#------------------------------------------------------------------------------
#$Date: 2016-03-21 18:14:26 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178806 $
#$URL: svn://www.crystallography.net/cod/cif/4/10/60/4106036.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4106036
loop_
_publ_author_name
'Giovanni Occhipinti'
'Christian Meermann'
'H. Martin Dietrich'
'Rannveig Litlabø'
'Florian Auras'
'Karl Wilhelm Törnroos'
'Cäcilia Maichle-Mössmer'
'Vidar R. Jensen'
'Reiner Anwander'
_publ_contact_author_address
;
Department of Chemistry,
University of Bergen,
Allégaten 41,
N-5007 Bergen,
Norway
;
_publ_contact_author_name
;
Prof. Karl Wilhelm Törnroos
;
_publ_section_title
;
 Synthesis and Stability of Homoleptic Metal(III) Tetramethylaluminates
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              6323
_journal_page_last               6337
_journal_paper_doi               10.1021/ja2001049
_journal_volume                  133
_journal_year                    2011
_chemical_formula_moiety         'C32 H80 Al4 Eu2'
_chemical_formula_sum            'C32 H80 Al4 Eu2'
_chemical_formula_weight         876.80
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           145
_symmetry_cell_setting           trigonal
_symmetry_space_group_name_Hall  'P 32'
_symmetry_space_group_name_H-M   'P 32'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            3
_cell_length_a                   11.8535(6)
_cell_length_b                   11.8535(6)
_cell_length_c                   27.0516(14)
_cell_measurement_reflns_used    9927
_cell_measurement_temperature    123(2)
_cell_measurement_theta_max      28.72
_cell_measurement_theta_min      2.49
_cell_volume                     3291.7(3)
_computing_cell_refinement       'Bruker SAINT'
_computing_data_collection       'Bruker APEX2'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 2008)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 2008)'
_diffrn_ambient_temperature      123(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'Bruker APEX-II CCD'
_diffrn_measurement_method       'φ and ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'Bruker TXS Rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0229
_diffrn_reflns_av_sigmaI/netI    0.0171
_diffrn_reflns_limit_h_max       16
_diffrn_reflns_limit_h_min       -16
_diffrn_reflns_limit_k_max       16
_diffrn_reflns_limit_k_min       -16
_diffrn_reflns_limit_l_max       36
_diffrn_reflns_limit_l_min       -36
_diffrn_reflns_number            50964
_diffrn_reflns_theta_full        28.75
_diffrn_reflns_theta_max         28.75
_diffrn_reflns_theta_min         1.98
_exptl_absorpt_coefficient_mu    2.929
_exptl_absorpt_correction_T_max  0.4737
_exptl_absorpt_correction_T_min  0.3871
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details
;
SADABS version 2008/1, G.M Sheldrick, University of 
Gẗtingen, Germany, 2008.
;
_exptl_crystal_colour            blue
_exptl_crystal_density_diffrn    1.327
_exptl_crystal_description       'triangular prism'
_exptl_crystal_F_000             1350
_exptl_crystal_size_max          0.40
_exptl_crystal_size_mid          0.38
_exptl_crystal_size_min          0.30
_refine_diff_density_max         3.625
_refine_diff_density_min         -1.278
_refine_diff_density_rms         0.140
_refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881'
_refine_ls_abs_structure_Flack   0.02(2)
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.159
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     392
_refine_ls_number_reflns         11318
_refine_ls_number_restraints     11
_refine_ls_restrained_S_all      1.159
_refine_ls_R_factor_all          0.0594
_refine_ls_R_factor_gt           0.0575
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0559P)²+12.6705P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1420
_refine_ls_wR_factor_ref         0.1439
_reflns_number_gt                10973
_reflns_number_total             11318
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ja2001049_si_010.cif
_cod_data_source_block           Compound5b
_cod_database_code               4106036
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z+2/3'
'-x+y, -x, z+1/3'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Eu1 Eu 0.74744(5) 0.65749(5) 0.315587(17) 0.05745(12) Uani 1 1 d . . .
Eu2 Eu 0.96924(4) 0.32409(4) 0.129301(16) 0.04898(10) Uani 1 1 d . A .
Al1 Al 0.6553(6) 0.8444(4) 0.29771(19) 0.0986(13) Uani 1 1 d D A .
Al2 Al 0.9984(3) 0.5572(3) 0.20252(13) 0.0604(7) Uani 1 1 d D . .
Al3 Al 0.7082(3) 0.1144(3) 0.06617(16) 0.0755(9) Uani 1 1 d . . .
Al4 Al 1.2241(3) 0.2842(3) 0.11686(12) 0.0579(6) Uani 1 1 d D . .
C1 C 0.672(13) 1.019(7) 0.282(5) 0.138(10) Uani 0.18(2) 1 d PD A 7
H1A H 0.6325 1.0152 0.2491 0.166 Uiso 0.18(2) 1 calc PR A 7
H1B H 0.6238 1.0402 0.3068 0.166 Uiso 0.18(2) 1 calc PR A 7
C2 C 0.810(12) 1.123(9) 0.282(5) 0.189(17) Uani 0.18(2) 1 d PD A 7
H2A H 0.8552 1.1069 0.2544 0.283 Uiso 0.18(2) 1 calc PR A 7
H2B H 0.8503 1.1223 0.3131 0.283 Uiso 0.18(2) 1 calc PR A 7
H2C H 0.8159 1.2076 0.2768 0.283 Uiso 0.18(2) 1 calc PR A 7
C1A C 0.570(3) 0.957(3) 0.2953(11) 0.138(10) Uani 0.82(2) 1 d PD A 8
H1C H 0.5106 0.9302 0.2664 0.166 Uiso 0.82(2) 1 calc PR A 8
H1D H 0.5158 0.9398 0.3253 0.166 Uiso 0.82(2) 1 calc PR A 8
C2A C 0.663(4) 1.098(2) 0.2919(11) 0.189(17) Uani 0.82(2) 1 d PD A 8
H2D H 0.7279 1.1138 0.2663 0.283 Uiso 0.82(2) 1 calc PR A 8
H2E H 0.7068 1.1295 0.3238 0.283 Uiso 0.82(2) 1 calc PR A 8
H2F H 0.6163 1.1439 0.2834 0.283 Uiso 0.82(2) 1 calc PR A 8
C3 C 0.669(2) 0.809(2) 0.3741(7) 0.127(8) Uani 1 1 d . A .
H3A H 0.7198 0.7644 0.3778 0.153 Uiso 1 1 calc R . .
H3B H 0.7151 0.8933 0.3918 0.153 Uiso 1 1 calc R . .
C4 C 0.546(4) 0.733(2) 0.3953(8) 0.207(18) Uani 1 1 d . . .
H4A H 0.5565 0.7191 0.4304 0.311 Uiso 1 1 calc R A .
H4B H 0.5007 0.6486 0.3784 0.311 Uiso 1 1 calc R . .
H4C H 0.4958 0.7774 0.3922 0.311 Uiso 1 1 calc R . .
C5 C 0.571(5) 0.694(4) 0.2646(10) 0.31(3) Uani 1 1 d . A .
H5A H 0.5879 0.6288 0.2807 0.375 Uiso 1 1 calc R . .
H5B H 0.4763 0.6611 0.2662 0.375 Uiso 1 1 calc R . .
C6 C 0.612(3) 0.707(3) 0.2108(8) 0.182(12) Uani 1 1 d . . .
H6A H 0.5594 0.6236 0.1939 0.273 Uiso 1 1 calc R A .
H6B H 0.7043 0.7324 0.2088 0.273 Uiso 1 1 calc R . .
H6C H 0.5989 0.7739 0.1948 0.273 Uiso 1 1 calc R . .
C7 C 0.835(3) 0.938(4) 0.3177(18) 0.127(11) Uani 0.36(2) 1 d PD A 5
H7A H 0.8336 1.0001 0.3420 0.153 Uiso 0.36(2) 1 calc PR A 5
H7B H 0.8403 0.8718 0.3382 0.153 Uiso 0.36(2) 1 calc PR A 5
C8 C 0.963(5) 1.010(5) 0.299(4) 0.191(18) Uani 0.36(2) 1 d PD A 5
H8A H 1.0250 1.0229 0.3260 0.286 Uiso 0.36(2) 1 calc PR A 5
H8B H 0.9797 1.0950 0.2876 0.286 Uiso 0.36(2) 1 calc PR A 5
H8C H 0.9748 0.9623 0.2722 0.286 Uiso 0.36(2) 1 calc PR A 5
C7A C 0.830(3) 0.925(2) 0.2689(13) 0.127(11) Uani 0.64(2) 1 d PD A 6
H7A1 H 0.8545 0.8567 0.2725 0.153 Uiso 0.64(2) 1 calc PR A 6
H7A2 H 0.8143 0.9277 0.2331 0.153 Uiso 0.64(2) 1 calc PR A 6
C8A C 0.9480(18) 1.0426(16) 0.2777(14) 0.191(18) Uani 0.64(2) 1 d PD A 6
H8D H 0.9919 1.0321 0.3065 0.286 Uiso 0.64(2) 1 calc PR A 6
H8E H 0.9290 1.1129 0.2839 0.286 Uiso 0.64(2) 1 calc PR A 6
H8F H 1.0046 1.0641 0.2486 0.286 Uiso 0.64(2) 1 calc PR A 6
C9 C 1.1784(18) 0.7016(16) 0.2181(14) 0.097(15) Uani 0.47(3) 1 d PRD A 1
H9A H 1.1970 0.6953 0.2533 0.116 Uiso 0.47(3) 1 calc PR A 1
H9B H 1.2414 0.6894 0.1981 0.116 Uiso 0.47(3) 1 calc PR A 1
C10 C 1.200(3) 0.840(2) 0.2082(12) 0.087(9) Uani 0.47(3) 1 d PD A 1
H10A H 1.1808 0.8467 0.1735 0.131 Uiso 0.47(3) 1 calc PR A 1
H10B H 1.2914 0.9044 0.2152 0.131 Uiso 0.47(3) 1 calc PR A 1
H10C H 1.1431 0.8554 0.2296 0.131 Uiso 0.47(3) 1 calc PR A 1
C9A C 1.160(2) 0.729(2) 0.2110(13) 0.082(10) Uani 0.53(3) 1 d PD A 2
H9C H 1.1551 0.7937 0.1892 0.098 Uiso 0.53(3) 1 calc PR A 2
H9D H 1.1645 0.7586 0.2456 0.098 Uiso 0.53(3) 1 calc PR A 2
C10A C 1.283(2) 0.725(3) 0.1992(13) 0.105(11) Uani 0.53(3) 1 d PD A 2
H10D H 1.2945 0.7261 0.1632 0.157 Uiso 0.53(3) 1 calc PR A 2
H10E H 1.2764 0.6452 0.2128 0.157 Uiso 0.53(3) 1 calc PR A 2
H10F H 1.3586 0.8010 0.2138 0.157 Uiso 0.53(3) 1 calc PR A 2
C11 C 0.9346(11) 0.5377(11) 0.1308(4) 0.068(3) Uani 1 1 d . A .
H11A H 1.0049 0.5497 0.1079 0.081 Uiso 1 1 calc R . .
H11B H 0.8592 0.4492 0.1257 0.081 Uiso 1 1 calc R . .
C12 C 0.8945(16) 0.6397(14) 0.1200(5) 0.092(4) Uani 1 1 d . . .
H12A H 0.8747 0.6379 0.0848 0.138 Uiso 1 1 calc R A .
H12B H 0.9660 0.7263 0.1289 0.138 Uiso 1 1 calc R . .
H12C H 0.8171 0.6201 0.1395 0.138 Uiso 1 1 calc R . .
C13 C 1.0096(9) 0.4002(9) 0.2267(4) 0.057(2) Uani 1 1 d . A .
H13A H 0.9265 0.3189 0.2203 0.069 Uiso 1 1 calc R . .
H13B H 1.0803 0.3952 0.2093 0.069 Uiso 1 1 calc R . .
C14 C 1.0379(17) 0.4182(15) 0.2837(5) 0.093(4) Uani 1 1 d . . .
H14A H 0.9636 0.4149 0.3009 0.139 Uiso 1 1 calc R A .
H14B H 1.1161 0.5026 0.2899 0.139 Uiso 1 1 calc R . .
H14C H 1.0519 0.3483 0.2960 0.139 Uiso 1 1 calc R . .
C15 C 0.8593(9) 0.5634(9) 0.2434(4) 0.062(2) Uani 1 1 d . A .
H15A H 0.8818 0.5661 0.2788 0.074 Uiso 1 1 calc R . .
H15B H 0.8597 0.6453 0.2357 0.074 Uiso 1 1 calc R . .
C16 C 0.7214(10) 0.4488(9) 0.2352(4) 0.060(2) Uani 1 1 d . . .
H16A H 0.6597 0.4606 0.2556 0.090 Uiso 1 1 calc R A .
H16B H 0.7184 0.3674 0.2445 0.090 Uiso 1 1 calc R . .
H16C H 0.6978 0.4449 0.2003 0.090 Uiso 1 1 calc R . .
C17 C 0.6626(18) -0.0649(14) 0.0481(9) 0.123(7) Uani 1 1 d . A .
H17A H 0.5696 -0.1234 0.0563 0.148 Uiso 1 1 calc R . .
H17B H 0.6713 -0.0681 0.0118 0.148 Uiso 1 1 calc R . .
C18 C 0.743(3) -0.1218(18) 0.0728(10) 0.147(9) Uani 1 1 d . . .
H18A H 0.8336 -0.0729 0.0613 0.221 Uiso 1 1 calc R A .
H18B H 0.7054 -0.2137 0.0637 0.221 Uiso 1 1 calc R . .
H18C H 0.7409 -0.1142 0.1088 0.221 Uiso 1 1 calc R . .
C19 C 0.5813(11) 0.1614(13) 0.0362(5) 0.077(3) Uani 1 1 d . A .
H19A H 0.5696 0.1357 0.0009 0.093 Uiso 1 1 calc R . .
H19B H 0.4960 0.1086 0.0527 0.093 Uiso 1 1 calc R . .
C20 C 0.6175(11) 0.3029(13) 0.0392(5) 0.081(3) Uani 1 1 d . . .
H20A H 0.6070 0.3242 0.0732 0.121 Uiso 1 1 calc R A .
H20B H 0.5606 0.3182 0.0173 0.121 Uiso 1 1 calc R . .
H20C H 0.7083 0.3581 0.0289 0.121 Uiso 1 1 calc R . .
C21 C 0.7048(9) 0.1451(15) 0.1401(5) 0.092(5) Uani 1 1 d . A .
H21A H 0.7619 0.1203 0.1581 0.110 Uiso 1 1 calc R . .
H21B H 0.7346 0.2379 0.1468 0.110 Uiso 1 1 calc R . .
C22 C 0.5631(13) 0.059(3) 0.1558(7) 0.182(13) Uani 1 1 d . . .
H22A H 0.5512 0.0835 0.1892 0.273 Uiso 1 1 calc R A .
H22B H 0.5409 -0.0323 0.1555 0.273 Uiso 1 1 calc R . .
H22C H 0.5062 0.0713 0.1328 0.273 Uiso 1 1 calc R . .
C23 C 0.8813(10) 0.2454(14) 0.0335(5) 0.077(3) Uani 1 1 d . A .
H23A H 0.9017 0.3357 0.0405 0.093 Uiso 1 1 calc R . .
H23B H 0.9531 0.2340 0.0464 0.093 Uiso 1 1 calc R . .
C24 C 0.8660(17) 0.220(2) -0.0232(5) 0.109(5) Uani 1 1 d . . .
H24A H 0.9455 0.2838 -0.0401 0.164 Uiso 1 1 calc R A .
H24B H 0.7918 0.2266 -0.0353 0.164 Uiso 1 1 calc R . .
H24C H 0.8508 0.1318 -0.0299 0.164 Uiso 1 1 calc R . .
C25 C 1.2305(11) 0.4532(11) 0.1012(5) 0.072(3) Uani 1 1 d . A .
H25A H 1.1657 0.4395 0.0754 0.087 Uiso 1 1 calc R . .
H25B H 1.2103 0.4878 0.1312 0.087 Uiso 1 1 calc R . .
C26 C 1.3689(11) 0.5500(11) 0.0828(7) 0.099(5) Uani 1 1 d . . .
H26A H 1.3672 0.6195 0.0639 0.148 Uiso 1 1 calc R A .
H26B H 1.4002 0.5042 0.0617 0.148 Uiso 1 1 calc R . .
H26C H 1.4274 0.5878 0.1112 0.148 Uiso 1 1 calc R . .
C27 C 1.0469(10) 0.1417(9) 0.1403(4) 0.065(3) Uani 1 1 d . A .
H27A H 1.0205 0.1699 0.1705 0.078 Uiso 1 1 calc R . .
H27B H 0.9805 0.1215 0.1144 0.078 Uiso 1 1 calc R . .
C28 C 1.0596(14) 0.0199(11) 0.1515(6) 0.089(4) Uani 1 1 d . . .
H28A H 0.9743 -0.0530 0.1609 0.133 Uiso 1 1 calc R A .
H28B H 1.1214 0.0396 0.1786 0.133 Uiso 1 1 calc R . .
H28C H 1.0911 -0.0036 0.1219 0.133 Uiso 1 1 calc R . .
C29 C 1.2603(9) 0.2216(11) 0.0525(4) 0.061(2) Uani 1 1 d . A .
H29A H 1.3547 0.2745 0.0453 0.074 Uiso 1 1 calc R . .
H29B H 1.2395 0.1303 0.0568 0.074 Uiso 1 1 calc R . .
C30 C 1.1878(17) 0.228(2) 0.0094(6) 0.122(6) Uani 1 1 d . . .
H30A H 1.2107 0.1948 -0.0199 0.184 Uiso 1 1 calc R A .
H30B H 1.2104 0.3185 0.0037 0.184 Uiso 1 1 calc R . .
H30C H 1.0941 0.1747 0.0157 0.184 Uiso 1 1 calc R . .
C31 C 1.3614(15) 0.322(2) 0.1659(6) 0.077(5) Uani 0.75(2) 1 d PD A 3
H31A H 1.3714 0.2443 0.1698 0.093 Uiso 0.75(2) 1 calc PR A 3
H31B H 1.4452 0.3944 0.1537 0.093 Uiso 0.75(2) 1 calc PR A 3
C32 C 1.3298(17) 0.359(2) 0.2159(5) 0.090(5) Uani 0.75(2) 1 d PD A 3
H32A H 1.2451 0.2885 0.2274 0.135 Uiso 0.75(2) 1 calc PR A 3
H32B H 1.3266 0.4393 0.2126 0.135 Uiso 0.75(2) 1 calc PR A 3
H32C H 1.3973 0.3717 0.2398 0.135 Uiso 0.75(2) 1 calc PR A 3
C31A C 1.335(6) 0.284(7) 0.1714(17) 0.077(5) Uani 0.25(2) 1 d PD A 4
H31C H 1.3974 0.3766 0.1790 0.093 Uiso 0.25(2) 1 calc PR A 4
H31D H 1.2775 0.2479 0.2006 0.093 Uiso 0.25(2) 1 calc PR A 4
C32A C 1.414(5) 0.214(6) 0.1675(18) 0.090(5) Uani 0.25(2) 1 d PD A 4
H32D H 1.4603 0.2239 0.1986 0.135 Uiso 0.25(2) 1 calc PR A 4
H32E H 1.4769 0.2519 0.1404 0.135 Uiso 0.25(2) 1 calc PR A 4
H32F H 1.3549 0.1212 0.1609 0.135 Uiso 0.25(2) 1 calc PR A 4
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Eu Eu -0.1578 3.6682 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C5 Eu1 C3 70.3(7) . .
C5 Eu1 C15 104.9(7) . .
C3 Eu1 C15 166.0(6) . .
C5 Eu1 C19 101.9(12) . 3_665
C3 Eu1 C19 93.2(6) . 3_665
C15 Eu1 C19 100.7(3) . 3_665
C5 Eu1 C29 152.6(7) . 3_775
C3 Eu1 C29 86.2(4) . 3_775
C15 Eu1 C29 94.6(3) . 3_775
C19 Eu1 C29 93.1(3) 3_665 3_775
C5 Eu1 C7 72.2(11) . .
C3 Eu1 C7 47.6(10) . .
C15 Eu1 C7 118.7(9) . .
C19 Eu1 C7 140.5(10) 3_665 .
C29 Eu1 C7 81.6(7) 3_775 .
C5 Eu1 Al1 36.5(7) . .
C3 Eu1 Al1 42.7(4) . .
C15 Eu1 Al1 126.3(3) . .
C19 Eu1 Al1 118.9(3) 3_665 .
C29 Eu1 Al1 116.1(2) 3_775 .
C7 Eu1 Al1 37.9(6) . .
C5 Eu1 C7A 60.1(12) . .
C3 Eu1 C7A 67.6(7) . .
C15 Eu1 C7A 98.6(6) . .
C19 Eu1 C7A 156.6(5) 3_665 .
C29 Eu1 C7A 98.5(7) 3_775 .
C7 Eu1 C7A 25.4(11) . .
Al1 Eu1 C7A 37.7(4) . .
C5 Eu1 C30 138.7(11) . 3_775
C3 Eu1 C30 96.8(5) . 3_775
C15 Eu1 C30 78.1(4) . 3_775
C19 Eu1 C30 118.3(4) 3_665 3_775
C29 Eu1 C30 28.1(4) 3_775 3_775
C7 Eu1 C30 70.7(7) . 3_775
Al1 Eu1 C30 108.6(4) . 3_775
C7A Eu1 C30 78.6(7) . 3_775
C13 Eu2 C27 94.7(3) . .
C13 Eu2 C11 76.5(3) . .
C27 Eu2 C11 168.2(4) . .
C13 Eu2 C23 168.6(3) . .
C27 Eu2 C23 93.1(4) . .
C11 Eu2 C23 96.8(4) . .
C13 Eu2 C21 95.4(4) . .
C27 Eu2 C21 94.7(4) . .
C11 Eu2 C21 94.0(4) . .
C23 Eu2 C21 75.6(4) . .
C13 Eu2 C25 96.8(3) . .
C27 Eu2 C25 75.2(3) . .
C11 Eu2 C25 97.7(3) . .
C23 Eu2 C25 93.3(3) . .
C21 Eu2 C25 164.8(4) . .
C13 Eu2 Al2 38.3(2) . .
C27 Eu2 Al2 131.4(3) . .
C11 Eu2 Al2 38.6(3) . .
C23 Eu2 Al2 135.4(3) . .
C21 Eu2 Al2 100.6(4) . .
C25 Eu2 Al2 94.7(3) . .
C13 Eu2 Al4 97.1(2) . .
C27 Eu2 Al4 37.83(19) . .
C11 Eu2 Al4 134.4(2) . .
C23 Eu2 Al4 94.2(2) . .
C21 Eu2 Al4 131.6(4) . .
C25 Eu2 Al4 37.4(3) . .
Al2 Eu2 Al4 117.68(8) . .
C13 Eu2 Al3 133.2(2) . .
C27 Eu2 Al3 91.1(3) . .
C11 Eu2 Al3 100.6(3) . .
C23 Eu2 Al3 38.2(3) . .
C21 Eu2 Al3 37.8(3) . .
C25 Eu2 Al3 129.5(3) . .
Al2 Eu2 Al3 127.58(9) . .
Al4 Eu2 Al3 114.73(9) . .
C5 Al1 C7 128(2) . .
C5 Al1 C7A 102.2(19) . .
C7 Al1 C7A 40.1(18) . .
C5 Al1 C1 129(4) . .
C7 Al1 C1 88(4) . .
C7A Al1 C1 83(4) . .
C5 Al1 C1A 115.0(13) . .
C7 Al1 C1A 113.6(18) . .
C7A Al1 C1A 114.9(11) . .
C1 Al1 C1A 32(3) . .
C5 Al1 C3 110.4(12) . .
C7 Al1 C3 70.8(15) . .
C7A Al1 C3 108.6(13) . .
C1 Al1 C3 115(4) . .
C1A Al1 C3 105.7(9) . .
C5 Al1 Eu1 64.3(7) . .
C7 Al1 Eu1 70.7(15) . .
C7A Al1 Eu1 74.5(8) . .
C1 Al1 Eu1 156(4) . .
C1A Al1 Eu1 170.0(8) . .
C3 Al1 Eu1 66.6(4) . .
C9A Al2 C9 14.7(11) . .
C9A Al2 C15 106.5(8) . .
C9 Al2 C15 113.3(10) . .
C9A Al2 C13 115.4(10) . .
C9 Al2 C13 100.7(7) . .
C15 Al2 C13 106.5(4) . .
C9A Al2 C11 109.6(11) . .
C9 Al2 C11 118.0(10) . .
C15 Al2 C11 105.1(5) . .
C13 Al2 C11 112.9(4) . .
C9A Al2 Eu2 125.1(8) . .
C9 Al2 Eu2 117.8(9) . .
C15 Al2 Eu2 128.2(3) . .
C13 Al2 Eu2 56.8(3) . .
C11 Al2 Eu2 57.0(3) . .
C17 Al3 C19 110.9(6) . .
C17 Al3 C21 114.6(8) . .
C19 Al3 C21 105.1(6) . .
C17 Al3 C23 109.9(8) . .
C19 Al3 C23 102.7(5) . .
C21 Al3 C23 112.9(5) . .
C17 Al3 Eu2 125.8(5) . .
C19 Al3 Eu2 123.1(4) . .
C21 Al3 Eu2 56.9(3) . .
C23 Al3 Eu2 56.6(3) . .
C31 Al4 C31A 12(2) . .
C31 Al4 C25 107.5(7) . .
C31A Al4 C25 118(2) . .
C31 Al4 C29 111.1(6) . .
C31A Al4 C29 112.4(17) . .
C25 Al4 C29 106.0(5) . .
C31 Al4 C27 111.9(6) . .
C31A Al4 C27 100(2) . .
C25 Al4 C27 113.7(4) . .
C29 Al4 C27 106.6(4) . .
C31 Al4 Eu2 127.6(5) . .
C31A Al4 Eu2 125.4(17) . .
C25 Al4 Eu2 57.3(3) . .
C29 Al4 Eu2 121.2(3) . .
C27 Al4 Eu2 56.4(3) . .
C2 C1 Al1 110(6) . .
C2 C1 H1A 109.6 . .
Al1 C1 H1A 109.6 . .
C2 C1 H1B 109.6 . .
Al1 C1 H1B 109.6 . .
H1A C1 H1B 108.1 . .
C1 C2 H2A 109.5 . .
C1 C2 H2B 109.5 . .
H2A C2 H2B 109.5 . .
C1 C2 H2C 109.5 . .
H2A C2 H2C 109.5 . .
H2B C2 H2C 109.5 . .
C2A C1A Al1 114(2) . .
C2A C1A H1C 108.8 . .
Al1 C1A H1C 108.8 . .
C2A C1A H1D 108.8 . .
Al1 C1A H1D 108.8 . .
H1C C1A H1D 107.7 . .
C1A C2A H2D 109.5 . .
C1A C2A H2E 109.5 . .
H2D C2A H2E 109.5 . .
C1A C2A H2F 109.5 . .
H2D C2A H2F 109.5 . .
H2E C2A H2F 109.5 . .
C4 C3 Al1 111.9(17) . .
C4 C3 Eu1 112.3(13) . .
Al1 C3 Eu1 70.7(5) . .
C4 C3 H3A 109.2 . .
Al1 C3 H3A 109.2 . .
Eu1 C3 H3A 41.0 . .
C4 C3 H3B 109.2 . .
Al1 C3 H3B 109.2 . .
Eu1 C3 H3B 134.7 . .
H3A C3 H3B 107.9 . .
C3 C4 H4A 109.5 . .
C3 C4 H4B 109.5 . .
H4A C4 H4B 109.5 . .
C3 C4 H4C 109.5 . .
H4A C4 H4C 109.5 . .
H4B C4 H4C 109.5 . .
C6 C5 Al1 113(3) . .
C6 C5 Eu1 106(2) . .
Al1 C5 Eu1 79.3(9) . .
C6 C5 H5A 109.0 . .
Al1 C5 H5A 109.0 . .
Eu1 C5 H5A 34.9 . .
C6 C5 H5B 109.0 . .
Al1 C5 H5B 109.0 . .
Eu1 C5 H5B 136.7 . .
H5A C5 H5B 107.8 . .
C5 C6 H6A 109.5 . .
C5 C6 H6B 109.5 . .
H6A C6 H6B 109.5 . .
C5 C6 H6C 109.5 . .
H6A C6 H6C 109.5 . .
H6B C6 H6C 109.5 . .
C8 C7 Al1 143(5) . .
C8 C7 Eu1 110(4) . .
Al1 C7 Eu1 71.3(13) . .
C8 C7 H7A 101.2 . .
Al1 C7 H7A 101.2 . .
Eu1 C7 H7A 136.4 . .
C8 C7 H7B 101.2 . .
Al1 C7 H7B 101.2 . .
Eu1 C7 H7B 40.6 . .
H7A C7 H7B 104.5 . .
C7 C8 H8A 109.5 . .
C7 C8 H8B 109.5 . .
H8A C8 H8B 109.5 . .
C7 C8 H8C 109.5 . .
H8A C8 H8C 109.5 . .
H8B C8 H8C 109.5 . .
C8A C7A Al1 134(2) . .
C8A C7A Eu1 126(2) . .
Al1 C7A Eu1 67.8(7) . .
C8A C7A H7A1 103.7 . .
Al1 C7A H7A1 103.7 . .
Eu1 C7A H7A1 36.2 . .
C8A C7A H7A2 103.7 . .
Al1 C7A H7A2 103.7 . .
Eu1 C7A H7A2 118.1 . .
H7A1 C7A H7A2 105.3 . .
C7A C8A H8D 109.5 . .
C7A C8A H8E 109.5 . .
H8D C8A H8E 109.5 . .
C7A C8A H8F 109.5 . .
H8D C8A H8F 109.5 . .
H8E C8A H8F 109.5 . .
C10 C9 Al2 114.4(17) . .
C10 C9 H9A 108.7 . .
Al2 C9 H9A 108.7 . .
C10 C9 H9B 108.7 . .
Al2 C9 H9B 108.7 . .
H9A C9 H9B 107.6 . .
C10A C9A Al2 113.0(16) . .
C10A C9A H9C 109.0 . .
Al2 C9A H9C 109.0 . .
C10A C9A H9D 109.0 . .
Al2 C9A H9D 109.0 . .
H9C C9A H9D 107.8 . .
C9A C10A H10D 109.5 . .
C9A C10A H10E 109.5 . .
H10D C10A H10E 109.5 . .
C9A C10A H10F 109.5 . .
H10D C10A H10F 109.5 . .
H10E C10A H10F 109.5 . .
C12 C11 Al2 109.5(9) . .
C12 C11 Eu2 165.5(10) . .
Al2 C11 Eu2 84.4(3) . .
C12 C11 H11A 109.8 . .
Al2 C11 H11A 109.8 . .
Eu2 C11 H11A 67.8 . .
C12 C11 H11B 109.8 . .
Al2 C11 H11B 109.8 . .
Eu2 C11 H11B 59.7 . .
H11A C11 H11B 108.2 . .
C11 C12 H12A 109.5 . .
C11 C12 H12B 109.5 . .
H12A C12 H12B 109.5 . .
C11 C12 H12C 109.5 . .
H12A C12 H12C 109.5 . .
H12B C12 H12C 109.5 . .
C14 C13 Al2 107.4(7) . .
C14 C13 Eu2 167.6(8) . .
Al2 C13 Eu2 84.9(4) . .
C14 C13 H13A 110.2 . .
Al2 C13 H13A 110.2 . .
Eu2 C13 H13A 65.6 . .
C14 C13 H13B 110.2 . .
Al2 C13 H13B 110.2 . .
Eu2 C13 H13B 62.4 . .
H13A C13 H13B 108.5 . .
C13 C14 H14A 109.5 . .
C13 C14 H14B 109.5 . .
H14A C14 H14B 109.5 . .
C13 C14 H14C 109.5 . .
H14A C14 H14C 109.5 . .
H14B C14 H14C 109.5 . .
C16 C15 Al2 114.7(6) . .
C16 C15 Eu1 87.0(5) . .
Al2 C15 Eu1 158.3(4) . .
C16 C15 H15A 108.6 . .
Al2 C15 H15A 108.6 . .
Eu1 C15 H15A 60.0 . .
C16 C15 H15B 108.6 . .
Al2 C15 H15B 108.6 . .
Eu1 C15 H15B 62.6 . .
H15A C15 H15B 107.6 . .
C15 C16 H16A 109.5 . .
C15 C16 H16B 109.5 . .
H16A C16 H16B 109.5 . .
C15 C16 H16C 109.5 . .
H16A C16 H16C 109.5 . .
H16B C16 H16C 109.5 . .
C18 C17 Al3 117.4(11) . .
C18 C17 H17A 108.0 . .
Al3 C17 H17A 108.0 . .
C18 C17 H17B 108.0 . .
Al3 C17 H17B 108.0 . .
H17A C17 H17B 107.2 . .
C17 C18 H18A 109.5 . .
C17 C18 H18B 109.5 . .
H18A C18 H18B 109.5 . .
C17 C18 H18C 109.5 . .
H18A C18 H18C 109.5 . .
H18B C18 H18C 109.5 . .
C20 C19 Al3 116.6(8) . .
C20 C19 Eu1 92.6(7) . 2_654
Al3 C19 Eu1 150.8(6) . 2_654
C20 C19 H19A 108.1 . .
Al3 C19 H19A 108.1 . .
Eu1 C19 H19A 57.3 2_654 .
C20 C19 H19B 108.1 . .
Al3 C19 H19B 108.1 . .
Eu1 C19 H19B 60.3 2_654 .
H19A C19 H19B 107.3 . .
C19 C20 H20A 109.5 . .
C19 C20 H20B 109.5 . .
H20A C20 H20B 109.5 . .
C19 C20 H20C 109.5 . .
H20A C20 H20C 109.5 . .
H20B C20 H20C 109.5 . .
C22 C21 Al3 105.6(11) . .
C22 C21 Eu2 168.9(13) . .
Al3 C21 Eu2 85.3(3) . .
C22 C21 H21A 110.6 . .
Al3 C21 H21A 110.6 . .
Eu2 C21 H21A 66.5 . .
C22 C21 H21B 110.6 . .
Al3 C21 H21B 110.6 . .
Eu2 C21 H21B 62.1 . .
H21A C21 H21B 108.8 . .
C21 C22 H22A 109.5 . .
C21 C22 H22B 109.5 . .
H22A C22 H22B 109.5 . .
C21 C22 H22C 109.5 . .
H22A C22 H22C 109.5 . .
H22B C22 H22C 109.5 . .
C24 C23 Al3 107.5(10) . .
C24 C23 Eu2 166.8(9) . .
Al3 C23 Eu2 85.2(4) . .
C24 C23 H23A 110.2 . .
Al3 C23 H23A 110.2 . .
Eu2 C23 H23A 66.9 . .
C24 C23 H23B 110.2 . .
Al3 C23 H23B 110.2 . .
Eu2 C23 H23B 60.8 . .
H23A C23 H23B 108.5 . .
C23 C24 H24A 109.5 . .
C23 C24 H24B 109.5 . .
H24A C24 H24B 109.5 . .
C23 C24 H24C 109.5 . .
H24A C24 H24C 109.5 . .
H24B C24 H24C 109.5 . .
C26 C25 Al4 107.8(8) . .
C26 C25 Eu2 166.9(9) . .
Al4 C25 Eu2 85.3(4) . .
C26 C25 H25A 110.2 . .
Al4 C25 H25A 110.2 . .
Eu2 C25 H25A 62.9 . .
C26 C25 H25B 110.2 . .
Al4 C25 H25B 110.2 . .
Eu2 C25 H25B 64.7 . .
H25A C25 H25B 108.5 . .
C25 C26 H26A 109.5 . .
C25 C26 H26B 109.5 . .
H26A C26 H26B 109.5 . .
C25 C26 H26C 109.5 . .
H26A C26 H26C 109.5 . .
H26B C26 H26C 109.5 . .
C28 C27 Al4 107.0(7) . .
C28 C27 Eu2 167.1(7) . .
Al4 C27 Eu2 85.8(3) . .
C28 C27 H27A 110.3 . .
Al4 C27 H27A 110.3 . .
Eu2 C27 H27A 62.5 . .
C28 C27 H27B 110.3 . .
Al4 C27 H27B 110.3 . .
Eu2 C27 H27B 65.0 . .
H27A C27 H27B 108.6 . .
C27 C28 H28A 109.5 . .
C27 C28 H28B 109.5 . .
H28A C28 H28B 109.5 . .
C27 C28 H28C 109.5 . .
H28A C28 H28C 109.5 . .
H28B C28 H28C 109.5 . .
C30 C29 Al4 115.3(8) . .
C30 C29 Eu1 82.6(7) . 2_754
Al4 C29 Eu1 161.1(5) . 2_754
C30 C29 H29A 108.5 . .
Al4 C29 H29A 108.5 . .
Eu1 C29 H29A 68.7 2_754 .
C30 C29 H29B 108.5 . .
Al4 C29 H29B 108.5 . .
Eu1 C29 H29B 57.3 2_754 .
H29A C29 H29B 107.5 . .
C29 C30 Eu1 69.2(7) . 2_754
C29 C30 H30A 109.5 . .
Eu1 C30 H30A 40.6 2_754 .
C29 C30 H30B 109.5 . .
Eu1 C30 H30B 129.2 2_754 .
H30A C30 H30B 109.5 . .
C29 C30 H30C 109.5 . .
Eu1 C30 H30C 118.8 2_754 .
H30A C30 H30C 109.5 . .
H30B C30 H30C 109.5 . .
C32 C31 Al4 111.6(11) . .
C32 C31 H31A 109.3 . .
Al4 C31 H31A 109.3 . .
C32 C31 H31B 109.3 . .
Al4 C31 H31B 109.3 . .
H31A C31 H31B 108.0 . .
C32A C31A Al4 122(3) . .
C32A C31A H31C 106.8 . .
Al4 C31A H31C 106.8 . .
C32A C31A H31D 106.8 . .
Al4 C31A H31D 106.8 . .
H31C C31A H31D 106.6 . .
C31A C32A H32D 109.5 . .
C31A C32A H32E 109.5 . .
H32D C32A H32E 109.5 . .
C31A C32A H32F 109.5 . .
H32D C32A H32F 109.5 . .
H32E C32A H32F 109.5 . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Eu1 C5 2.71(2) .
Eu1 C3 2.878(15) .
Eu1 C15 2.880(10) .
Eu1 C19 2.909(12) 3_665
Eu1 C29 2.918(10) 3_775
Eu1 C7 2.95(5) .
Eu1 Al1 2.959(4) .
Eu1 C7A 3.08(3) .
Eu1 C30 3.094(15) 3_775
Eu2 C13 2.749(10) .
Eu2 C27 2.756(10) .
Eu2 C11 2.761(10) .
Eu2 C23 2.776(12) .
Eu2 C21 2.786(9) .
Eu2 C25 2.787(10) .
Eu2 Al2 3.275(3) .
Eu2 Al4 3.301(3) .
Eu2 Al3 3.313(4) .
Al1 C5 1.79(3) .
Al1 C7 1.92(3) .
Al1 C7A 1.96(2) .
Al1 C1 2.03(3) .
Al1 C1A 2.04(2) .
Al1 C3 2.13(2) .
Al2 C9A 1.992(17) .
Al2 C9 2.001(18) .
Al2 C15 2.017(10) .
Al2 C13 2.038(10) .
Al2 C11 2.053(13) .
Al3 C17 1.975(15) .
Al3 C19 2.018(13) .
Al3 C21 2.036(14) .
Al3 C23 2.054(12) .
Al4 C31 1.969(14) .
Al4 C31A 1.97(2) .
Al4 C25 2.012(12) .
Al4 C29 2.021(10) .
Al4 C27 2.030(9) .
C1 C2 1.48(4) .
C1 H1A 0.9900 .
C1 H1B 0.9900 .
C2 H2A 0.9800 .
C2 H2B 0.9800 .
C2 H2C 0.9800 .
C1A C2A 1.48(4) .
C1A H1C 0.9900 .
C1A H1D 0.9900 .
C2A H2D 0.9800 .
C2A H2E 0.9800 .
C2A H2F 0.9800 .
C3 C4 1.39(3) .
C3 H3A 0.9900 .
C3 H3B 0.9900 .
C4 H4A 0.9800 .
C4 H4B 0.9800 .
C4 H4C 0.9800 .
C5 C6 1.52(4) .
C5 H5A 0.9900 .
C5 H5B 0.9900 .
C6 H6A 0.9800 .
C6 H6B 0.9800 .
C6 H6C 0.9800 .
C7 C8 1.41(4) .
C7 H7A 0.9900 .
C7 H7B 0.9900 .
C8 H8A 0.9800 .
C8 H8B 0.9800 .
C8 H8C 0.9800 .
C7A C8A 1.42(3) .
C7A H7A1 0.9900 .
C7A H7A2 0.9900 .
C8A H8D 0.9800 .
C8A H8E 0.9800 .
C8A H8F 0.9800 .
C9 C10 1.546(17) .
C9 H9A 0.9900 .
C9 H9B 0.9900 .
C10 H10A 0.9800 .
C10 H10B 0.9800 .
C10 H10C 0.9800 .
C9A C10A 1.523(19) .
C9A H9C 0.9900 .
C9A H9D 0.9900 .
C10A H10D 0.9800 .
C10A H10E 0.9800 .
C10A H10F 0.9800 .
C11 C12 1.532(14) .
C11 H11A 0.9900 .
C11 H11B 0.9900 .
C12 H12A 0.9800 .
C12 H12B 0.9800 .
C12 H12C 0.9800 .
C13 C14 1.570(16) .
C13 H13A 0.9900 .
C13 H13B 0.9900 .
C14 H14A 0.9800 .
C14 H14B 0.9800 .
C14 H14C 0.9800 .
C15 C16 1.532(13) .
C15 H15A 0.9900 .
C15 H15B 0.9900 .
C16 H16A 0.9800 .
C16 H16B 0.9800 .
C16 H16C 0.9800 .
C17 C18 1.57(2) .
C17 H17A 0.9900 .
C17 H17B 0.9900 .
C18 H18A 0.9800 .
C18 H18B 0.9800 .
C18 H18C 0.9800 .
C19 C20 1.511(18) .
C19 Eu1 2.909(12) 2_654
C19 H19A 0.9900 .
C19 H19B 0.9900 .
C20 H20A 0.9800 .
C20 H20B 0.9800 .
C20 H20C 0.9800 .
C21 C22 1.526(14) .
C21 H21A 0.9900 .
C21 H21B 0.9900 .
C22 H22A 0.9800 .
C22 H22B 0.9800 .
C22 H22C 0.9800 .
C23 C24 1.555(18) .
C23 H23A 0.9900 .
C23 H23B 0.9900 .
C24 H24A 0.9800 .
C24 H24B 0.9800 .
C24 H24C 0.9800 .
C25 C26 1.540(14) .
C25 H25A 0.9900 .
C25 H25B 0.9900 .
C26 H26A 0.9800 .
C26 H26B 0.9800 .
C26 H26C 0.9800 .
C27 C28 1.555(14) .
C27 H27A 0.9900 .
C27 H27B 0.9900 .
C28 H28A 0.9800 .
C28 H28B 0.9800 .
C28 H28C 0.9800 .
C29 C30 1.47(2) .
C29 Eu1 2.918(10) 2_754
C29 H29A 0.9900 .
C29 H29B 0.9900 .
C30 Eu1 3.094(15) 2_754
C30 H30A 0.9800 .
C30 H30B 0.9800 .
C30 H30C 0.9800 .
C31 C32 1.524(16) .
C31 H31A 0.9900 .
C31 H31B 0.9900 .
C32 H32A 0.9800 .
C32 H32B 0.9800 .
C32 H32C 0.9800 .
C31A C32A 1.54(2) .
C31A H31C 0.9900 .
C31A H31D 0.9900 .
C32A H32D 0.9800 .
C32A H32E 0.9800 .
C32A H32F 0.9800 .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C3 Eu1 Al1 C5 -129.1(19) . .
C15 Eu1 Al1 C5 62.7(18) . .
C19 Eu1 Al1 C5 -69.4(18) 3_665 .
C29 Eu1 Al1 C5 -179.2(18) 3_775 .
C7 Eu1 Al1 C5 154(2) . .
C7A Eu1 Al1 C5 112(2) . .
C30 Eu1 Al1 C5 151.4(18) 3_775 .
C5 Eu1 Al1 C7 -154(2) . .
C3 Eu1 Al1 C7 76.8(17) . .
C15 Eu1 Al1 C7 -91.5(16) . .
C19 Eu1 Al1 C7 136.5(16) 3_665 .
C29 Eu1 Al1 C7 26.6(16) 3_775 .
C7A Eu1 Al1 C7 -41.9(18) . .
C30 Eu1 Al1 C7 -2.8(16) 3_775 .
C5 Eu1 Al1 C7A -112(2) . .
C3 Eu1 Al1 C7A 118.7(14) . .
C15 Eu1 Al1 C7A -49.5(12) . .
C19 Eu1 Al1 C7A 178.4(12) 3_665 .
C29 Eu1 Al1 C7A 68.6(12) 3_775 .
C7 Eu1 Al1 C7A 41.9(18) . .
C30 Eu1 Al1 C7A 39.2(12) 3_775 .
C5 Eu1 Al1 C1 -131(10) . .
C3 Eu1 Al1 C1 100(10) . .
C15 Eu1 Al1 C1 -68(10) . .
C19 Eu1 Al1 C1 160(10) 3_665 .
C29 Eu1 Al1 C1 50(10) 3_775 .
C7 Eu1 Al1 C1 23(10) . .
C7A Eu1 Al1 C1 -19(10) . .
C30 Eu1 Al1 C1 20(10) 3_775 .
C5 Eu1 Al1 C1A 88(6) . .
C3 Eu1 Al1 C1A -41(6) . .
C15 Eu1 Al1 C1A 151(6) . .
C19 Eu1 Al1 C1A 19(6) 3_665 .
C29 Eu1 Al1 C1A -91(6) 3_775 .
C7 Eu1 Al1 C1A -117(6) . .
C7A Eu1 Al1 C1A -159(6) . .
C30 Eu1 Al1 C1A -120(6) 3_775 .
C5 Eu1 Al1 C3 129.1(19) . .
C15 Eu1 Al1 C3 -168.3(7) . .
C19 Eu1 Al1 C3 59.7(8) 3_665 .
C29 Eu1 Al1 C3 -50.1(8) 3_775 .
C7 Eu1 Al1 C3 -76.8(17) . .
C7A Eu1 Al1 C3 -118.7(14) . .
C30 Eu1 Al1 C3 -79.5(8) 3_775 .
C13 Eu2 Al2 C9A 99.6(13) . .
C27 Eu2 Al2 C9A 79.0(13) . .
C11 Eu2 Al2 C9A -91.9(13) . .
C23 Eu2 Al2 C9A -94.9(13) . .
C21 Eu2 Al2 C9A -175.1(13) . .
C25 Eu2 Al2 C9A 4.6(13) . .
Al4 Eu2 Al2 C9A 35.6(13) . .
Al3 Eu2 Al2 C9A -145.7(13) . .
C13 Eu2 Al2 C9 84.5(10) . .
C27 Eu2 Al2 C9 64.0(10) . .
C11 Eu2 Al2 C9 -107.0(10) . .
C23 Eu2 Al2 C9 -109.9(10) . .
C21 Eu2 Al2 C9 169.9(10) . .
C25 Eu2 Al2 C9 -10.4(10) . .
Al4 Eu2 Al2 C9 20.6(9) . .
Al3 Eu2 Al2 C9 -160.7(9) . .
C13 Eu2 Al2 C15 -85.2(6) . .
C27 Eu2 Al2 C15 -105.8(5) . .
C11 Eu2 Al2 C15 83.3(6) . .
C23 Eu2 Al2 C15 80.3(6) . .
C21 Eu2 Al2 C15 0.1(5) . .
C25 Eu2 Al2 C15 179.8(5) . .
Al4 Eu2 Al2 C15 -149.2(5) . .
Al3 Eu2 Al2 C15 29.5(5) . .
C27 Eu2 Al2 C13 -20.5(4) . .
C11 Eu2 Al2 C13 168.5(5) . .
C23 Eu2 Al2 C13 165.5(5) . .
C21 Eu2 Al2 C13 85.4(4) . .
C25 Eu2 Al2 C13 -95.0(4) . .
Al4 Eu2 Al2 C13 -64.0(3) . .
Al3 Eu2 Al2 C13 114.8(3) . .
C13 Eu2 Al2 C11 -168.5(5) . .
C27 Eu2 Al2 C11 170.9(4) . .
C23 Eu2 Al2 C11 -3.0(5) . .
C21 Eu2 Al2 C11 -83.1(4) . .
C25 Eu2 Al2 C11 96.5(5) . .
Al4 Eu2 Al2 C11 127.5(4) . .
Al3 Eu2 Al2 C11 -53.7(4) . .
C13 Eu2 Al3 C17 -99.6(10) . .
C27 Eu2 Al3 C17 -2.0(9) . .
C11 Eu2 Al3 C17 179.1(9) . .
C23 Eu2 Al3 C17 91.5(10) . .
C21 Eu2 Al3 C17 -98.2(11) . .
C25 Eu2 Al3 C17 69.7(10) . .
Al2 Eu2 Al3 C17 -150.2(9) . .
Al4 Eu2 Al3 C17 28.6(9) . .
C13 Eu2 Al3 C19 85.5(5) . .
C27 Eu2 Al3 C19 -176.9(5) . .
C11 Eu2 Al3 C19 4.2(5) . .
C23 Eu2 Al3 C19 -83.3(6) . .
C21 Eu2 Al3 C19 87.0(7) . .
C25 Eu2 Al3 C19 -105.2(5) . .
Al2 Eu2 Al3 C19 35.0(5) . .
Al4 Eu2 Al3 C19 -146.3(4) . .
C13 Eu2 Al3 C21 -1.4(6) . .
C27 Eu2 Al3 C21 96.1(6) . .
C11 Eu2 Al3 C21 -82.8(6) . .
C23 Eu2 Al3 C21 -170.3(7) . .
C25 Eu2 Al3 C21 167.9(6) . .
Al2 Eu2 Al3 C21 -52.0(6) . .
Al4 Eu2 Al3 C21 126.8(5) . .
C13 Eu2 Al3 C23 168.9(5) . .
C27 Eu2 Al3 C23 -93.5(5) . .
C11 Eu2 Al3 C23 87.5(5) . .
C21 Eu2 Al3 C23 170.3(7) . .
C25 Eu2 Al3 C23 -21.8(6) . .
Al2 Eu2 Al3 C23 118.3(5) . .
Al4 Eu2 Al3 C23 -62.9(5) . .
C13 Eu2 Al4 C31 -4.4(8) . .
C27 Eu2 Al4 C31 -93.0(8) . .
C11 Eu2 Al4 C31 73.5(8) . .
C23 Eu2 Al4 C31 177.4(8) . .
C21 Eu2 Al4 C31 -108.2(8) . .
C25 Eu2 Al4 C31 87.4(9) . .
Al2 Eu2 Al4 C31 29.7(7) . .
Al3 Eu2 Al4 C31 -149.2(7) . .
C13 Eu2 Al4 C31A 11(3) . .
C27 Eu2 Al4 C31A -78(3) . .
C11 Eu2 Al4 C31A 89(3) . .
C23 Eu2 Al4 C31A -167(3) . .
C21 Eu2 Al4 C31A -93(3) . .
C25 Eu2 Al4 C31A 103(3) . .
Al2 Eu2 Al4 C31A 45(3) . .
Al3 Eu2 Al4 C31A -134(3) . .
C13 Eu2 Al4 C25 -91.9(5) . .
C27 Eu2 Al4 C25 179.5(6) . .
C11 Eu2 Al4 C25 -13.9(6) . .
C23 Eu2 Al4 C25 89.9(5) . .
C21 Eu2 Al4 C25 164.4(6) . .
Al2 Eu2 Al4 C25 -57.7(5) . .
Al3 Eu2 Al4 C25 123.4(5) . .
C13 Eu2 Al4 C29 178.5(4) . .
C27 Eu2 Al4 C29 89.9(6) . .
C11 Eu2 Al4 C29 -103.5(5) . .
C23 Eu2 Al4 C29 0.3(5) . .
C21 Eu2 Al4 C29 74.7(5) . .
C25 Eu2 Al4 C29 -89.6(6) . .
Al2 Eu2 Al4 C29 -147.4(4) . .
Al3 Eu2 Al4 C29 33.8(4) . .
C13 Eu2 Al4 C27 88.6(5) . .
C11 Eu2 Al4 C27 166.6(5) . .
C23 Eu2 Al4 C27 -89.6(5) . .
C21 Eu2 Al4 C27 -15.2(5) . .
C25 Eu2 Al4 C27 -179.5(6) . .
Al2 Eu2 Al4 C27 122.7(4) . .
Al3 Eu2 Al4 C27 -56.1(4) . .
C5 Al1 C1 C2 -127(9) . .
C7 Al1 C1 C2 13(10) . .
C7A Al1 C1 C2 -27(9) . .
C1A Al1 C1 C2 159(16) . .
C3 Al1 C1 C2 80(10) . .
Eu1 Al1 C1 C2 -9(18) . .
C5 Al1 C1A C2A -142(3) . .
C7 Al1 C1A C2A 20(3) . .
C7A Al1 C1A C2A -24(3) . .
C1 Al1 C1A C2A -17(8) . .
C3 Al1 C1A C2A 96(2) . .
Eu1 Al1 C1A C2A 134(5) . .
C5 Al1 C3 C4 -59(2) . .
C7 Al1 C3 C4 176(2) . .
C7A Al1 C3 C4 -170.1(15) . .
C1 Al1 C3 C4 99(4) . .
C1A Al1 C3 C4 66.2(17) . .
Eu1 Al1 C3 C4 -107.0(14) . .
C5 Al1 C3 Eu1 48.3(15) . .
C7 Al1 C3 Eu1 -76.7(17) . .
C7A Al1 C3 Eu1 -63.1(9) . .
C1 Al1 C3 Eu1 -154(4) . .
C1A Al1 C3 Eu1 173.2(9) . .
C5 Eu1 C3 C4 77(2) . .
C15 Eu1 C3 C4 149(2) . .
C19 Eu1 C3 C4 -24.3(19) 3_665 .
C29 Eu1 C3 C4 -117.2(19) 3_775 .
C7 Eu1 C3 C4 161(2) . .
Al1 Eu1 C3 C4 106.5(19) . .
C7A Eu1 C3 C4 142(2) . .
C30 Eu1 C3 C4 -143.3(19) 3_775 .
C5 Eu1 C3 Al1 -29.3(13) . .
C15 Eu1 C3 Al1 42.9(19) . .
C19 Eu1 C3 Al1 -130.8(6) 3_665 .
C29 Eu1 C3 Al1 136.3(6) 3_775 .
C7 Eu1 C3 Al1 54.2(10) . .
C7A Eu1 C3 Al1 35.5(8) . .
C30 Eu1 C3 Al1 110.2(6) 3_775 .
C7 Al1 C5 C6 -71(3) . .
C7A Al1 C5 C6 -37(2) . .
C1 Al1 C5 C6 54(6) . .
C1A Al1 C5 C6 88(3) . .
C3 Al1 C5 C6 -152.3(19) . .
Eu1 Al1 C5 C6 -103(3) . .
C7 Al1 C5 Eu1 32(2) . .
C7A Al1 C5 Eu1 65.9(13) . .
C1 Al1 C5 Eu1 157(5) . .
C1A Al1 C5 Eu1 -168.9(8) . .
C3 Al1 C5 Eu1 -49.5(14) . .
C3 Eu1 C5 C6 145(3) . .
C15 Eu1 C5 C6 -21(3) . .
C19 Eu1 C5 C6 -126(2) 3_665 .
C29 Eu1 C5 C6 112.4(19) 3_775 .
C7 Eu1 C5 C6 95(3) . .
Al1 Eu1 C5 C6 111(3) . .
C7A Eu1 C5 C6 70(3) . .
C30 Eu1 C5 C6 67(2) 3_775 .
C3 Eu1 C5 Al1 34.0(12) . .
C15 Eu1 C5 Al1 -132.2(12) . .
C19 Eu1 C5 Al1 123.2(14) 3_665 .
C29 Eu1 C5 Al1 2(3) 3_775 .
C7 Eu1 C5 Al1 -16.4(15) . .
C7A Eu1 C5 Al1 -40.8(13) . .
C30 Eu1 C5 Al1 -43(2) 3_775 .
C5 Al1 C7 C8 68(7) . .
C7A Al1 C7 C8 10(5) . .
C1 Al1 C7 C8 -73(8) . .
C1A Al1 C7 C8 -91(7) . .
C3 Al1 C7 C8 169(7) . .
Eu1 Al1 C7 C8 98(7) . .
C5 Al1 C7 Eu1 -30(2) . .
C7A Al1 C7 Eu1 -89(2) . .
C1 Al1 C7 Eu1 -171(4) . .
C1A Al1 C7 Eu1 170.3(9) . .
C3 Al1 C7 Eu1 71.1(7) . .
C5 Eu1 C7 C8 -125(5) . .
C3 Eu1 C7 C8 156(5) . .
C15 Eu1 C7 C8 -27(5) . .
C19 Eu1 C7 C8 148(5) 3_665 .
C29 Eu1 C7 C8 63(5) 3_775 .
Al1 Eu1 C7 C8 -141(5) . .
C7A Eu1 C7 C8 -68(5) . .
C30 Eu1 C7 C8 36(5) 3_775 .
C5 Eu1 C7 Al1 15.8(13) . .
C3 Eu1 C7 Al1 -63.5(10) . .
C15 Eu1 C7 Al1 113.4(11) . .
C19 Eu1 C7 Al1 -71.3(18) 3_665 .
C29 Eu1 C7 Al1 -156.0(14) 3_775 .
C7A Eu1 C7 Al1 72.7(13) . .
C30 Eu1 C7 Al1 177.2(16) 3_775 .
C5 Al1 C7A C8A -178(3) . .
C7 Al1 C7A C8A -41(4) . .
C1 Al1 C7A C8A 53(5) . .
C1A Al1 C7A C8A 56(4) . .
C3 Al1 C7A C8A -62(3) . .
Eu1 Al1 C7A C8A -120(3) . .
C5 Al1 C7A Eu1 -58.6(8) . .
C7 Al1 C7A Eu1 78(3) . .
C1 Al1 C7A Eu1 173(4) . .
C1A Al1 C7A Eu1 176.1(11) . .
C3 Al1 C7A Eu1 58.1(7) . .
C5 Eu1 C7A C8A 169(3) . .
C3 Eu1 C7A C8A 89(3) . .
C15 Eu1 C7A C8A -89(3) . .
C19 Eu1 C7A C8A 126(2) 3_665 .
C29 Eu1 C7A C8A 7(3) 3_775 .
C7 Eu1 C7A C8A 56(3) . .
Al1 Eu1 C7A C8A 129(3) . .
C30 Eu1 C7A C8A -13(3) 3_775 .
C5 Eu1 C7A Al1 39.4(10) . .
C3 Eu1 C7A Al1 -40.1(8) . .
C15 Eu1 C7A Al1 141.7(9) . .
C19 Eu1 C7A Al1 -3(3) 3_665 .
C29 Eu1 C7A Al1 -122.3(9) 3_775 .
C7 Eu1 C7A Al1 -73.6(14) . .
C30 Eu1 C7A Al1 -142.4(11) 3_775 .
C9A Al2 C9 C10 4(5) . .
C15 Al2 C9 C10 -62(3) . .
C13 Al2 C9 C10 -175(2) . .
C11 Al2 C9 C10 62(3) . .
Eu2 Al2 C9 C10 127(2) . .
C9 Al2 C9A C10A 39(6) . .
C15 Al2 C9A C10A 159(2) . .
C13 Al2 C9A C10A 41(3) . .
C11 Al2 C9A C10A -88(2) . .
Eu2 Al2 C9A C10A -25(3) . .
C9A Al2 C11 C12 -64.7(12) . .
C9 Al2 C11 C12 -78.0(12) . .
C15 Al2 C11 C12 49.4(9) . .
C13 Al2 C11 C12 165.1(8) . .
Eu2 Al2 C11 C12 175.5(9) . .
C9A Al2 C11 Eu2 119.8(8) . .
C9 Al2 C11 Eu2 106.5(9) . .
C15 Al2 C11 Eu2 -126.1(3) . .
C13 Al2 C11 Eu2 -10.4(4) . .
C13 Eu2 C11 C12 -156(3) . .
C27 Eu2 C11 C12 162(3) . .
C23 Eu2 C11 C12 15(3) . .
C21 Eu2 C11 C12 -61(3) . .
C25 Eu2 C11 C12 109(3) . .
Al2 Eu2 C11 C12 -163(3) . .
Al4 Eu2 C11 C12 118(3) . .
Al3 Eu2 C11 C12 -23(3) . .
C13 Eu2 C11 Al2 7.3(3) . .
C27 Eu2 C11 Al2 -35.2(16) . .
C23 Eu2 C11 Al2 177.9(3) . .
C21 Eu2 C11 Al2 101.9(4) . .
C25 Eu2 C11 Al2 -87.8(4) . .
Al4 Eu2 C11 Al2 -79.4(4) . .
Al3 Eu2 C11 Al2 139.4(3) . .
C9A Al2 C13 C14 61.5(13) . .
C9 Al2 C13 C14 61.9(14) . .
C15 Al2 C13 C14 -56.5(9) . .
C11 Al2 C13 C14 -171.3(8) . .
Eu2 Al2 C13 C14 178.2(9) . .
C9A Al2 C13 Eu2 -116.7(10) . .
C9 Al2 C13 Eu2 -116.4(11) . .
C15 Al2 C13 Eu2 125.3(4) . .
C11 Al2 C13 Eu2 10.5(4) . .
C27 Eu2 C13 C14 -7(4) . .
C11 Eu2 C13 C14 -179(4) . .
C23 Eu2 C13 C14 126(4) . .
C21 Eu2 C13 C14 88(4) . .
C25 Eu2 C13 C14 -83(4) . .
Al2 Eu2 C13 C14 -172(4) . .
Al4 Eu2 C13 C14 -45(4) . .
Al3 Eu2 C13 C14 89(4) . .
C27 Eu2 C13 Al2 164.7(3) . .
C11 Eu2 C13 Al2 -7.3(3) . .
C23 Eu2 C13 Al2 -62(2) . .
C21 Eu2 C13 Al2 -100.2(4) . .
C25 Eu2 C13 Al2 89.0(4) . .
Al4 Eu2 C13 Al2 126.7(2) . .
Al3 Eu2 C13 Al2 -99.3(3) . .
C9A Al2 C15 C16 170.3(13) . .
C9 Al2 C15 C16 -175.7(11) . .
C13 Al2 C15 C16 -66.0(9) . .
C11 Al2 C15 C16 54.1(9) . .
Eu2 Al2 C15 C16 -5.6(11) . .
C9A Al2 C15 Eu1 -13(2) . .
C9 Al2 C15 Eu1 0.6(19) . .
C13 Al2 C15 Eu1 110.3(15) . .
C11 Al2 C15 Eu1 -129.6(15) . .
Eu2 Al2 C15 Eu1 170.7(12) . .
C5 Eu1 C15 C16 -59.9(13) . .
C3 Eu1 C15 C16 -128.0(15) . .
C19 Eu1 C15 C16 45.6(7) 3_665 .
C29 Eu1 C15 C16 139.6(6) 3_775 .
C7 Eu1 C15 C16 -137.5(9) . .
Al1 Eu1 C15 C16 -93.0(6) . .
C7A Eu1 C15 C16 -121.1(9) . .
C30 Eu1 C15 C16 162.5(7) 3_775 .
C5 Eu1 C15 Al2 123.5(19) . .
C3 Eu1 C15 Al2 55(3) . .
C19 Eu1 C15 Al2 -131.1(15) 3_665 .
C29 Eu1 C15 Al2 -37.0(16) 3_775 .
C7 Eu1 C15 Al2 45.9(18) . .
Al1 Eu1 C15 Al2 90.4(16) . .
C7A Eu1 C15 Al2 62.3(17) . .
C30 Eu1 C15 Al2 -14.1(15) 3_775 .
C19 Al3 C17 C18 -174.0(16) . .
C21 Al3 C17 C18 -55(2) . .
C23 Al3 C17 C18 73.2(19) . .
Eu2 Al3 C17 C18 11(2) . .
C17 Al3 C19 C20 -169.4(12) . .
C21 Al3 C19 C20 66.3(10) . .
C23 Al3 C19 C20 -52.0(11) . .
Eu2 Al3 C19 C20 6.2(11) . .
C17 Al3 C19 Eu1 7.4(15) . 2_654
C21 Al3 C19 Eu1 -117.0(11) . 2_654
C23 Al3 C19 Eu1 124.7(11) . 2_654
Eu2 Al3 C19 Eu1 -177.1(9) . 2_654
C17 Al3 C21 C22 -64.4(16) . .
C19 Al3 C21 C22 57.7(15) . .
C23 Al3 C21 C22 168.8(14) . .
Eu2 Al3 C21 C22 177.6(16) . .
C17 Al3 C21 Eu2 118.1(6) . .
C19 Al3 C21 Eu2 -119.9(4) . .
C23 Al3 C21 Eu2 -8.8(6) . .
C13 Eu2 C21 C22 11(7) . .
C27 Eu2 C21 C22 106(7) . .
C11 Eu2 C21 C22 -66(7) . .
C23 Eu2 C21 C22 -162(7) . .
C25 Eu2 C21 C22 154(7) . .
Al2 Eu2 C21 C22 -27(7) . .
Al4 Eu2 C21 C22 116(7) . .
Al3 Eu2 C21 C22 -168(7) . .
C13 Eu2 C21 Al3 178.9(5) . .
C27 Eu2 C21 Al3 -85.8(5) . .
C11 Eu2 C21 Al3 102.2(5) . .
C23 Eu2 C21 Al3 6.2(5) . .
C25 Eu2 C21 Al3 -38.1(17) . .
Al2 Eu2 C21 Al3 140.6(4) . .
Al4 Eu2 C21 Al3 -76.6(5) . .
C17 Al3 C23 C24 56.1(12) . .
C19 Al3 C23 C24 -62.0(11) . .
C21 Al3 C23 C24 -174.6(10) . .
Eu2 Al3 C23 C24 176.6(11) . .
C17 Al3 C23 Eu2 -120.5(6) . .
C19 Al3 C23 Eu2 121.4(5) . .
C21 Al3 C23 Eu2 8.8(6) . .
C13 Eu2 C23 C24 149(4) . .
C27 Eu2 C23 C24 -78(5) . .
C11 Eu2 C23 C24 96(5) . .
C21 Eu2 C23 C24 -172(5) . .
C25 Eu2 C23 C24 -2(5) . .
Al2 Eu2 C23 C24 98(5) . .
Al4 Eu2 C23 C24 -40(5) . .
Al3 Eu2 C23 C24 -165(5) . .
C13 Eu2 C23 Al3 -45(2) . .
C27 Eu2 C23 Al3 87.9(4) . .
C11 Eu2 C23 Al3 -98.5(4) . .
C21 Eu2 C23 Al3 -6.1(5) . .
C25 Eu2 C23 Al3 163.3(4) . .
Al2 Eu2 C23 Al3 -96.6(5) . .
Al4 Eu2 C23 Al3 125.8(4) . .
C31 Al4 C25 C26 57.0(12) . .
C31A Al4 C25 C26 65(2) . .
C29 Al4 C25 C26 -61.9(11) . .
C27 Al4 C25 C26 -178.6(10) . .
Eu2 Al4 C25 C26 -179.0(12) . .
C31 Al4 C25 Eu2 -124.0(6) . .
C31A Al4 C25 Eu2 -116(2) . .
C29 Al4 C25 Eu2 117.1(4) . .
C27 Al4 C25 Eu2 0.4(6) . .
C13 Eu2 C25 C26 -91(5) . .
C27 Eu2 C25 C26 176(5) . .
C11 Eu2 C25 C26 -14(5) . .
C23 Eu2 C25 C26 83(5) . .
C21 Eu2 C25 C26 126(4) . .
Al2 Eu2 C25 C26 -53(5) . .
Al4 Eu2 C25 C26 176(5) . .
Al3 Eu2 C25 C26 96(5) . .
C13 Eu2 C25 Al4 92.8(4) . .
C27 Eu2 C25 Al4 -0.3(4) . .
C11 Eu2 C25 Al4 170.0(4) . .
C23 Eu2 C25 Al4 -92.6(5) . .
C21 Eu2 C25 Al4 -50.0(16) . .
Al2 Eu2 C25 Al4 131.3(4) . .
Al3 Eu2 C25 Al4 -79.3(5) . .
C31 Al4 C27 C28 -57.1(11) . .
C31A Al4 C27 C28 -53(2) . .
C25 Al4 C27 C28 -179.1(9) . .
C29 Al4 C27 C28 64.6(10) . .
Eu2 Al4 C27 C28 -178.6(11) . .
C31 Al4 C27 Eu2 121.5(7) . .
C31A Al4 C27 Eu2 125.9(17) . .
C25 Al4 C27 Eu2 -0.4(6) . .
C29 Al4 C27 Eu2 -116.8(4) . .
C13 Eu2 C27 C28 79(4) . .
C11 Eu2 C27 C28 120(4) . .
C23 Eu2 C27 C28 -93(4) . .
C21 Eu2 C27 C28 -17(4) . .
C25 Eu2 C27 C28 174(4) . .
Al2 Eu2 C27 C28 91(4) . .
Al4 Eu2 C27 C28 174(5) . .
Al3 Eu2 C27 C28 -55(4) . .
C13 Eu2 C27 Al4 -95.5(4) . .
C11 Eu2 C27 Al4 -54.2(16) . .
C23 Eu2 C27 Al4 92.9(4) . .
C21 Eu2 C27 Al4 168.7(4) . .
C25 Eu2 C27 Al4 0.3(4) . .
Al2 Eu2 C27 Al4 -82.9(4) . .
Al3 Eu2 C27 Al4 131.0(4) . .
C31 Al4 C29 C30 -162.6(12) . .
C31A Al4 C29 C30 -176(3) . .
C25 Al4 C29 C30 -46.1(12) . .
C27 Al4 C29 C30 75.3(12) . .
Eu2 Al4 C29 C30 14.9(12) . .
C31 Al4 C29 Eu1 37.3(17) . 2_754
C31A Al4 C29 Eu1 24(3) . 2_754
C25 Al4 C29 Eu1 153.7(14) . 2_754
C27 Al4 C29 Eu1 -84.8(15) . 2_754
Eu2 Al4 C29 Eu1 -145.2(13) . 2_754
Al4 C29 C30 Eu1 -173.6(7) . 2_754
C31A Al4 C31 C32 -77(9) . .
C25 Al4 C31 C32 69.1(14) . .
C29 Al4 C31 C32 -175.4(12) . .
C27 Al4 C31 C32 -56.4(15) . .
Eu2 Al4 C31 C32 7.3(17) . .
C31 Al4 C31A C32A -100(12) . .
C25 Al4 C31A C32A -137(5) . .
C29 Al4 C31A C32A -14(6) . .
C27 Al4 C31A C32A 99(5) . .
Eu2 Al4 C31A C32A 155(4) . .
