#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/10/96/4109606.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4109606
loop_
_publ_author_name
'Jürgen Stahl'
'Wolfgang Mohr'
'Laura de Quadras'
'Thomas B. Peters'
'James C. Bohling'
'José Miguel Martín-Alvarez'
'Gareth R. Owen'
'Frank Hampel'
'John A. Gladysz'
_publ_section_title
;
 sp Carbon Chains Surrounded by sp3 Carbon Double Helices:
 Coordination-Driven Self-Assembly of Wirelike Pt(C\\tbC)nPt Moieties That
 Are Spanned by Two P(CH2)mP Linkages
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              8282
_journal_page_last               8295
_journal_paper_doi               10.1021/ja0716103
_journal_volume                  129
_journal_year                    2007
_chemical_formula_sum            'C94.5 H93 Cl5 F10 P4 Pt2'
_chemical_formula_weight         2110.00
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                77.8280(6)
_cell_angle_beta                 79.3644(6)
_cell_angle_gamma                87.8733(5)
_cell_formula_units_Z            2
_cell_length_a                   10.9876(1)
_cell_length_b                   17.2761(2)
_cell_length_c                   24.8047(2)
_cell_measurement_reflns_used    18783
_cell_measurement_temperature    173(2)
_cell_volume                     4523.57(8)
_computing_cell_refinement       DENZO-SMN
_computing_data_collection       'Nonius Collect'
_computing_data_reduction        DENZO-SMN
_computing_molecular_graphics    'SHELXTL NT'
_computing_publication_material  'SHELXTL NT'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      173(2)
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.992
_diffrn_measured_fraction_theta_max 0.992
_diffrn_measurement_device_type  'Nonius KappaCCD'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0198
_diffrn_reflns_av_sigmaI/netI    0.0310
_diffrn_reflns_limit_h_max       14
_diffrn_reflns_limit_h_min       -14
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       32
_diffrn_reflns_limit_l_min       -32
_diffrn_reflns_number            36689
_diffrn_reflns_theta_full        27.48
_diffrn_reflns_theta_max         27.48
_diffrn_reflns_theta_min         1.21
_exptl_absorpt_coefficient_mu    3.373
_exptl_absorpt_correction_T_max  0.7291
_exptl_absorpt_correction_T_min  0.3848
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   Scalepack
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.549
_exptl_crystal_description       plate
_exptl_crystal_F_000             2102
_exptl_crystal_size_max          0.35
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.10
_refine_diff_density_max         2.217
_refine_diff_density_min         -2.344
_refine_diff_density_rms         0.134
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.022
_refine_ls_hydrogen_treatment    'riding model'
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1053
_refine_ls_number_reflns         20581
_refine_ls_number_restraints     16
_refine_ls_restrained_S_all      1.032
_refine_ls_R_factor_all          0.0482
_refine_ls_R_factor_gt           0.0396
_refine_ls_shift/su_max          0.131
_refine_ls_shift/su_mean         0.009
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0602P)²+13.9824P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1040
_refine_ls_wR_factor_ref         0.1117
_reflns_number_gt                17663
_reflns_number_total             20581
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ja0716103si20070411_100938.cif
_cod_data_source_block           go07
_cod_original_formula_sum        'C94.50 H93 Cl5 F10 P4 Pt2'
_cod_database_code               4109606
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pt1 Pt -0.326585(15) 0.753058(11) -0.420550(6) 0.02975(6) Uani 1 1 d .
P1 P -0.50999(10) 0.73787(7) -0.44916(5) 0.0268(2) Uani 1 1 d .
C1 C -0.4190(4) 0.7375(3) -0.34120(18) 0.0358(11) Uani 1 1 d .
C1A C -0.6346(4) 0.7948(3) -0.4163(2) 0.0341(10) Uani 1 1 d .
H1AA H -0.7093 0.7910 -0.4326 0.041 Uiso 1 1 calc R
H1AB H -0.6548 0.7711 -0.3757 0.041 Uiso 1 1 calc R
C1B C -0.1600(8) 0.8311(11) -0.3397(4) 0.167(8) Uani 1 1 d .
H1BA H -0.1949 0.8014 -0.3016 0.200 Uiso 1 1 calc R
H1BB H -0.0756 0.8484 -0.3389 0.200 Uiso 1 1 calc R
Pt2 Pt -0.957807(14) 0.715609(9) 0.080133(6) 0.02168(5) Uani 1 1 d .
P2 P -0.14800(13) 0.76472(18) -0.38764(6) 0.0826(8) Uani 1 1 d D
C2 C -0.4753(5) 0.7332(3) -0.2941(2) 0.0388(11) Uani 1 1 d .
C2A C -0.6017(5) 0.8822(3) -0.4238(2) 0.0387(11) Uani 1 1 d .
H2AA H -0.5938 0.9080 -0.4640 0.046 Uiso 1 1 calc R
H2AB H -0.5206 0.8862 -0.4126 0.046 Uiso 1 1 calc R
C2B C -0.2356(10) 0.9011(10) -0.3529(5) 0.169(8) Uani 1 1 d .
H2BA H -0.3225 0.8892 -0.3455 0.203 Uiso 1 1 d R
H2BB H -0.2110 0.9284 -0.3911 0.203 Uiso 1 1 d R
P3 P -1.13972(10) 0.73410(7) 0.04545(4) 0.0254(2) Uani 1 1 d .
C3 C -0.5424(5) 0.7290(3) -0.24082(19) 0.0369(11) Uani 1 1 d .
C3A C -0.6998(5) 0.9260(3) -0.3889(2) 0.0427(12) Uani 1 1 d .
H3AA H -0.6838 0.9836 -0.4013 0.051 Uiso 1 1 calc R
H3AB H -0.7822 0.9156 -0.3966 0.051 Uiso 1 1 calc R
C3B C -0.2012(9) 0.9457(6) -0.3096(4) 0.051(2) Uiso 0.611(16) 1 d P
H3BA H -0.1227 0.9715 -0.3248 0.061 Uiso 0.611(16) 1 d PR
H3BB H -0.1942 0.9099 -0.2751 0.061 Uiso 0.611(16) 1 d PR
C3B' C -0.2455(16) 1.0028(10) -0.3411(7) 0.051(2) Uiso 0.39 1 d P
H3BC H -0.2879 1.0357 -0.3681 0.061 Uiso 0.389(16) 1 d PR
H3BD H -0.1632 1.0234 -0.3464 0.061 Uiso 0.389(16) 1 d PR
P4 P -0.77130(10) 0.70008(7) 0.11123(4) 0.0248(2) Uani 1 1 d .
C4 C -0.6031(5) 0.7246(3) -0.19415(19) 0.0361(10) Uani 1 1 d .
C4A C -0.7037(6) 0.9034(4) -0.3262(2) 0.0486(13) Uani 1 1 d .
H4AA H -0.6266 0.9214 -0.3174 0.058 Uiso 1 1 calc R
H4AB H -0.7079 0.8450 -0.3141 0.058 Uiso 1 1 calc R
C4B C -0.2924(9) 1.0009(6) -0.2975(6) 0.121(5) Uani 1 1 d .
H4BA H -0.3132 1.0271 -0.3328 0.145 Uiso 1 1 d R
H4BB H -0.2582 1.0400 -0.2823 0.145 Uiso 1 1 d R
C5 C -0.6718(5) 0.7193(3) -0.1417(2) 0.0375(11) Uani 1 1 d .
C5A C -0.8143(6) 0.9397(4) -0.2940(2) 0.0510(14) Uani 1 1 d .
H5AA H -0.8109 0.9978 -0.3077 0.061 Uiso 1 1 calc R
H5AB H -0.8907 0.9204 -0.3028 0.061 Uiso 1 1 calc R
C5B C -0.4131(7) 0.9703(5) -0.2590(3) 0.072(2) Uani 1 1 d .
H5BA H -0.4312 0.9186 -0.2640 0.086 Uiso 1 1 d R
H5BB H -0.4813 1.0046 -0.2667 0.086 Uiso 1 1 d R
C6 C -0.7346(5) 0.7149(3) -0.09506(19) 0.0340(10) Uani 1 1 d .
C6A C -0.8242(6) 0.9225(4) -0.2313(2) 0.0509(14) Uani 1 1 d .
H6AA H -0.7560 0.9497 -0.2217 0.061 Uiso 1 1 calc R
H6AB H -0.8148 0.8648 -0.2177 0.061 Uiso 1 1 calc R
C6B C -0.3996(10) 0.9664(5) -0.1994(3) 0.092(3) Uani 1 1 d .
H6BA H -0.3837 1.0187 -0.1948 0.110 Uiso 1 1 d R
H6BB H -0.3281 0.9345 -0.1931 0.110 Uiso 1 1 d R
C7 C -0.8047(4) 0.7119(3) -0.04313(19) 0.0325(10) Uani 1 1 d .
C7A C -0.9478(5) 0.9494(3) -0.2018(2) 0.0441(12) Uani 1 1 d .
H7AA H -0.9605 1.0058 -0.2185 0.053 Uiso 1 1 calc R
H7AB H -1.0150 0.9186 -0.2090 0.053 Uiso 1 1 calc R
C7B C -0.5012(8) 0.9324(5) -0.1579(3) 0.055(2) Uani 0.756(15) 1 d P
H7BA H -0.5222 0.8821 -0.1644 0.066 Uiso 0.756(15) 1 d PR
H7BB H -0.5709 0.9670 -0.1614 0.066 Uiso 0.756(15) 1 d PR
C7B' C -0.397(2) 0.8865(19) -0.1525(9) 0.057(9) Uani 0.244(15) 1 d P
H7BC H -0.3171 0.8644 -0.1486 0.068 Uiso 0.244(15) 1 d PR
H7BD H -0.4498 0.8487 -0.1604 0.068 Uiso 0.244(15) 1 d PR
C8 C -0.8654(4) 0.7103(3) 0.00316(17) 0.0288(9) Uani 1 1 d .
C8A C -0.9589(5) 0.9406(3) -0.1390(2) 0.0422(12) Uani 1 1 d .
H8AA H -0.9381 0.8855 -0.1224 0.051 Uiso 1 1 calc R
H8AB H -0.8982 0.9762 -0.1315 0.051 Uiso 1 1 calc R
C8B C -0.4742(9) 0.9222(5) -0.0957(3) 0.083(3) Uani 1 1 d .
H8BA H -0.4564 0.9726 -0.0884 0.099 Uiso 1 1 d R
H8BB H -0.4030 0.8888 -0.0923 0.099 Uiso 1 1 d R
C9A C -1.0864(5) 0.9598(3) -0.1113(2) 0.0413(11) Uani 1 1 d .
H9AA H -1.1448 0.9197 -0.1150 0.050 Uiso 1 1 calc R
H9AB H -1.1111 1.0119 -0.1318 0.050 Uiso 1 1 calc R
C9B C -0.5833(7) 0.8856(4) -0.0541(2) 0.065(2) Uani 1 1 d .
H9BA H -0.6600 0.9094 -0.0660 0.079 Uiso 1 1 calc R
H9BB H -0.5851 0.8283 -0.0537 0.079 Uiso 1 1 calc R
C10B C -0.5810(5) 0.8970(3) 0.0040(2) 0.0447(12) Uani 1 1 d .
H10C H -0.5919 0.9540 0.0045 0.054 Uiso 1 1 calc R
H10D H -0.4985 0.8812 0.0132 0.054 Uiso 1 1 calc R
C10A C -1.0998(6) 0.9627(3) -0.0492(2) 0.0484(13) Uani 1 1 d .
H10E H -1.0497 1.0073 -0.0459 0.058 Uiso 1 1 calc R
H10F H -1.1875 0.9735 -0.0347 0.058 Uiso 1 1 calc R
C11B C -0.6793(5) 0.8505(3) 0.0493(2) 0.0447(12) Uani 1 1 d .
H11A H -0.7599 0.8567 0.0364 0.054 Uiso 1 1 calc R
H11B H -0.6878 0.8725 0.0835 0.054 Uiso 1 1 calc R
C11A C -1.0600(6) 0.8869(3) -0.0127(2) 0.0424(12) Uani 1 1 d .
H11C H -1.0746 0.8929 0.0268 0.051 Uiso 1 1 calc R
H11D H -0.9701 0.8790 -0.0244 0.051 Uiso 1 1 calc R
C11 C -0.2306(4) 0.7772(3) -0.50228(17) 0.0337(10) Uani 1 1 d .
C12B C -0.6477(4) 0.7622(3) 0.0635(2) 0.0351(10) Uani 1 1 d .
H12A H -0.5725 0.7562 0.0806 0.042 Uiso 1 1 calc R
H12B H -0.6278 0.7425 0.0282 0.042 Uiso 1 1 calc R
C12A C -1.1303(5) 0.8129(3) -0.0165(2) 0.0370(11) Uani 1 1 d .
H12C H -1.0882 0.7924 -0.0496 0.044 Uiso 1 1 calc R
H12D H -1.2153 0.8285 -0.0224 0.044 Uiso 1 1 calc R
F12 F -0.2295(4) 0.6448(2) -0.51466(15) 0.0620(10) Uani 1 1 d .
C12 C -0.1966(5) 0.7217(4) -0.5350(2) 0.0430(13) Uani 1 1 d .
C13 C -0.1279(5) 0.7401(5) -0.5887(2) 0.0569(18) Uani 1 1 d .
F13 F -0.0963(4) 0.6819(3) -0.61802(15) 0.0832(14) Uani 1 1 d .
F14 F -0.0226(4) 0.8347(3) -0.66349(15) 0.0938(17) Uani 1 1 d .
C14 C -0.0897(5) 0.8160(5) -0.6115(2) 0.0598(19) Uani 1 1 d .
F15 F -0.0774(3) 0.9479(3) -0.60141(16) 0.0745(13) Uani 1 1 d .
C15 C -0.1194(5) 0.8731(4) -0.5805(2) 0.0514(16) Uani 1 1 d .
F16 F -0.2208(3) 0.9130(2) -0.50017(14) 0.0505(8) Uani 1 1 d .
C16 C -0.1911(4) 0.8526(4) -0.5274(2) 0.0394(12) Uani 1 1 d .
C21 C -0.1075(13) 0.6560(7) -0.3554(6) 0.0594(12) Uani 0.523(7) 1 d PD
C22 C -0.1815(12) 0.5869(7) -0.3516(6) 0.0594(12) Uani 0.523(7) 1 d P
H22A H -0.2570 0.5930 -0.3664 0.071 Uiso 0.523(7) 1 d PR
C23 C -0.1469(12) 0.5104(8) -0.3278(6) 0.0594(12) Uani 0.523(7) 1 d P
H23A H -0.1998 0.4672 -0.3273 0.071 Uiso 0.523(7) 1 d PR
C24 C -0.0465(11) 0.4975(8) -0.3041(6) 0.0594(12) Uani 0.523(7) 1 d P
H24A H -0.0254 0.4447 -0.2873 0.071 Uiso 0.523(7) 1 d PR
C25 C 0.0201(12) 0.5582(8) -0.3024(6) 0.0594(12) Uani 0.523(7) 1 d P
H25A H 0.0919 0.5480 -0.2851 0.071 Uiso 0.523(7) 1 d PR
C26 C -0.0062(12) 0.6358(8) -0.3278(6) 0.0594(12) Uani 0.523(7) 1 d P
H26A H 0.0498 0.6760 -0.3259 0.071 Uiso 0.523(7) 1 d PR
C21' C -0.0764(13) 0.7050(8) -0.3408(6) 0.0594(12) Uani 0.48 1 d PD
C22' C -0.1323(14) 0.6366(9) -0.3331(7) 0.0594(12) Uani 0.48 1 d P
H22B H -0.1843 0.6264 -0.3580 0.071 Uiso 0.477(7) 1 d PR
C23' C -0.0905(13) 0.5750(8) -0.2885(6) 0.0594(12) Uani 0.48 1 d P
H23B H -0.1464 0.5344 -0.2658 0.071 Uiso 0.477(7) 1 d PR
C24' C 0.0254(13) 0.5855(9) -0.2765(7) 0.0594(12) Uani 0.48 1 d P
H24B H 0.0706 0.5398 -0.2617 0.071 Uiso 0.477(7) 1 d PR
C25' C 0.0832(13) 0.6562(8) -0.2933(6) 0.0594(12) Uani 0.48 1 d P
H25B H 0.171(10) 0.6664(15) -0.276(2) 0.071 Uiso 0.477(7) 1 d PR
C26' C 0.0314(13) 0.7164(8) -0.3281(6) 0.0594(12) Uani 0.48 1 d P
H26B H 0.0747 0.7659 -0.3417 0.071 Uiso 0.477(7) 1 d PR
C31 C -0.0129(5) 0.7985(6) -0.4418(2) 0.075(3) Uani 1 1 d .
C32 C 0.0408(5) 0.7451(5) -0.4737(2) 0.063(2) Uani 1 1 d .
H32A H 0.0123 0.6918 -0.4646 0.076 Uiso 1 1 calc R
C33 C 0.1365(5) 0.7693(5) -0.5190(2) 0.0590(18) Uani 1 1 d .
H33A H 0.1733 0.7322 -0.5405 0.071 Uiso 1 1 calc R
C34 C 0.1778(5) 0.8456(6) -0.5328(3) 0.068(2) Uani 1 1 d .
H34A H 0.2417 0.8618 -0.5643 0.082 Uiso 1 1 calc R
C35 C 0.1261(6) 0.8995(6) -0.5008(3) 0.082(3) Uani 1 1 d .
H35A H 0.1551 0.9526 -0.5098 0.099 Uiso 1 1 calc R
C36 C 0.0303(6) 0.8743(7) -0.4550(3) 0.089(3) Uani 1 1 d .
H36A H -0.0050 0.9108 -0.4327 0.107 Uiso 1 1 calc R
C41 C -0.5108(4) 0.7674(3) -0.52443(17) 0.0277(9) Uani 1 1 d .
C42 C -0.4719(4) 0.8434(3) -0.5532(2) 0.0335(10) Uani 1 1 d .
H42A H -0.4442 0.8790 -0.5336 0.040 Uiso 1 1 calc R
C43 C -0.4736(5) 0.8674(3) -0.6101(2) 0.0424(12) Uani 1 1 d .
H43A H -0.4485 0.9196 -0.6291 0.051 Uiso 1 1 calc R
C44 C -0.5116(5) 0.8156(3) -0.6393(2) 0.0442(12) Uani 1 1 d .
H44A H -0.5127 0.8322 -0.6782 0.053 Uiso 1 1 calc R
C45 C -0.5479(6) 0.7400(4) -0.6118(2) 0.0472(13) Uani 1 1 d .
H45A H -0.5732 0.7042 -0.6319 0.057 Uiso 1 1 calc R
C46 C -0.5475(5) 0.7158(3) -0.5546(2) 0.0391(11) Uani 1 1 d .
H46A H -0.5727 0.6634 -0.5360 0.047 Uiso 1 1 calc R
C51 C -0.5629(5) 0.6360(3) -0.4313(2) 0.0414(12) Uani 1 1 d .
C52 C -0.6887(7) 0.6167(4) -0.4200(3) 0.0582(16) Uani 1 1 d .
H52A H -0.7501 0.6568 -0.4192 0.070 Uiso 1 1 calc R
C53 C -0.7226(9) 0.5354(5) -0.4098(3) 0.081(3) Uani 1 1 d .
H53A H -0.8077 0.5212 -0.4025 0.098 Uiso 1 1 calc R
C54 C -0.6340(11) 0.4775(4) -0.4105(3) 0.085(3) Uani 1 1 d .
H54A H -0.6576 0.4234 -0.4037 0.102 Uiso 1 1 calc R
C55 C -0.5123(10) 0.4977(4) -0.4208(3) 0.093(3) Uani 1 1 d .
H55A H -0.4512 0.4573 -0.4211 0.112 Uiso 1 1 calc R
C56 C -0.4760(7) 0.5755(4) -0.4309(3) 0.067(2) Uani 1 1 d .
H56A H -0.3903 0.5880 -0.4376 0.080 Uiso 1 1 calc R
C61 C -1.0548(4) 0.7250(3) 0.15859(16) 0.0232(8) Uani 1 1 d .
F62 F -1.0643(3) 0.58660(17) 0.19238(13) 0.0501(8) Uani 1 1 d .
C62 C -1.0926(4) 0.6606(3) 0.20082(18) 0.0317(9) Uani 1 1 d .
F63 F -1.1994(4) 0.6003(2) 0.29165(13) 0.0711(12) Uani 1 1 d .
C63 C -1.1645(5) 0.6662(3) 0.2523(2) 0.0413(12) Uani 1 1 d .
F64 F -1.2716(4) 0.7453(3) 0.31165(13) 0.0650(10) Uani 1 1 d .
C64 C -1.2007(5) 0.7388(4) 0.2624(2) 0.0421(12) Uani 1 1 d .
F65 F -1.2045(3) 0.8767(2) 0.23112(15) 0.0573(9) Uani 1 1 d .
C65 C -1.1666(4) 0.8050(3) 0.2218(2) 0.0357(10) Uani 1 1 d .
F66 F -1.0641(3) 0.86484(16) 0.13275(12) 0.0405(7) Uani 1 1 d .
C66 C -1.0944(4) 0.7967(3) 0.17123(18) 0.0278(9) Uani 1 1 d .
C71 C -1.1928(4) 0.6470(3) 0.02598(19) 0.0333(10) Uani 1 1 d .
C72 C -1.2963(5) 0.6532(4) -0.0002(2) 0.0497(14) Uani 1 1 d .
H72A H -1.3377 0.7024 -0.0081 0.060 Uiso 1 1 calc R
C73 C -1.3377(7) 0.5865(5) -0.0146(3) 0.069(2) Uani 1 1 d .
H73A H -1.4078 0.5900 -0.0324 0.083 Uiso 1 1 calc R
C74 C -1.2760(7) 0.5144(5) -0.0029(4) 0.077(2) Uani 1 1 d .
H74A H -1.3035 0.4690 -0.0133 0.092 Uiso 1 1 calc R
C75 C -1.1765(7) 0.5090(4) 0.0235(4) 0.073(2) Uani 1 1 d .
H75A H -1.1362 0.4595 0.0321 0.087 Uiso 1 1 calc R
C76 C -1.1334(5) 0.5753(3) 0.0378(3) 0.0505(14) Uani 1 1 d .
H76A H -1.0634 0.5712 0.0557 0.061 Uiso 1 1 calc R
C81 C -1.2745(4) 0.7597(3) 0.09370(19) 0.0312(9) Uani 1 1 d .
C82 C -1.3169(5) 0.8369(3) 0.0916(2) 0.0443(12) Uani 1 1 d .
H82A H -1.2813 0.8782 0.0617 0.053 Uiso 1 1 calc R
C83 C -1.4117(6) 0.8540(4) 0.1332(3) 0.0595(18) Uani 1 1 d .
H83A H -1.4396 0.9069 0.1318 0.071 Uiso 1 1 calc R
C84 C -1.4648(5) 0.7949(5) 0.1760(3) 0.0593(18) Uani 1 1 d .
H84A H -1.5291 0.8070 0.2043 0.071 Uiso 1 1 calc R
C85 C -1.4254(5) 0.7181(4) 0.1783(2) 0.0515(15) Uani 1 1 d .
H85A H -1.4631 0.6772 0.2079 0.062 Uiso 1 1 calc R
C86 C -1.3303(4) 0.7002(3) 0.1372(2) 0.0354(10) Uani 1 1 d .
H86A H -1.3035 0.6470 0.1390 0.042 Uiso 1 1 calc R
C91 C -0.7740(4) 0.7255(3) 0.17950(18) 0.0289(9) Uani 1 1 d .
C92 C -0.7384(5) 0.6730(4) 0.2243(2) 0.0435(12) Uani 1 1 d .
H92A H -0.7117 0.6213 0.2203 0.052 Uiso 1 1 calc R
C93 C -0.7416(6) 0.6959(5) 0.2750(2) 0.0592(18) Uani 1 1 d .
H93A H -0.7172 0.6596 0.3056 0.071 Uiso 1 1 calc R
C94 C -0.7802(5) 0.7714(5) 0.2811(3) 0.063(2) Uani 1 1 d .
H94A H -0.7802 0.7872 0.3156 0.075 Uiso 1 1 calc R
C95 C -0.8181(5) 0.8230(4) 0.2377(2) 0.0470(14) Uani 1 1 d .
H95A H -0.8470 0.8741 0.2423 0.056 Uiso 1 1 calc R
C96 C -0.8147(4) 0.8010(3) 0.1868(2) 0.0341(10) Uani 1 1 d .
H96A H -0.8401 0.8375 0.1566 0.041 Uiso 1 1 calc R
C101 C -0.7087(4) 0.6009(3) 0.1201(2) 0.0334(10) Uani 1 1 d .
C102 C -0.5825(5) 0.5852(3) 0.1081(2) 0.0434(12) Uani 1 1 d .
H10G H -0.5262 0.6275 0.0907 0.052 Uiso 1 1 calc R
C103 C -0.5379(6) 0.5089(4) 0.1212(3) 0.0589(17) Uani 1 1 d .
H10H H -0.4516 0.4995 0.1118 0.071 Uiso 1 1 calc R
C104 C -0.6145(7) 0.4477(4) 0.1470(3) 0.070(2) Uani 1 1 d .
H10I H -0.5826 0.3957 0.1562 0.084 Uiso 1 1 calc R
C105 C -0.7397(7) 0.4616(4) 0.1598(4) 0.083(3) Uani 1 1 d .
H10J H -0.7940 0.4189 0.1787 0.099 Uiso 1 1 calc R
C106 C -0.7875(6) 0.5370(4) 0.1456(3) 0.0632(19) Uani 1 1 d .
H10K H -0.8745 0.5452 0.1533 0.076 Uiso 1 1 calc R
C100 C 1.0251(10) 0.3186(10) 0.1314(6) 0.250(13) Uani 1 1 d D
H10A H 1.0720 0.3458 0.0946 0.300 Uiso 1 1 calc R
H10B H 0.9625 0.2850 0.1233 0.300 Uiso 1 1 calc R
Cl11 Cl 0.9489(5) 0.3870(5) 0.1595(4) 0.328(5) Uani 1 1 d D
Cl12 Cl 1.1287(7) 0.2543(2) 0.16369(19) 0.242(4) Uani 1 1 d D
C200 C 0.5814(8) 0.4602(5) 0.2800(3) 0.088(3) Uani 1 1 d D
H20A H 0.5537 0.4043 0.2887 0.106 Uiso 1 1 calc R
H20B H 0.6249 0.4676 0.3102 0.106 Uiso 1 1 calc R
Cl21 Cl 0.4550(4) 0.5192(3) 0.28089(15) 0.214(3) Uani 1 1 d D
Cl22 Cl 0.6849(2) 0.47693(15) 0.21763(10) 0.0871(6) Uani 1 1 d D
Cl32 Cl -0.1669(9) 0.4227(7) -0.4464(4) 0.189(4) Uani 0.50 1 d PD
C300 C -0.0380(14) 0.4753(9) -0.4800(7) 0.101(8) Uani 0.50 1 d PD
H30A H -0.0407 0.5018 -0.5179 0.121 Uiso 0.50 1 d PR
H30B H 0.0392 0.4484 -0.4769 0.121 Uiso 0.50 1 d PR
Cl31 Cl -0.0821(14) 0.5219(12) -0.4301(8) 0.57(3) Uani 0.50 1 d PD
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
C1 Pt1 C11 176.1(2) .
C1 Pt1 P2 88.39(15) .
C11 Pt1 P2 90.64(13) .
C1 Pt1 P1 88.97(15) .
C11 Pt1 P1 92.07(12) .
P2 Pt1 P1 177.12(5) .
C1 Pt1 Pt2 4.99(15) .
C11 Pt1 Pt2 171.35(15) .
P2 Pt1 Pt2 89.67(4) .
P1 Pt1 Pt2 87.79(3) .
C51 P1 C1A 106.1(2) .
C51 P1 C41 103.7(2) .
C1A P1 C41 105.0(2) .
C51 P1 Pt1 112.72(19) .
C1A P1 Pt1 111.64(16) .
C41 P1 Pt1 116.76(14) .
C2 C1 Pt1 176.0(5) .
C2A C1A P1 113.1(3) .
C2B C1B P2 115.2(7) .
C8 Pt2 C61 178.10(18) .
C8 Pt2 P3 89.60(13) .
C61 Pt2 P3 89.56(11) .
C8 Pt2 P4 88.37(13) .
C61 Pt2 P4 92.44(11) .
P3 Pt2 P4 177.55(4) .
C8 Pt2 Pt1 5.71(13) .
C61 Pt2 Pt1 172.70(12) .
P3 Pt2 Pt1 90.79(3) .
P4 Pt2 Pt1 87.05(3) .
C21' P2 C1B 84.3(8) .
C21' P2 C31 99.0(6) .
C1B P2 C31 105.6(5) .
C21' P2 C21 33.5(6) .
C1B P2 C21 114.0(7) .
C31 P2 C21 104.0(5) .
C21' P2 Pt1 133.2(5) .
C1B P2 Pt1 114.1(4) .
C31 P2 Pt1 114.93(18) .
C21 P2 Pt1 104.0(4) .
C21' P2 C22' 32.8(7) .
C1B P2 C22' 105.8(7) .
C31 P2 C22' 115.4(5) .
C21 P2 C22' 11.9(7) .
Pt1 P2 C22' 101.0(4) .
C1 C2 C3 178.5(6) .
C1A C2A C3A 112.1(4) .
C1B C2B C3B 97.5(11) .
C1B C2B C3B' 137.6(10) .
C3B C2B C3B' 42.8(7) .
C12A P3 C81 104.3(2) .
C12A P3 C71 105.7(2) .
C81 P3 C71 102.6(2) .
C12A P3 Pt2 113.26(17) .
C81 P3 Pt2 115.53(14) .
C71 P3 Pt2 114.17(17) .
C4 C3 C2 178.9(6) .
C4A C3A C2A 114.8(4) .
C3B' C3B C4B 48.8(9) .
C3B' C3B C2B 80.7(11) .
C4B C3B C2B 110.3(10) .
C4B C3B' C3B 71.7(12) .
C4B C3B' C2B 108.0(13) .
C3B C3B' C2B 56.5(9) .
C101 P4 C91 103.4(2) .
C101 P4 C12B 104.7(2) .
C91 P4 C12B 104.6(2) .
C101 P4 Pt2 115.42(16) .
C91 P4 Pt2 114.80(14) .
C12B P4 Pt2 112.68(17) .
C3 C4 C5 179.6(6) .
C3A C4A C5A 111.7(5) .
C3B' C4B C3B 59.5(10) .
C3B' C4B C5B 138.7(13) .
C3B C4B C5B 117.9(9) .
C6 C5 C4 179.2(6) .
C6A C5A C4A 115.7(5) .
C6B C5B C4B 108.8(8) .
C5 C6 C7 178.6(5) .
C5A C6A C7A 112.1(5) .
C7B C6B C5B 115.6(9) .
C7B C6B C7B' 53.6(9) .
C5B C6B C7B' 125.4(13) .
C8 C7 C6 178.7(5) .
C8A C7A C6A 114.6(5) .
C6B C7B C7B' 70.2(12) .
C6B C7B C8B 112.5(7) .
C7B' C7B C8B 70.4(12) .
C7B C7B' C6B 56.2(11) .
C7B C7B' C8B 60.8(11) .
C6B C7B' C8B 97.8(17) .
C7 C8 Pt2 175.1(4) .
C9A C8A C7A 112.3(4) .
C9B C8B C7B 110.1(7) .
C9B C8B C7B' 126.9(12) .
C7B C8B C7B' 48.8(9) .
C8A C9A C10A 115.1(5) .
C10B C9B C8B 112.6(5) .
C9B C10B C11B 114.5(5) .
C11A C10A C9A 114.2(5) .
C10B C11B C12B 112.1(5) .
C10A C11A C12A 112.7(4) .
C16 C11 C12 114.5(4) .
C16 C11 Pt1 120.3(4) .
C12 C11 Pt1 125.2(4) .
C11B C12B P4 114.6(3) .
C11A C12A P3 113.4(3) .
F12 C12 C13 116.7(5) .
F12 C12 C11 120.1(4) .
C13 C12 C11 123.2(6) .
C14 C13 C12 119.8(6) .
C14 C13 F13 120.4(5) .
C12 C13 F13 119.8(7) .
F14 C14 C15 120.3(7) .
F14 C14 C13 120.5(7) .
C15 C14 C13 119.3(5) .
C14 C15 F15 120.0(5) .
C14 C15 C16 119.1(6) .
F15 C15 C16 120.9(6) .
F16 C16 C11 120.3(4) .
F16 C16 C15 115.6(5) .
C11 C16 C15 124.1(6) .
C22' C21 C21' 99(3) .
C22' C21 C26 78(2) .
C21' C21 C26 67.7(11) .
C22' C21 C22 58(2) .
C21' C21 C22 155.6(18) .
C26 C21 C22 110.8(10) .
C22' C21 P2 126(3) .
C21' C21 P2 59.1(7) .
C26 C21 P2 123.3(11) .
C22 C21 P2 125.6(9) .
C22' C21 C23' 32.5(19) .
C21' C21 C23' 96.2(12) .
C26 C21 C23' 49.1(7) .
C22 C21 C23' 69.0(8) .
P2 C21 C23' 148.7(10) .
C22' C22 C23 110.4(13) .
C22' C22 C21 24.4(9) .
C23 C22 C21 122.6(11) .
C22' C22 C23' 48.8(9) .
C23 C22 C23' 62.4(8) .
C21 C22 C23' 68.0(9) .
C24 C23 C22 121.4(13) .
C24 C23 C23' 54.5(9) .
C22 C23 C23' 74.6(9) .
C25 C24 C23 119.1(12) .
C25 C24 C23' 51.7(9) .
C23 C24 C23' 79.4(10) .
C25 C24 C24' 18.1(8) .
C23 C24 C24' 120.5(10) .
C23' C24 C24' 43.1(7) .
C24' C25 C23' 79.5(16) .
C24' C25 C24 134.3(19) .
C23' C25 C24 72.3(11) .
C24' C25 C26 76.6(14) .
C23' C25 C26 68.4(10) .
C24 C25 C26 122.1(12) .
C24' C25 C25' 38.3(13) .
C23' C25 C25' 95.1(11) .
C24 C25 C25' 167.3(13) .
C26 C25 C25' 51.2(8) .
C25 C26 C22' 106.5(12) .
C25 C26 C21' 158.4(14) .
C22' C26 C21' 55.4(9) .
C25 C26 C21 123.6(13) .
C22' C26 C21 24.7(7) .
C21' C26 C21 44.9(8) .
C25 C26 C24' 35.8(8) .
C22' C26 C24' 116.3(12) .
C21' C26 C24' 136.2(14) .
C21 C26 C24' 140.8(13) .
C25 C26 C26' 137.9(12) .
C22' C26 C26' 108.8(11) .
C21' C26 C26' 54.3(9) .
C21 C26 C26' 97.6(10) .
C24' C26 C26' 106.1(12) .
C25 C26 C25' 82.7(10) .
C22' C26 C25' 144.3(14) .
C21' C26 C25' 105.4(12) .
C21 C26 C25' 150.1(13) .
C24' C26 C25' 53.7(9) .
C26' C26 C25' 55.3(9) .
C25 C26 C23' 50.8(8) .
C22' C26 C23' 61.7(9) .
C21' C26 C23' 107.6(11) .
C21 C26 C23' 85.4(10) .
C24' C26 C23' 55.9(9) .
C26' C26 C23' 135.4(14) .
C25' C26 C23' 105.1(11) .
C21 C21' C22' 27.0(11) .
C21 C21' C26' 129.3(15) .
C22' C21' C26' 126.3(13) .
C21 C21' C26 67.4(11) .
C22' C21' C26 62.5(10) .
C26' C21' C26 65.0(10) .
C21 C21' P2 87.4(9) .
C22' C21' P2 103.5(11) .
C26' C21' P2 127.4(12) .
C26 C21' P2 147.9(13) .
C21 C22' C22 98(3) .
C21 C22' C21' 54(2) .
C22 C22' C21' 150.5(16) .
C21 C22' C26 77(2) .
C22 C22' C26 124.5(15) .
C21' C22' C26 62.2(10) .
C21 C22' C23' 135(3) .
C22 C22' C23' 92.5(12) .
C21' C22' C23' 113.0(13) .
C26 C22' C23' 61.6(9) .
C21 C22' P2 42(2) .
C22 C22' P2 111.0(11) .
C21' C22' P2 43.7(7) .
C26 C22' P2 100.7(9) .
C23' C22' P2 156.3(12) .
C25 C23' C24' 38.8(9) .
C25 C23' C22' 110.9(14) .
C24' C23' C22' 116.8(13) .
C25 C23' C24 56.1(10) .
C24' C23' C24 89.1(11) .
C22' C23' C24 117.0(13) .
C25 C23' C26 60.8(10) .
C24' C23' C26 61.4(9) .
C22' C23' C26 56.7(9) .
C24 C23' C26 104.8(12) .
C25 C23' C23 94.5(12) .
C24' C23' C23 132.7(13) .
C22' C23' C23 81.1(10) .
C24 C23' C23 46.1(7) .
C26 C23' C23 109.5(11) .
C25 C23' C22 112.1(13) .
C24' C23' C22 142.2(13) .
C22' C23' C22 38.7(8) .
C24 C23' C22 85.1(9) .
C26 C23' C22 84.1(9) .
C23 C23' C22 43.0(6) .
C25 C23' C21 98.4(11) .
C24' C23' C21 106.8(11) .
C22' C23' C21 12.5(8) .
C24 C23' C21 111.2(11) .
C26 C23' C21 45.6(7) .
C23 C23' C21 82.5(8) .
C22 C23' C21 43.0(6) .
C25 C24' C25' 117.7(19) .
C25 C24' C23' 61.6(14) .
C25' C24' C23' 121.2(12) .
C25 C24' C26 67.6(13) .
C25' C24' C26 64.7(10) .
C23' C24' C26 62.7(9) .
C25 C24' C24 27.5(12) .
C25' C24' C24 143.8(13) .
C23' C24' C24 47.9(8) .
C26 C24' C24 83.7(10) .
C24' C25' C26' 118.7(13) .
C24' C25' C26 61.7(10) .
C26' C25' C26 60.7(9) .
C24' C25' C25 24.0(8) .
C26' C25' C25 106.8(11) .
C26 C25' C25 46.1(7) .
C21' C26' C25' 119.4(13) .
C21' C26' C26 60.8(10) .
C25' C26' C26 64.1(9) .
C32 C31 C36 119.1(6) .
C32 C31 P2 117.3(7) .
C36 C31 P2 123.4(6) .
C31 C32 C33 120.2(8) .
C34 C33 C32 120.7(7) .
C33 C34 C35 119.8(7) .
C34 C35 C36 119.0(9) .
C31 C36 C35 121.2(8) .
C46 C41 C42 118.3(4) .
C46 C41 P1 122.0(4) .
C42 C41 P1 119.7(3) .
C43 C42 C41 120.6(5) .
C44 C43 C42 120.2(5) .
C45 C44 C43 119.9(5) .
C44 C45 C46 120.2(5) .
C45 C46 C41 120.7(5) .
C52 C51 C56 119.0(6) .
C52 C51 P1 121.9(5) .
C56 C51 P1 119.1(5) .
C51 C52 C53 118.5(7) .
C54 C53 C52 120.8(8) .
C53 C54 C55 119.6(7) .
C56 C55 C54 121.2(8) .
C55 C56 C51 120.9(8) .
C66 C61 C62 114.3(4) .
C66 C61 Pt2 122.2(3) .
C62 C61 Pt2 123.3(3) .
F62 C62 C63 116.6(4) .
F62 C62 C61 119.7(4) .
C63 C62 C61 123.6(4) .
F63 C63 C64 120.1(4) .
F63 C63 C62 120.5(5) .
C64 C63 C62 119.4(5) .
F64 C64 C63 120.2(5) .
F64 C64 C65 120.2(5) .
C63 C64 C65 119.6(4) .
F65 C65 C64 119.8(4) .
F65 C65 C66 121.1(5) .
C64 C65 C66 119.1(4) .
F66 C66 C61 120.0(4) .
F66 C66 C65 116.0(4) .
C61 C66 C65 124.0(4) .
C76 C71 C72 120.2(5) .
C76 C71 P3 120.5(4) .
C72 C71 P3 119.2(4) .
C73 C72 C71 119.3(6) .
C72 C73 C74 119.9(6) .
C75 C74 C73 120.1(6) .
C74 C75 C76 120.6(7) .
C71 C76 C75 119.8(6) .
C82 C81 C86 118.6(5) .
C82 C81 P3 122.9(4) .
C86 C81 P3 118.3(4) .
C81 C82 C83 120.2(6) .
C84 C83 C82 120.4(6) .
C83 C84 C85 120.2(6) .
C84 C85 C86 120.1(6) .
C81 C86 C85 120.4(5) .
C92 C91 C96 118.6(4) .
C92 C91 P4 122.8(4) .
C96 C91 P4 118.6(4) .
C91 C92 C93 120.2(6) .
C92 C93 C94 120.3(6) .
C95 C94 C93 119.9(5) .
C94 C95 C96 120.2(6) .
C95 C96 C91 120.7(5) .
C102 C101 C106 117.5(5) .
C102 C101 P4 123.0(4) .
C106 C101 P4 119.2(4) .
C103 C102 C101 120.9(6) .
C104 C103 C102 121.3(6) .
C103 C104 C105 119.1(6) .
C106 C105 C104 120.9(7) .
C105 C106 C101 120.3(6) .
Cl11 C100 Cl12 123.5(7) .
Cl21 C200 Cl22 114.8(5) .
C300 Cl32 Cl31 48.2(5) .
C300 C300 Cl31 106.2(19) 2_564
C300 C300 Cl32 160(2) 2_564
Cl31 C300 Cl32 80.2(9) .
C300 Cl31 Cl32 51.7(7) .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pt1 C1 2.009(4) .
Pt1 C11 2.069(4) .
Pt1 P2 2.2907(15) .
Pt1 P1 2.2976(11) .
Pt1 Pt2 12.9580(2) .
P1 C51 1.812(5) .
P1 C1A 1.825(5) .
P1 C41 1.830(4) .
C1 C2 1.205(6) .
C1A C2A 1.531(7) .
C1B C2B 1.46(2) .
C1B P2 1.804(12) .
Pt2 C8 2.009(4) .
Pt2 C61 2.075(4) .
Pt2 P3 2.3040(11) .
Pt2 P4 2.3069(11) .
P2 C21' 1.674(11) .
P2 C31 1.830(7) .
P2 C21 1.949(12) .
P2 C22' 2.356(14) .
C2 C3 1.379(6) .
C2A C3A 1.536(7) .
C2B C3B 1.552(12) .
C2B C3B' 1.84(2) .
P3 C12A 1.816(5) .
P3 C81 1.828(5) .
P3 C71 1.820(4) .
C3 C4 1.214(7) .
C3A C4A 1.513(8) .
C3B C3B' 1.264(19) .
C3B C4B 1.393(13) .
C3B' C4B 1.103(18) .
P4 C101 1.807(5) .
P4 C91 1.832(4) .
P4 C12B 1.838(5) .
C4 C5 1.365(7) .
C4A C5A 1.518(8) .
C4B C5B 1.524(12) .
C5 C6 1.222(7) .
C5A C6A 1.504(8) .
C5B C6B 1.501(10) .
C6 C7 1.365(6) .
C6A C7A 1.526(8) .
C6B C7B 1.420(12) .
C6B C7B' 1.61(3) .
C7 C8 1.212(6) .
C7A C8A 1.516(7) .
C7B C7B' 1.38(3) .
C7B C8B 1.597(11) .
C7B' C8B 1.72(3) .
C8A C9A 1.500(8) .
C8B C9B 1.493(9) .
C9A C10A 1.531(7) .
C9B C10B 1.501(8) .
C10B C11B 1.519(7) .
C10A C11A 1.526(7) .
C11B C12B 1.532(7) .
C11A C12A 1.547(7) .
C11 C16 1.368(8) .
C11 C12 1.381(7) .
F12 C12 1.355(7) .
C12 C13 1.385(7) .
C13 C14 1.362(11) .
C13 F13 1.359(8) .
F14 C14 1.343(6) .
C14 C15 1.368(10) .
F15 C15 1.352(8) .
C15 C16 1.386(7) .
F16 C16 1.357(7) .
C21 C22' 0.604(18) .
C21 C21' 1.077(19) .
C21 C26 1.408(17) .
C21 C22 1.446(19) .
C21 C23' 1.965(18) .
C22 C22' 1.24(2) .
C22 C23 1.399(16) .
C22 C23' 1.979(19) .
C23 C24 1.334(16) .
C23 C23' 1.82(2) .
C24 C25 1.313(18) .
C24 C23' 1.507(19) .
C24 C24' 2.03(2) .
C25 C24' 0.885(18) .
C25 C23' 1.242(18) .
C25 C26 1.399(16) .
C25 C25' 1.93(2) .
C26 C22' 1.415(19) .
C26 C21' 1.411(16) .
C26 C24' 1.472(17) .
C26 C26' 1.465(19) .
C26 C25' 1.512(19) .
C26 C23' 1.489(19) .
C21' C22' 1.31(2) .
C21' C26' 1.313(18) .
C22' C23' 1.491(18) .
C23' C24' 1.387(19) .
C24' C25' 1.347(19) .
C25' C26' 1.381(17) .
C31 C32 1.385(11) .
C31 C36 1.362(14) .
C32 C33 1.393(8) .
C33 C34 1.363(11) .
C34 C35 1.388(11) .
C35 C36 1.405(11) .
C41 C46 1.392(7) .
C41 C42 1.396(6) .
C42 C43 1.390(7) .
C43 C44 1.381(8) .
C44 C45 1.375(8) .
C45 C46 1.393(7) .
C51 C52 1.397(8) .
C51 C56 1.390(9) .
C52 C53 1.423(9) .
C53 C54 1.371(13) .
C54 C55 1.359(13) .
C55 C56 1.375(9) .
C61 C66 1.377(6) .
C61 C62 1.375(6) .
F62 C62 1.354(6) .
C62 C63 1.392(6) .
F63 C63 1.349(6) .
C63 C64 1.362(8) .
F64 C64 1.346(5) .
C64 C65 1.367(8) .
F65 C65 1.345(6) .
C65 C66 1.387(6) .
F66 C66 1.358(5) .
C71 C76 1.380(8) .
C71 C72 1.401(7) .
C72 C73 1.391(8) .
C73 C74 1.397(12) .
C74 C75 1.365(11) .
C75 C76 1.392(8) .
C81 C82 1.390(7) .
C81 C86 1.391(7) .
C82 C83 1.396(8) .
C83 C84 1.366(10) .
C84 C85 1.372(10) .
C85 C86 1.393(7) .
C91 C92 1.385(7) .
C91 C96 1.400(7) .
C92 C93 1.389(8) .
C93 C94 1.387(10) .
C94 C95 1.365(9) .
C95 C96 1.386(7) .
C101 C102 1.393(7) .
C101 C106 1.394(8) .
C102 C103 1.384(8) .
C103 C104 1.349(10) .
C104 C105 1.377(10) .
C105 C106 1.387(9) .
C100 Cl11 1.625(9) .
C100 Cl12 1.744(11) .
C200 Cl21 1.692(8) .
C200 Cl22 1.721(8) .
Cl32 C300 1.693(14) .
Cl32 Cl31 2.127(19) .
C300 C300 1.34(3) 2_564
C300 Cl31 1.608(15) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C1 Pt1 P1 C51 -73.9(2) . .
C11 Pt1 P1 C51 109.9(2) . .
P2 Pt1 P1 C51 -50.6(15) . .
Pt2 Pt1 P1 C51 -78.78(18) . .
C1 Pt1 P1 C1A 45.4(2) . .
C11 Pt1 P1 C1A -130.8(2) . .
P2 Pt1 P1 C1A 68.7(15) . .
Pt2 Pt1 P1 C1A 40.50(18) . .
C1 Pt1 P1 C41 166.1(2) . .
C11 Pt1 P1 C41 -10.1(2) . .
P2 Pt1 P1 C41 -170.5(14) . .
Pt2 Pt1 P1 C41 161.26(17) . .
C11 Pt1 C1 C2 13(9) . .
P2 Pt1 C1 C2 89(7) . .
P1 Pt1 C1 C2 -92(7) . .
Pt2 Pt1 C1 C2 -16(5) . .
C51 P1 C1A C2A 176.1(4) . .
C41 P1 C1A C2A -74.4(4) . .
Pt1 P1 C1A C2A 53.0(4) . .
C1 Pt1 Pt2 C8 -40(2) . .
C11 Pt1 Pt2 C8 153.0(16) . .
P2 Pt1 Pt2 C8 -114.8(14) . .
P1 Pt1 Pt2 C8 63.8(13) . .
C1 Pt1 Pt2 C61 150(2) . .
C11 Pt1 Pt2 C61 -17.6(12) . .
P2 Pt1 Pt2 C61 74.5(9) . .
P1 Pt1 Pt2 C61 -106.9(9) . .
C1 Pt1 Pt2 P3 -117.8(17) . .
C11 Pt1 Pt2 P3 75.1(8) . .
P2 Pt1 Pt2 P3 167.21(8) . .
P1 Pt1 Pt2 P3 -14.15(4) . .
C1 Pt1 Pt2 P4 63.4(17) . .
C11 Pt1 Pt2 P4 -103.8(8) . .
P2 Pt1 Pt2 P4 -11.64(8) . .
P1 Pt1 Pt2 P4 167.00(4) . .
C2B C1B P2 C21' -172.2(10) . .
C2B C1B P2 C31 90.1(8) . .
C2B C1B P2 C21 -156.4(9) . .
C2B C1B P2 Pt1 -37.1(10) . .
C2B C1B P2 C22' -147.1(9) . .
C1 Pt1 P2 C21' 57.9(8) . .
C11 Pt1 P2 C21' -125.9(8) . .
P1 Pt1 P2 C21' 34.5(17) . .
Pt2 Pt1 P2 C21' 62.7(8) . .
C1 Pt1 P2 C1B -47.8(6) . .
C11 Pt1 P2 C1B 128.4(6) . .
P1 Pt1 P2 C1B -71.2(16) . .
Pt2 Pt1 P2 C1B -43.0(6) . .
C1 Pt1 P2 C31 -169.9(4) . .
C11 Pt1 P2 C31 6.3(4) . .
P1 Pt1 P2 C31 166.7(14) . .
Pt2 Pt1 P2 C31 -165.1(4) . .
C1 Pt1 P2 C21 77.0(5) . .
C11 Pt1 P2 C21 -106.8(5) . .
P1 Pt1 P2 C21 53.7(16) . .
Pt2 Pt1 P2 C21 81.9(5) . .
C1 Pt1 P2 C22' 65.2(5) . .
C11 Pt1 P2 C22' -118.6(5) . .
P1 Pt1 P2 C22' 41.8(16) . .
Pt2 Pt1 P2 C22' 70.0(4) . .
Pt1 C1 C2 C3 65(29) . .
P1 C1A C2A C3A -171.7(3) . .
P2 C1B C2B C3B -170.5(7) . .
P2 C1B C2B C3B' -153.1(11) . .
C8 Pt2 P3 C12A -50.9(2) . .
C61 Pt2 P3 C12A 127.4(2) . .
P4 Pt2 P3 C12A -17.4(10) . .
Pt1 Pt2 P3 C12A -45.33(19) . .
C8 Pt2 P3 C81 -171.2(2) . .
C61 Pt2 P3 C81 7.1(2) . .
P4 Pt2 P3 C81 -137.6(9) . .
Pt1 Pt2 P3 C81 -165.58(18) . .
C8 Pt2 P3 C71 70.1(2) . .
C61 Pt2 P3 C71 -111.6(2) . .
P4 Pt2 P3 C71 103.7(9) . .
Pt1 Pt2 P3 C71 75.73(17) . .
C1 C2 C3 C4 47(50) . .
C1A C2A C3A C4A 70.4(6) . .
C1B C2B C3B C3B' 162.8(11) . .
C1B C2B C3B C4B -157.8(9) . .
C3B' C2B C3B C4B 39.4(10) . .
C2B C3B C3B' C4B 127.6(11) . .
C4B C3B C3B' C2B -127.6(11) . .
C1B C2B C3B' C4B -78.1(19) . .
C3B C2B C3B' C4B -52.3(13) . .
C1B C2B C3B' C3B -25.8(16) . .
C8 Pt2 P4 C101 -75.7(2) . .
C61 Pt2 P4 C101 106.0(2) . .
P3 Pt2 P4 C101 -109.2(9) . .
Pt1 Pt2 P4 C101 -81.24(18) . .
C8 Pt2 P4 C91 164.2(2) . .
C61 Pt2 P4 C91 -14.1(2) . .
P3 Pt2 P4 C91 130.6(9) . .
Pt1 Pt2 P4 C91 158.62(17) . .
C8 Pt2 P4 C12B 44.5(2) . .
C61 Pt2 P4 C12B -133.7(2) . .
P3 Pt2 P4 C12B 11.0(9) . .
Pt1 Pt2 P4 C12B 38.98(17) . .
C2 C3 C4 C5 23(100) . .
C2A C3A C4A C5A -171.6(5) . .
C2B C3B' C4B C3B 44.0(10) . .
C3B C3B' C4B C5B -98.8(19) . .
C2B C3B' C4B C5B -55(2) . .
C2B C3B C4B C3B' -56.4(13) . .
C3B' C3B C4B C5B 132.5(16) . .
C2B C3B C4B C5B 76.0(14) . .
C3 C4 C5 C6 -67(100) . .
C3A C4A C5A C6A -178.3(5) . .
C3B' C4B C5B C6B 163(2) . .
C3B C4B C5B C6B 88.4(11) . .
C4 C5 C6 C7 -75(51) . .
C4A C5A C6A C7A -170.7(5) . .
C4B C5B C6B C7B -174.8(8) . .
C4B C5B C6B C7B' -112.6(14) . .
C5 C6 C7 C8 -47(45) . .
C5A C6A C7A C8A -174.6(5) . .
C5B C6B C7B C7B' 116.5(16) . .
C5B C6B C7B C8B 174.1(7) . .
C7B' C6B C7B C8B 57.6(15) . .
C8B C7B C7B' C6B -124.1(10) . .
C6B C7B C7B' C8B 124.1(10) . .
C5B C6B C7B' C7B -97.7(14) . .
C7B C6B C7B' C8B -46.9(9) . .
C5B C6B C7B' C8B -144.6(11) . .
C6 C7 C8 Pt2 14(34) . .
C61 Pt2 C8 C7 55(8) . .
P3 Pt2 C8 C7 119(5) . .
P4 Pt2 C8 C7 -60(5) . .
Pt1 Pt2 C8 C7 17(4) . .
C6A C7A C8A C9A -173.9(5) . .
C6B C7B C8B C9B -179.5(8) . .
C7B' C7B C8B C9B -121.9(15) . .
C6B C7B C8B C7B' -57.5(15) . .
C7B C7B' C8B C9B 85.1(15) . .
C6B C7B' C8B C9B 129.1(13) . .
C6B C7B' C8B C7B 44.0(9) . .
C7A C8A C9A C10A -172.4(4) . .
C7B C8B C9B C10B -162.4(7) . .
C7B' C8B C9B C10B 144.6(13) . .
C8B C9B C10B C11B -171.2(7) . .
C8A C9A C10A C11A -56.1(7) . .
C9B C10B C11B C12B 75.2(7) . .
C9A C10A C11A C12A -56.6(7) . .
C1 Pt1 C11 C16 2(3) . .
P2 Pt1 C11 C16 -73.7(4) . .
P1 Pt1 C11 C16 107.3(4) . .
Pt2 Pt1 C11 C16 18.3(11) . .
C1 Pt1 C11 C12 179(100) . .
P2 Pt1 C11 C12 103.5(4) . .
P1 Pt1 C11 C12 -75.5(4) . .
Pt2 Pt1 C11 C12 -164.4(6) . .
C10B C11B C12B P4 -172.6(4) . .
C101 P4 C12B C11B 179.9(4) . .
C91 P4 C12B C11B -71.7(4) . .
Pt2 P4 C12B C11B 53.7(4) . .
C10A C11A C12A P3 -154.1(4) . .
C81 P3 C12A C11A 84.7(4) . .
C71 P3 C12A C11A -167.4(4) . .
Pt2 P3 C12A C11A -41.7(5) . .
C16 C11 C12 F12 179.6(4) . .
Pt1 C11 C12 F12 2.2(7) . .
C16 C11 C12 C13 0.1(7) . .
Pt1 C11 C12 C13 -177.3(4) . .
F12 C12 C13 C14 -178.8(5) . .
C11 C12 C13 C14 0.7(9) . .
F12 C12 C13 F13 -0.5(8) . .
C11 C12 C13 F13 179.0(5) . .
C12 C13 C14 F14 179.7(5) . .
F13 C13 C14 F14 1.4(9) . .
C12 C13 C14 C15 0.4(9) . .
F13 C13 C14 C15 -177.9(5) . .
F14 C14 C15 F15 -2.4(8) . .
C13 C14 C15 F15 177.0(5) . .
F14 C14 C15 C16 178.5(5) . .
C13 C14 C15 C16 -2.1(8) . .
C12 C11 C16 F16 178.5(4) . .
Pt1 C11 C16 F16 -4.0(6) . .
C12 C11 C16 C15 -2.0(7) . .
Pt1 C11 C16 C15 175.5(4) . .
C14 C15 C16 F16 -177.4(5) . .
F15 C15 C16 F16 3.5(7) . .
C14 C15 C16 C11 3.0(8) . .
F15 C15 C16 C11 -176.1(5) . .
C21' P2 C21 C22' 78(4) . .
C1B P2 C21 C22' 48(4) . .
C31 P2 C21 C22' 163(3) . .
Pt1 P2 C21 C22' -77(3) . .
C1B P2 C21 C21' -29.5(14) . .
C31 P2 C21 C21' 85.0(13) . .
Pt1 P2 C21 C21' -154.3(12) . .
C22' P2 C21 C21' -78(4) . .
C21' P2 C21 C26 -22.7(13) . .
C1B P2 C21 C26 -52.2(14) . .
C31 P2 C21 C26 62.3(14) . .
Pt1 P2 C21 C26 -177.0(12) . .
C22' P2 C21 C26 -100(4) . .
C21' P2 C21 C22 151(2) . .
C1B P2 C21 C22 121.7(13) . .
C31 P2 C21 C22 -123.8(13) . .
Pt1 P2 C21 C22 -3.1(15) . .
C22' P2 C21 C22 74(3) . .
C21' P2 C21 C23' 41.9(17) . .
C1B P2 C21 C23' 12.4(19) . .
C31 P2 C21 C23' 126.9(17) . .
Pt1 P2 C21 C23' -112.4(17) . .
C22' P2 C21 C23' -36(3) . .
C21' C21 C22 C22' -21(3) . .
C26 C21 C22 C22' 61(2) . .
P2 C21 C22 C22' -114(3) . .
C23' C21 C22 C22' 34(2) . .
C22' C21 C22 C23 -66(3) . .
C21' C21 C22 C23 -87(3) . .
C26 C21 C22 C23 -5(2) . .
P2 C21 C22 C23 -179.9(12) . .
C23' C21 C22 C23 -31.6(14) . .
C22' C21 C22 C23' -34(2) . .
C21' C21 C22 C23' -56(3) . .
C26 C21 C22 C23' 26.2(12) . .
P2 C21 C22 C23' -148.3(14) . .
C22' C22 C23 C24 -20(2) . .
C21 C22 C23 C24 4(2) . .
C23' C22 C23 C24 -29.1(13) . .
C22' C22 C23 C23' 9.4(14) . .
C21 C22 C23 C23' 33.2(15) . .
C22 C23 C24 C25 1(2) . .
C23' C23 C24 C25 -34.3(13) . .
C22 C23 C24 C23' 35.2(15) . .
C22 C23 C24 C24' 22(2) . .
C23' C23 C24 C24' -13.4(10) . .
C23 C24 C25 C24' 99(2) . .
C23' C24 C25 C24' 55(2) . .
C23 C24 C25 C23' 44.8(16) . .
C24' C24 C25 C23' -55(2) . .
C23 C24 C25 C26 -4(2) . .
C23' C24 C25 C26 -48.8(14) . .
C24' C24 C25 C26 -103(3) . .
C23 C24 C25 C25' 50(6) . .
C23' C24 C25 C25' 6(5) . .
C24' C24 C25 C25' -49(5) . .
C24' C25 C26 C22' -112.2(17) . .
C23' C25 C26 C22' -28.4(14) . .
C24 C25 C26 C22' 22(2) . .
C25' C25 C26 C22' -144.7(16) . .
C24' C25 C26 C21' -81(4) . .
C23' C25 C26 C21' 2(4) . .
C24 C25 C26 C21' 53(5) . .
C25' C25 C26 C21' -114(4) . .
C24' C25 C26 C21 -132.1(19) . .
C23' C25 C26 C21 -48.3(17) . .
C24 C25 C26 C21 2(2) . .
C25' C25 C26 C21 -164.6(19) . .
C23' C25 C26 C24' 83.9(16) . .
C24 C25 C26 C24' 134(2) . .
C25' C25 C26 C24' -32.4(15) . .
C24' C25 C26 C26' 34(2) . .
C23' C25 C26 C26' 118(2) . .
C24 C25 C26 C26' 168.4(17) . .
C25' C25 C26 C26' 1.6(17) . .
C24' C25 C26 C25' 32.4(15) . .
C23' C25 C26 C25' 116.3(13) . .
C24 C25 C26 C25' 166.7(16) . .
C24' C25 C26 C23' -83.9(16) . .
C24 C25 C26 C23' 50.5(15) . .
C25' C25 C26 C23' -116.3(13) . .
C22' C21 C26 C25 51(3) . .
C21' C21 C26 C25 156.1(18) . .
C22 C21 C26 C25 2(2) . .
P2 C21 C26 C25 177.1(12) . .
C23' C21 C26 C25 35.5(13) . .
C21' C21 C26 C22' 105(3) . .
C22 C21 C26 C22' -49(2) . .
P2 C21 C26 C22' 126(3) . .
C23' C21 C26 C22' -16(3) . .
C22' C21 C26 C21' -105(3) . .
C22 C21 C26 C21' -153.7(19) . .
P2 C21 C26 C21' 21.0(11) . .
C23' C21 C26 C21' -120.7(14) . .
C22' C21 C26 C24' 8(4) . .
C21' C21 C26 C24' 113(2) . .
C22 C21 C26 C24' -41(3) . .
P2 C21 C26 C24' 133.7(18) . .
C23' C21 C26 C24' -7.9(18) . .
C22' C21 C26 C26' -119(3) . .
C21' C21 C26 C26' -14.6(14) . .
C22 C21 C26 C26' -168.3(13) . .
P2 C21 C26 C26' 6.4(16) . .
C23' C21 C26 C26' -135.2(14) . .
C22' C21 C26 C25' -97(3) . .
C21' C21 C26 C25' 8(3) . .
C22 C21 C26 C25' -146(2) . .
P2 C21 C26 C25' 29(3) . .
C23' C21 C26 C25' -113(3) . .
C22' C21 C26 C23' 16(3) . .
C21' C21 C26 C23' 120.7(14) . .
C22 C21 C26 C23' -33.1(14) . .
P2 C21 C26 C23' 141.6(12) . .
C26 C21 C21' C22' -73(2) . .
C22 C21 C21' C22' 18(2) . .
P2 C21 C21' C22' 127(2) . .
C23' C21 C21' C22' -33(2) . .
C22' C21 C21' C26' 95(3) . .
C26 C21 C21' C26' 21.1(18) . .
C22 C21 C21' C26' 113(3) . .
P2 C21 C21' C26' -139(2) . .
C23' C21 C21' C26' 62(2) . .
C22' C21 C21' C26 73(2) . .
C22 C21 C21' C26 92(3) . .
P2 C21 C21' C26 -159.6(11) . .
C23' C21 C21' C26 40.8(9) . .
C22' C21 C21' P2 -127(2) . .
C26 C21 C21' P2 159.6(11) . .
C22 C21 C21' P2 -109(3) . .
C23' C21 C21' P2 -159.6(8) . .
C25 C26 C21' C21 -66(4) . .
C22' C26 C21' C21 -29.4(13) . .
C24' C26 C21' C21 -123(2) . .
C26' C26 C21' C21 162.1(17) . .
C25' C26 C21' C21 -175.8(15) . .
C23' C26 C21' C21 -64.1(15) . .
C25 C26 C21' C22' -37(4) . .
C21 C26 C21' C22' 29.4(13) . .
C24' C26 C21' C22' -93(2) . .
C26' C26 C21' C22' -168.5(16) . .
C25' C26 C21' C22' -146.4(15) . .
C23' C26 C21' C22' -34.7(13) . .
C25 C26 C21' C26' 132(4) . .
C22' C26 C21' C26' 168.5(16) . .
C21 C26 C21' C26' -162.1(17) . .
C24' C26 C21' C26' 75.2(19) . .
C25' C26 C21' C26' 22.1(12) . .
C23' C26 C21' C26' 133.8(14) . .
C25 C26 C21' P2 -107(4) . .
C22' C26 C21' P2 -70(2) . .
C21 C26 C21' P2 -41(2) . .
C24' C26 C21' P2 -163.7(17) . .
C26' C26 C21' P2 121(2) . .
C25' C26 C21' P2 143.3(19) . .
C23' C26 C21' P2 -105(2) . .
C1B P2 C21' C21 153.2(13) . .
C31 P2 C21' C21 -101.9(12) . .
Pt1 P2 C21' C21 35.2(16) . .
C22' P2 C21' C21 21.9(12) . .
C1B P2 C21' C22' 131.2(12) . .
C31 P2 C21' C22' -123.8(12) . .
C21 P2 C21' C22' -21.9(12) . .
Pt1 P2 C21' C22' 13.3(16) . .
C1B P2 C21' C26' -67.0(16) . .
C31 P2 C21' C26' 37.9(17) . .
C21 P2 C21' C26' 140(2) . .
Pt1 P2 C21' C26' 175.0(12) . .
C22' P2 C21' C26' 162(2) . .
C1B P2 C21' C26 -170(2) . .
C31 P2 C21' C26 -65(2) . .
C21 P2 C21' C26 37.3(19) . .
Pt1 P2 C21' C26 72(2) . .
C22' P2 C21' C26 59(2) . .
C21' C21 C22' C22 171.3(12) . .
C26 C21 C22' C22 -123.8(14) . .
P2 C21 C22' C22 113(2) . .
C23' C21 C22' C22 -101(4) . .
C26 C21 C22' C21' 64.9(13) . .
C22 C21 C22' C21' -171.3(12) . .
P2 C21 C22' C21' -58(2) . .
C23' C21 C22' C21' 88(4) . .
C21' C21 C22' C26 -64.9(13) . .
C22 C21 C22' C26 123.8(14) . .
P2 C21 C22' C26 -123(2) . .
C23' C21 C22' C26 23(4) . .
C21' C21 C22' C23' -88(4) . .
C26 C21 C22' C23' -23(4) . .
C22 C21 C22' C23' 101(4) . .
P2 C21 C22' C23' -146(2) . .
C21' C21 C22' P2 58(2) . .
C26 C21 C22' P2 123(2) . .
C22 C21 C22' P2 -113(2) . .
C23' C21 C22' P2 146(2) . .
C23 C22 C22' C21 125(2) . .
C23' C22 C22' C21 136(3) . .
C23 C22 C22' C21' 139(3) . .
C21 C22 C22' C21' 14(2) . .
C23' C22 C22' C21' 150(4) . .
C23 C22 C22' C26 46(2) . .
C21 C22 C22' C26 -79(3) . .
C23' C22 C22' C26 56.7(13) . .
C23 C22 C22' C23' -11.1(16) . .
C21 C22 C22' C23' -136(3) . .
C23 C22 C22' P2 166.1(10) . .
C21 C22 C22' P2 41.2(19) . .
C23' C22 C22' P2 177.2(15) . .
C26' C21' C22' C21 -107(3) . .
C26 C21' C22' C21 -94(3) . .
P2 C21' C22' C21 55(2) . .
C21 C21' C22' C22 -18(3) . .
C26' C21' C22' C22 -125(3) . .
C26 C21' C22' C22 -112(3) . .
P2 C21' C22' C22 37(4) . .
C21 C21' C22' C26 94(3) . .
C26' C21' C22' C26 -13.0(18) . .
P2 C21' C22' C26 149.0(13) . .
C21 C21' C22' C23' 130(3) . .
C26' C21' C22' C23' 23(3) . .
C26 C21' C22' C23' 36.0(13) . .
P2 C21' C22' C23' -174.9(11) . .
C21 C21' C22' P2 -55(2) . .
C26' C21' C22' P2 -162(2) . .
C26 C21' C22' P2 -149.0(13) . .
C25 C26 C22' C21 -137(3) . .
C21' C26 C22' C21 56(2) . .
C24' C26 C22' C21 -174(3) . .
C26' C26 C22' C21 66(3) . .
C25' C26 C22' C21 122(3) . .
C23' C26 C22' C21 -162(3) . .
C25 C26 C22' C22 -47(2) . .
C21' C26 C22' C22 146(2) . .
C21 C26 C22' C22 90(3) . .
C24' C26 C22' C22 -84(2) . .
C26' C26 C22' C22 156.1(15) . .
C25' C26 C22' C22 -147.8(19) . .
C23' C26 C22' C22 -71.8(17) . .
C25 C26 C22' C21' 166.7(15) . .
C21 C26 C22' C21' -56(2) . .
C24' C26 C22' C21' 129.6(16) . .
C26' C26 C22' C21' 9.9(13) . .
C25' C26 C22' C21' 66(2) . .
C23' C26 C22' C21' 142.0(15) . .
C25 C26 C22' C23' 24.7(12) . .
C21' C26 C22' C23' -142.0(15) . .
C21 C26 C22' C23' 162(3) . .
C24' C26 C22' C23' -12.4(14) . .
C26' C26 C22' C23' -132.1(14) . .
C25' C26 C22' C23' -76(2) . .
C25 C26 C22' P2 -172.1(10) . .
C21' C26 C22' P2 21.2(9) . .
C21 C26 C22' P2 -35(2) . .
C24' C26 C22' P2 150.8(11) . .
C26' C26 C22' P2 31.1(13) . .
C25' C26 C22' P2 87(2) . .
C23' C26 C22' P2 163.2(12) . .
C21' P2 C22' C21 -84(3) . .
C1B P2 C22' C21 -135(3) . .
C31 P2 C22' C21 -19(4) . .
Pt1 P2 C22' C21 106(3) . .
C21' P2 C22' C22 -161(2) . .
C1B P2 C22' C22 147.6(12) . .
C31 P2 C22' C22 -96.1(12) . .
C21 P2 C22' C22 -77(4) . .
Pt1 P2 C22' C22 28.5(13) . .
C1B P2 C22' C21' -51.0(13) . .
C31 P2 C22' C21' 65.3(13) . .
C21 P2 C22' C21' 84(3) . .
Pt1 P2 C22' C21' -170.2(12) . .
C21' P2 C22' C26 -27.6(12) . .
C1B P2 C22' C26 -78.6(11) . .
C31 P2 C22' C26 37.7(12) . .
C21 P2 C22' C26 56(3) . .
Pt1 P2 C22' C26 162.2(10) . .
C21' P2 C22' C23' 12(3) . .
C1B P2 C22' C23' -39(3) . .
C31 P2 C22' C23' 77(3) . .
C21 P2 C22' C23' 96(4) . .
Pt1 P2 C22' C23' -159(3) . .
C24 C25 C23' C24' 143.6(17) . .
C26 C25 C23' C24' -79.6(14) . .
C25' C25 C23' C24' -35.1(12) . .
C24' C25 C23' C22' 107.2(17) . .
C24 C25 C23' C22' -109.2(14) . .
C26 C25 C23' C22' 27.6(13) . .
C25' C25 C23' C22' 72.1(14) . .
C24' C25 C23' C24 -143.6(17) . .
C26 C25 C23' C24 136.7(12) . .
C25' C25 C23' C24 -178.8(12) . .
C24' C25 C23' C26 79.6(14) . .
C24 C25 C23' C26 -136.7(12) . .
C25' C25 C23' C26 44.5(9) . .
C24' C25 C23' C23 -170.6(14) . .
C24 C25 C23' C23 -26.9(9) . .
C26 C25 C23' C23 109.8(10) . .
C25' C25 C23' C23 154.3(8) . .
C24' C25 C23' C22 148.9(14) . .
C24 C25 C23' C22 -67.5(11) . .
C26 C25 C23' C22 69.2(11) . .
C25' C25 C23' C22 113.8(10) . .
C24' C25 C23' C21 106.4(15) . .
C24 C25 C23' C21 -109.9(11) . .
C26 C25 C23' C21 26.8(10) . .
C25' C25 C23' C21 71.3(10) . .
C21 C22' C23' C25 -4(5) . .
C22 C22' C23' C25 99.6(16) . .
C21' C22' C23' C25 -65(2) . .
C26 C22' C23' C25 -28.9(14) . .
P2 C22' C23' C25 -74(3) . .
C21 C22' C23' C24' 39(5) . .
C22 C22' C23' C24' 141.7(16) . .
C21' C22' C23' C24' -23(2) . .
C26 C22' C23' C24' 13.3(15) . .
P2 C22' C23' C24' -32(4) . .
C21 C22' C23' C24 -65(5) . .
C22 C22' C23' C24 38.0(17) . .
C21' C22' C23' C24 -126.7(16) . .
C26 C22' C23' C24 -90.5(14) . .
P2 C22' C23' C24 -135(3) . .
C21 C22' C23' C26 25(4) . .
C22 C22' C23' C26 128.5(15) . .
C21' C22' C23' C26 -36.3(14) . .
P2 C22' C23' C26 -45(3) . .
C21 C22' C23' C23 -95(4) . .
C22 C22' C23' C23 8.1(12) . .
C21' C22' C23' C23 -156.6(15) . .
C26 C22' C23' C23 -120.4(11) . .
P2 C22' C23' C23 -165(3) . .
C21 C22' C23' C22 -103(5) . .
C21' C22' C23' C22 -165(2) . .
C26 C22' C23' C22 -128.5(15) . .
P2 C22' C23' C22 -173(4) . .
C22 C22' C23' C21 103(5) . .
C21' C22' C23' C21 -62(4) . .
C26 C22' C23' C21 -25(4) . .
P2 C22' C23' C21 -70(4) . .
C23 C24 C23' C25 -141.2(14) . .
C24' C24 C23' C25 21.8(10) . .
C25 C24 C23' C24' -21.8(10) . .
C23 C24 C23' C24' -163.0(12) . .
C25 C24 C23' C22' 98.1(15) . .
C23 C24 C23' C22' -43.1(14) . .
C24' C24 C23' C22' 119.9(16) . .
C25 C24 C23' C26 38.3(11) . .
C23 C24 C23' C26 -102.9(11) . .
C24' C24 C23' C26 60.1(10) . .
C25 C24 C23' C23 141.2(14) . .
C24' C24 C23' C23 163.0(12) . .
C25 C24 C23' C22 120.8(12) . .
C23 C24 C23' C22 -20.4(9) . .
C24' C24 C23' C22 142.6(12) . .
C25 C24 C23' C21 85.9(12) . .
C23 C24 C23' C21 -55.3(11) . .
C24' C24 C23' C21 107.7(13) . .
C22' C26 C23' C25 148.9(15) . .
C21' C26 C23' C25 -179.0(15) . .
C21 C26 C23' C25 141.4(14) . .
C24' C26 C23' C25 -44.6(10) . .
C26' C26 C23' C25 -122.5(17) . .
C25' C26 C23' C25 -67.1(13) . .
C25 C26 C23' C24' 44.6(10) . .
C22' C26 C23' C24' -166.5(15) . .
C21' C26 C23' C24' -134.4(15) . .
C21 C26 C23' C24' -174.0(14) . .
C26' C26 C23' C24' -77.9(17) . .
C25' C26 C23' C24' -22.5(12) . .
C25 C26 C23' C22' -148.9(15) . .
C21' C26 C23' C22' 32.1(13) . .
C21 C26 C23' C22' -7.5(13) . .
C24' C26 C23' C22' 166.5(15) . .
C26' C26 C23' C22' 88.6(17) . .
C25' C26 C23' C22' 144.1(14) . .
C25 C26 C23' C24 -36.0(11) . .
C22' C26 C23' C24 112.8(13) . .
C21' C26 C23' C24 144.9(12) . .
C21 C26 C23' C24 105.4(12) . .
C24' C26 C23' C24 -80.6(12) . .
C26' C26 C23' C24 -158.6(13) . .
C25' C26 C23' C24 -103.1(12) . .
C25 C26 C23' C23 -84.2(12) . .
C22' C26 C23' C23 64.7(11) . .
C21' C26 C23' C23 96.8(13) . .
C21 C26 C23' C23 57.2(11) . .
C24' C26 C23' C23 -128.8(13) . .
C26' C26 C23' C23 153.3(13) . .
C25' C26 C23' C23 -151.2(10) . .
C25 C26 C23' C22 -119.4(12) . .
C22' C26 C23' C22 29.5(10) . .
C21' C26 C23' C22 61.6(12) . .
C21 C26 C23' C22 22.0(10) . .
C24' C26 C23' C22 -164.0(12) . .
C26' C26 C23' C22 118.1(15) . .
C25' C26 C23' C22 173.5(10) . .
C25 C26 C23' C21 -141.4(14) . .
C22' C26 C23' C21 7.5(13) . .
C21' C26 C23' C21 39.6(10) . .
C24' C26 C23' C21 174.0(14) . .
C26' C26 C23' C21 96.1(16) . .
C25' C26 C23' C21 151.5(15) . .
C24 C23 C23' C25 31.4(11) . .
C22 C23 C23' C25 -117.9(12) . .
C24 C23 C23' C24' 23.4(16) . .
C22 C23 C23' C24' -126.0(17) . .
C24 C23 C23' C22' 141.9(13) . .
C22 C23 C23' C22' -7.4(11) . .
C22 C23 C23' C24 -149.3(13) . .
C24 C23 C23' C26 92.0(12) . .
C22 C23 C23' C26 -57.3(11) . .
C24 C23 C23' C22 149.3(13) . .
C24 C23 C23' C21 129.3(11) . .
C22 C23 C23' C21 -20.0(9) . .
C22' C22 C23' C25 -96.3(17) . .
C23 C22 C23' C25 71.9(13) . .
C21 C22 C23' C25 -78.3(14) . .
C22' C22 C23' C24' -64(2) . .
C23 C22 C23' C24' 104(2) . .
C21 C22 C23' C24' -46(2) . .
C23 C22 C23' C22' 168.2(17) . .
C21 C22 C23' C22' 18.1(13) . .
C22' C22 C23' C24 -146.6(16) . .
C23 C22 C23' C24 21.6(10) . .
C21 C22 C23' C24 -128.5(12) . .
C22' C22 C23' C26 -41.1(13) . .
C23 C22 C23' C26 127.1(12) . .
C21 C22 C23' C26 -23.1(10) . .
C22' C22 C23' C23 -168.2(17) . .
C21 C22 C23' C23 -150.2(13) . .
C22' C22 C23' C21 -18.1(13) . .
C23 C22 C23' C21 150.2(13) . .
C22' C21 C23' C25 177(5) . .
C21' C21 C23' C25 -86.6(16) . .
C26 C21 C23' C25 -33.4(13) . .
C22 C21 C23' C25 113.5(14) . .
P2 C21 C23' C25 -121.8(18) . .
C22' C21 C23' C24' -144(5) . .
C21' C21 C23' C24' -47.7(17) . .
C26 C21 C23' C24' 5.5(13) . .
C22 C21 C23' C24' 152.4(14) . .
P2 C21 C23' C24' -83(2) . .
C21' C21 C23' C22' 97(5) . .
C26 C21 C23' C22' 150(5) . .
C22 C21 C23' C22' -63(4) . .
P2 C21 C23' C22' 62(4) . .
C22' C21 C23' C24 120(5) . .
C21' C21 C23' C24 -143.4(14) . .
C26 C21 C23' C24 -90.2(13) . .
C22 C21 C23' C24 56.7(12) . .
P2 C21 C23' C24 -178.5(14) . .
C22' C21 C23' C26 -150(5) . .
C21' C21 C23' C26 -53.2(14) . .
C22 C21 C23' C26 146.9(14) . .
P2 C21 C23' C26 -88.4(19) . .
C22' C21 C23' C23 83(4) . .
C21' C21 C23' C23 179.9(13) . .
C26 C21 C23' C23 -126.9(12) . .
C22 C21 C23' C23 20.0(9) . .
P2 C21 C23' C23 144.7(17) . .
C22' C21 C23' C22 63(4) . .
C21' C21 C23' C22 159.9(17) . .
C26 C21 C23' C22 -146.9(14) . .
P2 C21 C23' C22 125(2) . .
C23' C25 C24' C25' -112.4(16) . .
C24 C25 C24' C25' -164.5(15) . .
C26 C25 C24' C25' -42.4(15) . .
C24 C25 C24' C23' -52.1(19) . .
C26 C25 C24' C23' 70.0(9) . .
C25' C25 C24' C23' 112.4(16) . .
C23' C25 C24' C26 -70.0(9) . .
C24 C25 C24' C26 -122(2) . .
C25' C25 C24' C26 42.4(15) . .
C23' C25 C24' C24 52.1(19) . .
C26 C25 C24' C24 122(2) . .
C25' C25 C24' C24 164.5(15) . .
C22' C23' C24' C25 -90.6(18) . .
C24 C23' C24' C25 29.5(14) . .
C26 C23' C24' C25 -78.0(15) . .
C23 C23' C24' C25 12.8(19) . .
C22 C23' C24' C25 -51(2) . .
C21 C23' C24' C25 -82.4(16) . .
C25 C23' C24' C25' 107(2) . .
C22' C23' C24' C25' 16(2) . .
C24 C23' C24' C25' 136.4(17) . .
C26 C23' C24' C25' 28.9(16) . .
C23 C23' C24' C25' 119.7(18) . .
C22 C23' C24' C25' 56(3) . .
C21 C23' C24' C25' 24(2) . .
C25 C23' C24' C26 78.0(15) . .
C22' C23' C24' C26 -12.6(14) . .
C24 C23' C24' C26 107.4(12) . .
C23 C23' C24' C26 90.8(16) . .
C22 C23' C24' C26 26.6(19) . .
C21 C23' C24' C26 -4.5(11) . .
C25 C23' C24' C24 -29.5(14) . .
C22' C23' C24' C24 -120.0(17) . .
C26 C23' C24' C24 -107.4(12) . .
C23 C23' C24' C24 -16.6(11) . .
C22 C23' C24' C24 -80.8(19) . .
C21 C23' C24' C24 -111.9(13) . .
C22' C26 C24' C25 81.8(19) . .
C21' C26 C24' C25 148(2) . .
C21 C26 C24' C25 78(3) . .
C26' C26 C24' C25 -157.0(16) . .
C25' C26 C24' C25 -138.7(18) . .
C23' C26 C24' C25 68.6(15) . .
C25 C26 C24' C25' 138.7(18) . .
C22' C26 C24' C25' -139.5(16) . .
C21' C26 C24' C25' -73.1(19) . .
C21 C26 C24' C25' -143(2) . .
C26' C26 C24' C25' -18.3(12) . .
C23' C26 C24' C25' -152.7(15) . .
C25 C26 C24' C23' -68.6(15) . .
C22' C26 C24' C23' 13.2(15) . .
C21' C26 C24' C23' 79.6(19) . .
C21 C26 C24' C23' 10(2) . .
C26' C26 C24' C23' 134.4(14) . .
C25' C26 C24' C23' 152.7(15) . .
C25 C26 C24' C24 -23.2(12) . .
C22' C26 C24' C24 58.6(14) . .
C21' C26 C24' C24 125.0(18) . .
C21 C26 C24' C24 55(2) . .
C26' C26 C24' C24 179.8(11) . .
C25' C26 C24' C24 -161.9(12) . .
C23' C26 C24' C24 45.4(9) . .
C23 C24 C24' C25 -91(3) . .
C23' C24 C24' C25 -111(2) . .
C25 C24 C24' C25' 24(2) . .
C23 C24 C24' C25' -67(2) . .
C23' C24 C24' C25' -87(2) . .
C25 C24 C24' C23' 111(3) . .
C23 C24 C24' C23' 19.5(14) . .
C25 C24 C24' C26 52(2) . .
C23 C24 C24' C26 -39.1(15) . .
C23' C24 C24' C26 -58.5(11) . .
C25 C24' C25' C26' 65(2) . .
C23' C24' C25' C26' -7(3) . .
C26 C24' C25' C26' 21.5(15) . .
C24 C24' C25' C26' 53(3) . .
C25 C24' C25' C26 43.6(17) . .
C23' C24' C25' C26 -28.4(15) . .
C24 C24' C25' C26 31.5(18) . .
C23' C24' C25' C25 -72.0(19) . .
C26 C24' C25' C25 -43.6(17) . .
C24 C24' C25' C25 -12.0(12) . .
C25 C26 C25' C24' -22.9(11) . .
C22' C26 C25' C24' 85(2) . .
C21' C26 C25' C24' 136.6(14) . .
C21 C26 C25' C24' 131(3) . .
C26' C26 C25' C24' 158.4(15) . .
C23' C26 C25' C24' 23.1(12) . .
C25 C26 C25' C26' 178.7(13) . .
C22' C26 C25' C26' -73(2) . .
C21' C26 C25' C26' -21.8(12) . .
C21 C26 C25' C26' -28(3) . .
C24' C26 C25' C26' -158.4(15) . .
C23' C26 C25' C26' -135.3(13) . .
C22' C26 C25' C25 108(2) . .
C21' C26 C25' C25 159.5(15) . .
C21 C26 C25' C25 154(3) . .
C24' C26 C25' C25 22.9(11) . .
C26' C26 C25' C25 -178.7(13) . .
C23' C26 C25' C25 46.0(9) . .
C23' C25 C25' C24' 65.9(19) . .
C24 C25 C25' C24' 60(5) . .
C26 C25 C25' C24' 123(2) . .
C24' C25 C25' C26' -124(2) . .
C23' C25 C25' C26' -58.0(15) . .
C24 C25 C25' C26' -63(6) . .
C26 C25 C25' C26' -1.2(12) . .
C24' C25 C25' C26 -123(2) . .
C23' C25 C25' C26 -56.8(12) . .
C24 C25 C25' C26 -62(5) . .
C21 C21' C26' C25' -49(3) . .
C22' C21' C26' C25' -14(3) . .
C26 C21' C26' C25' -27.1(15) . .
P2 C21' C26' C25' -172.2(13) . .
C21 C21' C26' C26 -21.5(18) . .
C22' C21' C26' C26 12.7(18) . .
P2 C21' C26' C26 -145.1(17) . .
C24' C25' C26' C21' 5(2) . .
C26 C25' C26' C21' 26.2(15) . .
C25 C25' C26' C21' 27.2(19) . .
C24' C25' C26' C26 -21.7(15) . .
C25 C25' C26' C26 1.0(10) . .
C25 C26 C26' C21' -156(2) . .
C22' C26 C26' C21' -10.0(13) . .
C21 C26 C26' C21' 12.6(12) . .
C24' C26 C26' C21' -135.8(14) . .
C25' C26 C26' C21' -153.8(15) . .
C23' C26 C26' C21' -78.4(17) . .
C25 C26 C26' C25' -2(2) . .
C22' C26 C26' C25' 143.8(15) . .
C21' C26 C26' C25' 153.8(15) . .
C21 C26 C26' C25' 166.5(14) . .
C24' C26 C26' C25' 18.0(12) . .
C23' C26 C26' C25' 75.4(16) . .
C21' P2 C31 C32 73.7(7) . .
C1B P2 C31 C32 160.2(7) . .
C21 P2 C31 C32 39.9(7) . .
Pt1 P2 C31 C32 -73.2(5) . .
C22' P2 C31 C32 43.8(7) . .
C21' P2 C31 C36 -111.7(8) . .
C1B P2 C31 C36 -25.1(8) . .
C21 P2 C31 C36 -145.5(7) . .
Pt1 P2 C31 C36 101.5(5) . .
C22' P2 C31 C36 -141.6(7) . .
C36 C31 C32 C33 -0.9(9) . .
P2 C31 C32 C33 174.0(4) . .
C31 C32 C33 C34 -0.5(9) . .
C32 C33 C34 C35 1.4(9) . .
C33 C34 C35 C36 -1.0(10) . .
C32 C31 C36 C35 1.4(10) . .
P2 C31 C36 C35 -173.2(5) . .
C34 C35 C36 C31 -0.5(11) . .
C51 P1 C41 C46 0.4(5) . .
C1A P1 C41 C46 -110.7(4) . .
Pt1 P1 C41 C46 125.1(4) . .
C51 P1 C41 C42 -178.6(4) . .
C1A P1 C41 C42 70.2(4) . .
Pt1 P1 C41 C42 -54.0(4) . .
C46 C41 C42 C43 1.9(7) . .
P1 C41 C42 C43 -179.0(4) . .
C41 C42 C43 C44 -1.2(7) . .
C42 C43 C44 C45 0.0(8) . .
C43 C44 C45 C46 0.6(9) . .
C44 C45 C46 C41 0.1(8) . .
C42 C41 C46 C45 -1.3(7) . .
P1 C41 C46 C45 179.6(4) . .
C1A P1 C51 C52 27.1(5) . .
C41 P1 C51 C52 -83.2(5) . .
Pt1 P1 C51 C52 149.6(4) . .
C1A P1 C51 C56 -155.3(5) . .
C41 P1 C51 C56 94.4(5) . .
Pt1 P1 C51 C56 -32.8(5) . .
C56 C51 C52 C53 -1.5(9) . .
P1 C51 C52 C53 176.1(5) . .
C51 C52 C53 C54 0.7(10) . .
C52 C53 C54 C55 0.2(12) . .
C53 C54 C55 C56 -0.2(13) . .
C54 C55 C56 C51 -0.7(12) . .
C52 C51 C56 C55 1.5(10) . .
P1 C51 C56 C55 -176.2(6) . .
C8 Pt2 C61 C66 -13(5) . .
P3 Pt2 C61 C66 -76.3(3) . .
P4 Pt2 C61 C66 102.3(3) . .
Pt1 Pt2 C61 C66 16.5(11) . .
C8 Pt2 C61 C62 163(5) . .
P3 Pt2 C61 C62 98.9(4) . .
P4 Pt2 C61 C62 -82.5(4) . .
Pt1 Pt2 C61 C62 -168.3(6) . .
C66 C61 C62 F62 176.9(4) . .
Pt2 C61 C62 F62 1.4(6) . .
C66 C61 C62 C63 -0.2(7) . .
Pt2 C61 C62 C63 -175.8(4) . .
F62 C62 C63 F63 2.0(8) . .
C61 C62 C63 F63 179.3(5) . .
F62 C62 C63 C64 -177.1(5) . .
C61 C62 C63 C64 0.1(8) . .
F63 C63 C64 F64 -0.1(8) . .
C62 C63 C64 F64 179.0(5) . .
F63 C63 C64 C65 -178.7(5) . .
C62 C63 C64 C65 0.4(8) . .
F64 C64 C65 F65 -0.1(8) . .
C63 C64 C65 F65 178.5(5) . .
F64 C64 C65 C66 -179.4(5) . .
C63 C64 C65 C66 -0.8(8) . .
C62 C61 C66 F66 -179.4(4) . .
Pt2 C61 C66 F66 -3.8(6) . .
C62 C61 C66 C65 -0.2(6) . .
Pt2 C61 C66 C65 175.4(3) . .
F65 C65 C66 F66 0.7(7) . .
C64 C65 C66 F66 180.0(4) . .
F65 C65 C66 C61 -178.6(4) . .
C64 C65 C66 C61 0.7(7) . .
C12A P3 C71 C76 132.1(5) . .
C81 P3 C71 C76 -118.9(5) . .
Pt2 P3 C71 C76 6.9(5) . .
C12A P3 C71 C72 -49.2(5) . .
C81 P3 C71 C72 59.9(4) . .
Pt2 P3 C71 C72 -174.4(4) . .
C76 C71 C72 C73 -0.6(8) . .
P3 C71 C72 C73 -179.3(5) . .
C71 C72 C73 C74 0.0(10) . .
C72 C73 C74 C75 1.1(12) . .
C73 C74 C75 C76 -1.5(12) . .
C72 C71 C76 C75 0.2(9) . .
P3 C71 C76 C75 178.9(5) . .
C74 C75 C76 C71 0.8(11) . .
C12A P3 C81 C82 -25.6(4) . .
C71 P3 C81 C82 -135.7(4) . .
Pt2 P3 C81 C82 99.4(4) . .
C12A P3 C81 C86 160.0(4) . .
C71 P3 C81 C86 49.9(4) . .
Pt2 P3 C81 C86 -75.0(4) . .
C86 C81 C82 C83 1.5(7) . .
P3 C81 C82 C83 -173.0(4) . .
C81 C82 C83 C84 -0.8(8) . .
C82 C83 C84 C85 -0.2(9) . .
C83 C84 C85 C86 0.6(9) . .
C82 C81 C86 C85 -1.1(7) . .
P3 C81 C86 C85 173.6(4) . .
C84 C85 C86 C81 0.0(8) . .
C101 P4 C91 C92 -2.4(5) . .
C12B P4 C91 C92 -111.8(4) . .
Pt2 P4 C91 C92 124.2(4) . .
C101 P4 C91 C96 178.0(4) . .
C12B P4 C91 C96 68.7(4) . .
Pt2 P4 C91 C96 -55.4(4) . .
C96 C91 C92 C93 -0.9(8) . .
P4 C91 C92 C93 179.5(4) . .
C91 C92 C93 C94 -0.1(9) . .
C92 C93 C94 C95 1.6(10) . .
C93 C94 C95 C96 -2.0(9) . .
C94 C95 C96 C91 0.9(8) . .
C92 C91 C96 C95 0.6(7) . .
P4 C91 C96 C95 -179.9(4) . .
C91 P4 C101 C102 -90.2(4) . .
C12B P4 C101 C102 19.1(5) . .
Pt2 P4 C101 C102 143.6(4) . .
C91 P4 C101 C106 82.6(5) . .
C12B P4 C101 C106 -168.1(5) . .
Pt2 P4 C101 C106 -43.6(5) . .
C106 C101 C102 C103 0.1(8) . .
P4 C101 C102 C103 173.0(4) . .
C101 C102 C103 C104 -1.5(10) . .
C102 C103 C104 C105 0.9(12) . .
C103 C104 C105 C106 1.2(14) . .
C104 C105 C106 C101 -2.7(13) . .
C102 C101 C106 C105 2.0(10) . .
P4 C101 C106 C105 -171.2(7) . .
Cl31 Cl32 C300 C300 -110(5) . 2_564
C300 C300 Cl31 Cl32 160(2) 2_564 .
