#------------------------------------------------------------------------------
#$Date: 2016-03-21 11:09:19 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178682 $
#$URL: svn://www.crystallography.net/cod/cif/4/07/93/4079399.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4079399
loop_
_publ_author_name
'Arii, Hidekazu'
'Hashimoto, Rei'
'Mochida, Kunio'
'Kawashima, Takayuki'
_publ_section_title
;
 Syntheses of Di- and Trinuclear Platinum Complexes with Multibridged
 Germanium Centers Derived from Unsymmetrical Digermanes
;
_journal_issue                   18
_journal_name_full               Organometallics
_journal_page_first              6635
_journal_paper_doi               10.1021/om3007147
_journal_volume                  31
_journal_year                    2012
_chemical_formula_sum            'C67 H68 Ge3 P4 Pt2'
_chemical_formula_weight         1605.04
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           11
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2yb'
_symmetry_space_group_name_H-M   'P 1 21/m 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 106.6870(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            2
_cell_length_a                   9.9454(11)
_cell_length_b                   25.845(3)
_cell_length_c                   12.3586(13)
_cell_measurement_reflns_used    9916
_cell_measurement_temperature    123
_cell_measurement_theta_max      27.54
_cell_measurement_theta_min      2.33
_cell_volume                     3042.9(6)
_computing_cell_refinement       'APEX2 (Bruker AXS, 2006)'
_computing_data_collection       'APEX2 (Bruker AXS, 2006)'
_computing_data_reduction        'SAINT (Bruker AXS, 2004)'
_computing_molecular_graphics    'XSHEL (Bruker AXS,2002)'
_computing_publication_material  'XCIF (Bruker AXS, 2001)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      123
_diffrn_detector_area_resol_mean 8.333
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'Bruker APEXII CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  'Bruker Helios multilayer confocal mirror'
_diffrn_radiation_source         'Bruker TXS fine-focus rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0271
_diffrn_reflns_av_sigmaI/netI    0.0216
_diffrn_reflns_limit_h_max       12
_diffrn_reflns_limit_h_min       -12
_diffrn_reflns_limit_k_max       33
_diffrn_reflns_limit_k_min       -33
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -16
_diffrn_reflns_number            34435
_diffrn_reflns_theta_full        27.59
_diffrn_reflns_theta_max         27.59
_diffrn_reflns_theta_min         1.58
_exptl_absorpt_coefficient_mu    6.191
_exptl_absorpt_correction_T_max  0.6711
_exptl_absorpt_correction_T_min  0.5764
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details
;
SADABS Sheldrick 1996
;
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.752
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1564
_exptl_crystal_size_max          0.10
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.07
_refine_diff_density_max         5.266
_refine_diff_density_min         -1.325
_refine_diff_density_rms         0.116
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.054
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     372
_refine_ls_number_reflns         7144
_refine_ls_number_restraints     40
_refine_ls_restrained_S_all      1.077
_refine_ls_R_factor_all          0.0334
_refine_ls_R_factor_gt           0.0276
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[\ss²(Fo²)+(0.0255P)²+8.6217P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0622
_refine_ls_wR_factor_ref         0.0646
_reflns_number_gt                6365
_reflns_number_total             7144
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om3007147_si_002.cif
_cod_data_source_block           complex3
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      'P2(1)/m  '
_cod_database_code               4079399
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z'
'-x, -y, -z'
'x, -y-1/2, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pt1 Pt 0.009650(14) 0.171631(5) 0.228350(11) 0.02092(5) Uani 1 1 d .
Ge1 Ge -0.03896(6) 0.2500 0.10777(4) 0.02131(11) Uani 1 2 d S
Ge2 Ge -0.29274(6) 0.2500 0.03870(5) 0.02671(13) Uani 1 2 d S
Ge3 Ge 0.04550(6) 0.2500 0.34634(5) 0.02470(12) Uani 1 2 d SD
P1 P 0.02482(10) 0.10628(4) 0.10679(8) 0.0242(2) Uani 1 1 d .
P2 P 0.03004(10) 0.10799(4) 0.36055(8) 0.02192(19) Uani 1 1 d .
C1 C 0.0111(4) 0.04410(15) 0.1775(3) 0.0270(8) Uani 1 1 d .
H1A H -0.0888 0.0358 0.1682 0.032 Uiso 1 1 calc R
H1B H 0.0523 0.0159 0.1431 0.032 Uiso 1 1 calc R
C2 C 0.0903(4) 0.04898(14) 0.3036(3) 0.0268(8) Uani 1 1 d .
H2A H 0.1925 0.0511 0.3136 0.032 Uiso 1 1 calc R
H2B H 0.0720 0.0182 0.3449 0.032 Uiso 1 1 calc R
C3 C -0.0880(4) 0.09573(17) -0.0367(3) 0.0306(9) Uani 1 1 d .
C4 C -0.0592(5) 0.1216(2) -0.1261(4) 0.0422(11) Uani 1 1 d .
H4 H 0.0182 0.1447 -0.1125 0.051 Uiso 1 1 calc R
C5 C -0.1449(6) 0.1135(2) -0.2366(4) 0.0551(15) Uani 1 1 d .
H5 H -0.1256 0.1312 -0.2979 0.066 Uiso 1 1 calc R
C6 C -0.2575(6) 0.0800(2) -0.2565(4) 0.0578(17) Uani 1 1 d .
H6 H -0.3134 0.0738 -0.3317 0.069 Uiso 1 1 calc R
C7 C -0.2889(5) 0.0556(2) -0.1690(5) 0.0514(14) Uani 1 1 d .
H7 H -0.3679 0.0333 -0.1832 0.062 Uiso 1 1 calc R
C8 C -0.2055(4) 0.06341(17) -0.0590(4) 0.0373(10) Uani 1 1 d .
H8 H -0.2286 0.0466 0.0017 0.045 Uiso 1 1 calc R
C9 C 0.2016(4) 0.10043(15) 0.0898(3) 0.0270(8) Uani 1 1 d .
C10 C 0.3111(5) 0.12865(18) 0.1595(4) 0.0378(10) Uani 1 1 d .
H10 H 0.2932 0.1527 0.2119 0.045 Uiso 1 1 calc R
C11 C 0.4477(5) 0.1218(2) 0.1527(5) 0.0479(12) Uani 1 1 d .
H11 H 0.5226 0.1411 0.2005 0.057 Uiso 1 1 calc R
C12 C 0.4743(5) 0.08715(19) 0.0773(4) 0.0435(11) Uani 1 1 d .
H12 H 0.5678 0.0823 0.0740 0.052 Uiso 1 1 calc R
C13 C 0.3664(5) 0.05933(19) 0.0062(4) 0.0388(10) Uani 1 1 d .
H13 H 0.3850 0.0358 -0.0468 0.047 Uiso 1 1 calc R
C14 C 0.2309(4) 0.06588(17) 0.0127(3) 0.0324(9) Uani 1 1 d .
H14 H 0.1566 0.0466 -0.0361 0.039 Uiso 1 1 calc R
C15 C -0.1365(4) 0.08966(15) 0.3853(3) 0.0251(8) Uani 1 1 d .
C16 C -0.2186(4) 0.12905(16) 0.4113(4) 0.0322(9) Uani 1 1 d .
H16 H -0.1883 0.1640 0.4137 0.039 Uiso 1 1 calc R
C17 C -0.3443(5) 0.11724(18) 0.4336(4) 0.0407(11) Uani 1 1 d .
H17 H -0.3982 0.1440 0.4536 0.049 Uiso 1 1 calc R
C18 C -0.3916(5) 0.06635(19) 0.4268(4) 0.0397(10) Uani 1 1 d .
H18 H -0.4789 0.0585 0.4399 0.048 Uiso 1 1 calc R
C19 C -0.3118(5) 0.02745(18) 0.4010(4) 0.0403(10) Uani 1 1 d .
H19 H -0.3434 -0.0074 0.3971 0.048 Uiso 1 1 calc R
C20 C -0.1843(5) 0.03917(16) 0.3806(4) 0.0343(9) Uani 1 1 d .
H20 H -0.1294 0.0121 0.3631 0.041 Uiso 1 1 calc R
C21 C 0.1519(4) 0.11049(14) 0.5023(3) 0.0235(7) Uani 1 1 d .
C22 C 0.2918(4) 0.12273(17) 0.5125(4) 0.0336(9) Uani 1 1 d .
H22 H 0.3200 0.1303 0.4470 0.040 Uiso 1 1 calc R
C23 C 0.3904(4) 0.12386(17) 0.6190(4) 0.0383(10) Uani 1 1 d .
H23 H 0.4859 0.1316 0.6256 0.046 Uiso 1 1 calc R
C24 C 0.3498(5) 0.11384(17) 0.7144(4) 0.0362(10) Uani 1 1 d .
H24 H 0.4171 0.1148 0.7867 0.043 Uiso 1 1 calc R
C25 C 0.2118(5) 0.10245(19) 0.7053(4) 0.0384(10) Uani 1 1 d .
H25 H 0.1839 0.0958 0.7713 0.046 Uiso 1 1 calc R
C26 C 0.1131(4) 0.10068(16) 0.5996(3) 0.0302(9) Uani 1 1 d .
H26 H 0.0181 0.0927 0.5940 0.036 Uiso 1 1 calc R
C27 C 0.0385(7) 0.2500 -0.0227(5) 0.0459(15) Uani 1 2 d SDU
C28 C -0.0459(9) 0.2500 -0.1339(6) 0.0587(18) Uani 1 2 d SDU
H28 H -0.1451 0.2500 -0.1488 0.070 Uiso 1 2 calc SR
C29 C 0.0117(12) 0.2500 -0.2232(8) 0.093(3) Uani 1 2 d SDU
H29 H -0.0469 0.2500 -0.2990 0.112 Uiso 1 2 calc SR
C30 C 0.1548(14) 0.2500 -0.2006(10) 0.117(3) Uani 1 2 d SDU
H30 H 0.1952 0.2500 -0.2615 0.141 Uiso 1 2 calc SR
C31 C 0.2403(13) 0.2500 -0.0927(10) 0.114(3) Uani 1 2 d SDU
H31 H 0.3393 0.2500 -0.0789 0.137 Uiso 1 2 calc SR
C32 C 0.1832(9) 0.2500 -0.0030(8) 0.082(2) Uani 1 2 d SDU
H32 H 0.2432 0.2500 0.0723 0.098 Uiso 1 2 calc SR
C33 C -0.3620(7) 0.2500 0.1727(6) 0.0418(15) Uani 1 2 d S
H33A H -0.3220 0.2795 0.2210 0.063 Uiso 0.50 1 calc PR
H33B H -0.3339 0.2178 0.2150 0.063 Uiso 0.50 1 calc PR
H33C H -0.4647 0.2527 0.1489 0.063 Uiso 0.50 1 calc PR
C34 C -0.3697(5) 0.18946(18) -0.0538(4) 0.0412(11) Uani 1 1 d .
H34A H -0.4725 0.1912 -0.0767 0.062 Uiso 1 1 calc R
H34B H -0.3388 0.1579 -0.0098 0.062 Uiso 1 1 calc R
H34C H -0.3364 0.1890 -0.1211 0.062 Uiso 1 1 calc R
C35 C 0.2478(7) 0.2500 0.4296(5) 0.0303(12) Uani 1 2 d S
C36 C 0.3488(7) 0.2500 0.3713(5) 0.0355(13) Uani 1 2 d S
H36 H 0.3192 0.2500 0.2910 0.043 Uiso 1 2 calc SR
C37 C 0.4931(7) 0.2500 0.4278(7) 0.0477(17) Uani 1 2 d S
H37 H 0.5600 0.2500 0.3863 0.057 Uiso 1 2 calc SR
C38 C 0.5365(8) 0.2500 0.5440(7) 0.056(2) Uani 1 2 d S
H38 H 0.6339 0.2500 0.5832 0.067 Uiso 1 2 calc SR
C39 C 0.4389(10) 0.2500 0.6036(7) 0.061(2) Uani 1 2 d S
H39 H 0.4694 0.2500 0.6838 0.073 Uiso 1 2 calc SR
C40 C 0.2965(8) 0.2500 0.5477(5) 0.0490(18) Uani 1 2 d S
H40 H 0.2308 0.2500 0.5903 0.059 Uiso 1 2 calc SR
H3H H -0.019(6) 0.2500 0.436(4) 0.05(2) Uiso 1 2 d SD
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ge Ge 0.1547 1.8001 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
P2 Pt1 P1 85.95(4) . .
P2 Pt1 Ge3 101.57(3) . .
P1 Pt1 Ge3 165.54(3) . .
P2 Pt1 Ge1 168.43(3) . .
P1 Pt1 Ge1 104.24(3) . .
Ge3 Pt1 Ge1 69.744(17) . .
C27 Ge1 Ge2 108.9(2) . .
C27 Ge1 Pt1 115.85(9) . 4_565
Ge2 Ge1 Pt1 102.448(17) . 4_565
C27 Ge1 Pt1 115.85(9) . .
Ge2 Ge1 Pt1 102.448(17) . .
Pt1 Ge1 Pt1 109.61(2) 4_565 .
C27 Ge1 Ge3 141.5(2) . .
Ge2 Ge1 Ge3 109.60(3) . .
Pt1 Ge1 Ge3 54.839(11) 4_565 .
Pt1 Ge1 Ge3 54.839(11) . .
C34 Ge2 C34 106.0(3) . 4_565
C34 Ge2 C33 108.56(18) . .
C34 Ge2 C33 108.56(18) 4_565 .
C34 Ge2 Ge1 113.51(14) . .
C34 Ge2 Ge1 113.51(14) 4_565 .
C33 Ge2 Ge1 106.5(2) . .
C35 Ge3 Pt1 105.11(9) . .
C35 Ge3 Pt1 105.11(9) . 4_565
Pt1 Ge3 Pt1 110.76(2) . 4_565
C35 Ge3 Ge1 119.73(17) . .
Pt1 Ge3 Ge1 55.417(12) . .
Pt1 Ge3 Ge1 55.417(12) 4_565 .
C35 Ge3 H3H 102(3) . .
Pt1 Ge3 H3H 116.0(11) . .
Pt1 Ge3 H3H 116.0(11) 4_565 .
Ge1 Ge3 H3H 138(3) . .
C3 P1 C9 102.58(18) . .
C3 P1 C1 102.73(19) . .
C9 P1 C1 100.68(18) . .
C3 P1 Pt1 127.46(13) . .
C9 P1 Pt1 112.40(13) . .
C1 P1 Pt1 107.59(12) . .
C21 P2 C15 103.45(17) . .
C21 P2 C2 101.31(17) . .
C15 P2 C2 104.92(18) . .
C21 P2 Pt1 124.00(12) . .
C15 P2 Pt1 114.01(12) . .
C2 P2 Pt1 107.05(13) . .
C2 C1 P1 108.7(3) . .
C2 C1 H1A 109.9 . .
P1 C1 H1A 109.9 . .
C2 C1 H1B 109.9 . .
P1 C1 H1B 109.9 . .
H1A C1 H1B 108.3 . .
C1 C2 P2 109.0(3) . .
C1 C2 H2A 109.9 . .
P2 C2 H2A 109.9 . .
C1 C2 H2B 109.9 . .
P2 C2 H2B 109.9 . .
H2A C2 H2B 108.3 . .
C4 C3 C8 118.8(4) . .
C4 C3 P1 119.4(3) . .
C8 C3 P1 121.8(3) . .
C3 C4 C5 119.7(5) . .
C3 C4 H4 120.1 . .
C5 C4 H4 120.1 . .
C6 C5 C4 120.2(5) . .
C6 C5 H5 119.9 . .
C4 C5 H5 119.9 . .
C7 C6 C5 120.5(5) . .
C7 C6 H6 119.8 . .
C5 C6 H6 119.8 . .
C6 C7 C8 120.1(5) . .
C6 C7 H7 119.9 . .
C8 C7 H7 119.9 . .
C7 C8 C3 120.6(5) . .
C7 C8 H8 119.7 . .
C3 C8 H8 119.7 . .
C10 C9 C14 118.7(4) . .
C10 C9 P1 119.5(3) . .
C14 C9 P1 121.7(3) . .
C9 C10 C11 120.0(4) . .
C9 C10 H10 120.0 . .
C11 C10 H10 120.0 . .
C12 C11 C10 120.3(4) . .
C12 C11 H11 119.8 . .
C10 C11 H11 119.8 . .
C11 C12 C13 120.4(4) . .
C11 C12 H12 119.8 . .
C13 C12 H12 119.8 . .
C12 C13 C14 119.5(4) . .
C12 C13 H13 120.2 . .
C14 C13 H13 120.2 . .
C13 C14 C9 121.0(4) . .
C13 C14 H14 119.5 . .
C9 C14 H14 119.5 . .
C20 C15 C16 118.7(4) . .
C20 C15 P2 123.6(3) . .
C16 C15 P2 117.8(3) . .
C17 C16 C15 120.2(4) . .
C17 C16 H16 119.9 . .
C15 C16 H16 119.9 . .
C16 C17 C18 120.2(4) . .
C16 C17 H17 119.9 . .
C18 C17 H17 119.9 . .
C19 C18 C17 119.9(4) . .
C19 C18 H18 120.1 . .
C17 C18 H18 120.1 . .
C18 C19 C20 119.9(4) . .
C18 C19 H19 120.0 . .
C20 C19 H19 120.0 . .
C15 C20 C19 121.0(4) . .
C15 C20 H20 119.5 . .
C19 C20 H20 119.5 . .
C26 C21 C22 118.7(4) . .
C26 C21 P2 123.5(3) . .
C22 C21 P2 117.7(3) . .
C21 C22 C23 120.1(4) . .
C21 C22 H22 120.0 . .
C23 C22 H22 120.0 . .
C24 C23 C22 120.2(4) . .
C24 C23 H23 119.9 . .
C22 C23 H23 119.9 . .
C25 C24 C23 120.1(4) . .
C25 C24 H24 120.0 . .
C23 C24 H24 120.0 . .
C24 C25 C26 120.2(4) . .
C24 C25 H25 119.9 . .
C26 C25 H25 119.9 . .
C21 C26 C25 120.7(4) . .
C21 C26 H26 119.6 . .
C25 C26 H26 119.6 . .
C32 C27 C28 118.3(7) . .
C32 C27 Ge1 118.9(6) . .
C28 C27 Ge1 122.7(5) . .
C29 C28 C27 121.3(8) . .
C29 C28 H28 119.4 . .
C27 C28 H28 119.4 . .
C30 C29 C28 118.8(9) . .
C30 C29 H29 120.6 . .
C28 C29 H29 120.6 . .
C31 C30 C29 121.4(9) . .
C31 C30 H30 119.3 . .
C29 C30 H30 119.3 . .
C30 C31 C32 120.1(11) . .
C30 C31 H31 120.0 . .
C32 C31 H31 120.0 . .
C31 C32 C27 120.1(10) . .
C31 C32 H32 119.9 . .
C27 C32 H32 119.9 . .
Ge2 C33 H33A 109.5 . .
Ge2 C33 H33B 109.5 . .
H33A C33 H33B 109.5 . .
Ge2 C33 H33C 109.5 . .
H33A C33 H33C 109.5 . .
H33B C33 H33C 109.5 . .
Ge2 C34 H34A 109.5 . .
Ge2 C34 H34B 109.5 . .
H34A C34 H34B 109.5 . .
Ge2 C34 H34C 109.5 . .
H34A C34 H34C 109.5 . .
H34B C34 H34C 109.5 . .
C36 C35 C40 117.0(6) . .
C36 C35 Ge3 120.5(4) . .
C40 C35 Ge3 122.6(5) . .
C35 C36 C37 121.8(6) . .
C35 C36 H36 119.1 . .
C37 C36 H36 119.1 . .
C38 C37 C36 119.3(8) . .
C38 C37 H37 120.3 . .
C36 C37 H37 120.3 . .
C37 C38 C39 120.0(7) . .
C37 C38 H38 120.0 . .
C39 C38 H38 120.0 . .
C38 C39 C40 120.7(7) . .
C38 C39 H39 119.7 . .
C40 C39 H39 119.7 . .
C39 C40 C35 121.2(7) . .
C39 C40 H40 119.4 . .
C35 C40 H40 119.4 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pt1 P2 2.2859(10) .
Pt1 P1 2.2939(10) .
Pt1 Ge3 2.4612(4) .
Pt1 Ge1 2.4786(4) .
Ge1 C27 1.976(6) .
Ge1 Ge2 2.4211(8) .
Ge1 Pt1 2.4785(4) 4_565
Ge1 Ge3 2.8243(8) .
Ge2 C34 1.959(4) .
Ge2 C34 1.959(4) 4_565
Ge2 C33 1.968(6) .
Ge3 C35 1.979(6) .
Ge3 Pt1 2.4612(4) 4_565
Ge3 H3H 1.433(10) .
P1 C3 1.826(4) .
P1 C9 1.836(4) .
P1 C1 1.853(4) .
P2 C21 1.823(4) .
P2 C15 1.831(4) .
P2 C2 1.850(4) .
C1 C2 1.536(5) .
C1 H1A 0.9900 .
C1 H1B 0.9900 .
C2 H2A 0.9900 .
C2 H2B 0.9900 .
C3 C4 1.391(6) .
C3 C8 1.399(6) .
C4 C5 1.402(6) .
C4 H4 0.9500 .
C5 C6 1.381(9) .
C5 H5 0.9500 .
C6 C7 1.363(8) .
C6 H6 0.9500 .
C7 C8 1.389(6) .
C7 H7 0.9500 .
C8 H8 0.9500 .
C9 C10 1.386(6) .
C9 C14 1.396(5) .
C10 C11 1.397(6) .
C10 H10 0.9500 .
C11 C12 1.371(7) .
C11 H11 0.9500 .
C12 C13 1.378(7) .
C12 H12 0.9500 .
C13 C14 1.383(6) .
C13 H13 0.9500 .
C14 H14 0.9500 .
C15 C20 1.384(6) .
C15 C16 1.399(5) .
C16 C17 1.389(6) .
C16 H16 0.9500 .
C17 C18 1.391(7) .
C17 H17 0.9500 .
C18 C19 1.373(7) .
C18 H18 0.9500 .
C19 C20 1.396(6) .
C19 H19 0.9500 .
C20 H20 0.9500 .
C21 C26 1.389(5) .
C21 C22 1.397(5) .
C22 C23 1.398(6) .
C22 H22 0.9500 .
C23 C24 1.377(6) .
C23 H23 0.9500 .
C24 C25 1.376(6) .
C24 H24 0.9500 .
C25 C26 1.391(6) .
C25 H25 0.9500 .
C26 H26 0.9500 .
C27 C32 1.389(11) .
C27 C28 1.390(10) .
C28 C29 1.382(11) .
C28 H28 0.9500 .
C29 C30 1.369(15) .
C29 H29 0.9500 .
C30 C31 1.360(16) .
C30 H30 0.9500 .
C31 C32 1.383(12) .
C31 H31 0.9500 .
C32 H32 0.9500 .
C33 H33A 0.9800 .
C33 H33B 0.9800 .
C33 H33C 0.9800 .
C34 H34A 0.9800 .
C34 H34B 0.9800 .
C34 H34C 0.9800 .
C35 C36 1.395(9) .
C35 C40 1.400(8) .
C36 C37 1.404(9) .
C36 H36 0.9500 .
C37 C38 1.376(11) .
C37 H37 0.9500 .
C38 C39 1.377(13) .
C38 H38 0.9500 .
C39 C40 1.386(11) .
C39 H39 0.9500 .
C40 H40 0.9500 .
