#------------------------------------------------------------------------------
#$Date: 2016-03-21 18:05:52 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178801 $
#$URL: svn://www.crystallography.net/cod/cif/4/10/55/4105536.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4105536
loop_
_publ_author_name
'Anantharamulu Navulla'
'Alexander A. Tsirlin'
'Artem M. Abakumov'
'Roman V. Shpanchenko'
'Haitao Zhang'
'Evgeny V. Dikarev'
_publ_contact_author_address
;
Department of Chemistry
University at Albany
1400 Washington ave
Albany NY 12222
USA
;
_publ_contact_author_email       dikarev@albany.edu
_publ_contact_author_fax         518-442-3462
_publ_contact_author_name
;
Dikarev, Evgeny V.
;
_publ_contact_author_phone       518-442-4401
_publ_section_title
;
 Fluorinated Heterometallic β-Diketonates as Volatile Single-Source
 Precursors for the Synthesis of Low-Valent Mixed-Metal Fluorides
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              692
_journal_page_last               694
_journal_paper_doi               10.1021/ja109128r
_journal_volume                  133
_journal_year                    2011
_chemical_formula_sum            'C20 H4 F24 O8 Pb Zn'
_chemical_formula_weight         1100.79
_chemical_name_systematic
; 
 catena-(di(hexafluoroacetylacetonate)-zinc(II)-
 di(hexafluoroacetylacetonate)-lead(II))
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 107.3070(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            8
_cell_length_a                   18.3980(16)
_cell_length_b                   14.4711(13)
_cell_length_c                   23.748(2)
_cell_measurement_reflns_used    8135
_cell_measurement_temperature    100(2)
_cell_measurement_theta_max      28.21
_cell_measurement_theta_min      2.28
_cell_volume                     6036.4(9)
_computing_cell_refinement       'SMART, SAINT'
_computing_data_collection       SMART
_computing_data_reduction        SAINT
_computing_molecular_graphics    'SHELXP-93 (Sheldrick, 1993)'
_computing_publication_material  'SHELXCIF-93 (Sheldrick, 1993)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.998
_diffrn_measured_fraction_theta_max 0.935
_diffrn_measurement_device_type  'Bruker SMART APEX CCD'
_diffrn_measurement_method       '0.3 deg wide ω exposures'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0330
_diffrn_reflns_av_sigmaI/netI    0.0331
_diffrn_reflns_limit_h_max       24
_diffrn_reflns_limit_h_min       -24
_diffrn_reflns_limit_k_max       18
_diffrn_reflns_limit_k_min       -18
_diffrn_reflns_limit_l_max       31
_diffrn_reflns_limit_l_min       -30
_diffrn_reflns_number            50446
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         28.26
_diffrn_reflns_theta_min         1.67
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count na
_diffrn_standards_interval_time  na
_diffrn_standards_number         'none (area detector data)'
_exptl_absorpt_coefficient_mu    6.559
_exptl_absorpt_correction_T_max  0.3848
_exptl_absorpt_correction_T_min  0.2280
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
 SADABS (Bruker-AXS 2003)
;
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.422
_exptl_crystal_density_method    none
_exptl_crystal_description       block
_exptl_crystal_F_000             4128
_exptl_crystal_size_max          0.32
_exptl_crystal_size_mid          0.18
_exptl_crystal_size_min          0.18
_refine_diff_density_max         3.293
_refine_diff_density_min         -2.004
_refine_diff_density_rms         0.192
_refine_ls_extinction_coef       noref
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.028
_refine_ls_hydrogen_treatment    noref
_refine_ls_matrix_type           full
_refine_ls_number_parameters     958
_refine_ls_number_reflns         13979
_refine_ls_number_restraints     30
_refine_ls_restrained_S_all      1.030
_refine_ls_R_factor_all          0.0635
_refine_ls_R_factor_gt           0.0433
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0642P)²+29.1052P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1092
_refine_ls_wR_factor_ref         0.1222
_reflns_number_gt                10283
_reflns_number_total             13979
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ja109128r_si_002_1.cif
_cod_data_source_block           PbZn(CF3COCHCOCF3)4_(5)
_cod_original_cell_volume        6036.5(9)
_cod_database_code               4105536
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_group
Pb1 Pb 0.265278(11) 0.763553(14) 0.537648(9) 0.01859(7) Uani 1 1 d . .
Pb2 Pb 0.239295(11) 0.261952(14) 0.462261(9) 0.01846(7) Uani 1 1 d . .
Zn1 Zn 0.23825(4) 0.51900(4) 0.51732(3) 0.02134(15) Uani 1 1 d . .
Zn2 Zn 0.22205(4) 0.01818(4) 0.48252(3) 0.02211(15) Uani 1 1 d . .
O1 O 0.3428(2) 0.8957(3) 0.57592(18) 0.0258(9) Uani 1 1 d . .
O2 O 0.3633(2) 0.7068(3) 0.61933(18) 0.0246(9) Uani 1 1 d . .
O3 O 0.2287(2) 0.8070(3) 0.62176(18) 0.0237(9) Uani 1 1 d . .
O4 O 0.2173(2) 0.6111(3) 0.57921(17) 0.0201(8) Uani 1 1 d . .
O5 O 0.3307(2) 0.5943(3) 0.51655(18) 0.0213(8) Uani 1 1 d . .
O6 O 0.3059(2) 0.4147(3) 0.55649(18) 0.0242(9) Uani 1 1 d . .
O7 O 0.1791(2) 0.6071(3) 0.45341(18) 0.0243(9) Uani 1 1 d . .
O8 O 0.1583(2) 0.4224(3) 0.48610(19) 0.0238(9) Uani 1 1 d . .
O9 O 0.2901(2) 0.3923(3) 0.42447(18) 0.0242(9) Uani 1 1 d . .
O10 O 0.2722(2) 0.2031(3) 0.38004(19) 0.0260(9) Uani 1 1 d . .
O11 O 0.1374(2) 0.3071(3) 0.37855(18) 0.0243(9) Uani 1 1 d . .
O12 O 0.1572(2) 0.1105(3) 0.41917(17) 0.0208(8) Uani 1 1 d . .
O13 O 0.3176(2) 0.0894(3) 0.48335(18) 0.0215(8) Uani 1 1 d . .
O14 O 0.2569(2) -0.0881(3) 0.44300(19) 0.0265(9) Uani 1 1 d . .
O15 O 0.2122(2) 0.1113(3) 0.54356(19) 0.0265(9) Uani 1 1 d . .
O16 O 0.1648(2) -0.0743(3) 0.51579(18) 0.0224(9) Uani 1 1 d . .
C1 C 0.3906(4) 0.9067(4) 0.6258(3) 0.0288(14) Uani 1 1 d . .
C2 C 0.4216(4) 0.8428(5) 0.6700(3) 0.0317(15) Uani 1 1 d . .
H2 H 0.4541 0.8643 0.7066 0.038 Uiso 1 1 calc R .
C3 C 0.4070(4) 0.7483(4) 0.6629(3) 0.0254(13) Uani 1 1 d . .
C4 C 0.4169(4) 1.0090(5) 0.6379(3) 0.0384(17) Uani 1 1 d D 1
F1 F 0.4382(8) 1.0462(10) 0.5942(5) 0.064(5) Uiso 0.50 1 d PD 1
F2 F 0.4809(5) 1.0171(6) 0.6846(4) 0.040(2) Uiso 0.50 1 d PD 1
F3 F 0.3610(6) 1.0588(9) 0.6461(6) 0.063(4) Uiso 0.50 1 d PD 1
C4X C 0.4169(4) 1.0090(5) 0.6379(3) 0.990 Uiso 0.00 1 d PD 2
F1X F 0.4551(6) 1.0330(8) 0.5998(4) 0.036(3) Uiso 0.50 1 d PD 2
F2X F 0.4539(5) 1.0249(6) 0.6946(4) 0.045(2) Uiso 0.50 1 d PD 2
F3X F 0.3560(5) 1.0657(7) 0.6258(5) 0.039(3) Uiso 0.50 1 d PD 2
C5 C 0.4488(4) 0.6852(5) 0.7143(3) 0.0346(15) Uani 1 1 d D 1
F4 F 0.4664(6) 0.7215(7) 0.7660(4) 0.055(3) Uiso 0.50 1 d PD 1
F5 F 0.5072(7) 0.6445(10) 0.7038(6) 0.091(4) Uiso 0.50 1 d PD 1
F6 F 0.4061(6) 0.6120(8) 0.7166(5) 0.075(3) Uiso 0.50 1 d PD 1
C5X C 0.4488(4) 0.6852(5) 0.7143(3) 0.990 Uiso 0.00 1 d PD 2
F4X F 0.4279(7) 0.7010(8) 0.7605(5) 0.065(3) Uiso 0.50 1 d PD 2
F5X F 0.5252(5) 0.6989(8) 0.7280(5) 0.058(3) Uiso 0.50 1 d PD 2
F6X F 0.4466(5) 0.5994(6) 0.6992(4) 0.051(2) Uiso 0.50 1 d PD 2
C6 C 0.2180(3) 0.7646(4) 0.6646(3) 0.0227(12) Uani 1 1 d . .
C7 C 0.2042(4) 0.6700(4) 0.6698(3) 0.0275(13) Uani 1 1 d . .
H7 H 0.1942 0.6507 0.7050 0.033 Uiso 1 1 calc R .
C8 C 0.2040(3) 0.6025(4) 0.6287(3) 0.0234(12) Uani 1 1 d . .
C9 C 0.2199(4) 0.8255(5) 0.7180(3) 0.0322(15) Uani 1 1 d . .
F7 F 0.2873(3) 0.8127(3) 0.75973(18) 0.0465(11) Uani 1 1 d . .
F8 F 0.2146(3) 0.9150(3) 0.70407(19) 0.0510(12) Uani 1 1 d . .
F9 F 0.1656(3) 0.8043(3) 0.7418(2) 0.0579(13) Uani 1 1 d . .
C10 C 0.1868(4) 0.5038(4) 0.6443(3) 0.0306(14) Uani 1 1 d . .
F10 F 0.1560(3) 0.4994(3) 0.6881(2) 0.0439(11) Uani 1 1 d . .
F11 F 0.1381(3) 0.4633(3) 0.5979(2) 0.0617(15) Uani 1 1 d . .
F12 F 0.2499(3) 0.4540(3) 0.6593(3) 0.0632(15) Uani 1 1 d . .
C11 C 0.3984(3) 0.5724(4) 0.5440(3) 0.0212(12) Uani 1 1 d . .
C12 C 0.4251(3) 0.4923(4) 0.5755(3) 0.0246(13) Uani 1 1 d . .
H12 H 0.4780 0.4872 0.5956 0.029 Uiso 1 1 calc R .
C13 C 0.3775(3) 0.4193(4) 0.5790(3) 0.0214(12) Uani 1 1 d . .
C14 C 0.4592(3) 0.6429(4) 0.5399(3) 0.0243(12) Uani 1 1 d . .
F13 F 0.4285(2) 0.7258(3) 0.52192(19) 0.0369(10) Uani 1 1 d . .
F14 F 0.5127(2) 0.6552(3) 0.59145(18) 0.0358(9) Uani 1 1 d . .
F15 F 0.4946(2) 0.6143(3) 0.5015(2) 0.0406(10) Uani 1 1 d . .
C15 C 0.4123(4) 0.3341(5) 0.6147(3) 0.0299(14) Uani 1 1 d . .
F16 F 0.3999(3) 0.3355(3) 0.6662(2) 0.0574(13) Uani 1 1 d . .
F17 F 0.4865(2) 0.3276(3) 0.6240(2) 0.0537(13) Uani 1 1 d . .
F18 F 0.3818(3) 0.2572(3) 0.5874(2) 0.0542(13) Uani 1 1 d . .
C16 C 0.1122(3) 0.5946(4) 0.4212(3) 0.0239(12) Uani 1 1 d . .
C17 C 0.0662(3) 0.5173(4) 0.4183(3) 0.0254(13) Uani 1 1 d . .
H17 H 0.0156 0.5183 0.3924 0.030 Uiso 1 1 calc R .
C18 C 0.0920(3) 0.4386(4) 0.4523(3) 0.0228(12) Uani 1 1 d . .
C19 C 0.0789(4) 0.6762(5) 0.3807(3) 0.0325(15) Uani 1 1 d D 1
F19 F 0.1082(7) 0.7551(7) 0.4045(5) 0.065(3) Uiso 0.50 1 d PD 1
F20 F 0.0941(7) 0.6636(8) 0.3303(5) 0.071(3) Uiso 0.50 1 d PD 1
F21 F 0.0055(5) 0.6833(8) 0.3703(5) 0.062(3) Uiso 0.50 1 d PD 1
C19X C 0.0789(4) 0.6762(5) 0.3807(3) 0.990 Uiso 0.00 1 d PD 2
F19X F 0.0717(6) 0.7495(6) 0.4124(4) 0.045(2) Uiso 0.50 1 d PD 2
F20X F 0.1228(5) 0.7017(7) 0.3487(4) 0.047(2) Uiso 0.50 1 d PD 2
F21X F 0.0087(4) 0.6598(6) 0.3436(4) 0.045(2) Uiso 0.50 1 d PD 2
C20 C 0.0333(3) 0.3630(4) 0.4522(3) 0.0273(13) Uani 1 1 d . .
F22 F -0.0034(2) 0.3862(3) 0.4913(2) 0.0442(11) Uani 1 1 d . .
F23 F -0.0187(2) 0.3529(3) 0.40014(19) 0.0386(10) Uani 1 1 d . .
F24 F 0.0667(2) 0.2815(3) 0.46854(18) 0.0337(9) Uani 1 1 d . .
C21 C 0.3033(3) 0.4021(4) 0.3759(3) 0.0232(12) Uani 1 1 d . .
C22 C 0.3018(4) 0.3375(4) 0.3323(3) 0.0285(14) Uani 1 1 d . .
H22 H 0.3117 0.3580 0.2973 0.034 Uiso 1 1 calc R .
C23 C 0.2863(4) 0.2429(4) 0.3377(3) 0.0240(13) Uani 1 1 d . .
C24 C 0.3223(4) 0.5019(5) 0.3637(3) 0.0297(14) Uani 1 1 d . .
F25 F 0.3783(2) 0.5350(3) 0.40913(19) 0.0428(10) Uani 1 1 d . .
F26 F 0.2621(2) 0.5561(3) 0.3570(2) 0.0498(12) Uani 1 1 d . .
F27 F 0.3458(3) 0.5114(3) 0.31619(19) 0.0461(11) Uani 1 1 d . .
C25 C 0.2843(4) 0.1803(5) 0.2852(3) 0.0318(14) Uani 1 1 d . .
F28 F 0.3275(3) 0.2093(4) 0.2537(2) 0.0661(16) Uani 1 1 d . .
F29 F 0.3023(4) 0.0944(3) 0.3019(2) 0.0683(16) Uani 1 1 d . .
F30 F 0.2128(3) 0.1777(3) 0.2483(2) 0.0542(12) Uani 1 1 d . .
C26 C 0.0937(4) 0.2651(4) 0.3358(3) 0.0248(13) Uani 1 1 d . .
C27 C 0.0771(3) 0.1708(4) 0.3283(3) 0.0260(13) Uani 1 1 d . .
H27 H 0.0419 0.1520 0.2920 0.031 Uiso 1 1 calc R .
C28 C 0.1075(3) 0.1031(4) 0.3690(3) 0.0250(13) Uani 1 1 d . .
C29 C 0.0525(4) 0.3294(5) 0.2834(3) 0.0357(16) Uani 1 1 d D 1
F31 F 0.0824(7) 0.4133(7) 0.2915(5) 0.074(3) Uiso 0.50 1 d PD 1
F32 F -0.0180(8) 0.3483(12) 0.2853(8) 0.119(6) Uiso 0.50 1 d PD 1
F33 F 0.0458(7) 0.2979(8) 0.2327(5) 0.067(3) Uiso 0.50 1 d PD 1
C29X C 0.0525(4) 0.3294(5) 0.2834(3) 0.990 Uiso 0.00 1 d PD 2
F31X F 0.0467(5) 0.4137(5) 0.3004(4) 0.0364(18) Uiso 0.50 1 d PD 2
F32X F -0.0232(4) 0.3060(6) 0.2626(4) 0.041(2) Uiso 0.50 1 d PD 2
F33X F 0.0808(5) 0.3173(6) 0.2394(4) 0.040(2) Uiso 0.50 1 d PD 2
C30 C 0.0788(4) 0.0038(5) 0.3515(3) 0.0353(15) Uani 1 1 d . .
F34 F 0.0097(3) 0.0008(3) 0.3133(2) 0.0558(13) Uani 1 1 d . .
F35 F 0.1253(3) -0.0390(4) 0.3273(3) 0.0755(17) Uani 1 1 d . .
F36 F 0.0765(3) -0.0439(3) 0.3982(2) 0.0650(16) Uani 1 1 d . .
C31 C 0.3632(3) 0.0652(4) 0.4552(3) 0.0228(12) Uani 1 1 d . .
C32 C 0.3634(3) -0.0149(4) 0.4236(3) 0.0265(13) Uani 1 1 d . .
H32 H 0.4008 -0.0222 0.4038 0.032 Uiso 1 1 calc R .
C33 C 0.3106(3) -0.0853(4) 0.4199(3) 0.0250(13) Uani 1 1 d . .
C34 C 0.4282(3) 0.1343(4) 0.4586(3) 0.0293(14) Uani 1 1 d . .
F37 F 0.4126(2) 0.2180(3) 0.47530(19) 0.0342(9) Uani 1 1 d . .
F38 F 0.4429(2) 0.1430(3) 0.4072(2) 0.0419(10) Uani 1 1 d . .
F39 F 0.4921(2) 0.1058(3) 0.4980(2) 0.0502(12) Uani 1 1 d . .
C35 C 0.3133(4) -0.1702(5) 0.3816(3) 0.0313(14) Uani 1 1 d . .
F40 F 0.3795(3) -0.1799(3) 0.3708(2) 0.0614(14) Uani 1 1 d . .
F41 F 0.3010(3) -0.2470(3) 0.4073(2) 0.0478(12) Uani 1 1 d . .
F42 F 0.2591(3) -0.1636(4) 0.3310(2) 0.0670(15) Uani 1 1 d . .
C36 C 0.1734(3) 0.1010(4) 0.5787(3) 0.0249(13) Uani 1 1 d . .
C37 C 0.1298(3) 0.0253(4) 0.5836(3) 0.0264(13) Uani 1 1 d . .
H37 H 0.1001 0.0289 0.6101 0.032 Uiso 1 1 calc R .
C38 C 0.1273(3) -0.0552(4) 0.5518(3) 0.0218(12) Uani 1 1 d . .
C39 C 0.1744(4) 0.1845(5) 0.6190(3) 0.0361(16) Uani 1 1 d D 1
F43 F 0.2201(6) 0.2496(6) 0.6142(5) 0.046(2) Uiso 0.50 1 d PD 1
F44 F 0.1013(5) 0.2146(7) 0.6097(5) 0.053(2) Uiso 0.50 1 d PD 1
F45 F 0.1976(6) 0.1575(7) 0.6755(4) 0.053(2) Uiso 0.50 1 d PD 1
C39X C 0.1744(4) 0.1845(5) 0.6190(3) 0.990 Uiso 0.00 1 d PD 2
F43X F 0.1891(6) 0.2613(5) 0.5956(4) 0.037(2) Uiso 0.50 1 d PD 2
F44X F 0.1181(6) 0.1926(8) 0.6391(5) 0.060(3) Uiso 0.50 1 d PD 2
F45X F 0.2368(7) 0.1704(9) 0.6677(5) 0.078(3) Uiso 0.50 1 d PD 2
C40 C 0.0689(3) -0.1287(4) 0.5545(3) 0.0304(14) Uani 1 1 d . .
F46 F -0.0001(2) -0.1044(3) 0.5194(2) 0.0493(12) Uani 1 1 d . .
F47 F 0.0629(2) -0.1398(3) 0.6088(2) 0.0415(10) Uani 1 1 d . .
F48 F 0.0848(2) -0.2110(3) 0.53548(17) 0.0320(8) Uani 1 1 d . .
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pb Pb -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_3
O2 Pb1 O3 74.94(14) .
O2 Pb1 O1 75.16(14) .
O3 Pb1 O1 75.84(14) .
O2 Pb1 O4 70.47(13) .
O3 Pb1 O4 72.56(13) .
O1 Pb1 O4 138.01(13) .
O2 Pb1 O5 65.52(13) .
O3 Pb1 O5 128.19(13) .
O1 Pb1 O5 121.29(13) .
O4 Pb1 O5 63.71(11) .
O2 Pb1 O16 135.07(13) 1_565
O3 Pb1 O16 67.42(13) 1_565
O1 Pb1 O16 72.65(13) 1_565
O4 Pb1 O16 117.73(11) 1_565
O5 Pb1 O16 159.40(12) 1_565
O10 Pb2 O11 75.01(14) .
O10 Pb2 O9 75.54(14) .
O11 Pb2 O9 76.63(14) .
O10 Pb2 O12 69.21(13) .
O11 Pb2 O12 72.08(13) .
O9 Pb2 O12 137.55(13) .
O10 Pb2 O13 65.80(13) .
O11 Pb2 O13 128.15(13) .
O9 Pb2 O13 121.51(12) .
O12 Pb2 O13 63.23(11) .
O10 Pb2 O8 136.08(13) .
O11 Pb2 O8 67.75(13) .
O9 Pb2 O8 73.94(13) .
O12 Pb2 O8 117.63(11) .
O13 Pb2 O8 158.05(12) .
O6 Zn1 O8 86.11(16) .
O6 Zn1 O5 90.13(16) .
O8 Zn1 O5 153.89(16) .
O6 Zn1 O7 160.24(17) .
O8 Zn1 O7 89.44(17) .
O5 Zn1 O7 85.43(16) .
O6 Zn1 O4 111.80(16) .
O8 Zn1 O4 115.70(15) .
O5 Zn1 O4 89.67(15) .
O7 Zn1 O4 87.46(16) .
O6 Zn1 C18 107.06(17) .
O8 Zn1 C18 20.96(17) .
O5 Zn1 C18 148.76(17) .
O7 Zn1 C18 69.50(17) .
O4 Zn1 C18 106.92(15) .
O6 Zn1 C13 20.64(16) .
O8 Zn1 C13 106.14(17) .
O5 Zn1 C13 69.95(16) .
O7 Zn1 C13 151.40(16) .
O4 Zn1 C13 106.15(16) .
C18 Zn1 C13 126.93(16) .
O6 Zn1 C11 69.64(16) .
O8 Zn1 C11 147.64(16) .
O5 Zn1 C11 20.87(16) .
O7 Zn1 C11 106.06(16) .
O4 Zn1 C11 93.64(15) .
C18 Zn1 C11 158.49(16) .
C13 Zn1 C11 49.23(16) .
O14 Zn2 O16 87.17(17) .
O14 Zn2 O15 162.65(18) .
O16 Zn2 O15 89.59(17) .
O14 Zn2 O13 89.84(16) .
O16 Zn2 O13 152.69(16) .
O15 Zn2 O13 85.24(16) .
O14 Zn2 O12 110.23(17) .
O16 Zn2 O12 117.06(16) .
O15 Zn2 O12 86.38(17) .
O13 Zn2 O12 89.39(15) .
O14 Zn2 C33 20.67(16) .
O16 Zn2 C33 107.20(17) .
O15 Zn2 C33 152.41(17) .
O13 Zn2 C33 69.72(16) .
O12 Zn2 C33 104.20(16) .
O14 Zn2 C38 108.16(17) .
O16 Zn2 C38 21.03(16) .
O15 Zn2 C38 69.17(16) .
O13 Zn2 C38 146.70(17) .
O12 Zn2 C38 109.10(15) .
C33 Zn2 C38 127.94(17) .
O14 Zn2 C31 69.35(16) .
O16 Zn2 C31 147.55(16) .
O15 Zn2 C31 106.08(17) .
O13 Zn2 C31 20.93(16) .
O12 Zn2 C31 92.60(15) .
C33 Zn2 C31 48.96(17) .
C38 Zn2 C31 157.06(15) .
C1 O1 Pb1 128.9(4) .
C1 O1 Zn2 137.4(4) 1_565
Pb1 O1 Zn2 88.10(12) 1_565
C3 O2 Pb1 130.8(4) .
C3 O2 Zn1 163.2(4) .
Pb1 O2 Zn1 64.44(9) .
C6 O3 Pb1 134.9(4) .
C8 O4 Zn1 135.0(4) .
C8 O4 Pb1 126.6(4) .
Zn1 O4 Pb1 96.65(14) .
C11 O5 Zn1 124.2(4) .
C11 O5 Pb1 122.1(3) .
Zn1 O5 Pb1 93.51(14) .
C13 O6 Zn1 125.6(4) .
C13 O6 Pb2 118.4(3) .
Zn1 O6 Pb2 98.26(15) .
C16 O7 Zn1 125.1(4) .
C16 O7 Pb1 135.6(4) .
Zn1 O7 Pb1 85.37(13) .
C18 O8 Zn1 124.6(4) .
C18 O8 Pb2 118.5(3) .
Zn1 O8 Pb2 105.49(15) .
C21 O9 Pb2 129.5(4) .
C21 O9 Zn1 137.9(4) .
Pb2 O9 Zn1 87.93(12) .
C23 O10 Pb2 131.4(4) .
C23 O10 Zn2 163.7(4) .
Pb2 O10 Zn2 64.34(9) .
C26 O11 Pb2 134.5(4) .
C28 O12 Zn2 135.6(4) .
C28 O12 Pb2 126.3(4) .
Zn2 O12 Pb2 96.40(14) .
C31 O13 Zn2 124.1(4) .
C31 O13 Pb2 121.9(3) .
Zn2 O13 Pb2 92.98(14) .
C33 O14 Zn2 125.3(4) .
C33 O14 Pb1 117.6(4) 1_545
Zn2 O14 Pb1 98.44(15) 1_545
C36 O15 Zn2 125.8(4) .
C36 O15 Pb2 137.4(4) .
Zn2 O15 Pb2 87.49(14) .
C38 O16 Zn2 124.8(4) .
C38 O16 Pb1 119.5(3) 1_545
Zn2 O16 Pb1 103.11(15) 1_545
O1 C1 C2 130.0(6) .
O1 C1 C4 112.7(6) .
C2 C1 C4 117.3(6) .
O1 C1 Pb1 34.0(3) .
C2 C1 Pb1 96.5(4) .
C4 C1 Pb1 145.6(4) .
O1 C1 Zn2 30.9(3) 1_565
C2 C1 Zn2 155.5(4) 1_565
C4 C1 Zn2 84.2(4) 1_565
Pb1 C1 Zn2 61.47(10) 1_565
C1 C2 C3 122.8(6) .
C1 C2 Pb1 62.0(3) .
C3 C2 Pb1 61.8(4) .
C1 C2 H2 118.6 .
C3 C2 H2 118.6 .
Pb1 C2 H2 169.8 .
O2 C3 C2 128.3(6) .
O2 C3 C5 114.7(6) .
C2 C3 C5 117.0(6) .
O2 C3 Pb1 32.6(3) .
C2 C3 Pb1 96.5(4) .
C5 C3 Pb1 145.5(4) .
F3 C4 F1 108.6(10) .
F3 C4 F2 111.0(9) .
F1 C4 F2 102.6(9) .
F3 C4 C1 109.4(8) .
F1 C4 C1 112.9(9) .
F2 C4 C1 112.2(7) .
C4 F1 Zn2 90.6(7) 1_565
C4 F3 Zn2 94.5(7) 1_565
F4 C5 F5 112.2(9) .
F4 C5 F6 105.6(9) .
F5 C5 F6 100.2(9) .
F4 C5 C3 116.1(7) .
F5 C5 C3 111.2(8) .
F6 C5 C3 110.1(7) .
O3 C6 C7 128.8(6) .
O3 C6 C9 114.7(5) .
C7 C6 C9 116.5(6) .
O3 C6 Pb1 29.9(3) .
C7 C6 Pb1 100.2(4) .
C9 C6 Pb1 142.3(4) .
C8 C7 C6 126.1(6) .
C8 C7 Pb1 67.4(3) .
C6 C7 Pb1 59.0(3) .
C8 C7 H7 116.9 .
C6 C7 H7 116.9 .
Pb1 C7 H7 173.5 .
O4 C8 C7 128.4(6) .
O4 C8 C10 115.0(5) .
C7 C8 C10 116.5(5) .
O4 C8 Zn1 28.3(3) .
C7 C8 Zn1 155.5(4) .
C10 C8 Zn1 87.2(3) .
O4 C8 Pb1 36.8(3) .
C7 C8 Pb1 91.8(4) .
C10 C8 Pb1 151.3(4) .
Zn1 C8 Pb1 64.11(11) .
F9 C9 F8 108.8(6) .
F9 C9 F7 107.5(5) .
F8 C9 F7 107.4(6) .
F9 C9 C6 112.6(6) .
F8 C9 C6 111.7(5) .
F7 C9 C6 108.5(5) .
F12 C10 F10 108.0(6) .
F12 C10 F11 107.7(6) .
F10 C10 F11 106.8(6) .
F12 C10 C8 110.2(5) .
F10 C10 C8 113.6(5) .
F11 C10 C8 110.2(5) .
F12 C10 Zn1 79.7(4) .
F10 C10 Zn1 171.1(5) .
F11 C10 Zn1 66.0(3) .
C8 C10 Zn1 66.2(3) .
C10 F11 Zn1 91.1(4) .
C10 F12 Zn1 78.1(4) .
O5 C11 C12 128.7(5) .
O5 C11 C14 115.2(5) .
C12 C11 C14 116.1(5) .
O5 C11 Zn1 34.9(3) .
C12 C11 Zn1 93.9(4) .
C14 C11 Zn1 150.0(4) .
O5 C11 Pb1 41.0(3) .
C12 C11 Pb1 140.9(4) .
C14 C11 Pb1 89.3(3) .
Zn1 C11 Pb1 64.76(10) .
C11 C12 C13 122.6(5) .
C11 C12 Zn1 61.5(3) .
C13 C12 Zn1 61.4(3) .
C11 C12 H12 118.7 .
C13 C12 H12 118.7 .
Zn1 C12 H12 174.5 .
O6 C13 C12 127.4(5) .
O6 C13 C15 113.9(5) .
C12 C13 C15 118.7(5) .
O6 C13 Zn1 33.8(3) .
C12 C13 Zn1 93.9(4) .
C15 C13 Zn1 146.9(4) .
O6 C13 Pb2 44.9(3) .
C12 C13 Pb2 133.8(4) .
C15 C13 Pb2 90.0(4) .
Zn1 C13 Pb2 69.05(11) .
F14 C14 F15 106.9(5) .
F14 C14 F13 107.4(5) .
F15 C14 F13 107.7(5) .
F14 C14 C11 112.6(5) .
F15 C14 C11 110.5(5) .
F13 C14 C11 111.5(5) .
F14 C14 Pb1 111.7(3) .
F15 C14 Pb1 138.4(4) .
F13 C14 Pb1 46.2(3) .
C11 C14 Pb1 67.9(3) .
C14 F13 Pb1 116.1(3) .
F16 C15 F17 107.7(6) .
F16 C15 F18 107.6(6) .
F17 C15 F18 106.8(6) .
F16 C15 C13 110.2(5) .
F17 C15 C13 113.2(5) .
F18 C15 C13 111.1(5) .
F16 C15 Pb2 120.8(4) .
F17 C15 Pb2 127.6(4) .
F18 C15 Pb2 42.6(3) .
C13 C15 Pb2 68.6(3) .
C15 F18 Pb2 121.7(4) .
O7 C16 C17 128.2(6) .
O7 C16 C19 114.2(5) .
C17 C16 C19 117.6(5) .
O7 C16 Zn1 34.4(3) .
C17 C16 Zn1 93.9(4) .
C19 C16 Zn1 148.3(4) .
O7 C16 Pb1 32.1(3) .
C17 C16 Pb1 142.8(4) .
C19 C16 Pb1 91.7(3) .
Zn1 C16 Pb1 58.33(10) .
C16 C17 C18 121.9(6) .
C16 C17 Zn1 61.5(3) .
C18 C17 Zn1 60.6(3) .
C16 C17 H17 119.0 .
C18 C17 H17 119.0 .
Zn1 C17 H17 175.7 .
O8 C18 C17 128.0(5) .
O8 C18 C20 114.4(5) .
C17 C18 C20 117.5(5) .
O8 C18 Zn1 34.5(3) .
C17 C18 Zn1 94.7(4) .
C20 C18 Zn1 145.3(4) .
O8 C18 Pb2 43.9(3) .
C17 C18 Pb2 136.2(4) .
C20 C18 Pb2 90.5(3) .
Zn1 C18 Pb2 72.39(12) .
F21 C19 F19 106.3(9) .
F21 C19 F20 109.1(9) .
F19 C19 F20 109.8(9) .
F21 C19 C16 112.2(7) .
F19 C19 C16 111.2(7) .
F20 C19 C16 108.1(7) .
C19 F19 Pb1 121.8(7) .
F23 C20 F24 108.4(5) .
F23 C20 F22 107.4(5) .
F24 C20 F22 107.6(5) .
F23 C20 C18 113.0(5) .
F24 C20 C18 111.5(5) .
F22 C20 C18 108.7(5) .
F23 C20 Pb2 115.0(4) .
F24 C20 Pb2 46.6(3) .
F22 C20 Pb2 135.4(4) .
C18 C20 Pb2 66.9(3) .
F23 C20 Zn1 135.2(4) .
F24 C20 Zn1 94.7(3) .
F22 C20 Zn1 100.9(3) .
C18 C20 Zn1 22.9(3) .
Pb2 C20 Zn1 56.86(8) .
C20 F24 Pb2 115.9(3) .
O9 C21 C22 130.0(6) .
O9 C21 C24 113.3(5) .
C22 C21 C24 116.7(5) .
O9 C21 Pb2 33.6(3) .
C22 C21 Pb2 96.7(4) .
C24 C21 Pb2 146.0(4) .
O9 C21 Zn1 30.6(3) .
C22 C21 Zn1 155.7(4) .
C24 C21 Zn1 84.6(3) .
Pb2 C21 Zn1 61.39(9) .
C21 C22 C23 123.0(6) .
C21 C22 Pb2 61.8(3) .
C23 C22 Pb2 61.6(4) .
C21 C22 H22 118.5 .
C23 C22 H22 118.5 .
Pb2 C22 H22 173.5 .
O10 C23 C22 127.9(6) .
O10 C23 C25 114.9(5) .
C22 C23 C25 117.2(6) .
O10 C23 Pb2 32.2(3) .
C22 C23 Pb2 96.5(4) .
C25 C23 Pb2 145.2(4) .
F26 C24 F27 107.9(5) .
F26 C24 F25 107.5(6) .
F27 C24 F25 106.2(5) .
F26 C24 C21 110.5(5) .
F27 C24 C21 114.0(5) .
F25 C24 C21 110.4(5) .
C24 F26 Zn1 97.5(4) .
F28 C25 F29 109.4(6) .
F28 C25 F30 106.1(6) .
F29 C25 F30 106.3(6) .
F28 C25 C23 113.7(6) .
F29 C25 C23 111.8(5) .
F30 C25 C23 109.1(5) .
O11 C26 C27 130.0(6) .
O11 C26 C29 113.7(5) .
C27 C26 C29 116.3(6) .
O11 C26 Pb2 30.2(3) .
C27 C26 Pb2 100.7(4) .
C29 C26 Pb2 142.0(4) .
C28 C27 C26 125.3(6) .
C28 C27 Pb2 67.2(3) .
C26 C27 Pb2 58.6(3) .
C28 C27 H27 117.4 .
C26 C27 H27 117.4 .
Pb2 C27 H27 171.4 .
O12 C28 C27 128.9(6) .
O12 C28 C30 115.1(5) .
C27 C28 C30 116.0(6) .
O12 C28 Zn2 27.9(3) .
C27 C28 Zn2 156.0(4) .
C30 C28 Zn2 87.5(4) .
O12 C28 Pb2 37.1(3) .
C27 C28 Pb2 92.1(4) .
C30 C28 Pb2 151.2(4) .
Zn2 C28 Pb2 64.08(11) .
F33 C29 F31 112.9(10) .
F33 C29 F32 106.7(11) .
F31 C29 F32 100.0(10) .
F33 C29 C26 115.7(8) .
F31 C29 C26 110.4(8) .
F32 C29 C26 110.0(9) .
F36 C30 F35 107.9(6) .
F36 C30 F34 107.1(6) .
F35 C30 F34 107.6(6) .
F36 C30 C28 110.8(6) .
F35 C30 C28 109.9(6) .
F34 C30 C28 113.4(6) .
F36 C30 Zn2 58.5(3) .
F35 C30 Zn2 90.0(4) .
F34 C30 Zn2 160.7(5) .
C28 C30 Zn2 65.8(3) .
C30 F35 Zn2 69.0(4) .
C30 F36 Zn2 99.2(4) .
O13 C31 C32 128.8(5) .
O13 C31 C34 114.7(5) .
C32 C31 C34 116.5(5) .
O13 C31 Zn2 34.9(3) .
C32 C31 Zn2 94.0(4) .
C34 C31 Zn2 149.4(4) .
O13 C31 Pb2 41.1(3) .
C32 C31 Pb2 140.8(4) .
C34 C31 Pb2 88.7(3) .
Zn2 C31 Pb2 64.48(11) .
C31 C32 C33 122.3(6) .
C31 C32 Zn2 61.6(3) .
C33 C32 Zn2 61.0(3) .
C31 C32 H32 118.8 .
C33 C32 H32 118.8 .
Zn2 C32 H32 175.0 .
O14 C33 C32 128.0(6) .
O14 C33 C35 113.4(5) .
C32 C33 C35 118.5(5) .
O14 C33 Zn2 34.0(3) .
C32 C33 Zn2 94.4(4) .
C35 C33 Zn2 146.2(4) .
O14 C33 Pb1 45.4(3) 1_545
C32 C33 Pb1 132.1(4) 1_545
C35 C33 Pb1 91.6(3) 1_545
Zn2 C33 Pb1 69.27(12) 1_545
F37 C34 F39 107.3(5) .
F37 C34 F38 107.9(5) .
F39 C34 F38 107.1(5) .
F37 C34 C31 111.9(5) .
F39 C34 C31 110.2(5) .
F38 C34 C31 112.3(5) .
F37 C34 Pb2 45.7(3) .
F39 C34 Pb2 136.7(4) .
F38 C34 Pb2 113.3(4) .
C31 C34 Pb2 68.4(3) .
C34 F37 Pb2 116.9(3) .
F42 C35 F41 107.1(6) .
F42 C35 F40 108.8(6) .
F41 C35 F40 107.2(6) .
F42 C35 C33 109.4(6) .
F41 C35 C33 111.0(5) .
F40 C35 C33 113.1(6) .
F42 C35 Pb1 121.6(4) 1_545
F41 C35 Pb1 44.3(3) 1_545
F40 C35 Pb1 126.8(5) 1_545
C33 C35 Pb1 66.8(3) 1_545
C35 F41 Pb1 119.8(4) 1_545
O15 C36 C37 127.4(6) .
O15 C36 C39 114.6(5) .
C37 C36 C39 118.0(6) .
O15 C36 Zn2 33.9(3) .
C37 C36 Zn2 93.5(4) .
C39 C36 Zn2 148.5(4) .
O15 C36 Pb2 30.5(3) .
C37 C36 Pb2 143.9(4) .
C39 C36 Pb2 91.3(4) .
Zn2 C36 Pb2 59.00(11) .
C38 C37 C36 123.3(6) .
C38 C37 Zn2 61.4(3) .
C36 C37 Zn2 62.0(3) .
C38 C37 H37 118.4 .
C36 C37 H37 118.4 .
Zn2 C37 H37 175.6 .
O16 C38 C37 127.6(5) .
O16 C38 C40 113.8(5) .
C37 C38 C40 118.3(5) .
O16 C38 Zn2 34.2(2) .
C37 C38 Zn2 94.1(4) .
C40 C38 Zn2 145.1(4) .
O16 C38 Pb1 43.2(3) 1_545
C37 C38 Pb1 136.7(4) 1_545
C40 C38 Pb1 91.1(3) 1_545
Zn2 C38 Pb1 70.72(12) 1_545
F43 C39 F45 106.1(8) .
F43 C39 F44 112.8(8) .
F45 C39 F44 105.0(8) .
F43 C39 C36 113.9(7) .
F45 C39 C36 109.6(7) .
F44 C39 C36 108.8(7) .
C39 F43 Pb2 111.8(6) .
F47 C40 F48 108.0(5) .
F47 C40 F46 107.3(5) .
F48 C40 F46 106.6(5) .
F47 C40 C38 112.7(6) .
F48 C40 C38 112.3(5) .
F46 C40 C38 109.7(5) .
F47 C40 Pb1 112.3(4) 1_545
F48 C40 Pb1 48.3(3) 1_545
F46 C40 Pb1 138.1(4) 1_545
C38 C40 Pb1 66.8(3) 1_545
C40 F48 Pb1 114.2(3) 1_545
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pb1 O2 2.368(4) .
Pb1 O3 2.375(4) .
Pb1 O1 2.397(4) .
Pb1 O4 2.672(4) .
Pb1 O5 2.838(4) .
Pb1 O16 2.935(4) 1_565
Pb2 O10 2.368(4) .
Pb2 O11 2.382(4) .
Pb2 O9 2.395(4) .
Pb2 O12 2.685(4) .
Pb2 O13 2.852(4) .
Pb2 O8 2.904(4) .
Zn1 O6 2.000(4) .
Zn1 O8 2.005(4) .
Zn1 O5 2.025(4) .
Zn1 O7 2.032(4) .
Zn1 O4 2.103(4) .
Zn1 C18 2.917(6) .
Zn1 C13 2.926(6) .
Zn1 C11 2.927(5) .
Zn2 O14 2.004(4) .
Zn2 O16 2.005(4) .
Zn2 O15 2.026(4) .
Zn2 O13 2.033(4) .
Zn2 O12 2.098(4) .
Zn2 C33 2.924(6) .
Zn2 C38 2.929(6) .
Zn2 C31 2.938(6) .
O1 C1 1.258(7) .
O1 Zn2 3.173(4) 1_565
O2 C3 1.258(8) .
O3 C6 1.252(7) .
O4 C8 1.276(7) .
O5 C11 1.261(7) .
O6 C13 1.268(7) .
O7 C16 1.253(7) .
O8 C18 1.267(7) .
O9 C21 1.256(7) .
O10 C23 1.252(7) .
O11 C26 1.249(7) .
O12 C28 1.272(7) .
O13 C31 1.268(7) .
O14 C33 1.265(7) .
O14 Pb1 3.079(4) 1_545
O15 C36 1.258(7) .
O16 C38 1.280(7) .
O16 Pb1 2.935(4) 1_545
C1 C2 1.388(9) .
C1 C4 1.559(9) .
C1 Zn2 4.186(7) 1_565
C2 C3 1.394(9) .
C2 H2 0.9500 .
C3 C5 1.535(9) .
C4 F3 1.316(12) .
C4 F1 1.327(12) .
C4 F2 1.361(10) .
F1 Zn2 4.091(15) 1_565
F3 Zn2 4.007(13) 1_565
F3X Zn2 3.624(10) 1_565
C5 F4 1.285(11) .
C5 F5 1.311(12) .
C5 F6 1.331(12) .
C6 C7 1.403(8) .
C6 C9 1.537(9) .
C7 C8 1.381(9) .
C7 H7 0.9500 .
C8 C10 1.533(8) .
C9 F9 1.323(8) .
C9 F8 1.333(7) .
C9 F7 1.349(8) .
C10 F12 1.322(8) .
C10 F10 1.326(7) .
C10 F11 1.331(8) .
C11 C12 1.389(8) .
C11 C14 1.538(8) .
C12 C13 1.390(8) .
C12 H12 0.9500 .
C13 C15 1.524(8) .
C14 F14 1.335(7) .
C14 F15 1.335(7) .
C14 F13 1.342(7) .
C15 F16 1.311(8) .
C15 F17 1.320(7) .
C15 F18 1.326(8) .
C16 C17 1.392(8) .
C16 C19 1.532(9) .
C17 C18 1.396(9) .
C17 H17 0.9500 .
C18 C20 1.536(8) .
C19 F21 1.303(11) .
C19 F19 1.317(11) .
C19 F20 1.320(11) .
C20 F23 1.327(7) .
C20 F24 1.334(7) .
C20 F22 1.344(7) .
C21 C22 1.388(9) .
C21 C24 1.534(8) .
C22 C23 1.412(8) .
C22 H22 0.9500 .
C23 C25 1.533(9) .
C24 F26 1.327(8) .
C24 F27 1.331(7) .
C24 F25 1.339(8) .
C25 F28 1.312(7) .
C25 F29 1.317(8) .
C25 F30 1.347(8) .
C26 C27 1.399(9) .
C26 C29 1.559(9) .
C27 C28 1.374(9) .
C27 H27 0.9500 .
C28 C30 1.545(9) .
C29 F33 1.258(11) .
C29 F31 1.325(12) .
C29 F32 1.339(14) .
C30 F36 1.318(8) .
C30 F35 1.319(8) .
C30 F34 1.324(8) .
C31 C32 1.382(8) .
C31 C34 1.542(8) .
C32 C33 1.391(8) .
C32 H32 0.9500 .
C33 C35 1.538(8) .
C33 Pb1 3.832(6) 1_545
C34 F37 1.331(7) .
C34 F39 1.332(7) .
C34 F38 1.333(8) .
C35 F42 1.318(8) .
C35 F41 1.320(8) .
C35 F40 1.323(8) .
C35 Pb1 4.169(7) 1_545
F41 Pb1 3.353(5) 1_545
C36 C37 1.383(8) .
C36 C39 1.537(9) .
C37 C38 1.382(9) .
C37 H37 0.9500 .
C38 C40 1.526(8) .
C38 Pb1 3.735(6) 1_545
C39 F43 1.291(10) .
C39 F45 1.341(11) .
C39 F44 1.367(11) .
C40 F47 1.335(8) .
C40 F48 1.337(7) .
C40 F46 1.343(7) .
C40 Pb1 4.062(6) 1_545
F48 Pb1 3.326(4) 1_545
