#------------------------------------------------------------------------------
#$Date: 2016-03-21 18:53:46 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178828 $
#$URL: svn://www.crystallography.net/cod/cif/4/10/82/4108240.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4108240
loop_
_publ_author_name
'Limin Wang'
'Zhongjia Tang'
'Bernd Lorenz'
'Arnold M. Guloy'
_publ_section_title
;
 Remarkable Rare-Earth Metal Silicide Oxides with Planar Si6 Rings
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              11258
_journal_page_last               11259
_journal_paper_doi               10.1021/ja803632x
_journal_volume                  130
_journal_year                    2008
_chemical_formula_sum            'La10 O3 Si8'
_chemical_formula_weight         1661.82
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           191
_symmetry_cell_setting           hexagonal
_symmetry_space_group_name_Hall  '-P 6 2'
_symmetry_space_group_name_H-M   'P 6/m m m'
_atom_sites_solution_hydrogens   none
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 90.00
_cell_angle_gamma                120.00
_cell_formula_units_Z            1
_cell_length_a                   10.975(3)
_cell_length_b                   10.975(3)
_cell_length_c                   4.6804(13)
_cell_measurement_reflns_used    1417
_cell_measurement_temperature    298(2)
_cell_measurement_theta_max      27.73
_cell_measurement_theta_min      3.71
_cell_volume                     488.2(2)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'Bruker SHELXTL'
_computing_structure_solution    'Bruker SHELXTL'
_diffrn_ambient_temperature      298(2)
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0386
_diffrn_reflns_av_sigmaI/netI    0.0188
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       6
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       6
_diffrn_reflns_limit_l_min       -5
_diffrn_reflns_number            3005
_diffrn_reflns_theta_full        27.75
_diffrn_reflns_theta_max         27.75
_diffrn_reflns_theta_min         2.14
_exptl_absorpt_coefficient_mu    21.828
_exptl_absorpt_correction_T_max  0.9685
_exptl_absorpt_correction_T_min  0.7463
_exptl_absorpt_correction_type   empirical
_exptl_crystal_colour            black
_exptl_crystal_density_diffrn    5.652
_exptl_crystal_description       block
_exptl_crystal_F_000             706
_exptl_crystal_size_max          0.12
_exptl_crystal_size_mid          0.06
_exptl_crystal_size_min          0.04
_refine_diff_density_max         1.003
_refine_diff_density_min         -0.623
_refine_diff_density_rms         0.145
_refine_ls_extinction_coef       0.00257(16)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.996
_refine_ls_hydrogen_treatment    none
_refine_ls_matrix_type           full
_refine_ls_number_parameters     20
_refine_ls_number_reflns         269
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.996
_refine_ls_R_factor_all          0.0144
_refine_ls_R_factor_gt           0.0125
_refine_ls_shift/su_max          0.000
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0130P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0263
_refine_ls_wR_factor_ref         0.0267
_reflns_number_gt                247
_reflns_number_total             269
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ja803632x-file003_1.cif
_cod_data_source_block           La10Si8O3
_cod_original_cell_volume        488.3(2)
_cod_database_code               4108240
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-y, x-y, z'
'-x+y, -x, z'
'-x, -y, z'
'y, -x+y, z'
'x-y, x, z'
'y, x, -z'
'x-y, -y, -z'
'-x, -x+y, -z'
'-y, -x, -z'
'-x+y, y, -z'
'x, x-y, -z'
'-x, -y, -z'
'y, -x+y, -z'
'x-y, x, -z'
'x, y, -z'
'-y, x-y, -z'
'-x+y, -x, -z'
'-y, -x, z'
'-x+y, y, z'
'x, x-y, z'
'y, x, z'
'x-y, -y, z'
'-x, -x+y, z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
La1 La 0.0000 0.0000 0.0000 0.00861(17) Uani 1 24 d S
La2 La 0.42064(4) 0.210319(18) 0.0000 0.01335(12) Uani 1 4 d S
La3 La 0.5000 0.0000 -0.5000 0.01227(14) Uani 1 8 d S
Si4 Si 0.0000 0.21679(14) -0.5000 0.0102(3) Uani 1 4 d S
Si5 Si 0.6667 0.3333 -0.5000 0.0122(6) Uani 1 12 d S
O1 O 0.5000 0.0000 -1.0000 0.057(3) Uani 1 8 d S
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
La La -0.2871 2.4523 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
Si4 La1 Si4 180.00(5) 14 2
Si4 La1 Si4 41.767(16) 14 3_556
Si4 La1 Si4 138.233(16) 2 3_556
Si4 La1 Si4 41.767(16) 14 1_556
Si4 La1 Si4 138.233(16) 2 1_556
Si4 La1 Si4 76.26(3) 3_556 1_556
Si4 La1 Si4 138.233(16) 14 15_554
Si4 La1 Si4 41.767(16) 2 15_554
Si4 La1 Si4 180.00(4) 3_556 15_554
Si4 La1 Si4 103.74(3) 1_556 15_554
Si4 La1 Si4 138.233(16) 14 13_554
Si4 La1 Si4 41.767(16) 2 13_554
Si4 La1 Si4 103.74(3) 3_556 13_554
Si4 La1 Si4 180.00(4) 1_556 13_554
Si4 La1 Si4 76.26(3) 15_554 13_554
Si4 La1 Si4 103.74(3) 14 3
Si4 La1 Si4 76.26(3) 2 3
Si4 La1 Si4 89.05(4) 3_556 3
Si4 La1 Si4 138.233(16) 1_556 3
Si4 La1 Si4 90.95(4) 15_554 3
Si4 La1 Si4 41.767(16) 13_554 3
Si4 La1 Si4 89.05(4) 14 14_554
Si4 La1 Si4 90.95(4) 2 14_554
Si4 La1 Si4 103.74(3) 3_556 14_554
Si4 La1 Si4 103.74(3) 1_556 14_554
Si4 La1 Si4 76.26(3) 15_554 14_554
Si4 La1 Si4 76.26(3) 13_554 14_554
Si4 La1 Si4 41.767(16) 3 14_554
Si4 La1 Si4 103.74(3) 14 .
Si4 La1 Si4 76.26(3) 2 .
Si4 La1 Si4 138.233(16) 3_556 .
Si4 La1 Si4 89.05(4) 1_556 .
Si4 La1 Si4 41.767(16) 15_554 .
Si4 La1 Si4 90.95(4) 13_554 .
Si4 La1 Si4 76.26(3) 3 .
Si4 La1 Si4 41.767(16) 14_554 .
Si4 La1 Si4 76.26(3) 14 15
Si4 La1 Si4 103.74(3) 2 15
Si4 La1 Si4 90.95(4) 3_556 15
Si4 La1 Si4 41.767(16) 1_556 15
Si4 La1 Si4 89.05(4) 15_554 15
Si4 La1 Si4 138.233(16) 13_554 15
Si4 La1 Si4 180.00(4) 3 15
Si4 La1 Si4 138.233(16) 14_554 15
Si4 La1 Si4 103.74(3) . 15
Si4 La1 Si4 76.26(3) 14 13
Si4 La1 Si4 103.74(3) 2 13
Si4 La1 Si4 41.767(16) 3_556 13
Si4 La1 Si4 90.95(4) 1_556 13
Si4 La1 Si4 138.233(16) 15_554 13
Si4 La1 Si4 89.05(4) 13_554 13
Si4 La1 Si4 103.74(3) 3 13
Si4 La1 Si4 138.233(16) 14_554 13
Si4 La1 Si4 180.00(4) . 13
Si4 La1 Si4 76.26(3) 15 13
Si4 La1 Si4 90.95(4) 14 2_556
Si4 La1 Si4 89.05(4) 2 2_556
Si4 La1 Si4 76.26(3) 3_556 2_556
Si4 La1 Si4 76.26(3) 1_556 2_556
Si4 La1 Si4 103.74(3) 15_554 2_556
Si4 La1 Si4 103.74(3) 13_554 2_556
Si4 La1 Si4 138.233(16) 3 2_556
Si4 La1 Si4 180.00(10) 14_554 2_556
Si4 La1 Si4 138.233(16) . 2_556
Si4 La1 Si4 41.767(16) 15 2_556
Si4 La1 Si4 41.767(16) 13 2_556
O1 La2 O1 149.256(13) 3_666 1_556
O1 La2 Si4 120.596(15) 3_666 3
O1 La2 Si4 78.80(2) 1_556 3
O1 La2 Si4 78.80(2) 3_666 14_554
O1 La2 Si4 120.596(15) 1_556 14_554
Si4 La2 Si4 42.77(4) 3 14_554
O1 La2 Si4 120.596(15) 3_666 3_556
O1 La2 Si4 78.80(2) 1_556 3_556
Si4 La2 Si4 91.65(3) 3 3_556
Si4 La2 Si4 107.14(5) 14_554 3_556
O1 La2 Si4 78.80(2) 3_666 14
O1 La2 Si4 120.596(15) 1_556 14
Si4 La2 Si4 107.14(5) 3 14
Si4 La2 Si4 91.65(3) 14_554 14
Si4 La2 Si4 42.77(4) 3_556 14
O1 La2 Si5 79.200(6) 3_666 1_556
O1 La2 Si5 79.200(6) 1_556 1_556
Si4 La2 Si5 157.99(2) 3 1_556
Si4 La2 Si5 157.99(2) 14_554 1_556
Si4 La2 Si5 84.98(3) 3_556 1_556
Si4 La2 Si5 84.98(3) 14 1_556
O1 La2 Si5 79.200(6) 3_666 .
O1 La2 Si5 79.200(6) 1_556 .
Si4 La2 Si5 84.98(3) 3 .
Si4 La2 Si5 84.98(3) 14_554 .
Si4 La2 Si5 157.99(2) 3_556 .
Si4 La2 Si5 157.99(2) 14 .
Si5 La2 Si5 90.04(2) 1_556 .
O1 La2 La3 39.433(10) 3_666 3_666
O1 La2 La3 131.592(10) 1_556 3_666
Si4 La2 La3 148.07(3) 3 3_666
Si4 La2 La3 107.795(19) 14_554 3_666
Si4 La2 La3 86.420(19) 3_556 3_666
Si4 La2 La3 52.73(3) 14 3_666
Si5 La2 La3 53.557(10) 1_556 3_666
Si5 La2 La3 107.733(16) . 3_666
O1 La2 La3 131.592(10) 3_666 .
O1 La2 La3 39.433(10) 1_556 .
Si4 La2 La3 52.73(3) 3 .
Si4 La2 La3 86.420(19) 14_554 .
Si4 La2 La3 107.795(19) 3_556 .
Si4 La2 La3 148.07(3) 14 .
Si5 La2 La3 107.733(16) 1_556 .
Si5 La2 La3 53.557(10) . .
La3 La2 La3 156.371(11) 3_666 .
O1 La2 La3 131.592(10) 3_666 1_556
O1 La2 La3 39.433(10) 1_556 1_556
Si4 La2 La3 107.795(19) 3 1_556
Si4 La2 La3 148.07(3) 14_554 1_556
Si4 La2 La3 52.73(3) 3_556 1_556
Si4 La2 La3 86.420(19) 14 1_556
Si5 La2 La3 53.557(10) 1_556 1_556
Si5 La2 La3 107.733(16) . 1_556
La3 La2 La3 96.273(19) 3_666 1_556
La3 La2 La3 78.87(2) . 1_556
O1 La2 La3 39.433(10) 3_666 3_665
O1 La2 La3 131.592(10) 1_556 3_665
Si4 La2 La3 86.420(19) 3 3_665
Si4 La2 La3 52.73(3) 14_554 3_665
Si4 La2 La3 148.07(3) 3_556 3_665
Si4 La2 La3 107.795(19) 14 3_665
Si5 La2 La3 107.733(15) 1_556 3_665
Si5 La2 La3 53.557(10) . 3_665
La3 La2 La3 78.87(2) 3_666 3_665
La3 La2 La3 96.273(19) . 3_665
La3 La2 La3 156.371(11) 1_556 3_665
O1 La3 O1 180.0 1_556 .
O1 La3 Si4 90.0 1_556 15_654
O1 La3 Si4 90.0 . 15_654
O1 La3 Si4 90.0 1_556 3
O1 La3 Si4 90.0 . 3
Si4 La3 Si4 180.0 15_654 3
O1 La3 Si5 90.0 1_556 13_654
O1 La3 Si5 90.0 . 13_654
Si4 La3 Si5 90.0 15_654 13_654
Si4 La3 Si5 90.0 3 13_654
O1 La3 Si5 90.0 1_556 .
O1 La3 Si5 90.0 . .
Si4 La3 Si5 90.0 15_654 .
Si4 La3 Si5 90.0 3 .
Si5 La3 Si5 180.0 13_654 .
O1 La3 La2 129.433(11) 1_556 14_554
O1 La3 La2 50.567(10) . 14_554
Si4 La3 La2 123.345(7) 15_654 14_554
Si4 La3 La2 56.655(7) 3 14_554
Si5 La3 La2 57.140(7) 13_654 14_554
Si5 La3 La2 122.860(7) . 14_554
O1 La3 La2 50.567(10) 1_556 2_655
O1 La3 La2 129.433(11) . 2_655
Si4 La3 La2 56.655(7) 15_654 2_655
Si4 La3 La2 123.345(7) 3 2_655
Si5 La3 La2 122.860(7) 13_654 2_655
Si5 La3 La2 57.140(7) . 2_655
La2 La3 La2 180.0 14_554 2_655
O1 La3 La2 129.433(10) 1_556 13_654
O1 La3 La2 50.567(10) . 13_654
Si4 La3 La2 56.655(7) 15_654 13_654
Si4 La3 La2 123.345(7) 3 13_654
Si5 La3 La2 57.140(7) 13_654 13_654
Si5 La3 La2 122.860(7) . 13_654
La2 La3 La2 66.690(15) 14_554 13_654
La2 La3 La2 113.310(15) 2_655 13_654
O1 La3 La2 50.567(10) 1_556 .
O1 La3 La2 129.433(10) . .
Si4 La3 La2 123.345(7) 15_654 .
Si4 La3 La2 56.655(7) 3 .
Si5 La3 La2 122.860(7) 13_654 .
Si5 La3 La2 57.140(7) . .
La2 La3 La2 113.310(15) 14_554 .
La2 La3 La2 66.690(15) 2_655 .
La2 La3 La2 180.0 13_654 .
O1 La3 La2 50.567(10) 1_556 14
O1 La3 La2 129.433(10) . 14
Si4 La3 La2 123.345(7) 15_654 14
Si4 La3 La2 56.655(7) 3 14
Si5 La3 La2 57.140(7) 13_654 14
Si5 La3 La2 122.860(7) . 14
La2 La3 La2 78.87(2) 14_554 14
La2 La3 La2 101.13(2) 2_655 14
La2 La3 La2 114.280(13) 13_654 14
La2 La3 La2 65.720(13) . 14
O1 La3 La2 129.433(10) 1_556 2_654
O1 La3 La2 50.567(10) . 2_654
Si4 La3 La2 56.655(7) 15_654 2_654
Si4 La3 La2 123.345(7) 3 2_654
Si5 La3 La2 122.860(7) 13_654 2_654
Si5 La3 La2 57.140(7) . 2_654
La2 La3 La2 101.13(2) 14_554 2_654
La2 La3 La2 78.87(2) 2_655 2_654
La2 La3 La2 65.720(13) 13_654 2_654
La2 La3 La2 114.280(13) . 2_654
La2 La3 La2 180.000(1) 14 2_654
Si4 Si4 Si4 120.0 15_554 14_554
Si4 Si4 La3 120.0 15_554 2
Si4 Si4 La3 120.0 14_554 2
Si4 Si4 La2 134.154(15) 15_554 15
Si4 Si4 La2 68.616(18) 14_554 15
La3 Si4 La2 70.61(3) 2 15
Si4 Si4 La2 68.616(18) 15_554 2_554
Si4 Si4 La2 134.154(15) 14_554 2_554
La3 Si4 La2 70.61(3) 2 2_554
La2 Si4 La2 141.22(5) 15 2_554
Si4 Si4 La2 134.154(15) 15_554 15_554
Si4 Si4 La2 68.616(18) 14_554 15_554
La3 Si4 La2 70.61(3) 2 15_554
La2 Si4 La2 91.65(3) 15 15_554
La2 Si4 La2 75.57(2) 2_554 15_554
Si4 Si4 La2 68.616(18) 15_554 2
Si4 Si4 La2 134.154(15) 14_554 2
La3 Si4 La2 70.61(3) 2 2
La2 Si4 La2 75.57(2) 15 2
La2 Si4 La2 91.65(3) 2_554 2
La2 Si4 La2 141.22(5) 15_554 2
Si4 Si4 La1 69.116(8) 15_554 1_554
Si4 Si4 La1 69.116(8) 14_554 1_554
La3 Si4 La1 135.47(2) 2 1_554
La2 Si4 La1 137.70(3) 15 1_554
La2 Si4 La1 74.558(19) 2_554 1_554
La2 Si4 La1 74.558(19) 15_554 1_554
La2 Si4 La1 137.70(3) 2 1_554
Si4 Si4 La1 69.116(8) 15_554 .
Si4 Si4 La1 69.116(8) 14_554 .
La3 Si4 La1 135.47(2) 2 .
La2 Si4 La1 74.558(19) 15 .
La2 Si4 La1 137.70(3) 2_554 .
La2 Si4 La1 137.70(3) 15_554 .
La2 Si4 La1 74.558(19) 2 .
La1 Si4 La1 89.05(4) 1_554 .
La3 Si5 La3 120.0 2_655 .
La3 Si5 La3 120.0 2_655 3_665
La3 Si5 La3 120.0 . 3_665
La3 Si5 La2 69.303(4) 2_655 2_655
La3 Si5 La2 69.303(4) . 2_655
La3 Si5 La2 134.979(11) 3_665 2_655
La3 Si5 La2 69.303(4) 2_655 2_654
La3 Si5 La2 69.303(4) . 2_654
La3 Si5 La2 134.979(12) 3_665 2_654
La2 Si5 La2 90.04(2) 2_655 2_654
La3 Si5 La2 134.979(11) 2_655 1_554
La3 Si5 La2 69.303(4) . 1_554
La3 Si5 La2 69.303(4) 3_665 1_554
La2 Si5 La2 138.606(9) 2_655 1_554
La2 Si5 La2 75.490(18) 2_654 1_554
La3 Si5 La2 69.303(4) 2_655 3_665
La3 Si5 La2 134.979(12) . 3_665
La3 Si5 La2 69.303(4) 3_665 3_665
La2 Si5 La2 75.490(18) 2_655 3_665
La2 Si5 La2 138.606(9) 2_654 3_665
La2 Si5 La2 138.606(9) 1_554 3_665
La3 Si5 La2 69.303(4) 2_655 3_664
La3 Si5 La2 134.979(11) . 3_664
La3 Si5 La2 69.303(4) 3_665 3_664
La2 Si5 La2 138.606(9) 2_655 3_664
La2 Si5 La2 75.490(18) 2_654 3_664
La2 Si5 La2 75.490(18) 1_554 3_664
La2 Si5 La2 90.04(2) 3_665 3_664
La3 Si5 La2 134.979(11) 2_655 .
La3 Si5 La2 69.303(4) . .
La3 Si5 La2 69.303(4) 3_665 .
La2 Si5 La2 75.490(18) 2_655 .
La2 Si5 La2 138.606(9) 2_654 .
La2 Si5 La2 90.04(2) 1_554 .
La2 Si5 La2 75.490(18) 3_665 .
La2 Si5 La2 138.606(9) 3_664 .
La3 O1 La3 180.0 1_554 .
La3 O1 La2 90.0 1_554 14_554
La3 O1 La2 90.0 . 14_554
La3 O1 La2 90.0 1_554 2_654
La3 O1 La2 90.0 . 2_654
La2 O1 La2 180.0 14_554 2_654
La3 O1 La2 90.0 1_554 1_554
La3 O1 La2 90.0 . 1_554
La2 O1 La2 89.256(13) 14_554 1_554
La2 O1 La2 90.744(13) 2_654 1_554
La3 O1 La2 90.0 1_554 13_654
La3 O1 La2 90.0 . 13_654
La2 O1 La2 90.744(13) 14_554 13_654
La2 O1 La2 89.256(13) 2_654 13_654
La2 O1 La2 180.0 1_554 13_654
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
La1 Si4 3.3373(12) 14
La1 Si4 3.3373(13) 2
La1 Si4 3.3373(12) 3_556
La1 Si4 3.3373(12) 1_556
La1 Si4 3.3373(12) 15_554
La1 Si4 3.3373(12) 13_554
La1 Si4 3.3373(12) 3
La1 Si4 3.3373(12) 14_554
La1 Si4 3.3373(12) .
La1 Si4 3.3373(12) 15
La1 Si4 3.3373(12) 13
La1 Si4 3.3373(12) 2_556
La2 O1 2.8457(7) 3_666
La2 O1 2.8457(7) 1_556
La2 Si4 3.2628(8) 3
La2 Si4 3.2628(8) 14_554
La2 Si4 3.2628(8) 3_556
La2 Si4 3.2628(8) 14
La2 Si5 3.3083(7) 1_556
La2 Si5 3.3083(7) .
La2 La3 3.6843(7) 3_666
La2 La3 3.6843(7) .
La2 La3 3.6843(7) 1_556
La2 La3 3.6843(7) 3_665
La3 O1 2.3402(6) 1_556
La3 O1 2.3402(6) .
La3 Si4 3.1084(17) 15_654
La3 Si4 3.1084(17) 3
La3 Si5 3.1683(8) 13_654
La3 Si5 3.1683(8) .
La3 La2 3.6843(7) 14_554
La3 La2 3.6843(7) 2_655
La3 La2 3.6843(7) 13_654
La3 La2 3.6843(7) 14
La3 La2 3.6843(7) 2_654
Si4 Si4 2.3793(16) 15_554
Si4 Si4 2.3793(16) 14_554
Si4 La3 3.1084(17) 2
Si4 La2 3.2628(8) 15
Si4 La2 3.2628(8) 2_554
Si4 La2 3.2628(8) 15_554
Si4 La2 3.2628(8) 2
Si4 La1 3.3373(12) 1_554
Si5 La3 3.1683(8) 2_655
Si5 La3 3.1683(8) 3_665
Si5 La2 3.3083(7) 2_655
Si5 La2 3.3083(7) 2_654
Si5 La2 3.3083(7) 1_554
Si5 La2 3.3083(7) 3_665
Si5 La2 3.3083(7) 3_664
O1 La3 2.3402(6) 1_554
O1 La2 2.8457(7) 14_554
O1 La2 2.8457(7) 2_654
O1 La2 2.8457(7) 1_554
O1 La2 2.8457(7) 13_654
