3
C24 C19 C20' 102.2(12) . .
C24 C19 C24' 49.4(5) . .
C20' C19 C24' 119.3(11) . .
C24 C19 C18 117.2(9) . .
C20' C19 C18 122.1(11) . .
C24' C19 C18 118.5(9) . .
C24 C19 C20 120.6(10) . .
C20' C19 C20 48.0(10) . .
C24' C19 C20 96.2(10) . .
C18 C19 C20 122.0(9) . .
C21 C20 C19 119.5(16) . .
C19 C20' C21' 119(2) . .
C22 C21 C20 117.6(18) . .
C22 C21' C20' 120(3) . .
C21 C22 C23' 106.9(16) . .
C21 C22 C21' 40.7(13) . .
C23' C22 C21' 120.2(17) . .
C21 C22 C23 125.0(14) . .
C23' C22 C23 44.4(12) . .
C21' C22 C23 105.3(15) . .
C24 C23 C22 114.2(15) . .
C22 C23' C24' 121.3(17) . .
C19 C24 C23 122.3(14) . .
C23' C24' C19 119.5(15) . .
C25 C25 C25 90.0 3_655 4_565
C25 C25 C25 45.0 3_655 2_665
C25 C25 C25 45.0 4_565 2_665
C25 C25 C26 89.9 3_655 .
C25 C25 C26 89.9 4_565 .
C25 C25 C26 89.9 2_665 .
C25 C25 C26 89.9 3_655 4_565
C25 C25 C26 70.0(8) 4_565 4_565
C25 C25 C26 75.9(6) 2_665 4_565
C26 C25 C26 19.9(8) . 4_565
C25 C25 C26 70.0(8) 3_655 3_655
C25 C25 C26 89.9 4_565 3_655
C25 C25 C26 75.9(6) 2_665 3_655
C26 C25 C26 19.9(8) . 3_655
C26 C25 C26 27.9(12) 4_565 3_655
C25 C25 C26 71.1(7) 3_655 2_665
C25 C25 C26 71.1(7) 4_565 2_665
C25 C25 C26 62.7(11) 2_665 2_665
C26 C25 C26 27.1(11) . 2_665
C26 C25 C26 18.8(7) 4_565 2_665
C26 C25 C26 18.8(7) 3_655 2_665
C25 C25 Cl1 113(2) 3_655 .
C25 C25 Cl1 148.6(16) 4_565 .
C25 C25 Cl1 151.8(15) 2_665 .
C26 C25 Cl1 70.1 . .
C26 C25 Cl1 88.4(8) 4_565 .
C26 C25 Cl1 79.3(8) 3_655 .
C26 C25 Cl1 95.7(11) 2_665 .
C25 C25 Cl1 137.7(17) 3_655 4_565
C25 C25 Cl1 52.8(19) 4_565 4_565
C25 C25 Cl1 95.5(19) 2_665 4_565
C26 C25 Cl1 72.8(2) . 4_565
C26 C25 Cl1 61.0(7) 4_565 4_565
C26 C25 Cl1 88.5(7) 3_655 4_565
C26 C25 Cl1 77.3(7) 2_665 4_565
Cl1 C25 Cl1 97.2(6) . 4_565
C25 C25 Cl1 24.2(13) 3_655 3_655
C25 C25 Cl1 108.0(16) 4_565 3_655
C25 C25 Cl1 64.7(16) 2_665 3_655
C26 C25 Cl1 74.32(16) . 3_655
C26 C25 Cl1 81.5(7) 4_565 3_655
C26 C25 Cl1 55.6(6) 3_655 3_655
C26 C25 Cl1 64.2(7) 2_665 3_655
Cl1 C25 Cl1 90.1(5) . 3_655
Cl1 C25 Cl1 141.40(15) 4_565 3_655
C25 C25 Cl1 60.0(15) 3_655 2_665
C25 C25 Cl1 33.9(14) 4_565 2_665
C25 C25 Cl1 19.8(11) 2_665 2_665
C26 C25 Cl1 75.7(2) . 2_665
C26 C25 Cl1 59.0(5) 4_565 2_665
C26 C25 Cl1 66.2(5) 3_655 2_665
C26 C25 Cl1 49.5(9) 2_665 2_665
Cl1 C25 Cl1 145.3(2) . 2_665
Cl1 C25 Cl1 78.2(4) 4_565 2_665
Cl1 C25 Cl1 74.6(3) 3_655 2_665
C26 C26 C26 90.0 3_655 4_565
C26 C26 C26 45.0 3_655 2_665
C26 C26 C26 45.0 4_565 2_665
C26 C26 C25 90.1 3_655 .
C26 C26 C25 90.1 4_565 .
C26 C26 C25 90.1 2_665 .
C26 C26 C25 70.0(8) 3_655 3_655
C26 C26 C25 90.1 4_565 3_655
C26 C26 C25 76.1(6) 2_665 3_655
C25 C26 C25 20.1(8) . 3_655
C26 C26 C25 90.1 3_655 4_565
C26 C26 C25 70.0(8) 4_565 4_565
C26 C26 C25 76.0(6) 2_665 4_565
C25 C26 C25 20.1(8) . 4_565
C25 C26 C25 28.2(12) 3_655 4_565
C26 C26 C25 71.1(7) 3_655 2_665
C26 C26 C25 71.1(7) 4_565 2_665
C26 C26 C25 62.7(11) 2_665 2_665
C25 C26 C25 27.4(11) . 2_665
C25 C26 C25 19.0(7) 3_655 2_665
C25 C26 C25 19.0(7) 4_565 2_665
C26 C26 Cl1 111.8(19) 3_655 .
C26 C26 Cl1 143.6(14) 4_565 .
C26 C26 Cl1 146.3(12) 2_665 .
C25 C26 Cl1 62.3 . .
C25 C26 Cl1 72.0(8) 3_655 .
C25 C26 Cl1 80.8(8) 4_565 .
C25 C26 Cl1 88.2(11) 2_665 .
C26 C26 Cl1 135.0(15) 3_655 4_565
C26 C26 Cl1 54.7(18) 4_565 4_565
C26 C26 Cl1 95.3(18) 2_665 4_565
C25 C26 Cl1 65.9(3) . 4_565
C25 C26 Cl1 82.0(7) 3_655 4_565
C25 C26 Cl1 54.4(6) 4_565 4_565
C25 C26 Cl1 71.3(6) 2_665 4_565
Cl1 C26 Cl1 90.7(5) . 4_565
C26 C26 Cl1 28.6(11) 3_655 3_655
C26 C26 Cl1 107.4(15) 4_565 3_655
C26 C26 Cl1 65.8(15) 2_665 3_655
C25 C26 Cl1 68.1(2) . 3_655
C25 C26 Cl1 49.3(6) 3_655 3_655
C25 C26 Cl1 75.7(7) 4_565 3_655
C25 C26 Cl1 58.7(7) 2_665 3_655
Cl1 C26 Cl1 85.0(5) . 3_655
Cl1 C26 Cl1 129.94(8) 4_565 3_655
C26 C26 Cl1 61.0(15) 3_655 2_665
C26 C26 Cl1 36.4(12) 4_565 2_665
C26 C26 Cl1 24.2(10) 2_665 2_665
C25 C26 Cl1 70.1(3) . 2_665
C25 C26 Cl1 60.9(5) 3_655 2_665
C25 C26 Cl1 53.4(5) 4_565 2_665
C25 C26 Cl1 43.8(8) 2_665 2_665
Cl1 C26 Cl1 132.0(3) . 2_665
Cl1 C26 Cl1 74.9(3) 4_565 2_665
Cl1 C26 Cl1 71.8(2) 3_655 2_665
C25 Cl1 C26 47.6 . .
C25 Cl1 C25 14.1(6) . 3_655
C26 Cl1 C25 47.0(2) . 3_655
C25 Cl1 C26 46.2(3) . 3_655
C26 Cl1 C26 13.5(6) . 3_655
C25 Cl1 C26 41.3(5) 3_655 3_655
C25 Cl1 C25 7.2(5) . 4_565
C26 Cl1 C25 43.61(16) . 4_565
C25 Cl1 C25 19.8(8) 3_655 4_565
C26 Cl1 C25 44.41(7) 3_655 4_565
C25 Cl1 C26 42.3(2) . 4_565
C26 Cl1 C26 7.8(4) . 4_565
C25 Cl1 C26 44.0 3_655 4_565
C26 Cl1 C26 18.9(8) 3_655 4_565
C25 Cl1 C26 37.5(4) 4_565 4_565
C25 Cl1 C25 8.4(5) . 2_665
C26 Cl1 C25 42.2(2) . 2_665
C25 Cl1 C25 8.5(5) 3_655 2_665
C26 Cl1 C25 39.0(3) 3_655 2_665
C25 Cl1 C25 12.0(4) 4_565 2_665
C26 Cl1 C25 38.1(3) 4_565 2_665
C25 Cl1 C26 40.5(3) . 2_665
C26 Cl1 C26 9.5(4) . 2_665
C25 Cl1 C26 38.1(3) 3_655 2_665
C26 Cl1 C26 8.6(4) 3_655 2_665
C25 Cl1 C26 37.6(3) 4_565 2_665
C26 Cl1 C26 11.6(4) 4_565 2_665
C25 Cl1 C26 34.2(5) 2_665 2_665
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pt1 C1 2.014(8) 4
Pt1 C1 2.014(8) 2
Pt1 C1 2.014(8) 3
Pt1 C1 2.014(8) .
Pt1 Cu2 2.9184(10) 2
Pt1 Cu2 2.9184(10) 3
Pt1 Cu2 2.9184(10) 4
Pt1 Cu2 2.9184(10) .
Pt1 Pt2 2.9955(8) .
Pt1 Pt1 3.9620(11) 8_556
Pt2 C9 2.012(7) 4
Pt2 C9 2.012(7) 2
Pt2 C9 2.012(7) 3
Pt2 C9 2.012(7) .
Pt2 Cu1 3.0266(10) .
Pt2 Cu1 3.0266(9) 3
Pt2 Cu1 3.0266(9) 4
Pt2 Cu1 3.0267(9) 2
Pt2 Pt3 3.8448(8) .
Pt3 C17 1.994(8) 4
Pt3 C17 1.994(8) 2
Pt3 C17 1.994(8) 3
Pt3 C17 1.994(8) .
Pt3 Cu1 3.0202(10) 2
Pt3 Cu1 3.0202(9) 4
Pt3 Cu1 3.0202(10) .
Pt3 Cu1 3.0202(10) 3
Cu1 C17 1.982(8) 4
Cu1 C9 1.995(7) 4
Cu1 C10 2.153(8) 4
Cu1 C18 2.158(8) 4
Cu1 Cu1 3.3001(13) 4
Cu1 Cu1 3.3001(13) 3
Cu2 C1 1.990(8) 3
Cu2 C1 1.990(8) 8_556
Cu2 C2 2.137(8) 8_556
Cu2 C2 2.137(8) 3
Cu2 Pt1 2.9184(10) 5_556
Cu2 Pt1 2.9184(10) 8_556
Cu2 Cu2 3.0308(19) 4
Cu2 Cu2 3.0308(19) 3
C1 C2 1.240(11) .
C1 Cu2 1.990(8) 4
C2 C3 1.401(11) .
C2 Cu2 2.137(8) 4
C3 C8 1.24(2) .
C3 C4' 1.32(2) .
C3 C8' 1.48(2) .
C3 C4 1.53(2) .
C4 C5 1.44(3) .
C4' C5' 1.47(3) .
C5 C6 1.46(3) .
C5' C6 1.14(2) .
C6 C7 1.24(3) .
C6 C7' 1.54(3) .
C7 C8 1.30(3) .
C7' C8' 1.37(3) .
C9 C10 1.207(10) .
C9 Cu1 1.995(7) 3
C10 C11 1.453(11) .
C10 Cu1 2.153(8) 3
C11 C16 1.365(19) .
C11 C12 1.392(18) .
C11 C16' 1.405(19) .
C11 C12' 1.45(2) .
C12 C13 1.38(3) .
C12' C13' 1.42(3) .
C13 C14 1.35(2) .
C13' C14 1.31(3) .
C14 C15 1.38(3) .
C14 C15' 1.41(3) .
C15 C16 1.43(3) .
C15' C16' 1.36(3) .
C17 C18 1.244(11) .
C17 Cu1 1.982(8) 3
C18 C19 1.438(10) .
C18 Cu1 2.158(8) 3
C19 C24 1.338(14) .
C19 C20' 1.352(19) .
C19 C24' 1.374(15) .
C19 C20 1.447(17) .
C20 C21 1.41(2) .
C20' C21' 1.39(3) .
C21 C22 1.27(3) .
C21' C22 1.36(4) .
C22 C23' 1.30(3) .
C22 C23 1.53(2) .
C23 C24 1.37(2) .
C23' C24' 1.37(3) .
C25 C25 0.48(2) 3_655
C25 C25 0.48(2) 4_565
C25 C25 0.68(3) 2_665
C25 C26 1.3080 .
C25 C26 1.392(8) 4_565
C25 C26 1.392(7) 3_655
C25 C26 1.472(14) 2_665
C25 Cl1 1.5678 .
C25 Cl1 1.81(2) 4_565
C25 Cl1 1.993(19) 3_655
C25 Cl1 2.19(3) 2_665
C26 C26 0.47(2) 3_655
C26 C26 0.47(2) 4_565
C26 C26 0.67(3) 2_665
C26 C25 1.392(7) 3_655
C26 C25 1.392(8) 4_565
C26 C25 1.472(14) 2_665
C26 Cl1 1.6658 .
C26 Cl1 1.89(2) 4_565
C26 Cl1 2.067(19) 3_655
C26 Cl1 2.26(3) 2_665
Cl1 C25 1.81(2) 3_655
Cl1 C26 1.89(2) 3_655
Cl1 C25 1.99(2) 4_565
Cl1 C26 2.067(19) 4_565
Cl1 C25 2.19(3) 2_665
Cl1 C26 2.26(3) 2_665
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
C1 Pt1 Pt2 C9 43.8(4) 4 . 4
C1 Pt1 Pt2 C9 133.8(4) 2 . 4
C1 Pt1 Pt2 C9 -136.2(4) 3 . 4
C1 Pt1 Pt2 C9 -46.2(4) . . 4
Cu2 Pt1 Pt2 C9 24.8(2) 2 . 4
Cu2 Pt1 Pt2 C9 114.8(2) 3 . 4
Cu2 Pt1 Pt2 C9 -65.2(2) 4 . 4
Cu2 Pt1 Pt2 C9 -155.2(2) . . 4
Pt1 Pt1 Pt2 C9 160(12) 8_556 . 4
C1 Pt1 Pt2 C9 -46.2(4) 4 . 2
C1 Pt1 Pt2 C9 43.8(4) 2 . 2
C1 Pt1 Pt2 C9 133.8(4) 3 . 2
C1 Pt1 Pt2 C9 -136.2(4) . . 2
Cu2 Pt1 Pt2 C9 -65.2(2) 2 . 2
Cu2 Pt1 Pt2 C9 24.8(2) 3 . 2
Cu2 Pt1 Pt2 C9 -155.2(2) 4 . 2
Cu2 Pt1 Pt2 C9 114.8(2) . . 2
Pt1 Pt1 Pt2 C9 70(12) 8_556 . 2
C1 Pt1 Pt2 C9 -136.2(4) 4 . 3
C1 Pt1 Pt2 C9 -46.2(4) 2 . 3
C1 Pt1 Pt2 C9 43.8(4) 3 . 3
C1 Pt1 Pt2 C9 133.8(4) . . 3
Cu2 Pt1 Pt2 C9 -155.2(2) 2 . 3
Cu2 Pt1 Pt2 C9 -65.2(2) 3 . 3
Cu2 Pt1 Pt2 C9 114.8(2) 4 . 3
Cu2 Pt1 Pt2 C9 24.8(2) . . 3
Pt1 Pt1 Pt2 C9 -20(12) 8_556 . 3
C1 Pt1 Pt2 C9 133.8(4) 4 . .
C1 Pt1 Pt2 C9 -136.2(4) 2 . .
C1 Pt1 Pt2 C9 -46.2(4) 3 . .
C1 Pt1 Pt2 C9 43.8(4) . . .
Cu2 Pt1 Pt2 C9 114.8(2) 2 . .
Cu2 Pt1 Pt2 C9 -155.2(2) 3 . .
Cu2 Pt1 Pt2 C9 24.8(2) 4 . .
Cu2 Pt1 Pt2 C9 -65.2(2) . . .
Pt1 Pt1 Pt2 C9 -110(12) 8_556 . .
C1 Pt1 Pt2 Cu1 44.3(3) 4 . .
C1 Pt1 Pt2 Cu1 134.3(3) 2 . .
C1 Pt1 Pt2 Cu1 -135.7(3) 3 . .
C1 Pt1 Pt2 Cu1 -45.7(3) . . .
Cu2 Pt1 Pt2 Cu1 25.24(2) 2 . .
Cu2 Pt1 Pt2 Cu1 115.24(2) 3 . .
Cu2 Pt1 Pt2 Cu1 -64.76(2) 4 . .
Cu2 Pt1 Pt2 Cu1 -154.76(2) . . .
Pt1 Pt1 Pt2 Cu1 160(12) 8_556 . .
C1 Pt1 Pt2 Cu1 134.3(3) 4 . 3
C1 Pt1 Pt2 Cu1 -135.7(3) 2 . 3
C1 Pt1 Pt2 Cu1 -45.7(3) 3 . 3
C1 Pt1 Pt2 Cu1 44.3(3) . . 3
Cu2 Pt1 Pt2 Cu1 115.24(2) 2 . 3
Cu2 Pt1 Pt2 Cu1 -154.76(2) 3 . 3
Cu2 Pt1 Pt2 Cu1 25.24(2) 4 . 3
Cu2 Pt1 Pt2 Cu1 -64.76(2) . . 3
Pt1 Pt1 Pt2 Cu1 -110(12) 8_556 . 3
C1 Pt1 Pt2 Cu1 -45.7(3) 4 . 4
C1 Pt1 Pt2 Cu1 44.3(3) 2 . 4
C1 Pt1 Pt2 Cu1 134.3(3) 3 . 4
C1 Pt1 Pt2 Cu1 -135.7(3) . . 4
Cu2 Pt1 Pt2 Cu1 -64.76(2) 2 . 4
Cu2 Pt1 Pt2 Cu1 25.24(2) 3 . 4
Cu2 Pt1 Pt2 Cu1 -154.76(2) 4 . 4
Cu2 Pt1 Pt2 Cu1 115.24(2) . . 4
Pt1 Pt1 Pt2 Cu1 70(12) 8_556 . 4
C1 Pt1 Pt2 Cu1 -135.7(3) 4 . 2
C1 Pt1 Pt2 Cu1 -45.7(3) 2 . 2
C1 Pt1 Pt2 Cu1 44.3(3) 3 . 2
C1 Pt1 Pt2 Cu1 134.3(3) . . 2
Cu2 Pt1 Pt2 Cu1 -154.76(2) 2 . 2
Cu2 Pt1 Pt2 Cu1 -64.76(2) 3 . 2
Cu2 Pt1 Pt2 Cu1 115.24(2) 4 . 2
Cu2 Pt1 Pt2 Cu1 25.24(2) . . 2
Pt1 Pt1 Pt2 Cu1 -20(12) 8_556 . 2
C1 Pt1 Pt2 Pt3 64(12) 4 . .
C1 Pt1 Pt2 Pt3 154(12) 2 . .
C1 Pt1 Pt2 Pt3 -116(12) 3 . .
C1 Pt1 Pt2 Pt3 -26(12) . . .
Cu2 Pt1 Pt2 Pt3 45(12) 2 . .
Cu2 Pt1 Pt2 Pt3 135(12) 3 . .
Cu2 Pt1 Pt2 Pt3 -45(12) 4 . .
Cu2 Pt1 Pt2 Pt3 -135(12) . . .
Pt1 Pt1 Pt2 Pt3 0(18) 8_556 . .
C9 Pt2 Pt3 C17 -0.9(3) 4 . 4
C9 Pt2 Pt3 C17 89.1(3) 2 . 4
C9 Pt2 Pt3 C17 179.1(3) 3 . 4
C9 Pt2 Pt3 C17 -90.9(3) . . 4
Pt1 Pt2 Pt3 C17 -21(100) . . 4
Cu1 Pt2 Pt3 C17 -1.4(3) . . 4
Cu1 Pt2 Pt3 C17 -91.4(3) 3 . 4
Cu1 Pt2 Pt3 C17 88.6(3) 4 . 4
Cu1 Pt2 Pt3 C17 178.6(3) 2 . 4
C9 Pt2 Pt3 C17 -90.9(3) 4 . 2
C9 Pt2 Pt3 C17 -0.9(3) 2 . 2
C9 Pt2 Pt3 C17 89.1(3) 3 . 2
C9 Pt2 Pt3 C17 179.1(3) . . 2
Pt1 Pt2 Pt3 C17 -111(100) . . 2
Cu1 Pt2 Pt3 C17 -91.4(3) . . 2
Cu1 Pt2 Pt3 C17 178.6(3) 3 . 2
Cu1 Pt2 Pt3 C17 -1.4(3) 4 . 2
Cu1 Pt2 Pt3 C17 88.6(3) 2 . 2
C9 Pt2 Pt3 C17 179.1(3) 4 . 3
C9 Pt2 Pt3 C17 -90.9(3) 2 . 3
C9 Pt2 Pt3 C17 -0.9(3) 3 . 3
C9 Pt2 Pt3 C17 89.1(3) . . 3
Pt1 Pt2 Pt3 C17 159(100) . . 3
Cu1 Pt2 Pt3 C17 178.6(3) . . 3
Cu1 Pt2 Pt3 C17 88.6(3) 3 . 3
Cu1 Pt2 Pt3 C17 -91.4(3) 4 . 3
Cu1 Pt2 Pt3 C17 -1.4(3) 2 . 3
C9 Pt2 Pt3 C17 89.1(3) 4 . .
C9 Pt2 Pt3 C17 179.1(3) 2 . .
C9 Pt2 Pt3 C17 -90.9(3) 3 . .
C9 Pt2 Pt3 C17 -0.9(3) . . .
Pt1 Pt2 Pt3 C17 69(100) . . .
Cu1 Pt2 Pt3 C17 88.6(3) . . .
Cu1 Pt2 Pt3 C17 -1.4(3) 3 . .
Cu1 Pt2 Pt3 C17 178.6(3) 4 . .
Cu1 Pt2 Pt3 C17 -91.4(3) 2 . .
C9 Pt2 Pt3 Cu1 -179.5(2) 4 . 2
C9 Pt2 Pt3 Cu1 -89.5(2) 2 . 2
C9 Pt2 Pt3 Cu1 0.5(2) 3 . 2
C9 Pt2 Pt3 Cu1 90.5(2) . . 2
Pt1 Pt2 Pt3 Cu1 160(63) . . 2
Cu1 Pt2 Pt3 Cu1 180.0 . . 2
Cu1 Pt2 Pt3 Cu1 90.0 3 . 2
Cu1 Pt2 Pt3 Cu1 -90.0 4 . 2
C9 Pt2 Pt3 Cu1 -89.5(2) 4 . 4
C9 Pt2 Pt3 Cu1 0.5(2) 2 . 4
C9 Pt2 Pt3 Cu1 90.5(2) 3 . 4
C9 Pt2 Pt3 Cu1 -179.5(2) . . 4
Pt1 Pt2 Pt3 Cu1 -110(64) . . 4
Cu1 Pt2 Pt3 Cu1 -90.0 . . 4
Cu1 Pt2 Pt3 Cu1 180.0 3 . 4
Cu1 Pt2 Pt3 Cu1 90.0 2 . 4
C9 Pt2 Pt3 Cu1 0.5(2) 4 . .
C9 Pt2 Pt3 Cu1 90.5(2) 2 . .
C9 Pt2 Pt3 Cu1 -179.5(2) 3 . .
C9 Pt2 Pt3 Cu1 -89.5(2) . . .
Pt1 Pt2 Pt3 Cu1 -20(64) . . .
Cu1 Pt2 Pt3 Cu1 -90.0 3 . .
Cu1 Pt2 Pt3 Cu1 90.0 4 . .
Cu1 Pt2 Pt3 Cu1 180.0 2 . .
C9 Pt2 Pt3 Cu1 90.5(2) 4 . 3
C9 Pt2 Pt3 Cu1 -179.5(2) 2 . 3
C9 Pt2 Pt3 Cu1 -89.5(2) 3 . 3
C9 Pt2 Pt3 Cu1 0.5(2) . . 3
Pt1 Pt2 Pt3 Cu1 70(63) . . 3
Cu1 Pt2 Pt3 Cu1 90.0 . . 3
Cu1 Pt2 Pt3 Cu1 180.0 4 . 3
Cu1 Pt2 Pt3 Cu1 -90.0 2 . 3
C17 Pt3 Cu1 C17 -88.0(3) 2 . 4
C17 Pt3 Cu1 C17 179.91(3) 3 . 4
C17 Pt3 Cu1 C17 90.5(3) . . 4
Cu1 Pt3 Cu1 C17 -177.8(4) 2 . 4
Cu1 Pt3 Cu1 C17 -120.2(4) 4 . 4
Cu1 Pt3 Cu1 C17 124.6(4) 3 . 4
Pt2 Pt3 Cu1 C17 -177.8(4) . . 4
C17 Pt3 Cu1 C9 177.3(5) 4 . 4
C17 Pt3 Cu1 C9 89.3(4) 2 . 4
C17 Pt3 Cu1 C9 -2.8(5) 3 . 4
C17 Pt3 Cu1 C9 -92.2(4) . . 4
Cu1 Pt3 Cu1 C9 -0.6(3) 2 . 4
Cu1 Pt3 Cu1 C9 57.0(3) 4 . 4
Cu1 Pt3 Cu1 C9 -58.1(3) 3 . 4
Pt2 Pt3 Cu1 C9 -0.6(3) . . 4
C17 Pt3 Cu1 C10 175.6(6) 4 . 4
C17 Pt3 Cu1 C10 87.6(5) 2 . 4
C17 Pt3 Cu1 C10 -4.5(6) 3 . 4
C17 Pt3 Cu1 C10 -93.9(5) . . 4
Cu1 Pt3 Cu1 C10 -2.2(4) 2 . 4
Cu1 Pt3 Cu1 C10 55.3(4) 4 . 4
Cu1 Pt3 Cu1 C10 -59.8(4) 3 . 4
Pt2 Pt3 Cu1 C10 -2.2(4) . . 4
C17 Pt3 Cu1 C18 -0.9(5) 4 . 4
C17 Pt3 Cu1 C18 -88.8(3) 2 . 4
C17 Pt3 Cu1 C18 179.0(5) 3 . 4
C17 Pt3 Cu1 C18 89.7(3) . . 4
Cu1 Pt3 Cu1 C18 -178.7(2) 2 . 4
Cu1 Pt3 Cu1 C18 -121.1(2) 4 . 4
Cu1 Pt3 Cu1 C18 123.7(2) 3 . 4
Pt2 Pt3 Cu1 C18 -178.7(2) . . 4
C17 Pt3 Cu1 Pt2 177.8(4) 4 . .
C17 Pt3 Cu1 Pt2 89.9(2) 2 . .
C17 Pt3 Cu1 Pt2 -2.3(4) 3 . .
C17 Pt3 Cu1 Pt2 -91.7(2) . . .
Cu1 Pt3 Cu1 Pt2 0.0 2 . .
Cu1 Pt3 Cu1 Pt2 57.591(10) 4 . .
Cu1 Pt3 Cu1 Pt2 -57.591(10) 3 . .
C17 Pt3 Cu1 Cu1 120.2(4) 4 . 4
C17 Pt3 Cu1 Cu1 32.3(2) 2 . 4
C17 Pt3 Cu1 Cu1 -59.9(4) 3 . 4
C17 Pt3 Cu1 Cu1 -149.2(2) . . 4
Cu1 Pt3 Cu1 Cu1 -57.591(10) 2 . 4
Cu1 Pt3 Cu1 Cu1 -115.18(2) 3 . 4
Pt2 Pt3 Cu1 Cu1 -57.591(10) . . 4
C17 Pt3 Cu1 Cu1 -124.6(4) 4 . 3
C17 Pt3 Cu1 Cu1 147.5(2) 2 . 3
C17 Pt3 Cu1 Cu1 55.3(4) 3 . 3
C17 Pt3 Cu1 Cu1 -34.1(2) . . 3
Cu1 Pt3 Cu1 Cu1 57.591(10) 2 . 3
Cu1 Pt3 Cu1 Cu1 115.18(2) 4 . 3
Pt2 Pt3 Cu1 Cu1 57.591(10) . . 3
C9 Pt2 Cu1 C17 -177.6(5) 4 . 4
C9 Pt2 Cu1 C17 -89.0(4) 2 . 4
C9 Pt2 Cu1 C17 2.4(5) 3 . 4
C9 Pt2 Cu1 C17 92.8(4) . . 4
Pt1 Pt2 Cu1 C17 -178.4(3) . . 4
Cu1 Pt2 Cu1 C17 59.1(3) 3 . 4
Cu1 Pt2 Cu1 C17 -55.9(3) 4 . 4
Cu1 Pt2 Cu1 C17 1.6(3) 2 . 4
Pt3 Pt2 Cu1 C17 1.6(3) . . 4
C9 Pt2 Cu1 C9 88.7(3) 2 . 4
C9 Pt2 Cu1 C9 -179.963(18) 3 . 4
C9 Pt2 Cu1 C9 -89.5(3) . . 4
Pt1 Pt2 Cu1 C9 -0.7(3) . . 4
Cu1 Pt2 Cu1 C9 -123.2(3) 3 . 4
Cu1 Pt2 Cu1 C9 121.8(3) 4 . 4
Cu1 Pt2 Cu1 C9 179.3(3) 2 . 4
Pt3 Pt2 Cu1 C9 179.3(3) . . 4
C9 Pt2 Cu1 C10 -0.3(4) 4 . 4
C9 Pt2 Cu1 C10 88.4(3) 2 . 4
C9 Pt2 Cu1 C10 179.7(4) 3 . 4
C9 Pt2 Cu1 C10 -89.8(3) . . 4
Pt1 Pt2 Cu1 C10 -1.0(2) . . 4
Cu1 Pt2 Cu1 C10 -123.5(2) 3 . 4
Cu1 Pt2 Cu1 C10 121.5(2) 4 . 4
Cu1 Pt2 Cu1 C10 179.0(2) 2 . 4
Pt3 Pt2 Cu1 C10 179.0(2) . . 4
C9 Pt2 Cu1 C18 -176.3(6) 4 . 4
C9 Pt2 Cu1 C18 -87.7(6) 2 . 4
C9 Pt2 Cu1 C18 3.7(6) 3 . 4
C9 Pt2 Cu1 C18 94.1(6) . . 4
Pt1 Pt2 Cu1 C18 -177.1(5) . . 4
Cu1 Pt2 Cu1 C18 60.4(5) 3 . 4
Cu1 Pt2 Cu1 C18 -54.6(5) 4 . 4
Cu1 Pt2 Cu1 C18 2.9(5) 2 . 4
Pt3 Pt2 Cu1 C18 2.9(5) . . 4
C9 Pt2 Cu1 Pt3 -179.3(3) 4 . .
C9 Pt2 Cu1 Pt3 -90.6(2) 2 . .
C9 Pt2 Cu1 Pt3 0.8(4) 3 . .
C9 Pt2 Cu1 Pt3 91.2(2) . . .
Pt1 Pt2 Cu1 Pt3 180.0 . . .
Cu1 Pt2 Cu1 Pt3 57.509(10) 3 . .
Cu1 Pt2 Cu1 Pt3 -57.509(10) 4 . .
Cu1 Pt2 Cu1 Pt3 0.0 2 . .
C9 Pt2 Cu1 Cu1 -121.8(3) 4 . 4
C9 Pt2 Cu1 Cu1 -33.1(2) 2 . 4
C9 Pt2 Cu1 Cu1 58.3(4) 3 . 4
C9 Pt2 Cu1 Cu1 148.7(2) . . 4
Pt1 Pt2 Cu1 Cu1 -122.491(10) . . 4
Cu1 Pt2 Cu1 Cu1 115.02(2) 3 . 4
Cu1 Pt2 Cu1 Cu1 57.510(10) 2 . 4
Pt3 Pt2 Cu1 Cu1 57.509(10) . . 4
C9 Pt2 Cu1 Cu1 123.2(3) 4 . 3
C9 Pt2 Cu1 Cu1 -148.1(2) 2 . 3
C9 Pt2 Cu1 Cu1 -56.7(4) 3 . 3
C9 Pt2 Cu1 Cu1 33.7(2) . . 3
Pt1 Pt2 Cu1 Cu1 122.491(10) . . 3
Cu1 Pt2 Cu1 Cu1 -115.02(2) 4 . 3
Cu1 Pt2 Cu1 Cu1 -57.509(10) 2 . 3
Pt3 Pt2 Cu1 Cu1 -57.509(10) . . 3
C1 Pt1 Cu2 C1 -176.9(2) 4 . 3
C1 Pt1 Cu2 C1 107.9(3) 2 . 3
C1 Pt1 Cu2 C1 -77.04(18) . . 3
Cu2 Pt1 Cu2 C1 -151.4(4) 2 . 3
Cu2 Pt1 Cu2 C1 152.8(4) 3 . 3
Cu2 Pt1 Cu2 C1 -95.6(4) 4 . 3
Pt2 Pt1 Cu2 C1 28.6(4) . . 3
Pt1 Pt1 Cu2 C1 -151.4(4) 8_556 . 3
C1 Pt1 Cu2 C1 -2.3(2) 4 . 8_556
C1 Pt1 Cu2 C1 -77.5(3) 2 . 8_556
C1 Pt1 Cu2 C1 174.6(2) 3 . 8_556
C1 Pt1 Cu2 C1 97.53(19) . . 8_556
Cu2 Pt1 Cu2 C1 23.2(3) 2 . 8_556
Cu2 Pt1 Cu2 C1 -32.7(3) 3 . 8_556
Cu2 Pt1 Cu2 C1 79.0(3) 4 . 8_556
Pt2 Pt1 Cu2 C1 -156.8(3) . . 8_556
Pt1 Pt1 Cu2 C1 23.2(3) 8_556 . 8_556
C1 Pt1 Cu2 C2 36.1(5) 4 . 8_556
C1 Pt1 Cu2 C2 -39.1(5) 2 . 8_556
C1 Pt1 Cu2 C2 -147.0(6) 3 . 8_556
C1 Pt1 Cu2 C2 136.0(5) . . 8_556
Cu2 Pt1 Cu2 C2 61.6(4) 2 . 8_556
Cu2 Pt1 Cu2 C2 5.8(4) 3 . 8_556
Cu2 Pt1 Cu2 C2 117.5(4) 4 . 8_556
Pt2 Pt1 Cu2 C2 -118.4(4) . . 8_556
Pt1 Pt1 Cu2 C2 61.6(4) 8_556 . 8_556
C1 Pt1 Cu2 C2 -174.8(4) 4 . 3
C1 Pt1 Cu2 C2 110.0(4) 2 . 3
C1 Pt1 Cu2 C2 2.1(5) 3 . 3
C1 Pt1 Cu2 C2 -75.0(4) . . 3
Cu2 Pt1 Cu2 C2 -149.3(2) 2 . 3
Cu2 Pt1 Cu2 C2 154.8(2) 3 . 3
Cu2 Pt1 Cu2 C2 -93.5(2) 4 . 3
Pt2 Pt1 Cu2 C2 30.7(2) . . 3
Pt1 Pt1 Cu2 C2 -149.3(2) 8_556 . 3
C1 Pt1 Cu2 Pt1 -25.5(3) 4 . 5_556
C1 Pt1 Cu2 Pt1 -100.7(2) 2 . 5_556
C1 Pt1 Cu2 Pt1 151.4(4) 3 . 5_556
C1 Pt1 Cu2 Pt1 74.3(2) . . 5_556
Cu2 Pt1 Cu2 Pt1 0.0 2 . 5_556
Cu2 Pt1 Cu2 Pt1 -55.831(10) 3 . 5_556
Cu2 Pt1 Cu2 Pt1 55.831(10) 4 . 5_556
Pt2 Pt1 Cu2 Pt1 180.0 . . 5_556
Pt1 Pt1 Cu2 Pt1 0.0 8_556 . 5_556
C1 Pt1 Cu2 Pt1 -25.5(3) 4 . 8_556
C1 Pt1 Cu2 Pt1 -100.7(2) 2 . 8_556
C1 Pt1 Cu2 Pt1 151.4(4) 3 . 8_556
C1 Pt1 Cu2 Pt1 74.3(2) . . 8_556
Cu2 Pt1 Cu2 Pt1 0.0 2 . 8_556
Cu2 Pt1 Cu2 Pt1 -55.831(10) 3 . 8_556
Cu2 Pt1 Cu2 Pt1 55.831(10) 4 . 8_556
Pt2 Pt1 Cu2 Pt1 180.0 . . 8_556
C1 Pt1 Cu2 Cu2 -81.3(3) 4 . 4
C1 Pt1 Cu2 Cu2 -156.5(2) 2 . 4
C1 Pt1 Cu2 Cu2 95.6(4) 3 . 4
C1 Pt1 Cu2 Cu2 18.5(2) . . 4
Cu2 Pt1 Cu2 Cu2 -55.831(10) 2 . 4
Cu2 Pt1 Cu2 Cu2 -111.663(19) 3 . 4
Pt2 Pt1 Cu2 Cu2 124.169(10) . . 4
Pt1 Pt1 Cu2 Cu2 -55.831(10) 8_556 . 4
C1 Pt1 Cu2 Cu2 30.4(3) 4 . 3
C1 Pt1 Cu2 Cu2 -44.9(2) 2 . 3
C1 Pt1 Cu2 Cu2 -152.8(4) 3 . 3
C1 Pt1 Cu2 Cu2 130.2(2) . . 3
Cu2 Pt1 Cu2 Cu2 55.831(10) 2 . 3
Cu2 Pt1 Cu2 Cu2 111.663(19) 4 . 3
Pt2 Pt1 Cu2 Cu2 -124.169(10) . . 3
Pt1 Pt1 Cu2 Cu2 55.831(10) 8_556 . 3
C1 Pt1 C1 C2 82(6) 4 . .
C1 Pt1 C1 C2 -5(6) 2 . .
C1 Pt1 C1 C2 -92(6) 3 . .
Cu2 Pt1 C1 C2 41(6) 2 . .
Cu2 Pt1 C1 C2 13(6) 3 . .
Cu2 Pt1 C1 C2 -26(6) 4 . .
Cu2 Pt1 C1 C2 -50(6) . . .
Pt2 Pt1 C1 C2 175(6) . . .
Pt1 Pt1 C1 C2 -5(6) 8_556 . .
C1 Pt1 C1 Cu2 107.3(3) 4 . 4
C1 Pt1 C1 Cu2 20.6(3) 2 . 4
C1 Pt1 C1 Cu2 -66.0(4) 3 . 4
Cu2 Pt1 C1 Cu2 66.9(3) 2 . 4
Cu2 Pt1 C1 Cu2 39.1(5) 3 . 4
Cu2 Pt1 C1 Cu2 -24.5(3) . . 4
Pt2 Pt1 C1 Cu2 -159.4(3) . . 4
Pt1 Pt1 C1 Cu2 20.6(3) 8_556 . 4
Cu2 C1 C2 C3 -162(5) 4 . .
Pt1 C1 C2 C3 -136(5) . . .
Pt1 C1 C2 Cu2 26(6) . . 4
C1 C2 C3 C8 104(5) . . .
Cu2 C2 C3 C8 -56.3(19) 4 . .
C1 C2 C3 C4' -160(5) . . .
Cu2 C2 C3 C4' 39.7(18) 4 . .
C1 C2 C3 C8' 26(6) . . .
Cu2 C2 C3 C8' -135.0(11) 4 . .
C1 C2 C3 C4 -93(5) . . .
Cu2 C2 C3 C4 106.0(11) 4 . .
C8 C3 C4 C5 -16(3) . . .
C4' C3 C4 C5 -66(2) . . .
C2 C3 C4 C5 180.0(16) . . .
C8' C3 C4 C5 49(2) . . .
C8 C3 C4' C5' -54(2) . . .
C2 C3 C4' C5' -178.6(16) . . .
C8' C3 C4' C5' -4(3) . . .
C4 C3 C4' C5' 80(2) . . .
C3 C4 C5 C6 2(3) . . .
C3 C4' C5' C6 -6(4) . . .
C4' C5' C6 C7 59(3) . . .
C4' C5' C6 C5 -71(3) . . .
C4' C5' C6 C7' 14(4) . . .
C4 C5 C6 C5' 67(2) . . .
C4 C5 C6 C7 14(3) . . .
C4 C5 C6 C7' -55(3) . . .
C5' C6 C7 C8 -69(3) . . .
C5 C6 C7 C8 -21(4) . . .
C7' C6 C7 C8 71(3) . . .
C5' C6 C7' C8' -11(3) . . .
C7 C6 C7' C8' -58(2) . . .
C5 C6 C7' C8' 53(2) . . .
C4' C3 C8 C7 55(2) . . .
C2 C3 C8 C7 175.3(18) . . .
C8' C3 C8 C7 -74(3) . . .
C4 C3 C8 C7 13(3) . . .
C6 C7 C8 C3 7(4) . . .
C6 C7' C8' C3 1(3) . . .
C8 C3 C8' C7' 62(2) . . .
C4' C3 C8' C7' 5(3) . . .
C2 C3 C8' C7' -179.7(18) . . .
C4 C3 C8' C7' -52(2) . . .
C9 Pt2 C9 C10 -72(29) 4 . .
C9 Pt2 C9 C10 -160(29) 2 . .
C9 Pt2 C9 C10 111(29) 3 . .
Pt1 Pt2 C9 C10 -160(29) . . .
Cu1 Pt2 C9 C10 -31(29) . . .
Cu1 Pt2 C9 C10 20(28) 3 . .
Cu1 Pt2 C9 C10 19(29) 4 . .
Cu1 Pt2 C9 C10 70(29) 2 . .
Pt3 Pt2 C9 C10 20(29) . . .
C9 Pt2 C9 Cu1 -91.7(3) 4 . 3
C9 Pt2 C9 Cu1 179.42(19) 2 . 3
C9 Pt2 C9 Cu1 90.6(3) 3 . 3
Pt1 Pt2 C9 Cu1 179.4(3) . . 3
Cu1 Pt2 C9 Cu1 -51.0(3) . . 3
Cu1 Pt2 C9 Cu1 -1.2(5) 4 . 3
Cu1 Pt2 C9 Cu1 49.9(3) 2 . 3
Pt3 Pt2 C9 Cu1 -0.6(3) . . 3
Cu1 C9 C10 C11 -176(3) 3 . .
Pt2 C9 C10 C11 164(27) . . .
Pt2 C9 C10 Cu1 -20(29) . . 3
C9 C10 C11 C16 -48(3) . . .
Cu1 C10 C11 C16 137.1(11) 3 . .
C9 C10 C11 C12 128(3) . . .
Cu1 C10 C11 C12 -46.9(14) 3 . .
C9 C10 C11 C16' 23(3) . . .
Cu1 C10 C11 C16' -152.5(10) 3 . .
C9 C10 C11 C12' -155(3) . . .
Cu1 C10 C11 C12' 30.0(14) 3 . .
C16 C11 C12 C13 -8(2) . . .
C16' C11 C12 C13 -60(2) . . .
C12' C11 C12 C13 62.7(19) . . .
C10 C11 C12 C13 176.3(16) . . .
C16 C11 C12' C13' 63.9(19) . . .
C12 C11 C12' C13' -59.5(18) . . .
C16' C11 C12' C13' 10(2) . . .
C10 C11 C12' C13' -172.5(14) . . .
C11 C12 C13 C14 11(3) . . .
C11 C12' C13' C14 -14(3) . . .
C12' C13' C14 C13 81(2) . . .
C12' C13' C14 C15 -48(2) . . .
C12' C13' C14 C15' 17(3) . . .
C12 C13 C14 C13' -81(2) . . .
C12 C13 C14 C15 -11(3) . . .
C12 C13 C14 C15' 52(2) . . .
C13' C14 C15 C16 59(2) . . .
C13 C14 C15 C16 8(3) . . .
C15' C14 C15 C16 -67(2) . . .
C13' C14 C15' C16' -14(4) . . .
C13 C14 C15' C16' -61(3) . . .
C15 C14 C15' C16' 65(2) . . .
C12 C11 C16 C15 4(3) . . .
C16' C11 C16 C15 70(2) . . .
C12' C11 C16 C15 -53(2) . . .
C10 C11 C16 C15 -179.6(16) . . .
C14 C15 C16 C11 -5(3) . . .
C14 C15' C16' C11 8(4) . . .
C16 C11 C16' C15' -76(2) . . .
C12 C11 C16' C15' 49(2) . . .
C12' C11 C16' C15' -7(3) . . .
C10 C11 C16' C15' 175(2) . . .
C17 Pt3 C17 C18 158(27) 4 . .
C17 Pt3 C17 C18 -113(28) 2 . .
C17 Pt3 C17 C18 -24(28) 3 . .
Cu1 Pt3 C17 C18 16(28) 2 . .
Cu1 Pt3 C17 C18 69(28) 4 . .
Cu1 Pt3 C17 C18 117(28) . . .
Cu1 Pt3 C17 C18 65(28) 3 . .
Pt2 Pt3 C17 C18 67(28) . . .
C17 Pt3 C17 Cu1 92.7(4) 4 . 3
C17 Pt3 C17 Cu1 -178.3(2) 2 . 3
C17 Pt3 C17 Cu1 -89.3(4) 3 . 3
Cu1 Pt3 C17 Cu1 -48.9(3) 2 . 3
Cu1 Pt3 C17 Cu1 3.4(6) 4 . 3
Cu1 Pt3 C17 Cu1 52.3(3) . . 3
Pt2 Pt3 C17 Cu1 1.7(3) . . 3
Cu1 C17 C18 C19 180(100) 3 . .
Pt3 C17 C18 C19 114(27) . . .
Pt3 C17 C18 Cu1 -65(28) . . 3
C17 C18 C19 C24 29(4) . . .
Cu1 C18 C19 C24 -151.3(9) 3 . .
C17 C18 C19 C20' 156(4) . . .
Cu1 C18 C19 C20' -24.2(16) 3 . .
C17 C18 C19 C24' -28(4) . . .
Cu1 C18 C19 C24' 152.2(9) 3 . .
C17 C18 C19 C20 -147(4) . . .
Cu1 C18 C19 C20 33.2(13) 3 . .
C24 C19 C20 C21 5(2) . . .
C20' C19 C20 C21 -73(2) . . .
C24' C19 C20 C21 51.1(18) . . .
C18 C19 C20 C21 -179.5(14) . . .
C24 C19 C20' C21' -55(2) . . .
C24' C19 C20' C21' -5(3) . . .
C18 C19 C20' C21' 171.7(17) . . .
C20 C19 C20' C21' 66(2) . . .
C19 C20 C21 C22 -9(3) . . .
C19 C20' C21' C22 11(4) . . .
C20 C21 C22 C23' -40(3) . . .
C20 C21 C22 C21' 77(3) . . .
C20 C21 C22 C23 6(3) . . .
C20' C21' C22 C21 -91(3) . . .
C20' C21' C22 C23' -10(4) . . .
C20' C21' C22 C23 35(3) . . .
C21 C22 C23 C24 2(3) . . .
C23' C22 C23 C24 80(2) . . .
C21' C22 C23 C24 -38(3) . . .
C21 C22 C23' C24' 45(3) . . .
C21' C22 C23' C24' 3(3) . . .
C23 C22 C23' C24' -78(2) . . .
C20' C19 C24 C23 51(2) . . .
C24' C19 C24 C23 -66.8(18) . . .
C18 C19 C24 C23 -172.2(15) . . .
C20 C19 C24 C23 3(2) . . .
C22 C23 C24 C19 -7(3) . . .
C22 C23' C24' C19 4(3) . . .
C24 C19 C24' C23' 77.8(17) . . .
C20' C19 C24' C23' -3(2) . . .
C18 C19 C24' C23' -179.4(15) . . .
C20 C19 C24' C23' -47.6(18) . . .
C25 C25 C26 C26 0.0 3_655 . 3_655
C25 C25 C26 C26 90.0 4_565 . 3_655
C25 C25 C26 C26 45.0 2_665 . 3_655
C26 C25 C26 C26 90.0 4_565 . 3_655
C26 C25 C26 C26 45.0 2_665 . 3_655
Cl1 C25 C26 C26 -115(2) . . 3_655
Cl1 C25 C26 C26 141(2) 4_565 . 3_655
Cl1 C25 C26 C26 -18.8(17) 3_655 . 3_655
Cl1 C25 C26 C26 58.9(16) 2_665 . 3_655
C25 C25 C26 C26 -90.0 3_655 . 4_565
C25 C25 C26 C26 0.0 4_565 . 4_565
C25 C25 C26 C26 -45.0 2_665 . 4_565
C26 C25 C26 C26 -90.0 3_655 . 4_565
C26 C25 C26 C26 -45.0 2_665 . 4_565
Cl1 C25 C26 C26 155(2) . . 4_565
Cl1 C25 C26 C26 51(2) 4_565 . 4_565
Cl1 C25 C26 C26 -108.8(16) 3_655 . 4_565
Cl1 C25 C26 C26 -31.1(16) 2_665 . 4_565
C25 C25 C26 C26 -45.0 3_655 . 2_665
C25 C25 C26 C26 45.0 4_565 . 2_665
C25 C25 C26 C26 0.0 2_665 . 2_665
C26 C25 C26 C26 45.0 4_565 . 2_665
C26 C25 C26 C26 -45.0 3_655 . 2_665
Cl1 C25 C26 C26 -160(2) . . 2_665
Cl1 C25 C26 C26 96(2) 4_565 . 2_665
Cl1 C25 C26 C26 -63.8(16) 3_655 . 2_665
Cl1 C25 C26 C26 13.9(16) 2_665 . 2_665
C25 C25 C26 C25 90.0 4_565 . 3_655
C25 C25 C26 C25 45.0 2_665 . 3_655
C26 C25 C26 C25 90.0 4_565 . 3_655
C26 C25 C26 C25 0.03(6) 3_655 . 3_655
C26 C25 C26 C25 45.0 2_665 . 3_655
Cl1 C25 C26 C25 -115(2) . . 3_655
Cl1 C25 C26 C25 141(2) 4_565 . 3_655
Cl1 C25 C26 C25 -18.7(16) 3_655 . 3_655
Cl1 C25 C26 C25 58.9(15) 2_665 . 3_655
C25 C25 C26 C25 -90.0 3_655 . 4_565
C25 C25 C26 C25 -45.0 2_665 . 4_565
C26 C25 C26 C25 0.0 4_565 . 4_565
C26 C25 C26 C25 -90.0 3_655 . 4_565
C26 C25 C26 C25 -45.0 2_665 . 4_565
Cl1 C25 C26 C25 155(2) . . 4_565
Cl1 C25 C26 C25 51(2) 4_565 . 4_565
Cl1 C25 C26 C25 -108.7(16) 3_655 . 4_565
Cl1 C25 C26 C25 -31.1(15) 2_665 . 4_565
C25 C25 C26 C25 -45.0 3_655 . 2_665
C25 C25 C26 C25 45.0 4_565 . 2_665
C26 C25 C26 C25 45.0 4_565 . 2_665
C26 C25 C26 C25 -44.97(6) 3_655 . 2_665
C26 C25 C26 C25 0.0 2_665 . 2_665
Cl1 C25 C26 C25 -160(2) . . 2_665
Cl1 C25 C26 C25 96(2) 4_565 . 2_665
Cl1 C25 C26 C25 -63.7(16) 3_655 . 2_665
Cl1 C25 C26 C25 13.9(15) 2_665 . 2_665
C25 C25 C26 Cl1 115(2) 3_655 . .
C25 C25 C26 Cl1 -155(2) 4_565 . .
C25 C25 C26 Cl1 160(2) 2_665 . .
C26 C25 C26 Cl1 -155(2) 4_565 . .
C26 C25 C26 Cl1 115(2) 3_655 . .
C26 C25 C26 Cl1 160(2) 2_665 . .
Cl1 C25 C26 Cl1 -104.5(6) 4_565 . .
Cl1 C25 C26 Cl1 96.0(6) 3_655 . .
Cl1 C25 C26 Cl1 173.7(7) 2_665 . .
C25 C25 C26 Cl1 -141(2) 3_655 . 4_565
C25 C25 C26 Cl1 -51(2) 4_565 . 4_565
C25 C25 C26 Cl1 -96(2) 2_665 . 4_565
C26 C25 C26 Cl1 -51(2) 4_565 . 4_565
C26 C25 C26 Cl1 -141(2) 3_655 . 4_565
C26 C25 C26 Cl1 -96(2) 2_665 . 4_565
Cl1 C25 C26 Cl1 104.5(6) . . 4_565
Cl1 C25 C26 Cl1 -159.5(8) 3_655 . 4_565
Cl1 C25 C26 Cl1 -81.8(5) 2_665 . 4_565
C25 C25 C26 Cl1 18.7(16) 3_655 . 3_655
C25 C25 C26 Cl1 108.7(16) 4_565 . 3_655
C25 C25 C26 Cl1 63.7(16) 2_665 . 3_655
C26 C25 C26 Cl1 108.8(16) 4_565 . 3_655
C26 C25 C26 Cl1 18.8(16) 3_655 . 3_655
C26 C25 C26 Cl1 63.8(16) 2_665 . 3_655
Cl1 C25 C26 Cl1 -96.0(6) . . 3_655
Cl1 C25 C26 Cl1 159.5(8) 4_565 . 3_655
Cl1 C25 C26 Cl1 77.7(4) 2_665 . 3_655
C25 C25 C26 Cl1 -58.9(16) 3_655 . 2_665
C25 C25 C26 Cl1 31.1(16) 4_565 . 2_665
C25 C25 C26 Cl1 -13.9(15) 2_665 . 2_665
C26 C25 C26 Cl1 31.1(16) 4_565 . 2_665
C26 C25 C26 Cl1 -58.9(16) 3_655 . 2_665
C26 C25 C26 Cl1 -13.9(16) 2_665 . 2_665
Cl1 C25 C26 Cl1 -173.7(7) . . 2_665
Cl1 C25 C26 Cl1 81.8(5) 4_565 . 2_665
Cl1 C25 C26 Cl1 -77.7(4) 3_655 . 2_665
C25 C25 Cl1 C26 -81.0(9) 3_655 . .
C25 C25 Cl1 C26 53(3) 4_565 . .
C25 C25 Cl1 C26 -47(3) 2_665 . .
C26 C25 Cl1 C26 8.2(8) 4_565 . .
C26 C25 Cl1 C26 -18.4(8) 3_655 . .
C26 C25 Cl1 C26 -9.1(9) 2_665 . .
Cl1 C25 Cl1 C26 68.8(3) 4_565 . .
Cl1 C25 Cl1 C26 -73.2(2) 3_655 . .
Cl1 C25 Cl1 C26 -10.8(11) 2_665 . .
C25 C25 Cl1 C25 134.4(19) 4_565 . 3_655
C25 C25 Cl1 C25 34(2) 2_665 . 3_655
C26 C25 Cl1 C25 81.0(9) . . 3_655
C26 C25 Cl1 C25 89.2(4) 4_565 . 3_655
C26 C25 Cl1 C25 62.6(10) 3_655 . 3_655
C26 C25 Cl1 C25 71.9(3) 2_665 . 3_655
Cl1 C25 Cl1 C25 149.8(6) 4_565 . 3_655
Cl1 C25 Cl1 C25 7.8(7) 3_655 . 3_655
Cl1 C25 Cl1 C25 70.2(4) 2_665 . 3_655
C25 C25 Cl1 C26 -62.6(10) 3_655 . 3_655
C25 C25 Cl1 C26 72(3) 4_565 . 3_655
C25 C25 Cl1 C26 -29(3) 2_665 . 3_655
C26 C25 Cl1 C26 18.4(8) . . 3_655
C26 C25 Cl1 C26 26.6(12) 4_565 . 3_655
C26 C25 Cl1 C26 9.2(8) 2_665 . 3_655
Cl1 C25 Cl1 C26 87.1(6) 4_565 . 3_655
Cl1 C25 Cl1 C26 -54.9(7) 3_655 . 3_655
Cl1 C25 Cl1 C26 7.6(9) 2_665 . 3_655
C25 C25 Cl1 C25 -134.4(19) 3_655 . 4_565
C25 C25 Cl1 C25 -100.6(6) 2_665 . 4_565
C26 C25 Cl1 C25 -53(3) . . 4_565
C26 C25 Cl1 C25 -45(2) 4_565 . 4_565
C26 C25 Cl1 C25 -72(3) 3_655 . 4_565
C26 C25 Cl1 C25 -62.6(19) 2_665 . 4_565
Cl1 C25 Cl1 C25 15(3) 4_565 . 4_565
Cl1 C25 Cl1 C25 -127(3) 3_655 . 4_565
Cl1 C25 Cl1 C25 -64.2(18) 2_665 . 4_565
C25 C25 Cl1 C26 -89.2(3) 3_655 . 4_565
C25 C25 Cl1 C26 45(2) 4_565 . 4_565
C25 C25 Cl1 C26 -55(3) 2_665 . 4_565
C26 C25 Cl1 C26 -8.2(8) . . 4_565
C26 C25 Cl1 C26 -26.6(12) 3_655 . 4_565
C26 C25 Cl1 C26 -17.3(7) 2_665 . 4_565
Cl1 C25 Cl1 C26 60.5(7) 4_565 . 4_565
Cl1 C25 Cl1 C26 -81.5(7) 3_655 . 4_565
Cl1 C25 Cl1 C26 -19.0(8) 2_665 . 4_565
C25 C25 Cl1 C25 -34(2) 3_655 . 2_665
C25 C25 Cl1 C25 100.6(6) 4_565 . 2_665
C26 C25 Cl1 C25 47(3) . . 2_665
C26 C25 Cl1 C25 55(3) 4_565 . 2_665
C26 C25 Cl1 C25 29(3) 3_655 . 2_665
C26 C25 Cl1 C25 38(2) 2_665 . 2_665
Cl1 C25 Cl1 C25 116(3) 4_565 . 2_665
Cl1 C25 Cl1 C25 -26(3) 3_655 . 2_665
Cl1 C25 Cl1 C25 36(2) 2_665 . 2_665
C25 C25 Cl1 C26 -71.9(3) 3_655 . 2_665
C25 C25 Cl1 C26 62.6(19) 4_565 . 2_665
C25 C25 Cl1 C26 -38(2) 2_665 . 2_665
C26 C25 Cl1 C26 9.1(9) . . 2_665
C26 C25 Cl1 C26 17.3(7) 4_565 . 2_665
C26 C25 Cl1 C26 -9.2(8) 3_655 . 2_665
Cl1 C25 Cl1 C26 77.9(7) 4_565 . 2_665
Cl1 C25 Cl1 C26 -64.1(7) 3_655 . 2_665
Cl1 C25 Cl1 C26 -1.67(16) 2_665 . 2_665
C26 C26 Cl1 C25 78.0(12) 3_655 . .
C26 C26 Cl1 C25 -45(3) 4_565 . .
C26 C26 Cl1 C25 39(3) 2_665 . .
C25 C26 Cl1 C25 19.2(8) 3_655 . .
C25 C26 Cl1 C25 -8.4(8) 4_565 . .
C25 C26 Cl1 C25 9.2(9) 2_665 . .
Cl1 C26 Cl1 C25 -62.1(3) 4_565 . .
Cl1 C26 Cl1 C25 67.9(3) 3_655 . .
Cl1 C26 Cl1 C25 8.0(8) 2_665 . .
C26 C26 Cl1 C25 58.8(12) 3_655 . 3_655
C26 C26 Cl1 C25 -64(3) 4_565 . 3_655
C26 C26 Cl1 C25 19(3) 2_665 . 3_655
C25 C26 Cl1 C25 -19.2(8) . . 3_655
C25 C26 Cl1 C25 -27.6(12) 4_565 . 3_655
C25 C26 Cl1 C25 -10.0(7) 2_665 . 3_655
Cl1 C26 Cl1 C25 -81.3(6) 4_565 . 3_655
Cl1 C26 Cl1 C25 48.7(6) 3_655 . 3_655
Cl1 C26 Cl1 C25 -11.2(7) 2_665 . 3_655
C26 C26 Cl1 C26 -122.8(17) 4_565 . 3_655
C26 C26 Cl1 C26 -39(2) 2_665 . 3_655
C25 C26 Cl1 C26 -78.0(12) . . 3_655
C25 C26 Cl1 C26 -58.8(11) 3_655 . 3_655
C25 C26 Cl1 C26 -86.4(5) 4_565 . 3_655
C25 C26 Cl1 C26 -68.8(4) 2_665 . 3_655
Cl1 C26 Cl1 C26 -140.1(9) 4_565 . 3_655
Cl1 C26 Cl1 C26 -10.1(9) 3_655 . 3_655
Cl1 C26 Cl1 C26 -70.0(5) 2_665 . 3_655
C26 C26 Cl1 C25 86.4(5) 3_655 . 4_565
C26 C26 Cl1 C25 -36(2) 4_565 . 4_565
C26 C26 Cl1 C25 47(3) 2_665 . 4_565
C25 C26 Cl1 C25 8.4(8) . . 4_565
C25 C26 Cl1 C25 27.6(12) 3_655 . 4_565
C25 C26 Cl1 C25 17.6(6) 2_665 . 4_565
Cl1 C26 Cl1 C25 -53.7(6) 4_565 . 4_565
Cl1 C26 Cl1 C25 76.3(7) 3_655 . 4_565
Cl1 C26 Cl1 C25 16.4(6) 2_665 . 4_565
C26 C26 Cl1 C26 122.8(17) 3_655 . 4_565
C26 C26 Cl1 C26 83.4(4) 2_665 . 4_565
C25 C26 Cl1 C26 45(3) . . 4_565
C25 C26 Cl1 C26 64(3) 3_655 . 4_565
C25 C26 Cl1 C26 36(2) 4_565 . 4_565
C25 C26 Cl1 C26 54(2) 2_665 . 4_565
Cl1 C26 Cl1 C26 -17(3) 4_565 . 4_565
Cl1 C26 Cl1 C26 113(3) 3_655 . 4_565
Cl1 C26 Cl1 C26 53(2) 2_665 . 4_565
C26 C26 Cl1 C25 68.8(4) 3_655 . 2_665
C26 C26 Cl1 C25 -54(2) 4_565 . 2_665
C26 C26 Cl1 C25 29(2) 2_665 . 2_665
C25 C26 Cl1 C25 -9.2(9) . . 2_665
C25 C26 Cl1 C25 10.0(7) 3_655 . 2_665
C25 C26 Cl1 C25 -17.6(6) 4_565 . 2_665
Cl1 C26 Cl1 C25 -71.3(6) 4_565 . 2_665
Cl1 C26 Cl1 C25 58.7(7) 3_655 . 2_665
Cl1 C26 Cl1 C25 -1.17(11) 2_665 . 2_665
C26 C26 Cl1 C26 39(2) 3_655 . 2_665
C26 C26 Cl1 C26 -83.4(4) 4_565 . 2_665
C25 C26 Cl1 C26 -39(3) . . 2_665
C25 C26 Cl1 C26 -19(3) 3_655 . 2_665
C25 C26 Cl1 C26 -47(3) 4_565 . 2_665
C25 C26 Cl1 C26 -29(2) 2_665 . 2_665
Cl1 C26 Cl1 C26 -101(3) 4_565 . 2_665
Cl1 C26 Cl1 C26 29(3) 3_655 . 2_665
Cl1 C26 Cl1 C26 -31(3) 2_665 . 2_665
C1 Pt1 Pt1 C1 -38.1(5) . 5_556 5_556
