#------------------------------------------------------------------------------
#$Date: 2016-03-21 13:50:05 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178703 $
#$URL: svn://www.crystallography.net/cod/cif/4/08/14/4081454.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4081454
loop_
_publ_author_name
'Ciabatti, Iacopo'
'Femoni, Cristina'
'Iapalucci, Maria Carmela'
'Longoni, Giuliano'
'Zacchini, Stefano'
_publ_section_title
;
 Tetrahedral [HnPt4(CO)4(P∧P)2]n+(n= 1, 2; P∧P =
 CH2═C(PPh2)2) Cationic Mono- and Dihydrido Carbonyl Clusters
 Obtained by Protonation of the Neutral Pt4(CO)4(P∧P)2
;
_journal_issue                   18
_journal_name_full               Organometallics
_journal_page_first              5180
_journal_paper_doi               10.1021/om400723w
_journal_volume                  32
_journal_year                    2013
_chemical_formula_sum            'C84 H60 O20 P4 Pt10'
_chemical_formula_weight         3464.10
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                110.466(8)
_cell_angle_beta                 112.289(7)
_cell_angle_gamma                97.834(6)
_cell_formula_units_Z            2
_cell_length_a                   17.102(7)
_cell_length_b                   17.132(7)
_cell_length_c                   18.094(12)
_cell_measurement_reflns_used    2313
_cell_measurement_temperature    293(2)
_cell_measurement_theta_max      21.836
_cell_measurement_theta_min      2.3505
_cell_volume                     4369(4)
_computing_cell_refinement       'APEX2 (Bruker AXS, 2006)'
_computing_data_collection       'APEX2 (Bruker AXS, 2006)'
_computing_data_reduction        'SAINT (Bruker AXS, 2004)'
_computing_molecular_graphics    'SCHAKAL99 (Keller, 1999)'
_computing_publication_material  'XCIF (Bruker AXS, 2001)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.959
_diffrn_measured_fraction_theta_max 0.959
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0666
_diffrn_reflns_av_sigmaI/netI    0.1267
_diffrn_reflns_limit_h_max       17
_diffrn_reflns_limit_h_min       -17
_diffrn_reflns_limit_k_max       17
_diffrn_reflns_limit_k_min       -17
_diffrn_reflns_limit_l_max       16
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            15784
_diffrn_reflns_theta_full        21.97
_diffrn_reflns_theta_max         21.97
_diffrn_reflns_theta_min         1.35
_exptl_absorpt_coefficient_mu    16.081
_exptl_absorpt_correction_T_max  0.2962
_exptl_absorpt_correction_T_min  0.1829
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details
;
 Data were corrected for Lorentz polarization and absorption
 effects (empirical absorption corrections SADABS).
 R(int) = 0.1451 (selected reflections only, before parameter refinement)
 R(int) = 0.0517 (selected reflections only, after parameter refinement)
;
_exptl_crystal_colour            red
_exptl_crystal_density_diffrn    2.633
_exptl_crystal_density_method    'not measured'
_exptl_crystal_description       plate
_exptl_crystal_F_000             3128
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.13
_exptl_crystal_size_min          0.10
_refine_diff_density_max         2.807
_refine_diff_density_min         -2.550
_refine_diff_density_rms         0.370
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.981
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     906
_refine_ls_number_reflns         10216
_refine_ls_number_restraints     822
_refine_ls_restrained_S_all      0.949
_refine_ls_R_factor_all          0.1254
_refine_ls_R_factor_gt           0.0720
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.1350P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1829
_refine_ls_wR_factor_ref         0.2360
_reflns_number_gt                6104
_reflns_number_total             10216
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            om400723w_si_001.cif
_cod_data_source_block           p-1_cif7
_cod_depositor_comments
;
The following automatic conversions were performed:

'_symmetry_cell_setting' value 'Triclinic' changed to 'triclinic'
according to /home/saulius/struct/CIF-dictionaries/cif_core.dic
dictionary named 'cif_core.dic' version 2.4.2 from 2011-04-26.

Automatic conversion script
Id: cif_fix_values 1891 2012-01-12 08:04:46Z andrius 
;
_cod_original_sg_symbol_H-M      P-1
_cod_database_code               4081454
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pt1 Pt 0.35242(10) 0.10548(10) 0.41387(9) 0.0579(5) Uani 1 1 d .
Pt2 Pt 0.39430(10) 0.25909(10) 0.41122(9) 0.0631(5) Uani 1 1 d .
Pt3 Pt 0.23547(10) 0.14271(10) 0.29408(9) 0.0602(5) Uani 1 1 d .
Pt4 Pt 0.24011(9) 0.14881(9) 0.51133(9) 0.0510(4) Uani 1 1 d .
Pt5 Pt 0.34064(9) 0.30799(9) 0.56106(8) 0.0492(4) Uani 1 1 d .
Pt6 Pt 0.17791(9) 0.24308(9) 0.42680(8) 0.0541(4) Uani 1 1 d .
Pt7 Pt 0.13153(10) 0.34993(10) 0.56790(9) 0.0597(5) Uani 1 1 d .
Pt8 Pt 0.27808(10) 0.36399(10) 0.70239(9) 0.0620(5) Uani 1 1 d .
Pt9 Pt 0.14064(10) 0.22002(10) 0.61489(10) 0.0615(5) Uani 1 1 d .
C1 C 0.241(3) 0.025(3) 0.302(3) 0.071(9) Uani 1 1 d U
C2 C 0.380(3) 0.021(3) 0.452(3) 0.087(10) Uani 1 1 d U
C3 C 0.468(3) 0.204(3) 0.474(3) 0.075(9) Uani 1 1 d U
C4 C 0.294(3) 0.266(3) 0.309(3) 0.082(10) Uani 1 1 d U
C5 C 0.367(2) 0.223(2) 0.613(2) 0.043(7) Uani 1 1 d U
C6 C 0.228(3) 0.054(3) 0.532(3) 0.079(10) Uani 1 1 d U
C7 C 0.120(2) 0.115(2) 0.402(2) 0.046(7) Uani 1 1 d U
C8 C 0.448(2) 0.398(2) 0.634(2) 0.061(8) Uani 1 1 d U
C9 C 0.272(3) 0.361(3) 0.488(3) 0.085(10) Uani 1 1 d U
C10 C 0.087(2) 0.246(2) 0.338(2) 0.063(8) Uani 1 1 d U
C11 C 0.245(3) 0.455(3) 0.665(3) 0.070(9) Uani 1 1 d U
C12 C 0.074(3) 0.397(2) 0.499(3) 0.073(9) Uani 1 1 d U
C13 C 0.256(3) 0.257(3) 0.725(3) 0.071(9) Uani 1 1 d U
C14 C 0.126(3) 0.104(3) 0.195(3) 0.082(10) Uani 1 1 d U
C15 C 0.477(4) 0.355(4) 0.444(4) 0.118(13) Uani 1 1 d U
C16 C 0.087(3) 0.107(3) 0.603(3) 0.100(12) Uani 1 1 d U
C17 C 0.391(4) 0.424(4) 0.797(4) 0.133(14) Uani 1 1 d U
C18 C 0.034(4) 0.237(3) 0.529(3) 0.110(12) Uani 1 1 d U
O1 O 0.2014(19) -0.0501(19) 0.2523(18) 0.091(8) Uani 1 1 d U
O2 O 0.393(2) -0.0361(19) 0.4674(19) 0.094(8) Uani 1 1 d U
O3 O 0.5478(19) 0.2197(18) 0.5296(19) 0.093(8) Uani 1 1 d U
O4 O 0.2765(19) 0.3134(18) 0.2759(18) 0.089(8) Uani 1 1 d U
O5 O 0.4246(16) 0.2124(14) 0.6708(15) 0.063(6) Uani 1 1 d U
O6 O 0.216(2) -0.0012(19) 0.5488(19) 0.094(8) Uani 1 1 d U
O7 O 0.0544(17) 0.0574(17) 0.3524(16) 0.076(7) Uani 1 1 d U
O8 O 0.5182(19) 0.4477(17) 0.6851(18) 0.085(7) Uani 1 1 d U
O9 O 0.2789(19) 0.4263(19) 0.4792(18) 0.088(8) Uani 1 1 d U
O10 O 0.0288(19) 0.2561(18) 0.2799(19) 0.097(8) Uani 1 1 d U
O11 O 0.262(2) 0.529(2) 0.6784(19) 0.096(8) Uani 1 1 d U
O12 O 0.0393(19) 0.4342(19) 0.4554(19) 0.096(8) Uani 1 1 d U
O13 O 0.2948(19) 0.2239(18) 0.7760(18) 0.089(8) Uani 1 1 d U
O14 O 0.0574(19) 0.0771(17) 0.1368(18) 0.087(8) Uani 1 1 d U
O15 O 0.522(2) 0.424(2) 0.452(2) 0.131(11) Uani 1 1 d U
O16 O 0.052(2) 0.042(2) 0.598(2) 0.119(10) Uani 1 1 d U
O17 O 0.454(3) 0.469(3) 0.858(3) 0.140(12) Uani 1 1 d U
O18 O -0.043(2) 0.201(2) 0.483(2) 0.128(11) Uani 1 1 d U
Pt10 Pt 0.0000 0.5000 1.0000 0.0351(5) Uani 1 2 d S
P1 P 0.0696(6) 0.6253(6) 0.9978(5) 0.051(2) Uani 1 1 d .
P2 P 0.0508(6) 0.4305(5) 0.8999(5) 0.043(2) Uani 1 1 d .
C101 C 0.0756(16) 0.5902(13) 0.8934(10) 0.062(6) Uani 1 1 d GU
C102 C 0.0884(15) 0.6491(10) 0.8592(12) 0.061(6) Uani 1 1 d GU
H102 H 0.0940 0.7076 0.8897 0.074 Uiso 1 1 calc R
C103 C 0.0929(15) 0.6206(12) 0.7793(13) 0.061(6) Uani 1 1 d GU
H103 H 0.1015 0.6601 0.7564 0.074 Uiso 1 1 calc R
C104 C 0.0845(15) 0.5332(13) 0.7337(10) 0.062(6) Uani 1 1 d GU
H104 H 0.0875 0.5141 0.6803 0.074 Uiso 1 1 calc R
C105 C 0.0716(15) 0.4743(10) 0.7680(12) 0.054(6) Uani 1 1 d GU
H105 H 0.0660 0.4158 0.7374 0.065 Uiso 1 1 calc R
C106 C 0.0672(15) 0.5027(12) 0.8478(12) 0.054(6) Uani 1 1 d GU
C107 C 0.0159(13) 0.7083(11) 1.0010(13) 0.049(6) Uani 1 1 d GU
C108 C -0.0564(14) 0.6976(11) 0.9248(11) 0.056(6) Uani 1 1 d GU
H108 H -0.0759 0.6481 0.8716 0.067 Uiso 1 1 calc R
C109 C -0.0994(12) 0.7610(13) 0.9281(11) 0.061(6) Uani 1 1 d GU
H109 H -0.1478 0.7539 0.8771 0.074 Uiso 1 1 calc R
C110 C -0.0702(13) 0.8351(11) 1.0075(14) 0.057(6) Uani 1 1 d GU
H110 H -0.0990 0.8775 1.0097 0.069 Uiso 1 1 calc R
C111 C 0.0021(14) 0.8457(10) 1.0837(11) 0.053(6) Uani 1 1 d GU
H111 H 0.0216 0.8952 1.1369 0.063 Uiso 1 1 calc R
C112 C 0.0452(12) 0.7823(13) 1.0804(11) 0.055(6) Uani 1 1 d GU
H112 H 0.0935 0.7894 1.1314 0.066 Uiso 1 1 calc R
C113 C 0.1837(11) 0.6774(15) 1.0810(14) 0.064(7) Uani 1 1 d GU
C114 C 0.2311(15) 0.7547(15) 1.0882(14) 0.069(7) Uani 1 1 d GU
H114 H 0.2029 0.7803 1.0524 0.082 Uiso 1 1 calc R
C115 C 0.3208(14) 0.7935(13) 1.1488(16) 0.077(7) Uani 1 1 d GU
H115 H 0.3525 0.8452 1.1536 0.092 Uiso 1 1 calc R
C116 C 0.3630(11) 0.7552(15) 1.2023(15) 0.079(7) Uani 1 1 d GU
H116 H 0.4230 0.7812 1.2428 0.095 Uiso 1 1 calc R
C117 C 0.3156(14) 0.6780(15) 1.1951(15) 0.084(7) Uani 1 1 d GU
H117 H 0.3438 0.6524 1.2309 0.100 Uiso 1 1 calc R
C118 C 0.2260(14) 0.6391(13) 1.1345(16) 0.073(7) Uani 1 1 d GU
H118 H 0.1942 0.5875 1.1297 0.087 Uiso 1 1 calc R
C119 C 0.1605(12) 0.4222(16) 0.9545(14) 0.067(7) Uani 1 1 d GU
C120 C 0.2147(15) 0.4120(16) 0.9131(12) 0.071(7) Uani 1 1 d GU
H120 H 0.1948 0.4093 0.8565 0.085 Uiso 1 1 calc R
C121 C 0.2987(13) 0.4058(16) 0.9563(14) 0.075(7) Uani 1 1 d GU
H121 H 0.3350 0.3990 0.9286 0.091 Uiso 1 1 calc R
C122 C 0.3284(11) 0.4099(16) 1.0409(14) 0.076(7) Uani 1 1 d GU
H122 H 0.3846 0.4058 1.0698 0.091 Uiso 1 1 calc R
C123 C 0.2742(15) 0.4201(16) 1.0823(12) 0.068(7) Uani 1 1 d GU
H123 H 0.2941 0.4229 1.1389 0.082 Uiso 1 1 calc R
C124 C 0.1902(13) 0.4263(16) 1.0391(14) 0.070(7) Uani 1 1 d GU
H124 H 0.1539 0.4332 1.0668 0.084 Uiso 1 1 calc R
C125 C -0.0196(18) 0.3311(14) 0.8056(16) 0.089(7) Uani 1 1 d GU
C126 C 0.0158(14) 0.2628(19) 0.7854(17) 0.092(7) Uani 1 1 d GU
H126 H 0.0758 0.2716 0.8187 0.111 Uiso 1 1 calc R
C127 C -0.038(2) 0.1814(16) 0.7154(19) 0.096(7) Uani 1 1 d GU
H127 H -0.0148 0.1357 0.7018 0.115 Uiso 1 1 calc R
C128 C -0.1282(19) 0.1682(15) 0.6656(16) 0.103(7) Uani 1 1 d GU
H128 H -0.1645 0.1137 0.6187 0.123 Uiso 1 1 calc R
C129 C -0.1636(14) 0.237(2) 0.6858(18) 0.104(8) Uani 1 1 d GU
H129 H -0.2237 0.2277 0.6525 0.124 Uiso 1 1 calc R
C130 C -0.109(2) 0.3180(17) 0.7558(19) 0.097(7) Uani 1 1 d GU
H130 H -0.1330 0.3637 0.7693 0.117 Uiso 1 1 calc R
Pt11 Pt 0.5000 1.0000 0.0000 0.0342(5) Uani 1 2 d S
P3 P 0.5432(6) 0.9137(6) 0.0733(5) 0.043(2) Uani 1 1 d .
P4 P 0.4317(6) 1.0409(5) 0.0904(5) 0.040(2) Uani 1 1 d .
C301 C 0.5346(13) 0.9570(12) 0.1761(10) 0.044(6) Uani 1 1 d GU
C302 C 0.5697(12) 0.9315(10) 0.2436(12) 0.046(6) Uani 1 1 d GU
H302 H 0.6006 0.8909 0.2381 0.055 Uiso 1 1 calc R
C303 C 0.5585(13) 0.9665(12) 0.3194(10) 0.039(5) Uani 1 1 d GU
H303 H 0.5819 0.9495 0.3645 0.047 Uiso 1 1 calc R
C304 C 0.5122(12) 1.0271(11) 0.3276(9) 0.038(5) Uani 1 1 d GU
H304 H 0.5047 1.0506 0.3783 0.046 Uiso 1 1 calc R
C305 C 0.4771(12) 1.0527(10) 0.2601(11) 0.037(5) Uani 1 1 d GU
H305 H 0.4461 1.0932 0.2656 0.044 Uiso 1 1 calc R
C306 C 0.4883(13) 1.0176(12) 0.1843(10) 0.040(5) Uani 1 1 d GU
C307 C 0.4728(13) 0.8011(10) 0.0164(14) 0.065(7) Uani 1 1 d GU
C308 C 0.4921(12) 0.7411(14) 0.0506(12) 0.068(7) Uani 1 1 d GU
H308 H 0.5443 0.7574 0.1022 0.082 Uiso 1 1 calc R
C309 C 0.4333(15) 0.6566(12) 0.0077(15) 0.078(7) Uani 1 1 d GU
H309 H 0.4462 0.6165 0.0306 0.093 Uiso 1 1 calc R
C310 C 0.3553(14) 0.6322(11) -0.0695(15) 0.080(7) Uani 1 1 d GU
H310 H 0.3159 0.5757 -0.0982 0.096 Uiso 1 1 calc R
C311 C 0.3360(12) 0.6922(14) -0.1037(13) 0.075(7) Uani 1 1 d GU
H311 H 0.2837 0.6759 -0.1553 0.090 Uiso 1 1 calc R
C312 C 0.3947(14) 0.7767(12) -0.0608(14) 0.067(7) Uani 1 1 d GU
H312 H 0.3818 0.8168 -0.0837 0.080 Uiso 1 1 calc R
C313 C 0.6559(11) 0.9129(15) 0.1123(15) 0.059(6) Uani 1 1 d GU
C314 C 0.7220(15) 0.9861(13) 0.1862(14) 0.070(7) Uani 1 1 d GU
H314 H 0.7070 1.0336 0.2152 0.084 Uiso 1 1 calc R
C315 C 0.8104(13) 0.9882(13) 0.2169(13) 0.075(7) Uani 1 1 d GU
H315 H 0.8546 1.0371 0.2664 0.090 Uiso 1 1 calc R
C316 C 0.8328(11) 0.9171(16) 0.1736(16) 0.074(7) Uani 1 1 d GU
H316 H 0.8920 0.9185 0.1942 0.088 Uiso 1 1 calc R
C317 C 0.7668(15) 0.8439(13) 0.0997(15) 0.075(7) Uani 1 1 d GU
H317 H 0.7818 0.7963 0.0708 0.090 Uiso 1 1 calc R
C318 C 0.6784(13) 0.8418(12) 0.0690(13) 0.067(7) Uani 1 1 d GU
H318 H 0.6342 0.7928 0.0196 0.080 Uiso 1 1 calc R
C319 C 0.3155(9) 0.9815(12) 0.0376(12) 0.045(5) Uani 1 1 d GU
C320 C 0.2670(13) 0.9892(12) 0.0850(9) 0.056(6) Uani 1 1 d GU
H320 H 0.2951 1.0241 0.1460 0.067 Uiso 1 1 calc R
C321 C 0.1764(13) 0.9446(13) 0.0412(13) 0.055(5) Uani 1 1 d GU
H321 H 0.1440 0.9498 0.0729 0.066 Uiso 1 1 calc R
C322 C 0.1344(9) 0.8924(12) -0.0500(13) 0.051(5) Uani 1 1 d GU
H322 H 0.0739 0.8626 -0.0793 0.061 Uiso 1 1 calc R
C323 C 0.1830(12) 0.8847(12) -0.0974(9) 0.051(5) Uani 1 1 d GU
H323 H 0.1548 0.8497 -0.1584 0.061 Uiso 1 1 calc R
C324 C 0.2735(12) 0.9292(13) -0.0536(12) 0.045(5) Uani 1 1 d GU
H324 H 0.3060 0.9240 -0.0853 0.054 Uiso 1 1 calc R
C325 C 0.4462(19) 1.1564(13) 0.1477(17) 0.080(7) Uani 1 1 d GU
C326 C 0.5331(16) 1.2118(19) 0.2021(18) 0.090(7) Uani 1 1 d GU
H326 H 0.5801 1.1886 0.2118 0.108 Uiso 1 1 calc R
C327 C 0.5498(15) 1.3020(17) 0.2418(16) 0.099(7) Uani 1 1 d GU
H327 H 0.6080 1.3391 0.2781 0.119 Uiso 1 1 calc R
C328 C 0.480(2) 1.3367(13) 0.2272(18) 0.100(7) Uani 1 1 d GU
H328 H 0.4907 1.3971 0.2538 0.120 Uiso 1 1 calc R
C329 C 0.3926(17) 1.2813(18) 0.1729(18) 0.093(7) Uani 1 1 d GU
H329 H 0.3456 1.3046 0.1632 0.112 Uiso 1 1 calc R
C330 C 0.3759(14) 1.1912(17) 0.1332(16) 0.087(7) Uani 1 1 d GU
H330 H 0.3178 1.1541 0.0968 0.104 Uiso 1 1 calc R
C401 C 0.818(3) 0.331(2) 0.398(3) 0.145(17) Uiso 1 1 d DU
H40A H 0.8439 0.3458 0.3642 0.217 Uiso 1 1 calc R
H40B H 0.8647 0.3460 0.4564 0.217 Uiso 1 1 calc R
H40C H 0.7773 0.3630 0.4038 0.217 Uiso 1 1 calc R
C402 C 0.770(3) 0.234(2) 0.352(2) 0.131(14) Uiso 1 1 d DU
C403 C 0.730(3) 0.206(3) 0.404(3) 0.130(15) Uiso 1 1 d DU
H40D H 0.6992 0.1441 0.3719 0.195 Uiso 1 1 calc R
H40E H 0.6887 0.2371 0.4109 0.195 Uiso 1 1 calc R
H40F H 0.7761 0.2187 0.4611 0.195 Uiso 1 1 calc R
O402 O 0.737(3) 0.196(2) 0.272(2) 0.165(16) Uiso 1 1 d D
C501 C 0.160(3) 0.494(4) 0.344(3) 0.153(18) Uiso 1 1 d DU
H50A H 0.0981 0.4835 0.3095 0.230 Uiso 1 1 calc R
H50B H 0.1798 0.5364 0.4041 0.230 Uiso 1 1 calc R
H50C H 0.1703 0.4402 0.3444 0.230 Uiso 1 1 calc R
C502 C 0.212(2) 0.528(3) 0.305(2) 0.145(16) Uiso 1 1 d DU
C503 C 0.311(2) 0.547(4) 0.356(3) 0.170(19) Uiso 1 1 d DU
H50D H 0.3407 0.5702 0.3293 0.255 Uiso 1 1 calc R
H50E H 0.3229 0.4936 0.3551 0.255 Uiso 1 1 calc R
H50F H 0.3315 0.5888 0.4164 0.255 Uiso 1 1 calc R
O502 O 0.179(2) 0.503(2) 0.225(2) 0.116(11) Uiso 1 1 d D
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C2 Pt1 C1 96.5(17) . .
C2 Pt1 C3 106.4(18) . .
C1 Pt1 C3 148.0(16) . .
C2 Pt1 Pt2 152.8(14) . .
C1 Pt1 Pt2 108.8(11) . .
C3 Pt1 Pt2 46.3(11) . .
C2 Pt1 Pt3 146.8(14) . .
C1 Pt1 Pt3 50.4(11) . .
C3 Pt1 Pt3 105.4(11) . .
Pt2 Pt1 Pt3 59.82(6) . .
C2 Pt1 Pt4 92.9(13) . .
C1 Pt1 Pt4 89.2(11) . .
C3 Pt1 Pt4 111.1(11) . .
Pt2 Pt1 Pt4 97.16(6) . .
Pt3 Pt1 Pt4 84.46(7) . .
C15 Pt2 C3 99(2) . .
C15 Pt2 C4 98(2) . .
C3 Pt2 C4 157.2(16) . .
C15 Pt2 Pt1 148.7(17) . .
C3 Pt2 Pt1 49.5(12) . .
C4 Pt2 Pt1 111.2(12) . .
C15 Pt2 Pt3 148.7(17) . .
C3 Pt2 Pt3 109.1(12) . .
C4 Pt2 Pt3 50.9(13) . .
Pt1 Pt2 Pt3 60.41(6) . .
C15 Pt2 Pt5 103.4(17) . .
C3 Pt2 Pt5 84.9(11) . .
C4 Pt2 Pt5 104.6(12) . .
Pt1 Pt2 Pt5 78.88(6) . .
Pt3 Pt2 Pt5 92.09(7) . .
C14 Pt3 C1 99.7(17) . .
C14 Pt3 C4 103.3(18) . .
C1 Pt3 C4 152.6(16) . .
C14 Pt3 Pt2 152.5(13) . .
C1 Pt3 Pt2 106.5(11) . .
C4 Pt3 Pt2 49.3(12) . .
C14 Pt3 Pt1 147.5(13) . .
C1 Pt3 Pt1 48.1(11) . .
C4 Pt3 Pt1 109.0(12) . .
Pt2 Pt3 Pt1 59.77(6) . .
C14 Pt3 Pt6 95.8(12) . .
C1 Pt3 Pt6 107.9(11) . .
C4 Pt3 Pt6 84.5(11) . .
Pt2 Pt3 Pt6 83.94(6) . .
Pt1 Pt3 Pt6 91.39(7) . .
C6 Pt4 C5 99.2(16) . .
C6 Pt4 C7 101.7(16) . .
C5 Pt4 C7 159.1(13) . .
C6 Pt4 Pt5 147.6(14) . .
C5 Pt4 Pt5 48.5(9) . .
C7 Pt4 Pt5 110.6(9) . .
C6 Pt4 Pt6 152.3(14) . .
C5 Pt4 Pt6 108.4(9) . .
C7 Pt4 Pt6 50.7(9) . .
Pt5 Pt4 Pt6 59.93(6) . .
C6 Pt4 Pt9 89.6(13) . .
C5 Pt4 Pt9 96.5(8) . .
C7 Pt4 Pt9 83.3(8) . .
Pt5 Pt4 Pt9 92.68(6) . .
Pt6 Pt4 Pt9 84.11(7) . .
C6 Pt4 Pt1 98.2(13) . .
C5 Pt4 Pt1 78.9(8) . .
C7 Pt4 Pt1 98.4(8) . .
Pt5 Pt4 Pt1 78.93(6) . .
Pt6 Pt4 Pt1 90.52(7) . .
Pt9 Pt4 Pt1 171.52(7) . .
C8 Pt5 C9 100.5(17) . .
C8 Pt5 C5 99.9(14) . .
C9 Pt5 C5 159.2(16) . .
C8 Pt5 Pt6 149.7(11) . .
C9 Pt5 Pt6 49.3(13) . .
C5 Pt5 Pt6 110.4(9) . .
C8 Pt5 Pt4 150.2(11) . .
C9 Pt5 Pt4 109.2(13) . .
C5 Pt5 Pt4 50.3(9) . .
Pt6 Pt5 Pt4 60.06(6) . .
C8 Pt5 Pt8 91.8(11) . .
C9 Pt5 Pt8 97.0(12) . .
C5 Pt5 Pt8 78.7(8) . .
Pt6 Pt5 Pt8 94.11(7) . .
Pt4 Pt5 Pt8 84.36(6) . .
C8 Pt5 Pt2 89.1(11) . .
C9 Pt5 Pt2 78.3(12) . .
C5 Pt5 Pt2 105.7(8) . .
Pt6 Pt5 Pt2 82.91(7) . .
Pt4 Pt5 Pt2 97.15(6) . .
Pt8 Pt5 Pt2 175.35(7) . .
C10 Pt6 C9 106.0(18) . .
C10 Pt6 C7 96.2(15) . .
C9 Pt6 C7 157.8(16) . .
C10 Pt6 Pt5 153.8(12) . .
C9 Pt6 Pt5 47.9(13) . .
C7 Pt6 Pt5 109.9(9) . .
C10 Pt6 Pt4 146.1(12) . .
C9 Pt6 Pt4 107.8(13) . .
C7 Pt6 Pt4 50.0(9) . .
Pt5 Pt6 Pt4 60.01(6) . .
C10 Pt6 Pt3 88.6(11) . .
C9 Pt6 Pt3 99.7(11) . .
C7 Pt6 Pt3 80.3(8) . .
Pt5 Pt6 Pt3 93.46(7) . .
Pt4 Pt6 Pt3 85.84(7) . .
C10 Pt6 Pt7 94.0(11) . .
C9 Pt6 Pt7 77.5(11) . .
C7 Pt6 Pt7 101.5(8) . .
Pt5 Pt6 Pt7 83.24(7) . .
Pt4 Pt6 Pt7 93.16(7) . .
Pt3 Pt6 Pt7 176.60(7) . .
C12 Pt7 C18 103.1(19) . .
C12 Pt7 C11 101.7(17) . .
C18 Pt7 C11 150.6(18) . .
C12 Pt7 Pt9 151.8(13) . .
C18 Pt7 Pt9 49.1(14) . .
C11 Pt7 Pt9 106.2(11) . .
C12 Pt7 Pt8 148.4(13) . .
C18 Pt7 Pt8 108.2(14) . .
C11 Pt7 Pt8 47.2(11) . .
Pt9 Pt7 Pt8 59.73(6) . .
C12 Pt7 Pt6 90.7(12) . .
C18 Pt7 Pt6 88.1(14) . .
C11 Pt7 Pt6 107.3(11) . .
Pt9 Pt7 Pt6 84.57(7) . .
Pt8 Pt7 Pt6 94.27(7) . .
C17 Pt8 C11 103(2) . .
C17 Pt8 C13 97(2) . .
C11 Pt8 C13 155.7(16) . .
C17 Pt8 Pt9 146.4(18) . .
C11 Pt8 Pt9 110.2(12) . .
C13 Pt8 Pt9 49.1(11) . .
C17 Pt8 Pt7 153.5(18) . .
C11 Pt8 Pt7 50.9(12) . .
C13 Pt8 Pt7 108.8(11) . .
Pt9 Pt8 Pt7 59.99(6) . .
C17 Pt8 Pt5 95.1(18) . .
C11 Pt8 Pt5 88.0(11) . .
C13 Pt8 Pt5 104.0(10) . .
Pt9 Pt8 Pt5 93.01(6) . .
Pt7 Pt8 Pt5 82.86(7) . .
C16 Pt9 C13 99.4(18) . .
C16 Pt9 C18 101(2) . .
C13 Pt9 C18 155.9(18) . .
C16 Pt9 Pt8 148.6(15) . .
C13 Pt9 Pt8 49.2(11) . .
C18 Pt9 Pt8 110.1(15) . .
C16 Pt9 Pt7 151.0(15) . .
C13 Pt9 Pt7 109.3(11) . .
C18 Pt9 Pt7 50.4(15) . .
Pt8 Pt9 Pt7 60.29(6) . .
C16 Pt9 Pt4 93.4(14) . .
C13 Pt9 Pt4 85.9(11) . .
C18 Pt9 Pt4 105.9(14) . .
Pt8 Pt9 Pt4 84.42(6) . .
Pt7 Pt9 Pt4 92.81(6) . .
O1 C1 Pt1 143(3) . .
O1 C1 Pt3 134(3) . .
Pt1 C1 Pt3 81.5(15) . .
O2 C2 Pt1 174(4) . .
O3 C3 Pt2 141(3) . .
O3 C3 Pt1 135(3) . .
Pt2 C3 Pt1 84.2(16) . .
O4 C4 Pt2 141(4) . .
O4 C4 Pt3 139(4) . .
Pt2 C4 Pt3 79.9(16) . .
O5 C5 Pt5 142(2) . .
O5 C5 Pt4 136(2) . .
Pt5 C5 Pt4 81.2(12) . .
O6 C6 Pt4 174(4) . .
O7 C7 Pt4 141(3) . .
O7 C7 Pt6 139(3) . .
Pt4 C7 Pt6 79.3(12) . .
O8 C8 Pt5 171(3) . .
O9 C9 Pt5 141(4) . .
O9 C9 Pt6 137(4) . .
Pt5 C9 Pt6 82.9(18) . .
O10 C10 Pt6 174(3) . .
O11 C11 Pt8 149(3) . .
O11 C11 Pt7 129(3) . .
Pt8 C11 Pt7 81.9(15) . .
O12 C12 Pt7 176(4) . .
O13 C13 Pt9 137(3) . .
O13 C13 Pt8 141(3) . .
Pt9 C13 Pt8 81.7(15) . .
O14 C14 Pt3 176(4) . .
O15 C15 Pt2 167(5) . .
O16 C16 Pt9 175(4) . .
O17 C17 Pt8 170(6) . .
O18 C18 Pt9 139(4) . .
O18 C18 Pt7 140(4) . .
Pt9 C18 Pt7 80(2) . .
P2 Pt10 P2 180.0(3) . 2_567
P2 Pt10 P1 83.0(3) . .
P2 Pt10 P1 97.0(3) 2_567 .
P2 Pt10 P1 97.0(3) . 2_567
P2 Pt10 P1 83.0(3) 2_567 2_567
P1 Pt10 P1 180.000(1) . 2_567
C107 P1 C113 107.8(11) . .
C107 P1 C101 105.4(11) . .
C113 P1 C101 103.9(12) . .
C107 P1 Pt10 117.6(8) . .
C113 P1 Pt10 113.9(9) . .
C101 P1 Pt10 107.0(8) . .
C125 P2 C119 110.6(13) . .
C125 P2 C106 101.4(12) . .
C119 P2 C106 103.8(11) . .
C125 P2 Pt10 119.5(11) . .
C119 P2 Pt10 112.5(8) . .
C106 P2 Pt10 107.1(7) . .
C102 C101 C106 120.0 . .
C102 C101 P1 121.1(12) . .
C106 C101 P1 118.9(12) . .
C103 C102 C101 120.0 . .
C103 C102 H102 120.0 . .
C101 C102 H102 120.0 . .
C102 C103 C104 120.0 . .
C102 C103 H103 120.0 . .
C104 C103 H103 120.0 . .
C103 C104 C105 120.0 . .
C103 C104 H104 120.0 . .
C105 C104 H104 120.0 . .
C106 C105 C104 120.0 . .
C106 C105 H105 120.0 . .
C104 C105 H105 120.0 . .
C105 C106 C101 120.0 . .
C105 C106 P2 123.8(11) . .
C101 C106 P2 116.2(11) . .
C108 C107 C112 120.0 . .
C108 C107 P1 120.1(12) . .
C112 C107 P1 119.9(12) . .
C107 C108 C109 120.0 . .
C107 C108 H108 120.0 . .
C109 C108 H108 120.0 . .
C108 C109 C110 120.0 . .
C108 C109 H109 120.0 . .
C110 C109 H109 120.0 . .
C111 C110 C109 120.0 . .
C111 C110 H110 120.0 . .
C109 C110 H110 120.0 . .
C110 C111 C112 120.0 . .
C110 C111 H111 120.0 . .
C112 C111 H111 120.0 . .
C111 C112 C107 120.0 . .
C111 C112 H112 120.0 . .
C107 C112 H112 120.0 . .
C114 C113 C118 120.0 . .
C114 C113 P1 119.0(14) . .
C118 C113 P1 120.9(14) . .
C115 C114 C113 120.0 . .
C115 C114 H114 120.0 . .
C113 C114 H114 120.0 . .
C114 C115 C116 120.0 . .
C114 C115 H115 120.0 . .
C116 C115 H115 120.0 . .
C117 C116 C115 120.0 . .
C117 C116 H116 120.0 . .
C115 C116 H116 120.0 . .
C118 C117 C116 120.0 . .
C118 C117 H117 120.0 . .
C116 C117 H117 120.0 . .
C117 C118 C113 120.0 . .
C117 C118 H118 120.0 . .
C113 C118 H118 120.0 . .
C120 C119 C124 120.0 . .
C120 C119 P2 121.0(13) . .
C124 C119 P2 119.0(12) . .
C121 C120 C119 120.0 . .
C121 C120 H120 120.0 . .
C119 C120 H120 120.0 . .
C122 C121 C120 120.0 . .
C122 C121 H121 120.0 . .
C120 C121 H121 120.0 . .
C121 C122 C123 120.0 . .
C121 C122 H122 120.0 . .
C123 C122 H122 120.0 . .
C124 C123 C122 120.0 . .
C124 C123 H123 120.0 . .
C122 C123 H123 120.0 . .
C123 C124 C119 120.0 . .
C123 C124 H124 120.0 . .
C119 C124 H124 120.0 . .
C126 C125 C130 120.0 . .
C126 C125 P2 117.8(18) . .
C130 C125 P2 122.0(18) . .
C125 C126 C127 120.0 . .
C125 C126 H126 120.0 . .
C127 C126 H126 120.0 . .
C128 C127 C126 120.0 . .
C128 C127 H127 120.0 . .
C126 C127 H127 120.0 . .
C127 C128 C129 120.0 . .
C127 C128 H128 120.0 . .
C129 C128 H128 120.0 . .
C130 C129 C128 120.0 . .
C130 C129 H129 120.0 . .
C128 C129 H129 120.0 . .
C129 C130 C125 120.0 . .
C129 C130 H130 120.0 . .
C125 C130 H130 120.0 . .
P4 Pt11 P4 180.000(1) . 2_675
P4 Pt11 P3 96.5(3) . 2_675
P4 Pt11 P3 83.5(3) 2_675 2_675
P4 Pt11 P3 83.5(3) . .
P4 Pt11 P3 96.5(3) 2_675 .
P3 Pt11 P3 180.0(2) 2_675 .
C313 P3 C307 107.5(11) . .
C313 P3 C301 101.9(10) . .
C307 P3 C301 103.7(11) . .
C313 P3 Pt11 118.3(9) . .
C307 P3 Pt11 115.4(8) . .
C301 P3 Pt11 108.3(7) . .
C319 P4 C325 108.4(12) . .
C319 P4 C306 108.0(10) . .
C325 P4 C306 100.6(11) . .
C319 P4 Pt11 114.0(7) . .
C325 P4 Pt11 118.4(10) . .
C306 P4 Pt11 106.1(7) . .
C302 C301 C306 120.0 . .
C302 C301 P3 123.7(11) . .
C306 C301 P3 116.3(11) . .
C303 C302 C301 120.0 . .
C303 C302 H302 120.0 . .
C301 C302 H302 120.0 . .
C302 C303 C304 120.0 . .
C302 C303 H303 120.0 . .
C304 C303 H303 120.0 . .
C305 C304 C303 120.0 . .
C305 C304 H304 120.0 . .
C303 C304 H304 120.0 . .
C304 C305 C306 120.0 . .
C304 C305 H305 120.0 . .
C306 C305 H305 120.0 . .
C305 C306 C301 120.0 . .
C305 C306 P4 120.1(10) . .
C301 C306 P4 119.5(10) . .
C308 C307 C312 120.0 . .
C308 C307 P3 121.8(13) . .
C312 C307 P3 118.1(13) . .
C307 C308 C309 120.0 . .
C307 C308 H308 120.0 . .
C309 C308 H308 120.0 . .
C310 C309 C308 120.0 . .
C310 C309 H309 120.0 . .
C308 C309 H309 120.0 . .
C309 C310 C311 120.0 . .
C309 C310 H310 120.0 . .
C311 C310 H310 120.0 . .
C310 C311 C312 120.0 . .
C310 C311 H311 120.0 . .
C312 C311 H311 120.0 . .
C311 C312 C307 120.0 . .
C311 C312 H312 120.0 . .
C307 C312 H312 120.0 . .
C314 C313 C318 120.0 . .
C314 C313 P3 118.7(13) . .
C318 C313 P3 121.3(13) . .
C313 C314 C315 120.0 . .
C313 C314 H314 120.0 . .
C315 C314 H314 120.0 . .
C314 C315 C316 120.0 . .
C314 C315 H315 120.0 . .
C316 C315 H315 120.0 . .
C317 C316 C315 120.0 . .
C317 C316 H316 120.0 . .
C315 C316 H316 120.0 . .
C318 C317 C316 120.0 . .
C318 C317 H317 120.0 . .
C316 C317 H317 120.0 . .
C317 C318 C313 120.0 . .
C317 C318 H318 120.0 . .
C313 C318 H318 120.0 . .
C320 C319 C324 120.0 . .
C320 C319 P4 121.6(12) . .
C324 C319 P4 118.3(12) . .
C321 C320 C319 120.0 . .
C321 C320 H320 120.0 . .
C319 C320 H320 120.0 . .
C322 C321 C320 120.0 . .
C322 C321 H321 120.0 . .
C320 C321 H321 120.0 . .
C321 C322 C323 120.0 . .
C321 C322 H322 120.0 . .
C323 C322 H322 120.0 . .
C324 C323 C322 120.0 . .
C324 C323 H323 120.0 . .
C322 C323 H323 120.0 . .
C323 C324 C319 120.0 . .
C323 C324 H324 120.0 . .
C319 C324 H324 120.0 . .
C326 C325 C330 120.0 . .
C326 C325 P4 116.7(17) . .
C330 C325 P4 123.0(17) . .
C325 C326 C327 120.0 . .
C325 C326 H326 120.0 . .
C327 C326 H326 120.0 . .
C328 C327 C326 120.0 . .
C328 C327 H327 120.0 . .
C326 C327 H327 120.0 . .
C327 C328 C329 120.0 . .
C327 C328 H328 120.0 . .
C329 C328 H328 120.0 . .
C328 C329 C330 120.0 . .
C328 C329 H329 120.0 . .
C330 C329 H329 120.0 . .
C329 C330 C325 120.0 . .
C329 C330 H330 120.0 . .
C325 C330 H330 120.0 . .
C402 C401 H40A 109.5 . .
C402 C401 H40B 109.5 . .
H40A C401 H40B 109.5 . .
C402 C401 H40C 109.5 . .
H40A C401 H40C 109.5 . .
H40B C401 H40C 109.5 . .
O402 C402 C403 122(3) . .
O402 C402 C401 119(3) . .
C403 C402 C401 112(3) . .
C402 C403 H40D 109.5 . .
C402 C403 H40E 109.5 . .
H40D C403 H40E 109.5 . .
C402 C403 H40F 109.5 . .
H40D C403 H40F 109.5 . .
H40E C403 H40F 109.5 . .
C502 C501 H50A 109.5 . .
C502 C501 H50B 109.5 . .
H50A C501 H50B 109.5 . .
C502 C501 H50C 109.5 . .
H50A C501 H50C 109.5 . .
H50B C501 H50C 109.5 . .
O502 C502 C501 120(3) . .
O502 C502 C503 119(3) . .
C501 C502 C503 113(3) . .
C502 C503 H50D 109.5 . .
C502 C503 H50E 109.5 . .
H50D C503 H50E 109.5 . .
C502 C503 H50F 109.5 . .
H50D C503 H50F 109.5 . .
H50E C503 H50F 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pt1 C2 1.85(5) .
Pt1 C1 2.01(4) .
Pt1 C3 2.03(4) .
Pt1 Pt2 2.654(2) .
Pt1 Pt3 2.670(2) .
Pt1 Pt4 3.065(2) .
Pt2 C15 1.77(6) .
Pt2 C3 1.93(4) .
Pt2 C4 2.04(4) .
Pt2 Pt3 2.655(2) .
Pt2 Pt5 3.066(3) .
Pt3 C14 1.85(4) .
Pt3 C1 2.08(4) .
Pt3 C4 2.09(5) .
Pt3 Pt6 3.010(2) .
Pt4 C6 1.79(4) .
Pt4 C5 2.07(3) .
Pt4 C7 2.07(3) .
Pt4 Pt5 2.652(2) .
Pt4 Pt6 2.653(2) .
Pt4 Pt9 3.046(2) .
Pt5 C8 1.86(4) .
Pt5 C9 1.98(5) .
Pt5 C5 2.01(3) .
Pt5 Pt6 2.650(2) .
Pt5 Pt8 3.040(2) .
Pt6 C10 1.78(4) .
Pt6 C9 2.02(5) .
Pt6 C7 2.09(3) .
Pt6 Pt7 3.027(2) .
Pt7 C12 1.78(4) .
Pt7 C18 2.07(5) .
Pt7 C11 2.08(4) .
Pt7 Pt9 2.649(2) .
Pt7 Pt8 2.657(2) .
Pt8 C17 1.85(6) .
Pt8 C11 1.97(4) .
Pt8 C13 2.02(4) .
Pt8 Pt9 2.642(2) .
Pt9 C16 1.92(5) .
Pt9 C13 2.02(4) .
Pt9 C18 2.03(5) .
C1 O1 1.19(4) .
C2 O2 1.13(5) .
C3 O3 1.28(4) .
C4 O4 1.17(4) .
C5 O5 1.22(4) .
C6 O6 1.10(4) .
C7 O7 1.16(4) .
C8 O8 1.16(4) .
C9 O9 1.18(5) .
C10 O10 1.23(4) .
C11 O11 1.18(4) .
C12 O12 1.22(4) .
C13 O13 1.28(4) .
C14 O14 1.13(4) .
C15 O15 1.23(5) .
C16 O16 1.15(5) .
C17 O17 1.12(6) .
C18 O18 1.19(5) .
Pt10 P2 2.329(8) .
Pt10 P2 2.329(8) 2_567
Pt10 P1 2.329(10) .
Pt10 P1 2.329(10) 2_567
P1 C107 1.790(16) .
P1 C113 1.798(18) .
P1 C101 1.819(15) .
P2 C125 1.76(2) .
P2 C119 1.811(17) .
P2 C106 1.849(18) .
C101 C102 1.3900 .
C101 C106 1.3900 .
C102 C103 1.3900 .
C102 H102 0.9300 .
C103 C104 1.3900 .
C103 H103 0.9300 .
C104 C105 1.3900 .
C104 H104 0.9300 .
C105 C106 1.3900 .
C105 H105 0.9300 .
C107 C108 1.3900 .
C107 C112 1.3900 .
C108 C109 1.3900 .
C108 H108 0.9300 .
C109 C110 1.3900 .
C109 H109 0.9300 .
C110 C111 1.3900 .
C110 H110 0.9300 .
C111 C112 1.3900 .
C111 H111 0.9300 .
C112 H112 0.9300 .
C113 C114 1.3900 .
C113 C118 1.3900 .
C114 C115 1.3900 .
C114 H114 0.9300 .
C115 C116 1.3900 .
C115 H115 0.9300 .
C116 C117 1.3900 .
C116 H116 0.9300 .
C117 C118 1.3900 .
C117 H117 0.9300 .
C118 H118 0.9300 .
C119 C120 1.3900 .
C119 C124 1.3900 .
C120 C121 1.3900 .
C120 H120 0.9300 .
C121 C122 1.3900 .
C121 H121 0.9300 .
C122 C123 1.3900 .
C122 H122 0.9300 .
C123 C124 1.3900 .
C123 H123 0.9300 .
C124 H124 0.9300 .
C125 C126 1.3900 .
C125 C130 1.3900 .
C126 C127 1.3900 .
C126 H126 0.9300 .
C127 C128 1.3900 .
C127 H127 0.9300 .
C128 C129 1.3900 .
C128 H128 0.9300 .
C129 C130 1.3900 .
C129 H129 0.9300 .
C130 H130 0.9300 .
Pt11 P4 2.325(8) .
Pt11 P4 2.325(8) 2_675
Pt11 P3 2.328(9) 2_675
Pt11 P3 2.328(9) .
P3 C313 1.789(17) .
P3 C307 1.807(16) .
P3 C301 1.817(14) .
P4 C319 1.796(16) .
P4 C325 1.81(2) .
P4 C306 1.821(15) .
C301 C302 1.3900 .
C301 C306 1.3900 .
C302 C303 1.3900 .
C302 H302 0.9300 .
C303 C304 1.3900 .
C303 H303 0.9300 .
C304 C305 1.3900 .
C304 H304 0.9300 .
C305 C306 1.3900 .
C305 H305 0.9300 .
C307 C308 1.3900 .
C307 C312 1.3900 .
C308 C309 1.3900 .
C308 H308 0.9300 .
C309 C310 1.3900 .
C309 H309 0.9300 .
C310 C311 1.3900 .
C310 H310 0.9300 .
C311 C312 1.3900 .
C311 H311 0.9300 .
C312 H312 0.9300 .
C313 C314 1.3900 .
C313 C318 1.3900 .
C314 C315 1.3900 .
C314 H314 0.9300 .
C315 C316 1.3900 .
C315 H315 0.9300 .
C316 C317 1.3900 .
C316 H316 0.9300 .
C317 C318 1.3900 .
C317 H317 0.9300 .
C318 H318 0.9300 .
C319 C320 1.3900 .
C319 C324 1.3900 .
C320 C321 1.3900 .
C320 H320 0.9300 .
C321 C322 1.3900 .
C321 H321 0.9300 .
C322 C323 1.3900 .
C322 H322 0.9300 .
C323 C324 1.3900 .
C323 H323 0.9300 .
C324 H324 0.9300 .
C325 C326 1.3900 .
C325 C330 1.3900 .
C326 C327 1.3900 .
C326 H326 0.9300 .
C327 C328 1.3900 .
C327 H327 0.9300 .
C328 C329 1.3900 .
C328 H328 0.9300 .
C329 C330 1.3900 .
C329 H329 0.9300 .
C330 H330 0.9300 .
C401 C402 1.508(9) .
C401 H40A 0.9600 .
C401 H40B 0.9600 .
C401 H40C 0.9600 .
C402 O402 1.209(9) .
C402 C403 1.507(9) .
C403 H40D 0.9600 .
C403 H40E 0.9600 .
C403 H40F 0.9600 .
C501 C502 1.507(9) .
C501 H50A 0.9600 .
C501 H50B 0.9600 .
C501 H50C 0.9600 .
C502 O502 1.208(9) .
C502 C503 1.508(9) .
C503 H50D 0.9600 .
C503 H50E 0.9600 .
C503 H50F 0.9600 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
C2 Pt1 Pt2 C15 6(4) .
C1 Pt1 Pt2 C15 -151(3) .
C3 Pt1 Pt2 C15 5(4) .
Pt3 Pt1 Pt2 C15 -164(3) .
Pt4 Pt1 Pt2 C15 117(3) .
C2 Pt1 Pt2 C3 2(3) .
C1 Pt1 Pt2 C3 -156.0(19) .
Pt3 Pt1 Pt2 C3 -168.3(15) .
Pt4 Pt1 Pt2 C3 112.4(15) .
C2 Pt1 Pt2 C4 167(3) .
C1 Pt1 Pt2 C4 9.7(17) .
C3 Pt1 Pt2 C4 165.7(19) .
Pt3 Pt1 Pt2 C4 -2.6(12) .
Pt4 Pt1 Pt2 C4 -81.9(12) .
C2 Pt1 Pt2 Pt3 170(3) .
C1 Pt1 Pt2 Pt3 12.3(12) .
C3 Pt1 Pt2 Pt3 168.3(15) .
Pt4 Pt1 Pt2 Pt3 -79.30(7) .
C2 Pt1 Pt2 Pt5 -91(3) .
C1 Pt1 Pt2 Pt5 111.2(12) .
C3 Pt1 Pt2 Pt5 -92.8(15) .
Pt3 Pt1 Pt2 Pt5 98.88(7) .
Pt4 Pt1 Pt2 Pt5 19.58(5) .
C15 Pt2 Pt3 C14 -10(4) .
C3 Pt2 Pt3 C14 -164(3) .
C4 Pt2 Pt3 C14 3(3) .
Pt1 Pt2 Pt3 C14 -174(3) .
Pt5 Pt2 Pt3 C14 110(3) .
C15 Pt2 Pt3 C1 152(3) .
C3 Pt2 Pt3 C1 -2.3(16) .
C4 Pt2 Pt3 C1 165.2(18) .
Pt1 Pt2 Pt3 C1 -11.7(11) .
Pt5 Pt2 Pt3 C1 -87.7(11) .
C15 Pt2 Pt3 C4 -13(4) .
C3 Pt2 Pt3 C4 -167.5(19) .
Pt1 Pt2 Pt3 C4 -176.9(14) .
Pt5 Pt2 Pt3 C4 107.1(14) .
C15 Pt2 Pt3 Pt1 164(3) .
C3 Pt2 Pt3 Pt1 9.4(12) .
C4 Pt2 Pt3 Pt1 176.9(14) .
Pt5 Pt2 Pt3 Pt1 -75.96(6) .
C15 Pt2 Pt3 Pt6 -101(3) .
C3 Pt2 Pt3 Pt6 104.6(12) .
C4 Pt2 Pt3 Pt6 -87.9(14) .
Pt1 Pt2 Pt3 Pt6 95.17(7) .
Pt5 Pt2 Pt3 Pt6 19.21(6) .
C2 Pt1 Pt3 C14 3(3) .
C1 Pt1 Pt3 C14 10(3) .
C3 Pt1 Pt3 C14 166(3) .
Pt2 Pt1 Pt3 C14 175(2) .
Pt4 Pt1 Pt3 C14 -84(2) .
C2 Pt1 Pt3 C1 -7(3) .
C3 Pt1 Pt3 C1 156.1(18) .
Pt2 Pt1 Pt3 C1 164.9(14) .
Pt4 Pt1 Pt3 C1 -93.5(14) .
C2 Pt1 Pt3 C4 -169(3) .
C1 Pt1 Pt3 C4 -162.4(18) .
C3 Pt1 Pt3 C4 -6.3(16) .
Pt2 Pt1 Pt3 C4 2.5(12) .
Pt4 Pt1 Pt3 C4 104.1(12) .
C2 Pt1 Pt3 Pt2 -172(2) .
C1 Pt1 Pt3 Pt2 -164.9(14) .
C3 Pt1 Pt3 Pt2 -8.8(11) .
Pt4 Pt1 Pt3 Pt2 101.62(6) .
C2 Pt1 Pt3 Pt6 106(2) .
C1 Pt1 Pt3 Pt6 113.0(14) .
C3 Pt1 Pt3 Pt6 -90.9(11) .
Pt2 Pt1 Pt3 Pt6 -82.16(6) .
Pt4 Pt1 Pt3 Pt6 19.46(6) .
C2 Pt1 Pt4 C6 -15.4(19) .
C1 Pt1 Pt4 C6 81.1(17) .
C3 Pt1 Pt4 C6 -124.3(18) .
Pt2 Pt1 Pt4 C6 -170.1(14) .
Pt3 Pt1 Pt4 C6 131.4(14) .
C2 Pt1 Pt4 C5 82.4(16) .
C1 Pt1 Pt4 C5 178.9(14) .
C3 Pt1 Pt4 C5 -26.5(15) .
Pt2 Pt1 Pt4 C5 -72.2(9) .
Pt3 Pt1 Pt4 C5 -130.8(9) .
C2 Pt1 Pt4 C7 -118.7(16) .
C1 Pt1 Pt4 C7 -22.1(14) .
C3 Pt1 Pt4 C7 132.5(15) .
Pt2 Pt1 Pt4 C7 86.7(9) .
Pt3 Pt1 Pt4 C7 28.1(9) .
C2 Pt1 Pt4 Pt5 131.8(13) .
C1 Pt1 Pt4 Pt5 -131.6(11) .
C3 Pt1 Pt4 Pt5 23.0(12) .
Pt2 Pt1 Pt4 Pt5 -22.80(6) .
Pt3 Pt1 Pt4 Pt5 -81.38(6) .
C2 Pt1 Pt4 Pt6 -169.0(13) .
C1 Pt1 Pt4 Pt6 -72.5(11) .
C3 Pt1 Pt4 Pt6 82.2(12) .
Pt2 Pt1 Pt4 Pt6 36.38(7) .
Pt3 Pt1 Pt4 Pt6 -22.20(6) .
C2 Pt1 Pt4 Pt9 140.4(14) .
C1 Pt1 Pt4 Pt9 -123.1(11) .
C3 Pt1 Pt4 Pt9 31.5(13) .
Pt2 Pt1 Pt4 Pt9 -14.3(5) .
Pt3 Pt1 Pt4 Pt9 -72.9(5) .
C6 Pt4 Pt5 C8 7(3) .
C5 Pt4 Pt5 C8 4(2) .
C7 Pt4 Pt5 C8 -176(2) .
Pt6 Pt4 Pt5 C8 -178(2) .
Pt9 Pt4 Pt5 C8 100(2) .
Pt1 Pt4 Pt5 C8 -81(2) .
C6 Pt4 Pt5 C9 -173(3) .
C5 Pt4 Pt5 C9 -175.5(16) .
C7 Pt4 Pt5 C9 4.8(15) .
Pt6 Pt4 Pt5 C9 2.5(12) .
Pt9 Pt4 Pt5 C9 -79.1(12) .
Pt1 Pt4 Pt5 C9 99.6(12) .
C6 Pt4 Pt5 C5 3(3) .
C7 Pt4 Pt5 C5 -179.7(14) .
Pt6 Pt4 Pt5 C5 178.0(11) .
Pt9 Pt4 Pt5 C5 96.4(11) .
Pt1 Pt4 Pt5 C5 -84.9(11) .
C6 Pt4 Pt5 Pt6 -175(2) .
C5 Pt4 Pt5 Pt6 -178.0(11) .
C7 Pt4 Pt5 Pt6 2.3(9) .
Pt9 Pt4 Pt5 Pt6 -81.62(7) .
Pt1 Pt4 Pt5 Pt6 97.12(7) .
C6 Pt4 Pt5 Pt8 -77(2) .
C5 Pt4 Pt5 Pt8 -79.9(11) .
C7 Pt4 Pt5 Pt8 100.3(9) .
Pt6 Pt4 Pt5 Pt8 98.04(7) .
Pt9 Pt4 Pt5 Pt8 16.42(6) .
Pt1 Pt4 Pt5 Pt8 -164.84(6) .
C6 Pt4 Pt5 Pt2 107(2) .
C5 Pt4 Pt5 Pt2 104.5(11) .
C7 Pt4 Pt5 Pt2 -75.3(9) .
Pt6 Pt4 Pt5 Pt2 -77.54(7) .
Pt9 Pt4 Pt5 Pt2 -159.16(6) .
Pt1 Pt4 Pt5 Pt2 19.59(5) .
C15 Pt2 Pt5 C8 -20(2) .
C3 Pt2 Pt5 C8 78.3(16) .
C4 Pt2 Pt5 C8 -122.7(16) .
Pt1 Pt2 Pt5 C8 128.0(10) .
Pt3 Pt2 Pt5 C8 -172.7(10) .
C15 Pt2 Pt5 C9 81(2) .
C3 Pt2 Pt5 C9 179.3(18) .
C4 Pt2 Pt5 C9 -21.8(18) .
Pt1 Pt2 Pt5 C9 -131.0(14) .
Pt3 Pt2 Pt5 C9 -71.8(14) .
C15 Pt2 Pt5 C5 -120(2) .
C3 Pt2 Pt5 C5 -21.7(15) .
C4 Pt2 Pt5 C5 137.2(16) .
Pt1 Pt2 Pt5 C5 28.0(9) .
Pt3 Pt2 Pt5 C5 87.2(9) .
C15 Pt2 Pt5 Pt6 130.6(18) .
C3 Pt2 Pt5 Pt6 -130.9(12) .
C4 Pt2 Pt5 Pt6 28.0(13) .
Pt1 Pt2 Pt5 Pt6 -81.28(6) .
Pt3 Pt2 Pt5 Pt6 -22.00(6) .
C15 Pt2 Pt5 Pt4 -170.9(18) .
C3 Pt2 Pt5 Pt4 -72.4(12) .
C4 Pt2 Pt5 Pt4 86.5(13) .
Pt1 Pt2 Pt5 Pt4 -22.79(6) .
Pt3 Pt2 Pt5 Pt4 36.50(7) .
C15 Pt2 Pt5 Pt8 80.4(19) .
C3 Pt2 Pt5 Pt8 179(100) .
C4 Pt2 Pt5 Pt8 -22.2(15) .
Pt1 Pt2 Pt5 Pt8 -131.5(8) .
Pt3 Pt2 Pt5 Pt8 -72.2(8) .
C8 Pt5 Pt6 C10 1(3) .
C9 Pt5 Pt6 C10 6(3) .
C5 Pt5 Pt6 C10 -179(3) .
Pt4 Pt5 Pt6 C10 -177(3) .
Pt8 Pt5 Pt6 C10 102(3) .
Pt2 Pt5 Pt6 C10 -75(3) .
C8 Pt5 Pt6 C9 -5(3) .
C5 Pt5 Pt6 C9 175.2(17) .
Pt4 Pt5 Pt6 C9 176.9(15) .
Pt8 Pt5 Pt6 C9 95.8(15) .
Pt2 Pt5 Pt6 C9 -80.6(15) .
C8 Pt5 Pt6 C7 176(2) .
C9 Pt5 Pt6 C7 -179.1(18) .
C5 Pt5 Pt6 C7 -3.9(12) .
Pt4 Pt5 Pt6 C7 -2.2(9) .
Pt8 Pt5 Pt6 C7 -83.3(9) .
Pt2 Pt5 Pt6 C7 100.3(9) .
C8 Pt5 Pt6 Pt4 178(2) .
C9 Pt5 Pt6 Pt4 -176.9(15) .
C5 Pt5 Pt6 Pt4 -1.7(9) .
Pt8 Pt5 Pt6 Pt4 -81.08(6) .
Pt2 Pt5 Pt6 Pt4 102.50(6) .
C8 Pt5 Pt6 Pt3 95(2) .
C9 Pt5 Pt6 Pt3 100.0(15) .
C5 Pt5 Pt6 Pt3 -84.8(9) .
Pt4 Pt5 Pt6 Pt3 -83.18(6) .
Pt8 Pt5 Pt6 Pt3 -164.27(6) .
Pt2 Pt5 Pt6 Pt3 19.31(6) .
C8 Pt5 Pt6 Pt7 -84(2) .
C9 Pt5 Pt6 Pt7 -79.2(15) .
C5 Pt5 Pt6 Pt7 96.0(9) .
Pt4 Pt5 Pt6 Pt7 97.61(6) .
Pt8 Pt5 Pt6 Pt7 16.53(6) .
Pt2 Pt5 Pt6 Pt7 -159.89(6) .
C6 Pt4 Pt6 C10 -8(3) .
C5 Pt4 Pt6 C10 179(2) .
C7 Pt4 Pt6 C10 0(2) .
Pt5 Pt4 Pt6 C10 178(2) .
Pt9 Pt4 Pt6 C10 -86(2) .
Pt1 Pt4 Pt6 C10 101(2) .
C6 Pt4 Pt6 C9 172(3) .
C5 Pt4 Pt6 C9 -0.9(15) .
C7 Pt4 Pt6 C9 -179.7(16) .
Pt5 Pt4 Pt6 C9 -2.4(12) .
Pt9 Pt4 Pt6 C9 94.1(12) .
Pt1 Pt4 Pt6 C9 -79.3(12) .
C6 Pt4 Pt6 C7 -8(3) .
C5 Pt4 Pt6 C7 178.8(13) .
Pt5 Pt4 Pt6 C7 177.3(11) .
Pt9 Pt4 Pt6 C7 -86.2(11) .
Pt1 Pt4 Pt6 C7 100.4(11) .
C6 Pt4 Pt6 Pt5 174(3) .
C5 Pt4 Pt6 Pt5 1.6(8) .
C7 Pt4 Pt6 Pt5 -177.3(11) .
Pt9 Pt4 Pt6 Pt5 96.54(6) .
Pt1 Pt4 Pt6 Pt5 -76.87(6) .
C6 Pt4 Pt6 Pt3 -89(3) .
C5 Pt4 Pt6 Pt3 98.0(8) .
C7 Pt4 Pt6 Pt3 -80.8(11) .
Pt5 Pt4 Pt6 Pt3 96.42(6) .
Pt9 Pt4 Pt6 Pt3 -167.04(6) .
Pt1 Pt4 Pt6 Pt3 19.54(5) .
C6 Pt4 Pt6 Pt7 94(3) .
C5 Pt4 Pt6 Pt7 -78.7(8) .
C7 Pt4 Pt6 Pt7 102.4(11) .
Pt5 Pt4 Pt6 Pt7 -80.33(6) .
Pt9 Pt4 Pt6 Pt7 16.21(6) .
Pt1 Pt4 Pt6 Pt7 -157.20(6) .
C14 Pt3 Pt6 C10 -20.9(18) .
C1 Pt3 Pt6 C10 -123.1(17) .
C4 Pt3 Pt6 C10 81.9(17) .
Pt2 Pt3 Pt6 C10 131.5(12) .
Pt1 Pt3 Pt6 C10 -169.1(12) .
C14 Pt3 Pt6 C9 -126.9(19) .
C1 Pt3 Pt6 C9 130.9(18) .
C4 Pt3 Pt6 C9 -24.1(18) .
Pt2 Pt3 Pt6 C9 25.4(13) .
Pt1 Pt3 Pt6 C9 84.8(13) .
C14 Pt3 Pt6 C7 75.6(16) .
C1 Pt3 Pt6 C7 -26.6(15) .
C4 Pt3 Pt6 C7 178.4(15) .
Pt2 Pt3 Pt6 C7 -132.0(9) .
Pt1 Pt3 Pt6 C7 -72.6(9) .
C14 Pt3 Pt6 Pt5 -174.8(13) .
C1 Pt3 Pt6 Pt5 83.1(12) .
C4 Pt3 Pt6 Pt5 -71.9(12) .
Pt2 Pt3 Pt6 Pt5 -22.41(7) .
Pt1 Pt3 Pt6 Pt5 36.99(7) .
C14 Pt3 Pt6 Pt4 125.7(13) .
C1 Pt3 Pt6 Pt4 23.5(12) .
C4 Pt3 Pt6 Pt4 -131.5(12) .
Pt2 Pt3 Pt6 Pt4 -81.99(7) .
Pt1 Pt3 Pt6 Pt4 -22.58(7) .
C14 Pt3 Pt6 Pt7 -161.3(17) .
C1 Pt3 Pt6 Pt7 96.5(17) .
C4 Pt3 Pt6 Pt7 -58.5(17) .
Pt2 Pt3 Pt6 Pt7 -9.0(12) .
Pt1 Pt3 Pt6 Pt7 50.4(12) .
C10 Pt6 Pt7 C12 -24.0(18) .
C9 Pt6 Pt7 C12 81.5(19) .
C7 Pt6 Pt7 C12 -121.2(16) .
Pt5 Pt6 Pt7 C12 129.8(13) .
Pt4 Pt6 Pt7 C12 -170.9(13) .
Pt3 Pt6 Pt7 C12 116.3(17) .
C10 Pt6 Pt7 C18 79.0(19) .
C9 Pt6 Pt7 C18 -175.4(19) .
C7 Pt6 Pt7 C18 -18.1(17) .
Pt5 Pt6 Pt7 C18 -127.1(14) .
Pt4 Pt6 Pt7 C18 -67.8(14) .
Pt3 Pt6 Pt7 C18 -140.6(18) .
C10 Pt6 Pt7 C11 -126.5(17) .
C9 Pt6 Pt7 C11 -20.9(17) .
C7 Pt6 Pt7 C11 136.4(15) .
Pt5 Pt6 Pt7 C11 27.3(11) .
Pt4 Pt6 Pt7 C11 86.6(11) .
Pt3 Pt6 Pt7 C11 13.8(17) .
C10 Pt6 Pt7 Pt9 128.1(12) .
C9 Pt6 Pt7 Pt9 -126.3(13) .
C7 Pt6 Pt7 Pt9 31.0(9) .
Pt5 Pt6 Pt7 Pt9 -78.01(7) .
Pt4 Pt6 Pt7 Pt9 -18.71(6) .
Pt3 Pt6 Pt7 Pt9 -91.5(12) .
C10 Pt6 Pt7 Pt8 -172.8(12) .
C9 Pt6 Pt7 Pt8 -67.3(13) .
C7 Pt6 Pt7 Pt8 90.0(9) .
Pt5 Pt6 Pt7 Pt8 -19.00(7) .
Pt4 Pt6 Pt7 Pt8 40.30(7) .
Pt3 Pt6 Pt7 Pt8 -32.5(12) .
C12 Pt7 Pt8 C17 5(5) .
C18 Pt7 Pt8 C17 -167(4) .
C11 Pt7 Pt8 C17 -6(4) .
Pt9 Pt7 Pt8 C17 -175(4) .
Pt6 Pt7 Pt8 C17 104(4) .
C12 Pt7 Pt8 C11 11(3) .
C18 Pt7 Pt8 C11 -161(2) .
Pt9 Pt7 Pt8 C11 -169.1(14) .
Pt6 Pt7 Pt8 C11 109.7(14) .
C12 Pt7 Pt8 C13 176(3) .
C18 Pt7 Pt8 C13 3.5(18) .
C11 Pt7 Pt8 C13 164.5(18) .
Pt9 Pt7 Pt8 C13 -4.7(11) .
Pt6 Pt7 Pt8 C13 -85.9(11) .
C12 Pt7 Pt8 Pt9 -180(2) .
C18 Pt7 Pt8 Pt9 8.2(15) .
C11 Pt7 Pt8 Pt9 169.1(14) .
Pt6 Pt7 Pt8 Pt9 -81.17(6) .
C12 Pt7 Pt8 Pt5 -82(2) .
C18 Pt7 Pt8 Pt5 105.9(15) .
C11 Pt7 Pt8 Pt5 -93.2(14) .
Pt9 Pt7 Pt8 Pt5 97.67(6) .
Pt6 Pt7 Pt8 Pt5 16.50(6) .
C8 Pt5 Pt8 C17 -22(2) .
C9 Pt5 Pt8 C17 -123(2) .
C5 Pt5 Pt8 C17 78(2) .
Pt6 Pt5 Pt8 C17 -172.3(18) .
Pt4 Pt5 Pt8 C17 128.3(18) .
Pt2 Pt5 Pt8 C17 -122(2) .
C8 Pt5 Pt8 C11 80.5(16) .
C9 Pt5 Pt8 C11 -20.4(18) .
C5 Pt5 Pt8 C11 -179.8(15) .
Pt6 Pt5 Pt8 C11 -69.8(12) .
Pt4 Pt5 Pt8 C11 -129.1(12) .
Pt2 Pt5 Pt8 C11 -19.9(14) .
C8 Pt5 Pt8 C13 -120.9(16) .
C9 Pt5 Pt8 C13 138.2(18) .
C5 Pt5 Pt8 C13 -21.2(15) .
Pt6 Pt5 Pt8 C13 88.8(12) .
Pt4 Pt5 Pt8 C13 29.4(12) .
Pt2 Pt5 Pt8 C13 138.6(14) .
C8 Pt5 Pt8 Pt9 -169.4(11) .
C9 Pt5 Pt8 Pt9 89.7(13) .
C5 Pt5 Pt8 Pt9 -69.7(9) .
Pt6 Pt5 Pt8 Pt9 40.32(7) .
Pt4 Pt5 Pt8 Pt9 -19.02(6) .
Pt2 Pt5 Pt8 Pt9 90.2(8) .
C8 Pt5 Pt8 Pt7 131.4(11) .
C9 Pt5 Pt8 Pt7 30.5(13) .
C5 Pt5 Pt8 Pt7 -128.9(9) .
Pt6 Pt5 Pt8 Pt7 -18.92(6) .
Pt4 Pt5 Pt8 Pt7 -78.26(6) .
Pt2 Pt5 Pt8 Pt7 30.9(8) .
C17 Pt8 Pt9 C16 0(4) .
C11 Pt8 Pt9 C16 -167(3) .
C13 Pt8 Pt9 C16 -2(3) .
Pt7 Pt8 Pt9 C16 -176(3) .
Pt5 Pt8 Pt9 C16 104(3) .
C17 Pt8 Pt9 C13 2(3) .
C11 Pt8 Pt9 C13 -165.2(18) .
Pt7 Pt8 Pt9 C13 -174.1(14) .
Pt5 Pt8 Pt9 C13 105.9(14) .
C17 Pt8 Pt9 C18 168(4) .
C11 Pt8 Pt9 C18 0.5(19) .
C13 Pt8 Pt9 C18 166(2) .
Pt7 Pt8 Pt9 C18 -8.5(15) .
Pt5 Pt8 Pt9 C18 -88.5(15) .
C17 Pt8 Pt9 Pt7 176(3) .
C11 Pt8 Pt9 Pt7 9.0(12) .
C13 Pt8 Pt9 Pt7 174.1(14) .
Pt5 Pt8 Pt9 Pt7 -79.97(7) .
C17 Pt8 Pt9 Pt4 -87(3) .
C11 Pt8 Pt9 Pt4 105.4(12) .
C13 Pt8 Pt9 Pt4 -89.4(14) .
Pt7 Pt8 Pt9 Pt4 96.45(7) .
Pt5 Pt8 Pt9 Pt4 16.49(6) .
C12 Pt7 Pt9 C16 -5(4) .
C18 Pt7 Pt9 C16 6(3) .
C11 Pt7 Pt9 C16 168(3) .
Pt8 Pt7 Pt9 C16 176(3) .
Pt6 Pt7 Pt9 C16 -86(3) .
C12 Pt7 Pt9 C13 -176(3) .
C18 Pt7 Pt9 C13 -165(2) .
C11 Pt7 Pt9 C13 -3.6(16) .
Pt8 Pt7 Pt9 C13 4.7(11) .
Pt6 Pt7 Pt9 C13 102.9(11) .
C12 Pt7 Pt9 C18 -11(3) .
C11 Pt7 Pt9 C18 161(2) .
Pt8 Pt7 Pt9 C18 169.6(19) .
Pt6 Pt7 Pt9 C18 -92.2(19) .
C12 Pt7 Pt9 Pt8 179(3) .
C18 Pt7 Pt9 Pt8 -169.6(19) .
C11 Pt7 Pt9 Pt8 -8.3(11) .
Pt6 Pt7 Pt9 Pt8 98.17(7) .
C12 Pt7 Pt9 Pt4 98(3) .
C18 Pt7 Pt9 Pt4 108.4(19) .
C11 Pt7 Pt9 Pt4 -90.2(11) .
Pt8 Pt7 Pt9 Pt4 -81.95(7) .
Pt6 Pt7 Pt9 Pt4 16.22(5) .
C6 Pt4 Pt9 C16 -20(2) .
C5 Pt4 Pt9 C16 -119.1(17) .
C7 Pt4 Pt9 C16 82.0(17) .
Pt5 Pt4 Pt9 C16 -167.6(15) .
Pt6 Pt4 Pt9 C16 133.0(15) .
Pt1 Pt4 Pt9 C16 -175.9(15) .
C6 Pt4 Pt9 C13 79.3(17) .
C5 Pt4 Pt9 C13 -19.9(14) .
C7 Pt4 Pt9 C13 -178.8(14) .
Pt5 Pt4 Pt9 C13 -68.4(11) .
Pt6 Pt4 Pt9 C13 -127.8(11) .
Pt1 Pt4 Pt9 C13 -76.7(12) .
C6 Pt4 Pt9 C18 -122(2) .
C5 Pt4 Pt9 C18 138.8(18) .
C7 Pt4 Pt9 C18 -20.1(18) .
Pt5 Pt4 Pt9 C18 90.3(16) .
Pt6 Pt4 Pt9 C18 30.9(16) .
Pt1 Pt4 Pt9 C18 82.0(16) .
C6 Pt4 Pt9 Pt8 128.7(13) .
C5 Pt4 Pt9 Pt8 29.5(9) .
C7 Pt4 Pt9 Pt8 -129.4(9) .
Pt5 Pt4 Pt9 Pt8 -18.98(6) .
Pt6 Pt4 Pt9 Pt8 -78.37(7) .
Pt1 Pt4 Pt9 Pt8 -27.3(5) .
C6 Pt4 Pt9 Pt7 -171.5(13) .
C5 Pt4 Pt9 Pt7 89.3(9) .
C7 Pt4 Pt9 Pt7 -69.7(9) .
Pt5 Pt4 Pt9 Pt7 40.80(7) .
Pt6 Pt4 Pt9 Pt7 -18.60(6) .
Pt1 Pt4 Pt9 Pt7 32.4(5) .
C2 Pt1 C1 O1 -17(6) .
C3 Pt1 C1 O1 119(5) .
Pt2 Pt1 C1 O1 153(5) .
Pt3 Pt1 C1 O1 167(6) .
Pt4 Pt1 C1 O1 -110(5) .
C2 Pt1 C1 Pt3 176.3(15) .
C3 Pt1 C1 Pt3 -48(3) .
Pt2 Pt1 C1 Pt3 -13.8(13) .
Pt4 Pt1 C1 Pt3 83.5(9) .
C14 Pt3 C1 O1 16(5) .
C4 Pt3 C1 O1 -130(4) .
Pt2 Pt3 C1 O1 -155(4) .
Pt1 Pt3 C1 O1 -169(5) .
Pt6 Pt3 C1 O1 116(4) .
C14 Pt3 C1 Pt1 -174.6(15) .
C4 Pt3 C1 Pt1 39(4) .
Pt2 Pt3 C1 Pt1 13.6(13) .
Pt6 Pt3 C1 Pt1 -75.2(11) .
C1 Pt1 C2 O2 29(38) .
C3 Pt1 C2 O2 -129(38) .
Pt2 Pt1 C2 O2 -130(36) .
Pt3 Pt1 C2 O2 34(39) .
Pt4 Pt1 C2 O2 118(38) .
C15 Pt2 C3 O3 6(5) .
C4 Pt2 C3 O3 147(4) .
Pt1 Pt2 C3 O3 -176(6) .
Pt3 Pt2 C3 O3 173(4) .
Pt5 Pt2 C3 O3 -97(5) .
C15 Pt2 C3 Pt1 -177.5(19) .
C4 Pt2 C3 Pt1 -36(5) .
Pt3 Pt2 C3 Pt1 -10.8(13) .
Pt5 Pt2 C3 Pt1 79.7(10) .
C2 Pt1 C3 O3 -3(5) .
C1 Pt1 C3 O3 -137(4) .
Pt2 Pt1 C3 O3 177(5) .
Pt3 Pt1 C3 O3 -173(4) .
Pt4 Pt1 C3 O3 97(4) .
C2 Pt1 C3 Pt2 -179.2(15) .
C1 Pt1 C3 Pt2 47(3) .
Pt3 Pt1 C3 Pt2 10.5(13) .
Pt4 Pt1 C3 Pt2 -79.4(12) .
C15 Pt2 C4 O4 -8(6) .
C3 Pt2 C4 O4 -149(5) .
Pt1 Pt2 C4 O4 -178(5) .
Pt3 Pt2 C4 O4 179(6) .
Pt5 Pt2 C4 O4 99(5) .
C15 Pt2 C4 Pt3 173.1(19) .
C3 Pt2 C4 Pt3 32(5) .
Pt1 Pt2 C4 Pt3 2.9(13) .
Pt5 Pt2 C4 Pt3 -80.6(10) .
C14 Pt3 C4 O4 2(5) .
C1 Pt3 C4 O4 148(4) .
Pt2 Pt3 C4 O4 -179(6) .
Pt1 Pt3 C4 O4 178(5) .
Pt6 Pt3 C4 O4 -93(5) .
C14 Pt3 C4 Pt2 -178.6(14) .
C1 Pt3 C4 Pt2 -32(4) .
Pt1 Pt3 C4 Pt2 -2.8(13) .
Pt6 Pt3 C4 Pt2 86.7(10) .
C8 Pt5 C5 O5 -1(4) .
C9 Pt5 C5 O5 -171(4) .
Pt6 Pt5 C5 O5 179(4) .
Pt4 Pt5 C5 O5 177(4) .
Pt8 Pt5 C5 O5 -91(4) .
Pt2 Pt5 C5 O5 91(4) .
C8 Pt5 C5 Pt4 -178.1(12) .
C9 Pt5 C5 Pt4 12(4) .
Pt6 Pt5 C5 Pt4 1.9(10) .
Pt8 Pt5 C5 Pt4 92.1(7) .
Pt2 Pt5 C5 Pt4 -86.3(7) .
C6 Pt4 C5 O5 4(4) .
C7 Pt4 C5 O5 -177(3) .
Pt5 Pt4 C5 O5 -178(4) .
Pt6 Pt4 C5 O5 -179(3) .
Pt9 Pt4 C5 O5 95(3) .
Pt1 Pt4 C5 O5 -93(3) .
C6 Pt4 C5 Pt5 -178.4(14) .
C7 Pt4 C5 Pt5 1(4) .
Pt6 Pt4 C5 Pt5 -1.8(10) .
Pt9 Pt4 C5 Pt5 -87.8(7) .
Pt1 Pt4 C5 Pt5 85.0(7) .
C5 Pt4 C6 O6 95(41) .
C7 Pt4 C6 O6 -84(41) .
Pt5 Pt4 C6 O6 93(41) .
Pt6 Pt4 C6 O6 -78(41) .
Pt9 Pt4 C6 O6 -1(41) .
Pt1 Pt4 C6 O6 175(41) .
C6 Pt4 C7 O7 -5(4) .
C5 Pt4 C7 O7 176(3) .
Pt5 Pt4 C7 O7 176(4) .
Pt6 Pt4 C7 O7 179(5) .
Pt9 Pt4 C7 O7 -93(4) .
Pt1 Pt4 C7 O7 95(4) .
C6 Pt4 C7 Pt6 176.0(14) .
C5 Pt4 C7 Pt6 -3(4) .
Pt5 Pt4 C7 Pt6 -2.5(10) .
Pt9 Pt4 C7 Pt6 87.8(7) .
Pt1 Pt4 C7 Pt6 -83.8(7) .
C10 Pt6 C7 O7 1(4) .
C9 Pt6 C7 O7 -178(4) .
Pt5 Pt6 C7 O7 -176(4) .
Pt4 Pt6 C7 O7 -179(5) .
Pt3 Pt6 C7 O7 -86(4) .
Pt7 Pt6 C7 O7 97(4) .
C10 Pt6 C7 Pt4 -179.7(13) .
C9 Pt6 C7 Pt4 1(4) .
Pt5 Pt6 C7 Pt4 2.5(10) .
Pt3 Pt6 C7 Pt4 92.7(7) .
Pt7 Pt6 C7 Pt4 -84.4(7) .
C9 Pt5 C8 O8 177(21) .
C5 Pt5 C8 O8 1(22) .
Pt6 Pt5 C8 O8 -179(100) .
Pt4 Pt5 C8 O8 -2(23) .
Pt8 Pt5 C8 O8 80(22) .
Pt2 Pt5 C8 O8 -105(22) .
C8 Pt5 C9 O9 -1(6) .
C5 Pt5 C9 O9 169(4) .
Pt6 Pt5 C9 O9 -178(6) .
Pt4 Pt5 C9 O9 179(5) .
Pt8 Pt5 C9 O9 92(5) .
Pt2 Pt5 C9 O9 -88(5) .
C8 Pt5 C9 Pt6 177.5(13) .
C5 Pt5 C9 Pt6 -13(5) .
Pt4 Pt5 C9 Pt6 -2.9(14) .
Pt8 Pt5 C9 Pt6 -89.4(10) .
Pt2 Pt5 C9 Pt6 90.7(10) .
C10 Pt6 C9 O9 1(5) .
C7 Pt6 C9 O9 -179(3) .
Pt5 Pt6 C9 O9 178(6) .
Pt4 Pt6 C9 O9 -179(4) .
Pt3 Pt6 C9 O9 93(5) .
Pt7 Pt6 C9 O9 -89(5) .
C10 Pt6 C9 Pt5 -177.2(14) .
C7 Pt6 C9 Pt5 2(4) .
Pt4 Pt6 C9 Pt5 2.9(14) .
Pt3 Pt6 C9 Pt5 -85.9(11) .
Pt7 Pt6 C9 Pt5 92.2(11) .
C9 Pt6 C10 O10 -5(34) .
C7 Pt6 C10 O10 175(33) .
Pt5 Pt6 C10 O10 -10(36) .
Pt4 Pt6 C10 O10 174(32) .
Pt3 Pt6 C10 O10 -105(33) .
Pt7 Pt6 C10 O10 73(33) .
C17 Pt8 C11 O11 -7(7) .
C13 Pt8 C11 O11 137(6) .
Pt9 Pt8 C11 O11 165(6) .
Pt7 Pt8 C11 O11 175(7) .
Pt5 Pt8 C11 O11 -102(7) .
C17 Pt8 C11 Pt7 177.2(19) .
C13 Pt8 C11 Pt7 -38(4) .
Pt9 Pt8 C11 Pt7 -10.0(13) .
Pt5 Pt8 C11 Pt7 82.5(9) .
C12 Pt7 C11 O11 9(4) .
C18 Pt7 C11 O11 -138(4) .
Pt9 Pt7 C11 O11 -167(4) .
Pt8 Pt7 C11 O11 -177(5) .
Pt6 Pt7 C11 O11 104(4) .
C12 Pt7 C11 Pt8 -174.0(14) .
C18 Pt7 C11 Pt8 39(4) .
Pt9 Pt7 C11 Pt8 9.8(13) .
Pt6 Pt7 C11 Pt8 -79.5(11) .
C18 Pt7 C12 O12 166(55) .
C11 Pt7 C12 O12 2(55) .
Pt9 Pt7 C12 O12 174(53) .
Pt8 Pt7 C12 O12 -7(57) .
Pt6 Pt7 C12 O12 -106(55) .
C16 Pt9 C13 O13 3(5) .
C18 Pt9 C13 O13 149(5) .
Pt8 Pt9 C13 O13 -176(5) .
Pt7 Pt9 C13 O13 179(4) .
Pt4 Pt9 C13 O13 -90(4) .
C16 Pt9 C13 Pt8 178.9(15) .
C18 Pt9 C13 Pt8 -35(5) .
Pt7 Pt9 C13 Pt8 -5.4(13) .
Pt4 Pt9 C13 Pt8 86.1(9) .
C17 Pt8 C13 O13 -3(5) .
C11 Pt8 C13 O13 -149(4) .
Pt9 Pt8 C13 O13 176(5) .
Pt7 Pt8 C13 O13 -179(4) .
Pt5 Pt8 C13 O13 94(5) .
C17 Pt8 C13 Pt9 -178.9(19) .
C11 Pt8 C13 Pt9 36(4) .
Pt7 Pt8 C13 Pt9 5.4(13) .
Pt5 Pt8 C13 Pt9 -81.7(10) .
C1 Pt3 C14 O14 38(61) .
C4 Pt3 C14 O14 -157(60) .
Pt2 Pt3 C14 O14 -160(59) .
Pt1 Pt3 C14 O14 30(62) .
Pt6 Pt3 C14 O14 -72(61) .
C3 Pt2 C15 O15 162(21) .
C4 Pt2 C15 O15 -3(21) .
Pt1 Pt2 C15 O15 159(18) .
Pt3 Pt2 C15 O15 7(24) .
Pt5 Pt2 C15 O15 -111(21) .
C13 Pt9 C16 O16 103(60) .
C18 Pt9 C16 O16 -64(60) .
Pt8 Pt9 C16 O16 104(60) .
Pt7 Pt9 C16 O16 -69(61) .
Pt4 Pt9 C16 O16 -171(60) .
C11 Pt8 C17 O17 48(35) .
C13 Pt8 C17 O17 -119(35) .
Pt9 Pt8 C17 O17 -120(34) .
Pt7 Pt8 C17 O17 52(37) .
Pt5 Pt8 C17 O17 137(35) .
C16 Pt9 C18 O18 4(7) .
C13 Pt9 C18 O18 -142(5) .
Pt8 Pt9 C18 O18 -170(6) .
Pt7 Pt9 C18 O18 -179(8) .
Pt4 Pt9 C18 O18 100(6) .
C16 Pt9 C18 Pt7 -176.9(16) .
C13 Pt9 C18 Pt7 37(5) .
Pt8 Pt9 C18 Pt7 9.6(17) .
Pt4 Pt9 C18 Pt7 -80.2(13) .
C12 Pt7 C18 O18 -6(7) .
C11 Pt7 C18 O18 141(6) .
Pt9 Pt7 C18 O18 179(8) .
Pt8 Pt7 C18 O18 170(6) .
Pt6 Pt7 C18 O18 -96(7) .
C12 Pt7 C18 Pt9 174.8(15) .
C11 Pt7 C18 Pt9 -39(4) .
Pt8 Pt7 C18 Pt9 -9.4(17) .
Pt6 Pt7 C18 Pt9 84.5(12) .
P2 Pt10 P1 C107 141.6(9) .
P2 Pt10 P1 C107 -38.4(9) 2_567
P1 Pt10 P1 C107 -179(13) 2_567
P2 Pt10 P1 C113 -90.8(10) .
P2 Pt10 P1 C113 89.2(10) 2_567
P1 Pt10 P1 C113 -51(13) 2_567
P2 Pt10 P1 C101 23.4(8) .
P2 Pt10 P1 C101 -156.6(8) 2_567
P1 Pt10 P1 C101 63(13) 2_567
P2 Pt10 P2 C125 71(100) 2_567
P1 Pt10 P2 C125 -137.8(12) .
P1 Pt10 P2 C125 42.2(12) 2_567
P2 Pt10 P2 C119 -61(100) 2_567
P1 Pt10 P2 C119 89.9(10) .
P1 Pt10 P2 C119 -90.1(10) 2_567
P2 Pt10 P2 C106 -175(100) 2_567
P1 Pt10 P2 C106 -23.5(8) .
P1 Pt10 P2 C106 156.5(8) 2_567
C107 P1 C101 C102 34.6(16) .
C113 P1 C101 C102 -78.6(15) .
Pt10 P1 C101 C102 160.5(10) .
C107 P1 C101 C106 -145.4(13) .
C113 P1 C101 C106 101.3(14) .
Pt10 P1 C101 C106 -19.5(13) .
C106 C101 C102 C103 0.0 .
P1 C101 C102 C103 179.9(17) .
C101 C102 C103 C104 0.0 .
C102 C103 C104 C105 0.0 .
C103 C104 C105 C106 0.0 .
C104 C105 C106 C101 0.0 .
C104 C105 C106 P2 -179.7(17) .
C102 C101 C106 C105 0.0 .
P1 C101 C106 C105 -179.9(17) .
C102 C101 C106 P2 179.8(16) .
P1 C101 C106 P2 -0.2(15) .
C125 P2 C106 C105 -34.4(17) .
C119 P2 C106 C105 80.3(15) .
Pt10 P2 C106 C105 -160.4(11) .
C125 P2 C106 C101 145.8(14) .
C119 P2 C106 C101 -99.4(13) .
Pt10 P2 C106 C101 19.8(12) .
C113 P1 C107 C108 152.0(13) .
C101 P1 C107 C108 41.4(15) .
Pt10 P1 C107 C108 -77.6(13) .
C113 P1 C107 C112 -29.8(16) .
C101 P1 C107 C112 -140.4(13) .
Pt10 P1 C107 C112 100.6(12) .
C112 C107 C108 C109 0.0 .
P1 C107 C108 C109 178.2(16) .
C107 C108 C109 C110 0.0 .
C108 C109 C110 C111 0.0 .
C109 C110 C111 C112 0.0 .
C110 C111 C112 C107 0.0 .
C108 C107 C112 C111 0.0 .
P1 C107 C112 C111 -178.2(16) .
C107 P1 C113 C114 -45.2(16) .
C101 P1 C113 C114 66.3(15) .
Pt10 P1 C113 C114 -177.7(10) .
C107 P1 C113 C118 138.3(14) .
C101 P1 C113 C118 -110.2(15) .
Pt10 P1 C113 C118 5.8(16) .
C118 C113 C114 C115 0.0 .
P1 C113 C114 C115 -176.5(18) .
C113 C114 C115 C116 0.0 .
C114 C115 C116 C117 0.0 .
C115 C116 C117 C118 0.0 .
C116 C117 C118 C113 0.0 .
C114 C113 C118 C117 0.0 .
P1 C113 C118 C117 176.5(19) .
C125 P2 C119 C120 66.1(18) .
C106 P2 C119 C120 -41.9(16) .
Pt10 P2 C119 C120 -157.4(11) .
C125 P2 C119 C124 -113.9(16) .
C106 P2 C119 C124 138.1(13) .
Pt10 P2 C119 C124 22.6(16) .
C124 C119 C120 C121 0.0 .
P2 C119 C120 C121 180.0(19) .
C119 C120 C121 C122 0.0 .
C120 C121 C122 C123 0.0 .
C121 C122 C123 C124 0.0 .
C122 C123 C124 C119 0.0 .
C120 C119 C124 C123 0.0 .
P2 C119 C124 C123 -180.0(19) .
C119 P2 C125 C126 -0.6(19) .
C106 P2 C125 C126 109.0(15) .
Pt10 P2 C125 C126 -133.6(13) .
C119 P2 C125 C130 175.0(14) .
C106 P2 C125 C130 -75.4(17) .
Pt10 P2 C125 C130 42.0(19) .
C130 C125 C126 C127 0.0 .
P2 C125 C126 C127 176(2) .
C125 C126 C127 C128 0.0 .
C126 C127 C128 C129 0.0 .
C127 C128 C129 C130 0.0 .
C128 C129 C130 C125 0.0 .
C126 C125 C130 C129 0.0 .
P2 C125 C130 C129 -175(2) .
P4 Pt11 P3 C313 -134.9(9) .
P4 Pt11 P3 C313 45.1(9) 2_675
P3 Pt11 P3 C313 10(100) 2_675
P4 Pt11 P3 C307 95.8(9) .
P4 Pt11 P3 C307 -84.2(9) 2_675
P3 Pt11 P3 C307 -119(100) 2_675
P4 Pt11 P3 C301 -19.8(8) .
P4 Pt11 P3 C301 160.2(8) 2_675
P3 Pt11 P3 C301 125(100) 2_675
P4 Pt11 P4 C319 -158(5) 2_675
P3 Pt11 P4 C319 82.8(8) 2_675
P3 Pt11 P4 C319 -97.2(8) .
P4 Pt11 P4 C325 72(6) 2_675
P3 Pt11 P4 C325 -46.4(11) 2_675
P3 Pt11 P4 C325 133.6(11) .
P4 Pt11 P4 C306 -40(5) 2_675
P3 Pt11 P4 C306 -158.4(7) 2_675
P3 Pt11 P4 C306 21.6(7) .
C313 P3 C301 C302 -42.8(15) .
C307 P3 C301 C302 68.8(14) .
Pt11 P3 C301 C302 -168.2(9) .
C313 P3 C301 C306 138.5(11) .
C307 P3 C301 C306 -109.9(12) .
Pt11 P3 C301 C306 13.1(11) .
C306 C301 C302 C303 0.0 .
P3 C301 C302 C303 -178.6(15) .
C301 C302 C303 C304 0.0 .
C302 C303 C304 C305 0.0 .
C303 C304 C305 C306 0.0 .
C304 C305 C306 C301 0.0 .
C304 C305 C306 P4 172.8(15) .
C302 C301 C306 C305 0.0 .
P3 C301 C306 C305 178.7(14) .
C302 C301 C306 P4 -172.9(15) .
P3 C301 C306 P4 5.8(13) .
C319 P4 C306 C305 -72.0(13) .
C325 P4 C306 C305 41.5(15) .
Pt11 P4 C306 C305 165.3(9) .
C319 P4 C306 C301 100.8(12) .
C325 P4 C306 C301 -145.7(12) .
Pt11 P4 C306 C301 -21.8(11) .
C313 P3 C307 C308 43.3(16) .
C301 P3 C307 C308 -64.1(15) .
Pt11 P3 C307 C308 177.6(11) .
C313 P3 C307 C312 -140.7(14) .
C301 P3 C307 C312 111.8(14) .
Pt11 P3 C307 C312 -6.4(15) .
C312 C307 C308 C309 0.0 .
P3 C307 C308 C309 175.9(18) .
C307 C308 C309 C310 0.0 .
C308 C309 C310 C311 0.0 .
C309 C310 C311 C312 0.0 .
C310 C311 C312 C307 0.0 .
C308 C307 C312 C311 0.0 .
P3 C307 C312 C311 -176.1(17) .
C307 P3 C313 C314 -153.7(13) .
C301 P3 C313 C314 -45.1(15) .
Pt11 P3 C313 C314 73.4(14) .
C307 P3 C313 C318 27.7(17) .
C301 P3 C313 C318 136.3(13) .
Pt11 P3 C313 C318 -105.2(13) .
C318 C313 C314 C315 0.0 .
P3 C313 C314 C315 -178.6(17) .
C313 C314 C315 C316 0.0 .
C314 C315 C316 C317 0.0 .
C315 C316 C317 C318 0.0 .
C316 C317 C318 C313 0.0 .
C314 C313 C318 C317 0.0 .
P3 C313 C318 C317 178.6(18) .
C325 P4 C319 C320 -54.4(15) .
C306 P4 C319 C320 53.8(13) .
Pt11 P4 C319 C320 171.5(9) .
C325 P4 C319 C324 123.3(13) .
C306 P4 C319 C324 -128.5(11) .
Pt11 P4 C319 C324 -10.8(13) .
C324 C319 C320 C321 0.0 .
P4 C319 C320 C321 177.6(15) .
C319 C320 C321 C322 0.0 .
C320 C321 C322 C323 0.0 .
C321 C322 C323 C324 0.0 .
C322 C323 C324 C319 0.0 .
C320 C319 C324 C323 0.0 .
P4 C319 C324 C323 -177.7(15) .
C319 P4 C325 C326 172.1(13) .
C306 P4 C325 C326 58.9(15) .
Pt11 P4 C325 C326 -56.1(15) .
C319 P4 C325 C330 -13.9(18) .
C306 P4 C325 C330 -127.1(15) .
Pt11 P4 C325 C330 117.9(14) .
C330 C325 C326 C327 0.0 .
P4 C325 C326 C327 174.2(19) .
C325 C326 C327 C328 0.0 .
C326 C327 C328 C329 0.0 .
C327 C328 C329 C330 0.0 .
C328 C329 C330 C325 0.0 .
C326 C325 C330 C329 0.0 .
P4 C325 C330 C329 -174(2) .
