#------------------------------------------------------------------------------
#$Date: 2016-02-14 06:40:26 +0200 (Sun, 14 Feb 2016) $
#$Revision: 176432 $
#$URL: svn://www.crystallography.net/cod/cif/4/08/10/4081058.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4081058
loop_
_publ_author_name
'Anderson, Craig M.'
'Crespo, Margarita'
'Kfoury, Nicole'
'Weinstein, Michael A.'
'Tanski, Joseph M.'
_publ_contact_author             'Craig Anderson'
_publ_section_title
;
 Regioselective C--H Activation Preceded by Csp2--Csp3Reductive
 Elimination from Cyclometalated Platinum(IV) Complexes
;
_journal_issue                   15
_journal_name_full               Organometallics
_journal_page_first              4199
_journal_paper_doi               10.1021/om400398g
_journal_volume                  32
_journal_year                    2013
_chemical_formula_moiety         'C34 H32 Cl2 N P Pt'
_chemical_formula_sum            'C34 H32 Cl2 N P Pt'
_chemical_formula_weight         751.57
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 92.8460(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   18.9326(8)
_cell_length_b                   11.4614(5)
_cell_length_c                   27.1739(12)
_cell_measurement_reflns_used    9907
_cell_measurement_temperature    125(2)
_cell_measurement_theta_max      31.68
_cell_measurement_theta_min      2.19
_cell_volume                     5889.3(4)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      125(2)
_diffrn_measured_fraction_theta_full 0.993
_diffrn_measured_fraction_theta_max 0.945
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0276
_diffrn_reflns_av_sigmaI/netI    0.0222
_diffrn_reflns_limit_h_max       26
_diffrn_reflns_limit_h_min       -27
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       39
_diffrn_reflns_limit_l_min       -38
_diffrn_reflns_number            47848
_diffrn_reflns_theta_full        31.00
_diffrn_reflns_theta_max         31.98
_diffrn_reflns_theta_min         2.08
_exptl_absorpt_coefficient_mu    5.026
_exptl_absorpt_correction_T_max  0.4331
_exptl_absorpt_correction_T_min  0.3335
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    1.695
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       block
_exptl_crystal_F_000             2960
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.28
_exptl_crystal_size_min          0.20
_refine_diff_density_max         1.176
_refine_diff_density_min         -0.634
_refine_diff_density_rms         0.090
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.036
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     354
_refine_ls_number_reflns         9640
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.036
_refine_ls_R_factor_all          0.0238
_refine_ls_R_factor_gt           0.0189
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0201P)²+3.9366P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0412
_refine_ls_wR_factor_ref         0.0424
_reflns_number_gt                8560
_reflns_number_total             9640
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om400398g_si_002.cif
_cod_data_source_block           ca1513pt
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Monoclinic' changed to 'monoclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_Hall     -C2yc
_cod_original_sg_symbol_H-M      C2/c
_cod_database_code               4081058
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pt Pt 0.252276(3) 0.190956(5) 0.136370(2) 0.01286(2) Uani 1 1 d .
Cl1 Cl 0.31968(2) 0.34194(4) 0.180407(16) 0.02102(9) Uani 1 1 d .
Cl2 Cl 0.01791(3) 0.71503(5) -0.04955(2) 0.03331(12) Uani 1 1 d .
P P 0.15771(2) 0.19038(4) 0.192828(16) 0.01290(8) Uani 1 1 d .
N N 0.20215(8) 0.31398(12) 0.08635(5) 0.0155(3) Uani 1 1 d .
C1 C 0.30298(10) 0.05805(16) 0.17578(7) 0.0212(4) Uani 1 1 d .
H1A H 0.3214 0.0009 0.1528 0.032 Uiso 1 1 calc R
H1B H 0.2694 0.0198 0.1968 0.032 Uiso 1 1 calc R
H1C H 0.3422 0.0906 0.1963 0.032 Uiso 1 1 calc R
C2 C 0.20019(9) 0.08053(15) 0.09014(6) 0.0155(3) Uani 1 1 d .
C3 C 0.19603(10) -0.04068(16) 0.09224(7) 0.0194(3) Uani 1 1 d .
H3A H 0.2211 -0.0816 0.1180 0.023 Uiso 1 1 calc R
C4 C 0.15550(11) -0.10240(16) 0.05691(7) 0.0235(4) Uani 1 1 d .
H4A H 0.1527 -0.1850 0.0592 0.028 Uiso 1 1 calc R
C5 C 0.11908(11) -0.04552(17) 0.01833(7) 0.0261(4) Uani 1 1 d .
H5A H 0.0920 -0.0889 -0.0057 0.031 Uiso 1 1 calc R
C6 C 0.12250(10) 0.07493(17) 0.01503(7) 0.0227(4) Uani 1 1 d .
H6A H 0.0978 0.1147 -0.0112 0.027 Uiso 1 1 calc R
C7 C 0.16275(9) 0.13767(15) 0.05081(6) 0.0161(3) Uani 1 1 d .
C8 C 0.16689(9) 0.26467(16) 0.05054(6) 0.0172(3) Uani 1 1 d .
H8A H 0.1443 0.3093 0.0248 0.021 Uiso 1 1 calc R
C9 C 0.21313(10) 0.44118(15) 0.08874(6) 0.0184(3) Uani 1 1 d .
H9A H 0.2626 0.4581 0.0810 0.022 Uiso 1 1 calc R
H9B H 0.2068 0.4673 0.1230 0.022 Uiso 1 1 calc R
C10 C 0.16482(9) 0.51200(15) 0.05467(6) 0.0169(3) Uani 1 1 d .
C11 C 0.18742(10) 0.55080(16) 0.00955(7) 0.0217(4) Uani 1 1 d .
H11A H 0.2342 0.5341 0.0005 0.026 Uiso 1 1 calc R
C12 C 0.14243(11) 0.61355(17) -0.02245(7) 0.0237(4) Uani 1 1 d .
H12A H 0.1581 0.6396 -0.0532 0.028 Uiso 1 1 calc R
C13 C 0.07481(10) 0.63754(16) -0.00902(7) 0.0211(4) Uani 1 1 d .
C14 C 0.05076(10) 0.60087(17) 0.03566(7) 0.0244(4) Uani 1 1 d .
H14A H 0.0040 0.6186 0.0445 0.029 Uiso 1 1 calc R
C15 C 0.09613(10) 0.53758(17) 0.06739(7) 0.0220(4) Uani 1 1 d .
H15A H 0.0801 0.5115 0.0981 0.026 Uiso 1 1 calc R
C16 C 0.10056(9) 0.31985(14) 0.19080(6) 0.0147(3) Uani 1 1 d .
C17 C 0.02776(9) 0.31666(16) 0.18092(7) 0.0188(3) Uani 1 1 d .
H17A H 0.0052 0.2441 0.1738 0.023 Uiso 1 1 calc R
C18 C -0.01235(10) 0.41814(17) 0.18132(7) 0.0223(4) Uani 1 1 d .
H18A H -0.0619 0.4147 0.1741 0.027 Uiso 1 1 calc R
C19 C 0.01944(10) 0.52381(16) 0.19219(7) 0.0207(4) Uani 1 1 d .
H19A H -0.0080 0.5932 0.1922 0.025 Uiso 1 1 calc R
C20 C 0.09199(10) 0.52813(16) 0.20322(7) 0.0204(4) Uani 1 1 d .
H20A H 0.1139 0.6006 0.2114 0.025 Uiso 1 1 calc R
C21 C 0.13257(9) 0.42702(15) 0.20235(6) 0.0172(3) Uani 1 1 d .
H21A H 0.1821 0.4308 0.2096 0.021 Uiso 1 1 calc R
C22 C 0.18031(9) 0.18357(14) 0.25924(6) 0.0152(3) Uani 1 1 d .
C23 C 0.24889(10) 0.20614(15) 0.27793(7) 0.0188(3) Uani 1 1 d .
H23A H 0.2856 0.2202 0.2561 0.023 Uiso 1 1 calc R
C24 C 0.26336(10) 0.20795(16) 0.32868(7) 0.0202(4) Uani 1 1 d .
H24A H 0.3101 0.2231 0.3413 0.024 Uiso 1 1 calc R
C25 C 0.21033(10) 0.18791(15) 0.36078(7) 0.0200(3) Uani 1 1 d .
H25A H 0.2206 0.1898 0.3954 0.024 Uiso 1 1 calc R
C26 C 0.14192(10) 0.16499(17) 0.34230(7) 0.0220(4) Uani 1 1 d .
H26A H 0.1054 0.1502 0.3643 0.026 Uiso 1 1 calc R
C27 C 0.12692(10) 0.16369(17) 0.29169(7) 0.0204(4) Uani 1 1 d .
H27A H 0.0800 0.1492 0.2792 0.024 Uiso 1 1 calc R
C28 C 0.09953(9) 0.06546(15) 0.18153(6) 0.0151(3) Uani 1 1 d .
C29 C 0.10469(10) -0.03314(16) 0.21159(7) 0.0201(3) Uani 1 1 d .
H29A H 0.1372 -0.0340 0.2394 0.024 Uiso 1 1 calc R
C30 C 0.06257(11) -0.13018(17) 0.20110(8) 0.0272(4) Uani 1 1 d .
H30A H 0.0663 -0.1966 0.2220 0.033 Uiso 1 1 calc R
C31 C 0.01526(11) -0.13116(18) 0.16065(9) 0.0300(5) Uani 1 1 d .
H31A H -0.0142 -0.1970 0.1541 0.036 Uiso 1 1 calc R
C32 C 0.01136(10) -0.03496(17) 0.12971(8) 0.0255(4) Uani 1 1 d .
H32A H -0.0204 -0.0355 0.1015 0.031 Uiso 1 1 calc R
C33 C 0.05347(9) 0.06205(16) 0.13953(7) 0.0189(3) Uani 1 1 d .
H33B H 0.0511 0.1267 0.1176 0.023 Uiso 1 1 calc R
C34 C 0.33574(10) 0.18342(17) 0.08881(7) 0.0239(4) Uani 1 1 d .
H34A H 0.3332 0.1101 0.0703 0.036 Uiso 1 1 calc R
H34B H 0.3808 0.1874 0.1081 0.036 Uiso 1 1 calc R
H34C H 0.3323 0.2493 0.0658 0.036 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
C2 Pt C1 93.47(7)
C2 Pt C34 87.13(7)
C1 Pt C34 86.79(8)
C2 Pt N 80.21(6)
C1 Pt N 171.81(6)
C34 Pt N 87.69(7)
C2 Pt P 92.25(5)
C1 Pt P 90.50(5)
C34 Pt P 177.18(6)
N Pt P 94.92(4)
C2 Pt Cl1 170.74(5)
C1 Pt Cl1 92.90(6)
C34 Pt Cl1 86.52(6)
N Pt Cl1 92.80(4)
P Pt Cl1 94.411(15)
C28 P C22 103.98(8)
C28 P C16 106.24(8)
C22 P C16 99.92(8)
C28 P Pt 110.85(5)
C22 P Pt 118.73(6)
C16 P Pt 115.66(6)
C8 N C9 122.41(15)
C8 N Pt 112.82(12)
C9 N Pt 124.40(11)
Pt C1 H1A 109.5
Pt C1 H1B 109.5
H1A C1 H1B 109.5
Pt C1 H1C 109.5
H1A C1 H1C 109.5
H1B C1 H1C 109.5
C3 C2 C7 117.76(16)
C3 C2 Pt 129.08(13)
C7 C2 Pt 113.16(12)
C4 C3 C2 120.60(17)
C4 C3 H3A 119.7
C2 C3 H3A 119.7
C5 C4 C3 121.21(18)
C5 C4 H4A 119.4
C3 C4 H4A 119.4
C6 C5 C4 119.59(17)
C6 C5 H5A 120.2
C4 C5 H5A 120.2
C5 C6 C7 119.43(18)
C5 C6 H6A 120.3
C7 C6 H6A 120.3
C6 C7 C2 121.40(16)
C6 C7 C8 122.38(16)
C2 C7 C8 116.19(15)
N C8 C7 117.51(16)
N C8 H8A 121.2
C7 C8 H8A 121.2
N C9 C10 115.22(14)
N C9 H9A 108.5
C10 C9 H9A 108.5
N C9 H9B 108.5
C10 C9 H9B 108.5
H9A C9 H9B 107.5
C11 C10 C15 118.88(17)
C11 C10 C9 120.65(16)
C15 C10 C9 120.45(16)
C12 C11 C10 120.77(18)
C12 C11 H11A 119.6
C10 C11 H11A 119.6
C13 C12 C11 119.18(17)
C13 C12 H12A 120.4
C11 C12 H12A 120.4
C12 C13 C14 121.55(17)
C12 C13 Cl2 119.18(15)
C14 C13 Cl2 119.27(15)
C13 C14 C15 118.86(18)
C13 C14 H14A 120.6
C15 C14 H14A 120.6
C14 C15 C10 120.75(17)
C14 C15 H15A 119.6
C10 C15 H15A 119.6
C17 C16 C21 118.72(16)
C17 C16 P 124.13(13)
C21 C16 P 117.07(13)
C18 C17 C16 120.86(17)
C18 C17 H17A 119.6
C16 C17 H17A 119.6
C19 C18 C17 120.30(17)
C19 C18 H18A 119.9
C17 C18 H18A 119.9
C18 C19 C20 119.55(17)
C18 C19 H19A 120.2
C20 C19 H19A 120.2
C21 C20 C19 120.42(17)
C21 C20 H20A 119.8
C19 C20 H20A 119.8
C20 C21 C16 120.13(16)
C20 C21 H21A 119.9
C16 C21 H21A 119.9
C27 C22 C23 119.44(16)
C27 C22 P 119.23(13)
C23 C22 P 121.17(13)
C24 C23 C22 119.81(17)
C24 C23 H23A 120.1
C22 C23 H23A 120.1
C25 C24 C23 120.62(17)
C25 C24 H24A 119.7
C23 C24 H24A 119.7
C24 C25 C26 119.77(17)
C24 C25 H25A 120.1
C26 C25 H25A 120.1
C27 C26 C25 119.99(18)
C27 C26 H26A 120.0
C25 C26 H26A 120.0
C26 C27 C22 120.37(17)
C26 C27 H27A 119.8
C22 C27 H27A 119.8
C29 C28 C33 118.47(16)
C29 C28 P 120.90(13)
C33 C28 P 120.33(13)
C30 C29 C28 120.36(18)
C30 C29 H29A 119.8
C28 C29 H29A 119.8
C31 C30 C29 120.79(19)
C31 C30 H30A 119.6
C29 C30 H30A 119.6
C30 C31 C32 119.24(18)
C30 C31 H31A 120.4
C32 C31 H31A 120.4
C31 C32 C33 120.55(18)
C31 C32 H32A 119.7
C33 C32 H32A 119.7
C32 C33 C28 120.50(17)
C32 C33 H33B 119.7
C28 C33 H33B 119.7
Pt C34 H34A 109.5
Pt C34 H34B 109.5
H34A C34 H34B 109.5
Pt C34 H34C 109.5
H34A C34 H34C 109.5
H34B C34 H34C 109.5
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
Pt C2 2.0073(17)
Pt C1 2.0704(17)
Pt C34 2.0923(19)
Pt N 2.1467(14)
Pt P 2.4150(4)
Pt Cl1 2.4298(4)
Cl2 C13 1.7449(19)
P C28 1.8231(17)
P C22 1.8356(17)
P C16 1.8357(17)
N C8 1.284(2)
N C9 1.474(2)
C1 H1A 0.9800
C1 H1B 0.9800
C1 H1C 0.9800
C2 C3 1.393(2)
C2 C7 1.414(2)
C3 C4 1.392(3)
C3 H3A 0.9500
C4 C5 1.388(3)
C4 H4A 0.9500
C5 C6 1.385(3)
C5 H5A 0.9500
C6 C7 1.403(2)
C6 H6A 0.9500
C7 C8 1.458(2)
C8 H8A 0.9500
C9 C10 1.506(2)
C9 H9A 0.9900
C9 H9B 0.9900
C10 C11 1.392(2)
C10 C15 1.393(3)
C11 C12 1.388(3)
C11 H11A 0.9500
C12 C13 1.376(3)
C12 H12A 0.9500
C13 C14 1.383(3)
C14 C15 1.391(3)
C14 H14A 0.9500
C15 H15A 0.9500
C16 C17 1.392(2)
C16 C21 1.398(2)
C17 C18 1.389(2)
C17 H17A 0.9500
C18 C19 1.378(3)
C18 H18A 0.9500
C19 C20 1.392(3)
C19 H19A 0.9500
C20 C21 1.391(2)
C20 H20A 0.9500
C21 H21A 0.9500
C22 C27 1.393(2)
C22 C23 1.395(2)
C23 C24 1.393(2)
C23 H23A 0.9500
C24 C25 1.381(3)
C24 H24A 0.9500
C25 C26 1.391(3)
C25 H25A 0.9500
C26 C27 1.391(3)
C26 H26A 0.9500
C27 H27A 0.9500
C28 C29 1.395(2)
C28 C33 1.402(2)
C29 C30 1.390(3)
C29 H29A 0.9500
C30 C31 1.383(3)
C30 H30A 0.9500
C31 C32 1.386(3)
C31 H31A 0.9500
C32 C33 1.386(3)
C32 H32A 0.9500
C33 H33B 0.9500
C34 H34A 0.9800
C34 H34B 0.9800
C34 H34C 0.9800
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
C2 Pt P C28 17.94(8)
C1 Pt P C28 -75.55(8)
C34 Pt P C28 -59.3(12)
N Pt P C28 98.30(7)
Cl1 Pt P C28 -168.50(6)
C2 Pt P C22 138.17(8)
C1 Pt P C22 44.68(8)
C34 Pt P C22 60.9(12)
N Pt P C22 -141.47(7)
Cl1 Pt P C22 -48.27(6)
C2 Pt P C16 -103.06(8)
C1 Pt P C16 163.45(8)
C34 Pt P C16 180(100)
N Pt P C16 -22.70(7)
Cl1 Pt P C16 70.50(6)
C2 Pt N C8 -3.13(13)
C1 Pt N C8 36.7(5)
C34 Pt N C8 84.36(14)
P Pt N C8 -94.56(13)
Cl1 Pt N C8 170.76(12)
C2 Pt N C9 -176.22(14)
C1 Pt N C9 -136.4(4)
C34 Pt N C9 -88.73(15)
P Pt N C9 92.34(13)
Cl1 Pt N C9 -2.33(14)
C1 Pt C2 C3 7.95(17)
C34 Pt C2 C3 94.56(17)
N Pt C2 C3 -177.29(17)
P Pt C2 C3 -82.69(16)
Cl1 Pt C2 C3 141.3(2)
C1 Pt C2 C7 -172.71(13)
C34 Pt C2 C7 -86.10(13)
N Pt C2 C7 2.04(12)
P Pt C2 C7 96.65(12)
Cl1 Pt C2 C7 -39.3(4)
C7 C2 C3 C4 -0.8(3)
Pt C2 C3 C4 178.56(14)
C2 C3 C4 C5 1.0(3)
C3 C4 C5 C6 -0.6(3)
C4 C5 C6 C7 0.0(3)
C5 C6 C7 C2 0.2(3)
C5 C6 C7 C8 -177.99(18)
C3 C2 C7 C6 0.1(3)
Pt C2 C7 C6 -179.27(14)
C3 C2 C7 C8 178.49(16)
Pt C2 C7 C8 -0.9(2)
C9 N C8 C7 176.77(16)
Pt N C8 C7 3.5(2)
C6 C7 C8 N 176.44(17)
C2 C7 C8 N -1.9(2)
C8 N C9 C10 16.0(2)
Pt N C9 C10 -171.54(12)
N C9 C10 C11 -98.0(2)
N C9 C10 C15 80.5(2)
C15 C10 C11 C12 -0.2(3)
C9 C10 C11 C12 178.37(17)
C10 C11 C12 C13 0.2(3)
C11 C12 C13 C14 0.2(3)
C11 C12 C13 Cl2 -179.28(15)
C12 C13 C14 C15 -0.5(3)
Cl2 C13 C14 C15 179.00(15)
C13 C14 C15 C10 0.4(3)
C11 C10 C15 C14 -0.1(3)
C9 C10 C15 C14 -178.66(17)
C28 P C16 C17 -1.66(18)
C22 P C16 C17 -109.50(16)
Pt P C16 C17 121.79(14)
C28 P C16 C21 175.09(13)
C22 P C16 C21 67.26(15)
Pt P C16 C21 -61.45(14)
C21 C16 C17 C18 1.5(3)
P C16 C17 C18 178.24(14)
C16 C17 C18 C19 -0.9(3)
C17 C18 C19 C20 -0.6(3)
C18 C19 C20 C21 1.3(3)
C19 C20 C21 C16 -0.6(3)
C17 C16 C21 C20 -0.8(3)
P C16 C21 C20 -177.76(14)
C28 P C22 C27 -45.72(16)
C16 P C22 C27 63.91(15)
Pt P C22 C27 -169.42(12)
C28 P C22 C23 138.90(14)
C16 P C22 C23 -111.47(15)
Pt P C22 C23 15.20(16)
C27 C22 C23 C24 0.4(3)
P C22 C23 C24 175.72(14)
C22 C23 C24 C25 -0.2(3)
C23 C24 C25 C26 0.4(3)
C24 C25 C26 C27 -0.8(3)
C25 C26 C27 C22 0.9(3)
C23 C22 C27 C26 -0.7(3)
P C22 C27 C26 -176.19(14)
C22 P C28 C29 -27.25(16)
C16 P C28 C29 -132.16(14)
Pt P C28 C29 101.42(14)
C22 P C28 C33 159.09(14)
C16 P C28 C33 54.17(16)
Pt P C28 C33 -72.24(14)
C33 C28 C29 C30 -2.9(3)
P C28 C29 C30 -176.66(14)
C28 C29 C30 C31 0.4(3)
C29 C30 C31 C32 1.6(3)
C30 C31 C32 C33 -1.1(3)
C31 C32 C33 C28 -1.4(3)
C29 C28 C33 C32 3.4(3)
P C28 C33 C32 177.20(14)
