#------------------------------------------------------------------------------
#$Date: 2016-02-14 06:40:26 +0200 (Sun, 14 Feb 2016) $
#$Revision: 176432 $
#$URL: svn://www.crystallography.net/cod/cif/4/08/12/4081252.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4081252
loop_
_publ_author_name
'Hoffmann, Florian'
'Wagler, Jörg'
'Roewer, Gerhard'
_publ_section_title
;
 Transition-Metal Complexes Containing Alkynylsilyl Functionalized
 η6-Arene Ligands
;
_journal_issue                   16
_journal_name_full               Organometallics
_journal_page_first              4531
_journal_paper_doi               10.1021/om400378s
_journal_volume                  32
_journal_year                    2013
_chemical_formula_moiety         '2(C29 H26 Cr Ni2 O3 Si), 0.5(C10 H8)'
_chemical_formula_sum            'C63 H56 Cr2 Ni4 O6 Si2'
_chemical_formula_weight         1304.02
_chemical_melting_point          383
_chemical_name_common
;
dicyclopentadienyldinickel[phenylethynyldimethylphenylsilane]tricarbonyl-
chromium - 0,25 naphthalene 
;
_chemical_name_systematic
; 
tricarbonyl-1kappa3C-dicyclopentadienyl-2(eta5),3(eta5)-[mu3-dimethyl[phenyl-
1(eta6)](phenylethynyl-2kappa2C,C':3kappa2C,C')silane]-1-chromium(0)-2,3-
bis[nickel(I)](Ni-Ni)-naphthalene (4/1) 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                97.025(7)
_cell_angle_beta                 104.083(7)
_cell_angle_gamma                105.141(7)
_cell_formula_units_Z            2
_cell_length_a                   12.5160(14)
_cell_length_b                   13.9396(17)
_cell_length_c                   18.172(2)
_cell_measurement_temperature    93(2)
_cell_volume                     2909.3(6)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'ORTEP32 (Farugia)'
_computing_publication_material  'Ciftab (Sheldrick)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      93(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.998
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0434
_diffrn_reflns_av_sigmaI/netI    0.0565
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       21
_diffrn_reflns_limit_l_min       -21
_diffrn_reflns_number            31172
_diffrn_reflns_theta_full        25.05
_diffrn_reflns_theta_max         25.05
_diffrn_reflns_theta_min         1.75
_exptl_absorpt_coefficient_mu    1.720
_exptl_absorpt_correction_T_max  0.9664
_exptl_absorpt_correction_T_min  0.8228
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            'metallic dark green'
_exptl_crystal_density_diffrn    1.489
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       piece
_exptl_crystal_F_000             1340
_exptl_crystal_size_max          0.18
_exptl_crystal_size_mid          0.07
_exptl_crystal_size_min          0.02
_refine_diff_density_max         0.872
_refine_diff_density_min         -0.571
_refine_diff_density_rms         0.083
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.043
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     694
_refine_ls_number_reflns         10286
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      1.043
_refine_ls_R_factor_all          0.0669
_refine_ls_R_factor_gt           0.0388
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0387P)²+1.4910P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0833
_refine_ls_wR_factor_ref         0.0891
_reflns_number_gt                7523
_reflns_number_total             10286
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om400378s_si_002.cif
_cod_data_source_block           fh20(compound11*0,25C10H8)
_cod_original_sg_symbol_Hall     -P1
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4081252
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Ni1 Ni 0.27066(4) 0.21244(3) 0.89786(3) 0.01653(12) Uani 1 1 d . A 1
Ni2 Ni 0.21293(4) 0.14540(3) 0.76524(3) 0.01620(11) Uani 1 1 d . A 1
Cr1 Cr -0.28792(5) 0.20034(5) 0.69018(3) 0.02381(16) Uani 1 1 d . A 1
Si1 Si 0.00811(8) 0.24241(7) 0.81667(6) 0.0153(2) Uani 1 1 d . A 1
O1 O -0.1938(3) 0.4260(3) 0.7021(2) 0.0596(10) Uani 1 1 d . A 1
O2 O -0.3728(3) 0.2360(3) 0.82862(17) 0.0474(9) Uani 1 1 d . A 1
O3 O -0.5074(3) 0.2262(3) 0.59511(18) 0.0623(12) Uani 1 1 d . A 1
C1 C -0.2290(4) 0.3388(4) 0.6988(3) 0.0360(11) Uani 1 1 d . A 1
C2 C -0.3389(3) 0.2222(4) 0.7756(2) 0.0344(11) Uani 1 1 d . A 1
C3 C -0.4228(4) 0.2148(4) 0.6319(2) 0.0406(12) Uani 1 1 d . A 1
C4 C -0.2132(3) 0.0895(3) 0.7436(2) 0.0242(9) Uani 1 1 d . A 1
H4 H -0.2079 0.0745 0.7937 0.029 Uiso 1 1 calc R A 1
C5 C -0.3126(3) 0.0347(3) 0.6822(2) 0.0301(10) Uani 1 1 d . A 1
H5 H -0.3721 -0.0170 0.6907 0.036 Uiso 1 1 calc R A 1
C6 C -0.3218(3) 0.0581(3) 0.6085(2) 0.0285(10) Uani 1 1 d . A 1
H6 H -0.3896 0.0237 0.5672 0.034 Uiso 1 1 calc R A 1
C7 C -0.2317(3) 0.1317(3) 0.5948(2) 0.0232(9) Uani 1 1 d . A 1
H7 H -0.2368 0.1451 0.5443 0.028 Uiso 1 1 calc R A 1
C8 C -0.1341(3) 0.1849(3) 0.6572(2) 0.0176(8) Uani 1 1 d . A 1
H8 H -0.0743 0.2357 0.6480 0.021 Uiso 1 1 calc R A 1
C9 C -0.1211(3) 0.1660(3) 0.7335(2) 0.0162(8) Uani 1 1 d . A 1
C10 C -0.0363(3) 0.2537(3) 0.9071(2) 0.0214(9) Uani 1 1 d . A 1
H10A H -0.0681 0.1859 0.9167 0.032 Uiso 1 1 d R A 1
H10B H -0.0952 0.2890 0.9015 0.032 Uiso 1 1 d R A 1
H10C H 0.0311 0.2922 0.9506 0.032 Uiso 1 1 d R A 1
C11 C 0.0733(3) 0.3680(3) 0.7947(2) 0.0220(9) Uani 1 1 d . A 1
H11A H 0.1442 0.4049 0.8361 0.033 Uiso 1 1 d R A 1
H11B H 0.0184 0.4072 0.7909 0.033 Uiso 1 1 d R A 1
H11C H 0.0918 0.3578 0.7454 0.033 Uiso 1 1 d R A 1
C12 C 0.1161(3) 0.1720(3) 0.8277(2) 0.0163(8) Uani 1 1 d . A 1
C13 C 0.1499(3) 0.0904(3) 0.84173(19) 0.0157(8) Uani 1 1 d . A 1
C14 C 0.1109(3) -0.0098(3) 0.8612(2) 0.0173(8) Uani 1 1 d . A 1
C15 C 0.1618(3) -0.0852(3) 0.8447(2) 0.0219(9) Uani 1 1 d . A 1
H15 H 0.2212 -0.0720 0.8198 0.026 Uiso 1 1 calc R A 1
C16 C 0.1260(3) -0.1792(3) 0.8645(2) 0.0282(10) Uani 1 1 d . A 1
H16 H 0.1600 -0.2302 0.8524 0.034 Uiso 1 1 calc R A 1
C17 C 0.0402(3) -0.1986(3) 0.9021(2) 0.0264(9) Uani 1 1 d . A 1
H17 H 0.0167 -0.2623 0.9166 0.032 Uiso 1 1 calc R A 1
C18 C -0.0106(3) -0.1247(3) 0.9182(2) 0.0222(9) Uani 1 1 d . A 1
H18 H -0.0694 -0.1381 0.9435 0.027 Uiso 1 1 calc R A 1
C19 C 0.0239(3) -0.0311(3) 0.8978(2) 0.0191(8) Uani 1 1 d . A 1
H19 H -0.0121 0.0189 0.9088 0.023 Uiso 1 1 calc R A 1
C20 C 0.2189(3) 0.0532(3) 0.6656(2) 0.0261(9) Uani 1 1 d . A 1
H20 H 0.1860 -0.0184 0.6515 0.031 Uiso 1 1 calc R A 1
C21 C 0.1623(3) 0.1260(3) 0.6437(2) 0.0248(9) Uani 1 1 d . A 1
H21 H 0.0845 0.1113 0.6133 0.030 Uiso 1 1 calc R A 1
C22 C 0.2420(3) 0.2242(3) 0.6751(2) 0.0258(9) Uani 1 1 d . A 1
H22 H 0.2282 0.2868 0.6685 0.031 Uiso 1 1 calc R A 1
C23 C 0.3460(3) 0.2111(3) 0.7183(2) 0.0269(9) Uani 1 1 d . A 1
H23 H 0.4139 0.2641 0.7469 0.032 Uiso 1 1 calc R A 1
C24 C 0.3323(3) 0.1062(3) 0.7120(2) 0.0276(10) Uani 1 1 d . A 1
H24 H 0.3893 0.0766 0.7349 0.033 Uiso 1 1 calc R A 1
C25 C 0.4084(4) 0.3499(3) 0.9365(2) 0.0354(11) Uani 1 1 d . A 1
H25 H 0.4285 0.3970 0.9048 0.043 Uiso 1 1 calc R A 1
C26 C 0.3305(4) 0.3501(3) 0.9802(2) 0.0360(11) Uani 1 1 d . A 1
H26 H 0.2889 0.3978 0.9838 0.043 Uiso 1 1 calc R A 1
C27 C 0.3244(3) 0.2668(3) 1.0179(2) 0.0263(9) Uani 1 1 d . A 1
H27 H 0.2764 0.2475 1.0502 0.032 Uiso 1 1 calc R A 1
C28 C 0.4016(3) 0.2174(3) 0.9995(2) 0.0195(8) Uani 1 1 d . A 1
H28 H 0.4171 0.1604 1.0185 0.023 Uiso 1 1 calc R A 1
C29 C 0.4520(3) 0.2673(3) 0.9480(2) 0.0239(9) Uani 1 1 d . A 1
H29 H 0.5059 0.2487 0.9249 0.029 Uiso 1 1 calc R A 1
Ni3 Ni 0.58095(4) 0.24364(3) 0.34025(3) 0.01589(12) Uani 1 1 d . B 1
Ni4 Ni 0.57955(4) 0.34213(3) 0.24532(3) 0.01772(12) Uani 1 1 d . B 1
Cr2 Cr 0.12866(5) 0.23519(5) 0.41646(4) 0.02733(17) Uani 1 1 d . B 1
Si2 Si 0.34494(9) 0.33104(8) 0.31185(6) 0.0187(2) Uani 1 1 d . B 1
O4 O 0.2380(3) 0.4414(3) 0.5200(2) 0.0800(14) Uani 1 1 d . B 1
O5 O -0.0360(3) 0.1927(4) 0.5110(2) 0.0846(16) Uani 1 1 d . B 1
O6 O -0.0289(3) 0.3252(3) 0.31438(19) 0.0545(10) Uani 1 1 d . B 1
C30 C 0.1965(4) 0.3620(4) 0.4800(3) 0.0512(14) Uani 1 1 d . B 1
C31 C 0.0267(4) 0.2101(4) 0.4739(3) 0.0490(14) Uani 1 1 d . B 1
C32 C 0.0314(4) 0.2902(4) 0.3531(2) 0.0364(11) Uani 1 1 d . B 1
C33 C 0.1538(3) 0.1592(3) 0.3114(2) 0.0242(9) Uani 1 1 d . B 1
H33 H 0.1218 0.1628 0.2591 0.029 Uiso 1 1 calc R B 1
C34 C 0.0932(3) 0.0833(3) 0.3433(2) 0.0308(10) Uani 1 1 d . B 1
H34 H 0.0226 0.0351 0.3126 0.037 Uiso 1 1 calc R B 1
C35 C 0.1385(3) 0.0795(3) 0.4215(2) 0.0320(10) Uani 1 1 d . B 1
H35 H 0.0969 0.0297 0.4439 0.038 Uiso 1 1 calc R B 1
C36 C 0.2453(3) 0.1491(3) 0.4670(2) 0.0283(10) Uani 1 1 d . B 1
H36 H 0.2764 0.1456 0.5194 0.034 Uiso 1 1 calc R B 1
C37 C 0.3045(3) 0.2234(3) 0.4333(2) 0.0222(9) Uani 1 1 d . B 1
H37 H 0.3759 0.2705 0.4641 0.027 Uiso 1 1 calc R B 1
C38 C 0.2621(3) 0.2311(3) 0.3552(2) 0.0189(8) Uani 1 1 d . B 1
C39 C 0.2456(3) 0.3549(3) 0.2262(2) 0.0271(9) Uani 1 1 d . B 1
H39A H 0.2895 0.4075 0.2045 0.041 Uiso 1 1 d R B 1
H39B H 0.1853 0.3774 0.2421 0.041 Uiso 1 1 d R B 1
H39C H 0.2099 0.2922 0.1869 0.041 Uiso 1 1 d R B 1
C40 C 0.4226(3) 0.4497(3) 0.3859(2) 0.0312(10) Uani 1 1 d . B 1
H40A H 0.4714 0.4343 0.4311 0.047 Uiso 1 1 d R B 1
H40B H 0.3662 0.4786 0.4017 0.047 Uiso 1 1 d R B 1
H40C H 0.4710 0.4986 0.3639 0.047 Uiso 1 1 d R B 1
C41 C 0.4503(3) 0.2773(3) 0.2800(2) 0.0173(8) Uani 1 1 d . B 1
C42 C 0.4798(3) 0.2088(3) 0.2372(2) 0.0152(8) Uani 1 1 d . B 1
C43 C 0.4379(3) 0.1175(3) 0.17624(19) 0.0153(8) Uani 1 1 d . B 1
C44 C 0.5161(3) 0.0704(3) 0.1571(2) 0.0244(9) Uani 1 1 d . B 1
H44 H 0.5958 0.0969 0.1850 0.029 Uiso 1 1 calc R B 1
C45 C 0.4793(4) -0.0141(3) 0.0983(2) 0.0319(10) Uani 1 1 d . B 1
H45 H 0.5335 -0.0452 0.0860 0.038 Uiso 1 1 calc R B 1
C46 C 0.3631(4) -0.0534(3) 0.0572(2) 0.0308(10) Uani 1 1 d . B 1
H46 H 0.3377 -0.1115 0.0168 0.037 Uiso 1 1 calc R B 1
C47 C 0.2846(3) -0.0080(3) 0.0752(2) 0.0241(9) Uani 1 1 d . B 1
H47 H 0.2052 -0.0346 0.0467 0.029 Uiso 1 1 calc R B 1
C48 C 0.3207(3) 0.0764(3) 0.1346(2) 0.0193(8) Uani 1 1 d . B 1
H48 H 0.2658 0.1065 0.1471 0.023 Uiso 1 1 calc R B 1
C49 C 0.6308(3) 0.1288(3) 0.3939(2) 0.0204(8) Uani 1 1 d . B 1
H49 H 0.6031 0.0584 0.3718 0.024 Uiso 1 1 calc R B 1
C50 C 0.5800(3) 0.1832(3) 0.4407(2) 0.0215(9) Uani 1 1 d . B 1
H50 H 0.5113 0.1550 0.4542 0.026 Uiso 1 1 calc R B 1
C51 C 0.6490(3) 0.2854(3) 0.4632(2) 0.0263(9) Uani 1 1 d . B 1
H51 H 0.6363 0.3376 0.4957 0.032 Uiso 1 1 calc R B 1
C52 C 0.7399(3) 0.2966(3) 0.4291(2) 0.0293(10) Uani 1 1 d . B 1
H52 H 0.7981 0.3582 0.4335 0.035 Uiso 1 1 calc R B 1
C53 C 0.7299(3) 0.1997(3) 0.3870(2) 0.0263(9) Uani 1 1 d . B 1
H53 H 0.7810 0.1855 0.3591 0.032 Uiso 1 1 calc R B 1
C54 C 0.6097(4) 0.4941(3) 0.2299(3) 0.0397(12) Uani 1 1 d . B 1
H54 H 0.5679 0.5382 0.2432 0.048 Uiso 1 1 calc R B 1
C55 C 0.5840(4) 0.4268(3) 0.1579(3) 0.0373(12) Uani 1 1 d . B 1
H55 H 0.5194 0.4173 0.1145 0.045 Uiso 1 1 calc R B 1
C56 C 0.6667(4) 0.3778(4) 0.1607(3) 0.0446(13) Uani 1 1 d . B 1
H56 H 0.6696 0.3304 0.1196 0.054 Uiso 1 1 calc R B 1
C57 C 0.7440(4) 0.4089(3) 0.2327(3) 0.0389(12) Uani 1 1 d . B 1
H57 H 0.8091 0.3857 0.2497 0.047 Uiso 1 1 calc R B 1
C58 C 0.7129(4) 0.4810(3) 0.2784(2) 0.0374(12) Uani 1 1 d . B 1
H58 H 0.7522 0.5141 0.3307 0.045 Uiso 1 1 calc R B 1
C60 C 0.9029(5) 0.5061(4) 0.9069(4) 0.0708(17) Uani 1 1 d . . 1
H60 H 0.9079 0.5271 0.8598 0.085 Uiso 1 1 calc R . 1
C61 C 0.7969(5) 0.4634(4) 0.9179(4) 0.0645(16) Uani 1 1 d . C 1
H61 H 0.7292 0.4593 0.8785 0.077 Uiso 1 1 calc R C 1
C62 C 0.7846(5) 0.4266(4) 0.9831(3) 0.0575(15) Uani 1 1 d . C 1
H62 H 0.7107 0.3944 0.9884 0.069 Uiso 1 1 calc R C 1
C63 C 0.8836(5) 0.4384(4) 1.0398(4) 0.0694(17) Uani 1 1 d . C 1
H63 H 0.8789 0.4167 1.0868 0.083 Uiso 1 1 calc R C 1
C64 C 0.9914(4) 0.4815(3) 1.0302(3) 0.0417(12) Uani 1 1 d . . 1
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cr Cr 0.3209 0.6236 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ni Ni 0.3393 1.1124 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C13 Ni1 C12 40.80(14) . .
C13 Ni1 C27 126.76(15) . .
C12 Ni1 C27 128.47(15) . .
C13 Ni1 C29 141.04(16) . .
C12 Ni1 C29 164.62(14) . .
C27 Ni1 C29 65.12(15) . .
C13 Ni1 C26 150.49(17) . .
C12 Ni1 C26 119.52(16) . .
C27 Ni1 C26 39.20(16) . .
C29 Ni1 C26 64.98(16) . .
C13 Ni1 C25 167.96(16) . .
C12 Ni1 C25 134.54(16) . .
C27 Ni1 C25 65.27(16) . .
C29 Ni1 C25 39.00(15) . .
C26 Ni1 C25 38.56(17) . .
C13 Ni1 C28 123.21(14) . .
C12 Ni1 C28 156.31(14) . .
C27 Ni1 C28 38.75(14) . .
C29 Ni1 C28 38.62(13) . .
C26 Ni1 C28 64.98(15) . .
C25 Ni1 C28 64.97(14) . .
C13 Ni1 Ni2 51.98(10) . .
C12 Ni1 Ni2 52.51(10) . .
C27 Ni1 Ni2 177.44(11) . .
C29 Ni1 Ni2 114.27(11) . .
C26 Ni1 Ni2 143.14(13) . .
C25 Ni1 Ni2 115.98(12) . .
C28 Ni1 Ni2 139.26(10) . .
C13 Ni2 C12 41.16(14) . .
C13 Ni2 C23 155.49(15) . .
C12 Ni2 C23 145.13(16) . .
C13 Ni2 C21 136.69(15) . .
C12 Ni2 C21 122.93(15) . .
C23 Ni2 C21 65.56(15) . .
C13 Ni2 C24 130.41(15) . .
C12 Ni2 C24 170.50(15) . .
C23 Ni2 C24 39.19(15) . .
C21 Ni2 C24 65.76(15) . .
C13 Ni2 C20 122.51(15) . .
C12 Ni2 C20 144.90(15) . .
C23 Ni2 C20 65.44(15) . .
C21 Ni2 C20 39.39(15) . .
C24 Ni2 C20 38.93(15) . .
C13 Ni2 C22 163.29(15) . .
C12 Ni2 C22 123.16(15) . .
C23 Ni2 C22 39.06(15) . .
C21 Ni2 C22 39.12(14) . .
C24 Ni2 C22 65.71(15) . .
C20 Ni2 C22 65.68(15) . .
C13 Ni2 Ni1 52.80(11) . .
C12 Ni2 Ni1 52.97(10) . .
C23 Ni2 Ni1 108.70(11) . .
C21 Ni2 Ni1 164.35(11) . .
C24 Ni2 Ni1 119.89(12) . .
C20 Ni2 Ni1 153.55(11) . .
C22 Ni2 Ni1 127.30(11) . .
C3 Cr1 C2 87.66(17) . .
C3 Cr1 C1 85.1(2) . .
C2 Cr1 C1 90.1(2) . .
C3 Cr1 C6 88.64(19) . .
C2 Cr1 C6 129.47(18) . .
C1 Cr1 C6 139.67(17) . .
C3 Cr1 C8 130.32(16) . .
C2 Cr1 C8 141.51(16) . .
C1 Cr1 C8 87.73(16) . .
C6 Cr1 C8 66.65(14) . .
C3 Cr1 C4 142.80(19) . .
C2 Cr1 C4 87.71(17) . .
C1 Cr1 C4 131.80(17) . .
C6 Cr1 C4 66.60(14) . .
C8 Cr1 C4 66.09(13) . .
C3 Cr1 C7 98.69(16) . .
C2 Cr1 C7 164.11(18) . .
C1 Cr1 C7 104.90(17) . .
C6 Cr1 C7 37.03(13) . .
C8 Cr1 C7 36.98(13) . .
C4 Cr1 C7 78.41(14) . .
C3 Cr1 C5 107.4(2) . .
C2 Cr1 C5 97.77(18) . .
C1 Cr1 C5 165.40(16) . .
C6 Cr1 C5 36.86(14) . .
C8 Cr1 C5 78.45(14) . .
C4 Cr1 C5 37.11(14) . .
C7 Cr1 C5 66.46(14) . .
C3 Cr1 C9 166.17(17) . .
C2 Cr1 C9 105.58(15) . .
C1 Cr1 C9 98.60(16) . .
C6 Cr1 C9 79.91(14) . .
C8 Cr1 C9 37.30(12) . .
C4 Cr1 C9 37.11(13) . .
C7 Cr1 C9 67.49(13) . .
C5 Cr1 C9 67.47(13) . .
C12 Si1 C10 108.51(16) . .
C12 Si1 C11 108.59(16) . .
C10 Si1 C11 112.71(18) . .
C12 Si1 C9 107.65(16) . .
C10 Si1 C9 109.24(16) . .
C11 Si1 C9 109.99(16) . .
O1 C1 Cr1 178.1(4) . .
O2 C2 Cr1 178.8(4) . .
O3 C3 Cr1 178.5(5) . .
C5 C4 C9 122.7(3) . .
C5 C4 Cr1 72.2(2) . .
C9 C4 Cr1 72.7(2) . .
C5 C4 H4 118.6 . .
C9 C4 H4 118.6 . .
Cr1 C4 H4 129.0 . .
C6 C5 C4 118.8(4) . .
C6 C5 Cr1 70.6(2) . .
C4 C5 Cr1 70.7(2) . .
C6 C5 H5 120.6 . .
C4 C5 H5 120.6 . .
Cr1 C5 H5 130.7 . .
C5 C6 C7 120.8(4) . .
C5 C6 Cr1 72.6(2) . .
C7 C6 Cr1 72.4(2) . .
C5 C6 H6 119.6 . .
C7 C6 H6 119.6 . .
Cr1 C6 H6 127.6 . .
C8 C7 C6 118.9(3) . .
C8 C7 Cr1 70.7(2) . .
C6 C7 Cr1 70.6(2) . .
C8 C7 H7 120.6 . .
C6 C7 H7 120.6 . .
Cr1 C7 H7 130.7 . .
C7 C8 C9 122.7(3) . .
C7 C8 Cr1 72.3(2) . .
C9 C8 Cr1 72.8(2) . .
C7 C8 H8 118.6 . .
C9 C8 H8 118.6 . .
Cr1 C8 H8 128.7 . .
C4 C9 C8 115.9(3) . .
C4 C9 Si1 122.3(3) . .
C8 C9 Si1 121.7(3) . .
C4 C9 Cr1 70.2(2) . .
C8 C9 Cr1 69.93(19) . .
Si1 C9 Cr1 127.74(18) . .
Si1 C10 H10A 109.5 . .
Si1 C10 H10B 109.5 . .
H10A C10 H10B 109.5 . .
Si1 C10 H10C 109.5 . .
H10A C10 H10C 109.5 . .
H10B C10 H10C 109.5 . .
Si1 C11 H11A 109.5 . .
Si1 C11 H11B 109.5 . .
H11A C11 H11B 109.5 . .
Si1 C11 H11C 109.5 . .
H11A C11 H11C 109.5 . .
H11B C11 H11C 109.5 . .
C13 C12 Si1 152.1(3) . .
C13 C12 Ni2 68.6(2) . .
Si1 C12 Ni2 132.41(19) . .
C13 C12 Ni1 69.2(2) . .
Si1 C12 Ni1 128.65(19) . .
Ni2 C12 Ni1 74.51(12) . .
C12 C13 C14 142.5(3) . .
C12 C13 Ni2 70.2(2) . .
C14 C13 Ni2 137.5(3) . .
C12 C13 Ni1 70.0(2) . .
C14 C13 Ni1 132.0(2) . .
Ni2 C13 Ni1 75.22(12) . .
C19 C14 C15 118.7(3) . .
C19 C14 C13 120.6(3) . .
C15 C14 C13 120.7(3) . .
C16 C15 C14 120.4(4) . .
C16 C15 H15 119.8 . .
C14 C15 H15 119.8 . .
C15 C16 C17 120.1(4) . .
C15 C16 H16 119.9 . .
C17 C16 H16 119.9 . .
C18 C17 C16 119.7(4) . .
C18 C17 H17 120.1 . .
C16 C17 H17 120.1 . .
C17 C18 C19 120.5(4) . .
C17 C18 H18 119.8 . .
C19 C18 H18 119.8 . .
C18 C19 C14 120.6(3) . .
C18 C19 H19 119.7 . .
C14 C19 H19 119.7 . .
C24 C20 C21 107.9(3) . .
C24 C20 Ni2 70.4(2) . .
C21 C20 Ni2 69.9(2) . .
C24 C20 H20 126.0 . .
C21 C20 H20 126.0 . .
Ni2 C20 H20 125.3 . .
C22 C21 C20 108.3(3) . .
C22 C21 Ni2 71.4(2) . .
C20 C21 Ni2 70.7(2) . .
C22 C21 H21 125.8 . .
C20 C21 H21 125.8 . .
Ni2 C21 H21 123.7 . .
C23 C22 C21 107.0(3) . .
C23 C22 Ni2 69.4(2) . .
C21 C22 Ni2 69.5(2) . .
C23 C22 H22 126.5 . .
C21 C22 H22 126.5 . .
Ni2 C22 H22 126.2 . .
C22 C23 C24 108.9(4) . .
C22 C23 Ni2 71.5(2) . .
C24 C23 Ni2 70.8(2) . .
C22 C23 H23 125.5 . .
C24 C23 H23 125.5 . .
Ni2 C23 H23 123.7 . .
C20 C24 C23 107.8(4) . .
C20 C24 Ni2 70.7(2) . .
C23 C24 Ni2 70.0(2) . .
C20 C24 H24 126.1 . .
C23 C24 H24 126.1 . .
Ni2 C24 H24 124.8 . .
C26 C25 C29 107.9(3) . .
C26 C25 Ni1 70.6(2) . .
C29 C25 Ni1 70.4(2) . .
C26 C25 H25 126.1 . .
C29 C25 H25 126.1 . .
Ni1 C25 H25 124.5 . .
C25 C26 C27 107.9(4) . .
C25 C26 Ni1 70.8(2) . .
C27 C26 Ni1 69.7(2) . .
C25 C26 H26 126.0 . .
C27 C26 H26 126.0 . .
Ni1 C26 H26 125.1 . .
C28 C27 C26 108.2(4) . .
C28 C27 Ni1 71.9(2) . .
C26 C27 Ni1 71.1(2) . .
C28 C27 H27 125.9 . .
C26 C27 H27 125.9 . .
Ni1 C27 H27 122.7 . .
C27 C28 C29 107.8(3) . .
C27 C28 Ni1 69.4(2) . .
C29 C28 Ni1 70.2(2) . .
C27 C28 H28 126.1 . .
C29 C28 H28 126.1 . .
Ni1 C28 H28 126.0 . .
C28 C29 C25 108.2(4) . .
C28 C29 Ni1 71.2(2) . .
C25 C29 Ni1 70.6(2) . .
C28 C29 H29 125.9 . .
C25 C29 H29 125.9 . .
Ni1 C29 H29 123.9 . .
C42 Ni3 C41 40.80(15) . .
C42 Ni3 C50 134.22(14) . .
C41 Ni3 C50 123.14(14) . .
C42 Ni3 C52 157.42(15) . .
C41 Ni3 C52 146.60(16) . .
C50 Ni3 C52 65.25(15) . .
C42 Ni3 C49 119.74(15) . .
C41 Ni3 C49 143.76(14) . .
C50 Ni3 C49 39.72(14) . .
C52 Ni3 C49 65.61(15) . .
C42 Ni3 C53 129.72(16) . .
C41 Ni3 C53 169.69(15) . .
C50 Ni3 C53 65.60(15) . .
C52 Ni3 C53 39.30(15) . .
C49 Ni3 C53 38.84(14) . .
C42 Ni3 C51 163.21(15) . .
C41 Ni3 C51 124.74(16) . .
C50 Ni3 C51 38.84(14) . .
C52 Ni3 C51 38.60(15) . .
C49 Ni3 C51 65.70(15) . .
C53 Ni3 C51 65.31(16) . .
C42 Ni3 Ni4 52.52(10) . .
C41 Ni3 Ni4 52.60(10) . .
C50 Ni3 Ni4 167.38(11) . .
C52 Ni3 Ni4 111.27(11) . .
C49 Ni3 Ni4 151.61(10) . .
C53 Ni3 Ni4 120.18(11) . .
C51 Ni3 Ni4 130.89(11) . .
C42 Ni4 C41 40.88(15) . .
C42 Ni4 C55 127.43(15) . .
C41 Ni4 C55 129.18(16) . .
C42 Ni4 C58 166.16(15) . .
C41 Ni4 C58 136.93(17) . .
C55 Ni4 C58 65.83(16) . .
C42 Ni4 C57 137.94(17) . .
C41 Ni4 C57 166.38(17) . .
C55 Ni4 C57 63.89(17) . .
C58 Ni4 C57 39.32(17) . .
C42 Ni4 C54 152.28(16) . .
C41 Ni4 C54 120.66(16) . .
C55 Ni4 C54 39.56(17) . .
C58 Ni4 C54 40.00(17) . .
C57 Ni4 C54 65.71(17) . .
C42 Ni4 C56 121.64(17) . .
C41 Ni4 C56 154.63(18) . .
C55 Ni4 C56 38.05(17) . .
C58 Ni4 C56 65.13(18) . .
C57 Ni4 C56 37.61(17) . .
C54 Ni4 C56 65.42(18) . .
C42 Ni4 Ni3 52.35(10) . .
C41 Ni4 Ni3 53.07(10) . .
C55 Ni4 Ni3 176.98(14) . .
C58 Ni4 Ni3 114.17(11) . .
C57 Ni4 Ni3 114.04(13) . .
C54 Ni4 Ni3 142.32(14) . .
C56 Ni4 Ni3 138.98(14) . .
C31 Cr2 C30 87.7(2) . .
C31 Cr2 C32 89.42(19) . .
C30 Cr2 C32 88.2(2) . .
C31 Cr2 C37 132.50(17) . .
C30 Cr2 C37 86.79(17) . .
C32 Cr2 C37 137.42(16) . .
C31 Cr2 C33 137.5(2) . .
C30 Cr2 C33 134.52(19) . .
C32 Cr2 C33 87.83(17) . .
C37 Cr2 C33 66.80(14) . .
C31 Cr2 C35 86.3(2) . .
C30 Cr2 C35 136.4(2) . .
C32 Cr2 C35 134.79(18) . .
C37 Cr2 C35 66.66(14) . .
C33 Cr2 C35 66.67(15) . .
C31 Cr2 C36 99.15(17) . .
C30 Cr2 C36 102.07(19) . .
C32 Cr2 C36 166.80(17) . .
C37 Cr2 C36 37.03(13) . .
C33 Cr2 C36 79.06(15) . .
C35 Cr2 C36 37.12(14) . .
C31 Cr2 C38 165.64(19) . .
C30 Cr2 C38 100.02(17) . .
C32 Cr2 C38 102.83(16) . .
C37 Cr2 C38 37.27(13) . .
C33 Cr2 C38 37.68(13) . .
C35 Cr2 C38 79.76(14) . .
C36 Cr2 C38 67.51(14) . .
C31 Cr2 C34 102.9(2) . .
C30 Cr2 C34 165.46(17) . .
C32 Cr2 C34 101.63(18) . .
C37 Cr2 C34 78.72(14) . .
C33 Cr2 C34 36.98(14) . .
C35 Cr2 C34 36.91(14) . .
C36 Cr2 C34 66.78(15) . .
C38 Cr2 C34 67.56(13) . .
C41 Si2 C40 109.87(17) . .
C41 Si2 C39 109.28(17) . .
C40 Si2 C39 111.37(19) . .
C41 Si2 C38 105.45(16) . .
C40 Si2 C38 110.45(18) . .
C39 Si2 C38 110.24(17) . .
O4 C30 Cr2 179.3(4) . .
O5 C31 Cr2 178.2(4) . .
O6 C32 Cr2 179.3(4) . .
C34 C33 C38 122.0(4) . .
C34 C33 Cr2 72.7(2) . .
C38 C33 Cr2 72.3(2) . .
C34 C33 H33 119.0 . .
C38 C33 H33 119.0 . .
Cr2 C33 H33 128.3 . .
C33 C34 C35 119.2(4) . .
C33 C34 Cr2 70.3(2) . .
C35 C34 Cr2 71.0(2) . .
C33 C34 H34 120.4 . .
C35 C34 H34 120.4 . .
Cr2 C34 H34 131.0 . .
C34 C35 C36 120.7(4) . .
C34 C35 Cr2 72.1(2) . .
C36 C35 Cr2 71.7(2) . .
C34 C35 H35 119.7 . .
C36 C35 H35 119.7 . .
Cr2 C35 H35 128.9 . .
C37 C36 C35 118.9(4) . .
C37 C36 Cr2 70.6(2) . .
C35 C36 Cr2 71.2(2) . .
C37 C36 H36 120.6 . .
C35 C36 H36 120.6 . .
Cr2 C36 H36 130.1 . .
C36 C37 C38 122.6(4) . .
C36 C37 Cr2 72.4(2) . .
C38 C37 Cr2 72.5(2) . .
C36 C37 H37 118.7 . .
C38 C37 H37 118.7 . .
Cr2 C37 H37 128.9 . .
C37 C38 C33 116.6(3) . .
C37 C38 Si2 121.4(3) . .
C33 C38 Si2 122.0(3) . .
C37 C38 Cr2 70.2(2) . .
C33 C38 Cr2 70.0(2) . .
Si2 C38 Cr2 130.38(19) . .
Si2 C39 H39A 109.5 . .
Si2 C39 H39B 109.5 . .
H39A C39 H39B 109.5 . .
Si2 C39 H39C 109.5 . .
H39A C39 H39C 109.5 . .
H39B C39 H39C 109.5 . .
Si2 C40 H40A 109.5 . .
Si2 C40 H40B 109.5 . .
H40A C40 H40B 109.5 . .
Si2 C40 H40C 109.5 . .
H40A C40 H40C 109.5 . .
H40B C40 H40C 109.5 . .
C42 C41 Si2 153.5(3) . .
C42 C41 Ni4 69.2(2) . .
Si2 C41 Ni4 129.5(2) . .
C42 C41 Ni3 68.6(2) . .
Si2 C41 Ni3 130.0(2) . .
Ni4 C41 Ni3 74.32(12) . .
C41 C42 C43 145.9(3) . .
C41 C42 Ni3 70.6(2) . .
C43 C42 Ni3 133.7(3) . .
C41 C42 Ni4 69.9(2) . .
C43 C42 Ni4 132.2(2) . .
Ni3 C42 Ni4 75.13(13) . .
C44 C43 C48 118.4(3) . .
C44 C43 C42 119.8(3) . .
C48 C43 C42 121.8(3) . .
C45 C44 C43 121.0(4) . .
C45 C44 H44 119.5 . .
C43 C44 H44 119.5 . .
C44 C45 C46 120.0(4) . .
C44 C45 H45 120.0 . .
C46 C45 H45 120.0 . .
C47 C46 C45 119.9(4) . .
C47 C46 H46 120.1 . .
C45 C46 H46 120.1 . .
C46 C47 C48 120.5(4) . .
C46 C47 H47 119.7 . .
C48 C47 H47 119.7 . .
C47 C48 C43 120.3(4) . .
C47 C48 H48 119.9 . .
C43 C48 H48 119.9 . .
C53 C49 C50 107.1(3) . .
C53 C49 Ni3 70.7(2) . .
C50 C49 Ni3 69.4(2) . .
C53 C49 H49 126.5 . .
C50 C49 H49 126.5 . .
Ni3 C49 H49 125.1 . .
C51 C50 C49 108.5(3) . .
C51 C50 Ni3 71.8(2) . .
C49 C50 Ni3 70.9(2) . .
C51 C50 H50 125.7 . .
C49 C50 H50 125.7 . .
Ni3 C50 H50 123.2 . .
C52 C51 C50 107.9(4) . .
C52 C51 Ni3 70.1(2) . .
C50 C51 Ni3 69.4(2) . .
C52 C51 H51 126.0 . .
C50 C51 H51 126.0 . .
Ni3 C51 H51 126.0 . .
C51 C52 C53 108.5(3) . .
C51 C52 Ni3 71.3(2) . .
C53 C52 Ni3 70.7(2) . .
C51 C52 H52 125.8 . .
C53 C52 H52 125.8 . .
Ni3 C52 H52 123.9 . .
C49 C53 C52 108.0(3) . .
C49 C53 Ni3 70.4(2) . .
C52 C53 Ni3 70.0(2) . .
C49 C53 H53 126.0 . .
C52 C53 H53 126.0 . .
Ni3 C53 H53 125.1 . .
C55 C54 C58 105.3(4) . .
C55 C54 Ni4 69.3(2) . .
C58 C54 Ni4 69.5(2) . .
C55 C54 H54 127.3 . .
C58 C54 H54 127.3 . .
Ni4 C54 H54 125.4 . .
C56 C55 C54 109.9(4) . .
C56 C55 Ni4 72.2(2) . .
C54 C55 Ni4 71.1(2) . .
C56 C55 H55 125.1 . .
C54 C55 H55 125.1 . .
Ni4 C55 H55 123.2 . .
C57 C56 C55 108.4(5) . .
C57 C56 Ni4 70.4(2) . .
C55 C56 Ni4 69.7(3) . .
C57 C56 H56 125.8 . .
C55 C56 H56 125.8 . .
Ni4 C56 H56 125.6 . .
C56 C57 C58 110.0(4) . .
C56 C57 Ni4 72.0(2) . .
C58 C57 Ni4 70.3(2) . .
C56 C57 H57 125.0 . .
C58 C57 H57 125.0 . .
Ni4 C57 H57 124.3 . .
C57 C58 C54 106.4(4) . .
C57 C58 Ni4 70.4(2) . .
C54 C58 Ni4 70.5(2) . .
C57 C58 H58 126.8 . .
C54 C58 H58 126.8 . .
Ni4 C58 H58 124.0 . .
C61 C60 C64 118.8(6) . 2_767
C61 C60 H60 120.6 . .
C64 C60 H60 120.6 2_767 .
C62 C61 C60 123.0(6) . .
C62 C61 H61 118.5 . .
C60 C61 H61 118.5 . .
C63 C62 C61 116.7(6) . .
C63 C62 H62 121.7 . .
C61 C62 H62 121.7 . .
C62 C63 C64 121.2(6) . .
C62 C63 H63 119.4 . .
C64 C63 H63 119.4 . .
C64 C64 C63 124.9(7) 2_767 .
C64 C64 C60 115.2(6) 2_767 2_767
C63 C64 C60 119.9(5) . 2_767
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ni1 C13 1.923(4) .
Ni1 C12 1.934(3) .
Ni1 C27 2.098(4) .
Ni1 C29 2.117(4) .
Ni1 C26 2.117(4) .
Ni1 C25 2.120(4) .
Ni1 C28 2.131(4) .
Ni1 Ni2 2.3351(7) .
Ni2 C13 1.902(3) .
Ni2 C12 1.923(3) .
Ni2 C23 2.103(4) .
Ni2 C21 2.106(4) .
Ni2 C24 2.113(4) .
Ni2 C20 2.117(4) .
Ni2 C22 2.131(4) .
Cr1 C3 1.836(4) .
Cr1 C2 1.837(4) .
Cr1 C1 1.850(5) .
Cr1 C6 2.203(4) .
Cr1 C8 2.205(3) .
Cr1 C4 2.210(4) .
Cr1 C7 2.226(4) .
Cr1 C5 2.229(4) .
Cr1 C9 2.242(3) .
Si1 C12 1.854(4) .
Si1 C10 1.860(4) .
Si1 C11 1.864(4) .
Si1 C9 1.884(4) .
O1 C1 1.167(5) .
O2 C2 1.159(5) .
O3 C3 1.168(5) .
C4 C5 1.413(5) .
C4 C9 1.417(5) .
C4 H4 0.9500 .
C5 C6 1.401(5) .
C5 H5 0.9500 .
C6 C7 1.407(5) .
C6 H6 0.9500 .
C7 C8 1.405(5) .
C7 H7 0.9500 .
C8 C9 1.422(5) .
C8 H8 0.9500 .
C10 H10A 0.9800 .
C10 H10B 0.9800 .
C10 H10C 0.9800 .
C11 H11A 0.9800 .
C11 H11B 0.9800 .
C11 H11C 0.9800 .
C12 C13 1.345(5) .
C13 C14 1.471(5) .
C14 C19 1.395(5) .
C14 C15 1.403(5) .
C15 C16 1.390(5) .
C15 H15 0.9500 .
C16 C17 1.394(5) .
C16 H16 0.9500 .
C17 C18 1.381(5) .
C17 H17 0.9500 .
C18 C19 1.390(5) .
C18 H18 0.9500 .
C19 H19 0.9500 .
C20 C24 1.410(5) .
C20 C21 1.423(5) .
C20 H20 0.9500 .
C21 C22 1.418(5) .
C21 H21 0.9500 .
C22 C23 1.416(6) .
C22 H22 0.9500 .
C23 C24 1.414(5) .
C23 H23 0.9500 .
C24 H24 0.9500 .
C25 C26 1.399(6) .
C25 C29 1.414(6) .
C25 H25 0.9500 .
C26 C27 1.414(6) .
C26 H26 0.9500 .
C27 C28 1.403(5) .
C27 H27 0.9500 .
C28 C29 1.405(5) .
C28 H28 0.9500 .
C29 H29 0.9500 .
Ni3 C42 1.910(3) .
Ni3 C41 1.936(4) .
Ni3 C50 2.103(4) .
Ni3 C52 2.119(4) .
Ni3 C49 2.124(4) .
Ni3 C53 2.127(4) .
Ni3 C51 2.134(4) .
Ni3 Ni4 2.3321(7) .
Ni4 C42 1.915(3) .
Ni4 C41 1.924(3) .
Ni4 C55 2.095(4) .
Ni4 C58 2.106(4) .
Ni4 C57 2.106(4) .
Ni4 C54 2.119(4) .
Ni4 C56 2.126(4) .
Cr2 C31 1.828(5) .
Cr2 C30 1.848(5) .
Cr2 C32 1.849(5) .
Cr2 C37 2.200(4) .
Cr2 C33 2.200(4) .
Cr2 C35 2.217(4) .
Cr2 C36 2.224(4) .
Cr2 C38 2.229(3) .
Cr2 C34 2.232(4) .
Si2 C41 1.848(4) .
Si2 C40 1.863(4) .
Si2 C39 1.866(4) .
Si2 C38 1.884(4) .
O4 C30 1.160(6) .
O5 C31 1.153(5) .
O6 C32 1.149(5) .
C33 C34 1.406(5) .
C33 C38 1.431(5) .
C33 H33 0.9500 .
C34 C35 1.408(5) .
C34 H34 0.9500 .
C35 C36 1.414(5) .
C35 H35 0.9500 .
C36 C37 1.405(5) .
C36 H36 0.9500 .
C37 C38 1.416(5) .
C37 H37 0.9500 .
C39 H39A 0.9800 .
C39 H39B 0.9800 .
C39 H39C 0.9800 .
C40 H40A 0.9800 .
C40 H40B 0.9800 .
C40 H40C 0.9800 .
C41 C42 1.341(5) .
C42 C43 1.464(5) .
C43 C44 1.398(5) .
C43 C48 1.403(5) .
C44 C45 1.383(5) .
C44 H44 0.9500 .
C45 C46 1.389(6) .
C45 H45 0.9500 .
C46 C47 1.380(6) .
C46 H46 0.9500 .
C47 C48 1.389(5) .
C47 H47 0.9500 .
C48 H48 0.9500 .
C49 C53 1.413(5) .
C49 C50 1.436(5) .
C49 H49 0.9500 .
C50 C51 1.409(5) .
C50 H50 0.9500 .
C51 C52 1.406(5) .
C51 H51 0.9500 .
C52 C53 1.428(6) .
C52 H52 0.9500 .
C53 H53 0.9500 .
C54 C55 1.426(6) .
C54 C58 1.445(6) .
C54 H54 0.9500 .
C55 C56 1.376(6) .
C55 H55 0.9500 .
C56 C57 1.364(6) .
C56 H56 0.9500 .
C57 C58 1.417(6) .
C57 H57 0.9500 .
C58 H58 0.9500 .
C60 C61 1.377(7) .
C60 C64 1.478(7) 2_767
C60 H60 0.9500 .
C61 C62 1.375(7) .
C61 H61 0.9500 .
C62 C63 1.362(7) .
C62 H62 0.9500 .
C63 C64 1.388(7) .
C63 H63 0.9500 .
C64 C64 1.309(9) 2_767
C64 C60 1.478(7) 2_767
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C12 Ni1 Ni2 C13 -52.31(18) . .
C29 Ni1 Ni2 C13 136.91(18) . .
C26 Ni1 Ni2 C13 -143.0(2) . .
C25 Ni1 Ni2 C13 -179.86(19) . .
C28 Ni1 Ni2 C13 99.1(2) . .
C13 Ni1 Ni2 C12 52.31(18) . .
C29 Ni1 Ni2 C12 -170.79(18) . .
C26 Ni1 Ni2 C12 -90.7(2) . .
C25 Ni1 Ni2 C12 -127.56(19) . .
C28 Ni1 Ni2 C12 151.4(2) . .
C13 Ni1 Ni2 C23 -161.63(18) . .
C12 Ni1 Ni2 C23 146.06(18) . .
C29 Ni1 Ni2 C23 -24.73(17) . .
C26 Ni1 Ni2 C23 55.4(2) . .
C25 Ni1 Ni2 C23 18.50(18) . .
C28 Ni1 Ni2 C23 -62.56(19) . .
C13 Ni1 Ni2 C21 132.6(4) . .
C12 Ni1 Ni2 C21 80.3(4) . .
C29 Ni1 Ni2 C21 -90.5(4) . .
C26 Ni1 Ni2 C21 -10.4(5) . .
C25 Ni1 Ni2 C21 -47.2(4) . .
C28 Ni1 Ni2 C21 -128.3(4) . .
C13 Ni1 Ni2 C24 -120.16(18) . .
C12 Ni1 Ni2 C24 -172.47(18) . .
C29 Ni1 Ni2 C24 16.75(17) . .
C26 Ni1 Ni2 C24 96.8(2) . .
C25 Ni1 Ni2 C24 59.98(19) . .
C28 Ni1 Ni2 C24 -21.1(2) . .
C13 Ni1 Ni2 C20 -89.4(3) . .
C12 Ni1 Ni2 C20 -141.7(3) . .
C29 Ni1 Ni2 C20 47.5(3) . .
C26 Ni1 Ni2 C20 127.6(3) . .
C25 Ni1 Ni2 C20 90.8(3) . .
C28 Ni1 Ni2 C20 9.7(3) . .
C13 Ni1 Ni2 C22 158.96(19) . .
C12 Ni1 Ni2 C22 106.65(19) . .
C29 Ni1 Ni2 C22 -64.13(18) . .
C26 Ni1 Ni2 C22 16.0(2) . .
C25 Ni1 Ni2 C22 -20.9(2) . .
C28 Ni1 Ni2 C22 -102.0(2) . .
C3 Cr1 C4 C5 23.0(4) . .
C2 Cr1 C4 C5 106.1(3) . .
C1 Cr1 C4 C5 -165.9(3) . .
C6 Cr1 C4 C5 -29.2(2) . .
C8 Cr1 C4 C5 -102.9(3) . .
C7 Cr1 C4 C5 -66.1(2) . .
C9 Cr1 C4 C5 -134.0(3) . .
C3 Cr1 C4 C9 157.0(3) . .
C2 Cr1 C4 C9 -119.9(2) . .
C1 Cr1 C4 C9 -31.8(3) . .
C6 Cr1 C4 C9 104.8(2) . .
C8 Cr1 C4 C9 31.1(2) . .
C7 Cr1 C4 C9 67.9(2) . .
C5 Cr1 C4 C9 134.0(3) . .
C9 C4 C5 C6 -1.2(6) . .
Cr1 C4 C5 C6 53.4(4) . .
C9 C4 C5 Cr1 -54.7(3) . .
C3 Cr1 C5 C6 62.6(3) . .
C2 Cr1 C5 C6 152.6(2) . .
C1 Cr1 C5 C6 -85.5(7) . .
C8 Cr1 C5 C6 -66.3(2) . .
C4 Cr1 C5 C6 -131.7(3) . .
C7 Cr1 C5 C6 -29.5(2) . .
C9 Cr1 C5 C6 -103.7(2) . .
C3 Cr1 C5 C4 -165.7(2) . .
C2 Cr1 C5 C4 -75.7(3) . .
C1 Cr1 C5 C4 46.3(8) . .
C6 Cr1 C5 C4 131.7(3) . .
C8 Cr1 C5 C4 65.4(2) . .
C7 Cr1 C5 C4 102.3(3) . .
C9 Cr1 C5 C4 28.0(2) . .
C4 C5 C6 C7 2.7(6) . .
Cr1 C5 C6 C7 56.2(4) . .
C4 C5 C6 Cr1 -53.5(4) . .
C3 Cr1 C6 C5 -122.1(3) . .
C2 Cr1 C6 C5 -36.2(3) . .
C1 Cr1 C6 C5 157.2(3) . .
C8 Cr1 C6 C5 102.3(2) . .
C4 Cr1 C6 C5 29.4(2) . .
C7 Cr1 C6 C5 131.5(3) . .
C9 Cr1 C6 C5 65.7(2) . .
C3 Cr1 C6 C7 106.4(2) . .
C2 Cr1 C6 C7 -167.7(2) . .
C1 Cr1 C6 C7 25.6(3) . .
C8 Cr1 C6 C7 -29.2(2) . .
C4 Cr1 C6 C7 -102.1(2) . .
C5 Cr1 C6 C7 -131.5(3) . .
C9 Cr1 C6 C7 -65.8(2) . .
C5 C6 C7 C8 -2.8(6) . .
Cr1 C6 C7 C8 53.5(3) . .
C5 C6 C7 Cr1 -56.3(4) . .
C3 Cr1 C7 C8 152.3(3) . .
C2 Cr1 C7 C8 -95.0(6) . .
C1 Cr1 C7 C8 65.1(3) . .
C6 Cr1 C7 C8 -131.8(3) . .
C4 Cr1 C7 C8 -65.4(2) . .
C5 Cr1 C7 C8 -102.4(2) . .
C9 Cr1 C7 C8 -28.2(2) . .
C3 Cr1 C7 C6 -76.0(3) . .
C2 Cr1 C7 C6 36.8(7) . .
C1 Cr1 C7 C6 -163.2(2) . .
C8 Cr1 C7 C6 131.8(3) . .
C4 Cr1 C7 C6 66.3(2) . .
C5 Cr1 C7 C6 29.3(2) . .
C9 Cr1 C7 C6 103.6(2) . .
C6 C7 C8 C9 1.5(6) . .
Cr1 C7 C8 C9 54.9(3) . .
C6 C7 C8 Cr1 -53.5(3) . .
C3 Cr1 C8 C7 -37.1(3) . .
C2 Cr1 C8 C7 154.0(3) . .
C1 Cr1 C8 C7 -118.7(3) . .
C6 Cr1 C8 C7 29.3(2) . .
C4 Cr1 C8 C7 102.9(2) . .
C5 Cr1 C8 C7 66.0(2) . .
C9 Cr1 C8 C7 133.9(3) . .
C3 Cr1 C8 C9 -171.0(3) . .
C2 Cr1 C8 C9 20.1(4) . .
C1 Cr1 C8 C9 107.4(2) . .
C6 Cr1 C8 C9 -104.6(2) . .
C4 Cr1 C8 C9 -31.0(2) . .
C7 Cr1 C8 C9 -133.9(3) . .
C5 Cr1 C8 C9 -67.8(2) . .
C5 C4 C9 C8 0.0(5) . .
Cr1 C4 C9 C8 -54.5(3) . .
C5 C4 C9 Si1 177.3(3) . .
Cr1 C4 C9 Si1 122.8(3) . .
C5 C4 C9 Cr1 54.5(4) . .
C7 C8 C9 C4 -0.1(5) . .
Cr1 C8 C9 C4 54.6(3) . .
C7 C8 C9 Si1 -177.4(3) . .
Cr1 C8 C9 Si1 -122.7(3) . .
C7 C8 C9 Cr1 -54.7(3) . .
C12 Si1 C9 C4 88.0(3) . .
C10 Si1 C9 C4 -29.7(3) . .
C11 Si1 C9 C4 -153.9(3) . .
C12 Si1 C9 C8 -94.8(3) . .
C10 Si1 C9 C8 147.5(3) . .
C11 Si1 C9 C8 23.3(3) . .
C12 Si1 C9 Cr1 177.02(19) . .
C10 Si1 C9 Cr1 59.4(2) . .
C11 Si1 C9 Cr1 -64.8(2) . .
C3 Cr1 C9 C4 -98.8(8) . .
C2 Cr1 C9 C4 64.1(3) . .
C1 Cr1 C9 C4 156.6(2) . .
C6 Cr1 C9 C4 -64.3(2) . .
C8 Cr1 C9 C4 -128.8(3) . .
C7 Cr1 C9 C4 -100.8(2) . .
C5 Cr1 C9 C4 -28.0(2) . .
C3 Cr1 C9 C8 30.0(8) . .
C2 Cr1 C9 C8 -167.1(2) . .
C1 Cr1 C9 C8 -74.6(2) . .
C6 Cr1 C9 C8 64.5(2) . .
C4 Cr1 C9 C8 128.8(3) . .
C7 Cr1 C9 C8 28.0(2) . .
C5 Cr1 C9 C8 100.8(2) . .
C3 Cr1 C9 Si1 145.0(7) . .
C2 Cr1 C9 Si1 -52.1(3) . .
C1 Cr1 C9 Si1 40.4(3) . .
C6 Cr1 C9 Si1 179.6(2) . .
C8 Cr1 C9 Si1 115.1(3) . .
C4 Cr1 C9 Si1 -116.1(3) . .
C7 Cr1 C9 Si1 143.1(2) . .
C5 Cr1 C9 Si1 -144.2(3) . .
C10 Si1 C12 C13 56.5(6) . .
C11 Si1 C12 C13 179.3(6) . .
C9 Si1 C12 C13 -61.6(6) . .
C10 Si1 C12 Ni2 -171.5(2) . .
C11 Si1 C12 Ni2 -48.6(3) . .
C9 Si1 C12 Ni2 70.4(3) . .
C10 Si1 C12 Ni1 -66.0(3) . .
C11 Si1 C12 Ni1 56.9(3) . .
C9 Si1 C12 Ni1 175.9(2) . .
C23 Ni2 C12 C13 -140.9(3) . .
C21 Ni2 C12 C13 125.2(2) . .
C20 Ni2 C12 C13 78.0(3) . .
C22 Ni2 C12 C13 172.3(2) . .
Ni1 Ni2 C12 C13 -73.3(2) . .
C13 Ni2 C12 Si1 -158.1(4) . .
C23 Ni2 C12 Si1 61.0(4) . .
C21 Ni2 C12 Si1 -32.9(3) . .
C20 Ni2 C12 Si1 -80.0(4) . .
C22 Ni2 C12 Si1 14.2(3) . .
Ni1 Ni2 C12 Si1 128.7(3) . .
C13 Ni2 C12 Ni1 73.3(2) . .
C23 Ni2 C12 Ni1 -67.7(3) . .
C21 Ni2 C12 Ni1 -161.53(13) . .
C20 Ni2 C12 Ni1 151.3(2) . .
C22 Ni2 C12 Ni1 -114.45(15) . .
C27 Ni1 C12 C13 -104.4(2) . .
C29 Ni1 C12 C13 106.0(6) . .
C26 Ni1 C12 C13 -151.0(2) . .
C25 Ni1 C12 C13 163.7(2) . .
C28 Ni1 C12 C13 -56.4(4) . .
Ni2 Ni1 C12 C13 72.58(19) . .
C13 Ni1 C12 Si1 155.0(4) . .
C27 Ni1 C12 Si1 50.6(3) . .
C29 Ni1 C12 Si1 -99.0(6) . .
C26 Ni1 C12 Si1 4.0(3) . .
C25 Ni1 C12 Si1 -41.3(3) . .
C28 Ni1 C12 Si1 98.7(4) . .
Ni2 Ni1 C12 Si1 -132.4(3) . .
C13 Ni1 C12 Ni2 -72.58(19) . .
C27 Ni1 C12 Ni2 -177.01(14) . .
C29 Ni1 C12 Ni2 33.4(6) . .
C26 Ni1 C12 Ni2 136.43(16) . .
C25 Ni1 C12 Ni2 91.1(2) . .
C28 Ni1 C12 Ni2 -128.9(3) . .
Si1 C12 C13 C14 -1.1(10) . .
Ni2 C12 C13 C14 -145.0(5) . .
Ni1 C12 C13 C14 134.1(5) . .
Si1 C12 C13 Ni2 143.9(6) . .
Ni1 C12 C13 Ni2 -80.92(10) . .
Si1 C12 C13 Ni1 -135.2(6) . .
Ni2 C12 C13 Ni1 80.92(10) . .
C23 Ni2 C13 C12 119.7(4) . .
C21 Ni2 C13 C12 -89.5(3) . .
C24 Ni2 C13 C12 173.8(2) . .
C20 Ni2 C13 C12 -138.2(2) . .
C22 Ni2 C13 C12 -23.0(6) . .
Ni1 Ni2 C13 C12 73.7(2) . .
C12 Ni2 C13 C14 148.8(5) . .
C23 Ni2 C13 C14 -91.5(5) . .
C21 Ni2 C13 C14 59.4(5) . .
C24 Ni2 C13 C14 -37.4(5) . .
C20 Ni2 C13 C14 10.7(4) . .
C22 Ni2 C13 C14 125.8(5) . .
Ni1 Ni2 C13 C14 -137.5(4) . .
C12 Ni2 C13 Ni1 -73.7(2) . .
C23 Ni2 C13 Ni1 46.0(4) . .
C21 Ni2 C13 Ni1 -163.18(17) . .
C24 Ni2 C13 Ni1 100.10(19) . .
C20 Ni2 C13 Ni1 148.12(14) . .
C22 Ni2 C13 Ni1 -96.7(5) . .
C27 Ni1 C13 C12 108.8(2) . .
C29 Ni1 C13 C12 -156.1(2) . .
C26 Ni1 C13 C12 58.9(4) . .
C25 Ni1 C13 C12 -73.4(8) . .
C28 Ni1 C13 C12 156.4(2) . .
Ni2 Ni1 C13 C12 -73.95(19) . .
C12 Ni1 C13 C14 -143.9(4) . .
C27 Ni1 C13 C14 -35.1(4) . .
C29 Ni1 C13 C14 60.0(4) . .
C26 Ni1 C13 C14 -85.0(5) . .
C25 Ni1 C13 C14 142.7(7) . .
C28 Ni1 C13 C14 12.5(4) . .
Ni2 Ni1 C13 C14 142.1(4) . .
C12 Ni1 C13 Ni2 73.95(19) . .
C27 Ni1 C13 Ni2 -177.20(14) . .
C29 Ni1 C13 Ni2 -82.1(2) . .
C26 Ni1 C13 Ni2 132.9(3) . .
C25 Ni1 C13 Ni2 0.6(8) . .
C28 Ni1 C13 Ni2 -129.62(13) . .
C12 C13 C14 C19 -23.6(7) . .
Ni2 C13 C14 C19 -150.5(3) . .
Ni1 C13 C14 C19 91.1(4) . .
C12 C13 C14 C15 157.6(5) . .
Ni2 C13 C14 C15 30.7(6) . .
Ni1 C13 C14 C15 -87.7(4) . .
C19 C14 C15 C16 0.0(5) . .
C13 C14 C15 C16 178.8(3) . .
C14 C15 C16 C17 -1.0(6) . .
C15 C16 C17 C18 1.2(6) . .
C16 C17 C18 C19 -0.5(6) . .
C17 C18 C19 C14 -0.5(5) . .
C15 C14 C19 C18 0.7(5) . .
C13 C14 C19 C18 -178.0(3) . .
C13 Ni2 C20 C24 -115.7(2) . .
C12 Ni2 C20 C24 -165.5(3) . .
C23 Ni2 C20 C24 37.8(2) . .
C21 Ni2 C20 C24 118.6(3) . .
C22 Ni2 C20 C24 80.9(3) . .
Ni1 Ni2 C20 C24 -44.9(4) . .
C13 Ni2 C20 C21 125.7(2) . .
C12 Ni2 C20 C21 75.9(3) . .
C23 Ni2 C20 C21 -80.8(2) . .
C24 Ni2 C20 C21 -118.6(3) . .
C22 Ni2 C20 C21 -37.7(2) . .
Ni1 Ni2 C20 C21 -163.5(2) . .
C24 C20 C21 C22 1.4(4) . .
Ni2 C20 C21 C22 61.8(3) . .
C24 C20 C21 Ni2 -60.4(3) . .
C13 Ni2 C21 C22 155.3(2) . .
C12 Ni2 C21 C22 103.7(3) . .
C23 Ni2 C21 C22 -37.5(2) . .
C24 Ni2 C21 C22 -80.7(2) . .
C20 Ni2 C21 C22 -118.0(3) . .
Ni1 Ni2 C21 C22 34.0(5) . .
C13 Ni2 C21 C20 -86.7(3) . .
C12 Ni2 C21 C20 -138.4(2) . .
C23 Ni2 C21 C20 80.4(2) . .
C24 Ni2 C21 C20 37.3(2) . .
C22 Ni2 C21 C20 118.0(3) . .
Ni1 Ni2 C21 C20 152.0(3) . .
C20 C21 C22 C23 -1.9(4) . .
Ni2 C21 C22 C23 59.5(3) . .
C20 C21 C22 Ni2 -61.4(2) . .
C13 Ni2 C22 C23 156.5(5) . .
C12 Ni2 C22 C23 138.6(2) . .
C21 Ni2 C22 C23 -118.3(3) . .
C24 Ni2 C22 C23 -37.5(2) . .
C20 Ni2 C22 C23 -80.4(2) . .
Ni1 Ni2 C22 C23 72.6(2) . .
C13 Ni2 C22 C21 -85.2(6) . .
C12 Ni2 C22 C21 -103.1(3) . .
C23 Ni2 C22 C21 118.3(3) . .
C24 Ni2 C22 C21 80.8(2) . .
C20 Ni2 C22 C21 37.9(2) . .
Ni1 Ni2 C22 C21 -169.06(18) . .
C21 C22 C23 C24 1.7(4) . .
Ni2 C22 C23 C24 61.2(3) . .
C21 C22 C23 Ni2 -59.6(3) . .
C13 Ni2 C23 C22 -164.0(3) . .
C12 Ni2 C23 C22 -75.5(3) . .
C21 Ni2 C23 C22 37.6(2) . .
C24 Ni2 C23 C22 118.6(3) . .
C20 Ni2 C23 C22 81.1(2) . .
Ni1 Ni2 C23 C22 -126.7(2) . .
C13 Ni2 C23 C24 77.4(4) . .
C12 Ni2 C23 C24 165.9(3) . .
C21 Ni2 C23 C24 -81.0(3) . .
C20 Ni2 C23 C24 -37.5(2) . .
C22 Ni2 C23 C24 -118.6(3) . .
Ni1 Ni2 C23 C24 114.7(2) . .
C21 C20 C24 C23 -0.4(4) . .
Ni2 C20 C24 C23 -60.5(3) . .
C21 C20 C24 Ni2 60.1(3) . .
C22 C23 C24 C20 -0.8(4) . .
Ni2 C23 C24 C20 60.9(3) . .
C22 C23 C24 Ni2 -61.7(3) . .
C13 Ni2 C24 C20 94.0(3) . .
C23 Ni2 C24 C20 -118.1(3) . .
C21 Ni2 C24 C20 -37.7(2) . .
C22 Ni2 C24 C20 -80.8(3) . .
Ni1 Ni2 C24 C20 158.73(19) . .
C13 Ni2 C24 C23 -147.9(2) . .
C21 Ni2 C24 C23 80.5(3) . .
C20 Ni2 C24 C23 118.1(3) . .
C22 Ni2 C24 C23 37.4(2) . .
Ni1 Ni2 C24 C23 -83.1(2) . .
C13 Ni1 C25 C26 144.2(7) . .
C12 Ni1 C25 C26 82.8(3) . .
C27 Ni1 C25 C26 -37.7(2) . .
C29 Ni1 C25 C26 -118.1(3) . .
C28 Ni1 C25 C26 -80.6(2) . .
Ni2 Ni1 C25 C26 144.7(2) . .
C13 Ni1 C25 C29 -97.7(8) . .
C12 Ni1 C25 C29 -159.1(2) . .
C27 Ni1 C25 C29 80.4(2) . .
C26 Ni1 C25 C29 118.1(3) . .
C28 Ni1 C25 C29 37.5(2) . .
Ni2 Ni1 C25 C29 -97.2(2) . .
C29 C25 C26 C27 -0.8(4) . .
Ni1 C25 C26 C27 60.0(3) . .
C29 C25 C26 Ni1 -60.8(3) . .
C13 Ni1 C26 C25 -165.7(3) . .
C12 Ni1 C26 C25 -125.6(2) . .
C27 Ni1 C26 C25 118.4(3) . .
C29 Ni1 C26 C25 37.8(2) . .
C28 Ni1 C26 C25 80.6(2) . .
Ni2 Ni1 C26 C25 -59.9(3) . .
C13 Ni1 C26 C27 75.9(4) . .
C12 Ni1 C26 C27 115.9(2) . .
C29 Ni1 C26 C27 -80.7(2) . .
C25 Ni1 C26 C27 -118.4(3) . .
C28 Ni1 C26 C27 -37.9(2) . .
Ni2 Ni1 C26 C27 -178.33(17) . .
C25 C26 C27 C28 2.0(4) . .
Ni1 C26 C27 C28 62.7(3) . .
C25 C26 C27 Ni1 -60.8(3) . .
C13 Ni1 C27 C28 99.3(2) . .
C12 Ni1 C27 C28 151.5(2) . .
C29 Ni1 C27 C28 -37.0(2) . .
C26 Ni1 C27 C28 -117.3(3) . .
C25 Ni1 C27 C28 -80.2(2) . .
C13 Ni1 C27 C26 -143.4(3) . .
C12 Ni1 C27 C26 -91.2(3) . .
C29 Ni1 C27 C26 80.3(3) . .
C25 Ni1 C27 C26 37.1(2) . .
C28 Ni1 C27 C26 117.3(3) . .
C26 C27 C28 C29 -2.4(4) . .
Ni1 C27 C28 C29 59.9(3) . .
C26 C27 C28 Ni1 -62.3(3) . .
C13 Ni1 C28 C27 -109.1(2) . .
C12 Ni1 C28 C27 -68.5(4) . .
C29 Ni1 C28 C27 118.9(3) . .
C26 Ni1 C28 C27 38.3(2) . .
C25 Ni1 C28 C27 81.0(3) . .
Ni2 Ni1 C28 C27 -177.50(18) . .
C13 Ni1 C28 C29 132.0(2) . .
C12 Ni1 C28 C29 172.6(3) . .
C27 Ni1 C28 C29 -118.9(3) . .
C26 Ni1 C28 C29 -80.6(3) . .
C25 Ni1 C28 C29 -37.8(2) . .
Ni2 Ni1 C28 C29 63.6(3) . .
C27 C28 C29 C25 1.9(4) . .
Ni1 C28 C29 C25 61.3(3) . .
C27 C28 C29 Ni1 -59.4(3) . .
C26 C25 C29 C28 -0.7(4) . .
Ni1 C25 C29 C28 -61.7(3) . .
C26 C25 C29 Ni1 61.0(3) . .
C13 Ni1 C29 C28 -81.2(3) . .
C12 Ni1 C29 C28 -168.7(5) . .
C27 Ni1 C29 C28 37.2(2) . .
C26 Ni1 C29 C28 80.6(3) . .
C25 Ni1 C29 C28 118.0(3) . .
Ni2 Ni1 C29 C28 -140.1(2) . .
C13 Ni1 C29 C25 160.8(3) . .
C12 Ni1 C29 C25 73.3(6) . .
C27 Ni1 C29 C25 -80.8(3) . .
C26 Ni1 C29 C25 -37.4(2) . .
C28 Ni1 C29 C25 -118.0(3) . .
Ni2 Ni1 C29 C25 101.9(2) . .
C41 Ni3 Ni4 C42 -52.07(18) . .
C50 Ni3 Ni4 C42 -126.7(5) . .
C52 Ni3 Ni4 C42 161.82(19) . .
C49 Ni3 Ni4 C42 84.0(3) . .
C53 Ni3 Ni4 C42 119.06(19) . .
C51 Ni3 Ni4 C42 -158.7(2) . .
C42 Ni3 Ni4 C41 52.07(18) . .
C50 Ni3 Ni4 C41 -74.7(5) . .
C52 Ni3 Ni4 C41 -146.11(19) . .
C49 Ni3 Ni4 C41 136.1(3) . .
C53 Ni3 Ni4 C41 171.13(19) . .
C51 Ni3 Ni4 C41 -106.7(2) . .
C42 Ni3 Ni4 C58 -176.3(2) . .
C41 Ni3 Ni4 C58 131.6(2) . .
C50 Ni3 Ni4 C58 57.0(5) . .
C52 Ni3 Ni4 C58 -14.5(2) . .
C49 Ni3 Ni4 C58 -92.3(3) . .
C53 Ni3 Ni4 C58 -57.2(2) . .
C51 Ni3 Ni4 C58 25.0(2) . .
C42 Ni3 Ni4 C57 -133.1(2) . .
C41 Ni3 Ni4 C57 174.9(2) . .
C50 Ni3 Ni4 C57 100.2(5) . .
C52 Ni3 Ni4 C57 28.8(2) . .
C49 Ni3 Ni4 C57 -49.0(3) . .
C53 Ni3 Ni4 C57 -14.0(2) . .
C51 Ni3 Ni4 C57 68.2(2) . .
C42 Ni3 Ni4 C54 146.1(2) . .
C41 Ni3 Ni4 C54 94.0(2) . .
C50 Ni3 Ni4 C54 19.4(5) . .
C52 Ni3 Ni4 C54 -52.1(2) . .
C49 Ni3 Ni4 C54 -129.8(3) . .
C53 Ni3 Ni4 C54 -94.8(2) . .
C51 Ni3 Ni4 C54 -12.6(3) . .
C42 Ni3 Ni4 C56 -97.0(2) . .
C41 Ni3 Ni4 C56 -149.1(3) . .
C50 Ni3 Ni4 C56 136.2(5) . .
C52 Ni3 Ni4 C56 64.8(2) . .
C49 Ni3 Ni4 C56 -13.0(3) . .
C53 Ni3 Ni4 C56 22.0(2) . .
C51 Ni3 Ni4 C56 104.2(3) . .
C31 Cr2 C33 C34 -25.9(4) . .
C30 Cr2 C33 C34 162.0(3) . .
C32 Cr2 C33 C34 -112.7(3) . .
C37 Cr2 C33 C34 102.4(3) . .
C35 Cr2 C33 C34 29.0(2) . .
C36 Cr2 C33 C34 65.7(2) . .
C38 Cr2 C33 C34 133.0(3) . .
C31 Cr2 C33 C38 -158.9(3) . .
C30 Cr2 C33 C38 29.0(4) . .
C32 Cr2 C33 C38 114.4(3) . .
C37 Cr2 C33 C38 -30.5(2) . .
C35 Cr2 C33 C38 -104.0(2) . .
C36 Cr2 C33 C38 -67.2(2) . .
C34 Cr2 C33 C38 -133.0(3) . .
C38 C33 C34 C35 1.9(6) . .
Cr2 C33 C34 C35 -53.3(4) . .
C38 C33 C34 Cr2 55.3(3) . .
C31 Cr2 C34 C33 162.4(2) . .
C30 Cr2 C34 C33 -61.5(9) . .
C32 Cr2 C34 C33 70.3(3) . .
C37 Cr2 C34 C33 -66.2(2) . .
C35 Cr2 C34 C33 -132.2(3) . .
C36 Cr2 C34 C33 -103.1(2) . .
C38 Cr2 C34 C33 -28.9(2) . .
C31 Cr2 C34 C35 -65.4(3) . .
C30 Cr2 C34 C35 70.7(9) . .
C32 Cr2 C34 C35 -157.5(2) . .
C37 Cr2 C34 C35 66.0(2) . .
C33 Cr2 C34 C35 132.2(3) . .
C36 Cr2 C34 C35 29.1(2) . .
C38 Cr2 C34 C35 103.3(2) . .
C33 C34 C35 C36 -1.9(6) . .
Cr2 C34 C35 C36 -54.9(4) . .
C33 C34 C35 Cr2 53.0(4) . .
C31 Cr2 C35 C34 117.4(3) . .
C30 Cr2 C35 C34 -159.9(3) . .
C32 Cr2 C35 C34 31.9(3) . .
C37 Cr2 C35 C34 -102.7(2) . .
C33 Cr2 C35 C34 -29.0(2) . .
C36 Cr2 C35 C34 -132.2(3) . .
C38 Cr2 C35 C34 -66.1(2) . .
C31 Cr2 C35 C36 -110.5(3) . .
C30 Cr2 C35 C36 -27.7(4) . .
C32 Cr2 C35 C36 164.0(2) . .
C37 Cr2 C35 C36 29.5(2) . .
C33 Cr2 C35 C36 103.1(2) . .
C38 Cr2 C35 C36 66.1(2) . .
C34 Cr2 C35 C36 132.2(3) . .
C34 C35 C36 C37 1.2(6) . .
Cr2 C35 C36 C37 -53.9(3) . .
C34 C35 C36 Cr2 55.1(4) . .
C31 Cr2 C36 C37 -157.3(3) . .
C30 Cr2 C36 C37 -67.8(3) . .
C32 Cr2 C36 C37 72.7(8) . .
C33 Cr2 C36 C37 65.8(2) . .
C35 Cr2 C36 C37 131.4(4) . .
C38 Cr2 C36 C37 28.2(2) . .
C34 Cr2 C36 C37 102.4(3) . .
C31 Cr2 C36 C35 71.3(3) . .
C30 Cr2 C36 C35 160.8(3) . .
C32 Cr2 C36 C35 -58.7(8) . .
C37 Cr2 C36 C35 -131.4(4) . .
C33 Cr2 C36 C35 -65.6(2) . .
C38 Cr2 C36 C35 -103.2(3) . .
C34 Cr2 C36 C35 -29.0(2) . .
C35 C36 C37 C38 -0.6(6) . .
Cr2 C36 C37 C38 -54.7(3) . .
C35 C36 C37 Cr2 54.2(3) . .
C31 Cr2 C37 C36 31.1(4) . .
C30 Cr2 C37 C36 115.0(3) . .
C32 Cr2 C37 C36 -161.2(3) . .
C33 Cr2 C37 C36 -103.0(3) . .
C35 Cr2 C37 C36 -29.5(2) . .
C38 Cr2 C37 C36 -133.9(3) . .
C34 Cr2 C37 C36 -66.2(2) . .
C31 Cr2 C37 C38 164.9(3) . .
C30 Cr2 C37 C38 -111.2(3) . .
C32 Cr2 C37 C38 -27.3(4) . .
C33 Cr2 C37 C38 30.8(2) . .
C35 Cr2 C37 C38 104.3(3) . .
C36 Cr2 C37 C38 133.9(3) . .
C34 Cr2 C37 C38 67.6(2) . .
C36 C37 C38 C33 0.6(5) . .
Cr2 C37 C38 C33 -54.1(3) . .
C36 C37 C38 Si2 -179.4(3) . .
Cr2 C37 C38 Si2 126.0(3) . .
C36 C37 C38 Cr2 54.7(3) . .
C34 C33 C38 C37 -1.3(5) . .
Cr2 C33 C38 C37 54.2(3) . .
C34 C33 C38 Si2 178.7(3) . .
Cr2 C33 C38 Si2 -125.9(3) . .
C34 C33 C38 Cr2 -55.5(3) . .
C41 Si2 C38 C37 84.6(3) . .
C40 Si2 C38 C37 -34.1(4) . .
C39 Si2 C38 C37 -157.6(3) . .
C41 Si2 C38 C33 -95.3(3) . .
C40 Si2 C38 C33 146.0(3) . .
C39 Si2 C38 C33 22.5(4) . .
C41 Si2 C38 Cr2 174.5(2) . .
C40 Si2 C38 Cr2 55.8(3) . .
C39 Si2 C38 Cr2 -67.7(3) . .
C31 Cr2 C38 C37 -50.6(8) . .
C30 Cr2 C38 C37 71.0(3) . .
C32 Cr2 C38 C37 161.4(3) . .
C33 Cr2 C38 C37 -129.6(3) . .
C35 Cr2 C38 C37 -64.7(2) . .
C36 Cr2 C38 C37 -28.0(2) . .
C34 Cr2 C38 C37 -101.1(3) . .
C31 Cr2 C38 C33 79.0(8) . .
C30 Cr2 C38 C33 -159.4(3) . .
C32 Cr2 C38 C33 -69.0(3) . .
C37 Cr2 C38 C33 129.6(3) . .
C35 Cr2 C38 C33 64.9(2) . .
C36 Cr2 C38 C33 101.5(2) . .
C34 Cr2 C38 C33 28.4(2) . .
C31 Cr2 C38 Si2 -165.5(7) . .
C30 Cr2 C38 Si2 -43.9(3) . .
C32 Cr2 C38 Si2 46.6(3) . .
C37 Cr2 C38 Si2 -114.8(3) . .
C33 Cr2 C38 Si2 115.6(3) . .
C35 Cr2 C38 Si2 -179.5(3) . .
C36 Cr2 C38 Si2 -142.9(3) . .
C34 Cr2 C38 Si2 144.0(3) . .
C40 Si2 C41 C42 -178.7(6) . .
C39 Si2 C41 C42 -56.2(7) . .
C38 Si2 C41 C42 62.3(6) . .
C40 Si2 C41 Ni4 -50.2(3) . .
C39 Si2 C41 Ni4 72.2(3) . .
C38 Si2 C41 Ni4 -169.3(2) . .
C40 Si2 C41 Ni3 53.4(3) . .
C39 Si2 C41 Ni3 175.9(2) . .
C38 Si2 C41 Ni3 -65.7(3) . .
C55 Ni4 C41 C42 104.9(3) . .
C58 Ni4 C41 C42 -159.5(2) . .
C57 Ni4 C41 C42 -92.9(8) . .
C54 Ni4 C41 C42 152.6(2) . .
C56 Ni4 C41 C42 55.6(5) . .
Ni3 Ni4 C41 C42 -72.6(2) . .
C42 Ni4 C41 Si2 -158.0(4) . .
C55 Ni4 C41 Si2 -53.2(3) . .
C58 Ni4 C41 Si2 42.5(4) . .
C57 Ni4 C41 Si2 109.1(7) . .
C54 Ni4 C41 Si2 -5.5(3) . .
C56 Ni4 C41 Si2 -102.5(4) . .
Ni3 Ni4 C41 Si2 129.4(3) . .
C42 Ni4 C41 Ni3 72.6(2) . .
C55 Ni4 C41 Ni3 177.44(17) . .
C58 Ni4 C41 Ni3 -86.9(2) . .
C57 Ni4 C41 Ni3 -20.3(8) . .
C54 Ni4 C41 Ni3 -134.86(17) . .
C56 Ni4 C41 Ni3 128.2(4) . .
C50 Ni3 C41 C42 -121.2(2) . .
C52 Ni3 C41 C42 144.1(3) . .
C49 Ni3 C41 C42 -72.8(3) . .
C53 Ni3 C41 C42 25.2(9) . .
C51 Ni3 C41 C42 -168.4(2) . .
Ni4 Ni3 C41 C42 73.36(19) . .
C42 Ni3 C41 Si2 157.8(4) . .
C50 Ni3 C41 Si2 36.6(3) . .
C52 Ni3 C41 Si2 -58.1(4) . .
C49 Ni3 C41 Si2 85.0(3) . .
C53 Ni3 C41 Si2 -177.0(7) . .
C51 Ni3 C41 Si2 -10.7(3) . .
Ni4 Ni3 C41 Si2 -128.9(3) . .
C42 Ni3 C41 Ni4 -73.36(19) . .
C50 Ni3 C41 Ni4 165.43(13) . .
C52 Ni3 C41 Ni4 70.7(3) . .
C49 Ni3 C41 Ni4 -146.11(19) . .
C53 Ni3 C41 Ni4 -48.2(9) . .
C51 Ni3 C41 Ni4 118.21(15) . .
Si2 C41 C42 C43 2.3(11) . .
Ni4 C41 C42 C43 -137.4(6) . .
Ni3 C41 C42 C43 141.9(6) . .
Si2 C41 C42 Ni3 -139.6(6) . .
Ni4 C41 C42 Ni3 80.72(10) . .
Si2 C41 C42 Ni4 139.7(6) . .
Ni3 C41 C42 Ni4 -80.72(10) . .
C50 Ni3 C42 C41 92.3(3) . .
C52 Ni3 C42 C41 -122.8(4) . .
C49 Ni3 C42 C41 139.4(2) . .
C53 Ni3 C42 C41 -174.3(2) . .
C51 Ni3 C42 C41 34.8(6) . .
Ni4 Ni3 C42 C41 -73.6(2) . .
C41 Ni3 C42 C43 -151.4(4) . .
C50 Ni3 C42 C43 -59.1(4) . .
C52 Ni3 C42 C43 85.8(5) . .
C49 Ni3 C42 C43 -12.0(4) . .
C53 Ni3 C42 C43 34.3(4) . .
C51 Ni3 C42 C43 -116.6(5) . .
Ni4 Ni3 C42 C43 135.0(4) . .
C41 Ni3 C42 Ni4 73.6(2) . .
C50 Ni3 C42 Ni4 165.86(15) . .
C52 Ni3 C42 Ni4 -49.2(4) . .
C49 Ni3 C42 Ni4 -147.00(12) . .
C53 Ni3 C42 Ni4 -100.76(17) . .
C51 Ni3 C42 Ni4 108.4(5) . .
C55 Ni4 C42 C41 -109.4(3) . .
C58 Ni4 C42 C41 88.7(8) . .
C57 Ni4 C42 C41 159.5(3) . .
C54 Ni4 C42 C41 -58.5(4) . .
C56 Ni4 C42 C41 -155.5(2) . .
Ni3 Ni4 C42 C41 74.4(2) . .
C41 Ni4 C42 C43 149.2(4) . .
C55 Ni4 C42 C43 39.8(4) . .
C58 Ni4 C42 C43 -122.1(7) . .
C57 Ni4 C42 C43 -51.4(4) . .
C54 Ni4 C42 C43 90.7(5) . .
C56 Ni4 C42 C43 -6.3(4) . .
Ni3 Ni4 C42 C43 -136.4(4) . .
C41 Ni4 C42 Ni3 -74.4(2) . .
C55 Ni4 C42 Ni3 176.20(18) . .
C58 Ni4 C42 Ni3 14.2(8) . .
C57 Ni4 C42 Ni3 85.0(2) . .
C54 Ni4 C42 Ni3 -132.9(3) . .
C56 Ni4 C42 Ni3 130.08(18) . .
C41 C42 C43 C44 -174.8(5) . .
Ni3 C42 C43 C44 -48.4(5) . .
Ni4 C42 C43 C44 64.4(5) . .
C41 C42 C43 C48 6.7(7) . .
Ni3 C42 C43 C48 133.0(3) . .
Ni4 C42 C43 C48 -114.2(4) . .
C48 C43 C44 C45 0.5(5) . .
C42 C43 C44 C45 -178.1(3) . .
C43 C44 C45 C46 0.0(6) . .
C44 C45 C46 C47 0.0(6) . .
C45 C46 C47 C48 -0.5(6) . .
C46 C47 C48 C43 1.0(5) . .
C44 C43 C48 C47 -1.0(5) . .
C42 C43 C48 C47 177.6(3) . .
C42 Ni3 C49 C53 117.6(2) . .
C41 Ni3 C49 C53 163.6(3) . .
C50 Ni3 C49 C53 -117.7(3) . .
C52 Ni3 C49 C53 -37.7(2) . .
C51 Ni3 C49 C53 -80.2(2) . .
Ni4 Ni3 C49 C53 52.3(3) . .
C42 Ni3 C49 C50 -124.7(2) . .
C41 Ni3 C49 C50 -78.8(3) . .
C52 Ni3 C49 C50 80.0(2) . .
C53 Ni3 C49 C50 117.7(3) . .
C51 Ni3 C49 C50 37.5(2) . .
Ni4 Ni3 C49 C50 169.93(18) . .
C53 C49 C50 C51 -1.3(4) . .
Ni3 C49 C50 C51 -62.3(2) . .
C53 C49 C50 Ni3 61.0(2) . .
C42 Ni3 C50 C51 -157.1(2) . .
C41 Ni3 C50 C51 -105.9(3) . .
C52 Ni3 C50 C51 36.9(2) . .
C49 Ni3 C50 C51 117.9(3) . .
C53 Ni3 C50 C51 80.3(2) . .
Ni4 Ni3 C50 C51 -39.7(6) . .
C42 Ni3 C50 C49 84.9(3) . .
C41 Ni3 C50 C49 136.2(2) . .
C52 Ni3 C50 C49 -81.0(2) . .
C53 Ni3 C50 C49 -37.6(2) . .
C51 Ni3 C50 C49 -117.9(3) . .
Ni4 Ni3 C50 C49 -157.6(4) . .
C49 C50 C51 C52 2.0(4) . .
Ni3 C50 C51 C52 -59.8(3) . .
C49 C50 C51 Ni3 61.7(2) . .
C42 Ni3 C51 C52 -166.4(5) . .
C41 Ni3 C51 C52 -139.4(2) . .
C50 Ni3 C51 C52 119.0(3) . .
C49 Ni3 C51 C52 80.8(2) . .
C53 Ni3 C51 C52 37.9(2) . .
Ni4 Ni3 C51 C52 -71.6(3) . .
C42 Ni3 C51 C50 74.5(6) . .
C41 Ni3 C51 C50 101.5(3) . .
C52 Ni3 C51 C50 -119.0(3) . .
C49 Ni3 C51 C50 -38.3(2) . .
C53 Ni3 C51 C50 -81.1(2) . .
Ni4 Ni3 C51 C50 169.36(18) . .
C50 C51 C52 C53 -1.9(4) . .
Ni3 C51 C52 C53 -61.2(3) . .
C50 C51 C52 Ni3 59.3(3) . .
C42 Ni3 C52 C51 169.8(4) . .
C41 Ni3 C52 C51 76.1(3) . .
C50 Ni3 C52 C51 -37.1(2) . .
C49 Ni3 C52 C51 -81.0(2) . .
C53 Ni3 C52 C51 -118.2(3) . .
Ni4 Ni3 C52 C51 129.7(2) . .
C42 Ni3 C52 C53 -71.9(5) . .
C41 Ni3 C52 C53 -165.7(3) . .
C50 Ni3 C52 C53 81.1(2) . .
C49 Ni3 C52 C53 37.2(2) . .
C51 Ni3 C52 C53 118.2(3) . .
Ni4 Ni3 C52 C53 -112.1(2) . .
C50 C49 C53 C52 0.1(4) . .
Ni3 C49 C53 C52 60.2(3) . .
C50 C49 C53 Ni3 -60.1(2) . .
C51 C52 C53 C49 1.1(4) . .
Ni3 C52 C53 C49 -60.5(2) . .
C51 C52 C53 Ni3 61.6(3) . .
C42 Ni3 C53 C49 -89.8(3) . .
C41 Ni3 C53 C49 -111.0(8) . .
C50 Ni3 C53 C49 38.4(2) . .
C52 Ni3 C53 C49 118.5(3) . .
C51 Ni3 C53 C49 81.3(2) . .
Ni4 Ni3 C53 C49 -154.21(18) . .
C42 Ni3 C53 C52 151.7(2) . .
C41 Ni3 C53 C52 130.5(8) . .
C50 Ni3 C53 C52 -80.1(2) . .
C49 Ni3 C53 C52 -118.5(3) . .
C51 Ni3 C53 C52 -37.2(2) . .
Ni4 Ni3 C53 C52 87.2(2) . .
C42 Ni4 C54 C55 -75.4(4) . .
C41 Ni4 C54 C55 -115.8(3) . .
C58 Ni4 C54 C55 116.3(4) . .
C57 Ni4 C54 C55 77.8(3) . .
C56 Ni4 C54 C55 36.3(3) . .
Ni3 Ni4 C54 C55 176.2(2) . .
C42 Ni4 C54 C58 168.3(3) . .
C41 Ni4 C54 C58 127.9(3) . .
C55 Ni4 C54 C58 -116.3(4) . .
C57 Ni4 C54 C58 -38.5(3) . .
C56 Ni4 C54 C58 -80.0(3) . .
Ni3 Ni4 C54 C58 59.9(3) . .
C58 C54 C55 C56 -1.6(4) . .
Ni4 C54 C55 C56 -62.2(3) . .
C58 C54 C55 Ni4 60.6(3) . .
C42 Ni4 C55 C56 -95.4(3) . .
C41 Ni4 C55 C56 -148.2(3) . .
C58 Ni4 C55 C56 80.0(3) . .
C57 Ni4 C55 C56 36.4(3) . .
C54 Ni4 C55 C56 119.1(4) . .
C42 Ni4 C55 C54 145.5(2) . .
C41 Ni4 C55 C54 92.7(3) . .
C58 Ni4 C55 C54 -39.2(3) . .
C57 Ni4 C55 C54 -82.8(3) . .
C56 Ni4 C55 C54 -119.1(4) . .
C54 C55 C56 C57 1.5(5) . .
Ni4 C55 C56 C57 -60.0(3) . .
C54 C55 C56 Ni4 61.5(3) . .
C42 Ni4 C56 C57 -129.0(3) . .
C41 Ni4 C56 C57 -168.3(4) . .
C55 Ni4 C56 C57 119.2(4) . .
C58 Ni4 C56 C57 37.3(3) . .
C54 Ni4 C56 C57 81.5(3) . .
Ni3 Ni4 C56 C57 -61.6(4) . .
C42 Ni4 C56 C55 111.8(3) . .
C41 Ni4 C56 C55 72.4(5) . .
C58 Ni4 C56 C55 -82.0(3) . .
C57 Ni4 C56 C55 -119.2(4) . .
C54 Ni4 C56 C55 -37.7(3) . .
Ni3 Ni4 C56 C55 179.1(2) . .
C55 C56 C57 C58 -0.7(5) . .
Ni4 C56 C57 C58 -60.3(3) . .
C55 C56 C57 Ni4 59.6(3) . .
C42 Ni4 C57 C56 81.0(4) . .
C41 Ni4 C57 C56 158.4(7) . .
C55 Ni4 C57 C56 -36.8(3) . .
C58 Ni4 C57 C56 -119.8(4) . .
C54 Ni4 C57 C56 -80.7(3) . .
Ni3 Ni4 C57 C56 140.8(3) . .
C42 Ni4 C57 C58 -159.1(2) . .
C41 Ni4 C57 C58 -81.7(8) . .
C55 Ni4 C57 C58 83.0(3) . .
C54 Ni4 C57 C58 39.2(3) . .
C56 Ni4 C57 C58 119.8(4) . .
Ni3 Ni4 C57 C58 -99.4(2) . .
C56 C57 C58 C54 -0.3(4) . .
Ni4 C57 C58 C54 -61.6(3) . .
C56 C57 C58 Ni4 61.4(3) . .
C55 C54 C58 C57 1.1(4) . .
Ni4 C54 C58 C57 61.6(3) . .
C55 C54 C58 Ni4 -60.4(3) . .
C42 Ni4 C58 C57 86.7(7) . .
C41 Ni4 C58 C57 160.1(3) . .
C55 Ni4 C58 C57 -77.7(3) . .
C54 Ni4 C58 C57 -116.4(4) . .
C56 Ni4 C58 C57 -35.7(3) . .
Ni3 Ni4 C58 C57 99.0(2) . .
C42 Ni4 C58 C54 -156.9(6) . .
C41 Ni4 C58 C54 -83.5(3) . .
C55 Ni4 C58 C54 38.8(3) . .
C57 Ni4 C58 C54 116.4(4) . .
C56 Ni4 C58 C54 80.7(3) . .
Ni3 Ni4 C58 C54 -144.6(2) . .
C64 C60 C61 C62 -3.7(9) 2_767 .
C60 C61 C62 C63 3.2(9) . .
C61 C62 C63 C64 -2.8(8) . .
C62 C63 C64 C64 3.4(10) . 2_767
C62 C63 C64 C60 179.5(5) . 2_767
