#------------------------------------------------------------------------------
#$Date: 2015-09-06 03:22:01 +0300 (Sun, 06 Sep 2015) $
#$Revision: 154740 $
#$URL: svn://www.crystallography.net/cod/cif/4/08/61/4086181.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4086181
loop_
_publ_author_name
'DeMott, Jessica C.'
'Gu, Weixing'
'McCulloch, Billy J.'
'Herbert, David E.'
'Goshert, Mitchell D.'
'Walensky, Justin R.'
'Zhou, Jia'
'Ozerov, Oleg V.'
_publ_section_title
;
 Silyl--Silylene Interplay in Cationic PSiP Pincer Complexes of Platinum
;
_journal_issue                   16
_journal_name_full               Organometallics
_journal_page_first              3930
_journal_paper_doi               10.1021/acs.organomet.5b00596
_journal_volume                  34
_journal_year                    2015
_chemical_formula_moiety         'C50 H74 B22 Cl22 O P4 Pt2 Si2, 5(C6 H4 F2)'
_chemical_formula_sum            'C80 H94 B22 Cl22 F10 O P4 Pt2 Si2'
_chemical_formula_weight         2849.51
_chemical_name_systematic
;
 ?
;
_space_group_crystal_system      monoclinic
_space_group_IT_number           15
_space_group_name_Hall           '-C 2yc'
_space_group_name_H-M_alt        'C 1 2/c 1'
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-2013
_cell_angle_alpha                90
_cell_angle_beta                 111.822(4)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   29.543(6)
_cell_length_b                   16.580(3)
_cell_length_c                   25.060(4)
_cell_measurement_reflns_used    9943
_cell_measurement_temperature    110(2)
_cell_measurement_theta_max      22.69
_cell_measurement_theta_min      2.41
_cell_volume                     11395(4)
_computing_cell_refinement       'Apex2 v2013.2-0 (Bruker AXS, 2008)'
_computing_data_collection       'Apex2 v2013.2-0 (Bruker AXS, 2008)'
_computing_data_reduction        'SAINT v8.18c (Bruker AXS, 2008)'
_computing_molecular_graphics    'shelXle rev 647 (Hubschle et al, 2011)'
_computing_structure_refinement  'SHELXL-2013/4 (Sheldrick, 2013)'
_computing_structure_solution    'SHELXS-2013/4 (Sheldrick, 2013)'
_diffrn_ambient_temperature      110(2)
_diffrn_measured_fraction_theta_full 1.000
_diffrn_measured_fraction_theta_max 0.994
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.1286
_diffrn_reflns_av_unetI/netI     0.0716
_diffrn_reflns_laue_measured_fraction_full 1.000
_diffrn_reflns_laue_measured_fraction_max 0.994
_diffrn_reflns_limit_h_max       38
_diffrn_reflns_limit_h_min       -38
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_number            129301
_diffrn_reflns_point_group_measured_fraction_full 1.000
_diffrn_reflns_point_group_measured_fraction_max 0.994
_diffrn_reflns_theta_full        25.242
_diffrn_reflns_theta_max         27.557
_diffrn_reflns_theta_min         1.435
_exptl_absorpt_coefficient_mu    3.105
_exptl_absorpt_correction_T_max  0.7456
_exptl_absorpt_correction_T_min  0.5123
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'SADABS 2008/1 (Sheldrick, 2008)'
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.661
_exptl_crystal_description       sheet
_exptl_crystal_F_000             5600
_exptl_crystal_size_max          0.185
_exptl_crystal_size_mid          0.125
_exptl_crystal_size_min          0.023
_refine_diff_density_max         1.514
_refine_diff_density_min         -1.482
_refine_diff_density_rms         0.154
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.040
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     690
_refine_ls_number_reflns         13082
_refine_ls_number_restraints     108
_refine_ls_restrained_S_all      1.038
_refine_ls_R_factor_all          0.1039
_refine_ls_R_factor_gt           0.0540
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0446P)²+115.4077P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1107
_refine_ls_wR_factor_ref         0.1350
_reflns_Friedel_coverage         0.000
_reflns_number_gt                8527
_reflns_number_total             13082
_reflns_threshold_expression     'I > 2σ(I)'
_cod_data_source_file            om5b00596_si_003.cif
_cod_data_source_block           10
_cod_depositor_comments
'Adding full bibliography for 4086177--4086181.cif.'
_cod_original_cell_volume        11396(4)
_cod_database_code               4086181
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
_shelx_estimated_absorpt_t_min   0.597
_shelx_estimated_absorpt_t_max   0.932
_computing_refinement_gui        'shelXle rev 647 (Hubschle et al, 2011)'
_shelxl_version_number           2013-4
loop_
_space_group_symop_operation_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_site_symmetry_order
_atom_site_calc_flag
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
Pt1 Pt 0.05781(2) 0.24378(2) 0.38039(2) 0.02878(8) Uani 1 1 d . . . . .
Cl1 Cl 0.14813(9) -0.23549(11) 0.31845(9) 0.0589(6) Uani 1 1 d . . . . .
B1 B 0.1516(3) -0.1622(4) 0.3707(4) 0.038(2) Uani 1 1 d . . . . .
C1 C 0.1836(3) -0.1793(4) 0.4425(3) 0.048(2) Uani 1 1 d . . . . .
H1 H 0.1995 -0.2313 0.4529 0.11(4) Uiso 1 1 calc R . . . .
P1 P 0.12689(7) 0.31415(10) 0.38786(8) 0.0322(4) Uani 1 1 d . . . . .
Si1 Si 0.01471(7) 0.33818(10) 0.31752(8) 0.0290(4) Uani 1 1 d . . . . .
O1 O 0.0000 0.3124(3) 0.2500 0.0253(14) Uani 1 2 d S T P . .
Cl4 Cl 0.26952(8) -0.10648(13) 0.53945(10) 0.0679(7) Uani 1 1 d . . . . .
P2 P -0.01459(7) 0.20689(11) 0.38689(8) 0.0348(4) Uani 1 1 d . . . . .
B2 B 0.1217(3) -0.1766(5) 0.4205(4) 0.041(2) Uani 1 1 d . . . . .
C2 C 0.0565(3) 0.4279(4) 0.3320(3) 0.0380(18) Uani 1 1 d . . . . .
Cl2 Cl 0.08805(9) -0.26585(12) 0.41757(11) 0.0643(7) Uani 1 1 d . . . . .
C3 C 0.1069(3) 0.4137(4) 0.3573(3) 0.0402(19) Uani 1 1 d . . . . .
Cl3 Cl 0.16231(10) -0.18537(14) 0.55229(10) 0.0714(7) Uani 1 1 d . . . . .
B4 B 0.2130(3) -0.0967(5) 0.4821(4) 0.047(3) Uani 1 1 d . . . . .
C4 C 0.1393(3) 0.4769(4) 0.3645(4) 0.056(3) Uani 1 1 d . . . . .
H4 H 0.1733 0.4675 0.3830 0.068 Uiso 1 1 calc R U . . .
B5 B 0.2082(3) -0.1128(5) 0.4088(4) 0.044(2) Uani 1 1 d . . . . .
Cl5 Cl 0.26067(8) -0.13715(14) 0.39573(12) 0.0692(7) Uani 1 1 d . . . . .
C5 C 0.1228(3) 0.5531(5) 0.3451(4) 0.070(3) Uani 1 1 d . . . . .
H5 H 0.1453 0.5952 0.3474 0.084 Uiso 1 1 calc R U . . .
B6 B 0.1037(3) -0.0973(5) 0.3703(4) 0.037(2) Uani 1 1 d . . . . .
Cl6 Cl 0.04692(7) -0.09636(12) 0.31142(9) 0.0548(6) Uani 1 1 d . . . . .
C6 C 0.0730(3) 0.5679(4) 0.3221(4) 0.064(3) Uani 1 1 d . . . . .
H6 H 0.0613 0.6208 0.3102 0.076 Uiso 1 1 calc R U . . .
B7 B 0.1082(4) -0.0816(5) 0.4423(4) 0.047(2) Uani 1 1 d . . . . .
Cl7 Cl 0.05549(9) -0.06679(14) 0.45857(12) 0.0652(7) Uani 1 1 d . . . . .
C7 C 0.0409(3) 0.5065(4) 0.3165(3) 0.048(2) Uani 1 1 d . . . . .
H7 H 0.0070 0.5177 0.3016 0.058 Uiso 1 1 calc R U . . .
C8 C -0.0442(3) 0.3492(4) 0.3272(3) 0.0357(17) Uani 1 1 d . . . . .
Cl8 Cl 0.17210(9) 0.03679(12) 0.53795(9) 0.0609(6) Uani 1 1 d . . . . .
B8 B 0.1652(3) -0.0317(5) 0.4809(4) 0.040(2) Uani 1 1 d . . . . .
C10 C -0.1035(3) 0.2912(6) 0.3621(4) 0.060(2) Uani 1 1 d . . . . .
H10 H -0.1128 0.2499 0.3823 0.072 Uiso 1 1 calc R U . . .
Cl10 Cl 0.15557(8) -0.01487(12) 0.29672(9) 0.0494(5) Uani 1 1 d . . . . .
B10 B 0.1573(3) -0.0564(5) 0.3624(4) 0.037(2) Uani 1 1 d . . . . .
C9 C -0.0580(3) 0.2879(5) 0.3559(3) 0.0411(18) Uani 1 1 d . . . . .
B9 B 0.1955(3) -0.0165(5) 0.4304(4) 0.037(2) Uani 1 1 d . . . . .
Cl9 Cl 0.23403(7) 0.06728(11) 0.43597(10) 0.0510(5) Uani 1 1 d . . . . .
B3 B 0.1593(4) -0.1362(5) 0.4883(4) 0.046(2) Uani 1 1 d . . . . .
C11 C -0.1346(3) 0.3558(6) 0.3383(5) 0.072(3) Uani 1 1 d . . . . .
H11 H -0.1654 0.3579 0.3421 0.086 Uiso 1 1 calc R U . . .
Cl11 Cl 0.10140(7) 0.08741(10) 0.38590(8) 0.0401(4) Uani 1 1 d . . . . .
B11 B 0.1315(3) -0.0069(4) 0.4071(3) 0.0321(18) Uani 1 1 d . . . . .
C12 C -0.1218(3) 0.4158(6) 0.3098(4) 0.064(3) Uani 1 1 d . . . . .
H12 H -0.1435 0.4593 0.2939 0.076 Uiso 1 1 calc R U . . .
C20 C -0.0394(3) 0.1091(4) 0.3536(3) 0.0395(18) Uani 1 1 d . . . . .
H20 H -0.0179 0.0664 0.3785 0.047 Uiso 1 1 calc R U . . .
C13 C -0.0773(3) 0.4131(5) 0.3043(3) 0.046(2) Uani 1 1 d . . . . .
H13 H -0.0686 0.4555 0.2845 0.055 Uiso 1 1 calc R U . . .
C23 C -0.0085(3) 0.1997(5) 0.4621(3) 0.0452(19) Uani 1 1 d . . . . .
H23 H -0.0398 0.1783 0.4632 0.054 Uiso 1 1 calc R U . . .
C14 C 0.1639(3) 0.3334(4) 0.4644(3) 0.0420(19) Uani 1 1 d . . . . .
H14 H 0.1938 0.3633 0.4662 0.050 Uiso 1 1 calc R U . . .
C24 C 0.0014(5) 0.2812(6) 0.4917(4) 0.082(3) Uani 1 1 d . . . . .
H24A H 0.0051 0.2747 0.5320 0.122 Uiso 1 1 calc R U . . .
H24B H -0.0259 0.3176 0.4724 0.122 Uiso 1 1 calc R U . . .
H24C H 0.0314 0.3040 0.4899 0.122 Uiso 1 1 calc R U . . .
C15 C 0.1799(3) 0.2553(5) 0.4966(3) 0.050(2) Uani 1 1 d . . . . .
H15A H 0.1511 0.2238 0.4942 0.076 Uiso 1 1 calc R U . . .
H15B H 0.1995 0.2669 0.5370 0.076 Uiso 1 1 calc R U . . .
H15C H 0.1994 0.2245 0.4796 0.076 Uiso 1 1 calc R U . . .
C1_1 C 0.2654(4) 0.1245(7) 0.2935(4) 0.078(3) Uani 1 1 d D . . . .
C2_1 C 0.2588(4) 0.1743(7) 0.2477(5) 0.081(3) Uani 1 1 d D . . . .
C3_1 C 0.2496(5) 0.1417(9) 0.1961(5) 0.106(4) Uani 1 1 d D . . . .
H3_1 H 0.2456 0.1752 0.1639 0.128 Uiso 1 1 calc R U . . .
C4_1 C 0.2461(5) 0.0586(9) 0.1897(5) 0.110(5) Uani 1 1 d D . . . .
H4_1 H 0.2383 0.0363 0.1525 0.132 Uiso 1 1 calc R U . . .
C5_1 C 0.2532(4) 0.0088(8) 0.2339(6) 0.098(4) Uani 1 1 d D . . . .
H5_1 H 0.2511 -0.0480 0.2288 0.117 Uiso 1 1 calc R U . . .
C6_1 C 0.2641(4) 0.0436(7) 0.2887(5) 0.090(4) Uani 1 1 d D . . . .
H6_1 H 0.2704 0.0104 0.3216 0.108 Uiso 1 1 calc R U . . .
F1_1 F 0.2755(3) 0.1597(4) 0.3461(3) 0.105(2) Uani 1 1 d D . . . .
F2_1 F 0.2599(3) 0.2544(4) 0.2538(4) 0.118(3) Uani 1 1 d D . . . .
C1_2 C -0.0658(4) -0.2987(8) 0.3320(6) 0.094(4) Uani 1 1 d D . . . .
C2_2 C -0.1048(5) -0.3020(6) 0.3491(6) 0.099(4) Uani 1 1 d D . . . .
C3_2 C -0.1268(4) -0.2348(6) 0.3597(5) 0.085(3) Uani 1 1 d D . . . .
H3_2 H -0.1527 -0.2384 0.3736 0.102 Uiso 1 1 calc R U . . .
C4_2 C -0.1098(5) -0.1618(7) 0.3494(5) 0.086(4) Uani 1 1 d D . . . .
H4_2 H -0.1248 -0.1134 0.3548 0.103 Uiso 1 1 calc R U . . .
C5_2 C -0.0720(5) -0.1584(8) 0.3317(5) 0.100(4) Uani 1 1 d D . . . .
H5_2 H -0.0601 -0.1073 0.3256 0.120 Uiso 1 1 calc R U . . .
C6_2 C -0.0497(4) -0.2291(8) 0.3219(5) 0.098(4) Uani 1 1 d D . . . .
H6_2 H -0.0237 -0.2263 0.3083 0.117 Uiso 1 1 calc R U . . .
F1_2 F -0.0469(4) -0.3685(5) 0.3215(4) 0.167(4) Uani 1 1 d D . . . .
F2_2 F -0.1198(4) -0.3763(6) 0.3582(5) 0.189(5) Uani 1 1 d D . . . .
C1_3 C -0.0435(10) 0.498(3) 0.4649(14) 0.154(9) Uani 0.5 1 d D U P A -1
C2_3 C -0.0234(11) 0.481(4) 0.5223(14) 0.181(13) Uani 0.5 1 d D U P A -1
C3_3 C 0.0242(12) 0.493(4) 0.5532(17) 0.187(16) Uani 0.5 1 d D U P A -1
H3_3 H 0.0374 0.4844 0.5936 0.224 Uiso 0.5 1 calc R U P A -1
C4_3 C 0.0529(11) 0.517(3) 0.5238(17) 0.160(12) Uani 0.5 1 d D U P A -1
H4_3 H 0.0871 0.5222 0.5442 0.192 Uiso 0.5 1 calc R U P A -1
C5_3 C 0.0345(11) 0.534(3) 0.4676(15) 0.149(10) Uani 0.5 1 d D U P A -1
H5_3 H 0.0550 0.5531 0.4488 0.179 Uiso 0.5 1 calc R U P A -1
C6_3 C -0.0159(11) 0.523(2) 0.4367(15) 0.153(10) Uani 0.5 1 d D U P A -1
H6_3 H -0.0298 0.5328 0.3965 0.184 Uiso 0.5 1 calc R U P A -1
F1_3 F -0.0929(8) 0.4865(15) 0.4402(9) 0.206(9) Uani 0.5 1 d D U P A -1
F2_3 F -0.0543(9) 0.457(2) 0.5466(11) 0.208(10) Uani 0.5 1 d D U P A -1
C25 C 0.0322(3) 0.1405(6) 0.4941(3) 0.061(3) Uani 1 1 d . . . . .
H25A H 0.0351 0.1364 0.5342 0.092 Uiso 1 1 calc R U . . .
H25B H 0.0631 0.1598 0.4927 0.092 Uiso 1 1 calc R U . . .
H25C H 0.0245 0.0873 0.4759 0.092 Uiso 1 1 calc R U . . .
C16 C 0.1366(3) 0.3858(6) 0.4919(4) 0.065(3) Uani 1 1 d . . . . .
H16A H 0.1304 0.4388 0.4733 0.098 Uiso 1 1 calc R U . . .
H16B H 0.1562 0.3923 0.5329 0.098 Uiso 1 1 calc R U . . .
H16C H 0.1055 0.3601 0.4874 0.098 Uiso 1 1 calc R U . . .
C17 C 0.1690(3) 0.2707(4) 0.3577(3) 0.0344(16) Uani 1 1 d . . . . .
H17 H 0.1840 0.2226 0.3819 0.041 Uiso 1 1 calc R U . . .
C19 C 0.1421(3) 0.2391(5) 0.2977(3) 0.0469(19) Uani 1 1 d . . . . .
H19A H 0.1266 0.2842 0.2721 0.070 Uiso 1 1 calc R U . . .
H19B H 0.1171 0.2007 0.2982 0.070 Uiso 1 1 calc R U . . .
H19C H 0.1651 0.2121 0.2838 0.070 Uiso 1 1 calc R U . . .
C18 C 0.2115(3) 0.3247(5) 0.3593(4) 0.057(2) Uani 1 1 d . . . . .
H18A H 0.2347 0.2932 0.3482 0.085 Uiso 1 1 calc R U . . .
H18B H 0.2280 0.3457 0.3984 0.085 Uiso 1 1 calc R U . . .
H18C H 0.1991 0.3697 0.3325 0.085 Uiso 1 1 calc R U . . .
C21 C -0.0352(3) 0.1022(4) 0.2955(3) 0.0394(18) Uani 1 1 d . . . . .
H21A H -0.0559 0.1430 0.2695 0.059 Uiso 1 1 calc R U . . .
H21B H -0.0457 0.0484 0.2796 0.059 Uiso 1 1 calc R U . . .
H21C H -0.0012 0.1109 0.2997 0.059 Uiso 1 1 calc R U . . .
C22 C -0.0911(3) 0.0908(6) 0.3502(4) 0.061(2) Uani 1 1 d . . . . .
H22A H -0.1141 0.1275 0.3227 0.091 Uiso 1 1 calc R U . . .
H22B H -0.0929 0.0981 0.3882 0.091 Uiso 1 1 calc R U . . .
H22C H -0.0995 0.0350 0.3375 0.091 Uiso 1 1 calc R U . . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
Si1 Pt1 P2 86.28(7) .
Si1 Pt1 P1 87.60(7) .
P2 Pt1 P1 162.88(7) .
Si1 Pt1 Cl11 141.97(6) .
P2 Pt1 Cl11 99.76(6) .
P1 Pt1 Cl11 94.91(6) .
C1 B1 Cl1 121.5(5) .
C1 B1 B6 103.6(6) .
Cl1 B1 B6 126.0(5) .
C1 B1 B10 104.3(5) .
Cl1 B1 B10 125.0(6) .
B6 B1 B10 60.8(5) .
C1 B1 B5 58.3(5) .
Cl1 B1 B5 119.8(6) .
B6 B1 B5 108.1(5) .
B10 B1 B5 60.1(5) .
C1 B1 B2 58.0(5) .
Cl1 B1 B2 121.2(5) .
B6 B1 B2 59.2(5) .
B10 B1 B2 107.8(6) .
B5 B1 B2 107.2(6) .
B2 C1 B5 115.3(6) .
B2 C1 B1 63.3(5) .
B5 C1 B1 62.9(5) .
B2 C1 B3 62.6(5) .
B5 C1 B3 115.0(6) .
B1 C1 B3 115.3(6) .
B2 C1 B4 114.6(6) .
B5 C1 B4 63.6(5) .
B1 C1 B4 115.8(6) .
B3 C1 B4 62.1(5) .
B2 C1 H1 117.6 .
B5 C1 H1 117.1 .
B1 C1 H1 116.9 .
B3 C1 H1 117.9 .
B4 C1 H1 117.4 .
C3 P1 C17 110.4(4) .
C3 P1 C14 104.7(3) .
C17 P1 C14 105.4(3) .
C3 P1 Pt1 106.6(3) .
C17 P1 Pt1 119.2(2) .
C14 P1 Pt1 109.7(3) .
O1 Si1 C8 105.0(2) .
O1 Si1 C2 108.0(3) .
C8 Si1 C2 118.5(3) .
O1 Si1 Pt1 113.91(19) .
C8 Si1 Pt1 107.0(2) .
C2 Si1 Pt1 104.8(2) .
Si1 O1 Si1 149.8(4) 2
C9 P2 C23 105.8(4) .
C9 P2 C20 110.9(4) .
C23 P2 C20 106.1(4) .
C9 P2 Pt1 107.6(3) .
C23 P2 Pt1 110.7(3) .
C20 P2 Pt1 115.3(3) .
C1 B2 B6 104.6(6) .
C1 B2 B7 105.1(6) .
B6 B2 B7 60.7(5) .
C1 B2 Cl2 120.8(5) .
B6 B2 Cl2 125.4(6) .
B7 B2 Cl2 125.0(7) .
C1 B2 B3 59.1(5) .
B6 B2 B3 108.5(6) .
B7 B2 B3 60.0(5) .
Cl2 B2 B3 119.8(6) .
C1 B2 B1 58.7(5) .
B6 B2 B1 59.8(5) .
B7 B2 B1 108.8(6) .
Cl2 B2 B1 119.8(6) .
B3 B2 B1 108.6(6) .
C7 C2 C3 118.0(7) .
C7 C2 Si1 124.2(6) .
C3 C2 Si1 117.6(5) .
C4 C3 C2 119.8(6) .
C4 C3 P1 121.9(6) .
C2 C3 P1 117.8(5) .
C1 B4 Cl4 121.3(5) .
C1 B4 B8 104.2(6) .
Cl4 B4 B8 125.4(6) .
C1 B4 B3 58.8(5) .
Cl4 B4 B3 120.2(7) .
B8 B4 B3 59.5(5) .
C1 B4 B9 102.9(6) .
Cl4 B4 B9 126.1(6) .
B8 B4 B9 61.4(5) .
B3 B4 B9 108.0(6) .
C1 B4 B5 57.7(5) .
Cl4 B4 B5 120.6(6) .
B8 B4 B5 108.2(6) .
B3 B4 B5 107.4(6) .
B9 B4 B5 58.8(5) .
C5 C4 C3 120.7(8) .
C5 C4 H4 119.6 .
C3 C4 H4 119.6 .
C1 B5 Cl5 120.9(5) .
C1 B5 B9 104.7(7) .
Cl5 B5 B9 124.7(6) .
C1 B5 B1 58.8(5) .
Cl5 B5 B1 120.9(6) .
B9 B5 B1 108.3(6) .
C1 B5 B10 104.5(6) .
Cl5 B5 B10 126.1(7) .
B9 B5 B10 60.3(4) .
B1 B5 B10 59.9(4) .
C1 B5 B4 58.7(5) .
Cl5 B5 B4 118.9(6) .
B9 B5 B4 60.2(5) .
B1 B5 B4 108.4(7) .
B10 B5 B4 108.3(6) .
C4 C5 C6 119.4(8) .
C4 C5 H5 120.3 .
C6 C5 H5 120.3 .
B2 B6 B1 61.0(5) .
B2 B6 Cl6 122.7(5) .
B1 B6 Cl6 121.1(5) .
B2 B6 B7 59.7(5) .
B1 B6 B7 108.9(6) .
Cl6 B6 B7 122.1(6) .
B2 B6 B11 107.4(6) .
B1 B6 B11 107.1(6) .
Cl6 B6 B11 122.0(5) .
B7 B6 B11 60.5(5) .
B2 B6 B10 108.5(6) .
B1 B6 B10 59.9(5) .
Cl6 B6 B10 120.3(6) .
B7 B6 B10 108.6(6) .
B11 B6 B10 59.2(5) .
C7 C6 C5 120.0(7) .
C7 C6 H6 120.0 .
C5 C6 H6 120.0 .
B2 B7 Cl7 121.0(6) .
B2 B7 B3 60.5(5) .
Cl7 B7 B3 122.1(6) .
B2 B7 B6 59.6(5) .
Cl7 B7 B6 120.9(6) .
B3 B7 B6 108.0(7) .
B2 B7 B11 107.0(7) .
Cl7 B7 B11 123.2(6) .
B3 B7 B11 106.5(7) .
B6 B7 B11 60.1(5) .
B2 B7 B8 107.7(6) .
Cl7 B7 B8 122.7(6) .
B3 B7 B8 59.0(5) .
B6 B7 B8 108.3(7) .
B11 B7 B8 59.8(5) .
C6 C7 C2 121.8(8) .
C6 C7 H7 119.1 .
C2 C7 H7 119.1 .
C9 C8 C13 117.8(7) .
C9 C8 Si1 117.8(5) .
C13 C8 Si1 124.3(6) .
B3 B8 B4 60.5(5) .
B3 B8 Cl8 122.1(6) .
B4 B8 Cl8 121.6(6) .
B3 B8 B11 107.2(6) .
B4 B8 B11 107.0(6) .
Cl8 B8 B11 122.4(5) .
B3 B8 B7 59.6(5) .
B4 B8 B7 108.1(6) .
Cl8 B8 B7 122.0(6) .
B11 B8 B7 60.1(5) .
B3 B8 B9 107.7(6) .
B4 B8 B9 60.0(5) .
Cl8 B8 B9 122.2(6) .
B11 B8 B9 58.6(5) .
B7 B8 B9 107.0(6) .
C11 C10 C9 119.1(9) .
C11 C10 H10 120.5 .
C9 C10 H10 120.5 .
Cl10 B10 B11 122.5(5) .
Cl10 B10 B1 121.5(6) .
B11 B10 B1 107.4(6) .
Cl10 B10 B9 122.3(6) .
B11 B10 B9 59.5(5) .
B1 B10 B9 107.8(6) .
Cl10 B10 B5 122.5(6) .
B11 B10 B5 106.6(6) .
B1 B10 B5 60.1(5) .
B9 B10 B5 59.4(5) .
Cl10 B10 B6 121.9(5) .
B11 B10 B6 60.2(5) .
B1 B10 B6 59.3(5) .
B9 B10 B6 107.7(6) .
B5 B10 B6 107.0(6) .
C8 C9 C10 120.3(7) .
C8 C9 P2 117.6(6) .
C10 C9 P2 122.1(6) .
B11 B9 Cl9 122.2(5) .
B11 B9 B5 107.6(6) .
Cl9 B9 B5 122.0(6) .
B11 B9 B10 59.9(5) .
Cl9 B9 B10 121.8(6) .
B5 B9 B10 60.3(5) .
B11 B9 B4 107.0(6) .
Cl9 B9 B4 121.4(5) .
B5 B9 B4 61.0(5) .
B10 B9 B4 109.0(6) .
B11 B9 B8 60.0(5) .
Cl9 B9 B8 121.5(5) .
B5 B9 B8 107.6(6) .
B10 B9 B8 108.3(6) .
B4 B9 B8 58.6(5) .
C1 B3 B8 104.8(7) .
C1 B3 B7 104.1(6) .
B8 B3 B7 61.4(5) .
C1 B3 Cl3 121.4(6) .
B8 B3 Cl3 125.1(6) .
B7 B3 Cl3 124.7(7) .
C1 B3 B4 59.1(5) .
B8 B3 B4 60.0(5) .
B7 B3 B4 109.1(6) .
Cl3 B3 B4 120.2(6) .
C1 B3 B2 58.2(5) .
B8 B3 B2 108.8(6) .
B7 B3 B2 59.5(5) .
Cl3 B3 B2 119.6(6) .
B4 B3 B2 108.5(7) .
C12 C11 C10 121.4(8) .
C12 C11 H11 119.3 .
C10 C11 H11 119.3 .
B11 Cl11 Pt1 166.4(3) .
B9 B11 B10 60.5(5) .
B9 B11 Cl11 122.2(5) .
B10 B11 Cl11 120.1(5) .
B9 B11 B6 108.8(6) .
B10 B11 B6 60.6(5) .
Cl11 B11 B6 120.0(5) .
B9 B11 B8 61.4(5) .
B10 B11 B8 109.9(6) .
Cl11 B11 B8 122.3(5) .
B6 B11 B8 108.2(5) .
B9 B11 B7 109.4(6) .
B10 B11 B7 108.9(6) .
Cl11 B11 B7 120.8(6) .
B6 B11 B7 59.4(5) .
B8 B11 B7 60.2(5) .
C11 C12 C13 119.5(8) .
C11 C12 H12 120.2 .
C13 C12 H12 120.2 .
C21 C20 C22 111.7(6) .
C21 C20 P2 109.9(5) .
C22 C20 P2 114.9(6) .
C21 C20 H20 106.6 .
C22 C20 H20 106.6 .
P2 C20 H20 106.6 .
C12 C13 C8 121.9(8) .
C12 C13 H13 119.1 .
C8 C13 H13 119.1 .
C24 C23 C25 110.2(7) .
C24 C23 P2 111.9(6) .
C25 C23 P2 109.9(6) .
C24 C23 H23 108.3 .
C25 C23 H23 108.3 .
P2 C23 H23 108.3 .
C15 C14 C16 111.2(7) .
C15 C14 P1 110.8(5) .
C16 C14 P1 111.3(5) .
C15 C14 H14 107.8 .
C16 C14 H14 107.8 .
P1 C14 H14 107.8 .
C23 C24 H24A 109.5 .
C23 C24 H24B 109.5 .
H24A C24 H24B 109.5 .
C23 C24 H24C 109.5 .
H24A C24 H24C 109.5 .
H24B C24 H24C 109.5 .
C14 C15 H15A 109.5 .
C14 C15 H15B 109.5 .
H15A C15 H15B 109.5 .
C14 C15 H15C 109.5 .
H15A C15 H15C 109.5 .
H15B C15 H15C 109.5 .
C6_1 C1_1 F1_1 120.1(10) .
C6_1 C1_1 C2_1 122.3(11) .
F1_1 C1_1 C2_1 117.5(10) .
C3_1 C2_1 F2_1 120.2(11) .
C3_1 C2_1 C1_1 118.8(11) .
F2_1 C2_1 C1_1 120.9(10) .
C2_1 C3_1 C4_1 119.7(12) .
C2_1 C3_1 H3_1 120.2 .
C4_1 C3_1 H3_1 120.2 .
C5_1 C4_1 C3_1 122.5(12) .
C5_1 C4_1 H4_1 118.8 .
C3_1 C4_1 H4_1 118.8 .
C4_1 C5_1 C6_1 117.6(12) .
C4_1 C5_1 H5_1 121.2 .
C6_1 C5_1 H5_1 121.2 .
C1_1 C6_1 C5_1 119.0(11) .
C1_1 C6_1 H6_1 120.5 .
C5_1 C6_1 H6_1 120.5 .
C6_2 C1_2 F1_2 120.6(13) .
C6_2 C1_2 C2_2 120.4(11) .
F1_2 C1_2 C2_2 118.8(12) .
F2_2 C2_2 C3_2 120.0(13) .
F2_2 C2_2 C1_2 117.0(12) .
C3_2 C2_2 C1_2 123.0(11) .
C2_2 C3_2 C4_2 116.7(12) .
C2_2 C3_2 H3_2 121.7 .
C4_2 C3_2 H3_2 121.7 .
C5_2 C4_2 C3_2 120.4(12) .
C5_2 C4_2 H4_2 119.8 .
C3_2 C4_2 H4_2 119.8 .
C4_2 C5_2 C6_2 121.4(12) .
C4_2 C5_2 H5_2 119.3 .
C6_2 C5_2 H5_2 119.3 .
C1_2 C6_2 C5_2 118.1(12) .
C1_2 C6_2 H6_2 120.9 .
C5_2 C6_2 H6_2 120.9 .
C6_3 C1_3 C2_3 120.9(19) .
C6_3 C1_3 F1_3 124(2) .
C2_3 C1_3 F1_3 115(2) .
F2_3 C2_3 C3_3 122(2) .
F2_3 C2_3 C1_3 116(2) .
C3_3 C2_3 C1_3 121.9(19) .
C2_3 C3_3 C4_3 117(2) .
C2_3 C3_3 H3_3 121.4 .
C4_3 C3_3 H3_3 121.4 .
C5_3 C4_3 C3_3 122(2) .
C5_3 C4_3 H4_3 118.8 .
C3_3 C4_3 H4_3 118.8 .
C4_3 C5_3 C6_3 119(2) .
C4_3 C5_3 H5_3 120.5 .
C6_3 C5_3 H5_3 120.5 .
C1_3 C6_3 C5_3 119(2) .
C1_3 C6_3 H6_3 120.7 .
C5_3 C6_3 H6_3 120.7 .
C23 C25 H25A 109.5 .
C23 C25 H25B 109.5 .
H25A C25 H25B 109.5 .
C23 C25 H25C 109.5 .
H25A C25 H25C 109.5 .
H25B C25 H25C 109.5 .
C14 C16 H16A 109.5 .
C14 C16 H16B 109.5 .
H16A C16 H16B 109.5 .
C14 C16 H16C 109.5 .
H16A C16 H16C 109.5 .
H16B C16 H16C 109.5 .
C19 C17 C18 110.6(7) .
C19 C17 P1 111.1(5) .
C18 C17 P1 115.9(5) .
C19 C17 H17 106.2 .
C18 C17 H17 106.2 .
P1 C17 H17 106.2 .
C17 C19 H19A 109.5 .
C17 C19 H19B 109.5 .
H19A C19 H19B 109.5 .
C17 C19 H19C 109.5 .
H19A C19 H19C 109.5 .
H19B C19 H19C 109.5 .
C17 C18 H18A 109.5 .
C17 C18 H18B 109.5 .
H18A C18 H18B 109.5 .
C17 C18 H18C 109.5 .
H18A C18 H18C 109.5 .
H18B C18 H18C 109.5 .
C20 C21 H21A 109.5 .
C20 C21 H21B 109.5 .
H21A C21 H21B 109.5 .
C20 C21 H21C 109.5 .
H21A C21 H21C 109.5 .
H21B C21 H21C 109.5 .
C20 C22 H22A 109.5 .
C20 C22 H22B 109.5 .
H22A C22 H22B 109.5 .
C20 C22 H22C 109.5 .
H22A C22 H22C 109.5 .
H22B C22 H22C 109.5 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pt1 Si1 2.2499(18) .
Pt1 P2 2.288(2) .
Pt1 P1 2.2973(19) .
Pt1 Cl11 2.8753(16) .
Cl1 B1 1.762(9) .
B1 C1 1.716(11) .
B1 B6 1.772(12) .
B1 B10 1.782(11) .
B1 B5 1.786(12) .
B1 B2 1.793(14) .
C1 B2 1.703(12) .
C1 B5 1.706(13) .
C1 B3 1.719(13) .
C1 B4 1.724(11) .
C1 H1 0.9700 .
P1 C3 1.823(7) .
P1 C17 1.827(8) .
P1 C14 1.847(7) .
Si1 O1 1.639(2) .
Si1 C8 1.854(7) .
Si1 C2 1.881(7) .
O1 Si1 1.639(2) 2
Cl4 B4 1.759(8) .
P2 C9 1.821(8) .
P2 C23 1.829(8) .
P2 C20 1.846(7) .
B2 B6 1.761(11) .
B2 B7 1.761(12) .
B2 Cl2 1.768(9) .
B2 B3 1.779(12) .
C2 C7 1.388(9) .
C2 C3 1.403(10) .
C3 C4 1.387(10) .
Cl3 B3 1.772(10) .
B4 B8 1.768(12) .
B4 B3 1.776(15) .
B4 B9 1.794(12) .
B4 B5 1.808(14) .
C4 C5 1.376(10) .
C4 H4 0.9500 .
B5 Cl5 1.748(10) .
B5 B9 1.770(11) .
B5 B10 1.786(12) .
C5 C6 1.388(12) .
C5 H5 0.9500 .
B6 Cl6 1.775(8) .
B6 B7 1.780(13) .
B6 B11 1.791(11) .
B6 B10 1.798(13) .
C6 C7 1.363(11) .
C6 H6 0.9500 .
B7 Cl7 1.769(11) .
B7 B3 1.769(13) .
B7 B11 1.798(12) .
B7 B8 1.800(13) .
C7 H7 0.9500 .
C8 C9 1.391(10) .
C8 C13 1.411(9) .
Cl8 B8 1.778(9) .
B8 B3 1.758(11) .
B8 B11 1.793(11) .
B8 B9 1.819(13) .
C10 C11 1.393(12) .
C10 C9 1.409(11) .
C10 H10 0.9500 .
Cl10 B10 1.766(9) .
B10 B11 1.774(12) .
B10 B9 1.785(11) .
B9 B11 1.767(12) .
B9 Cl9 1.769(8) .
C11 C12 1.356(13) .
C11 H11 0.9500 .
Cl11 B11 1.779(7) .
C12 C13 1.373(11) .
C12 H12 0.9500 .
C20 C21 1.513(10) .
C20 C22 1.528(11) .
C20 H20 1.0000 .
C13 H13 0.9500 .
C23 C24 1.518(12) .
C23 C25 1.527(11) .
C23 H23 1.0000 .
C14 C15 1.505(10) .
C14 C16 1.516(11) .
C14 H14 1.0000 .
C24 H24A 0.9800 .
C24 H24B 0.9800 .
C24 H24C 0.9800 .
C15 H15A 0.9800 .
C15 H15B 0.9800 .
C15 H15C 0.9800 .
C1_1 C6_1 1.346(13) .
C1_1 F1_1 1.368(11) .
C1_1 C2_1 1.369(12) .
C2_1 C3_1 1.333(13) .
C2_1 F2_1 1.336(11) .
C3_1 C4_1 1.386(14) .
C3_1 H3_1 0.9500 .
C4_1 C5_1 1.334(14) .
C4_1 H4_1 0.9500 .
C5_1 C6_1 1.410(14) .
C5_1 H5_1 0.9500 .
C6_1 H6_1 0.9500 .
C1_2 C6_2 1.309(14) .
C1_2 F1_2 1.353(11) .
C1_2 C2_2 1.372(14) .
C2_2 F2_2 1.356(12) .
C2_2 C3_2 1.366(13) .
C3_2 C4_2 1.371(13) .
C3_2 H3_2 0.9500 .
C4_2 C5_2 1.350(14) .
C4_2 H4_2 0.9500 .
C5_2 C6_2 1.410(14) .
C5_2 H5_2 0.9500 .
C6_2 H6_2 0.9500 .
C1_3 C6_3 1.326(19) .
C1_3 C2_3 1.367(18) .
C1_3 F1_3 1.371(17) .
C2_3 F2_3 1.331(18) .
C2_3 C3_3 1.344(19) .
C3_3 C4_3 1.375(19) .
C3_3 H3_3 0.9500 .
C4_3 C5_3 1.338(19) .
C4_3 H4_3 0.9500 .
C5_3 C6_3 1.414(19) .
C5_3 H5_3 0.9500 .
C6_3 H6_3 0.9500 .
C25 H25A 0.9800 .
C25 H25B 0.9800 .
C25 H25C 0.9800 .
C16 H16A 0.9800 .
C16 H16B 0.9800 .
C16 H16C 0.9800 .
C17 C19 1.510(10) .
C17 C18 1.530(10) .
C17 H17 1.0000 .
C19 H19A 0.9800 .
C19 H19B 0.9800 .
C19 H19C 0.9800 .
C18 H18A 0.9800 .
C18 H18B 0.9800 .
C18 H18C 0.9800 .
C21 H21A 0.9800 .
C21 H21B 0.9800 .
C21 H21C 0.9800 .
C22 H22A 0.9800 .
C22 H22B 0.9800 .
C22 H22C 0.9800 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_4
Cl1 B1 C1 B2 -109.5(7) .
B6 B1 C1 B2 39.5(5) .
B10 B1 C1 B2 102.3(6) .
B5 B1 C1 B2 142.6(6) .
Cl1 B1 C1 B5 107.9(7) .
B6 B1 C1 B5 -103.1(6) .
B10 B1 C1 B5 -40.3(6) .
B2 B1 C1 B5 -142.6(6) .
Cl1 B1 C1 B3 -145.7(6) .
B6 B1 C1 B3 3.3(8) .
B10 B1 C1 B3 66.2(8) .
B5 B1 C1 B3 106.5(7) .
B2 B1 C1 B3 -36.2(6) .
Cl1 B1 C1 B4 144.6(7) .
B6 B1 C1 B4 -66.4(8) .
B10 B1 C1 B4 -3.6(9) .
B5 B1 C1 B4 36.7(7) .
B2 B1 C1 B4 -105.9(7) .
C8 Si1 O1 Si1 88.1(2) 2
C2 Si1 O1 Si1 -39.3(2) 2
Pt1 Si1 O1 Si1 -155.23(11) 2
B5 C1 B2 B6 -3.3(8) .
B1 C1 B2 B6 -40.0(5) .
B3 C1 B2 B6 103.0(6) .
B4 C1 B2 B6 67.8(8) .
B5 C1 B2 B7 -66.4(8) .
B1 C1 B2 B7 -103.1(6) .
B3 C1 B2 B7 40.0(6) .
B4 C1 B2 B7 4.8(9) .
B5 C1 B2 Cl2 145.1(6) .
B1 C1 B2 Cl2 108.4(7) .
B3 C1 B2 Cl2 -108.5(7) .
B4 C1 B2 Cl2 -143.8(7) .
B5 C1 B2 B3 -106.4(7) .
B1 C1 B2 B3 -143.1(6) .
B4 C1 B2 B3 -35.2(7) .
B5 C1 B2 B1 36.7(6) .
B3 C1 B2 B1 143.1(6) .
B4 C1 B2 B1 107.8(7) .
Cl1 B1 B2 C1 110.0(6) .
B6 B1 B2 C1 -134.0(6) .
B10 B1 B2 C1 -96.0(6) .
B5 B1 B2 C1 -32.7(5) .
C1 B1 B2 B6 134.0(6) .
Cl1 B1 B2 B6 -116.1(6) .
B10 B1 B2 B6 37.9(5) .
B5 B1 B2 B6 101.3(6) .
C1 B1 B2 B7 96.7(6) .
Cl1 B1 B2 B7 -153.3(6) .
B6 B1 B2 B7 -37.3(6) .
B10 B1 B2 B7 0.7(8) .
B5 B1 B2 B7 64.0(7) .
C1 B1 B2 Cl2 -110.0(6) .
Cl1 B1 B2 Cl2 0.0(9) .
B6 B1 B2 Cl2 116.1(6) .
B10 B1 B2 Cl2 154.0(5) .
B5 B1 B2 Cl2 -142.6(5) .
C1 B1 B2 B3 33.0(5) .
Cl1 B1 B2 B3 143.0(5) .
B6 B1 B2 B3 -101.0(6) .
B10 B1 B2 B3 -63.0(7) .
B5 B1 B2 B3 0.3(7) .
O1 Si1 C2 C7 78.9(7) .
C8 Si1 C2 C7 -40.2(8) .
Pt1 Si1 C2 C7 -159.4(7) .
O1 Si1 C2 C3 -97.4(6) .
C8 Si1 C2 C3 143.5(6) .
Pt1 Si1 C2 C3 24.4(7) .
C7 C2 C3 C4 -1.8(12) .
Si1 C2 C3 C4 174.7(7) .
C7 C2 C3 P1 170.5(6) .
Si1 C2 C3 P1 -13.0(9) .
C17 P1 C3 C4 -61.7(8) .
C14 P1 C3 C4 51.3(8) .
Pt1 P1 C3 C4 167.5(7) .
C17 P1 C3 C2 126.1(6) .
C14 P1 C3 C2 -120.9(6) .
Pt1 P1 C3 C2 -4.7(7) .
B2 C1 B4 Cl4 144.0(7) .
B5 C1 B4 Cl4 -108.7(8) .
B1 C1 B4 Cl4 -145.1(7) .
B3 C1 B4 Cl4 108.6(8) .
B2 C1 B4 B8 -4.6(9) .
B5 C1 B4 B8 102.7(6) .
B1 C1 B4 B8 66.3(9) .
B3 C1 B4 B8 -40.0(6) .
B2 C1 B4 B3 35.4(6) .
B5 C1 B4 B3 142.7(6) .
B1 C1 B4 B3 106.3(7) .
B2 C1 B4 B9 -68.0(9) .
B5 C1 B4 B9 39.3(6) .
B1 C1 B4 B9 2.9(9) .
B3 C1 B4 B9 -103.4(7) .
B2 C1 B4 B5 -107.3(7) .
B1 C1 B4 B5 -36.4(7) .
B3 C1 B4 B5 -142.7(6) .
C2 C3 C4 C5 -2.5(14) .
P1 C3 C4 C5 -174.6(8) .
B2 C1 B5 Cl5 -146.5(6) .
B1 C1 B5 Cl5 -109.7(7) .
B3 C1 B5 Cl5 143.4(6) .
B4 C1 B5 Cl5 107.2(7) .
B2 C1 B5 B9 65.9(8) .
B1 C1 B5 B9 102.7(6) .
B3 C1 B5 B9 -4.2(8) .
B4 C1 B5 B9 -40.4(5) .
B2 C1 B5 B1 -36.8(6) .
B3 C1 B5 B1 -106.9(7) .
B4 C1 B5 B1 -143.1(6) .
B2 C1 B5 B10 3.4(8) .
B1 C1 B5 B10 40.2(5) .
B3 C1 B5 B10 -66.7(8) .
B4 C1 B5 B10 -102.9(6) .
B2 C1 B5 B4 106.3(7) .
B1 C1 B5 B4 143.1(6) .
B3 C1 B5 B4 36.2(6) .
Cl1 B1 B5 C1 -110.7(6) .
B6 B1 B5 C1 95.0(7) .
B10 B1 B5 C1 133.7(7) .
B2 B1 B5 C1 32.6(5) .
C1 B1 B5 Cl5 109.8(7) .
Cl1 B1 B5 Cl5 -0.9(9) .
B6 B1 B5 Cl5 -155.2(6) .
B10 B1 B5 Cl5 -116.5(8) .
B2 B1 B5 Cl5 142.4(6) .
C1 B1 B5 B9 -96.5(7) .
Cl1 B1 B5 B9 152.9(6) .
B6 B1 B5 B9 -1.4(9) .
B10 B1 B5 B9 37.2(6) .
B2 B1 B5 B9 -63.9(7) .
C1 B1 B5 B10 -133.7(7) .
Cl1 B1 B5 B10 115.6(7) .
B6 B1 B5 B10 -38.7(6) .
B2 B1 B5 B10 -101.1(6) .
C1 B1 B5 B4 -32.7(5) .
Cl1 B1 B5 B4 -143.4(6) .
B6 B1 B5 B4 62.3(7) .
B10 B1 B5 B4 101.0(6) .
B2 B1 B5 B4 -0.1(7) .
Cl4 B4 B5 C1 109.9(7) .
B8 B4 B5 C1 -95.7(7) .
B3 B4 B5 C1 -32.9(5) .
B9 B4 B5 C1 -133.8(6) .
C1 B4 B5 Cl5 -110.6(7) .
Cl4 B4 B5 Cl5 -0.7(9) .
B8 B4 B5 Cl5 153.8(6) .
B3 B4 B5 Cl5 -143.4(6) .
B9 B4 B5 Cl5 115.6(7) .
C1 B4 B5 B9 133.8(6) .
Cl4 B4 B5 B9 -116.3(7) .
B8 B4 B5 B9 38.1(6) .
B3 B4 B5 B9 100.9(6) .
C1 B4 B5 B1 32.8(5) .
Cl4 B4 B5 B1 142.7(6) .
B8 B4 B5 B1 -62.9(7) .
B3 B4 B5 B1 -0.1(7) .
B9 B4 B5 B1 -101.0(6) .
C1 B4 B5 B10 96.2(7) .
Cl4 B4 B5 B10 -153.9(6) .
B8 B4 B5 B10 0.5(8) .
B3 B4 B5 B10 63.3(7) .
B9 B4 B5 B10 -37.6(6) .
C3 C4 C5 C6 4.9(16) .
C1 B2 B6 B1 39.5(5) .
B7 B2 B6 B1 138.9(6) .
Cl2 B2 B6 B1 -107.0(8) .
B3 B2 B6 B1 101.3(7) .
C1 B2 B6 Cl6 149.7(6) .
B7 B2 B6 Cl6 -110.9(8) .
Cl2 B2 B6 Cl6 3.2(11) .
B3 B2 B6 Cl6 -148.5(6) .
B1 B2 B6 Cl6 110.2(7) .
C1 B2 B6 B7 -99.4(7) .
Cl2 B2 B6 B7 114.1(8) .
B3 B2 B6 B7 -37.6(7) .
B1 B2 B6 B7 -138.9(6) .
C1 B2 B6 B11 -60.8(8) .
B7 B2 B6 B11 38.6(6) .
Cl2 B2 B6 B11 152.7(7) .
B3 B2 B6 B11 1.0(9) .
B1 B2 B6 B11 -100.3(6) .
C1 B2 B6 B10 1.8(8) .
B7 B2 B6 B10 101.2(6) .
Cl2 B2 B6 B10 -144.7(7) .
B3 B2 B6 B10 63.6(8) .
B1 B2 B6 B10 -37.7(5) .
C1 B1 B6 B2 -38.9(5) .
Cl1 B1 B6 B2 108.2(7) .
B10 B1 B6 B2 -137.9(6) .
B5 B1 B6 B2 -99.6(7) .
C1 B1 B6 Cl6 -151.7(6) .
Cl1 B1 B6 Cl6 -4.7(10) .
B10 B1 B6 Cl6 109.3(7) .
B5 B1 B6 Cl6 147.6(6) .
B2 B1 B6 Cl6 -112.8(7) .
C1 B1 B6 B7 -2.1(7) .
Cl1 B1 B6 B7 145.0(6) .
B10 B1 B6 B7 -101.0(6) .
B5 B1 B6 B7 -62.7(8) .
B2 B1 B6 B7 36.8(6) .
C1 B1 B6 B11 61.8(7) .
Cl1 B1 B6 B11 -151.1(6) .
B10 B1 B6 B11 -37.1(6) .
B5 B1 B6 B11 1.2(8) .
B2 B1 B6 B11 100.7(6) .
C1 B1 B6 B10 99.0(6) .
Cl1 B1 B6 B10 -114.0(8) .
B5 B1 B6 B10 38.3(6) .
B2 B1 B6 B10 137.9(6) .
C4 C5 C6 C7 -2.9(15) .
C1 B2 B7 Cl7 -151.5(6) .
B6 B2 B7 Cl7 110.1(7) .
Cl2 B2 B7 Cl7 -4.7(10) .
B3 B2 B7 Cl7 -111.9(8) .
B1 B2 B7 Cl7 147.0(6) .
C1 B2 B7 B3 -39.6(6) .
B6 B2 B7 B3 -138.0(7) .
Cl2 B2 B7 B3 107.2(8) .
B1 B2 B7 B3 -101.1(7) .
C1 B2 B7 B6 98.5(7) .
Cl2 B2 B7 B6 -114.8(7) .
B3 B2 B7 B6 138.0(7) .
B1 B2 B7 B6 36.9(6) .
C1 B2 B7 B11 60.1(8) .
B6 B2 B7 B11 -38.4(6) .
Cl2 B2 B7 B11 -153.1(6) .
B3 B2 B7 B11 99.7(7) .
B1 B2 B7 B11 -1.5(8) .
C1 B2 B7 B8 -2.9(8) .
B6 B2 B7 B8 -101.3(7) .
Cl2 B2 B7 B8 143.9(6) .
B3 B2 B7 B8 36.7(6) .
B1 B2 B7 B8 -64.4(7) .
B1 B6 B7 B2 -37.4(6) .
Cl6 B6 B7 B2 111.9(7) .
B11 B6 B7 B2 -136.8(6) .
B10 B6 B7 B2 -101.0(6) .
B2 B6 B7 Cl7 -110.2(7) .
B1 B6 B7 Cl7 -147.6(6) .
Cl6 B6 B7 Cl7 1.7(9) .
B11 B6 B7 Cl7 113.0(7) .
B10 B6 B7 Cl7 148.8(5) .
B2 B6 B7 B3 37.7(6) .
B1 B6 B7 B3 0.3(8) .
Cl6 B6 B7 B3 149.6(6) .
B11 B6 B7 B3 -99.1(7) .
B10 B6 B7 B3 -63.3(7) .
B2 B6 B7 B11 136.8(6) .
B1 B6 B7 B11 99.4(6) .
Cl6 B6 B7 B11 -111.3(6) .
B10 B6 B7 B11 35.8(5) .
B2 B6 B7 B8 100.2(7) .
B1 B6 B7 B8 62.8(7) .
Cl6 B6 B7 B8 -148.0(5) .
B11 B6 B7 B8 -36.6(5) .
B10 B6 B7 B8 -0.8(7) .
C5 C6 C7 C2 -1.6(14) .
C3 C2 C7 C6 3.9(13) .
Si1 C2 C7 C6 -172.3(7) .
O1 Si1 C8 C9 104.0(6) .
C2 Si1 C8 C9 -135.3(6) .
Pt1 Si1 C8 C9 -17.3(6) .
O1 Si1 C8 C13 -71.9(7) .
C2 Si1 C8 C13 48.7(7) .
Pt1 Si1 C8 C13 166.7(6) .
C1 B4 B8 B3 39.7(6) .
Cl4 B4 B8 B3 -107.3(9) .
B9 B4 B8 B3 136.9(6) .
B5 B4 B8 B3 99.9(7) .
C1 B4 B8 Cl8 151.3(6) .
Cl4 B4 B8 Cl8 4.4(11) .
B3 B4 B8 Cl8 111.6(7) .
B9 B4 B8 Cl8 -111.5(7) .
B5 B4 B8 Cl8 -148.5(6) .
C1 B4 B8 B11 -60.8(8) .
Cl4 B4 B8 B11 152.2(7) .
B3 B4 B8 B11 -100.5(6) .
B9 B4 B8 B11 36.3(5) .
B5 B4 B8 B11 -0.7(8) .
C1 B4 B8 B7 2.5(8) .
Cl4 B4 B8 B7 -144.5(7) .
B3 B4 B8 B7 -37.2(6) .
B9 B4 B8 B7 99.6(6) .
B5 B4 B8 B7 62.6(8) .
C1 B4 B8 B9 -97.2(6) .
Cl4 B4 B8 B9 115.9(8) .
B3 B4 B8 B9 -136.9(6) .
B5 B4 B8 B9 -37.0(6) .
B2 B7 B8 B3 -37.4(6) .
Cl7 B7 B8 B3 110.6(8) .
B6 B7 B8 B3 -100.4(7) .
B11 B7 B8 B3 -137.2(7) .
B2 B7 B8 B4 0.2(9) .
Cl7 B7 B8 B4 148.2(6) .
B3 B7 B8 B4 37.6(6) .
B6 B7 B8 B4 -62.8(7) .
B11 B7 B8 B4 -99.6(7) .
B2 B7 B8 Cl8 -148.5(6) .
Cl7 B7 B8 Cl8 -0.5(9) .
B3 B7 B8 Cl8 -111.1(7) .
B6 B7 B8 Cl8 148.4(6) .
B11 B7 B8 Cl8 111.7(6) .
B2 B7 B8 B11 99.8(7) .
Cl7 B7 B8 B11 -112.2(7) .
B3 B7 B8 B11 137.2(7) .
B6 B7 B8 B11 36.7(5) .
B2 B7 B8 B9 63.5(7) .
Cl7 B7 B8 B9 -148.6(6) .
B3 B7 B8 B9 100.9(6) .
B6 B7 B8 B9 0.4(7) .
B11 B7 B8 B9 -36.3(5) .
C1 B1 B10 Cl10 151.3(6) .
Cl1 B1 B10 Cl10 4.6(10) .
B6 B1 B10 Cl10 -110.9(7) .
B5 B1 B10 Cl10 112.0(7) .
B2 B1 B10 Cl10 -148.1(6) .
C1 B1 B10 B11 -60.1(7) .
Cl1 B1 B10 B11 153.2(6) .
B6 B1 B10 B11 37.7(5) .
B5 B1 B10 B11 -99.5(7) .
B2 B1 B10 B11 0.4(7) .
C1 B1 B10 B9 2.7(8) .
Cl1 B1 B10 B9 -144.0(6) .
B6 B1 B10 B9 100.4(7) .
B5 B1 B10 B9 -36.7(6) .
B2 B1 B10 B9 63.2(7) .
C1 B1 B10 B5 39.4(6) .
Cl1 B1 B10 B5 -107.3(8) .
B6 B1 B10 B5 137.2(7) .
B2 B1 B10 B5 99.9(7) .
C1 B1 B10 B6 -97.8(7) .
Cl1 B1 B10 B6 115.5(7) .
B5 B1 B10 B6 -137.2(7) .
B2 B1 B10 B6 -37.2(5) .
C1 B5 B10 Cl10 -150.0(6) .
Cl5 B5 B10 Cl10 -2.2(10) .
B9 B5 B10 Cl10 111.1(7) .
B1 B5 B10 Cl10 -110.3(7) .
B4 B5 B10 Cl10 148.6(6) .
C1 B5 B10 B11 61.2(7) .
Cl5 B5 B10 B11 -151.0(6) .
B9 B5 B10 B11 -37.7(6) .
B1 B5 B10 B11 100.9(7) .
B4 B5 B10 B11 -0.2(8) .
C1 B5 B10 B1 -39.7(6) .
Cl5 B5 B10 B1 108.2(8) .
B9 B5 B10 B1 -138.6(7) .
B4 B5 B10 B1 -101.0(7) .
C1 B5 B10 B9 98.9(7) .
Cl5 B5 B10 B9 -113.2(8) .
B1 B5 B10 B9 138.6(7) .
B4 B5 B10 B9 37.6(6) .
C1 B5 B10 B6 -2.0(7) .
Cl5 B5 B10 B6 145.9(6) .
B9 B5 B10 B6 -100.9(7) .
B1 B5 B10 B6 37.7(6) .
B4 B5 B10 B6 -63.3(7) .
B2 B6 B10 Cl10 148.4(6) .
B1 B6 B10 Cl10 110.2(7) .
Cl6 B6 B10 Cl10 -0.4(9) .
B7 B6 B10 Cl10 -148.3(5) .
B11 B6 B10 Cl10 -112.0(6) .
B2 B6 B10 B11 -99.6(6) .
B1 B6 B10 B11 -137.8(6) .
Cl6 B6 B10 B11 111.5(6) .
B7 B6 B10 B11 -36.3(5) .
B2 B6 B10 B1 38.2(6) .
Cl6 B6 B10 B1 -110.7(6) .
B7 B6 B10 B1 101.5(6) .
B11 B6 B10 B1 137.8(6) .
B2 B6 B10 B9 -62.4(7) .
B1 B6 B10 B9 -100.6(6) .
Cl6 B6 B10 B9 148.8(5) .
B7 B6 B10 B9 0.9(7) .
B11 B6 B10 B9 37.2(5) .
B2 B6 B10 B5 0.2(8) .
B1 B6 B10 B5 -38.0(6) .
Cl6 B6 B10 B5 -148.7(5) .
B7 B6 B10 B5 63.5(7) .
B11 B6 B10 B5 99.8(6) .
C13 C8 C9 C10 -0.8(11) .
Si1 C8 C9 C10 -177.0(6) .
C13 C8 C9 P2 -178.5(5) .
Si1 C8 C9 P2 5.3(8) .
C11 C10 C9 C8 1.1(13) .
C11 C10 C9 P2 178.7(7) .
C23 P2 C9 C8 127.5(6) .
C20 P2 C9 C8 -117.8(6) .
Pt1 P2 C9 C8 9.2(7) .
C23 P2 C9 C10 -50.2(8) .
C20 P2 C9 C10 64.5(8) .
Pt1 P2 C9 C10 -168.5(7) .
C1 B5 B9 B11 -60.4(7) .
Cl5 B5 B9 B11 153.6(6) .
B1 B5 B9 B11 1.1(9) .
B10 B5 B9 B11 38.1(6) .
B4 B5 B9 B11 -100.0(7) .
C1 B5 B9 Cl9 150.5(6) .
Cl5 B5 B9 Cl9 4.5(10) .
B1 B5 B9 Cl9 -148.0(6) .
B10 B5 B9 Cl9 -111.0(7) .
B4 B5 B9 Cl9 110.8(7) .
C1 B5 B9 B10 -98.5(6) .
Cl5 B5 B9 B10 115.5(8) .
B1 B5 B9 B10 -37.0(6) .
B4 B5 B9 B10 -138.2(7) .
C1 B5 B9 B4 39.6(6) .
Cl5 B5 B9 B4 -106.3(8) .
B1 B5 B9 B4 101.1(7) .
B10 B5 B9 B4 138.2(7) .
C1 B5 B9 B8 2.9(7) .
Cl5 B5 B9 B8 -143.1(7) .
B1 B5 B9 B8 64.4(8) .
B10 B5 B9 B8 101.4(6) .
B4 B5 B9 B8 -36.7(6) .
Cl10 B10 B9 B11 111.5(6) .
B1 B10 B9 B11 -100.1(7) .
B5 B10 B9 B11 -137.1(7) .
B6 B10 B9 B11 -37.5(5) .
Cl10 B10 B9 Cl9 0.0(9) .
B11 B10 B9 Cl9 -111.5(6) .
B1 B10 B9 Cl9 148.4(6) .
B5 B10 B9 Cl9 111.4(7) .
B6 B10 B9 Cl9 -149.0(5) .
Cl10 B10 B9 B5 -111.4(7) .
B11 B10 B9 B5 137.1(7) .
B1 B10 B9 B5 37.0(6) .
B6 B10 B9 B5 99.6(6) .
Cl10 B10 B9 B4 -149.4(6) .
B11 B10 B9 B4 99.0(7) .
B1 B10 B9 B4 -1.1(9) .
B5 B10 B9 B4 -38.1(7) .
B6 B10 B9 B4 61.5(7) .
Cl10 B10 B9 B8 148.4(6) .
B11 B10 B9 B8 36.9(5) .
B1 B10 B9 B8 -63.3(7) .
B5 B10 B9 B8 -100.3(6) .
B6 B10 B9 B8 -0.6(7) .
C1 B4 B9 B11 62.4(8) .
Cl4 B4 B9 B11 -151.7(7) .
B8 B4 B9 B11 -37.0(6) .
B3 B4 B9 B11 1.3(8) .
B5 B4 B9 B11 101.1(6) .
C1 B4 B9 Cl9 -150.5(6) .
Cl4 B4 B9 Cl9 -4.6(11) .
B8 B4 B9 Cl9 110.1(7) .
B3 B4 B9 Cl9 148.4(6) .
B5 B4 B9 Cl9 -111.8(7) .
C1 B4 B9 B5 -38.8(6) .
Cl4 B4 B9 B5 107.2(8) .
B8 B4 B9 B5 -138.1(6) .
B3 B4 B9 B5 -99.8(7) .
C1 B4 B9 B10 -1.0(9) .
Cl4 B4 B9 B10 145.0(7) .
B8 B4 B9 B10 -100.3(7) .
B3 B4 B9 B10 -62.0(8) .
B5 B4 B9 B10 37.8(6) .
C1 B4 B9 B8 99.3(7) .
Cl4 B4 B9 B8 -114.8(8) .
B3 B4 B9 B8 38.3(6) .
B5 B4 B9 B8 138.1(6) .
B3 B8 B9 B11 99.7(6) .
B4 B8 B9 B11 138.4(6) .
Cl8 B8 B9 B11 -111.0(6) .
B7 B8 B9 B11 37.0(5) .
B3 B8 B9 Cl9 -148.6(6) .
B4 B8 B9 Cl9 -110.0(6) .
Cl8 B8 B9 Cl9 0.7(9) .
B11 B8 B9 Cl9 111.6(6) .
B7 B8 B9 Cl9 148.6(5) .
B3 B8 B9 B5 -0.9(8) .
B4 B8 B9 B5 37.8(5) .
Cl8 B8 B9 B5 148.4(6) .
B11 B8 B9 B5 -100.6(6) .
B7 B8 B9 B5 -63.6(7) .
B3 B8 B9 B10 62.9(7) .
B4 B8 B9 B10 101.6(6) .
Cl8 B8 B9 B10 -147.8(5) .
B11 B8 B9 B10 -36.8(5) .
B7 B8 B9 B10 0.1(7) .
B3 B8 B9 B4 -38.7(6) .
Cl8 B8 B9 B4 110.6(7) .
B11 B8 B9 B4 -138.4(6) .
B7 B8 B9 B4 -101.4(6) .
B2 C1 B3 B8 -103.2(6) .
B5 C1 B3 B8 3.6(8) .
B1 C1 B3 B8 -66.8(8) .
B4 C1 B3 B8 40.4(6) .
B2 C1 B3 B7 -39.6(6) .
B5 C1 B3 B7 67.3(8) .
B1 C1 B3 B7 -3.1(8) .
B4 C1 B3 B7 104.0(6) .
B2 C1 B3 Cl3 107.7(7) .
B5 C1 B3 Cl3 -145.5(6) .
B1 C1 B3 Cl3 144.1(6) .
B4 C1 B3 Cl3 -108.7(7) .
B2 C1 B3 B4 -143.6(6) .
B5 C1 B3 B4 -36.8(6) .
B1 C1 B3 B4 -107.2(7) .
B5 C1 B3 B2 106.8(7) .
B1 C1 B3 B2 36.4(6) .
B4 C1 B3 B2 143.6(6) .
B4 B8 B3 C1 -40.0(6) .
Cl8 B8 B3 C1 -150.8(6) .
B11 B8 B3 C1 60.2(8) .
B7 B8 B3 C1 98.2(7) .
B9 B8 B3 C1 -1.5(8) .
B4 B8 B3 B7 -138.2(7) .
Cl8 B8 B3 B7 110.9(8) .
B11 B8 B3 B7 -38.1(6) .
B9 B8 B3 B7 -99.7(7) .
B4 B8 B3 Cl3 107.7(8) .
Cl8 B8 B3 Cl3 -3.2(12) .
B11 B8 B3 Cl3 -152.2(7) .
B7 B8 B3 Cl3 -114.1(9) .
B9 B8 B3 Cl3 146.1(7) .
Cl8 B8 B3 B4 -110.9(7) .
B11 B8 B3 B4 100.1(7) .
B7 B8 B3 B4 138.2(7) .
B9 B8 B3 B4 38.4(6) .
B4 B8 B3 B2 -101.0(7) .
Cl8 B8 B3 B2 148.2(7) .
B11 B8 B3 B2 -0.8(9) .
B7 B8 B3 B2 37.2(7) .
B9 B8 B3 B2 -62.5(8) .
B2 B7 B3 C1 38.9(6) .
Cl7 B7 B3 C1 149.0(6) .
B6 B7 B3 C1 1.6(8) .
B11 B7 B3 C1 -61.7(7) .
B8 B7 B3 C1 -99.4(7) .
B2 B7 B3 B8 138.4(7) .
Cl7 B7 B3 B8 -111.6(8) .
B6 B7 B3 B8 101.0(7) .
B11 B7 B3 B8 37.8(6) .
B2 B7 B3 Cl3 -106.9(8) .
Cl7 B7 B3 Cl3 3.2(10) .
B6 B7 B3 Cl3 -144.3(6) .
B11 B7 B3 Cl3 152.5(6) .
B8 B7 B3 Cl3 114.8(8) .
B2 B7 B3 B4 100.7(7) .
Cl7 B7 B3 B4 -149.2(6) .
B6 B7 B3 B4 63.3(8) .
B11 B7 B3 B4 0.1(8) .
B8 B7 B3 B4 -37.7(6) .
Cl7 B7 B3 B2 110.1(8) .
B6 B7 B3 B2 -37.4(6) .
B11 B7 B3 B2 -100.6(7) .
B8 B7 B3 B2 -138.4(7) .
Cl4 B4 B3 C1 -110.6(6) .
B8 B4 B3 C1 133.7(6) .
B9 B4 B3 C1 94.5(6) .
B5 B4 B3 C1 32.4(5) .
C1 B4 B3 B8 -133.7(6) .
Cl4 B4 B3 B8 115.8(7) .
B9 B4 B3 B8 -39.2(6) .
B5 B4 B3 B8 -101.2(6) .
C1 B4 B3 B7 -95.4(7) .
Cl4 B4 B3 B7 154.1(6) .
B8 B4 B3 B7 38.3(6) .
B9 B4 B3 B7 -0.9(8) .
B5 B4 B3 B7 -63.0(7) .
C1 B4 B3 Cl3 110.7(7) .
Cl4 B4 B3 Cl3 0.2(9) .
B8 B4 B3 Cl3 -115.6(7) .
B9 B4 B3 Cl3 -154.8(6) .
B5 B4 B3 Cl3 143.2(6) .
C1 B4 B3 B2 -32.1(5) .
Cl4 B4 B3 B2 -142.7(6) .
B8 B4 B3 B2 101.5(6) .
B9 B4 B3 B2 62.4(7) .
B5 B4 B3 B2 0.3(7) .
B6 B2 B3 C1 -96.3(7) .
B7 B2 B3 C1 -134.2(7) .
Cl2 B2 B3 C1 110.1(7) .
B1 B2 B3 C1 -32.8(5) .
C1 B2 B3 B8 96.2(7) .
B6 B2 B3 B8 -0.1(9) .
B7 B2 B3 B8 -38.0(7) .
Cl2 B2 B3 B8 -153.7(6) .
B1 B2 B3 B8 63.4(8) .
C1 B2 B3 B7 134.2(7) .
B6 B2 B3 B7 37.9(6) .
Cl2 B2 B3 B7 -115.6(8) .
B1 B2 B3 B7 101.4(7) .
C1 B2 B3 Cl3 -110.6(7) .
B6 B2 B3 Cl3 153.1(6) .
B7 B2 B3 Cl3 115.1(8) .
Cl2 B2 B3 Cl3 -0.5(10) .
B1 B2 B3 Cl3 -143.5(6) .
C1 B2 B3 B4 32.5(5) .
B6 B2 B3 B4 -63.8(8) .
B7 B2 B3 B4 -101.8(7) .
Cl2 B2 B3 B4 142.6(6) .
B1 B2 B3 B4 -0.4(8) .
C9 C10 C11 C12 -0.7(16) .
Cl9 B9 B11 B10 110.7(7) .
B5 B9 B11 B10 -38.3(6) .
B4 B9 B11 B10 -102.5(6) .
B8 B9 B11 B10 -138.9(6) .
Cl9 B9 B11 Cl11 1.7(10) .
B5 B9 B11 Cl11 -147.4(6) .
B10 B9 B11 Cl11 -109.0(7) .
B4 B9 B11 Cl11 148.4(6) .
B8 B9 B11 Cl11 112.1(7) .
Cl9 B9 B11 B6 148.7(6) .
B5 B9 B11 B6 -0.4(8) .
B10 B9 B11 B6 38.0(6) .
B4 B9 B11 B6 -64.6(7) .
B8 B9 B11 B6 -100.9(6) .
Cl9 B9 B11 B8 -110.4(7) .
B5 B9 B11 B8 100.5(7) .
B10 B9 B11 B8 138.9(6) .
B4 B9 B11 B8 36.3(5) .
Cl9 B9 B11 B7 -148.0(6) .
B5 B9 B11 B7 62.9(8) .
B10 B9 B11 B7 101.2(6) .
B4 B9 B11 B7 -1.3(8) .
B8 B9 B11 B7 -37.6(6) .
Cl10 B10 B11 B9 -111.1(7) .
B1 B10 B11 B9 100.8(6) .
B5 B10 B11 B9 37.7(5) .
B6 B10 B11 B9 138.1(6) .
Cl10 B10 B11 Cl11 1.2(9) .
B1 B10 B11 Cl11 -146.9(5) .
B9 B10 B11 Cl11 112.3(6) .
B5 B10 B11 Cl11 150.0(5) .
B6 B10 B11 Cl11 -109.7(6) .
Cl10 B10 B11 B6 110.8(7) .
B1 B10 B11 B6 -37.3(5) .
B9 B10 B11 B6 -138.1(6) .
B5 B10 B11 B6 -100.4(6) .
Cl10 B10 B11 B8 -149.0(6) .
B1 B10 B11 B8 62.9(7) .
B9 B10 B11 B8 -37.9(6) .
B5 B10 B11 B8 -0.3(8) .
B6 B10 B11 B8 100.1(6) .
Cl10 B10 B11 B7 146.8(6) .
B1 B10 B11 B7 -1.3(7) .
B9 B10 B11 B7 -102.1(6) .
B5 B10 B11 B7 -64.5(7) .
B6 B10 B11 B7 35.9(5) .
Pt1 Cl11 B11 B9 -85.8(14) .
Pt1 Cl11 B11 B10 -157.9(9) .
Pt1 Cl11 B11 B6 130.8(10) .
Pt1 Cl11 B11 B8 -11.5(17) .
Pt1 Cl11 B11 B7 60.6(14) .
B2 B6 B11 B9 63.7(8) .
B1 B6 B11 B9 -0.5(8) .
Cl6 B6 B11 B9 -146.6(6) .
B7 B6 B11 B9 101.9(6) .
B10 B6 B11 B9 -37.9(6) .
B2 B6 B11 B10 101.6(7) .
B1 B6 B11 B10 37.4(6) .
Cl6 B6 B11 B10 -108.6(7) .
B7 B6 B11 B10 139.8(6) .
B2 B6 B11 Cl11 -148.5(6) .
B1 B6 B11 Cl11 147.3(6) .
Cl6 B6 B11 Cl11 1.3(10) .
B7 B6 B11 Cl11 -110.3(7) .
B10 B6 B11 Cl11 109.9(7) .
B2 B6 B11 B8 -1.5(8) .
B1 B6 B11 B8 -65.7(8) .
Cl6 B6 B11 B8 148.3(6) .
B7 B6 B11 B8 36.7(6) .
B10 B6 B11 B8 -103.1(6) .
B2 B6 B11 B7 -38.2(6) .
B1 B6 B11 B7 -102.4(7) .
Cl6 B6 B11 B7 111.5(8) .
B10 B6 B11 B7 -139.8(6) .
B3 B8 B11 B9 -100.6(7) .
B4 B8 B11 B9 -37.0(6) .
Cl8 B8 B11 B9 110.6(7) .
B7 B8 B11 B9 -138.4(6) .
B3 B8 B11 B10 -63.0(8) .
B4 B8 B11 B10 0.6(8) .
Cl8 B8 B11 B10 148.1(6) .
B7 B8 B11 B10 -100.9(6) .
B9 B8 B11 B10 37.5(5) .
B3 B8 B11 Cl11 147.5(6) .
B4 B8 B11 Cl11 -148.9(6) .
Cl8 B8 B11 Cl11 -1.4(10) .
B7 B8 B11 Cl11 109.7(7) .
B9 B8 B11 Cl11 -111.9(7) .
B3 B8 B11 B6 1.4(9) .
B4 B8 B11 B6 65.0(8) .
Cl8 B8 B11 B6 -147.4(6) .
B7 B8 B11 B6 -36.4(6) .
B9 B8 B11 B6 102.0(6) .
B3 B8 B11 B7 37.9(6) .
B4 B8 B11 B7 101.5(7) .
Cl8 B8 B11 B7 -111.0(8) .
B9 B8 B11 B7 138.4(6) .
B2 B7 B11 B9 -62.7(8) .
Cl7 B7 B11 B9 149.7(6) .
B3 B7 B11 B9 0.8(8) .
B6 B7 B11 B9 -100.9(6) .
B8 B7 B11 B9 38.2(6) .
B2 B7 B11 B10 1.7(8) .
Cl7 B7 B11 B10 -145.8(6) .
B3 B7 B11 B10 65.2(7) .
B6 B7 B11 B10 -36.4(6) .
B8 B7 B11 B10 102.7(6) .
B2 B7 B11 Cl11 147.1(6) .
Cl7 B7 B11 Cl11 -0.5(10) .
B3 B7 B11 Cl11 -149.4(6) .
B6 B7 B11 Cl11 108.9(6) .
B8 B7 B11 Cl11 -112.0(6) .
B2 B7 B11 B6 38.2(6) .
Cl7 B7 B11 B6 -109.4(8) .
B3 B7 B11 B6 101.7(7) .
B8 B7 B11 B6 139.1(6) .
B2 B7 B11 B8 -100.9(7) .
Cl7 B7 B11 B8 111.5(8) .
B3 B7 B11 B8 -37.4(6) .
B6 B7 B11 B8 -139.1(6) .
C10 C11 C12 C13 0.0(16) .
C9 P2 C20 C21 78.2(6) .
C23 P2 C20 C21 -167.4(5) .
Pt1 P2 C20 C21 -44.3(6) .
C9 P2 C20 C22 -48.7(7) .
C23 P2 C20 C22 65.7(7) .
Pt1 P2 C20 C22 -171.3(5) .
C11 C12 C13 C8 0.3(14) .
C9 C8 C13 C12 0.1(12) .
Si1 C8 C13 C12 176.0(7) .
C9 P2 C23 C24 -50.0(8) .
C20 P2 C23 C24 -167.9(7) .
Pt1 P2 C23 C24 66.2(7) .
C9 P2 C23 C25 -172.8(6) .
C20 P2 C23 C25 69.3(7) .
Pt1 P2 C23 C25 -56.5(6) .
C3 P1 C14 C15 175.6(6) .
C17 P1 C14 C15 -67.9(7) .
Pt1 P1 C14 C15 61.5(6) .
C3 P1 C14 C16 51.3(7) .
C17 P1 C14 C16 167.8(6) .
Pt1 P1 C14 C16 -62.8(6) .
C6_1 C1_1 C2_1 C3_1 1(2) .
F1_1 C1_1 C2_1 C3_1 179.0(11) .
C6_1 C1_1 C2_1 F2_1 179.5(12) .
F1_1 C1_1 C2_1 F2_1 -3.0(17) .
F2_1 C2_1 C3_1 C4_1 -176.8(12) .
C1_1 C2_1 C3_1 C4_1 1(2) .
C2_1 C3_1 C4_1 C5_1 -2(2) .
C3_1 C4_1 C5_1 C6_1 1(2) .
F1_1 C1_1 C6_1 C5_1 179.5(10) .
C2_1 C1_1 C6_1 C5_1 -3.1(19) .
C4_1 C5_1 C6_1 C1_1 1.8(19) .
C6_2 C1_2 C2_2 F2_2 179.2(12) .
F1_2 C1_2 C2_2 F2_2 4.5(19) .
C6_2 C1_2 C2_2 C3_2 -4(2) .
F1_2 C1_2 C2_2 C3_2 -178.9(11) .
F2_2 C2_2 C3_2 C4_2 -179.8(12) .
C1_2 C2_2 C3_2 C4_2 3.6(19) .
C2_2 C3_2 C4_2 C5_2 -2.3(18) .
C3_2 C4_2 C5_2 C6_2 1.6(19) .
F1_2 C1_2 C6_2 C5_2 177.7(11) .
C2_2 C1_2 C6_2 C5_2 3.0(19) .
C4_2 C5_2 C6_2 C1_2 -1.9(19) .
C6_3 C1_3 C2_3 F2_3 179(4) .
F1_3 C1_3 C2_3 F2_3 -1(7) .
C6_3 C1_3 C2_3 C3_3 4(8) .
F1_3 C1_3 C2_3 C3_3 -177(5) .
F2_3 C2_3 C3_3 C4_3 180(5) .
C1_3 C2_3 C3_3 C4_3 -5(10) .
C2_3 C3_3 C4_3 C5_3 4(8) .
C3_3 C4_3 C5_3 C6_3 -3(7) .
C2_3 C1_3 C6_3 C5_3 -2(5) .
F1_3 C1_3 C6_3 C5_3 178(4) .
C4_3 C5_3 C6_3 C1_3 2(6) .
C3 P1 C17 C19 -76.8(6) .
C14 P1 C17 C19 170.6(5) .
Pt1 P1 C17 C19 47.0(6) .
C3 P1 C17 C18 50.6(7) .
C14 P1 C17 C18 -62.0(6) .
Pt1 P1 C17 C18 174.4(5) .
