#------------------------------------------------------------------------------
#$Date: 2016-03-21 18:05:52 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178801 $
#$URL: svn://www.crystallography.net/cod/cif/4/10/55/4105505.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4105505
loop_
_publ_author_name
'Guang-Gang Gao'
'Ping-Shing Cheng'
'Thomas C. W. Mak'
_publ_section_title
;
 Acid-Induced Surface Functionalization of Polyoxometalate by Enclosure in
 a Polyhedral Silver-Alkynyl Cage
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              18257
_journal_page_last               18259
_journal_paper_doi               10.1021/ja907900b
_journal_volume                  131
_journal_year                    2009
_chemical_formula_moiety
;
C96 H126 Ag24 F18 O19 V2, 2(C H4 O)
;
_chemical_formula_sum            'C98 H134 Ag24 F18 O21 V2'
_chemical_formula_weight         4680.82
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                113.8210(10)
_cell_angle_beta                 101.1410(10)
_cell_angle_gamma                105.9020(10)
_cell_formula_units_Z            2
_cell_length_a                   15.1091(11)
_cell_length_b                   15.8098(12)
_cell_length_c                   16.8562(12)
_cell_measurement_reflns_used    3566
_cell_measurement_temperature    190(2)
_cell_measurement_theta_max      27.50
_cell_measurement_theta_min      1.80
_cell_volume                     3324.5(4)
_computing_cell_refinement       SAINT(Bruker,2001)
_computing_data_collection       APEX2(Bruker,2003)
_computing_data_reduction        APEX2(Bruker,2003)
_computing_molecular_graphics    DIAMOND
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_diffrn_ambient_temperature      190(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'SMART CCD APEX II'
_diffrn_measurement_method       ω
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0257
_diffrn_reflns_av_sigmaI/netI    0.0182
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_h_min       -18
_diffrn_reflns_limit_k_max       19
_diffrn_reflns_limit_k_min       -19
_diffrn_reflns_limit_l_max       20
_diffrn_reflns_limit_l_min       -20
_diffrn_reflns_number            61456
_diffrn_reflns_theta_full        26.00
_diffrn_reflns_theta_max         26.00
_diffrn_reflns_theta_min         1.67
_exptl_absorpt_coefficient_mu    3.653
_exptl_absorpt_correction_T_max  0.650
_exptl_absorpt_correction_T_min  0.560
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    4.678
_exptl_crystal_description       block
_exptl_crystal_F_000             2226
_exptl_crystal_size_max          0.16
_exptl_crystal_size_mid          0.14
_exptl_crystal_size_min          0.12
_refine_diff_density_max         1.677
_refine_diff_density_min         -1.357
_refine_diff_density_rms         0.149
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   0.994
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     692
_refine_ls_number_reflns         13001
_refine_ls_number_restraints     4
_refine_ls_restrained_S_all      0.998
_refine_ls_R_factor_all          0.0427
_refine_ls_R_factor_gt           0.0372
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0401P)²+26.8512P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0923
_refine_ls_wR_factor_ref         0.0981
_reflns_number_gt                11683
_reflns_number_total             13001
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ja907900b_si_002_3.cif
_cod_data_source_block           3
_cod_database_code               4105505
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1A Ag 0.7453(7) 0.4628(7) 0.7255(6) 0.076(2) Uani 0.30 1 d P
Ag1B Ag 0.7398(2) 0.4712(2) 0.7435(2) 0.0406(4) Uani 0.70 1 d P
Ag2 Ag 0.80265(3) 0.59882(3) 0.65973(3) 0.03749(11) Uani 1 1 d .
Ag3A Ag 0.6859(3) 0.66182(18) 0.7826(2) 0.0359(4) Uani 0.70 1 d P
Ag3B Ag 0.6944(7) 0.6563(7) 0.7892(7) 0.068(2) Uani 0.30 1 d P
Ag4 Ag 0.52837(3) 0.80125(3) 0.64107(3) 0.03852(11) Uani 1 1 d .
Ag5 Ag 0.68571(4) 0.72126(4) 0.64443(3) 0.04604(12) Uani 1 1 d .
Ag6 Ag 0.72226(3) 0.55949(3) 0.45706(3) 0.03564(10) Uani 1 1 d .
Ag7 Ag 0.66681(4) 0.34036(4) 0.40546(3) 0.03905(11) Uani 1 1 d .
Ag8 Ag 0.60368(4) 0.54273(3) 0.28823(3) 0.03744(11) Uani 1 1 d .
Ag9 Ag 0.69518(4) 0.74312(4) 0.48253(3) 0.04001(11) Uani 1 1 d .
Ag10 Ag 0.50769(3) 0.34745(4) 0.28417(4) 0.04280(12) Uani 1 1 d .
Ag11 Ag 0.36652(4) 0.74413(4) 0.45165(3) 0.03830(11) Uani 1 1 d .
Ag12 Ag 0.50248(3) 0.69436(4) 0.32691(3) 0.03827(11) Uani 1 1 d .
V V 0.54113(6) 0.44163(6) 0.55775(6) 0.02395(17) Uani 1 1 d .
O1 O 0.6524(3) 0.4498(4) 0.5552(3) 0.0600(15) Uani 1 1 d .
O2 O 0.5451(3) 0.4986(3) 0.6674(3) 0.0480(11) Uani 1 1 d .
O3 O 0.4645(4) 0.3201(4) 0.5032(4) 0.0640(16) Uani 1 1 d .
O4 O 0.4692(9) 0.4732(11) 0.4858(12) 0.094(5) Uani 0.50 1 d P
O5 O 0.8347(4) 0.4524(5) 0.4858(5) 0.0722(17) Uani 1 1 d .
O6 O 0.9042(5) 0.5061(5) 0.6338(5) 0.0751(17) Uani 1 1 d .
O7 O 0.7556(5) 0.9055(5) 0.6044(5) 0.098(3) Uani 1 1 d .
O8 O 0.6396(5) 0.9479(4) 0.6557(5) 0.0780(18) Uani 1 1 d .
O9 O 0.4212(4) 0.3289(4) 0.1283(4) 0.0616(14) Uani 1 1 d .
O10 O 0.5297(4) 0.4549(5) 0.1263(4) 0.0639(14) Uani 1 1 d .
O11 O 0.9239(6) 0.4638(6) 0.7822(6) 0.094(2) Uani 1 1 d .
H1O H 0.9241 0.4693 0.7343 0.113 Uiso 1 1 d R
C1 C 0.8211(5) 0.6310(5) 0.8056(4) 0.0439(15) Uani 1 1 d .
C2 C 0.8778(4) 0.6738(4) 0.8827(4) 0.0382(13) Uani 1 1 d .
C3 C 0.9539(5) 0.7282(5) 0.9762(4) 0.0474(16) Uani 1 1 d .
C4 C 1.0519(7) 0.7303(9) 0.9662(7) 0.092(3) Uani 1 1 d .
H4A H 1.0476 0.6627 0.9334 0.138 Uiso 1 1 calc R
H4B H 1.1014 0.7644 1.0264 0.138 Uiso 1 1 calc R
H4C H 1.0690 0.7651 0.9326 0.138 Uiso 1 1 calc R
C5 C 0.9300(9) 0.6703(11) 1.0286(7) 0.117(5) Uani 1 1 d .
H5A H 0.9265 0.6033 0.9942 0.175 Uiso 1 1 calc R
H5B H 0.8681 0.6673 1.0364 0.175 Uiso 1 1 calc R
H5C H 0.9804 0.7039 1.0882 0.175 Uiso 1 1 calc R
C6 C 0.9600(11) 0.8317(9) 1.0261(8) 0.143(7) Uani 1 1 d .
H6A H 1.0091 0.8661 1.0864 0.214 Uiso 1 1 calc R
H6B H 0.8977 0.8300 1.0320 0.214 Uiso 1 1 calc R
H6C H 0.9771 0.8664 0.9924 0.214 Uiso 1 1 calc R
C7 C 0.6666(4) 0.4336(4) 0.3225(4) 0.0303(11) Uani 1 1 d .
C8 C 0.6961(4) 0.3819(5) 0.2683(4) 0.0377(13) Uani 1 1 d .
C9 C 0.7369(6) 0.3255(7) 0.2029(5) 0.066(2) Uani 1 1 d .
C10 C 0.7226(10) 0.2211(9) 0.2030(9) 0.104(4) Uiso 1 1 d .
H10A H 0.7554 0.2344 0.2642 0.156 Uiso 1 1 calc R
H10B H 0.7499 0.1845 0.1609 0.156 Uiso 1 1 calc R
H10C H 0.6539 0.1820 0.1841 0.156 Uiso 1 1 calc R
C11 C 0.8467(10) 0.3794(11) 0.2420(10) 0.113(4) Uiso 1 1 d .
H11A H 0.8705 0.3901 0.3037 0.170 Uiso 1 1 calc R
H11B H 0.8644 0.4431 0.2430 0.170 Uiso 1 1 calc R
H11C H 0.8753 0.3396 0.2041 0.170 Uiso 1 1 calc R
C12 C 0.6877(11) 0.3009(11) 0.1109(10) 0.118(4) Uiso 1 1 d .
H12A H 0.7159 0.2639 0.0702 0.177 Uiso 1 1 calc R
H12B H 0.6944 0.3616 0.1079 0.177 Uiso 1 1 calc R
H12C H 0.6194 0.2607 0.0926 0.177 Uiso 1 1 calc R
C13 C 0.7987(4) 0.6973(4) 0.5799(4) 0.0346(12) Uani 1 1 d .
C14 C 0.8713(5) 0.7640(5) 0.6447(4) 0.0368(13) Uani 1 1 d .
C15 C 0.9606(5) 0.8496(5) 0.7199(5) 0.0476(16) Uani 1 1 d .
C16 C 0.9331(7) 0.9008(6) 0.8044(6) 0.073(3) Uani 1 1 d .
H16A H 0.9902 0.9562 0.8534 0.110 Uiso 1 1 calc R
H16B H 0.9073 0.8533 0.8243 0.110 Uiso 1 1 calc R
H16C H 0.8843 0.9249 0.7884 0.110 Uiso 1 1 calc R
C17 C 0.9997(6) 0.9214(7) 0.6854(8) 0.082(3) Uani 1 1 d .
H17A H 1.0578 0.9770 0.7329 0.124 Uiso 1 1 calc R
H17B H 0.9509 0.9456 0.6695 0.124 Uiso 1 1 calc R
H17C H 1.0152 0.8872 0.6317 0.124 Uiso 1 1 calc R
C18 C 1.0352(6) 0.8089(6) 0.7457(6) 0.064(2) Uani 1 1 d .
H18A H 1.0934 0.8636 0.7940 0.095 Uiso 1 1 calc R
H18B H 1.0513 0.7744 0.6925 0.095 Uiso 1 1 calc R
H18C H 1.0081 0.7631 0.7668 0.095 Uiso 1 1 calc R
C19 C 0.6311(4) 0.7798(4) 0.7532(4) 0.0360(12) Uani 1 1 d .
C20 C 0.6421(4) 0.8528(5) 0.8228(5) 0.0410(14) Uani 1 1 d .
C21 C 0.6610(7) 0.9421(6) 0.9092(6) 0.068(2) Uani 1 1 d .
C22 C 0.759(2) 0.978(2) 0.9646(19) 0.245(13) Uiso 1 1 d .
H22A H 0.7687 0.9272 0.9790 0.367 Uiso 1 1 calc R
H22B H 0.7740 1.0376 1.0207 0.367 Uiso 1 1 calc R
H22C H 0.8012 0.9921 0.9319 0.367 Uiso 1 1 calc R
C23 C 0.5992(14) 0.9199(14) 0.9609(13) 0.155(6) Uiso 1 1 d .
H23A H 0.5315 0.8942 0.9239 0.233 Uiso 1 1 calc R
H23B H 0.6143 0.9803 1.0168 0.233 Uiso 1 1 calc R
H23C H 0.6111 0.8707 0.9759 0.233 Uiso 1 1 calc R
C24 C 0.6604(19) 1.0246(19) 0.8942(18) 0.224(11) Uiso 1 1 d .
H24A H 0.5972 1.0067 0.8521 0.336 Uiso 1 1 calc R
H24B H 0.7098 1.0407 0.8685 0.336 Uiso 1 1 calc R
H24C H 0.6735 1.0819 0.9519 0.336 Uiso 1 1 calc R
C25 C 0.6465(4) 0.7115(5) 0.3322(4) 0.0366(13) Uani 1 1 d .
C26 C 0.7288(5) 0.7323(5) 0.3307(5) 0.0438(15) Uani 1 1 d .
C27 C 0.8257(6) 0.7543(8) 0.3178(7) 0.078(3) Uani 1 1 d D
C28 C 0.9014(11) 0.7655(12) 0.3939(9) 0.135(5) Uiso 1 1 d D
H28A H 0.8742 0.7180 0.4132 0.203 Uiso 1 1 calc R
H28B H 0.9257 0.8325 0.4447 0.203 Uiso 1 1 calc R
H28C H 0.9542 0.7535 0.3738 0.203 Uiso 1 1 calc R
C29 C 0.8134(16) 0.6564(11) 0.2318(10) 0.198(9) Uiso 1 1 d D
H29A H 0.7655 0.6451 0.1781 0.297 Uiso 1 1 calc R
H29B H 0.7921 0.6002 0.2425 0.297 Uiso 1 1 calc R
H29C H 0.8751 0.6640 0.2223 0.297 Uiso 1 1 calc R
C30 C 0.8424(12) 0.8284(11) 0.2853(11) 0.133(5) Uiso 1 1 d D
H30A H 0.7824 0.8144 0.2411 0.199 Uiso 1 1 calc R
H30B H 0.8914 0.8248 0.2567 0.199 Uiso 1 1 calc R
H30C H 0.8645 0.8946 0.3367 0.199 Uiso 1 1 calc R
C31 C 0.3789(5) 0.8027(5) 0.5982(4) 0.0382(13) Uani 1 1 d .
C32 C 0.3649(5) 0.8752(5) 0.6001(5) 0.0431(14) Uani 1 1 d .
C33 C 0.3499(7) 0.9685(6) 0.6123(7) 0.068(2) Uani 1 1 d .
C34 C 0.3583(10) 1.0280(8) 0.7125(8) 0.107(4) Uani 1 1 d .
H34A H 0.3492 1.0888 0.7221 0.161 Uiso 1 1 calc R
H34B H 0.4220 1.0445 0.7526 0.161 Uiso 1 1 calc R
H34C H 0.3090 0.9884 0.7258 0.161 Uiso 1 1 calc R
C35 C 0.2468(10) 0.9391(9) 0.5476(10) 0.117(5) Uani 1 1 d .
H35A H 0.2365 0.9987 0.5552 0.175 Uiso 1 1 calc R
H35B H 0.1985 0.9005 0.5627 0.175 Uiso 1 1 calc R
H35C H 0.2411 0.8996 0.4847 0.175 Uiso 1 1 calc R
C36 C 0.4265(11) 1.0268(8) 0.5875(11) 0.121(5) Uani 1 1 d .
H36A H 0.4184 1.0876 0.5957 0.181 Uiso 1 1 calc R
H36B H 0.4191 0.9867 0.5242 0.181 Uiso 1 1 calc R
H36C H 0.4906 1.0431 0.6268 0.181 Uiso 1 1 calc R
C37 C 0.3527(4) 0.6935(4) 0.3127(4) 0.0352(12) Uani 1 1 d .
C38 C 0.3404(4) 0.6695(5) 0.2313(4) 0.0369(13) Uani 1 1 d .
C39 C 0.3219(6) 0.6537(6) 0.1361(5) 0.0546(18) Uani 1 1 d .
C40 C 0.3437(7) 0.5637(7) 0.0787(5) 0.070(2) Uani 1 1 d .
H40A H 0.3317 0.5538 0.0169 0.105 Uiso 1 1 calc R
H40B H 0.3020 0.5046 0.0771 0.105 Uiso 1 1 calc R
H40C H 0.4111 0.5763 0.1060 0.105 Uiso 1 1 calc R
C41 C 0.3907(9) 0.7503(8) 0.1425(7) 0.086(3) Uani 1 1 d .
H41A H 0.3806 0.7427 0.0815 0.129 Uiso 1 1 calc R
H41B H 0.4576 0.7622 0.1706 0.129 Uiso 1 1 calc R
H41C H 0.3767 0.8063 0.1792 0.129 Uiso 1 1 calc R
C42 C 0.2152(7) 0.6338(8) 0.0932(6) 0.079(3) Uani 1 1 d .
H42A H 0.2029 0.6235 0.0313 0.119 Uiso 1 1 calc R
H42B H 0.2017 0.6905 0.1292 0.119 Uiso 1 1 calc R
H42C H 0.1736 0.5749 0.0920 0.119 Uiso 1 1 calc R
C43 C 0.8844(6) 0.4530(6) 0.5504(6) 0.0601(19) Uani 1 1 d .
C44 C 0.9359(8) 0.3773(9) 0.5284(7) 0.078(3) Uani 1 1 d .
F1 F 1.0271(6) 0.4129(7) 0.5794(8) 0.153(4) Uani 1 1 d .
F2 F 0.8908(7) 0.2981(7) 0.5103(15) 0.324(13) Uani 1 1 d .
F3 F 0.9647(8) 0.3746(8) 0.4563(8) 0.167(4) Uiso 1 1 d .
C45 C 0.7204(6) 0.9625(5) 0.6453(5) 0.0492(17) Uani 1 1 d .
C46 C 0.7895(6) 1.0741(5) 0.6958(6) 0.0558(18) Uani 1 1 d .
C47 C 0.4567(6) 0.3769(6) 0.0919(5) 0.0472(16) Uani 1 1 d .
F4 F 0.7434(4) 1.1315(4) 0.6872(5) 0.096(2) Uani 1 1 d .
F5 F 0.8278(6) 1.1058(5) 0.7844(4) 0.130(3) Uani 1 1 d .
F6 F 0.8634(5) 1.0944(5) 0.6681(6) 0.104(2) Uani 1 1 d .
C48 C 0.4046(6) 0.3289(7) -0.0126(6) 0.061(2) Uani 1 1 d .
C49 C 0.9371(13) 0.3711(13) 0.7603(12) 0.144(6) Uiso 1 1 d .
H49A H 0.9964 0.3756 0.7465 0.216 Uiso 1 1 calc R
H49B H 0.8823 0.3166 0.7077 0.216 Uiso 1 1 calc R
H49C H 0.9413 0.3593 0.8123 0.216 Uiso 1 1 calc R
F7 F 0.3073(6) 0.2994(6) -0.0311(6) 0.121(2) Uiso 1 1 d .
F8 F 0.4201(5) 0.2490(6) -0.0574(5) 0.110(2) Uiso 1 1 d .
F9 F 0.4246(5) 0.3862(5) -0.0489(4) 0.104(2) Uani 1 1 d .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
V V 0.3005 0.5294 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C1 Ag1A C37 159.0(4) . 2_666
C1 Ag1A C38 132.5(4) . 2_666
C37 Ag1A C38 28.3(2) 2_666 2_666
C1 Ag1A Ag2 51.3(2) . .
C37 Ag1A Ag2 145.2(4) 2_666 .
C38 Ag1A Ag2 169.3(4) 2_666 .
C1 Ag1A Ag11 155.2(4) . 2_666
C37 Ag1A Ag11 42.4(2) 2_666 2_666
C38 Ag1A Ag11 70.6(3) 2_666 2_666
Ag2 Ag1A Ag11 104.3(3) . 2_666
C1 Ag1A Ag3B 40.1(3) . .
C37 Ag1A Ag3B 127.2(4) 2_666 .
C38 Ag1A Ag3B 116.0(3) 2_666 .
Ag2 Ag1A Ag3B 59.3(2) . .
Ag11 Ag1A Ag3B 128.9(4) 2_666 .
C1 Ag1A Ag3A 41.7(2) . .
C37 Ag1A Ag3A 126.6(3) 2_666 .
C38 Ag1A Ag3A 116.7(3) 2_666 .
Ag2 Ag1A Ag3A 58.19(17) . .
Ag11 Ag1A Ag3A 126.5(3) 2_666 .
Ag3B Ag1A Ag3A 2.6(2) . .
C1 Ag1B C37 174.9(3) . 2_666
C1 Ag1B C38 146.3(3) . 2_666
C37 Ag1B C38 29.7(2) 2_666 2_666
C1 Ag1B Ag2 49.04(19) . .
C37 Ag1B Ag2 134.7(2) 2_666 .
C38 Ag1B Ag2 164.2(2) 2_666 .
C1 Ag1B Ag3B 42.7(3) . .
C37 Ag1B Ag3B 133.9(3) 2_666 .
C38 Ag1B Ag3B 125.9(3) 2_666 .
Ag2 Ag1B Ag3B 59.7(2) . .
C1 Ag1B Ag3A 44.25(19) . .
C37 Ag1B Ag3A 132.63(18) 2_666 .
C38 Ag1B Ag3A 126.20(17) 2_666 .
Ag2 Ag1B Ag3A 58.72(8) . .
Ag3B Ag1B Ag3A 2.5(3) . .
C1 Ag1B Ag11 145.3(2) . 2_666
C37 Ag1B Ag11 38.78(16) 2_666 2_666
C38 Ag1B Ag11 68.36(17) 2_666 2_666
Ag2 Ag1B Ag11 96.32(9) . 2_666
Ag3B Ag1B Ag11 127.0(2) . 2_666
Ag3A Ag1B Ag11 124.50(11) . 2_666
C1 Ag2 O6 97.1(2) . .
C1 Ag2 C13 134.2(2) . .
O6 Ag2 C13 116.5(2) . .
C1 Ag2 O1 109.1(2) . .
O6 Ag2 O1 93.1(2) . .
C13 Ag2 O1 99.8(2) . .
C1 Ag2 C14 113.3(2) . .
O6 Ag2 C14 111.6(2) . .
C13 Ag2 C14 27.13(19) . .
O1 Ag2 C14 126.8(2) . .
C1 Ag2 Ag1A 51.3(2) . .
O6 Ag2 Ag1A 74.7(2) . .
C13 Ag2 Ag1A 162.5(2) . .
O1 Ag2 Ag1A 65.0(2) . .
C14 Ag2 Ag1A 164.6(2) . .
C1 Ag2 Ag1B 46.60(17) . .
O6 Ag2 Ag1B 79.09(17) . .
C13 Ag2 Ag1B 161.27(15) . .
O1 Ag2 Ag1B 67.57(16) . .
C14 Ag2 Ag1B 159.53(15) . .
Ag1A Ag2 Ag1B 5.5(2) . .
C1 Ag2 Ag3B 43.5(3) . .
O6 Ag2 Ag3B 136.8(2) . .
C13 Ag2 Ag3B 105.9(2) . .
O1 Ag2 Ag3B 87.2(2) . .
C14 Ag2 Ag3B 102.3(2) . .
Ag1A Ag2 Ag3B 66.4(2) . .
Ag1B Ag2 Ag3B 61.19(16) . .
C1 Ag2 Ag5 99.01(18) . .
O6 Ag2 Ag5 162.95(16) . .
C13 Ag2 Ag5 46.99(14) . .
O1 Ag2 Ag5 86.98(14) . .
C14 Ag2 Ag5 56.40(13) . .
Ag1A Ag2 Ag5 120.27(16) . .
Ag1B Ag2 Ag5 116.37(5) . .
Ag3B Ag2 Ag5 60.21(16) . .
C1 Ag2 Ag3A 47.28(19) . .
O6 Ag2 Ag3A 140.75(17) . .
C13 Ag2 Ag3A 102.22(15) . .
O1 Ag2 Ag3A 86.28(12) . .
C14 Ag2 Ag3A 99.71(14) . .
Ag1A Ag2 Ag3A 69.57(16) . .
Ag1B Ag2 Ag3A 64.41(6) . .
Ag3B Ag2 Ag3A 4.0(2) . .
Ag5 Ag2 Ag3A 56.29(6) . .
C1 Ag2 Ag6 164.25(18) . .
O6 Ag2 Ag6 96.98(16) . .
C13 Ag2 Ag6 42.11(14) . .
O1 Ag2 Ag6 63.07(14) . .
C14 Ag2 Ag6 67.53(13) . .
Ag1A Ag2 Ag6 126.77(19) . .
Ag1B Ag2 Ag6 130.21(7) . .
Ag3B Ag2 Ag6 120.84(18) . .
Ag5 Ag2 Ag6 67.865(15) . .
Ag3A Ag2 Ag6 117.11(7) . .
C1 Ag3A O9 127.9(3) . 2_666
C1 Ag3A C19 139.3(3) . .
O9 Ag3A C19 82.9(2) 2_666 .
C1 Ag3A O2 108.1(2) . .
O9 Ag3A O2 82.6(2) 2_666 .
C19 Ag3A O2 101.0(2) . .
C1 Ag3A Ag5 104.5(2) . .
O9 Ag3A Ag5 126.84(18) 2_666 .
C19 Ag3A Ag5 46.91(16) . .
O2 Ag3A Ag5 90.03(16) . .
C1 Ag3A Ag10 166.0(2) . 2_666
O9 Ag3A Ag10 57.25(16) 2_666 2_666
C19 Ag3A Ag10 49.18(15) . 2_666
O2 Ag3A Ag10 58.25(14) . 2_666
Ag5 Ag3A Ag10 74.20(8) . 2_666
C1 Ag3A Ag2 47.78(19) . .
O9 Ag3A Ag2 166.48(17) 2_666 .
C19 Ag3A Ag2 107.75(19) . .
O2 Ag3A Ag2 87.17(13) . .
Ag5 Ag3A Ag2 61.67(7) . .
Ag10 Ag3A Ag2 123.55(12) 2_666 .
C1 Ag3A Ag1B 42.60(17) . .
O9 Ag3A Ag1B 110.61(17) 2_666 .
C19 Ag3A Ag1B 159.4(2) . .
O2 Ag3A Ag1B 66.95(14) . .
Ag5 Ag3A Ag1B 114.36(12) . .
Ag10 Ag3A Ag1B 124.68(11) 2_666 .
Ag2 Ag3A Ag1B 56.86(7) . .
C1 Ag3A Ag1A 42.1(2) . .
O9 Ag3A Ag1A 115.0(2) 2_666 .
C19 Ag3A Ag1A 154.9(2) . .
O2 Ag3A Ag1A 66.3(2) . .
Ag5 Ag3A Ag1A 109.42(17) . .
Ag10 Ag3A Ag1A 124.54(19) 2_666 .
Ag2 Ag3A Ag1A 52.24(14) . .
Ag1B Ag3A Ag1A 4.95(19) . .
C1 Ag3B O9 135.9(5) . 2_666
C1 Ag3B O2 112.5(4) . .
O9 Ag3B O2 81.1(3) 2_666 .
C1 Ag3B C19 137.4(5) . .
O9 Ag3B C19 78.3(3) 2_666 .
O2 Ag3B C19 94.7(4) . .
C1 Ag3B Ag2 48.9(3) . .
O9 Ag3B Ag2 168.4(4) 2_666 .
O2 Ag3B Ag2 87.3(3) . .
C19 Ag3B Ag2 103.7(3) . .
C1 Ag3B Ag5 104.0(4) . .
O9 Ag3B Ag5 119.1(3) 2_666 .
O2 Ag3B Ag5 85.7(3) . .
C19 Ag3B Ag5 43.88(19) . .
Ag2 Ag3B Ag5 60.4(2) . .
C1 Ag3B Ag1B 45.6(2) . .
O9 Ag3B Ag1B 115.2(4) 2_666 .
O2 Ag3B Ag1B 69.3(2) . .
C19 Ag3B Ag1B 155.8(4) . .
Ag2 Ag3B Ag1B 59.07(18) . .
Ag5 Ag3B Ag1B 114.6(3) . .
C1 Ag3B Ag10 165.7(5) . 2_666
O9 Ag3B Ag10 54.3(2) 2_666 2_666
O2 Ag3B Ag10 55.4(2) . 2_666
C19 Ag3B Ag10 45.78(19) . 2_666
Ag2 Ag3B Ag10 118.9(3) . 2_666
Ag5 Ag3B Ag10 69.46(19) . 2_666
Ag1B Ag3B Ag10 124.3(3) . 2_666
C1 Ag3B Ag1A 44.9(3) . .
O9 Ag3B Ag1A 119.6(4) 2_666 .
O2 Ag3B Ag1A 68.6(3) . .
C19 Ag3B Ag1A 151.3(4) . .
Ag2 Ag3B Ag1A 54.2(2) . .
Ag5 Ag3B Ag1A 109.5(3) . .
Ag1B Ag3B Ag1A 5.1(2) . .
Ag10 Ag3B Ag1A 124.0(4) 2_666 .
C31 Ag4 O8 106.3(2) . .
C31 Ag4 C19 140.8(2) . .
O8 Ag4 C19 99.9(2) . .
C31 Ag4 O3 103.6(2) . 2_666
O8 Ag4 O3 98.0(2) . 2_666
C19 Ag4 O3 101.0(2) . 2_666
C31 Ag4 Ag7 47.30(16) . 2_666
O8 Ag4 Ag7 153.52(17) . 2_666
C19 Ag4 Ag7 104.21(14) . 2_666
O3 Ag4 Ag7 88.20(11) 2_666 2_666
C31 Ag4 Ag5 158.94(16) . .
O8 Ag4 Ag5 89.26(17) . .
C19 Ag4 Ag5 44.97(15) . .
O3 Ag4 Ag5 59.29(15) 2_666 .
Ag7 Ag4 Ag5 115.65(2) 2_666 .
C31 Ag4 Ag10 101.85(16) . 2_666
O8 Ag4 Ag10 146.04(17) . 2_666
C19 Ag4 Ag10 46.39(14) . 2_666
O3 Ag4 Ag10 93.38(15) 2_666 2_666
Ag7 Ag4 Ag10 58.156(16) 2_666 2_666
Ag5 Ag4 Ag10 69.383(17) . 2_666
C31 Ag4 Ag11 43.03(16) . .
O8 Ag4 Ag11 95.98(17) . .
C19 Ag4 Ag11 159.46(14) . .
O3 Ag4 Ag11 63.62(16) 2_666 .
Ag7 Ag4 Ag11 63.713(16) 2_666 .
Ag5 Ag4 Ag11 122.84(2) . .
Ag10 Ag4 Ag11 117.668(19) 2_666 .
C19 Ag5 C13 156.7(2) . .
C19 Ag5 C14 130.6(2) . .
C13 Ag5 C14 26.5(2) . .
C19 Ag5 Ag3A 56.05(17) . .
C13 Ag5 Ag3A 113.77(16) . .
C14 Ag5 Ag3A 103.50(14) . .
C19 Ag5 Ag9 136.29(16) . .
C13 Ag5 Ag9 56.36(14) . .
C14 Ag5 Ag9 71.03(13) . .
Ag3A Ag5 Ag9 167.25(6) . .
C19 Ag5 Ag4 52.84(16) . .
C13 Ag5 Ag4 142.00(14) . .
C14 Ag5 Ag4 141.48(13) . .
Ag3A Ag5 Ag4 104.21(7) . .
Ag9 Ag5 Ag4 86.189(19) . .
C19 Ag5 Ag3B 58.5(2) . .
C13 Ag5 Ag3B 111.0(2) . .
C14 Ag5 Ag3B 100.9(2) . .
Ag3A Ag5 Ag3B 2.8(2) . .
Ag9 Ag5 Ag3B 165.07(17) . .
Ag4 Ag5 Ag3B 106.96(18) . .
C19 Ag5 Ag2 117.08(16) . .
C13 Ag5 Ag2 53.03(14) . .
C14 Ag5 Ag2 55.43(12) . .
Ag3A Ag5 Ag2 62.04(6) . .
Ag9 Ag5 Ag2 106.30(2) . .
Ag4 Ag5 Ag2 162.88(2) . .
Ag3B Ag5 Ag2 59.40(18) . .
C13 Ag6 C7 168.0(2) . .
C13 Ag6 Ag9 57.10(15) . .
C7 Ag6 Ag9 119.67(15) . .
C13 Ag6 Ag8 122.58(15) . .
C7 Ag6 Ag8 53.69(15) . .
Ag9 Ag6 Ag8 66.142(16) . .
C13 Ag6 Ag7 135.38(15) . .
C7 Ag6 Ag7 52.27(14) . .
Ag9 Ag6 Ag7 158.25(2) . .
Ag8 Ag6 Ag7 101.112(18) . .
C13 Ag6 Ag2 51.07(15) . .
C7 Ag6 Ag2 136.23(15) . .
Ag9 Ag6 Ag2 103.088(18) . .
Ag8 Ag6 Ag2 162.80(2) . .
Ag7 Ag6 Ag2 84.503(17) . .
C31 Ag7 O5 118.5(2) 2_666 .
C31 Ag7 C7 148.3(2) 2_666 .
O5 Ag7 C7 84.3(2) . .
C31 Ag7 O1 101.2(2) 2_666 .
O5 Ag7 O1 81.3(2) . .
C7 Ag7 O1 104.1(2) . .
C31 Ag7 Ag4 50.18(17) 2_666 2_666
O5 Ag7 Ag4 162.37(17) . 2_666
C7 Ag7 Ag4 111.89(14) . 2_666
O1 Ag7 Ag4 87.72(11) . 2_666
C31 Ag7 Ag10 109.75(17) 2_666 .
O5 Ag7 Ag10 131.14(15) . .
C7 Ag7 Ag10 48.41(14) . .
O1 Ag7 Ag10 97.06(14) . .
Ag4 Ag7 Ag10 63.746(17) 2_666 .
C31 Ag7 Ag6 165.35(17) 2_666 .
O5 Ag7 Ag6 61.28(15) . .
C7 Ag7 Ag6 44.24(13) . .
O1 Ag7 Ag6 64.20(14) . .
Ag4 Ag7 Ag6 125.49(2) 2_666 .
Ag10 Ag7 Ag6 74.068(16) . .
C31 Ag7 Ag11 42.51(16) 2_666 2_666
O5 Ag7 Ag11 99.32(16) . 2_666
C7 Ag7 Ag11 162.59(13) . 2_666
O1 Ag7 Ag11 60.11(15) . 2_666
Ag4 Ag7 Ag11 63.139(16) 2_666 2_666
Ag10 Ag7 Ag11 122.23(2) . 2_666
Ag6 Ag7 Ag11 123.18(2) . 2_666
C25 Ag8 O10 106.3(2) . .
C25 Ag8 C7 140.4(2) . .
O10 Ag8 C7 104.0(2) . .
C25 Ag8 O2 102.60(19) . 2_666
O10 Ag8 O2 99.78(18) . 2_666
C7 Ag8 O2 96.58(18) . 2_666
C25 Ag8 Ag6 99.69(15) . .
O10 Ag8 Ag6 149.55(15) . .
C7 Ag8 Ag6 45.81(13) . .
O2 Ag8 Ag6 89.54(12) 2_666 .
C25 Ag8 Ag10 157.44(15) . .
O10 Ag8 Ag10 86.94(15) . .
C7 Ag8 Ag10 47.08(14) . .
O2 Ag8 Ag10 56.36(11) 2_666 .
Ag6 Ag8 Ag10 74.178(17) . .
C25 Ag8 Ag12 42.49(15) . .
O10 Ag8 Ag12 97.11(15) . .
C7 Ag8 Ag12 153.11(13) . .
O2 Ag8 Ag12 63.15(12) 2_666 .
Ag6 Ag8 Ag12 112.86(2) . .
Ag10 Ag8 Ag12 119.12(2) . .
C25 Ag8 Ag9 46.03(15) . .
O10 Ag8 Ag9 152.09(15) . .
C7 Ag8 Ag9 102.49(14) . .
O2 Ag8 Ag9 85.69(10) 2_666 .
Ag6 Ag8 Ag9 56.807(16) . .
Ag10 Ag8 Ag9 117.96(2) . .
Ag12 Ag8 Ag9 60.806(16) . .
C25 Ag9 O7 121.0(3) . .
C25 Ag9 O3 100.2(2) . 2_666
O7 Ag9 O3 98.4(2) . 2_666
C25 Ag9 C13 138.3(2) . .
O7 Ag9 C13 89.9(2) . .
O3 Ag9 C13 102.1(2) 2_666 .
C25 Ag9 C26 27.0(2) . .
O7 Ag9 C26 114.0(3) . .
O3 Ag9 C26 126.7(2) 2_666 .
C13 Ag9 C26 118.16(19) . .
C25 Ag9 Ag5 158.40(15) . .
O7 Ag9 Ag5 74.5(2) . .
O3 Ag9 Ag5 60.58(15) 2_666 .
C13 Ag9 Ag5 47.98(14) . .
C26 Ag9 Ag5 165.19(13) . .
C25 Ag9 Ag6 100.40(15) . .
O7 Ag9 Ag6 134.76(19) . .
O3 Ag9 Ag6 90.85(15) 2_666 .
C13 Ag9 Ag6 44.88(14) . .
C26 Ag9 Ag6 94.14(14) . .
Ag5 Ag9 Ag6 72.074(17) . .
C25 Ag9 Ag12 41.15(15) . .
O7 Ag9 Ag12 112.33(17) . .
O3 Ag9 Ag12 60.91(15) 2_666 .
C13 Ag9 Ag12 152.89(14) . .
C26 Ag9 Ag12 67.90(15) . .
Ag5 Ag9 Ag12 121.45(2) . .
Ag6 Ag9 Ag12 110.834(19) . .
C25 Ag9 Ag8 46.54(15) . .
O7 Ag9 Ag8 167.4(2) . .
O3 Ag9 Ag8 84.38(10) 2_666 .
C13 Ag9 Ag8 101.50(14) . .
C26 Ag9 Ag8 55.90(16) . .
Ag5 Ag9 Ag8 117.13(2) . .
Ag6 Ag9 Ag8 57.051(15) . .
Ag12 Ag9 Ag8 58.356(15) . .
C7 Ag10 C19 159.5(2) . 2_666
C7 Ag10 O9 106.87(19) . .
C19 Ag10 O9 83.3(2) 2_666 .
C7 Ag10 Ag3A 145.05(15) . 2_666
C19 Ag10 Ag3A 54.96(16) 2_666 2_666
O9 Ag10 Ag3A 52.32(15) . 2_666
C7 Ag10 Ag7 54.17(14) . .
C19 Ag10 Ag7 108.79(15) 2_666 .
O9 Ag10 Ag7 150.75(13) . .
Ag3A Ag10 Ag7 155.58(7) 2_666 .
C7 Ag10 Ag8 51.91(14) . .
C19 Ag10 Ag8 147.99(15) 2_666 .
O9 Ag10 Ag8 72.70(13) . .
Ag3A Ag10 Ag8 93.19(5) 2_666 .
Ag7 Ag10 Ag8 102.36(2) . .
C7 Ag10 Ag3B 142.8(2) . 2_666
C19 Ag10 Ag3B 57.1(2) 2_666 2_666
O9 Ag10 Ag3B 50.7(2) . 2_666
Ag3A Ag10 Ag3B 2.3(2) 2_666 2_666
Ag7 Ag10 Ag3B 157.54(19) . 2_666
Ag8 Ag10 Ag3B 90.99(16) . 2_666
C7 Ag10 Ag4 111.99(14) . 2_666
C19 Ag10 Ag4 51.06(15) 2_666 2_666
O9 Ag10 Ag4 130.65(13) . 2_666
Ag3A Ag10 Ag4 101.75(6) 2_666 2_666
Ag7 Ag10 Ag4 58.097(16) . 2_666
Ag8 Ag10 Ag4 156.65(2) . 2_666
Ag3B Ag10 Ag4 104.07(17) 2_666 2_666
C37 Ag11 C31 177.5(2) . .
C37 Ag11 C32 149.0(2) . .
C31 Ag11 C32 28.5(2) . .
C37 Ag11 Ag1A 46.5(2) . 2_666
C31 Ag11 Ag1A 134.9(2) . 2_666
C32 Ag11 Ag1A 148.1(2) . 2_666
C37 Ag11 Ag4 137.75(16) . .
C31 Ag11 Ag4 43.94(16) . .
C32 Ag11 Ag4 63.36(15) . .
Ag1A Ag11 Ag4 128.61(17) 2_666 .
C37 Ag11 Ag12 43.00(16) . .
C31 Ag11 Ag12 138.52(17) . .
C32 Ag11 Ag12 143.13(15) . .
Ag1A Ag11 Ag12 68.78(14) 2_666 .
Ag4 Ag11 Ag12 94.793(18) . .
C37 Ag11 Ag7 140.88(15) . 2_666
C31 Ag11 Ag7 41.11(15) . 2_666
C32 Ag11 Ag7 67.56(15) . 2_666
Ag1A Ag11 Ag7 95.54(16) 2_666 2_666
Ag4 Ag11 Ag7 53.148(15) . 2_666
Ag12 Ag11 Ag7 124.380(18) . 2_666
C37 Ag11 Ag1B 42.71(17) . 2_666
C31 Ag11 Ag1B 138.78(17) . 2_666
C32 Ag11 Ag1B 152.21(16) . 2_666
Ag1A Ag11 Ag1B 4.33(18) 2_666 2_666
Ag4 Ag11 Ag1B 128.86(5) . 2_666
Ag12 Ag11 Ag1B 64.63(4) . 2_666
Ag7 Ag11 Ag1B 98.90(6) 2_666 2_666
C25 Ag12 C37 170.9(2) . .
C25 Ag12 C38 144.7(2) . .
C37 Ag12 C38 29.5(2) . .
C25 Ag12 Ag8 48.18(16) . .
C37 Ag12 Ag8 138.84(15) . .
C38 Ag12 Ag8 127.42(14) . .
C25 Ag12 Ag9 46.03(16) . .
C37 Ag12 Ag9 139.26(16) . .
C38 Ag12 Ag9 168.64(15) . .
Ag8 Ag12 Ag9 60.838(15) . .
C25 Ag12 Ag11 144.00(17) . .
C37 Ag12 Ag11 39.87(16) . .
C38 Ag12 Ag11 69.31(15) . .
Ag8 Ag12 Ag11 131.914(19) . .
Ag9 Ag12 Ag11 99.396(19) . .
O1 V O2 110.2(2) . .
O1 V O3 109.4(3) . .
O2 V O3 110.6(2) . .
O1 V O4 119.2(6) . .
O2 V O4 112.1(7) . .
O3 V O4 94.2(5) . .
O1 V O4 97.1(6) . 2_666
O2 V O4 105.6(7) . 2_666
O3 V O4 123.0(5) . 2_666
O4 V O4 30.4(7) . 2_666
V O1 Ag2 124.1(2) . .
V O1 Ag7 118.1(2) . .
Ag2 O1 Ag7 113.28(17) . .
V O2 Ag8 122.1(2) . 2_666
V O2 Ag3A 119.2(2) . .
Ag8 O2 Ag3A 116.21(18) 2_666 .
V O2 Ag3B 120.0(3) . .
Ag8 O2 Ag3B 116.7(3) 2_666 .
V O3 Ag9 124.8(3) . 2_666
V O3 Ag4 120.9(2) . 2_666
Ag9 O3 Ag4 110.46(17) 2_666 2_666
O4 O4 V 75.9(13) 2_666 .
O4 O4 V 73.7(14) 2_666 2_666
V O4 V 149.6(7) . 2_666
C43 O5 Ag7 122.1(6) . .
C43 O6 Ag2 110.6(6) . .
C45 O7 Ag9 135.9(6) . .
C45 O8 Ag4 128.3(5) . .
C47 O9 Ag3A 136.0(5) . 2_666
C47 O9 Ag3B 131.8(5) . 2_666
C47 O9 Ag10 126.0(5) . .
Ag3A O9 Ag10 70.42(16) 2_666 .
Ag3B O9 Ag10 75.0(3) 2_666 .
C47 O10 Ag8 117.7(5) . .
C2 C1 Ag3B 116.2(6) . .
C2 C1 Ag1B 118.0(5) . .
Ag3B C1 Ag1B 91.7(4) . .
C2 C1 Ag3A 117.7(6) . .
Ag1B C1 Ag3A 93.2(3) . .
C2 C1 Ag2 145.0(6) . .
Ag3B C1 Ag2 87.7(4) . .
Ag1B C1 Ag2 84.4(2) . .
Ag3A C1 Ag2 84.9(2) . .
C2 C1 Ag1A 122.1(5) . .
Ag1B C1 Ag1A 7.9(2) . .
Ag3A C1 Ag1A 96.2(3) . .
Ag2 C1 Ag1A 77.4(3) . .
C1 C2 C3 176.2(7) . .
C6 C3 C2 110.2(7) . .
C6 C3 C4 109.7(9) . .
C2 C3 C4 108.9(6) . .
C6 C3 C5 111.7(10) . .
C2 C3 C5 109.3(6) . .
C4 C3 C5 107.0(9) . .
C8 C7 Ag6 139.3(5) . .
C8 C7 Ag10 107.9(4) . .
Ag6 C7 Ag10 110.4(2) . .
C8 C7 Ag8 119.2(4) . .
Ag6 C7 Ag8 80.50(18) . .
Ag10 C7 Ag8 81.00(18) . .
C8 C7 Ag7 91.7(4) . .
Ag6 C7 Ag7 83.49(18) . .
Ag10 C7 Ag7 77.42(17) . .
Ag8 C7 Ag7 146.6(2) . .
C7 C8 C9 175.8(7) . .
C12 C9 C8 111.8(8) . .
C12 C9 C11 118.1(10) . .
C8 C9 C11 108.2(8) . .
C12 C9 C10 106.8(9) . .
C8 C9 C10 109.3(8) . .
C11 C9 C10 102.0(9) . .
C14 C13 Ag6 154.7(5) . .
C14 C13 Ag5 98.6(4) . .
Ag6 C13 Ag5 104.5(3) . .
C14 C13 Ag2 86.9(4) . .
Ag6 C13 Ag2 86.8(2) . .
Ag5 C13 Ag2 79.98(18) . .
C14 C13 Ag9 118.5(4) . .
Ag6 C13 Ag9 78.02(18) . .
Ag5 C13 Ag9 75.67(18) . .
Ag2 C13 Ag9 146.9(3) . .
C13 C14 C15 175.7(7) . .
C13 C14 Ag2 66.0(4) . .
C15 C14 Ag2 118.2(4) . .
C13 C14 Ag5 54.9(4) . .
C15 C14 Ag5 126.4(4) . .
Ag2 C14 Ag5 68.18(15) . .
C14 C15 C17 108.2(6) . .
C14 C15 C18 108.7(6) . .
C17 C15 C18 111.4(7) . .
C14 C15 C16 108.8(6) . .
C17 C15 C16 111.1(7) . .
C18 C15 C16 108.7(7) . .
C20 C19 Ag5 146.1(5) . .
C20 C19 Ag10 109.7(5) . 2_666
Ag5 C19 Ag10 104.1(2) . 2_666
C20 C19 Ag4 99.5(5) . .
Ag5 C19 Ag4 82.2(2) . .
Ag10 C19 Ag4 82.55(19) 2_666 .
C20 C19 Ag3A 113.4(5) . .
Ag5 C19 Ag3A 77.0(2) . .
Ag10 C19 Ag3A 75.85(19) 2_666 .
Ag4 C19 Ag3A 145.1(3) . .
C20 C19 Ag3B 112.0(5) . .
Ag5 C19 Ag3B 77.6(3) . .
Ag10 C19 Ag3B 77.1(3) 2_666 .
Ag4 C19 Ag3B 146.7(3) . .
C19 C20 C21 176.9(8) . .
C22 C21 C24 101.8(16) . .
C22 C21 C23 107.8(15) . .
C24 C21 C23 114.7(14) . .
C22 C21 C20 107.8(13) . .
C24 C21 C20 111.4(13) . .
C23 C21 C20 112.5(9) . .
C26 C25 Ag12 169.7(5) . .
C26 C25 Ag9 93.3(5) . .
Ag12 C25 Ag9 92.8(2) . .
C26 C25 Ag8 99.3(5) . .
Ag12 C25 Ag8 89.3(2) . .
Ag9 C25 Ag8 87.43(19) . .
C25 C26 C27 173.6(8) . .
C25 C26 Ag9 59.8(4) . .
C27 C26 Ag9 126.6(5) . .
C28 C27 C30 120.8(10) . .
C28 C27 C26 111.6(9) . .
C30 C27 C26 110.2(8) . .
C28 C27 C29 104.6(9) . .
C30 C27 C29 102.7(10) . .
C26 C27 C29 105.2(11) . .
C32 C31 Ag7 152.4(6) . 2_666
C32 C31 Ag11 90.9(5) . .
Ag7 C31 Ag11 96.4(2) 2_666 .
C32 C31 Ag4 123.7(5) . .
Ag7 C31 Ag4 82.52(19) 2_666 .
Ag11 C31 Ag4 93.0(2) . .
C31 C32 C33 174.5(8) . .
C31 C32 Ag11 60.6(4) . .
C33 C32 Ag11 124.9(6) . .
C32 C33 C36 108.3(8) . .
C32 C33 C34 107.9(8) . .
C36 C33 C34 111.9(10) . .
C32 C33 C35 109.0(7) . .
C36 C33 C35 109.9(10) . .
C34 C33 C35 109.8(10) . .
C38 C37 Ag11 174.2(5) . .
C38 C37 Ag12 87.2(4) . .
Ag11 C37 Ag12 97.1(2) . .
C38 C37 Ag1A 91.4(5) . 2_666
Ag11 C37 Ag1A 91.1(3) . 2_666
Ag12 C37 Ag1A 106.4(3) . 2_666
C38 C37 Ag1B 84.3(4) . 2_666
Ag11 C37 Ag1B 98.5(2) . 2_666
Ag12 C37 Ag1B 102.3(2) . 2_666
C37 C38 C39 171.6(6) . .
C37 C38 Ag1B 66.1(4) . 2_666
C39 C38 Ag1B 119.5(5) . 2_666
C37 C38 Ag12 63.3(4) . .
C39 C38 Ag12 121.2(5) . .
Ag1B C38 Ag12 89.80(19) 2_666 .
C37 C38 Ag1A 60.3(4) . 2_666
C39 C38 Ag1A 124.7(5) . 2_666
Ag12 C38 Ag1A 89.7(3) . 2_666
C38 C39 C42 109.2(7) . .
C38 C39 C40 109.7(6) . .
C42 C39 C40 109.6(7) . .
C38 C39 C41 107.2(6) . .
C42 C39 C41 110.7(8) . .
C40 C39 C41 110.3(8) . .
O5 C43 O6 130.2(9) . .
O5 C43 C44 116.6(8) . .
O6 C43 C44 113.2(8) . .
F2 C44 F1 115.6(12) . .
F2 C44 F3 108.5(14) . .
F1 C44 F3 89.3(10) . .
F2 C44 C43 116.6(10) . .
F1 C44 C43 115.8(10) . .
F3 C44 C43 106.8(9) . .
O7 C45 O8 132.2(7) . .
O7 C45 C46 114.3(8) . .
O8 C45 C46 113.4(7) . .
F6 C46 F5 105.8(8) . .
F6 C46 F4 106.1(7) . .
F5 C46 F4 107.2(8) . .
F6 C46 C45 114.8(7) . .
F5 C46 C45 110.4(6) . .
F4 C46 C45 112.0(7) . .
O10 C47 O9 129.4(7) . .
O10 C47 C48 115.6(6) . .
O9 C47 C48 115.0(7) . .
F9 C48 F8 108.4(7) . .
F9 C48 F7 104.4(8) . .
F8 C48 F7 106.7(8) . .
F9 C48 C47 116.4(8) . .
F8 C48 C47 111.0(7) . .
F7 C48 C47 109.3(7) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1A C1 2.245(11) .
Ag1A C37 2.248(11) 2_666
Ag1A C38 2.587(10) 2_666
Ag1A Ag2 2.807(9) .
Ag1A Ag11 3.099(9) 2_666
Ag1A Ag3B 3.171(11) .
Ag1A Ag3A 3.327(9) .
Ag1B C1 2.158(7) .
Ag1B C37 2.265(7) 2_666
Ag1B C38 2.466(7) 2_666
Ag1B Ag2 2.955(3) .
Ag1B Ag3B 3.019(9) .
Ag1B Ag3A 3.183(3) .
Ag1B Ag11 3.302(3) 2_666
Ag2 C1 2.243(7) .
Ag2 O6 2.382(6) .
Ag2 C13 2.439(5) .
Ag2 O1 2.445(5) .
Ag2 C14 2.666(6) .
Ag2 Ag3B 2.976(10) .
Ag2 Ag5 3.0061(7) .
Ag2 Ag3A 3.017(3) .
Ag2 Ag6 3.1303(7) .
Ag3A C1 2.225(8) .
Ag3A O9 2.406(6) 2_666
Ag3A C19 2.418(6) .
Ag3A O2 2.511(5) .
Ag3A Ag5 2.841(3) .
Ag3A Ag10 2.864(3) 2_666
Ag3B C1 2.050(12) .
Ag3B O9 2.437(12) 2_666
Ag3B O2 2.552(11) .
Ag3B C19 2.619(10) .
Ag3B Ag5 3.000(9) .
Ag3B Ag10 3.040(9) 2_666
Ag4 C31 2.244(6) .
Ag4 O8 2.346(6) .
Ag4 C19 2.401(6) .
Ag4 O3 2.460(4) 2_666
Ag4 Ag7 2.8973(7) 2_666
Ag4 Ag5 2.9845(7) .
Ag4 Ag10 3.0608(7) 2_666
Ag4 Ag11 3.2301(7) .
Ag5 C19 2.129(6) .
Ag5 C13 2.232(6) .
Ag5 C14 2.697(6) .
Ag5 Ag9 2.9110(7) .
Ag6 C13 2.102(6) .
Ag6 C7 2.124(6) .
Ag6 Ag9 2.9142(7) .
Ag6 Ag8 2.9223(7) .
Ag6 Ag7 3.0255(7) .
Ag7 C31 2.148(6) 2_666
Ag7 O5 2.383(6) .
Ag7 C7 2.408(5) .
Ag7 O1 2.511(4) .
Ag7 Ag4 2.8973(7) 2_666
Ag7 Ag10 2.8991(7) .
Ag7 Ag11 3.2464(6) 2_666
Ag8 C25 2.314(6) .
Ag8 O10 2.353(6) .
Ag8 C7 2.388(5) .
Ag8 O2 2.505(4) 2_666
Ag8 Ag10 2.9963(7) .
Ag8 Ag12 3.1050(7) .
Ag8 Ag9 3.1849(7) .
Ag9 C25 2.294(6) .
Ag9 O7 2.318(6) .
Ag9 O3 2.444(5) 2_666
Ag9 C13 2.501(6) .
Ag9 C26 2.651(7) .
Ag9 Ag12 3.1839(7) .
Ag10 C7 2.222(6) .
Ag10 C19 2.235(6) 2_666
Ag10 O9 2.557(5) .
Ag10 Ag3A 2.864(3) 2_666
Ag10 Ag3B 3.040(9) 2_666
Ag10 Ag4 3.0608(7) 2_666
Ag11 C37 2.091(6) .
Ag11 C31 2.207(6) .
Ag11 C32 2.533(7) .
Ag11 Ag1A 3.099(9) 2_666
Ag11 Ag12 3.2371(7) .
Ag11 Ag7 3.2464(7) 2_666
Ag11 Ag1B 3.302(3) 2_666
Ag12 C25 2.098(6) .
Ag12 C37 2.225(6) .
Ag12 C38 2.487(6) .
V O1 1.660(5) .
V O2 1.678(4) .
V O3 1.680(5) .
V O4 1.783(11) .
V O4 1.802(12) 2_666
O2 Ag8 2.505(4) 2_666
O3 Ag9 2.444(5) 2_666
O3 Ag4 2.460(4) 2_666
O4 O4 0.94(2) 2_666
O4 V 1.802(12) 2_666
O5 C43 1.193(10) .
O6 C43 1.231(10) .
O7 C45 1.213(10) .
O8 C45 1.240(10) .
O9 C47 1.234(8) .
O9 Ag3A 2.406(6) 2_666
O9 Ag3B 2.437(12) 2_666
O10 C47 1.226(9) .
O11 C49 1.441(17) .
C1 C2 1.192(9) .
C2 C3 1.486(9) .
C3 C6 1.472(13) .
C3 C4 1.516(12) .
C3 C5 1.532(13) .
C7 C8 1.207(8) .
C8 C9 1.470(9) .
C9 C12 1.421(15) .
C9 C11 1.504(15) .
C9 C10 1.605(15) .
C13 C14 1.218(9) .
C14 C15 1.487(9) .
C15 C17 1.509(11) .
C15 C18 1.518(10) .
C15 C16 1.529(11) .
C19 C20 1.208(9) .
C19 Ag10 2.235(6) 2_666
C20 C21 1.467(10) .
C21 C22 1.40(3) .
C21 C24 1.43(2) .
C21 C23 1.462(19) .
C25 C26 1.203(9) .
C26 C27 1.489(9) .
C27 C28 1.457(15) .
C27 C30 1.465(15) .
C27 C29 1.57(2) .
C31 C32 1.209(8) .
C31 Ag7 2.148(6) 2_666
C32 C33 1.493(9) .
C33 C36 1.509(14) .
C33 C34 1.524(15) .
C33 C35 1.538(14) .
C37 C38 1.226(9) .
C37 Ag1A 2.248(11) 2_666
C37 Ag1B 2.265(7) 2_666
C38 C39 1.477(9) .
C38 Ag1B 2.466(7) 2_666
C38 Ag1A 2.587(10) 2_666
C39 C42 1.520(12) .
C39 C40 1.528(11) .
C39 C41 1.544(12) .
C43 C44 1.562(13) .
C44 F2 1.126(13) .
C44 F1 1.296(13) .
C44 F3 1.357(14) .
C45 C46 1.536(9) .
C46 F6 1.300(10) .
C46 F5 1.312(10) .
C46 F4 1.321(9) .
C47 C48 1.534(11) .
C48 F9 1.287(10) .
C48 F8 1.298(11) .
C48 F7 1.343(11) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C1 Ag3A Ag5 Ag2 21.93(18) . .
O9 Ag3A Ag5 Ag2 -167.5(2) 2_666 .
C19 Ag3A Ag5 Ag2 168.1(2) . .
O2 Ag3A Ag5 Ag2 -86.77(13) . .
Ag10 Ag3A Ag5 Ag2 -143.61(7) 2_666 .
Ag1B Ag3A Ag5 Ag2 -22.21(9) . .
Ag1A Ag3A Ag5 Ag2 -21.94(18) . .
C31 Ag4 Ag5 C19 -116.7(5) . .
O8 Ag4 Ag5 C19 104.8(3) . .
O3 Ag4 Ag5 C19 -155.5(2) 2_666 .
Ag7 Ag4 Ag5 C19 -84.5(2) 2_666 .
Ag10 Ag4 Ag5 C19 -48.2(2) 2_666 .
Ag11 Ag4 Ag5 C19 -158.6(2) . .
C31 Ag4 Ag5 C13 88.8(5) . .
O8 Ag4 Ag5 C13 -49.7(3) . .
C19 Ag4 Ag5 C13 -154.4(3) . .
O3 Ag4 Ag5 C13 50.1(3) 2_666 .
Ag7 Ag4 Ag5 C13 121.0(3) 2_666 .
Ag10 Ag4 Ag5 C13 157.3(3) 2_666 .
Ag11 Ag4 Ag5 C13 47.0(3) . .
C31 Ag4 Ag5 C14 132.3(5) . .
O8 Ag4 Ag5 C14 -6.2(3) . .
C19 Ag4 Ag5 C14 -111.0(3) . .
O3 Ag4 Ag5 C14 93.5(3) 2_666 .
Ag7 Ag4 Ag5 C14 164.5(2) 2_666 .
Ag10 Ag4 Ag5 C14 -159.2(2) 2_666 .
Ag11 Ag4 Ag5 C14 90.4(2) . .
C31 Ag4 Ag5 Ag3A -92.9(4) . .
O8 Ag4 Ag5 Ag3A 128.62(19) . .
C19 Ag4 Ag5 Ag3A 23.8(2) . .
O3 Ag4 Ag5 Ag3A -131.66(15) 2_666 .
Ag7 Ag4 Ag5 Ag3A -60.68(7) 2_666 .
Ag10 Ag4 Ag5 Ag3A -24.39(6) 2_666 .
Ag11 Ag4 Ag5 Ag3A -134.73(6) . .
C31 Ag4 Ag5 Ag9 79.6(4) . .
O8 Ag4 Ag5 Ag9 -58.85(18) . .
C19 Ag4 Ag5 Ag9 -163.63(19) . .
O3 Ag4 Ag5 Ag9 40.87(14) 2_666 .
Ag7 Ag4 Ag5 Ag9 111.85(2) 2_666 .
Ag10 Ag4 Ag5 Ag9 148.14(2) 2_666 .
Ag11 Ag4 Ag5 Ag9 37.79(3) . .
C31 Ag4 Ag5 Ag3B -93.2(5) . .
O8 Ag4 Ag5 Ag3B 128.3(3) . .
C19 Ag4 Ag5 Ag3B 23.6(3) . .
O3 Ag4 Ag5 Ag3B -131.9(2) 2_666 .
Ag7 Ag4 Ag5 Ag3B -61.0(2) 2_666 .
Ag10 Ag4 Ag5 Ag3B -24.7(2) 2_666 .
Ag11 Ag4 Ag5 Ag3B -135.0(2) . .
C31 Ag4 Ag5 Ag2 -58.1(4) . .
O8 Ag4 Ag5 Ag2 163.5(2) . .
C19 Ag4 Ag5 Ag2 58.7(2) . .
O3 Ag4 Ag5 Ag2 -96.83(16) 2_666 .
Ag7 Ag4 Ag5 Ag2 -25.85(9) 2_666 .
Ag10 Ag4 Ag5 Ag2 10.44(8) 2_666 .
Ag11 Ag4 Ag5 Ag2 -99.91(8) . .
C1 Ag3B Ag5 C19 -146.6(5) . .
O9 Ag3B Ag5 C19 23.9(4) 2_666 .
O2 Ag3B Ag5 C19 101.3(3) . .
Ag2 Ag3B Ag5 C19 -169.4(3) . .
Ag1B Ag3B Ag5 C19 166.2(5) . .
Ag10 Ag3B Ag5 C19 46.8(2) 2_666 .
Ag1A Ag3B Ag5 C19 166.8(5) . .
C1 Ag3B Ag5 C13 10.2(5) . .
O9 Ag3B Ag5 C13 -179.3(4) 2_666 .
O2 Ag3B Ag5 C13 -102.0(3) . .
C19 Ag3B Ag5 C13 156.7(3) . .
Ag2 Ag3B Ag5 C13 -12.7(2) . .
Ag1B Ag3B Ag5 C13 -37.1(4) . .
Ag10 Ag3B Ag5 C13 -156.47(18) 2_666 .
Ag1A Ag3B Ag5 C13 -36.4(4) . .
C1 Ag3B Ag5 C14 -15.4(4) . .
O9 Ag3B Ag5 C14 155.1(4) 2_666 .
O2 Ag3B Ag5 C14 -127.5(2) . .
C19 Ag3B Ag5 C14 131.2(2) . .
Ag2 Ag3B Ag5 C14 -38.21(19) . .
Ag1B Ag3B Ag5 C14 -62.6(4) . .
Ag10 Ag3B Ag5 C14 177.96(16) 2_666 .
Ag1A Ag3B Ag5 C14 -62.0(4) . .
C1 Ag3B Ag5 Ag3A -174(5) . .
O9 Ag3B Ag5 Ag3A -4(5) 2_666 .
O2 Ag3B Ag5 Ag3A 74(5) . .
C19 Ag3B Ag5 Ag3A -28(5) . .
Ag2 Ag3B Ag5 Ag3A 163(5) . .
Ag1B Ag3B Ag5 Ag3A 139(5) . .
Ag10 Ag3B Ag5 Ag3A 19(5) 2_666 .
Ag1A Ag3B Ag5 Ag3A 139(5) . .
C1 Ag3B Ag5 Ag9 40.5(10) . .
O9 Ag3B Ag5 Ag9 -149.0(5) 2_666 .
O2 Ag3B Ag5 Ag9 -71.6(8) . .
C19 Ag3B Ag5 Ag9 -172.9(6) . .
Ag2 Ag3B Ag5 Ag9 17.7(8) . .
Ag1B Ag3B Ag5 Ag9 -6.7(10) . .
Ag10 Ag3B Ag5 Ag9 -126.1(7) 2_666 .
Ag1A Ag3B Ag5 Ag9 -6.1(10) . .
C1 Ag3B Ag5 Ag4 -168.5(3) . .
O9 Ag3B Ag5 Ag4 2.0(4) 2_666 .
O2 Ag3B Ag5 Ag4 79.3(2) . .
C19 Ag3B Ag5 Ag4 -21.9(3) . .
Ag2 Ag3B Ag5 Ag4 168.66(7) . .
Ag1B Ag3B Ag5 Ag4 144.2(3) . .
Ag10 Ag3B Ag5 Ag4 24.84(17) 2_666 .
Ag1A Ag3B Ag5 Ag4 144.9(3) . .
C1 Ag3B Ag5 Ag2 22.8(3) . .
O9 Ag3B Ag5 Ag2 -166.7(5) 2_666 .
O2 Ag3B Ag5 Ag2 -89.3(2) . .
C19 Ag3B Ag5 Ag2 169.4(3) . .
Ag1B Ag3B Ag5 Ag2 -24.4(2) . .
Ag10 Ag3B Ag5 Ag2 -143.8(2) 2_666 .
Ag1A Ag3B Ag5 Ag2 -23.8(2) . .
C1 Ag2 Ag5 C19 -10.2(2) . .
O6 Ag2 Ag5 C19 -170.8(6) . .
C13 Ag2 Ag5 C19 -155.0(3) . .
O1 Ag2 Ag5 C19 98.6(2) . .
C14 Ag2 Ag5 C19 -122.3(2) . .
Ag1A Ag2 Ag5 C19 40.0(3) . .
Ag1B Ag2 Ag5 C19 35.51(19) . .
Ag3B Ag2 Ag5 C19 10.1(3) . .
Ag3A Ag2 Ag5 C19 11.06(19) . .
Ag6 Ag2 Ag5 C19 160.69(18) . .
C1 Ag2 Ag5 C13 144.8(3) . .
O6 Ag2 Ag5 C13 -15.8(6) . .
O1 Ag2 Ag5 C13 -106.4(2) . .
C14 Ag2 Ag5 C13 32.7(2) . .
Ag1A Ag2 Ag5 C13 -165.0(3) . .
Ag1B Ag2 Ag5 C13 -169.5(2) . .
Ag3B Ag2 Ag5 C13 165.2(3) . .
Ag3A Ag2 Ag5 C13 166.1(2) . .
Ag6 Ag2 Ag5 C13 -44.28(19) . .
C1 Ag2 Ag5 C14 112.1(2) . .
O6 Ag2 Ag5 C14 -48.5(6) . .
C13 Ag2 Ag5 C14 -32.7(2) . .
O1 Ag2 Ag5 C14 -139.1(2) . .
Ag1A Ag2 Ag5 C14 162.3(3) . .
Ag1B Ag2 Ag5 C14 157.83(18) . .
Ag3B Ag2 Ag5 C14 132.5(3) . .
Ag3A Ag2 Ag5 C14 133.38(17) . .
Ag6 Ag2 Ag5 C14 -76.99(16) . .
C1 Ag2 Ag5 Ag3A -21.30(18) . .
O6 Ag2 Ag5 Ag3A 178.1(6) . .
C13 Ag2 Ag5 Ag3A -166.1(2) . .
O1 Ag2 Ag5 Ag3A 87.54(14) . .
C14 Ag2 Ag5 Ag3A -133.38(17) . .
Ag1A Ag2 Ag5 Ag3A 28.9(2) . .
Ag1B Ag2 Ag5 Ag3A 24.45(10) . .
Ag3B Ag2 Ag5 Ag3A -0.9(3) . .
Ag6 Ag2 Ag5 Ag3A 149.63(7) . .
C1 Ag2 Ag5 Ag9 164.29(16) . .
O6 Ag2 Ag5 Ag9 3.7(6) . .
C13 Ag2 Ag5 Ag9 19.50(19) . .
O1 Ag2 Ag5 Ag9 -86.87(13) . .
C14 Ag2 Ag5 Ag9 52.21(16) . .
Ag1A Ag2 Ag5 Ag9 -145.5(2) . .
Ag1B Ag2 Ag5 Ag9 -149.96(7) . .
Ag3B Ag2 Ag5 Ag9 -175.3(2) . .
Ag3A Ag2 Ag5 Ag9 -174.41(7) . .
Ag6 Ag2 Ag5 Ag9 -24.782(19) . .
C1 Ag2 Ag5 Ag4 -60.11(18) . .
O6 Ag2 Ag5 Ag4 139.3(6) . .
C13 Ag2 Ag5 Ag4 155.1(2) . .
O1 Ag2 Ag5 Ag4 48.73(15) . .
C14 Ag2 Ag5 Ag4 -172.19(18) . .
Ag1A Ag2 Ag5 Ag4 -9.9(2) . .
Ag1B Ag2 Ag5 Ag4 -14.36(11) . .
Ag3B Ag2 Ag5 Ag4 -39.7(2) . .
Ag3A Ag2 Ag5 Ag4 -38.81(10) . .
Ag6 Ag2 Ag5 Ag4 110.82(8) . .
C1 Ag2 Ag5 Ag3B -20.4(3) . .
O6 Ag2 Ag5 Ag3B 179.0(6) . .
C13 Ag2 Ag5 Ag3B -165.2(3) . .
O1 Ag2 Ag5 Ag3B 88.5(3) . .
C14 Ag2 Ag5 Ag3B -132.5(3) . .
Ag1A Ag2 Ag5 Ag3B 29.8(3) . .
Ag1B Ag2 Ag5 Ag3B 25.4(2) . .
Ag3A Ag2 Ag5 Ag3B 0.9(3) . .
Ag6 Ag2 Ag5 Ag3B 150.5(2) . .
C1 Ag2 Ag6 C13 84.6(6) . .
O6 Ag2 Ag6 C13 -122.3(3) . .
O1 Ag2 Ag6 C13 147.8(3) . .
C14 Ag2 Ag6 C13 -11.8(3) . .
Ag1A Ag2 Ag6 C13 161.6(3) . .
Ag1B Ag2 Ag6 C13 156.1(2) . .
Ag3B Ag2 Ag6 C13 79.4(3) . .
Ag5 Ag2 Ag6 C13 49.6(2) . .
Ag3A Ag2 Ag6 C13 77.8(2) . .
C1 Ag2 Ag6 C7 -108.4(6) . .
O6 Ag2 Ag6 C7 44.7(3) . .
C13 Ag2 Ag6 C7 167.0(3) . .
O1 Ag2 Ag6 C7 -45.2(3) . .
C14 Ag2 Ag6 C7 155.2(3) . .
Ag1A Ag2 Ag6 C7 -31.3(3) . .
Ag1B Ag2 Ag6 C7 -36.9(2) . .
Ag3B Ag2 Ag6 C7 -113.6(3) . .
Ag5 Ag2 Ag6 C7 -143.4(2) . .
Ag3A Ag2 Ag6 C7 -115.2(2) . .
C1 Ag2 Ag6 Ag9 59.4(6) . .
O6 Ag2 Ag6 Ag9 -147.54(17) . .
C13 Ag2 Ag6 Ag9 -25.2(2) . .
O1 Ag2 Ag6 Ag9 122.58(13) . .
C14 Ag2 Ag6 Ag9 -37.06(14) . .
Ag1A Ag2 Ag6 Ag9 136.42(19) . .
Ag1B Ag2 Ag6 Ag9 130.87(6) . .
Ag3B Ag2 Ag6 Ag9 54.2(2) . .
Ag5 Ag2 Ag6 Ag9 24.367(19) . .
Ag3A Ag2 Ag6 Ag9 52.56(6) . .
C1 Ag2 Ag6 Ag8 10.2(6) . .
O6 Ag2 Ag6 Ag8 163.26(18) . .
C13 Ag2 Ag6 Ag8 -74.4(2) . .
O1 Ag2 Ag6 Ag8 73.37(15) . .
C14 Ag2 Ag6 Ag8 -86.27(16) . .
Ag1A Ag2 Ag6 Ag8 87.2(2) . .
Ag1B Ag2 Ag6 Ag8 81.66(9) . .
Ag3B Ag2 Ag6 Ag8 5.0(2) . .
Ag5 Ag2 Ag6 Ag8 -24.84(7) . .
Ag3A Ag2 Ag6 Ag8 3.35(9) . .
C1 Ag2 Ag6 Ag7 -100.0(6) . .
O6 Ag2 Ag6 Ag7 53.14(17) . .
C13 Ag2 Ag6 Ag7 175.5(2) . .
O1 Ag2 Ag6 Ag7 -36.75(13) . .
C14 Ag2 Ag6 Ag7 163.62(14) . .
Ag1A Ag2 Ag6 Ag7 -22.91(19) . .
Ag1B Ag2 Ag6 Ag7 -28.45(6) . .
Ag3B Ag2 Ag6 Ag7 -105.2(2) . .
Ag5 Ag2 Ag6 Ag7 -134.96(2) . .
Ag3A Ag2 Ag6 Ag7 -106.76(6) . .
C13 Ag6 Ag7 C31 39.2(7) . 2_666
C7 Ag6 Ag7 C31 -153.2(7) . 2_666
Ag9 Ag6 Ag7 C31 -77.7(7) . 2_666
Ag8 Ag6 Ag7 C31 -129.4(7) . 2_666
Ag2 Ag6 Ag7 C31 34.2(7) . 2_666
C13 Ag6 Ag7 O5 -54.0(3) . .
C7 Ag6 Ag7 O5 113.6(3) . .
Ag9 Ag6 Ag7 O5 -170.9(2) . .
Ag8 Ag6 Ag7 O5 137.4(2) . .
Ag2 Ag6 Ag7 O5 -59.0(2) . .
C13 Ag6 Ag7 C7 -167.6(3) . .
Ag9 Ag6 Ag7 C7 75.49(19) . .
Ag8 Ag6 Ag7 C7 23.80(19) . .
Ag2 Ag6 Ag7 C7 -172.63(19) . .
C13 Ag6 Ag7 O1 40.3(3) . .
C7 Ag6 Ag7 O1 -152.1(2) . .
Ag9 Ag6 Ag7 O1 -76.64(14) . .
Ag8 Ag6 Ag7 O1 -128.32(13) . .
Ag2 Ag6 Ag7 O1 35.24(13) . .
C13 Ag6 Ag7 Ag4 106.8(2) . 2_666
C7 Ag6 Ag7 Ag4 -85.64(19) . 2_666
Ag9 Ag6 Ag7 Ag4 -10.16(7) . 2_666
Ag8 Ag6 Ag7 Ag4 -61.84(3) . 2_666
Ag2 Ag6 Ag7 Ag4 101.72(3) . 2_666
C13 Ag6 Ag7 Ag10 146.5(2) . .
C7 Ag6 Ag7 Ag10 -45.87(19) . .
Ag9 Ag6 Ag7 Ag10 29.62(6) . .
Ag8 Ag6 Ag7 Ag10 -22.068(19) . .
Ag2 Ag6 Ag7 Ag10 141.499(19) . .
C13 Ag6 Ag7 Ag11 28.1(2) . 2_666
C7 Ag6 Ag7 Ag11 -164.30(19) . 2_666
Ag9 Ag6 Ag7 Ag11 -88.81(6) . 2_666
Ag8 Ag6 Ag7 Ag11 -140.50(2) . 2_666
Ag2 Ag6 Ag7 Ag11 23.07(2) . 2_666
C13 Ag6 Ag8 C25 8.5(3) . .
C7 Ag6 Ag8 C25 -157.6(2) . .
Ag9 Ag6 Ag8 C25 17.56(15) . .
Ag7 Ag6 Ag8 C25 179.02(15) . .
Ag2 Ag6 Ag8 C25 71.30(17) . .
C13 Ag6 Ag8 O10 157.1(4) . .
C7 Ag6 Ag8 O10 -9.1(3) . .
Ag9 Ag6 Ag8 O10 166.1(3) . .
Ag7 Ag6 Ag8 O10 -32.4(3) . .
Ag2 Ag6 Ag8 O10 -140.2(3) . .
C13 Ag6 Ag8 C7 166.2(3) . .
Ag9 Ag6 Ag8 C7 175.21(18) . .
Ag7 Ag6 Ag8 C7 -23.33(18) . .
Ag2 Ag6 Ag8 C7 -131.1(2) . .
C13 Ag6 Ag8 O2 -94.2(2) . 2_666
C7 Ag6 Ag8 O2 99.6(2) . 2_666
Ag9 Ag6 Ag8 O2 -85.15(11) . 2_666
Ag7 Ag6 Ag8 O2 76.31(11) . 2_666
Ag2 Ag6 Ag8 O2 -31.41(13) . 2_666
C13 Ag6 Ag8 Ag10 -149.2(2) . .
C7 Ag6 Ag8 Ag10 44.64(18) . .
Ag9 Ag6 Ag8 Ag10 -140.15(2) . .
Ag7 Ag6 Ag8 Ag10 21.305(19) . .
Ag2 Ag6 Ag8 Ag10 -86.42(7) . .
C13 Ag6 Ag8 Ag12 -33.8(2) . .
C7 Ag6 Ag8 Ag12 160.07(18) . .
Ag9 Ag6 Ag8 Ag12 -24.721(19) . .
Ag7 Ag6 Ag8 Ag12 136.738(19) . .
Ag2 Ag6 Ag8 Ag12 29.01(8) . .
C13 Ag6 Ag8 Ag9 -9.1(2) . .
C7 Ag6 Ag8 Ag9 -175.21(18) . .
Ag7 Ag6 Ag8 Ag9 161.46(2) . .
Ag2 Ag6 Ag8 Ag9 53.73(7) . .
C19 Ag5 Ag9 C25 -88.6(5) . .
C13 Ag5 Ag9 C25 117.1(5) . .
C14 Ag5 Ag9 C25 141.9(4) . .
Ag3A Ag5 Ag9 C25 75.5(5) . .
Ag4 Ag5 Ag9 C25 -69.6(4) . .
Ag3B Ag5 Ag9 C25 82.6(9) . .
Ag2 Ag5 Ag9 C25 98.5(4) . .
C19 Ag5 Ag9 O7 49.8(3) . .
C13 Ag5 Ag9 O7 -104.4(2) . .
C14 Ag5 Ag9 O7 -79.6(2) . .
Ag3A Ag5 Ag9 O7 -146.0(4) . .
Ag4 Ag5 Ag9 O7 68.82(17) . .
Ag3B Ag5 Ag9 O7 -138.9(8) . .
Ag2 Ag5 Ag9 O7 -123.09(17) . .
C19 Ag5 Ag9 O3 -59.5(3) . 2_666
C13 Ag5 Ag9 O3 146.2(2) . 2_666
C14 Ag5 Ag9 O3 171.0(2) . 2_666
Ag3A Ag5 Ag9 O3 104.6(4) . 2_666
Ag4 Ag5 Ag9 O3 -40.53(14) . 2_666
Ag3B Ag5 Ag9 O3 111.8(8) . 2_666
Ag2 Ag5 Ag9 O3 127.56(14) . 2_666
C19 Ag5 Ag9 C13 154.3(3) . .
C14 Ag5 Ag9 C13 24.8(2) . .
Ag3A Ag5 Ag9 C13 -41.6(4) . .
Ag4 Ag5 Ag9 C13 173.22(19) . .
Ag3B Ag5 Ag9 C13 -34.5(8) . .
Ag2 Ag5 Ag9 C13 -18.69(18) . .
C19 Ag5 Ag9 C26 176.8(7) . .
C13 Ag5 Ag9 C26 22.6(7) . .
C14 Ag5 Ag9 C26 47.4(6) . .
Ag3A Ag5 Ag9 C26 -19.0(7) . .
Ag4 Ag5 Ag9 C26 -164.2(6) . .
Ag3B Ag5 Ag9 C26 -11.9(10) . .
Ag2 Ag5 Ag9 C26 3.9(6) . .
C19 Ag5 Ag9 Ag6 -161.1(2) . .
C13 Ag5 Ag9 Ag6 44.68(18) . .
C14 Ag5 Ag9 Ag6 69.47(13) . .
Ag3A Ag5 Ag9 Ag6 3.1(3) . .
Ag4 Ag5 Ag9 Ag6 -142.09(2) . .
Ag3B Ag5 Ag9 Ag6 10.2(8) . .
Ag2 Ag5 Ag9 Ag6 26.00(2) . .
C19 Ag5 Ag9 Ag12 -57.2(2) . .
C13 Ag5 Ag9 Ag12 148.59(18) . .
C14 Ag5 Ag9 Ag12 173.38(14) . .
Ag3A Ag5 Ag9 Ag12 107.0(3) . .
Ag4 Ag5 Ag9 Ag12 -38.19(3) . .
Ag3B Ag5 Ag9 Ag12 114.1(8) . .
Ag2 Ag5 Ag9 Ag12 129.90(2) . .
C19 Ag5 Ag9 Ag8 -125.0(2) . .
C13 Ag5 Ag9 Ag8 80.78(18) . .
C14 Ag5 Ag9 Ag8 105.57(14) . .
Ag3A Ag5 Ag9 Ag8 39.2(3) . .
Ag4 Ag5 Ag9 Ag8 -106.00(2) . .
Ag3B Ag5 Ag9 Ag8 46.3(8) . .
Ag2 Ag5 Ag9 Ag8 62.10(3) . .
C13 Ag6 Ag9 C25 153.2(2) . .
C7 Ag6 Ag9 C25 -13.3(2) . .
Ag8 Ag6 Ag9 C25 -17.76(16) . .
Ag7 Ag6 Ag9 C25 -75.10(17) . .
Ag2 Ag6 Ag9 C25 176.41(16) . .
C13 Ag6 Ag9 O7 -3.6(4) . .
C7 Ag6 Ag9 O7 -170.0(4) . .
Ag8 Ag6 Ag9 O7 -174.5(3) . .
Ag7 Ag6 Ag9 O7 128.2(3) . .
Ag2 Ag6 Ag9 O7 19.7(3) . .
C13 Ag6 Ag9 O3 -106.4(2) . 2_666
C7 Ag6 Ag9 O3 87.2(2) . 2_666
Ag8 Ag6 Ag9 O3 82.74(13) . 2_666
Ag7 Ag6 Ag9 O3 25.40(14) . 2_666
Ag2 Ag6 Ag9 O3 -83.10(13) . 2_666
C7 Ag6 Ag9 C13 -166.5(3) . .
Ag8 Ag6 Ag9 C13 -170.9(2) . .
Ag7 Ag6 Ag9 C13 131.8(2) . .
Ag2 Ag6 Ag9 C13 23.3(2) . .
C13 Ag6 Ag9 C26 126.7(2) . .
C7 Ag6 Ag9 C26 -39.8(2) . .
Ag8 Ag6 Ag9 C26 -44.20(16) . .
Ag7 Ag6 Ag9 C26 -101.54(16) . .
Ag2 Ag6 Ag9 C26 149.96(16) . .
C13 Ag6 Ag9 Ag5 -47.76(19) . .
C7 Ag6 Ag9 Ag5 145.77(17) . .
Ag8 Ag6 Ag9 Ag5 141.33(2) . .
Ag7 Ag6 Ag9 Ag5 83.99(6) . .
Ag2 Ag6 Ag9 Ag5 -24.506(19) . .
C13 Ag6 Ag9 Ag12 -165.38(19) . .
C7 Ag6 Ag9 Ag12 28.15(17) . .
Ag8 Ag6 Ag9 Ag12 23.710(19) . .
Ag7 Ag6 Ag9 Ag12 -33.63(6) . .
Ag2 Ag6 Ag9 Ag12 -142.125(19) . .
C13 Ag6 Ag9 Ag8 170.91(19) . .
C7 Ag6 Ag9 Ag8 4.44(17) . .
Ag7 Ag6 Ag9 Ag8 -57.34(5) . .
Ag2 Ag6 Ag9 Ag8 -165.83(2) . .
O10 Ag8 Ag9 C25 -9.4(4) . .
C7 Ag8 Ag9 C25 152.1(2) . .
O2 Ag8 Ag9 C25 -112.1(2) 2_666 .
Ag6 Ag8 Ag9 C25 155.6(2) . .
Ag10 Ag8 Ag9 C25 -160.2(2) . .
Ag12 Ag8 Ag9 C25 -50.6(2) . .
C25 Ag8 Ag9 O7 6.1(9) . .
O10 Ag8 Ag9 O7 -3.2(9) . .
C7 Ag8 Ag9 O7 158.2(9) . .
O2 Ag8 Ag9 O7 -106.0(9) 2_666 .
Ag6 Ag8 Ag9 O7 161.7(9) . .
Ag10 Ag8 Ag9 O7 -154.0(9) . .
Ag12 Ag8 Ag9 O7 -44.5(9) . .
C25 Ag8 Ag9 O3 109.7(3) . 2_666
O10 Ag8 Ag9 O3 100.4(4) . 2_666
C7 Ag8 Ag9 O3 -98.2(2) . 2_666
O2 Ag8 Ag9 O3 -2.4(2) 2_666 2_666
Ag6 Ag8 Ag9 O3 -94.68(17) . 2_666
Ag10 Ag8 Ag9 O3 -50.42(17) . 2_666
Ag12 Ag8 Ag9 O3 59.12(16) . 2_666
C25 Ag8 Ag9 C13 -149.1(3) . .
O10 Ag8 Ag9 C13 -158.4(3) . .
C7 Ag8 Ag9 C13 3.01(19) . .
O2 Ag8 Ag9 C13 98.81(19) 2_666 .
Ag6 Ag8 Ag9 C13 6.53(14) . .
Ag10 Ag8 Ag9 C13 50.79(14) . .
Ag12 Ag8 Ag9 C13 160.34(14) . .
C25 Ag8 Ag9 C26 -32.7(3) . .
O10 Ag8 Ag9 C26 -42.1(4) . .
C7 Ag8 Ag9 C26 119.4(2) . .
O2 Ag8 Ag9 C26 -144.8(2) 2_666 .
Ag6 Ag8 Ag9 C26 122.88(16) . .
Ag10 Ag8 Ag9 C26 167.14(16) . .
Ag12 Ag8 Ag9 C26 -83.32(16) . .
C25 Ag8 Ag9 Ag5 162.5(2) . .
O10 Ag8 Ag9 Ag5 153.2(3) . .
C7 Ag8 Ag9 Ag5 -45.43(13) . .
O2 Ag8 Ag9 Ag5 50.36(13) 2_666 .
Ag6 Ag8 Ag9 Ag5 -41.91(2) . .
Ag10 Ag8 Ag9 Ag5 2.35(3) . .
Ag12 Ag8 Ag9 Ag5 111.89(2) . .
C25 Ag8 Ag9 Ag6 -155.6(2) . .
O10 Ag8 Ag9 Ag6 -164.9(3) . .
C7 Ag8 Ag9 Ag6 -3.52(13) . .
O2 Ag8 Ag9 Ag6 92.27(13) 2_666 .
Ag10 Ag8 Ag9 Ag6 44.26(2) . .
Ag12 Ag8 Ag9 Ag6 153.80(2) . .
C25 Ag8 Ag9 Ag12 50.6(2) . .
O10 Ag8 Ag9 Ag12 41.3(3) . .
C7 Ag8 Ag9 Ag12 -157.32(13) . .
O2 Ag8 Ag9 Ag12 -61.53(12) 2_666 .
Ag6 Ag8 Ag9 Ag12 -153.80(2) . .
Ag10 Ag8 Ag9 Ag12 -109.54(2) . .
C31 Ag7 Ag10 C7 -152.8(2) 2_666 .
O5 Ag7 Ag10 C7 17.9(3) . .
O1 Ag7 Ag10 C7 102.6(2) . .
Ag4 Ag7 Ag10 C7 -173.48(17) 2_666 .
Ag6 Ag7 Ag10 C7 42.03(17) . .
Ag11 Ag7 Ag10 C7 161.56(17) 2_666 .
C31 Ag7 Ag10 C19 14.2(2) 2_666 2_666
O5 Ag7 Ag10 C19 -175.0(3) . 2_666
C7 Ag7 Ag10 C19 167.1(2) . 2_666
O1 Ag7 Ag10 C19 -90.3(2) . 2_666
Ag4 Ag7 Ag10 C19 -6.41(16) 2_666 2_666
Ag6 Ag7 Ag10 C19 -150.90(17) . 2_666
Ag11 Ag7 Ag10 C19 -31.37(17) 2_666 2_666
C31 Ag7 Ag10 O9 -96.7(3) 2_666 .
O5 Ag7 Ag10 O9 74.1(4) . .
C7 Ag7 Ag10 O9 56.2(3) . .
O1 Ag7 Ag10 O9 158.8(3) . .
Ag4 Ag7 Ag10 O9 -117.3(3) 2_666 .
Ag6 Ag7 Ag10 O9 98.2(3) . .
Ag11 Ag7 Ag10 O9 -142.3(3) 2_666 .
C31 Ag7 Ag10 Ag3A 58.4(2) 2_666 2_666
O5 Ag7 Ag10 Ag3A -130.8(3) . 2_666
C7 Ag7 Ag10 Ag3A -148.8(2) . 2_666
O1 Ag7 Ag10 Ag3A -46.19(18) . 2_666
Ag4 Ag7 Ag10 Ag3A 37.74(13) 2_666 2_666
Ag6 Ag7 Ag10 Ag3A -106.76(13) . 2_666
Ag11 Ag7 Ag10 Ag3A 12.77(14) 2_666 2_666
C31 Ag7 Ag10 Ag8 -173.26(18) 2_666 .
O5 Ag7 Ag10 Ag8 -2.5(2) . .
C7 Ag7 Ag10 Ag8 -20.43(17) . .
O1 Ag7 Ag10 Ag8 82.17(12) . .
Ag4 Ag7 Ag10 Ag8 166.09(2) 2_666 .
Ag6 Ag7 Ag10 Ag8 21.598(19) . .
Ag11 Ag7 Ag10 Ag8 141.13(2) 2_666 .
C31 Ag7 Ag10 Ag3B 61.5(5) 2_666 2_666
O5 Ag7 Ag10 Ag3B -127.7(5) . 2_666
C7 Ag7 Ag10 Ag3B -145.6(5) . 2_666
O1 Ag7 Ag10 Ag3B -43.0(5) . 2_666
Ag4 Ag7 Ag10 Ag3B 40.9(4) 2_666 2_666
Ag6 Ag7 Ag10 Ag3B -103.6(4) . 2_666
Ag11 Ag7 Ag10 Ag3B 15.9(4) 2_666 2_666
C31 Ag7 Ag10 Ag4 20.64(18) 2_666 2_666
O5 Ag7 Ag10 Ag4 -168.6(2) . 2_666
C7 Ag7 Ag10 Ag4 173.48(17) . 2_666
O1 Ag7 Ag10 Ag4 -83.92(12) . 2_666
Ag6 Ag7 Ag10 Ag4 -144.49(2) . 2_666
Ag11 Ag7 Ag10 Ag4 -24.96(2) 2_666 2_666
C25 Ag8 Ag10 C7 -120.4(4) . .
O10 Ag8 Ag10 C7 112.4(2) . .
O2 Ag8 Ag10 C7 -143.7(2) 2_666 .
Ag6 Ag8 Ag10 C7 -43.46(18) . .
Ag12 Ag8 Ag10 C7 -151.18(18) . .
Ag9 Ag8 Ag10 C7 -80.84(18) . .
C25 Ag8 Ag10 C19 67.2(5) . 2_666
O10 Ag8 Ag10 C19 -60.0(3) . 2_666
C7 Ag8 Ag10 C19 -172.4(3) . 2_666
O2 Ag8 Ag10 C19 43.9(3) 2_666 2_666
Ag6 Ag8 Ag10 C19 144.1(3) . 2_666
Ag12 Ag8 Ag10 C19 36.4(3) . 2_666
Ag9 Ag8 Ag10 C19 106.8(3) . 2_666
C25 Ag8 Ag10 O9 110.5(4) . .
O10 Ag8 Ag10 O9 -16.7(2) . .
C7 Ag8 Ag10 O9 -129.1(2) . .
O2 Ag8 Ag10 O9 87.19(18) 2_666 .
Ag6 Ag8 Ag10 O9 -172.53(13) . .
Ag12 Ag8 Ag10 O9 79.76(13) . .
Ag9 Ag8 Ag10 O9 150.10(13) . .
C25 Ag8 Ag10 Ag3A 61.7(4) . 2_666
O10 Ag8 Ag10 Ag3A -65.49(16) . 2_666
C7 Ag8 Ag10 Ag3A -177.88(19) . 2_666
O2 Ag8 Ag10 Ag3A 38.38(15) 2_666 2_666
Ag6 Ag8 Ag10 Ag3A 138.66(7) . 2_666
Ag12 Ag8 Ag10 Ag3A 30.95(7) . 2_666
Ag9 Ag8 Ag10 Ag3A 101.29(7) . 2_666
C25 Ag8 Ag10 Ag7 -99.3(4) . .
O10 Ag8 Ag10 Ag7 133.46(15) . .
C7 Ag8 Ag10 Ag7 21.07(18) . .
O2 Ag8 Ag10 Ag7 -122.67(13) 2_666 .
Ag6 Ag8 Ag10 Ag7 -22.388(19) . .
Ag12 Ag8 Ag10 Ag7 -130.10(2) . .
Ag9 Ag8 Ag10 Ag7 -59.76(3) . .
C25 Ag8 Ag10 Ag3B 62.5(4) . 2_666
O10 Ag8 Ag10 Ag3B -64.7(2) . 2_666
C7 Ag8 Ag10 Ag3B -177.1(3) . 2_666
O2 Ag8 Ag10 Ag3B 39.1(2) 2_666 2_666
Ag6 Ag8 Ag10 Ag3B 139.42(19) . 2_666
Ag12 Ag8 Ag10 Ag3B 31.71(19) . 2_666
Ag9 Ag8 Ag10 Ag3B 102.05(19) . 2_666
C25 Ag8 Ag10 Ag4 -68.3(4) . 2_666
O10 Ag8 Ag10 Ag4 164.44(16) . 2_666
C7 Ag8 Ag10 Ag4 52.06(18) . 2_666
O2 Ag8 Ag10 Ag4 -91.68(14) 2_666 2_666
Ag6 Ag8 Ag10 Ag4 8.59(6) . 2_666
Ag12 Ag8 Ag10 Ag4 -99.12(6) . 2_666
Ag9 Ag8 Ag10 Ag4 -28.78(7) . 2_666
C31 Ag4 Ag11 C37 177.3(3) . .
O8 Ag4 Ag11 C37 69.7(3) . .
C19 Ag4 Ag11 C37 -70.6(5) . .
O3 Ag4 Ag11 C37 -26.2(3) 2_666 .
Ag7 Ag4 Ag11 C37 -128.1(2) 2_666 .
Ag5 Ag4 Ag11 C37 -23.3(2) . .
Ag10 Ag4 Ag11 C37 -105.5(2) 2_666 .
O8 Ag4 Ag11 C31 -107.6(3) . .
C19 Ag4 Ag11 C31 112.1(5) . .
O3 Ag4 Ag11 C31 156.5(3) 2_666 .
Ag7 Ag4 Ag11 C31 54.6(2) 2_666 .
Ag5 Ag4 Ag11 C31 159.4(2) . .
Ag10 Ag4 Ag11 C31 77.2(2) 2_666 .
C31 Ag4 Ag11 C32 26.3(3) . .
O8 Ag4 Ag11 C32 -81.3(2) . .
C19 Ag4 Ag11 C32 138.4(5) . .
O3 Ag4 Ag11 C32 -177.2(2) 2_666 .
Ag7 Ag4 Ag11 C32 80.92(17) 2_666 .
Ag5 Ag4 Ag11 C32 -174.25(17) . .
Ag10 Ag4 Ag11 C32 103.49(17) 2_666 .
C31 Ag4 Ag11 Ag1A -118.2(3) . 2_666
O8 Ag4 Ag11 Ag1A 134.2(3) . 2_666
C19 Ag4 Ag11 Ag1A -6.2(5) . 2_666
O3 Ag4 Ag11 Ag1A 38.2(2) 2_666 2_666
Ag7 Ag4 Ag11 Ag1A -63.63(18) 2_666 2_666
Ag5 Ag4 Ag11 Ag1A 41.20(19) . 2_666
Ag10 Ag4 Ag11 Ag1A -41.06(19) 2_666 2_666
C31 Ag4 Ag11 Ag12 175.2(2) . .
O8 Ag4 Ag11 Ag12 67.63(18) . .
C19 Ag4 Ag11 Ag12 -72.7(4) . .
O3 Ag4 Ag11 Ag12 -28.31(13) 2_666 .
Ag7 Ag4 Ag11 Ag12 -130.189(19) 2_666 .
Ag5 Ag4 Ag11 Ag12 -25.36(3) . .
Ag10 Ag4 Ag11 Ag12 -107.62(2) 2_666 .
C31 Ag4 Ag11 Ag7 -54.6(2) . 2_666
O8 Ag4 Ag11 Ag7 -162.19(18) . 2_666
C19 Ag4 Ag11 Ag7 57.5(4) . 2_666
O3 Ag4 Ag11 Ag7 101.87(13) 2_666 2_666
Ag5 Ag4 Ag11 Ag7 104.83(3) . 2_666
Ag10 Ag4 Ag11 Ag7 22.57(2) 2_666 2_666
C31 Ag4 Ag11 Ag1B -123.8(2) . 2_666
O8 Ag4 Ag11 Ag1B 128.64(19) . 2_666
C19 Ag4 Ag11 Ag1B -11.7(4) . 2_666
O3 Ag4 Ag11 Ag1B 32.70(14) 2_666 2_666
Ag7 Ag4 Ag11 Ag1B -69.17(6) 2_666 2_666
Ag5 Ag4 Ag11 Ag1B 35.66(7) . 2_666
Ag10 Ag4 Ag11 Ag1B -46.60(7) 2_666 2_666
O10 Ag8 Ag12 C25 -106.5(3) . .
C7 Ag8 Ag12 C25 111.8(4) . .
O2 Ag8 Ag12 C25 156.2(2) 2_666 .
Ag6 Ag8 Ag12 C25 79.1(2) . .
Ag10 Ag8 Ag12 C25 163.1(2) . .
Ag9 Ag8 Ag12 C25 55.4(2) . .
C25 Ag8 Ag12 C37 171.7(3) . .
O10 Ag8 Ag12 C37 65.3(3) . .
C7 Ag8 Ag12 C37 -76.5(4) . .
O2 Ag8 Ag12 C37 -32.1(3) 2_666 .
Ag6 Ag8 Ag12 C37 -109.2(2) . .
Ag10 Ag8 Ag12 C37 -25.2(2) . .
Ag9 Ag8 Ag12 C37 -132.8(2) . .
C25 Ag8 Ag12 C38 133.9(3) . .
O10 Ag8 Ag12 C38 27.5(2) . .
C7 Ag8 Ag12 C38 -114.3(4) . .
O2 Ag8 Ag12 C38 -69.9(2) 2_666 .
Ag6 Ag8 Ag12 C38 -147.02(18) . .
Ag10 Ag8 Ag12 C38 -62.99(18) . .
Ag9 Ag8 Ag12 C38 -170.66(18) . .
C25 Ag8 Ag12 Ag9 -55.4(2) . .
O10 Ag8 Ag12 Ag9 -161.88(15) . .
C7 Ag8 Ag12 Ag9 56.3(3) . .
O2 Ag8 Ag12 Ag9 100.74(12) 2_666 .
Ag6 Ag8 Ag12 Ag9 23.634(19) . .
Ag10 Ag8 Ag12 Ag9 107.67(2) . .
C25 Ag8 Ag12 Ag11 -131.0(2) . .
O10 Ag8 Ag12 Ag11 122.58(15) . .
C7 Ag8 Ag12 Ag11 -19.2(3) . .
O2 Ag8 Ag12 Ag11 25.19(12) 2_666 .
Ag6 Ag8 Ag12 Ag11 -51.91(3) . .
Ag10 Ag8 Ag12 Ag11 32.13(4) . .
Ag9 Ag8 Ag12 Ag11 -75.54(3) . .
O7 Ag9 Ag12 C25 112.0(3) . .
O3 Ag9 Ag12 C25 -160.7(3) 2_666 .
C13 Ag9 Ag12 C25 -104.9(4) . .
C26 Ag9 Ag12 C25 4.1(3) . .
Ag5 Ag9 Ag12 C25 -163.0(2) . .
Ag6 Ag9 Ag12 C25 -81.8(2) . .
Ag8 Ag9 Ag12 C25 -58.5(2) . .
C25 Ag9 Ag12 C37 -169.2(3) . .
O7 Ag9 Ag12 C37 -57.2(3) . .
O3 Ag9 Ag12 C37 30.1(3) 2_666 .
C13 Ag9 Ag12 C37 85.9(4) . .
C26 Ag9 Ag12 C37 -165.1(3) . .
Ag5 Ag9 Ag12 C37 27.8(2) . .
Ag6 Ag9 Ag12 C37 109.0(2) . .
Ag8 Ag9 Ag12 C37 132.3(2) . .
C25 Ag9 Ag12 C38 -162.4(7) . .
O7 Ag9 Ag12 C38 -50.4(7) . .
O3 Ag9 Ag12 C38 36.9(7) 2_666 .
C13 Ag9 Ag12 C38 92.7(8) . .
C26 Ag9 Ag12 C38 -158.3(7) . .
Ag5 Ag9 Ag12 C38 34.6(7) . .
Ag6 Ag9 Ag12 C38 115.8(7) . .
Ag8 Ag9 Ag12 C38 139.1(7) . .
C25 Ag9 Ag12 Ag8 58.5(2) . .
O7 Ag9 Ag12 Ag8 170.5(3) . .
O3 Ag9 Ag12 Ag8 -102.19(14) 2_666 .
C13 Ag9 Ag12 Ag8 -46.4(3) . .
C26 Ag9 Ag12 Ag8 62.57(16) . .
Ag5 Ag9 Ag12 Ag8 -104.53(3) . .
Ag6 Ag9 Ag12 Ag8 -23.351(18) . .
C25 Ag9 Ag12 Ag11 -168.4(2) . .
O7 Ag9 Ag12 Ag11 -56.4(3) . .
O3 Ag9 Ag12 Ag11 30.89(14) 2_666 .
C13 Ag9 Ag12 Ag11 86.7(3) . .
C26 Ag9 Ag12 Ag11 -164.34(16) . .
Ag5 Ag9 Ag12 Ag11 28.55(3) . .
Ag6 Ag9 Ag12 Ag11 109.73(2) . .
Ag8 Ag9 Ag12 Ag11 133.082(19) . .
C37 Ag11 Ag12 C25 166.6(4) . .
C31 Ag11 Ag12 C25 -10.5(4) . .
C32 Ag11 Ag12 C25 34.8(4) . .
Ag1A Ag11 Ag12 C25 -145.2(3) 2_666 .
Ag4 Ag11 Ag12 C25 -15.5(3) . .
Ag7 Ag11 Ag12 C25 -63.3(3) 2_666 .
Ag1B Ag11 Ag12 C25 -146.6(3) 2_666 .
C31 Ag11 Ag12 C37 -177.1(3) . .
C32 Ag11 Ag12 C37 -131.7(3) . .
Ag1A Ag11 Ag12 C37 48.2(3) 2_666 .
Ag4 Ag11 Ag12 C37 177.9(2) . .
Ag7 Ag11 Ag12 C37 130.1(2) 2_666 .
Ag1B Ag11 Ag12 C37 46.8(2) 2_666 .
C37 Ag11 Ag12 C38 2.1(3) . .
C31 Ag11 Ag12 C38 -175.0(3) . .
C32 Ag11 Ag12 C38 -129.7(3) . .
Ag1A Ag11 Ag12 C38 50.2(2) 2_666 .
Ag4 Ag11 Ag12 C38 179.97(15) . .
Ag7 Ag11 Ag12 C38 132.19(15) 2_666 .
Ag1B Ag11 Ag12 C38 48.90(16) 2_666 .
C37 Ag11 Ag12 Ag8 -120.2(2) . .
C31 Ag11 Ag12 Ag8 62.7(2) . .
C32 Ag11 Ag12 Ag8 108.0(2) . .
Ag1A Ag11 Ag12 Ag8 -72.04(18) 2_666 .
Ag4 Ag11 Ag12 Ag8 57.70(3) . .
Ag7 Ag11 Ag12 Ag8 9.91(4) 2_666 .
Ag1B Ag11 Ag12 Ag8 -73.37(6) 2_666 .
C37 Ag11 Ag12 Ag9 -179.2(2) . .
C31 Ag11 Ag12 Ag9 3.7(2) . .
C32 Ag11 Ag12 Ag9 49.0(2) . .
Ag1A Ag11 Ag12 Ag9 -131.03(18) 2_666 .
Ag4 Ag11 Ag12 Ag9 -1.291(19) . .
Ag7 Ag11 Ag12 Ag9 -49.08(3) 2_666 .
Ag1B Ag11 Ag12 Ag9 -132.37(6) 2_666 .
O2 V O1 Ag2 -39.1(5) . .
O3 V O1 Ag2 -160.8(3) . .
O4 V O1 Ag2 92.6(7) . .
O4 V O1 Ag2 70.5(7) 2_666 .
O2 V O1 Ag7 166.5(3) . .
O3 V O1 Ag7 44.7(4) . .
O4 V O1 Ag7 -61.8(7) . .
O4 V O1 Ag7 -84.0(6) 2_666 .
C1 Ag2 O1 V 61.0(4) . .
O6 Ag2 O1 V 159.5(4) . .
C13 Ag2 O1 V -82.9(4) . .
C14 Ag2 O1 V -80.5(4) . .
Ag1A Ag2 O1 V 88.0(4) . .
Ag1B Ag2 O1 V 82.7(4) . .
Ag3B Ag2 O1 V 22.8(4) . .
Ag5 Ag2 O1 V -37.5(4) . .
Ag3A Ag2 O1 V 18.9(4) . .
Ag6 Ag2 O1 V -104.2(4) . .
C1 Ag2 O1 Ag7 -143.5(3) . .
O6 Ag2 O1 Ag7 -44.9(3) . .
C13 Ag2 O1 Ag7 72.6(3) . .
C14 Ag2 O1 Ag7 75.1(3) . .
Ag1A Ag2 O1 Ag7 -116.4(3) . .
Ag1B Ag2 O1 Ag7 -121.8(3) . .
Ag3B Ag2 O1 Ag7 178.3(3) . .
Ag5 Ag2 O1 Ag7 118.0(2) . .
Ag3A Ag2 O1 Ag7 174.4(2) . .
Ag6 Ag2 O1 Ag7 51.37(19) . .
C31 Ag7 O1 V -76.3(4) 2_666 .
O5 Ag7 O1 V 166.2(4) . .
C7 Ag7 O1 V 84.3(4) . .
Ag4 Ag7 O1 V -27.7(3) 2_666 .
Ag10 Ag7 O1 V 35.5(3) . .
Ag6 Ag7 O1 V 104.0(4) . .
Ag11 Ag7 O1 V -87.8(3) 2_666 .
C31 Ag7 O1 Ag2 126.6(3) 2_666 .
O5 Ag7 O1 Ag2 9.0(3) . .
C7 Ag7 O1 Ag2 -72.8(3) . .
Ag4 Ag7 O1 Ag2 175.2(2) 2_666 .
Ag10 Ag7 O1 Ag2 -121.6(2) . .
Ag6 Ag7 O1 Ag2 -53.2(2) . .
Ag11 Ag7 O1 Ag2 115.1(3) 2_666 .
C1 Ag3A O2 V -67.8(4) . .
O9 Ag3A O2 V 164.7(3) 2_666 .
C19 Ag3A O2 V 83.4(3) . .
Ag5 Ag3A O2 V 37.5(3) . .
Ag10 Ag3A O2 V 108.8(3) 2_666 .
Ag2 Ag3A O2 V -24.2(3) . .
Ag1B Ag3A O2 V -79.1(3) . .
Ag1A Ag3A O2 V -73.8(3) . .
O1 V O3 Ag9 163.2(4) . 2_666
O2 V O3 Ag9 41.7(5) . 2_666
O4 V O3 Ag9 -73.8(8) . 2_666
O4 V O3 Ag9 -84.2(9) 2_666 2_666
O1 V O3 Ag4 -40.9(5) . 2_666
O2 V O3 Ag4 -162.4(3) . 2_666
O4 V O3 Ag4 82.1(8) . 2_666
O4 V O3 Ag4 71.7(9) 2_666 2_666
O1 V O4 O4 -48(3) . 2_666
O2 V O4 O4 83(3) . 2_666
O3 V O4 O4 -163(2) . 2_666
O1 V O4 V -48(3) . 2_666
O2 V O4 V 83(3) . 2_666
O3 V O4 V -163(2) . 2_666
O4 V O4 V 0.000(3) 2_666 2_666
C31 Ag7 O5 C43 -29.4(8) 2_666 .
C7 Ag7 O5 C43 173.9(7) . .
O1 Ag7 O5 C43 68.6(7) . .
Ag4 Ag7 O5 C43 16.4(11) 2_666 .
Ag10 Ag7 O5 C43 160.5(6) . .
Ag6 Ag7 O5 C43 133.9(8) . .
Ag11 Ag7 O5 C43 11.0(7) 2_666 .
C1 Ag2 O6 C43 159.3(6) . .
C13 Ag2 O6 C43 -52.9(7) . .
O1 Ag2 O6 C43 49.7(6) . .
C14 Ag2 O6 C43 -82.1(6) . .
Ag1A Ag2 O6 C43 112.7(6) . .
Ag1B Ag2 O6 C43 116.1(6) . .
Ag3B Ag2 O6 C43 138.8(6) . .
Ag5 Ag2 O6 C43 -40.0(10) . .
Ag3A Ag2 O6 C43 137.5(5) . .
Ag6 Ag2 O6 C43 -13.6(6) . .
C25 Ag9 O7 C45 82.1(11) . .
O3 Ag9 O7 C45 -25.2(11) 2_666 .
C13 Ag9 O7 C45 -127.4(10) . .
C26 Ag9 O7 C45 111.6(10) . .
Ag5 Ag9 O7 C45 -81.4(10) . .
Ag6 Ag9 O7 C45 -124.9(9) . .
Ag12 Ag9 O7 C45 36.8(11) . .
Ag8 Ag9 O7 C45 76.9(16) . .
C31 Ag4 O8 C45 -151.6(7) . .
C19 Ag4 O8 C45 57.9(7) . .
O3 Ag4 O8 C45 -44.8(7) 2_666 .
Ag7 Ag4 O8 C45 -146.9(5) 2_666 .
Ag5 Ag4 O8 C45 14.0(7) . .
Ag10 Ag4 O8 C45 63.5(9) 2_666 .
Ag11 Ag4 O8 C45 -108.9(7) . .
C7 Ag10 O9 C47 -14.7(6) . .
C19 Ag10 O9 C47 -176.5(6) 2_666 .
Ag3A Ag10 O9 C47 133.3(6) 2_666 .
Ag7 Ag10 O9 C47 -59.4(7) . .
Ag8 Ag10 O9 C47 25.0(5) . .
Ag3B Ag10 O9 C47 131.1(6) 2_666 .
Ag4 Ag10 O9 C47 -155.6(5) 2_666 .
C13 Ag2 C1 Ag3A 60.3(3) . .
O1 Ag2 C1 Ag3A -65.6(2) . .
C14 Ag2 C1 Ag3A 81.5(2) . .
Ag1A Ag2 C1 Ag3A -97.5(3) . .
Ag1B Ag2 C1 Ag3A -93.7(2) . .
Ag3B Ag2 C1 Ag3A -1.8(3) . .
Ag5 Ag2 C1 Ag3A 24.28(18) . .
Ag6 Ag2 C1 Ag3A -8.3(7) . .
O6 Ag2 C1 Ag1A -63.8(3) . .
C13 Ag2 C1 Ag1A 157.8(3) . .
O1 Ag2 C1 Ag1A 31.9(3) . .
C14 Ag2 C1 Ag1A 179.0(3) . .
Ag1B Ag2 C1 Ag1A 3.8(3) . .
Ag3B Ag2 C1 Ag1A 95.7(4) . .
Ag5 Ag2 C1 Ag1A 121.8(3) . .
Ag3A Ag2 C1 Ag1A 97.5(3) . .
Ag6 Ag2 C1 Ag1A 89.2(6) . .
C37 Ag1A C1 C2 63.7(17) 2_666 .
C38 Ag1A C1 C2 44.9(10) 2_666 .
Ag2 Ag1A C1 C2 -148.3(8) . .
Ag11 Ag1A C1 C2 -159.0(8) 2_666 .
Ag3B Ag1A C1 C2 125.3(9) . .
Ag3A Ag1A C1 C2 128.4(8) . .
