#------------------------------------------------------------------------------
#$Date: 2016-03-21 13:10:46 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178692 $
#$URL: svn://www.crystallography.net/cod/cif/4/08/03/4080352.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4080352
loop_
_publ_author_name
'Edelmann, Anja'
'Lorenz, Volker'
'Hrib, Cristian G.'
'Hilfert, Liane'
'Blaurock, Steffen'
'Edelmann, Frank T.'
_publ_section_title
;
 Steric Effects in Lanthanide Sandwich Complexes Containing Bulky
 Cyclooctatetraenyl Ligands
;
_journal_issue                   5
_journal_name_full               Organometallics
_journal_page_first              1435
_journal_paper_doi               10.1021/om3010993
_journal_volume                  32
_journal_year                    2013
_chemical_formula_sum            'C42 H72 Ho2 Si6'
_chemical_formula_weight         1075.40
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                87.29(3)
_cell_angle_beta                 81.26(3)
_cell_angle_gamma                86.64(3)
_cell_formula_units_Z            2
_cell_length_a                   11.800(2)
_cell_length_b                   13.130(3)
_cell_length_c                   15.747(3)
_cell_measurement_reflns_used    18950
_cell_measurement_temperature    133(2)
_cell_measurement_theta_max      29.49
_cell_measurement_theta_min      2.00
_cell_volume                     2405.4(8)
_computing_cell_refinement       'STOE X-AREA'
_computing_data_collection       'STOE X-AREA'
_computing_data_reduction        'STOE X-RED'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      133(2)
_diffrn_detector_area_resol_mean 6.67
_diffrn_measured_fraction_theta_full 0.990
_diffrn_measured_fraction_theta_max 0.990
_diffrn_measurement_device_type  'STOE IPDS 2T'
_diffrn_measurement_method       'rotation method'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0763
_diffrn_reflns_av_sigmaI/netI    0.1185
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       19
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            20858
_diffrn_reflns_theta_full        26.37
_diffrn_reflns_theta_max         26.37
_diffrn_reflns_theta_min         1.99
_exptl_absorpt_coefficient_mu    3.441
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            orange
_exptl_crystal_density_diffrn    1.485
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       prism
_exptl_crystal_F_000             1084
_exptl_crystal_size_max          0.14
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_min          0.08
_refine_diff_density_max         1.868
_refine_diff_density_min         -1.686
_refine_diff_density_rms         0.163
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.979
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     502
_refine_ls_number_reflns         9741
_refine_ls_number_restraints     81
_refine_ls_restrained_S_all      0.999
_refine_ls_R_factor_all          0.1077
_refine_ls_R_factor_gt           0.0583
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0343P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0906
_refine_ls_wR_factor_ref         0.1011
_reflns_number_gt                6338
_reflns_number_total             9741
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om3010993_si_003.cif
_cod_data_source_block           ip169
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4080352
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ho1 Ho 0.42255(3) 1.07621(3) 0.40465(2) 0.01945(11) Uani 1 1 d . . .
Ho2 Ho 0.93179(4) 0.56686(3) 0.11258(2) 0.02511(13) Uani 1 1 d . . .
Si1 Si 0.2445(2) 1.3373(2) 0.49489(16) 0.0374(7) Uani 1 1 d . . .
Si3 Si 0.2527(2) 0.8213(2) 0.52674(16) 0.0312(6) Uani 1 1 d . . .
C1 C 0.2980(8) 1.2417(7) 0.4112(5) 0.029(2) Uani 1 1 d . . .
C2 C 0.4064(8) 1.2632(7) 0.3603(5) 0.028(2) Uani 1 1 d . . .
H2 H 0.4354 1.3248 0.3752 0.034 Uiso 1 1 calc R . .
C3 C 0.4803(8) 1.2142(7) 0.2933(5) 0.027(2) Uani 1 1 d . . .
H3 H 0.5467 1.2519 0.2754 0.032 Uiso 1 1 calc R . .
C4 C 0.4840(8) 1.1245(7) 0.2449(5) 0.022(2) Uani 1 1 d . A .
C5 C 0.4054(8) 1.0472(7) 0.2484(5) 0.029(2) Uani 1 1 d . . .
H5 H 0.4324 0.9960 0.2085 0.035 Uiso 1 1 calc R . .
C6 C 0.2975(9) 1.0256(9) 0.2954(6) 0.036(2) Uani 1 1 d . . .
H6 H 0.2686 0.9649 0.2785 0.044 Uiso 1 1 calc R . .
C7 C 0.2231(8) 1.0733(8) 0.3615(6) 0.036(2) Uani 1 1 d . . .
H7 H 0.1558 1.0368 0.3788 0.043 Uiso 1 1 calc R . .
C8 C 0.2231(8) 1.1617(8) 0.4087(5) 0.031(2) Uani 1 1 d . . .
H8 H 0.1553 1.1698 0.4495 0.037 Uiso 1 1 calc R . .
C9 C 0.1544(13) 1.2753(12) 0.5878(8) 0.080(5) Uani 1 1 d . . .
H9A H 0.1952 1.2132 0.6067 0.120 Uiso 1 1 calc R . .
H9B H 0.0818 1.2576 0.5707 0.120 Uiso 1 1 calc R . .
H9C H 0.1387 1.3225 0.6352 0.120 Uiso 1 1 calc R . .
C10 C 0.3629(12) 1.3947(10) 0.5357(8) 0.065(4) Uani 1 1 d . . .
H10A H 0.4020 1.4403 0.4910 0.097 Uiso 1 1 calc R . .
H10B H 0.4176 1.3407 0.5516 0.097 Uiso 1 1 calc R . .
H10C H 0.3323 1.4338 0.5864 0.097 Uiso 1 1 calc R . .
C11 C 0.1590(15) 1.4415(13) 0.4463(9) 0.098(7) Uani 1 1 d . . .
H11A H 0.1524 1.5015 0.4818 0.147 Uiso 1 1 calc R . .
H11B H 0.0822 1.4186 0.4433 0.147 Uiso 1 1 calc R . .
H11C H 0.1972 1.4593 0.3883 0.147 Uiso 1 1 calc R . .
Si2 Si 0.6129(2) 1.1079(2) 0.15971(15) 0.0338(6) Uani 1 1 d D . .
C12 C 0.6623(19) 0.9714(10) 0.1503(13) 0.062(7) Uani 0.606(14) 1 d PDU A 1
H12A H 0.7448 0.9664 0.1289 0.093 Uiso 0.606(14) 1 calc PR A 1
H12B H 0.6206 0.9395 0.1101 0.093 Uiso 0.606(14) 1 calc PR A 1
H12C H 0.6476 0.9362 0.2068 0.093 Uiso 0.606(14) 1 calc PR A 1
C13 C 0.5808(15) 1.1611(15) 0.0564(8) 0.050(5) Uani 0.606(14) 1 d PDU A 1
H13A H 0.6527 1.1712 0.0174 0.075 Uiso 0.606(14) 1 calc PR A 1
H13B H 0.5377 1.2269 0.0648 0.075 Uiso 0.606(14) 1 calc PR A 1
H13C H 0.5348 1.1140 0.0314 0.075 Uiso 0.606(14) 1 calc PR A 1
C14 C 0.7434(13) 1.1698(15) 0.1875(12) 0.061(6) Uani 0.606(14) 1 d PD A 1
H14A H 0.7589 1.1438 0.2442 0.091 Uiso 0.606(14) 1 calc PR A 1
H14B H 0.7285 1.2440 0.1885 0.091 Uiso 0.606(14) 1 calc PR A 1
H14C H 0.8101 1.1536 0.1443 0.091 Uiso 0.606(14) 1 calc PR A 1
C12' C 0.7278(18) 1.0255(17) 0.1944(15) 0.035(6) Uiso 0.394(14) 1 d PDU A 2
H12D H 0.7003 0.9569 0.2089 0.053 Uiso 0.394(14) 1 calc PR A 2
H12E H 0.7519 1.0534 0.2450 0.053 Uiso 0.394(14) 1 calc PR A 2
H12F H 0.7931 1.0218 0.1478 0.053 Uiso 0.394(14) 1 calc PR A 2
C13' C 0.562(2) 1.0488(19) 0.0661(14) 0.047(7) Uiso 0.394(14) 1 d PDU A 2
H13D H 0.6169 1.0610 0.0138 0.070 Uiso 0.394(14) 1 calc PR A 2
H13E H 0.4866 1.0796 0.0582 0.070 Uiso 0.394(14) 1 calc PR A 2
H13F H 0.5565 0.9752 0.0777 0.070 Uiso 0.394(14) 1 calc PR A 2
C14' C 0.658(2) 1.2365(14) 0.1220(18) 0.056(8) Uiso 0.394(14) 1 d PD A 2
H14D H 0.6781 1.2727 0.1702 0.084 Uiso 0.394(14) 1 calc PR A 2
H14E H 0.5951 1.2746 0.0986 0.084 Uiso 0.394(14) 1 calc PR A 2
H14F H 0.7251 1.2305 0.0770 0.084 Uiso 0.394(14) 1 calc PR A 2
C15 C 0.3759(7) 0.9104(6) 0.5145(5) 0.0189(17) Uani 1 1 d . . .
C16 C 0.3581(8) 0.9977(7) 0.5678(5) 0.023(2) Uani 1 1 d . . .
H16 H 0.2855 0.9989 0.6033 0.027 Uiso 1 1 calc R . .
C17 C 0.4713(7) 0.8804(7) 0.4533(5) 0.023(2) Uani 1 1 d . . .
H17 H 0.4598 0.8180 0.4285 0.028 Uiso 1 1 calc R . .
C18 C 0.5784(7) 0.9183(7) 0.4196(5) 0.022(2) Uani 1 1 d . . .
H18 H 0.6190 0.8757 0.3768 0.027 Uiso 1 1 calc R . .
C19 C 0.2326(11) 0.7758(10) 0.4204(8) 0.058(3) Uani 1 1 d . . .
H19A H 0.1665 0.7328 0.4275 0.087 Uiso 1 1 calc R . .
H19B H 0.3017 0.7360 0.3958 0.087 Uiso 1 1 calc R . .
H19C H 0.2192 0.8346 0.3819 0.087 Uiso 1 1 calc R . .
C20 C 0.2838(10) 0.7072(9) 0.5945(10) 0.070(4) Uani 1 1 d . . .
H20A H 0.2262 0.6569 0.5921 0.106 Uiso 1 1 calc R . .
H20B H 0.2813 0.7268 0.6540 0.106 Uiso 1 1 calc R . .
H20C H 0.3603 0.6773 0.5731 0.106 Uiso 1 1 calc R . .
C21 C 0.1160(8) 0.8867(10) 0.5751(7) 0.050(3) Uani 1 1 d . . .
H21A H 0.1002 0.9480 0.5400 0.074 Uiso 1 1 calc R . .
H21B H 0.1224 0.9061 0.6334 0.074 Uiso 1 1 calc R . .
H21C H 0.0532 0.8405 0.5774 0.074 Uiso 1 1 calc R . .
Si4 Si 1.0825(3) 0.8325(2) 0.15985(18) 0.0414(7) Uani 1 1 d . . .
C31 C 0.9870(9) 0.7230(7) 0.1846(5) 0.038(3) Uani 1 1 d . . .
C32 C 0.8762(9) 0.7462(7) 0.1626(5) 0.031(2) Uani 1 1 d . . .
H32 H 0.8698 0.8134 0.1381 0.037 Uiso 1 1 calc R . .
C33 C 0.7733(9) 0.6965(7) 0.1672(5) 0.031(2) Uani 1 1 d . . .
H33 H 0.7173 0.7385 0.1430 0.038 Uiso 1 1 calc R . .
C34 C 0.7296(9) 0.6019(8) 0.1976(6) 0.043(3) Uani 1 1 d . B .
C35 C 0.7810(11) 0.5156(8) 0.2385(6) 0.054(4) Uani 1 1 d . . .
H35 H 0.7305 0.4613 0.2512 0.065 Uiso 1 1 calc R . .
C36 C 0.8893(12) 0.4916(9) 0.2648(6) 0.054(4) Uani 1 1 d . . .
H36 H 0.8934 0.4257 0.2920 0.064 Uiso 1 1 calc R . .
C37 C 0.9922(12) 0.5417(9) 0.2602(6) 0.048(3) Uani 1 1 d . . .
H37 H 1.0480 0.5022 0.2870 0.057 Uiso 1 1 calc R . .
C38 C 1.0328(11) 0.6348(8) 0.2263(6) 0.044(3) Uani 1 1 d . . .
H38 H 1.1108 0.6410 0.2325 0.052 Uiso 1 1 calc R . .
C39 C 1.0776(12) 0.8894(10) 0.0502(8) 0.060(3) Uani 1 1 d . . .
H39A H 1.1081 0.8390 0.0075 0.090 Uiso 1 1 calc R . .
H39B H 1.1241 0.9495 0.0414 0.090 Uiso 1 1 calc R . .
H39C H 0.9980 0.9097 0.0439 0.090 Uiso 1 1 calc R . .
C40 C 1.2352(11) 0.7926(10) 0.1664(8) 0.063(4) Uani 1 1 d . . .
H40A H 1.2422 0.7673 0.2250 0.094 Uiso 1 1 calc R . .
H40B H 1.2831 0.8512 0.1515 0.094 Uiso 1 1 calc R . .
H40C H 1.2607 0.7383 0.1261 0.094 Uiso 1 1 calc R . .
C41 C 1.0297(10) 0.9317(9) 0.2378(8) 0.060(3) Uani 1 1 d . . .
H41A H 0.9531 0.9582 0.2282 0.090 Uiso 1 1 calc R . .
H41B H 1.0824 0.9876 0.2301 0.090 Uiso 1 1 calc R . .
H41C H 1.0257 0.9021 0.2964 0.090 Uiso 1 1 calc R . .
Si5 Si 0.5783(3) 0.5857(3) 0.1806(3) 0.0832(16) Uani 1 1 d D . .
C42 C 0.4643(15) 0.584(2) 0.2718(12) 0.069(8) Uani 0.559(16) 1 d PDU B 1
H42A H 0.4489 0.6532 0.2933 0.103 Uiso 0.559(16) 1 calc PR B 1
H42B H 0.4878 0.5380 0.3175 0.103 Uiso 0.559(16) 1 calc PR B 1
H42C H 0.3947 0.5603 0.2540 0.103 Uiso 0.559(16) 1 calc PR B 1
C43 C 0.573(2) 0.4554(15) 0.1294(16) 0.090(10) Uani 0.559(16) 1 d PD B 1
H43A H 0.5237 0.4110 0.1687 0.136 Uiso 0.559(16) 1 calc PR B 1
H43B H 0.6511 0.4233 0.1187 0.136 Uiso 0.559(16) 1 calc PR B 1
H43C H 0.5429 0.4657 0.0750 0.136 Uiso 0.559(16) 1 calc PR B 1
C44 C 0.5308(17) 0.6599(17) 0.0871(11) 0.059(7) Uani 0.559(16) 1 d PDU B 1
H44A H 0.5932 0.6587 0.0383 0.089 Uiso 0.559(16) 1 calc PR B 1
H44B H 0.5105 0.7307 0.1028 0.089 Uiso 0.559(16) 1 calc PR B 1
H44C H 0.4636 0.6294 0.0710 0.089 Uiso 0.559(16) 1 calc PR B 1
C42' C 0.519(2) 0.4925(17) 0.2646(13) 0.048(7) Uiso 0.441(16) 1 d PDU B 2
H42D H 0.4374 0.4856 0.2615 0.072 Uiso 0.441(16) 1 calc PR B 2
H42E H 0.5273 0.5162 0.3213 0.072 Uiso 0.441(16) 1 calc PR B 2
H42F H 0.5606 0.4262 0.2556 0.072 Uiso 0.441(16) 1 calc PR B 2
C43' C 0.552(3) 0.577(2) 0.0743(11) 0.058(8) Uiso 0.441(16) 1 d PDU B 2
H43D H 0.5994 0.5197 0.0474 0.088 Uiso 0.441(16) 1 calc PR B 2
H43E H 0.5721 0.6404 0.0417 0.088 Uiso 0.441(16) 1 calc PR B 2
H43F H 0.4709 0.5655 0.0744 0.088 Uiso 0.441(16) 1 calc PR B 2
C44' C 0.515(3) 0.7112(18) 0.223(2) 0.106(14) Uiso 0.441(16) 1 d PD B 2
H44D H 0.5462 0.7668 0.1839 0.159 Uiso 0.441(16) 1 calc PR B 2
H44E H 0.5353 0.7192 0.2801 0.159 Uiso 0.441(16) 1 calc PR B 2
H44F H 0.4316 0.7130 0.2261 0.159 Uiso 0.441(16) 1 calc PR B 2
C45 C 1.0777(8) 0.3971(7) 0.0625(5) 0.025(2) Uani 1 1 d . . .
C46 C 1.1415(8) 0.4847(8) 0.0356(5) 0.027(2) Uani 1 1 d . . .
H46 H 1.2157 0.4792 0.0523 0.033 Uiso 1 1 calc R . .
C47 C 0.9662(8) 0.3748(7) 0.0504(5) 0.026(2) Uani 1 1 d . . .
H47 H 0.9453 0.3107 0.0768 0.031 Uiso 1 1 calc R . .
C48 C 0.8788(8) 0.4211(7) 0.0105(5) 0.0246(19) Uani 1 1 d . . .
H48 H 0.8152 0.3790 0.0149 0.030 Uiso 1 1 calc R . .
Si6 Si 1.1524(3) 0.2967(2) 0.12849(16) 0.0453(8) Uani 1 1 d D . .
C49 C 1.0615(16) 0.2570(16) 0.2288(11) 0.034(6) Uiso 0.57(4) 1 d PDU C 1
H49A H 0.9931 0.2263 0.2151 0.051 Uiso 0.57(4) 1 calc PR C 1
H49B H 1.0383 0.3167 0.2637 0.051 Uiso 0.57(4) 1 calc PR C 1
H49C H 1.1049 0.2069 0.2611 0.051 Uiso 0.57(4) 1 calc PR C 1
C50 C 1.2783(16) 0.3584(14) 0.1640(16) 0.039(5) Uiso 0.57(4) 1 d PDU C 1
H50A H 1.3198 0.3084 0.1977 0.058 Uiso 0.57(4) 1 calc PR C 1
H50B H 1.2499 0.4167 0.1993 0.058 Uiso 0.57(4) 1 calc PR C 1
H50C H 1.3303 0.3820 0.1132 0.058 Uiso 0.57(4) 1 calc PR C 1
C51 C 1.205(2) 0.1850(15) 0.0629(13) 0.034(7) Uiso 0.57(4) 1 d PDU C 1
H51A H 1.2489 0.1366 0.0962 0.050 Uiso 0.57(4) 1 calc PR C 1
H51B H 1.2545 0.2079 0.0106 0.050 Uiso 0.57(4) 1 calc PR C 1
H51C H 1.1395 0.1515 0.0472 0.050 Uiso 0.57(4) 1 calc PR C 1
C49' C 1.0333(19) 0.229(2) 0.201(2) 0.043(8) Uiso 0.43(4) 1 d PDU C 2
H49D H 0.9872 0.1944 0.1658 0.064 Uiso 0.43(4) 1 calc PR C 2
H49E H 0.9842 0.2798 0.2355 0.064 Uiso 0.43(4) 1 calc PR C 2
H49F H 1.0671 0.1793 0.2394 0.064 Uiso 0.43(4) 1 calc PR C 2
C50' C 1.250(3) 0.345(3) 0.196(3) 0.071(11) Uiso 0.43(4) 1 d PDU C 2
H50D H 1.2926 0.2879 0.2204 0.107 Uiso 0.43(4) 1 calc PR C 2
H50E H 1.2057 0.3846 0.2418 0.107 Uiso 0.43(4) 1 calc PR C 2
H50F H 1.3044 0.3894 0.1601 0.107 Uiso 0.43(4) 1 calc PR C 2
C51' C 1.230(3) 0.196(2) 0.0582(18) 0.039(10) Uiso 0.43(4) 1 d PDU C 2
H51D H 1.2791 0.1526 0.0911 0.059 Uiso 0.43(4) 1 calc PR C 2
H51E H 1.2772 0.2289 0.0090 0.059 Uiso 0.43(4) 1 calc PR C 2
H51F H 1.1740 0.1549 0.0376 0.059 Uiso 0.43(4) 1 calc PR C 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ho Ho -0.2175 4.6783 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C3 Ho1 C2 32.7(3) . .
C3 Ho1 C8 84.1(3) . .
C2 Ho1 C8 61.9(3) . .
C3 Ho1 C5 61.3(3) . .
C2 Ho1 C5 84.5(3) . .
C8 Ho1 C5 84.0(3) . .
C3 Ho1 C1 62.9(3) . .
C2 Ho1 C1 32.9(3) . .
C8 Ho1 C1 32.4(3) . .
C5 Ho1 C1 94.3(3) . .
C3 Ho1 C7 92.1(3) . .
C2 Ho1 C7 83.9(3) . .
C8 Ho1 C7 32.1(3) . .
C5 Ho1 C7 61.2(3) . .
C1 Ho1 C7 62.0(3) . .
C3 Ho1 C6 83.4(3) . .
C2 Ho1 C6 92.9(3) . .
C8 Ho1 C6 61.4(3) . .
C5 Ho1 C6 32.0(3) . .
C1 Ho1 C6 84.8(3) . .
C7 Ho1 C6 31.8(3) . .
C3 Ho1 C4 32.6(3) . .
C2 Ho1 C4 62.9(3) . .
C8 Ho1 C4 93.7(3) . .
C5 Ho1 C4 31.9(3) . .
C1 Ho1 C4 86.4(3) . .
C7 Ho1 C4 83.9(3) . .
C6 Ho1 C4 61.4(3) . .
C3 Ho1 C17 143.4(3) . .
C2 Ho1 C17 171.9(3) . .
C8 Ho1 C17 126.0(3) . .
C5 Ho1 C17 98.0(3) . .
C1 Ho1 C17 153.4(3) . .
C7 Ho1 C17 104.1(3) . .
C6 Ho1 C17 93.3(3) . .
C4 Ho1 C17 115.9(3) . .
C3 Ho1 C18 116.8(3) . .
C2 Ho1 C18 142.3(3) . .
C8 Ho1 C18 155.8(3) . .
C5 Ho1 C18 95.3(3) . .
C1 Ho1 C18 168.5(3) . .
C7 Ho1 C18 128.8(3) . .
C6 Ho1 C18 106.7(3) . .
C4 Ho1 C18 98.4(2) . .
C17 Ho1 C18 30.0(3) . .
C3 Ho1 C16 155.2(3) . .
C2 Ho1 C16 124.8(3) . .
C8 Ho1 C16 89.2(3) . .
C5 Ho1 C16 141.7(3) . .
C1 Ho1 C16 99.9(3) . .
C7 Ho1 C16 94.8(3) . .
C6 Ho1 C16 114.1(3) . .
C4 Ho1 C16 172.1(3) . .
C17 Ho1 C16 56.8(3) . .
C18 Ho1 C16 76.3(2) . .
C3 Ho1 C15 173.4(3) . .
C2 Ho1 C15 153.9(3) . .
C8 Ho1 C15 100.8(3) . .
C5 Ho1 C15 114.5(3) . .
C1 Ho1 C15 123.4(3) . .
C7 Ho1 C15 89.9(3) . .
C6 Ho1 C15 95.1(3) . .
C4 Ho1 C15 141.7(3) . .
C17 Ho1 C15 30.1(2) . .
C18 Ho1 C15 57.4(2) . .
C16 Ho1 C15 30.5(3) . .
C38 Ho2 C33 83.9(3) . .
C38 Ho2 C37 32.0(4) . .
C33 Ho2 C37 91.6(3) . .
C38 Ho2 C32 61.4(3) . .
C33 Ho2 C32 32.1(3) . .
C37 Ho2 C32 82.9(3) . .
C38 Ho2 C36 61.7(5) . .
C33 Ho2 C36 83.0(3) . .
C37 Ho2 C36 32.2(4) . .
C32 Ho2 C36 91.9(3) . .
C38 Ho2 C35 84.7(4) . .
C33 Ho2 C35 61.1(3) . .
C37 Ho2 C35 61.8(4) . .
C32 Ho2 C35 83.7(3) . .
C36 Ho2 C35 32.3(4) . .
C38 Ho2 C31 32.6(3) . .
C33 Ho2 C31 62.1(3) . .
C37 Ho2 C31 61.8(3) . .
C32 Ho2 C31 32.3(3) . .
C36 Ho2 C31 84.7(4) . .
C35 Ho2 C31 94.3(4) . .
C38 Ho2 C34 93.9(4) . .
C33 Ho2 C34 32.0(3) . .
C37 Ho2 C34 84.2(4) . .
C32 Ho2 C34 61.7(3) . .
C36 Ho2 C34 61.8(3) . .
C35 Ho2 C34 32.3(3) . .
C31 Ho2 C34 85.5(4) . .
C38 Ho2 C48 154.8(3) . .
C33 Ho2 C48 117.3(3) . .
C37 Ho2 C48 127.6(3) . .
C32 Ho2 C48 143.6(3) . .
C36 Ho2 C48 105.2(4) . .
C35 Ho2 C48 93.7(4) . .
C31 Ho2 C48 170.1(3) . .
C34 Ho2 C48 98.1(3) . .
C38 Ho2 C46 167.2(4) . 2_765
C33 Ho2 C46 100.2(3) . 2_765
C37 Ho2 C46 157.9(4) . 2_765
C32 Ho2 C46 116.7(3) . 2_765
C36 Ho2 C46 130.7(4) . 2_765
C35 Ho2 C46 108.0(4) . 2_765
C31 Ho2 C46 140.3(3) . 2_765
C34 Ho2 C46 95.9(3) . 2_765
C48 Ho2 C46 30.4(3) . 2_765
C38 Ho2 C48 92.9(3) . 2_765
C33 Ho2 C48 132.5(3) . 2_765
C37 Ho2 C48 110.0(4) . 2_765
C32 Ho2 C48 107.3(3) . 2_765
C36 Ho2 C48 135.9(3) . 2_765
C35 Ho2 C48 165.9(3) . 2_765
C31 Ho2 C48 91.1(3) . 2_765
C34 Ho2 C48 161.6(3) . 2_765
C48 Ho2 C48 82.6(3) . 2_765
C46 Ho2 C48 75.3(3) 2_765 2_765
C38 Ho2 C47 125.4(3) . .
C33 Ho2 C47 141.6(3) . .
C37 Ho2 C47 102.4(3) . .
C32 Ho2 C47 172.8(3) . .
C36 Ho2 C47 90.2(3) . .
C35 Ho2 C47 94.4(3) . .
C31 Ho2 C47 154.9(3) . .
C34 Ho2 C47 113.6(3) . .
C48 Ho2 C47 29.4(3) . .
C46 Ho2 C47 57.3(3) 2_765 .
C48 Ho2 C47 75.7(3) 2_765 .
C10 Si1 C11 107.9(8) . .
C10 Si1 C9 107.7(7) . .
C11 Si1 C9 109.9(8) . .
C10 Si1 C1 112.0(5) . .
C11 Si1 C1 109.0(5) . .
C9 Si1 C1 110.4(6) . .
C20 Si3 C19 107.1(7) . .
C20 Si3 C21 109.3(6) . .
C19 Si3 C21 108.1(6) . .
C20 Si3 C15 110.5(4) . .
C19 Si3 C15 110.5(5) . .
C21 Si3 C15 111.2(5) . .
C8 C1 C2 131.5(8) . .
C8 C1 Si1 113.9(7) . .
C2 C1 Si1 114.6(7) . .
C8 C1 Ho1 73.5(5) . .
C2 C1 Ho1 72.6(5) . .
Si1 C1 Ho1 136.0(4) . .
C3 C2 C1 135.2(10) . .
C3 C2 Ho1 73.1(5) . .
C1 C2 Ho1 74.5(5) . .
C2 C3 C4 138.4(9) . .
C2 C3 Ho1 74.2(5) . .
C4 C3 Ho1 76.0(5) . .
C5 C4 C3 130.9(8) . .
C5 C4 Si2 114.0(6) . .
C3 C4 Si2 115.1(7) . .
C5 C4 Ho1 73.1(5) . .
C3 C4 Ho1 71.4(4) . .
Si2 C4 Ho1 139.0(4) . .
C6 C5 C4 136.9(9) . .
C6 C5 Ho1 74.6(5) . .
C4 C5 Ho1 74.9(5) . .
C5 C6 C7 134.5(11) . .
C5 C6 Ho1 73.3(6) . .
C7 C6 Ho1 73.5(6) . .
C6 C7 C8 136.1(10) . .
C6 C7 Ho1 74.7(6) . .
C8 C7 Ho1 73.6(5) . .
C7 C8 C1 136.4(9) . .
C7 C8 Ho1 74.3(5) . .
C1 C8 Ho1 74.1(5) . .
C12' Si2 C13 135.0(10) . .
C12' Si2 C14' 113.4(12) . .
C13 Si2 C14' 60.0(11) . .
C12' Si2 C12 43.5(10) . .
C13 Si2 C12 110.2(9) . .
C14' Si2 C12 140.7(12) . .
C12' Si2 C4 113.6(8) . .
C13 Si2 C4 110.4(6) . .
C14' Si2 C4 107.4(10) . .
C12 Si2 C4 111.4(7) . .
C12' Si2 C13' 108.7(11) . .
C13 Si2 C13' 47.7(9) . .
C14' Si2 C13' 106.7(11) . .
C12 Si2 C13' 68.1(11) . .
C4 Si2 C13' 106.7(9) . .
C12' Si2 C14 61.8(11) . .
C13 Si2 C14 109.1(9) . .
C14' Si2 C14 54.8(10) . .
C12 Si2 C14 103.1(9) . .
C4 Si2 C14 112.4(6) . .
C13' Si2 C14 140.2(10) . .
C17 C15 C16 129.9(8) . .
C17 C15 Si3 114.4(7) . .
C16 C15 Si3 115.7(6) . .
C17 C15 Ho1 73.3(5) . .
C16 C15 Ho1 74.5(5) . .
Si3 C15 Ho1 130.6(3) . .
C17 C15 Ho1 73.2(5) . 2_676
C16 C15 Ho1 72.2(5) . 2_676
Si3 C15 Ho1 135.1(3) . 2_676
Ho1 C15 Ho1 94.4(2) . 2_676
C18 C16 C15 135.9(8) 2_676 .
C18 C16 Ho1 76.5(5) 2_676 .
C15 C16 Ho1 75.1(4) . .
C18 C16 Ho1 72.0(5) 2_676 2_676
C15 C16 Ho1 78.5(4) . 2_676
Ho1 C16 Ho1 96.4(3) . 2_676
C18 C17 C15 137.0(9) . .
C18 C17 Ho1 75.5(5) . .
C15 C17 Ho1 76.5(5) . .
C18 C17 Ho1 73.5(5) . 2_676
C15 C17 Ho1 78.0(5) . 2_676
Ho1 C17 Ho1 96.7(3) . 2_676
C17 C18 C16 137.1(8) . 2_676
C17 C18 Ho1 74.5(5) . .
C16 C18 Ho1 78.5(5) 2_676 .
C17 C18 Ho1 77.4(5) . 2_676
C16 C18 Ho1 73.9(5) 2_676 2_676
Ho1 C18 Ho1 97.6(3) . 2_676
C41 Si4 C39 107.8(6) . .
C41 Si4 C31 107.4(5) . .
C39 Si4 C31 112.1(5) . .
C41 Si4 C40 110.7(5) . .
C39 Si4 C40 107.1(6) . .
C31 Si4 C40 111.6(6) . .
C32 C31 C38 130.8(11) . .
C32 C31 Si4 112.3(7) . .
C38 C31 Si4 116.8(8) . .
C32 C31 Ho2 73.2(5) . .
C38 C31 Ho2 72.4(6) . .
Si4 C31 Ho2 139.4(4) . .
C33 C32 C31 137.0(9) . .
C33 C32 Ho2 73.7(5) . .
C31 C32 Ho2 74.5(5) . .
C32 C33 C34 138.0(9) . .
C32 C33 Ho2 74.1(5) . .
C34 C33 Ho2 75.9(5) . .
C33 C34 C35 131.2(11) . .
C33 C34 Si5 114.6(7) . .
C35 C34 Si5 114.3(9) . .
C33 C34 Ho2 72.1(5) . .
C35 C34 Ho2 72.6(5) . .
Si5 C34 Ho2 136.5(5) . .
C36 C35 C34 135.2(12) . .
C36 C35 Ho2 73.4(6) . .
C34 C35 Ho2 75.1(5) . .
C37 C36 C35 135.5(10) . .
C37 C36 Ho2 73.8(6) . .
C35 C36 Ho2 74.3(6) . .
C38 C37 C36 135.8(10) . .
C38 C37 Ho2 73.4(6) . .
C36 C37 Ho2 74.0(6) . .
C37 C38 C31 136.3(12) . .
C37 C38 Ho2 74.7(7) . .
C31 C38 Ho2 75.0(6) . .
C43' Si5 C42 122.5(12) . .
C43' Si5 C42' 120.0(13) . .
C42 Si5 C42' 42.7(10) . .
C43' Si5 C44 36.0(11) . .
C42 Si5 C44 111.0(10) . .
C42' Si5 C44 137.9(10) . .
C43' Si5 C34 117.6(10) . .
C42 Si5 C34 119.9(8) . .
C42' Si5 C34 106.2(9) . .
C44 Si5 C34 115.8(7) . .
C43' Si5 C44' 109.0(13) . .
C42 Si5 C44' 61.9(15) . .
C42' Si5 C44' 103.2(13) . .
C44 Si5 C44' 73.8(12) . .
C34 Si5 C44' 97.5(14) . .
C43' Si5 C43 58.2(11) . .
C42 Si5 C43 104.4(11) . .
C42' Si5 C43 71.1(12) . .
C44 Si5 C43 93.7(10) . .
C34 Si5 C43 107.9(8) . .
C44' Si5 C43 154.5(15) . .
C47 C45 C46 130.1(8) . .
C47 C45 Si6 114.8(7) . .
C46 C45 Si6 115.1(7) . .
C47 C45 Ho2 73.9(5) . 2_765
C46 C45 Ho2 72.8(5) . 2_765
Si6 C45 Ho2 134.9(4) . 2_765
C47 C45 Ho2 72.6(5) . .
C46 C45 Ho2 73.8(5) . .
Si6 C45 Ho2 131.0(4) . .
Ho2 C45 Ho2 94.1(2) 2_765 .
C45 C46 C48 135.7(8) . 2_765
C45 C46 Ho2 77.4(5) . 2_765
C48 C46 Ho2 74.0(5) 2_765 2_765
C45 C46 Ho2 76.6(5) . .
C48 C46 Ho2 73.6(5) 2_765 .
Ho2 C46 Ho2 96.2(3) 2_765 .
C48 C47 C45 137.2(9) . .
C48 C47 Ho2 74.6(5) . .
C45 C47 Ho2 78.0(5) . .
C48 C47 Ho2 74.4(5) . 2_765
C45 C47 Ho2 76.7(5) . 2_765
Ho2 C47 Ho2 96.4(3) . 2_765
C47 C48 C46 137.1(9) . 2_765
C47 C48 Ho2 76.0(5) . .
C46 C48 Ho2 75.5(5) 2_765 .
C47 C48 Ho2 76.4(5) . 2_765
C46 C48 Ho2 76.2(5) 2_765 2_765
Ho2 C48 Ho2 97.4(3) . 2_765
C49 Si6 C51 111.1(10) . .
C49 Si6 C50' 87.5(14) . .
C51 Si6 C50' 117.5(15) . .
C49 Si6 C51' 118.9(13) . .
C51 Si6 C51' 10.3(14) . .
C50' Si6 C51' 109.7(13) . .
C49 Si6 C49' 21.8(9) . .
C51 Si6 C49' 96.1(13) . .
C50' Si6 C49' 108.8(14) . .
C51' Si6 C49' 105.6(12) . .
C49 Si6 C50 105.2(9) . .
C51 Si6 C50 109.9(10) . .
C50' Si6 C50 17.7(13) . .
C51' Si6 C50 100.5(13) . .
C49' Si6 C50 126.4(11) . .
C49 Si6 C45 112.9(6) . .
C51 Si6 C45 110.5(8) . .
C50' Si6 C45 115.5(13) . .
C51' Si6 C45 110.7(11) . .
C49' Si6 C45 106.0(9) . .
C50 Si6 C45 107.1(7) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ho1 C3 2.510(8) .
Ho1 C2 2.524(9) .
Ho1 C8 2.541(8) .
Ho1 C5 2.547(9) .
Ho1 C1 2.548(9) .
Ho1 C7 2.549(9) .
Ho1 C6 2.564(10) .
Ho1 C4 2.570(7) .
Ho1 C17 2.703(9) .
Ho1 C18 2.716(8) .
Ho1 C16 2.736(8) .
Ho1 C15 2.744(8) .
Ho2 C38 2.519(11) .
Ho2 C33 2.531(8) .
Ho2 C37 2.535(10) .
Ho2 C32 2.536(8) .
Ho2 C36 2.538(10) .
Ho2 C35 2.548(10) .
Ho2 C31 2.553(10) .
Ho2 C34 2.580(9) .
Ho2 C48 2.716(9) .
Ho2 C46 2.735(9) 2_765
Ho2 C48 2.734(8) 2_765
Ho2 C47 2.734(9) .
Si1 C10 1.838(13) .
Si1 C11 1.856(12) .
Si1 C9 1.858(13) .
Si1 C1 1.877(9) .
Si3 C20 1.850(11) .
Si3 C19 1.857(12) .
Si3 C21 1.855(10) .
Si3 C15 1.900(9) .
C1 C8 1.418(14) .
C1 C2 1.437(13) .
C2 C3 1.417(11) .
C3 C4 1.427(12) .
C4 C5 1.408(14) .
C4 Si2 1.879(8) .
C5 C6 1.410(14) .
C6 C7 1.402(13) .
C7 C8 1.407(13) .
Si2 C12' 1.818(14) .
Si2 C13 1.825(12) .
Si2 C14' 1.845(15) .
Si2 C12 1.858(12) .
Si2 C13' 1.888(15) .
Si2 C14 1.900(14) .
C15 C17 1.416(11) .
C15 C16 1.439(12) .
C15 Ho1 2.881(8) 2_676
C16 C18 1.407(13) 2_676
C16 Ho1 2.799(8) 2_676
C17 C18 1.404(13) .
C17 Ho1 2.820(8) 2_676
C18 C16 1.407(13) 2_676
C18 Ho1 2.769(8) 2_676
Si4 C41 1.849(11) .
Si4 C39 1.856(12) .
Si4 C31 1.868(12) .
Si4 C40 1.864(13) .
C31 C32 1.416(13) .
C31 C38 1.424(13) .
C32 C33 1.403(14) .
C33 C34 1.408(14) .
C34 C35 1.427(13) .
C34 Si5 1.870(13) .
C35 C36 1.416(18) .
C36 C37 1.405(18) .
C37 C38 1.392(17) .
Si5 C43' 1.758(15) .
Si5 C42 1.812(14) .
Si5 C42' 1.844(15) .
Si5 C44 1.867(14) .
Si5 C44' 1.875(17) .
Si5 C43 1.934(16) .
C45 C47 1.407(13) .
C45 C46 1.423(14) .
C45 Si6 1.899(8) .
C45 Ho2 2.793(8) 2_765
C46 C48 1.431(12) 2_765
C46 Ho2 2.735(9) 2_765
C47 C48 1.385(12) .
C47 Ho2 2.758(9) 2_765
C48 C46 1.431(12) 2_765
C48 Ho2 2.734(8) 2_765
Si6 C49 1.841(12) .
Si6 C51 1.856(12) .
Si6 C50' 1.837(15) .
Si6 C51' 1.867(14) .
Si6 C49' 1.904(14) .
Si6 C50 1.901(13) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C10 Si1 C1 C8 149.9(7) . .
C11 Si1 C1 C8 -90.8(9) . .
C9 Si1 C1 C8 29.9(8) . .
C10 Si1 C1 C2 -30.9(8) . .
C11 Si1 C1 C2 88.4(9) . .
C9 Si1 C1 C2 -150.9(7) . .
C10 Si1 C1 Ho1 59.1(9) . .
C11 Si1 C1 Ho1 178.4(9) . .
C9 Si1 C1 Ho1 -60.8(9) . .
C3 Ho1 C1 C8 126.3(6) . .
C2 Ho1 C1 C8 144.7(7) . .
C5 Ho1 C1 C8 71.7(5) . .
C7 Ho1 C1 C8 17.7(5) . .
C6 Ho1 C1 C8 41.1(5) . .
C4 Ho1 C1 C8 102.7(5) . .
C17 Ho1 C1 C8 -45.7(8) . .
C18 Ho1 C1 C8 -142.2(13) . .
C16 Ho1 C1 C8 -72.5(5) . .
C15 Ho1 C1 C8 -51.5(5) . .
C3 Ho1 C1 C2 -18.4(5) . .
C8 Ho1 C1 C2 -144.7(7) . .
C5 Ho1 C1 C2 -73.0(5) . .
C7 Ho1 C1 C2 -127.0(6) . .
C6 Ho1 C1 C2 -103.6(5) . .
C4 Ho1 C1 C2 -42.0(5) . .
C17 Ho1 C1 C2 169.6(6) . .
C18 Ho1 C1 C2 73.1(14) . .
C16 Ho1 C1 C2 142.8(5) . .
C15 Ho1 C1 C2 163.7(5) . .
C3 Ho1 C1 Si1 -126.1(8) . .
C2 Ho1 C1 Si1 -107.7(9) . .
C8 Ho1 C1 Si1 107.6(9) . .
C5 Ho1 C1 Si1 179.3(7) . .
C7 Ho1 C1 Si1 125.3(8) . .
C6 Ho1 C1 Si1 148.7(8) . .
C4 Ho1 C1 Si1 -149.7(8) . .
C17 Ho1 C1 Si1 61.9(11) . .
C18 Ho1 C1 Si1 -34.6(19) . .
C16 Ho1 C1 Si1 35.1(8) . .
C15 Ho1 C1 Si1 56.1(8) . .
C8 C1 C2 C3 -2.8(15) . .
Si1 C1 C2 C3 178.2(8) . .
Ho1 C1 C2 C3 44.9(9) . .
C8 C1 C2 Ho1 -47.7(8) . .
Si1 C1 C2 Ho1 133.3(5) . .
C8 Ho1 C2 C3 -128.1(6) . .
C5 Ho1 C2 C3 -42.0(6) . .
C1 Ho1 C2 C3 -148.7(8) . .
C7 Ho1 C2 C3 -103.5(6) . .
C6 Ho1 C2 C3 -72.9(6) . .
C4 Ho1 C2 C3 -17.3(5) . .
C17 Ho1 C2 C3 66(2) . .
C18 Ho1 C2 C3 49.5(7) . .
C16 Ho1 C2 C3 164.8(5) . .
C15 Ho1 C2 C3 179.3(6) . .
C3 Ho1 C2 C1 148.7(8) . .
C8 Ho1 C2 C1 20.5(5) . .
C5 Ho1 C2 C1 106.7(5) . .
C7 Ho1 C2 C1 45.1(5) . .
C6 Ho1 C2 C1 75.7(5) . .
C4 Ho1 C2 C1 131.4(6) . .
C17 Ho1 C2 C1 -144.9(17) . .
C18 Ho1 C2 C1 -161.8(4) . .
C16 Ho1 C2 C1 -46.5(6) . .
C15 Ho1 C2 C1 -32.1(9) . .
C1 C2 C3 C4 0.5(17) . .
Ho1 C2 C3 C4 45.8(10) . .
C1 C2 C3 Ho1 -45.3(9) . .
C8 Ho1 C3 C2 44.2(6) . .
C5 Ho1 C3 C2 130.6(6) . .
C1 Ho1 C3 C2 18.5(5) . .
C7 Ho1 C3 C2 75.3(6) . .
C6 Ho1 C3 C2 106.0(6) . .
C4 Ho1 C3 C2 150.6(8) . .
C17 Ho1 C3 C2 -167.5(5) . .
C18 Ho1 C3 C2 -148.6(5) . .
C16 Ho1 C3 C2 -30.9(10) . .
C15 Ho1 C3 C2 -177(2) . .
C2 Ho1 C3 C4 -150.6(8) . .
C8 Ho1 C3 C4 -106.4(5) . .
C5 Ho1 C3 C4 -20.0(5) . .
C1 Ho1 C3 C4 -132.1(6) . .
C7 Ho1 C3 C4 -75.2(5) . .
C6 Ho1 C3 C4 -44.6(5) . .
C17 Ho1 C3 C4 42.0(8) . .
C18 Ho1 C3 C4 60.9(6) . .
C16 Ho1 C3 C4 178.6(6) . .
C15 Ho1 C3 C4 32(3) . .
C2 C3 C4 C5 0.5(16) . .
Ho1 C3 C4 C5 45.9(8) . .
C2 C3 C4 Si2 178.5(8) . .
Ho1 C3 C4 Si2 -136.2(5) . .
C2 C3 C4 Ho1 -45.3(9) . .
C3 Ho1 C4 C5 -145.5(8) . .
C2 Ho1 C4 C5 -128.1(6) . .
C8 Ho1 C4 C5 -72.5(5) . .
C1 Ho1 C4 C5 -104.0(5) . .
C7 Ho1 C4 C5 -41.9(5) . .
C6 Ho1 C4 C5 -18.0(5) . .
C17 Ho1 C4 C5 60.8(5) . .
C18 Ho1 C4 C5 86.5(5) . .
C16 Ho1 C4 C5 39(2) . .
C15 Ho1 C4 C5 40.2(7) . .
C2 Ho1 C4 C3 17.3(5) . .
C8 Ho1 C4 C3 73.0(5) . .
C5 Ho1 C4 C3 145.5(8) . .
C1 Ho1 C4 C3 41.5(5) . .
C7 Ho1 C4 C3 103.6(5) . .
C6 Ho1 C4 C3 127.4(6) . .
C17 Ho1 C4 C3 -153.7(5) . .
C18 Ho1 C4 C3 -128.0(5) . .
C16 Ho1 C4 C3 -175.6(18) . .
C15 Ho1 C4 C3 -174.3(5) . .
C3 Ho1 C4 Si2 107.2(10) . .
C2 Ho1 C4 Si2 124.5(8) . .
C8 Ho1 C4 Si2 -179.8(7) . .
C5 Ho1 C4 Si2 -107.3(9) . .
C1 Ho1 C4 Si2 148.6(8) . .
C7 Ho1 C4 Si2 -149.2(8) . .
C6 Ho1 C4 Si2 -125.4(8) . .
C17 Ho1 C4 Si2 -46.5(8) . .
C18 Ho1 C4 Si2 -20.8(8) . .
C16 Ho1 C4 Si2 -68(2) . .
C15 Ho1 C4 Si2 -67.2(9) . .
C3 C4 C5 C6 1.1(17) . .
Si2 C4 C5 C6 -176.9(9) . .
Ho1 C4 C5 C6 46.4(10) . .
C3 C4 C5 Ho1 -45.3(8) . .
Si2 C4 C5 Ho1 136.7(5) . .
C3 Ho1 C5 C6 -128.8(6) . .
C2 Ho1 C5 C6 -104.5(6) . .
C8 Ho1 C5 C6 -42.3(6) . .
C1 Ho1 C5 C6 -73.0(6) . .
C7 Ho1 C5 C6 -18.4(6) . .
C4 Ho1 C5 C6 -149.1(8) . .
C17 Ho1 C5 C6 83.3(6) . .
C18 Ho1 C5 C6 113.4(6) . .
C16 Ho1 C5 C6 38.8(7) . .
C15 Ho1 C5 C6 56.9(6) . .
C3 Ho1 C5 C4 20.4(5) . .
C2 Ho1 C5 C4 44.7(5) . .
C8 Ho1 C5 C4 106.9(5) . .
C1 Ho1 C5 C4 76.2(5) . .
C7 Ho1 C5 C4 130.8(6) . .
C6 Ho1 C5 C4 149.1(8) . .
C17 Ho1 C5 C4 -127.5(5) . .
C18 Ho1 C5 C4 -97.4(5) . .
C16 Ho1 C5 C4 -172.0(4) . .
C15 Ho1 C5 C4 -153.9(4) . .
C4 C5 C6 C7 -1.7(18) . .
Ho1 C5 C6 C7 44.8(10) . .
C4 C5 C6 Ho1 -46.5(10) . .
C3 Ho1 C6 C5 43.5(6) . .
C2 Ho1 C6 C5 74.8(6) . .
C8 Ho1 C6 C5 130.4(7) . .
C1 Ho1 C6 C5 106.8(6) . .
C7 Ho1 C6 C5 148.4(9) . .
C4 Ho1 C6 C5 18.0(5) . .
C17 Ho1 C6 C5 -99.9(6) . .
C18 Ho1 C6 C5 -72.6(6) . .
C16 Ho1 C6 C5 -154.8(5) . .
C15 Ho1 C6 C5 -130.1(6) . .
C3 Ho1 C6 C7 -104.9(6) . .
C2 Ho1 C6 C7 -73.6(6) . .
C8 Ho1 C6 C7 -18.0(6) . .
C5 Ho1 C6 C7 -148.4(9) . .
C1 Ho1 C6 C7 -41.6(6) . .
C4 Ho1 C6 C7 -130.4(7) . .
C17 Ho1 C6 C7 111.7(6) . .
C18 Ho1 C6 C7 139.0(6) . .
C16 Ho1 C6 C7 56.8(7) . .
C15 Ho1 C6 C7 81.6(6) . .
C5 C6 C7 C8 0.3(18) . .
Ho1 C6 C7 C8 45.0(10) . .
C5 C6 C7 Ho1 -44.7(10) . .
C3 Ho1 C7 C6 73.9(6) . .
C2 Ho1 C7 C6 105.6(6) . .
C8 Ho1 C7 C6 149.3(9) . .
C5 Ho1 C7 C6 18.5(6) . .
C1 Ho1 C7 C6 131.4(7) . .
C4 Ho1 C7 C6 42.3(6) . .
C17 Ho1 C7 C6 -73.0(6) . .
C18 Ho1 C7 C6 -53.6(7) . .
C16 Ho1 C7 C6 -129.9(6) . .
C15 Ho1 C7 C6 -99.9(6) . .
C3 Ho1 C7 C8 -75.4(6) . .
C2 Ho1 C7 C8 -43.7(6) . .
C5 Ho1 C7 C8 -130.8(7) . .
C1 Ho1 C7 C8 -17.8(5) . .
C6 Ho1 C7 C8 -149.3(9) . .
C4 Ho1 C7 C8 -107.0(6) . .
C17 Ho1 C7 C8 137.7(5) . .
C18 Ho1 C7 C8 157.1(5) . .
C16 Ho1 C7 C8 80.8(6) . .
C15 Ho1 C7 C8 110.9(6) . .
C6 C7 C8 C1 -0.5(18) . .
Ho1 C7 C8 C1 44.8(10) . .
C6 C7 C8 Ho1 -45.3(10) . .
C2 C1 C8 C7 2.5(16) . .
Si1 C1 C8 C7 -178.5(8) . .
Ho1 C1 C8 C7 -44.9(10) . .
C2 C1 C8 Ho1 47.4(8) . .
Si1 C1 C8 Ho1 -133.6(5) . .
C3 Ho1 C8 C7 103.5(6) . .
C2 Ho1 C8 C7 128.8(6) . .
C5 Ho1 C8 C7 41.8(6) . .
C1 Ho1 C8 C7 149.7(8) . .
C6 Ho1 C8 C7 17.9(5) . .
C4 Ho1 C8 C7 72.3(6) . .
C17 Ho1 C8 C7 -53.7(6) . .
C18 Ho1 C8 C7 -47.7(9) . .
C16 Ho1 C8 C7 -100.4(6) . .
C15 Ho1 C8 C7 -72.1(6) . .
C3 Ho1 C8 C1 -46.1(5) . .
C2 Ho1 C8 C1 -20.9(5) . .
C5 Ho1 C8 C1 -107.8(5) . .
C7 Ho1 C8 C1 -149.7(8) . .
C6 Ho1 C8 C1 -131.8(6) . .
C4 Ho1 C8 C1 -77.3(5) . .
C17 Ho1 C8 C1 156.6(4) . .
C18 Ho1 C8 C1 162.6(5) . .
C16 Ho1 C8 C1 110.0(5) . .
C15 Ho1 C8 C1 138.3(5) . .
C5 C4 Si2 C12' -85.4(11) . .
C3 C4 Si2 C12' 96.3(11) . .
Ho1 C4 Si2 C12' 6.1(12) . .
C5 C4 Si2 C13 84.6(9) . .
C3 C4 Si2 C13 -93.7(9) . .
Ho1 C4 Si2 C13 176.2(9) . .
C5 C4 Si2 C14' 148.4(11) . .
C3 C4 Si2 C14' -30.0(11) . .
Ho1 C4 Si2 C14' -120.1(11) . .
C5 C4 Si2 C12 -38.2(11) . .
C3 C4 Si2 C12 143.5(10) . .
Ho1 C4 Si2 C12 53.4(11) . .
C5 C4 Si2 C13' 34.3(11) . .
C3 C4 Si2 C13' -144.0(10) . .
Ho1 C4 Si2 C13' 125.9(11) . .
C5 C4 Si2 C14 -153.2(9) . .
C3 C4 Si2 C14 28.4(9) . .
Ho1 C4 Si2 C14 -61.7(10) . .
C20 Si3 C15 C17 79.0(8) . .
C19 Si3 C15 C17 -39.4(7) . .
C21 Si3 C15 C17 -159.4(6) . .
C20 Si3 C15 C16 -101.3(8) . .
C19 Si3 C15 C16 140.3(6) . .
C21 Si3 C15 C16 20.3(7) . .
C20 Si3 C15 Ho1 167.5(6) . .
C19 Si3 C15 Ho1 49.1(7) . .
C21 Si3 C15 Ho1 -70.9(6) . .
C20 Si3 C15 Ho1 -11.3(8) . 2_676
C19 Si3 C15 Ho1 -129.7(6) . 2_676
C21 Si3 C15 Ho1 110.3(6) . 2_676
C3 Ho1 C15 C17 12(3) . .
C2 Ho1 C15 C17 -165.0(6) . .
C8 Ho1 C15 C17 149.5(5) . .
C5 Ho1 C15 C17 61.2(5) . .
C1 Ho1 C15 C17 174.8(5) . .
C7 Ho1 C15 C17 119.2(5) . .
C6 Ho1 C15 C17 87.7(5) . .
C4 Ho1 C15 C17 39.2(7) . .
C18 Ho1 C15 C17 -18.9(5) . .
C16 Ho1 C15 C17 -141.1(7) . .
C3 Ho1 C15 C16 153(2) . .
C2 Ho1 C15 C16 -23.8(8) . .
C8 Ho1 C15 C16 -69.3(5) . .
C5 Ho1 C15 C16 -157.6(5) . .
C1 Ho1 C15 C16 -44.1(6) . .
C7 Ho1 C15 C16 -99.7(5) . .
C6 Ho1 C15 C16 -131.1(5) . .
C4 Ho1 C15 C16 -179.7(5) . .
C17 Ho1 C15 C16 141.1(7) . .
C18 Ho1 C15 C16 122.2(5) . .
C3 Ho1 C15 Si3 -97(2) . .
C2 Ho1 C15 Si3 86.9(8) . .
C8 Ho1 C15 Si3 41.4(5) . .
C5 Ho1 C15 Si3 -46.9(6) . .
C1 Ho1 C15 Si3 66.7(6) . .
C7 Ho1 C15 Si3 11.1(5) . .
C6 Ho1 C15 Si3 -20.4(5) . .
C4 Ho1 C15 Si3 -68.9(7) . .
C17 Ho1 C15 Si3 -108.1(7) . .
C18 Ho1 C15 Si3 -127.0(6) . .
C16 Ho1 C15 Si3 110.7(7) . .
C3 Ho1 C15 Ho1 83(2) . 2_676
C2 Ho1 C15 Ho1 -94.0(6) . 2_676
C8 Ho1 C15 Ho1 -139.4(3) . 2_676
C5 Ho1 C15 Ho1 132.2(3) . 2_676
C1 Ho1 C15 Ho1 -114.2(3) . 2_676
C7 Ho1 C15 Ho1 -169.8(3) . 2_676
C6 Ho1 C15 Ho1 158.7(3) . 2_676
C4 Ho1 C15 Ho1 110.2(4) . 2_676
C17 Ho1 C15 Ho1 71.0(5) . 2_676
C18 Ho1 C15 Ho1 52.1(3) . 2_676
C16 Ho1 C15 Ho1 -70.1(5) . 2_676
C17 C15 C16 C18 0.1(14) . 2_676
Si3 C15 C16 C18 -179.5(7) . 2_676
Ho1 C15 C16 C18 -51.5(9) . 2_676
Ho1 C15 C16 C18 48.4(9) 2_676 2_676
C17 C15 C16 Ho1 51.6(7) . .
Si3 C15 C16 Ho1 -128.0(4) . .
Ho1 C15 C16 Ho1 99.9(2) 2_676 .
C17 C15 C16 Ho1 -48.3(8) . 2_676
Si3 C15 C16 Ho1 132.1(4) . 2_676
Ho1 C15 C16 Ho1 -99.9(2) . 2_676
C3 Ho1 C16 C18 -26.8(9) . 2_676
C2 Ho1 C16 C18 -46.5(6) . 2_676
C8 Ho1 C16 C18 -100.8(5) . 2_676
C5 Ho1 C16 C18 179.9(5) . 2_676
C1 Ho1 C16 C18 -70.1(5) . 2_676
C7 Ho1 C16 C18 -132.4(5) . 2_676
C6 Ho1 C16 C18 -158.7(5) . 2_676
C4 Ho1 C16 C18 147.5(18) . 2_676
C17 Ho1 C16 C18 123.9(6) . 2_676
C18 Ho1 C16 C18 98.8(5) . 2_676
C15 Ho1 C16 C18 146.0(7) . 2_676
C3 Ho1 C16 C15 -172.8(6) . .
C2 Ho1 C16 C15 167.5(4) . .
C8 Ho1 C16 C15 113.2(5) . .
C5 Ho1 C16 C15 33.9(7) . .
C1 Ho1 C16 C15 143.9(5) . .
C7 Ho1 C16 C15 81.6(5) . .
C6 Ho1 C16 C15 55.3(5) . .
C4 Ho1 C16 C15 2(2) . .
C17 Ho1 C16 C15 -22.1(4) . .
C18 Ho1 C16 C15 -47.2(5) . .
C3 Ho1 C16 Ho1 -96.5(6) . 2_676
C2 Ho1 C16 Ho1 -116.2(3) . 2_676
C8 Ho1 C16 Ho1 -170.5(3) . 2_676
C5 Ho1 C16 Ho1 110.2(4) . 2_676
C1 Ho1 C16 Ho1 -139.8(3) . 2_676
C7 Ho1 C16 Ho1 157.9(3) . 2_676
C6 Ho1 C16 Ho1 131.6(3) . 2_676
C4 Ho1 C16 Ho1 78(2) . 2_676
C17 Ho1 C16 Ho1 54.2(3) . 2_676
C18 Ho1 C16 Ho1 29.1(3) . 2_676
C15 Ho1 C16 Ho1 76.3(4) . 2_676
C16 C15 C17 C18 -1.3(15) . .
Si3 C15 C17 C18 178.3(8) . .
Ho1 C15 C17 C18 50.7(9) . .
Ho1 C15 C17 C18 -49.3(9) 2_676 .
C16 C15 C17 Ho1 -52.0(7) . .
Si3 C15 C17 Ho1 127.5(4) . .
Ho1 C15 C17 Ho1 -100.0(2) 2_676 .
C16 C15 C17 Ho1 48.0(7) . 2_676
Si3 C15 C17 Ho1 -132.5(4) . 2_676
Ho1 C15 C17 Ho1 100.0(2) . 2_676
C3 Ho1 C17 C18 35.3(7) . .
C2 Ho1 C17 C18 -21(2) . .
C8 Ho1 C17 C18 175.1(4) . .
C5 Ho1 C17 C18 86.7(5) . .
C1 Ho1 C17 C18 -156.6(6) . .
C7 Ho1 C17 C18 148.9(5) . .
C6 Ho1 C17 C18 118.5(5) . .
C4 Ho1 C17 C18 58.9(6) . .
C16 Ho1 C17 C18 -124.6(6) . .
C15 Ho1 C17 C18 -146.9(8) . .
C3 Ho1 C17 C15 -177.8(5) . .
C2 Ho1 C17 C15 126.1(17) . .
C8 Ho1 C17 C15 -38.0(6) . .
C5 Ho1 C17 C15 -126.4(5) . .
C1 Ho1 C17 C15 -9.7(9) . .
C7 Ho1 C17 C15 -64.2(5) . .
C6 Ho1 C17 C15 -94.5(5) . .
C4 Ho1 C17 C15 -154.2(5) . .
C18 Ho1 C17 C15 146.9(8) . .
C16 Ho1 C17 C15 22.3(5) . .
C3 Ho1 C17 Ho1 106.3(4) . 2_676
C2 Ho1 C17 Ho1 50.1(19) . 2_676
C8 Ho1 C17 Ho1 -113.9(3) . 2_676
C5 Ho1 C17 Ho1 157.7(3) . 2_676
C1 Ho1 C17 Ho1 -85.7(6) . 2_676
C7 Ho1 C17 Ho1 -140.1(3) . 2_676
C6 Ho1 C17 Ho1 -170.5(3) . 2_676
C4 Ho1 C17 Ho1 129.9(3) . 2_676
C18 Ho1 C17 Ho1 71.0(5) . 2_676
C16 Ho1 C17 Ho1 -53.6(3) . 2_676
C15 Ho1 C17 Ho1 -76.0(5) . 2_676
C15 C17 C18 C16 1.8(17) . 2_676
Ho1 C17 C18 C16 52.8(9) . 2_676
Ho1 C17 C18 C16 -48.8(9) 2_676 2_676
C15 C17 C18 Ho1 -51.0(9) . .
Ho1 C17 C18 Ho1 -101.7(2) 2_676 .
C15 C17 C18 Ho1 50.6(9) . 2_676
Ho1 C17 C18 Ho1 101.7(2) . 2_676
C3 Ho1 C18 C17 -157.3(5) . .
C2 Ho1 C18 C17 175.3(5) . .
C8 Ho1 C18 C17 -9.7(9) . .
C5 Ho1 C18 C17 -96.9(5) . .
C1 Ho1 C18 C17 117.1(14) . .
C7 Ho1 C18 C17 -40.0(6) . .
C6 Ho1 C18 C17 -66.3(5) . .
C4 Ho1 C18 C17 -128.9(5) . .
C16 Ho1 C18 C17 45.1(5) . .
C15 Ho1 C18 C17 19.0(4) . .
C3 Ho1 C18 C16 56.3(5) . 2_676
C2 Ho1 C18 C16 28.9(7) . 2_676
C8 Ho1 C18 C16 -156.1(6) . 2_676
C5 Ho1 C18 C16 116.7(5) . 2_676
C1 Ho1 C18 C16 -29.3(16) . 2_676
C7 Ho1 C18 C16 173.6(5) . 2_676
C6 Ho1 C18 C16 147.3(5) . 2_676
C4 Ho1 C18 C16 84.7(5) . 2_676
C17 Ho1 C18 C16 -146.4(7) . 2_676
C16 Ho1 C18 C16 -101.3(5) . 2_676
C15 Ho1 C18 C16 -127.5(5) . 2_676
C3 Ho1 C18 Ho1 128.1(3) . 2_676
C2 Ho1 C18 Ho1 100.6(4) . 2_676
C8 Ho1 C18 Ho1 -84.4(7) . 2_676
C5 Ho1 C18 Ho1 -171.5(3) . 2_676
C1 Ho1 C18 Ho1 42.4(15) . 2_676
C7 Ho1 C18 Ho1 -114.7(3) . 2_676
C6 Ho1 C18 Ho1 -141.0(3) . 2_676
C4 Ho1 C18 Ho1 156.5(3) . 2_676
C17 Ho1 C18 Ho1 -74.6(5) . 2_676
C16 Ho1 C18 Ho1 -29.5(3) . 2_676
C15 Ho1 C18 Ho1 -55.7(3) . 2_676
C41 Si4 C31 C32 70.9(7) . .
C39 Si4 C31 C32 -47.3(8) . .
C40 Si4 C31 C32 -167.5(7) . .
C41 Si4 C31 C38 -105.3(8) . .
C39 Si4 C31 C38 136.4(7) . .
C40 Si4 C31 C38 16.2(8) . .
C41 Si4 C31 Ho2 160.8(7) . .
C39 Si4 C31 Ho2 42.5(9) . .
C40 Si4 C31 Ho2 -77.7(8) . .
C38 Ho2 C31 C32 -144.3(9) . .
C33 Ho2 C31 C32 -17.1(5) . .
C37 Ho2 C31 C32 -125.8(7) . .
C36 Ho2 C31 C32 -102.0(6) . .
C35 Ho2 C31 C32 -71.1(6) . .
C34 Ho2 C31 C32 -40.0(6) . .
C48 Ho2 C31 C32 72.1(19) . .
C46 Ho2 C31 C32 53.9(8) 2_765 .
C48 Ho2 C31 C32 121.9(5) 2_765 .
C47 Ho2 C31 C32 178.9(6) . .
C33 Ho2 C31 C38 127.2(7) . .
C37 Ho2 C31 C38 18.5(6) . .
C32 Ho2 C31 C38 144.3(9) . .
C36 Ho2 C31 C38 42.3(7) . .
C35 Ho2 C31 C38 73.2(7) . .
C34 Ho2 C31 C38 104.4(7) . .
C48 Ho2 C31 C38 -143.5(16) . .
C46 Ho2 C31 C38 -161.8(6) 2_765 .
C48 Ho2 C31 C38 -93.7(6) 2_765 .
C47 Ho2 C31 C38 -36.7(10) . .
C38 Ho2 C31 Si4 110.9(10) . .
C33 Ho2 C31 Si4 -122.0(7) . .
C37 Ho2 C31 Si4 129.4(8) . .
C32 Ho2 C31 Si4 -104.8(9) . .
C36 Ho2 C31 Si4 153.2(7) . .
C35 Ho2 C31 Si4 -175.9(7) . .
C34 Ho2 C31 Si4 -144.8(7) . .
C48 Ho2 C31 Si4 -33(2) . .
C46 Ho2 C31 Si4 -50.9(9) 2_765 .
C48 Ho2 C31 Si4 17.1(7) 2_765 .
C47 Ho2 C31 Si4 74.1(9) . .
C38 C31 C32 C33 -3.6(17) . .
Si4 C31 C32 C33 -179.1(9) . .
Ho2 C31 C32 C33 43.6(10) . .
C38 C31 C32 Ho2 -47.2(9) . .
Si4 C31 C32 Ho2 137.2(5) . .
C38 Ho2 C32 C33 -129.7(6) . .
C37 Ho2 C32 C33 -104.6(6) . .
C36 Ho2 C32 C33 -73.7(6) . .
C35 Ho2 C32 C33 -42.3(5) . .
C31 Ho2 C32 C33 -150.7(8) . .
C34 Ho2 C32 C33 -17.4(5) . .
C48 Ho2 C32 C33 45.3(7) . .
C46 Ho2 C32 C33 64.6(6) 2_765 .
C48 Ho2 C32 C33 146.6(5) 2_765 .
C47 Ho2 C32 C33 33(3) . .
C38 Ho2 C32 C31 21.0(6) . .
C33 Ho2 C32 C31 150.7(8) . .
C37 Ho2 C32 C31 46.1(6) . .
C36 Ho2 C32 C31 77.0(6) . .
C35 Ho2 C32 C31 108.3(6) . .
C34 Ho2 C32 C31 133.3(6) . .
C48 Ho2 C32 C31 -164.0(5) . .
C46 Ho2 C32 C31 -144.7(5) 2_765 .
C48 Ho2 C32 C31 -62.8(6) 2_765 .
C47 Ho2 C32 C31 -176(2) . .
C31 C32 C33 C34 2.2(19) . .
Ho2 C32 C33 C34 46.0(11) . .
C31 C32 C33 Ho2 -43.8(10) . .
C38 Ho2 C33 C32 42.8(5) . .
C37 Ho2 C33 C32 73.9(6) . .
C36 Ho2 C33 C32 104.9(6) . .
C35 Ho2 C33 C32 130.1(6) . .
C31 Ho2 C33 C32 17.2(5) . .
C34 Ho2 C33 C32 150.2(9) . .
C48 Ho2 C33 C32 -151.6(5) . .
C46 Ho2 C33 C32 -124.9(5) 2_765 .
C48 Ho2 C33 C32 -45.6(6) 2_765 .
C47 Ho2 C33 C32 -173.7(5) . .
C38 Ho2 C33 C34 -107.5(6) . .
C37 Ho2 C33 C34 -76.4(7) . .
C32 Ho2 C33 C34 -150.2(9) . .
C36 Ho2 C33 C34 -45.3(7) . .
C35 Ho2 C33 C34 -20.1(6) . .
C31 Ho2 C33 C34 -133.0(7) . .
C48 Ho2 C33 C34 58.2(6) . .
C46 Ho2 C33 C34 84.9(6) 2_765 .
C48 Ho2 C33 C34 164.2(5) 2_765 .
C47 Ho2 C33 C34 36.1(8) . .
C32 C33 C34 C35 0.1(19) . .
Ho2 C33 C34 C35 45.7(10) . .
C32 C33 C34 Si5 -179.2(9) . .
Ho2 C33 C34 Si5 -133.7(6) . .
C32 C33 C34 Ho2 -45.5(11) . .
C38 Ho2 C34 C33 71.9(6) . .
C37 Ho2 C34 C33 102.5(6) . .
C32 Ho2 C34 C33 17.4(5) . .
C36 Ho2 C34 C33 126.8(8) . .
C35 Ho2 C34 C33 145.6(11) . .
C31 Ho2 C34 C33 40.4(6) . .
C48 Ho2 C34 C33 -130.3(6) . .
C46 Ho2 C34 C33 -99.7(6) 2_765 .
C48 Ho2 C34 C33 -39.5(14) 2_765 .
C47 Ho2 C34 C33 -156.5(5) . .
C38 Ho2 C34 C35 -73.7(8) . .
C33 Ho2 C34 C35 -145.6(11) . .
C37 Ho2 C34 C35 -43.2(8) . .
C32 Ho2 C34 C35 -128.2(8) . .
C36 Ho2 C34 C35 -18.9(8) . .
C31 Ho2 C34 C35 -105.2(8) . .
C48 Ho2 C34 C35 84.0(7) . .
C46 Ho2 C34 C35 114.6(7) 2_765 .
C48 Ho2 C34 C35 174.9(9) 2_765 .
C47 Ho2 C34 C35 57.9(8) . .
C38 Ho2 C34 Si5 179.1(7) . .
C33 Ho2 C34 Si5 107.2(9) . .
C37 Ho2 C34 Si5 -150.4(7) . .
C32 Ho2 C34 Si5 124.6(7) . .
C36 Ho2 C34 Si5 -126.1(8) . .
C35 Ho2 C34 Si5 -107.2(11) . .
C31 Ho2 C34 Si5 147.5(7) . .
C48 Ho2 C34 Si5 -23.2(7) . .
C46 Ho2 C34 Si5 7.4(7) 2_765 .
C48 Ho2 C34 Si5 67.7(14) 2_765 .
C47 Ho2 C34 Si5 -49.3(7) . .
C33 C34 C35 C36 1.0(19) . .
Si5 C34 C35 C36 -179.7(10) . .
Ho2 C34 C35 C36 46.5(11) . .
C33 C34 C35 Ho2 -45.5(10) . .
Si5 C34 C35 Ho2 133.8(6) . .
C38 Ho2 C35 C36 -41.9(7) . .
C33 Ho2 C35 C36 -127.8(8) . .
C37 Ho2 C35 C36 -18.4(7) . .
C32 Ho2 C35 C36 -103.7(7) . .
C31 Ho2 C35 C36 -73.1(7) . .
C34 Ho2 C35 C36 -147.8(12) . .
C48 Ho2 C35 C36 112.8(7) . .
C46 Ho2 C35 C36 140.3(7) 2_765 .
C48 Ho2 C35 C36 38.9(19) 2_765 .
C47 Ho2 C35 C36 83.3(7) . .
C38 Ho2 C35 C34 105.9(7) . .
C33 Ho2 C35 C34 20.0(7) . .
C37 Ho2 C35 C34 129.4(8) . .
C32 Ho2 C35 C34 44.1(7) . .
C36 Ho2 C35 C34 147.8(12) . .
C31 Ho2 C35 C34 74.7(7) . .
C48 Ho2 C35 C34 -99.4(7) . .
C46 Ho2 C35 C34 -71.9(8) 2_765 .
C48 Ho2 C35 C34 -173.3(12) 2_765 .
C47 Ho2 C35 C34 -128.9(7) . .
C34 C35 C36 C37 -1(2) . .
Ho2 C35 C36 C37 45.6(12) . .
C34 C35 C36 Ho2 -47.0(11) . .
C38 Ho2 C36 C37 -17.6(6) . .
C33 Ho2 C36 C37 -104.4(6) . .
C32 Ho2 C36 C37 -73.5(6) . .
C35 Ho2 C36 C37 -148.5(10) . .
C31 Ho2 C36 C37 -41.9(6) . .
C34 Ho2 C36 C37 -129.7(7) . .
C48 Ho2 C36 C37 139.1(6) . .
C46 Ho2 C36 C37 158.2(5) 2_765 .
C48 Ho2 C36 C37 44.1(8) 2_765 .
C47 Ho2 C36 C37 113.5(6) . .
C38 Ho2 C36 C35 130.9(8) . .
C33 Ho2 C36 C35 44.1(7) . .
C37 Ho2 C36 C35 148.5(10) . .
C32 Ho2 C36 C35 75.1(7) . .
C31 Ho2 C36 C35 106.6(7) . .
C34 Ho2 C36 C35 18.9(6) . .
C48 Ho2 C36 C35 -72.3(7) . .
C46 Ho2 C36 C35 -53.3(8) 2_765 .
C48 Ho2 C36 C35 -167.3(6) 2_765 .
C47 Ho2 C36 C35 -98.0(7) . .
C35 C36 C37 C38 -2(2) . .
Ho2 C36 C37 C38 43.7(12) . .
C35 C36 C37 Ho2 -45.7(12) . .
C33 Ho2 C37 C38 -75.7(7) . .
C32 Ho2 C37 C38 -44.7(7) . .
C36 Ho2 C37 C38 -149.8(10) . .
C35 Ho2 C37 C38 -131.4(7) . .
C31 Ho2 C37 C38 -18.8(6) . .
C34 Ho2 C37 C38 -106.9(7) . .
C48 Ho2 C37 C38 157.3(6) . .
C46 Ho2 C37 C38 161.7(8) 2_765 .
C48 Ho2 C37 C38 61.2(7) 2_765 .
C47 Ho2 C37 C38 140.2(6) . .
C38 Ho2 C37 C36 149.8(10) . .
C33 Ho2 C37 C36 74.1(6) . .
C32 Ho2 C37 C36 105.1(6) . .
C35 Ho2 C37 C36 18.5(6) . .
C31 Ho2 C37 C36 131.0(7) . .
C34 Ho2 C37 C36 43.0(6) . .
C48 Ho2 C37 C36 -52.9(7) . .
C46 Ho2 C37 C36 -48.5(12) 2_765 .
C48 Ho2 C37 C36 -149.0(6) 2_765 .
C47 Ho2 C37 C36 -69.9(6) . .
C36 C37 C38 C31 4(2) . .
Ho2 C37 C38 C31 47.6(11) . .
C36 C37 C38 Ho2 -43.9(12) . .
C32 C31 C38 C37 0.0(18) . .
Si4 C31 C38 C37 175.4(9) . .
Ho2 C31 C38 C37 -47.5(11) . .
C32 C31 C38 Ho2 47.5(9) . .
Si4 C31 C38 Ho2 -137.1(6) . .
C33 Ho2 C38 C37 103.0(7) . .
C32 Ho2 C38 C37 127.3(8) . .
C36 Ho2 C38 C37 17.7(6) . .
C35 Ho2 C38 C37 41.6(7) . .
C31 Ho2 C38 C37 148.1(10) . .
C34 Ho2 C38 C37 72.6(7) . .
C48 Ho2 C38 C37 -45.8(11) . .
C46 Ho2 C38 C37 -147.8(12) 2_765 .
C48 Ho2 C38 C37 -124.5(7) 2_765 .
C47 Ho2 C38 C37 -50.0(8) . .
C33 Ho2 C38 C31 -45.1(6) . .
C37 Ho2 C38 C31 -148.1(10) . .
C32 Ho2 C38 C31 -20.8(6) . .
C36 Ho2 C38 C31 -130.4(7) . .
C35 Ho2 C38 C31 -106.5(6) . .
C34 Ho2 C38 C31 -75.5(6) . .
C48 Ho2 C38 C31 166.1(6) . .
C46 Ho2 C38 C31 64.1(15) 2_765 .
C48 Ho2 C38 C31 87.4(6) 2_765 .
C47 Ho2 C38 C31 161.8(5) . .
C33 C34 Si5 C43' 68.1(13) . .
C35 C34 Si5 C43' -111.4(13) . .
Ho2 C34 Si5 C43' -21.4(13) . .
C33 C34 Si5 C42 -109.8(12) . .
C35 C34 Si5 C42 70.7(13) . .
Ho2 C34 Si5 C42 160.7(11) . .
C33 C34 Si5 C42' -154.2(10) . .
C35 C34 Si5 C42' 26.4(12) . .
Ho2 C34 Si5 C42' 116.3(10) . .
C33 C34 Si5 C44 27.6(12) . .
C35 C34 Si5 C44 -151.8(10) . .
Ho2 C34 Si5 C44 -61.9(11) . .
C33 C34 Si5 C44' -48.0(13) . .
C35 C34 Si5 C44' 132.5(13) . .
Ho2 C34 Si5 C44' -137.5(13) . .
C33 C34 Si5 C43 131.0(11) . .
C35 C34 Si5 C43 -48.5(11) . .
Ho2 C34 Si5 C43 41.5(11) . .
C38 Ho2 C45 C47 150.1(5) . .
C33 Ho2 C45 C47 34.8(16) . .
C37 Ho2 C45 C47 120.8(6) . .
C32 Ho2 C45 C47 -174.1(6) . .
C36 Ho2 C45 C47 88.8(6) . .
C35 Ho2 C45 C47 62.0(6) . .
C31 Ho2 C45 C47 172.9(5) . .
C34 Ho2 C45 C47 42.1(7) . .
C48 Ho2 C45 C47 -18.9(5) . .
C46 Ho2 C45 C47 -42.9(5) 2_765 .
C48 Ho2 C45 C47 -123.4(5) 2_765 .
C38 Ho2 C45 C46 -67.3(5) . .
C33 Ho2 C45 C46 177.3(13) . .
C37 Ho2 C45 C46 -96.7(6) . .
C32 Ho2 C45 C46 -31.6(9) . .
C36 Ho2 C45 C46 -128.7(6) . .
C35 Ho2 C45 C46 -155.5(5) . .
C31 Ho2 C45 C46 -44.6(6) . .
C34 Ho2 C45 C46 -175.4(5) . .
C48 Ho2 C45 C46 123.6(5) . .
C46 Ho2 C45 C46 99.7(5) 2_765 .
C48 Ho2 C45 C46 19.2(4) 2_765 .
C47 Ho2 C45 C46 142.5(7) . .
C38 Ho2 C45 Si6 42.1(7) . .
C33 Ho2 C45 Si6 -73.2(17) . .
C37 Ho2 C45 Si6 12.8(7) . .
C32 Ho2 C45 Si6 77.9(9) . .
C36 Ho2 C45 Si6 -19.2(7) . .
C35 Ho2 C45 Si6 -46.0(8) . .
C31 Ho2 C45 Si6 64.9(7) . .
C34 Ho2 C45 Si6 -65.9(8) . .
C48 Ho2 C45 Si6 -126.9(7) . .
C46 Ho2 C45 Si6 -150.8(7) 2_765 .
C48 Ho2 C45 Si6 128.6(7) 2_765 .
C47 Ho2 C45 Si6 -108.0(9) . .
C38 Ho2 C45 Ho2 -138.1(3) . 2_765
C33 Ho2 C45 Ho2 106.5(14) . 2_765
C37 Ho2 C45 Ho2 -167.5(4) . 2_765
C32 Ho2 C45 Ho2 -102.4(6) . 2_765
C36 Ho2 C45 Ho2 160.5(4) . 2_765
C35 Ho2 C45 Ho2 133.7(4) . 2_765
C31 Ho2 C45 Ho2 -115.3(3) . 2_765
C34 Ho2 C45 Ho2 113.8(4) . 2_765
C48 Ho2 C45 Ho2 52.8(3) . 2_765
C46 Ho2 C45 Ho2 28.9(3) 2_765 2_765
C48 Ho2 C45 Ho2 -51.6(3) 2_765 2_765
C47 Ho2 C45 Ho2 71.8(5) . 2_765
C47 C45 C46 C48 0.5(17) . 2_765
Si6 C45 C46 C48 -177.1(8) . 2_765
Ho2 C45 C46 C48 50.8(10) 2_765 2_765
Ho2 C45 C46 C48 -48.9(10) . 2_765
C47 C45 C46 Ho2 -50.3(9) . 2_765
Si6 C45 C46 Ho2 132.1(5) . 2_765
Ho2 C45 C46 Ho2 -99.62(19) . 2_765
C47 C45 C46 Ho2 49.3(9) . .
Si6 C45 C46 Ho2 -128.2(5) . .
Ho2 C45 C46 Ho2 99.62(19) 2_765 .
C38 Ho2 C46 C45 114.9(5) . .
C33 Ho2 C46 C45 -178.5(7) . .
C37 Ho2 C46 C45 83.0(6) . .
C32 Ho2 C46 C45 164.8(5) . .
C36 Ho2 C46 C45 55.6(6) . .
C35 Ho2 C46 C45 34.0(7) . .
C31 Ho2 C46 C45 144.3(5) . .
C34 Ho2 C46 C45 13.9(16) . .
C48 Ho2 C46 C45 -45.7(5) . .
C46 Ho2 C46 C45 -75.4(5) 2_765 .
C48 Ho2 C46 C45 -146.7(8) 2_765 .
C47 Ho2 C46 C45 -21.2(4) . .
C38 Ho2 C46 C48 -98.4(6) . 2_765
C33 Ho2 C46 C48 -31.8(11) . 2_765
C37 Ho2 C46 C48 -130.2(6) . 2_765
C32 Ho2 C46 C48 -48.5(6) . 2_765
C36 Ho2 C46 C48 -157.7(6) . 2_765
C35 Ho2 C46 C48 -179.2(6) . 2_765
C31 Ho2 C46 C48 -68.9(5) . 2_765
C34 Ho2 C46 C48 160.7(13) . 2_765
C48 Ho2 C46 C48 101.0(5) . 2_765
C46 Ho2 C46 C48 71.3(5) 2_765 2_765
C47 Ho2 C46 C48 125.5(6) . 2_765
C38 Ho2 C46 Ho2 -169.7(4) . 2_765
C33 Ho2 C46 Ho2 -103.1(8) . 2_765
C37 Ho2 C46 Ho2 158.4(4) . 2_765
C32 Ho2 C46 Ho2 -119.8(3) . 2_765
C36 Ho2 C46 Ho2 131.0(4) . 2_765
C35 Ho2 C46 Ho2 109.5(5) . 2_765
C31 Ho2 C46 Ho2 -140.3(3) . 2_765
C34 Ho2 C46 Ho2 89.4(14) . 2_765
C48 Ho2 C46 Ho2 29.7(3) . 2_765
C46 Ho2 C46 Ho2 0.0 2_765 2_765
C48 Ho2 C46 Ho2 -71.3(5) 2_765 2_765
C47 Ho2 C46 Ho2 54.2(3) . 2_765
C46 C45 C47 C48 1.3(18) . .
Si6 C45 C47 C48 178.8(9) . .
Ho2 C45 C47 C48 -48.6(11) 2_765 .
Ho2 C45 C47 C48 51.0(10) . .
C46 C45 C47 Ho2 -49.7(9) . .
Si6 C45 C47 Ho2 127.8(5) . .
Ho2 C45 C47 Ho2 -99.6(2) 2_765 .
C46 C45 C47 Ho2 49.9(9) . 2_765
Si6 C45 C47 Ho2 -132.5(5) . 2_765
Ho2 C45 C47 Ho2 99.6(2) . 2_765
C38 Ho2 C47 C48 176.3(5) . .
C33 Ho2 C47 C48 42.8(7) . .
C37 Ho2 C47 C48 151.7(6) . .
C32 Ho2 C47 C48 15(3) . .
C36 Ho2 C47 C48 121.7(6) . .
C35 Ho2 C47 C48 89.7(6) . .
C31 Ho2 C47 C48 -160.4(6) . .
C34 Ho2 C47 C48 62.7(6) . .
C46 Ho2 C47 C48 -18.9(5) 2_765 .
C48 Ho2 C47 C48 -100.5(5) 2_765 .
C38 Ho2 C47 C45 -36.9(6) . .
C33 Ho2 C47 C45 -170.5(4) . .
C37 Ho2 C47 C45 -61.5(6) . .
C32 Ho2 C47 C45 162(2) . .
C36 Ho2 C47 C45 -91.5(6) . .
C35 Ho2 C47 C45 -123.6(5) . .
C31 Ho2 C47 C45 -13.6(9) . .
C34 Ho2 C47 C45 -150.6(5) . .
C48 Ho2 C47 C45 146.8(8) . .
C46 Ho2 C47 C45 127.9(6) 2_765 .
C48 Ho2 C47 C45 46.3(5) 2_765 .
C38 Ho2 C47 Ho2 -111.9(4) . 2_765
C33 Ho2 C47 Ho2 114.6(4) . 2_765
C37 Ho2 C47 Ho2 -136.4(4) . 2_765
C32 Ho2 C47 Ho2 87(2) . 2_765
C36 Ho2 C47 Ho2 -166.4(4) . 2_765
C35 Ho2 C47 Ho2 161.5(4) . 2_765
C31 Ho2 C47 Ho2 -88.6(7) . 2_765
C34 Ho2 C47 Ho2 134.5(3) . 2_765
C48 Ho2 C47 Ho2 71.8(5) . 2_765
C46 Ho2 C47 Ho2 53.0(3) 2_765 2_765
C48 Ho2 C47 Ho2 -28.6(2) 2_765 2_765
C45 C47 C48 C46 -2.3(18) . 2_765
Ho2 C47 C48 C46 49.7(10) . 2_765
Ho2 C47 C48 C46 -51.6(10) 2_765 2_765
C45 C47 C48 Ho2 -52.1(11) . .
Ho2 C47 C48 Ho2 -101.4(2) 2_765 .
C45 C47 C48 Ho2 49.3(11) . 2_765
Ho2 C47 C48 Ho2 101.4(2) . 2_765
C38 Ho2 C48 C47 -7.1(10) . .
C33 Ho2 C48 C47 -151.7(5) . .
C37 Ho2 C48 C47 -35.7(7) . .
C32 Ho2 C48 C47 -176.9(6) . .
C36 Ho2 C48 C47 -61.8(6) . .
C35 Ho2 C48 C47 -92.5(5) . .
C31 Ho2 C48 C47 124.3(17) . .
C34 Ho2 C48 C47 -124.6(5) . .
C46 Ho2 C48 C47 147.5(8) 2_765 .
C48 Ho2 C48 C47 73.9(5) 2_765 .
C38 Ho2 C48 C46 -154.6(8) . 2_765
C33 Ho2 C48 C46 60.8(6) . 2_765
C37 Ho2 C48 C46 176.8(6) . 2_765
C32 Ho2 C48 C46 35.6(7) . 2_765
C36 Ho2 C48 C46 150.7(5) . 2_765
C35 Ho2 C48 C46 120.0(5) . 2_765
C31 Ho2 C48 C46 -23.3(19) . 2_765
C34 Ho2 C48 C46 87.8(5) . 2_765
C48 Ho2 C48 C46 -73.6(5) 2_765 2_765
C47 Ho2 C48 C46 -147.5(8) . 2_765
C38 Ho2 C48 Ho2 -81.0(8) . 2_765
C33 Ho2 C48 Ho2 134.4(3) . 2_765
C37 Ho2 C48 Ho2 -109.6(4) . 2_765
C32 Ho2 C48 Ho2 109.2(5) . 2_765
C36 Ho2 C48 Ho2 -135.7(3) . 2_765
C35 Ho2 C48 Ho2 -166.4(3) . 2_765
C31 Ho2 C48 Ho2 50.4(18) . 2_765
C34 Ho2 C48 Ho2 161.4(3) . 2_765
C46 Ho2 C48 Ho2 73.6(5) 2_765 2_765
C48 Ho2 C48 Ho2 0.0 2_765 2_765
C47 Ho2 C48 Ho2 -73.9(5) . 2_765
C47 C45 Si6 C49 -48.3(12) . .
C46 C45 Si6 C49 129.6(11) . .
Ho2 C45 Si6 C49 -140.0(11) 2_765 .
Ho2 C45 Si6 C49 39.6(11) . .
C47 C45 Si6 C51 76.7(12) . .
C46 C45 Si6 C51 -105.4(12) . .
Ho2 C45 Si6 C51 -15.0(12) 2_765 .
Ho2 C45 Si6 C51 164.6(11) . .
C47 C45 Si6 C50' -146.9(17) . .
C46 C45 Si6 C50' 31.0(17) . .
Ho2 C45 Si6 C50' 121.4(17) 2_765 .
Ho2 C45 Si6 C50' -58.9(17) . .
C47 C45 Si6 C51' 87.7(14) . .
C46 C45 Si6 C51' -94.4(15) . .
Ho2 C45 Si6 C51' -4.0(15) 2_765 .
Ho2 C45 Si6 C51' 175.6(14) . .
C47 C45 Si6 C49' -26.4(14) . .
C46 C45 Si6 C49' 151.6(14) . .
Ho2 C45 Si6 C49' -118.1(14) 2_765 .
Ho2 C45 Si6 C49' 61.6(14) . .
C47 C45 Si6 C50 -163.6(10) . .
C46 C45 Si6 C50 14.3(10) . .
Ho2 C45 Si6 C50 104.7(10) 2_765 .
Ho2 C45 Si6 C50 -75.7(10) . .
