#------------------------------------------------------------------------------
#$Date: 2016-03-21 19:15:46 +0200 (Mon, 21 Mar 2016) $
#$Revision: 178842 $
#$URL: svn://www.crystallography.net/cod/cif/4/10/96/4109607.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4109607
loop_
_publ_author_name
'Jürgen Stahl'
'Wolfgang Mohr'
'Laura de Quadras'
'Thomas B. Peters'
'James C. Bohling'
'José Miguel Martín-Alvarez'
'Gareth R. Owen'
'Frank Hampel'
'John A. Gladysz'
_publ_section_title
;
 sp Carbon Chains Surrounded by sp3 Carbon Double Helices:
 Coordination-Driven Self-Assembly of Wirelike Pt(C\\tbC)nPt Moieties That
 Are Spanned by Two P(CH2)mP Linkages
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              8282
_journal_page_last               8295
_journal_paper_doi               10.1021/ja0716103
_journal_volume                  129
_journal_year                    2007
_chemical_formula_sum            'C108.67 H113.33 Cl1.33 F10 P4 Pt2'
_chemical_formula_weight         2170.65
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                89.0910(10)
_cell_angle_beta                 82.5860(10)
_cell_angle_gamma                83.3660(10)
_cell_formula_units_Z            3
_cell_length_a                   12.1498(3)
_cell_length_b                   23.1843(6)
_cell_length_c                   26.5928(8)
_cell_measurement_reflns_used    19422
_cell_measurement_temperature    173(2)
_cell_volume                     7378.4(3)
_computing_cell_refinement       DENZO-SMN
_computing_data_collection       'Nonius Collect'
_computing_data_reduction        DENZO-SMN
_computing_molecular_graphics    'SHELXTL NT 5.1'
_computing_publication_material  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      173(2)
_diffrn_detector_area_resol_mean 9
_diffrn_measured_fraction_theta_full 0.988
_diffrn_measured_fraction_theta_max 0.988
_diffrn_measurement_device_type  'Nonius KappaCCD'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus rotating anode'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0933
_diffrn_reflns_av_sigmaI/netI    0.1377
_diffrn_reflns_limit_h_max       13
_diffrn_reflns_limit_h_min       -13
_diffrn_reflns_limit_k_max       25
_diffrn_reflns_limit_k_min       -25
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            36790
_diffrn_reflns_theta_full        23.27
_diffrn_reflns_theta_max         23.27
_diffrn_reflns_theta_min         2.25
_exptl_absorpt_coefficient_mu    3.008
_exptl_absorpt_correction_T_max  0.8642
_exptl_absorpt_correction_T_min  0.4656
_exptl_absorpt_correction_type   empirical
_exptl_absorpt_process_details   Scalepack
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.466
_exptl_crystal_description       plate
_exptl_crystal_F_000             3282
_exptl_crystal_size_max          0.30
_exptl_crystal_size_mid          0.30
_exptl_crystal_size_min          0.05
_refine_diff_density_max         1.344
_refine_diff_density_min         -1.259
_refine_diff_density_rms         0.151
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.100
_refine_ls_hydrogen_treatment    'riding model'
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1432
_refine_ls_number_reflns         20990
_refine_ls_number_restraints     2
_refine_ls_restrained_S_all      1.100
_refine_ls_R_factor_all          0.1524
_refine_ls_R_factor_gt           0.0757
_refine_ls_shift/su_max          0.490
_refine_ls_shift/su_mean         0.023
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0417P)²+58.5057P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1467
_refine_ls_wR_factor_ref         0.1781
_reflns_number_gt                12158
_reflns_number_total             20990
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ja0716103si20070411_100958.cif
_cod_data_source_block           wm08
_cod_database_code               4109607
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Pt1 Pt -0.56739(5) 0.18896(2) 0.53905(2) 0.04202(17) Uani 1 1 d .
P1 P -0.7171(3) 0.18037(17) 0.60000(14) 0.0452(10) Uani 1 1 d .
C1 C -0.6717(11) 0.1898(6) 0.4884(5) 0.043(4) Uani 1 1 d .
C1A C -0.7948(13) 0.1187(7) 0.5878(6) 0.060(4) Uani 1 1 d .
C2A C -0.7154(17) 0.0647(9) 0.5719(8) 0.0938(16) Uani 1 1 d .
H2AA H -0.6666 0.0521 0.5994 0.113 Uiso 1 1 d R
H2AB H -0.6651 0.0710 0.5430 0.113 Uiso 1 1 d R
C3A C -0.7812(17) 0.0143(9) 0.5618(8) 0.0938(16) Uani 1 1 d .
H3AA H -0.8315 0.0089 0.5925 0.113 Uiso 1 1 d R
H3AB H -0.7291 -0.0222 0.5588 0.113 Uiso 1 1 d R
C4A C -0.8441(17) 0.0212(9) 0.5183(7) 0.0938(16) Uani 1 1 d .
H4AA H -0.8954 0.0532 0.5224 0.113 Uiso 1 1 d R
H4AB H -0.8834 -0.0137 0.5164 0.113 Uiso 1 1 d R
C5A C -0.7772(17) 0.0247(9) 0.4684(7) 0.0938(16) Uani 1 1 d .
H5AA H -0.7142 -0.0081 0.4639 0.113 Uiso 1 1 d R
H5AB H -0.7432 0.0595 0.4652 0.113 Uiso 1 1 d R
C6A C -0.8567(17) 0.0211(9) 0.4274(7) 0.0938(16) Uani 1 1 d .
H6AA H -0.9071 0.0543 0.4274 0.113 Uiso 1 1 d R
H6AB H -0.8950 -0.0132 0.4340 0.113 Uiso 1 1 d R
C7A C -0.7960(17) 0.0148(9) 0.3784(7) 0.0938(16) Uani 1 1 d .
H7AA H -0.7408 -0.0237 0.3838 0.113 Uiso 1 1 d R
H7AB H -0.7549 0.0433 0.3767 0.113 Uiso 1 1 d R
C8A C -0.8717(17) 0.0043(9) 0.3349(8) 0.0938(16) Uani 1 1 d .
H8AA H -0.8212 0.0052 0.3033 0.113 Uiso 1 1 d R
H8AB H -0.9250 0.0378 0.3350 0.113 Uiso 1 1 d R
C9A C -0.9311(17) -0.0459(9) 0.3344(8) 0.0938(16) Uani 1 1 d .
H9AA H -0.9865 -0.0451 0.3639 0.113 Uiso 1 1 d R
H9AB H -0.8756 -0.0804 0.3406 0.113 Uiso 1 1 d R
C10A C -0.9797(17) -0.0549(9) 0.2855(8) 0.0938(16) Uani 1 1 d .
H10A H -1.0160 -0.0903 0.2869 0.113 Uiso 1 1 d R
H10B H -0.9213 -0.0590 0.2570 0.113 Uiso 1 1 d R
C11A C -1.0625(17) -0.0073(9) 0.2766(8) 0.0938(16) Uani 1 1 d .
H11A H -1.0238 0.0298 0.2745 0.113 Uiso 1 1 d R
H11B H -1.1188 -0.0016 0.3045 0.113 Uiso 1 1 d R
C12A C -1.1337(18) -0.0065(9) 0.2291(7) 0.0938(16) Uani 1 1 d .
H12A H -1.1996 -0.0001 0.2293 0.113 Uiso 1 1 d R
H12I H -1.1135 -0.0542 0.2203 0.113 Uiso 1 1 d R
C13A C -1.0764(18) -0.0021(9) 0.1834(8) 0.0938(16) Uani 1 1 d .
H13A H -1.0015 -0.0205 0.1737 0.113 Uiso 1 1 d R
H13D H -1.0654 0.0398 0.1888 0.113 Uiso 1 1 d R
C14A C -1.1582(17) -0.0016(9) 0.1379(7) 0.0938(16) Uani 1 1 d .
H14A H -1.2129 0.0296 0.1403 0.113 Uiso 1 1 d R
H14B H -1.1951 -0.0380 0.1451 0.113 Uiso 1 1 d R
C15A C -1.0871(17) -0.0063(9) 0.0924(7) 0.0938(16) Uani 1 1 d .
H15A H -1.0225 -0.0343 0.0981 0.113 Uiso 1 1 d R
H15B H -1.0616 0.0301 0.0868 0.113 Uiso 1 1 d R
C16A C -1.1415(17) -0.0233(9) 0.0471(8) 0.0938(16) Uani 1 1 d .
H16A H -1.1718 -0.0602 0.0567 0.113 Uiso 1 1 d R
H16D H -1.0812 -0.0343 0.0198 0.113 Uiso 1 1 d R
C17A C -1.2277(17) 0.0213(9) 0.0280(8) 0.0938(16) Uani 1 1 d .
H17A H -1.2830 0.0292 0.0569 0.113 Uiso 1 1 d R
H17B H -1.2598 0.0006 0.0035 0.113 Uiso 1 1 d R
C18A C -1.1780(12) 0.0746(6) 0.0066(6) 0.056(4) Uani 1 1 d .
H18A H -1.1398 0.0898 0.0322 0.067 Uiso 1 1 d R
H18B H -1.1199 0.0620 -0.0212 0.067 Uiso 1 1 d R
C1B C -0.4613(14) 0.2630(6) 0.4346(6) 0.060(4) Uani 1 1 d .
C2B C -0.508(2) 0.3181(10) 0.4640(10) 0.125(2) Uani 1 1 d .
H2BA H -0.5785 0.3089 0.4856 0.150 Uiso 1 1 d R
H2BB H -0.4582 0.3244 0.4886 0.150 Uiso 1 1 d R
C3B C -0.534(2) 0.3700(10) 0.4306(10) 0.125(2) Uani 1 1 d .
H3BA H -0.4654 0.3770 0.4116 0.150 Uiso 1 1 d R
H3BB H -0.5597 0.4048 0.4519 0.150 Uiso 1 1 d R
C4B C -0.621(2) 0.3635(10) 0.3965(10) 0.125(2) Uani 1 1 d .
H4BA H -0.5972 0.3263 0.3774 0.150 Uiso 1 1 d R
H4BB H -0.6276 0.3930 0.3729 0.150 Uiso 1 1 d R
C5B C -0.739(2) 0.3563(10) 0.4248(10) 0.125(2) Uani 1 1 d .
H5BA H -0.7605 0.3871 0.4487 0.150 Uiso 1 1 d R
H5BB H -0.7375 0.3197 0.4457 0.150 Uiso 1 1 d R
C6B C -0.823(2) 0.3555(10) 0.3881(10) 0.125(2) Uani 1 1 d .
H6BA H -0.7958 0.3220 0.3649 0.150 Uiso 1 1 d R
H6BB H -0.8221 0.3891 0.3695 0.150 Uiso 1 1 d R
C7B C -0.940(2) 0.3468(10) 0.4134(10) 0.125(2) Uani 1 1 d D
H7BA H -0.9613 0.3776 0.4364 0.150 Uiso 1 1 d R
H7BB H -0.9315 0.3102 0.4356 0.150 Uiso 1 1 d R
C8B C -0.999(2) 0.3429(10) 0.3711(9) 0.125(2) Uani 1 1 d D
H8BA H -1.0180 0.3903 0.3816 0.150 Uiso 1 1 d R
H8BB H -0.9486 0.3417 0.3477 0.150 Uiso 1 1 d R
C9B C -1.107(2) 0.3426(10) 0.3647(10) 0.125(2) Uani 1 1 d D
H9BA H -1.1415 0.3707 0.3909 0.150 Uiso 1 1 d R
H9BB H -1.1017 0.3050 0.3842 0.150 Uiso 1 1 d R
C10B C -1.193(2) 0.3361(11) 0.3285(9) 0.125(2) Uani 1 1 d .
H10C H -1.2682 0.3416 0.3502 0.150 Uiso 1 1 d R
H10D H -1.1763 0.2991 0.3173 0.150 Uiso 1 1 d R
C11B C -1.198(2) 0.3867(10) 0.3080(10) 0.125(2) Uani 1 1 d .
H11C H -1.1039 0.3620 0.2766 0.150 Uiso 1 1 d R
H11D H -1.1378 0.4032 0.3242 0.150 Uiso 1 1 d R
C12B C -1.317(2) 0.3960(10) 0.2795(10) 0.125(2) Uani 1 1 d .
H12B H -1.3274 0.4351 0.2834 0.150 Uiso 1 1 d R
H12C H -1.3628 0.3781 0.3102 0.150 Uiso 1 1 d R
C13B C -1.290(2) 0.3620(10) 0.2348(10) 0.125(2) Uani 1 1 d .
H13B H -1.2684 0.3188 0.2393 0.150 Uiso 1 1 d R
H13C H -1.2233 0.3737 0.2132 0.150 Uiso 1 1 d R
C14B C -1.418(2) 0.3775(10) 0.2088(10) 0.125(2) Uani 1 1 d .
H14C H -1.4261 0.4189 0.1936 0.150 Uiso 1 1 d R
H14D H -1.4852 0.3794 0.2346 0.150 Uiso 1 1 d R
C15B C -1.413(2) 0.3303(10) 0.1676(10) 0.125(2) Uani 1 1 d .
H15C H -1.4062 0.2910 0.1831 0.150 Uiso 1 1 d R
H15D H -1.3402 0.3288 0.1434 0.150 Uiso 1 1 d R
C16B C -1.511(2) 0.3413(10) 0.1384(10) 0.125(2) Uani 1 1 d .
H16B H -1.5036 0.3740 0.1180 0.150 Uiso 1 1 d R
H16C H -1.5757 0.3488 0.1640 0.150 Uiso 1 1 d R
C17B C -1.527(2) 0.2884(10) 0.1085(9) 0.125(2) Uani 1 1 d .
H17C H -1.4536 0.2757 0.0885 0.150 Uiso 1 1 d R
H17D H -1.5780 0.2987 0.0857 0.150 Uiso 1 1 d R
C18B C -1.5625(13) 0.2385(6) 0.1383(6) 0.058(4) Uani 1 1 d .
H18C H -1.5077 0.2286 0.1624 0.069 Uiso 1 1 d R
H18D H -1.6315 0.2504 0.1582 0.069 Uiso 1 1 d R
C1' C -1.9352(12) 0.5304(6) 0.2357(6) 0.051(4) Uani 1 1 d .
C1C C -2.0686(14) 0.4632(8) 0.1538(8) 0.082(6) Uani 1 1 d .
C2C C -2.120(2) 0.5186(11) 0.1265(10) 0.134(2) Uani 1 1 d .
H2CA H -2.0990 0.5120 0.0916 0.161 Uiso 1 1 d R
H2CB H -2.0899 0.5510 0.1376 0.161 Uiso 1 1 d R
C3C C -2.243(2) 0.5272(12) 0.1385(10) 0.134(2) Uani 1 1 d .
H3CA H -2.2684 0.4926 0.1255 0.161 Uiso 1 1 d R
H3CB H -2.2671 0.5591 0.1207 0.161 Uiso 1 1 d R
C4C C -2.288(2) 0.5351(12) 0.1905(10) 0.134(2) Uani 1 1 d .
H4CA H -2.2669 0.4980 0.2106 0.161 Uiso 1 1 d R
H4CB H -2.3681 0.5388 0.1955 0.161 Uiso 1 1 d R
C5C C -2.247(2) 0.5865(12) 0.2181(10) 0.134(2) Uani 1 1 d .
H5CA H -2.2457 0.6154 0.1940 0.161 Uiso 1 1 d R
H5CB H -2.1721 0.5730 0.2248 0.161 Uiso 1 1 d R
C6C C -2.312(2) 0.6094(12) 0.2701(9) 0.134(2) Uani 1 1 d .
H6CA H -2.3944 0.6068 0.2676 0.161 Uiso 1 1 d R
H6CB H -2.3019 0.6457 0.2750 0.161 Uiso 1 1 d R
C7C C -2.290(2) 0.5776(12) 0.3118(9) 0.134(2) Uani 1 1 d .
H7CA H -2.2080 0.5669 0.3075 0.161 Uiso 1 1 d R
H7CB H -2.3169 0.5377 0.3082 0.161 Uiso 1 1 d R
C8C C -2.341(2) 0.6064(11) 0.3636(9) 0.134(2) Uani 1 1 d .
H8CA H -2.4157 0.6196 0.3640 0.161 Uiso 1 1 d R
H8CB H -2.2991 0.6388 0.3686 0.161 Uiso 1 1 d R
C9C C -2.326(2) 0.5699(11) 0.4081(10) 0.134(2) Uani 1 1 d D
H9CA H -2.2514 0.5732 0.4096 0.161 Uiso 1 1 d R
H9CB H -2.3733 0.5948 0.4326 0.161 Uiso 1 1 d R
C10C C -2.326(2) 0.5159(11) 0.4262(9) 0.134(2) Uani 1 1 d D
H10E H -2.2980 0.4984 0.4028 0.161 Uiso 1 1 d R
H10F H -2.4132 0.5237 0.4316 0.161 Uiso 1 1 d R
C11C C -2.315(2) 0.4933(12) 0.4734(9) 0.134(2) Uani 1 1 d D
H11J H -2.3747 0.5121 0.4908 0.161 Uiso 1 1 d R
H11K H -2.2470 0.5105 0.4761 0.161 Uiso 1 1 d R
C12C C -2.298(2) 0.4409(12) 0.4894(10) 0.134(2) Uani 1 1 d .
H12J H -2.2400 0.4280 0.4632 0.161 Uiso 1 1 d R
H12K H -2.3669 0.4301 0.4818 0.161 Uiso 1 1 d R
C13C C -2.280(2) 0.4221(12) 0.5395(10) 0.134(2) Uani 1 1 d .
H13E H -2.1959 0.4271 0.5400 0.161 Uiso 1 1 d R
H13F H -2.2787 0.3813 0.5427 0.161 Uiso 1 1 d R
C14C C -2.335(2) 0.4478(12) 0.5843(10) 0.134(2) Uani 1 1 d .
H14E H -2.4128 0.4403 0.5843 0.161 Uiso 1 1 d R
H14F H -2.3340 0.4882 0.5799 0.161 Uiso 1 1 d R
C15C C -2.305(2) 0.4370(12) 0.6337(10) 0.134(2) Uani 1 1 d .
H15E H -2.2279 0.4452 0.6331 0.161 Uiso 1 1 d R
H15F H -2.2974 0.3938 0.6353 0.161 Uiso 1 1 d R
C16C C -2.362(2) 0.4543(12) 0.6788(10) 0.134(2) Uani 1 1 d .
H16E H -2.4324 0.4396 0.6816 0.161 Uiso 1 1 d R
H16K H -2.3751 0.4954 0.6758 0.161 Uiso 1 1 d R
C17C C -2.324(2) 0.4443(11) 0.7306(9) 0.134(2) Uani 1 1 d .
H17E H -2.3874 0.4418 0.7553 0.161 Uiso 1 1 d R
H17F H -2.2867 0.4765 0.7395 0.161 Uiso 1 1 d R
C18C C -2.2474(13) 0.3898(7) 0.7367(6) 0.063(5) Uani 1 1 d .
H18E H -2.1767 0.3917 0.7148 0.076 Uiso 1 1 d R
H18F H -2.2776 0.3563 0.7277 0.076 Uiso 1 1 d R
Pt2 Pt -1.43023(5) 0.15182(3) 0.04191(2) 0.04471(18) Uani 1 1 d .
P2 P -0.4265(3) 0.19874(17) 0.47349(15) 0.0462(10) Uani 1 1 d .
C2 C -0.7364(14) 0.1896(6) 0.4576(6) 0.056(4) Uani 1 1 d .
C2' C -1.9689(14) 0.5231(7) 0.2805(7) 0.059(4) Uani 1 1 d .
Pt3 Pt -1.84735(5) 0.53715(3) 0.16913(2) 0.04929(19) Uani 1 1 d .
P3 P -1.2733(3) 0.13219(17) -0.01664(14) 0.0455(10) Uani 1 1 d .
C3 C -0.8031(14) 0.1859(7) 0.4197(6) 0.062(5) Uani 1 1 d .
C3' C -1.9898(13) 0.5167(7) 0.3318(7) 0.059(4) Uani 1 1 d .
P4 P -1.5761(3) 0.17194(17) 0.10573(15) 0.0480(10) Uani 1 1 d .
C4 C -0.8651(15) 0.1823(7) 0.3869(7) 0.067(5) Uani 1 1 d .
C4' C -1.9987(14) 0.5118(7) 0.3766(8) 0.065(5) Uani 1 1 d .
P5 P -1.9149(3) 0.45400(18) 0.14593(17) 0.0578(11) Uani 1 1 d .
C5 C -0.9285(17) 0.1780(8) 0.3486(7) 0.081(6) Uani 1 1 d .
C5' C -2.0015(15) 0.5070(7) 0.4286(7) 0.069(5) Uani 1 1 d .
P6 P -1.7908(3) 0.62090(17) 0.19930(15) 0.0500(10) Uani 1 1 d .
C6 C -0.9737(16) 0.1736(8) 0.3131(7) 0.079(6) Uani 1 1 d .
C6' C -2.0008(15) 0.5030(7) 0.4750(7) 0.069(5) Uani 1 1 d .
C7 C -1.0355(17) 0.1713(8) 0.2740(8) 0.084(6) Uani 1 1 d .
C8 C -1.0932(18) 0.1689(8) 0.2399(7) 0.087(7) Uani 1 1 d .
C9 C -1.1519(16) 0.1660(8) 0.2008(7) 0.071(5) Uani 1 1 d .
C10 C -1.2048(15) 0.1634(7) 0.1657(7) 0.068(5) Uani 1 1 d .
C11 C -1.2700(12) 0.1609(7) 0.1260(6) 0.055(4) Uani 1 1 d .
C12 C -1.3275(12) 0.1571(7) 0.0941(6) 0.053(4) Uani 1 1 d .
C31 C -0.8252(13) 0.2411(6) 0.6040(6) 0.054(4) Uani 1 1 d .
C32 C -0.8246(14) 0.2861(7) 0.5679(6) 0.061(4) Uani 1 1 d .
C33 C -0.9136(15) 0.3313(7) 0.5725(7) 0.070(5) Uani 1 1 d .
C34 C -1.0027(16) 0.3313(8) 0.6112(8) 0.076(5) Uani 1 1 d .
C35 C -1.0069(16) 0.2856(9) 0.6456(8) 0.085(6) Uani 1 1 d .
C36 C -0.9175(14) 0.2415(8) 0.6427(7) 0.068(5) Uani 1 1 d .
C41 C -0.6838(12) 0.1735(7) 0.6655(6) 0.050(4) Uani 1 1 d .
C42 C -0.6507(12) 0.2200(8) 0.6867(5) 0.058(5) Uani 1 1 d .
C43 C -0.6116(14) 0.2181(9) 0.7350(6) 0.069(5) Uani 1 1 d .
C44 C -0.6136(15) 0.1680(10) 0.7615(7) 0.075(5) Uani 1 1 d .
C45 C -0.6518(17) 0.1199(10) 0.7417(9) 0.091(6) Uani 1 1 d .
C46 C -0.6899(15) 0.1200(8) 0.6927(7) 0.072(5) Uani 1 1 d .
C51 C -0.4615(11) 0.1874(6) 0.5931(5) 0.038(3) Uani 1 1 d .
F52 F -0.4400(7) 0.2867(4) 0.5833(3) 0.068(3) Uani 1 1 d .
C52 C -0.4157(12) 0.2357(6) 0.6069(5) 0.043(4) Uani 1 1 d .
F53 F -0.3120(9) 0.2864(5) 0.6578(4) 0.091(3) Uani 1 1 d .
C53 C -0.3510(15) 0.2376(8) 0.6464(7) 0.067(5) Uani 1 1 d .
F54 F -0.2680(9) 0.1882(5) 0.7117(4) 0.097(4) Uani 1 1 d .
C54 C -0.3245(15) 0.1875(8) 0.6726(6) 0.067(5) Uani 1 1 d .
F55 F -0.3520(8) 0.0899(4) 0.6900(3) 0.077(3) Uani 1 1 d .
C55 C -0.3703(15) 0.1386(8) 0.6611(6) 0.070(5) Uani 1 1 d .
F56 F -0.4710(7) 0.0881(3) 0.6117(3) 0.057(2) Uani 1 1 d .
C56 C -0.4337(13) 0.1390(7) 0.6201(5) 0.053(4) Uani 1 1 d .
C61 C -0.2895(14) 0.2020(7) 0.4906(6) 0.061(4) Uani 1 1 d .
C62 C -0.2424(13) 0.2550(8) 0.4888(7) 0.071(5) Uani 1 1 d .
C63 C -0.1333(17) 0.2545(8) 0.5061(8) 0.086(6) Uani 1 1 d .
C64 C -0.0776(14) 0.2039(10) 0.5236(8) 0.084(6) Uani 1 1 d .
C65 C -0.1313(15) 0.1552(8) 0.5279(8) 0.079(5) Uani 1 1 d .
C66 C -0.2335(14) 0.1533(7) 0.5109(7) 0.068(5) Uani 1 1 d .
C71 C -0.4013(14) 0.1415(6) 0.4261(6) 0.054(4) Uani 1 1 d .
C72 C -0.4783(12) 0.0996(7) 0.4264(7) 0.061(4) Uani 1 1 d .
C73 C -0.4640(16) 0.0605(7) 0.3854(7) 0.073(5) Uani 1 1 d .
C74A C -0.3746(19) 0.0611(8) 0.3470(7) 0.082(6) Uani 1 1 d .
C75 C -0.298(2) 0.1022(9) 0.3483(8) 0.094(7) Uani 1 1 d .
C76 C -0.3097(16) 0.1413(8) 0.3867(7) 0.079(5) Uani 1 1 d .
C81 C -1.1870(14) 0.1902(6) -0.0283(6) 0.053(4) Uani 1 1 d .
C82 C -1.2069(14) 0.2400(7) 0.0048(6) 0.066(5) Uani 1 1 d .
C83 C -1.1321(17) 0.2833(8) -0.0040(9) 0.083(6) Uani 1 1 d .
C84 C -1.0463(17) 0.2772(9) -0.0443(9) 0.082(6) Uani 1 1 d .
C85 C -1.0253(15) 0.2281(9) -0.0763(7) 0.077(5) Uani 1 1 d .
C86 C -1.0965(13) 0.1857(8) -0.0674(7) 0.067(5) Uani 1 1 d .
C91 C -1.2873(12) 0.1120(7) -0.0821(6) 0.053(4) Uani 1 1 d .
C92 C -1.2551(13) 0.0556(7) -0.1007(6) 0.059(4) Uani 1 1 d .
C93 C -1.2749(18) 0.0446(9) -0.1507(7) 0.088(6) Uani 1 1 d .
C94 C -1.3184(16) 0.0887(11) -0.1812(7) 0.084(6) Uani 1 1 d .
C95 C -1.3499(15) 0.1428(9) -0.1605(7) 0.073(5) Uani 1 1 d .
C96 C -1.3371(13) 0.1564(7) -0.1121(5) 0.057(4) Uani 1 1 d .
C101 C -1.5346(11) 0.1482(6) -0.0125(5) 0.039(3) Uani 1 1 d .
F102 F -1.4815(7) 0.0491(3) -0.0294(3) 0.059(2) Uani 1 1 d .
C102 C -1.5416(12) 0.0985(7) -0.0390(6) 0.047(4) Uani 1 1 d .
F103 F -1.6071(7) 0.0477(4) -0.1040(3) 0.067(2) Uani 1 1 d .
C103 C -1.6117(14) 0.0975(7) -0.0780(6) 0.060(5) Uani 1 1 d .
F104 F -1.7439(8) 0.1450(4) -0.1255(3) 0.078(3) Uani 1 1 d .
C104 C -1.6763(13) 0.1466(8) -0.0894(6) 0.052(4) Uani 1 1 d .
F105 F -1.7403(7) 0.2442(4) -0.0728(3) 0.070(3) Uani 1 1 d .
C105 C -1.6748(13) 0.1961(7) -0.0633(6) 0.054(4) Uani 1 1 d .
F106 F -1.6040(7) 0.2471(3) -0.0018(3) 0.059(2) Uani 1 1 d .
C106 C -1.6043(11) 0.1954(6) -0.0251(5) 0.043(4) Uani 1 1 d .
C111 C -1.7162(12) 0.1770(6) 0.0890(5) 0.045(4) Uani 1 1 d .
C112 C -1.7822(14) 0.2306(7) 0.0869(7) 0.067(5) Uani 1 1 d .
C113 C -1.8908(18) 0.2300(9) 0.0723(8) 0.093(6) Uani 1 1 d .
C114 C -1.9330(15) 0.1812(9) 0.0603(8) 0.084(6) Uani 1 1 d .
C115 C -1.8622(16) 0.1278(9) 0.0625(7) 0.081(6) Uani 1 1 d .
C116 C -1.7576(13) 0.1250(7) 0.0766(6) 0.059(4) Uani 1 1 d .
C121 C -1.5831(13) 0.1199(6) 0.1577(6) 0.052(4) Uani 1 1 d .
C122 C -1.6745(14) 0.1272(7) 0.1965(6) 0.062(5) Uani 1 1 d .
C123 C -1.6781(19) 0.0895(9) 0.2388(7) 0.085(6) Uani 1 1 d .
C124 C -1.5913(17) 0.0446(8) 0.2406(6) 0.067(5) Uani 1 1 d .
C125 C -1.5079(16) 0.0356(7) 0.2004(8) 0.078(5) Uani 1 1 d .
C126 C -1.5025(13) 0.0730(7) 0.1609(6) 0.060(4) Uani 1 1 d .
C161 C -1.8990(13) 0.6820(7) 0.2046(6) 0.057(4) Uani 1 1 d .
C162 C -2.0088(14) 0.6766(7) 0.2026(6) 0.065(5) Uani 1 1 d .
C163 C -2.0908(13) 0.7248(9) 0.2078(7) 0.075(5) Uani 1 1 d .
C164 C -2.0617(16) 0.7787(8) 0.2157(6) 0.069(5) Uani 1 1 d .
C165 C -1.9524(18) 0.7868(8) 0.2168(7) 0.074(5) Uani 1 1 d .
C166 C -1.8698(14) 0.7395(7) 0.2122(7) 0.067(5) Uani 1 1 d .
C171 C -1.6760(13) 0.6513(6) 0.1620(5) 0.050(4) Uani 1 1 d .
C172 C -1.5706(14) 0.6516(7) 0.1814(7) 0.072(5) Uani 1 1 d .
C173 C -1.4812(15) 0.6708(8) 0.1486(8) 0.080(6) Uani 1 1 d .
C174 C -1.4933(16) 0.6890(7) 0.1006(8) 0.075(5) Uani 1 1 d .
C175 C -1.5978(15) 0.6894(7) 0.0829(7) 0.065(5) Uani 1 1 d .
C176 C -1.6894(13) 0.6726(6) 0.1139(6) 0.054(4) Uani 1 1 d .
C181 C -1.7476(11) 0.5424(5) 0.1033(6) 0.040(4) Uani 1 1 d .
F182 F -1.5821(8) 0.5192(4) 0.1394(3) 0.069(3) Uani 1 1 d .
C182 C -1.6329(12) 0.5363(6) 0.0999(5) 0.040(3) Uani 1 1 d .
F183 F -1.4490(7) 0.5415(4) 0.0556(4) 0.077(3) Uani 1 1 d .
C183 C -1.5594(13) 0.5458(7) 0.0550(6) 0.056(4) Uani 1 1 d .
F184 F -1.5386(8) 0.5748(4) -0.0306(4) 0.086(3) Uani 1 1 d .
C184 C -1.6052(15) 0.5627(7) 0.0115(6) 0.064(5) Uani 1 1 d .
F185 F -1.7629(8) 0.5825(4) -0.0306(4) 0.076(3) Uani 1 1 d .
C185 C -1.7210(14) 0.5680(7) 0.0127(6) 0.060(4) Uani 1 1 d .
F186 F -1.8960(7) 0.5653(4) 0.0546(3) 0.069(3) Uani 1 1 d .
C186 C -1.7832(12) 0.5583(6) 0.0561(6) 0.049(4) Uani 1 1 d .
C191 C -1.8681(13) 0.4253(7) 0.0829(7) 0.058(4) Uani 1 1 d .
C192 C -1.9400(15) 0.4197(8) 0.0461(8) 0.081(6) Uani 1 1 d .
C193 C -1.889(2) 0.3970(9) -0.0023(8) 0.097(7) Uani 1 1 d .
C194 C -1.7804(17) 0.3781(8) -0.0117(7) 0.075(5) Uani 1 1 d .
C195 C -1.7123(14) 0.3856(6) 0.0251(6) 0.055(4) Uani 1 1 d .
C196 C -1.7524(13) 0.4071(6) 0.0712(6) 0.052(4) Uani 1 1 d .
C201 C -1.8781(16) 0.3903(8) 0.1869(6) 0.071(5) Uani 1 1 d .
C202 C -1.7978(17) 0.3947(9) 0.2192(7) 0.085(6) Uani 1 1 d .
C203 C -1.766(2) 0.3462(11) 0.2485(8) 0.115(9) Uani 1 1 d .
C204 C -1.821(3) 0.2956(10) 0.2421(10) 0.116(10) Uani 1 1 d .
C205 C -1.899(2) 0.2942(10) 0.2087(10) 0.106(8) Uani 1 1 d .
C206 C -1.931(2) 0.3401(8) 0.1807(8) 0.099(7) Uani 1 1 d .
C300 C -0.473(6) 0.1792(14) 0.274(3) 0.49(6) Uani 1 1 d .
Cl31 Cl -0.4135(15) 0.2373(7) 0.2847(5) 0.299(7) Uani 1 1 d .
Cl32 Cl -0.6202(11) 0.2046(8) 0.3211(5) 0.312(10) Uani 1 1 d .
H30A H -0.4181 0.1429 0.2776 0.375 Uiso 1 1 d R
H30B H -0.4746 0.1773 0.2313 0.375 Uiso 1 1 d R
H1AA H -0.8432 0.1299 0.5630 0.375 Uiso 1 1 d R
H1AB H -0.8433 0.1114 0.6194 0.375 Uiso 1 1 d R
H1BA H -0.5192 0.2556 0.4119 0.375 Uiso 1 1 d R
H1BB H -0.3997 0.2734 0.4120 0.375 Uiso 1 1 d R
H1CA H -2.1018 0.4308 0.1432 0.375 Uiso 1 1 d R
H1CB H -2.1020 0.4689 0.1907 0.375 Uiso 1 1 d R
H32A H -0.7668 0.2876 0.5406 0.375 Uiso 1 1 d R
H33A H -0.9161 0.3621 0.5475 0.375 Uiso 1 1 d R
H34A H -1.0621 0.3655 0.6155 0.375 Uiso 1 1 d R
H35A H -1.0783 0.2819 0.6711 0.375 Uiso 1 1 d R
H36A H -0.9212 0.2122 0.6670 0.375 Uiso 1 1 d R
H42A H -0.6567 0.2583 0.6691 0.375 Uiso 1 1 d R
H43A H -0.5862 0.2518 0.7479 0.375 Uiso 1 1 d R
H44A H -0.5929 0.1655 0.7939 0.375 Uiso 1 1 d R
H45A H -0.6601 0.0857 0.7628 0.375 Uiso 1 1 d R
H46A H -0.7200 0.0867 0.6784 0.375 Uiso 1 1 d R
H62A H -0.2826 0.2906 0.4760 0.375 Uiso 1 1 d R
H63A H -0.1050 0.2917 0.5070 0.375 Uiso 1 1 d R
H64A H -0.0048 0.2065 0.5314 0.375 Uiso 1 1 d R
H65A H -0.0997 0.1213 0.5428 0.375 Uiso 1 1 d R
H66A H -0.2719 0.1197 0.5139 0.375 Uiso 1 1 d R
H72A H -0.5385 0.0981 0.4546 0.375 Uiso 1 1 d R
H73A H -0.5209 0.0357 0.3842 0.375 Uiso 1 1 d R
H74A H -0.3717 0.0359 0.3201 0.375 Uiso 1 1 d R
H75A H -0.2380 0.1023 0.3220 0.375 Uiso 1 1 d R
H76A H -0.2581 0.1697 0.3886 0.375 Uiso 1 1 d R
H82A H -1.2718 0.2453 0.0311 0.375 Uiso 1 1 d R
H83A H -1.1457 0.3180 0.0171 0.375 Uiso 1 1 d R
H84A H -1.0000 0.3088 -0.0496 0.375 Uiso 1 1 d R
H85A H -0.9698 0.2272 -0.1044 0.375 Uiso 1 1 d R
H86A H -1.0847 0.1525 -0.0876 0.375 Uiso 1 1 d R
H92A H -1.2252 0.0267 -0.0793 0.375 Uiso 1 1 d R
H93A H -1.2616 0.0051 -0.1627 0.375 Uiso 1 1 d R
H94A H -1.3298 0.0816 -0.2162 0.375 Uiso 1 1 d R
H95A H -1.3813 0.1733 -0.1820 0.375 Uiso 1 1 d R
H96A H -1.3664 0.1958 -0.0981 0.375 Uiso 1 1 d R
H11E H -1.7610 0.2679 0.0952 0.375 Uiso 1 1 d R
H11F H -1.9436 0.2668 0.0723 0.375 Uiso 1 1 d R
H11G H -2.0106 0.1840 0.0509 0.375 Uiso 1 1 d R
H11H H -1.8928 0.0940 0.0533 0.375 Uiso 1 1 d R
H11I H -1.7190 0.0887 0.0810 0.375 Uiso 1 1 d R
H12D H -1.7366 0.1594 0.1942 0.375 Uiso 1 1 d R
H12E H -1.7428 0.0970 0.2667 0.375 Uiso 1 1 d R
H12F H -1.5922 0.0211 0.2708 0.375 Uiso 1 1 d R
H12G H -1.4535 0.0030 0.2016 0.375 Uiso 1 1 d R
H12H H -1.4486 0.0670 0.1317 0.375 Uiso 1 1 d R
H16F H -2.0344 0.6407 0.1987 0.375 Uiso 1 1 d R
H16G H -2.1697 0.7220 0.2043 0.375 Uiso 1 1 d R
H16H H -2.1220 0.8140 0.2207 0.375 Uiso 1 1 d R
H16I H -1.9318 0.8260 0.2212 0.375 Uiso 1 1 d R
H16J H -1.7961 0.7466 0.2128 0.375 Uiso 1 1 d R
H17G H -1.5645 0.6386 0.2150 0.375 Uiso 1 1 d R
H17H H -1.4139 0.6750 0.1625 0.375 Uiso 1 1 d R
H17I H -1.4306 0.7000 0.0776 0.375 Uiso 1 1 d R
H17J H -1.6107 0.7036 0.0486 0.375 Uiso 1 1 d R
H17K H -1.7650 0.6774 0.1020 0.375 Uiso 1 1 d R
H19A H -2.0235 0.4309 0.0551 0.375 Uiso 1 1 d R
H19B H -1.9410 0.3987 -0.0273 0.375 Uiso 1 1 d R
H19C H -1.7476 0.3633 -0.0448 0.375 Uiso 1 1 d R
H19D H -1.6368 0.3739 0.0191 0.375 Uiso 1 1 d R
H19E H -1.7082 0.4111 0.0961 0.375 Uiso 1 1 d R
H20A H -1.7671 0.4311 0.2207 0.375 Uiso 1 1 d R
H20B H -1.7219 0.3484 0.2723 0.375 Uiso 1 1 d R
H20C H -1.8074 0.2620 0.2624 0.375 Uiso 1 1 d R
H20D H -1.9372 0.2604 0.2061 0.375 Uiso 1 1 d R
H20E H -1.9871 0.3408 0.1573 0.375 Uiso 1 1 d R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Pt Pt -1.7033 8.3905 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Cl Cl 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C1 Pt1 C51 178.6(6) . .
C1 Pt1 P1 87.5(4) . .
C51 Pt1 P1 91.2(4) . .
C1 Pt1 P2 88.3(4) . .
C51 Pt1 P2 93.0(4) . .
P1 Pt1 P2 175.70(13) . .
C1 Pt1 Pt2 5.2(4) . .
C51 Pt1 Pt2 175.4(4) . .
P1 Pt1 Pt2 91.15(9) . .
P2 Pt1 Pt2 84.65(9) . .
C31 P1 C41 102.8(7) . .
C31 P1 C1A 102.3(6) . .
C41 P1 C1A 107.7(8) . .
C31 P1 Pt1 114.9(6) . .
C41 P1 Pt1 115.3(5) . .
C1A P1 Pt1 112.6(5) . .
C2 C1 Pt1 179.0(14) . .
C2A C1A P1 111.2(11) . .
C1A C2A C3A 110.4(16) . .
C4A C3A C2A 116.2(18) . .
C5A C4A C3A 115.9(18) . .
C4A C5A C6A 107.6(17) . .
C7A C6A C5A 111.1(17) . .
C6A C7A C8A 113.6(17) . .
C9A C8A C7A 122.3(18) . .
C8A C9A C10A 115.1(18) . .
C11A C10A C9A 111.0(18) . .
C10A C11A C12A 122.2(17) . .
C13A C12A C11A 116.1(18) . .
C12A C13A C14A 111.7(18) . .
C15A C14A C13A 106.1(17) . .
C14A C15A C16A 114.4(17) . .
C15A C16A C17A 117.1(18) . .
C18A C17A C16A 112.5(16) . .
C17A C18A P3 116.9(11) . .
C2B C1B P2 115.5(13) . .
C3B C2B C1B 114(2) . .
C2B C3B C4B 115(2) . .
C3B C4B C5B 115(2) . .
C6B C5B C4B 111(2) . .
C5B C6B C7B 114(2) . .
C8B C7B C6B 102(2) . .
C9B C8B C7B 135(3) . .
C8B C9B C10B 148(3) . .
C11B C10B C9B 100(2) . .
C10B C11B C12B 107(2) . .
C13B C12B C11B 104(2) . .
C12B C13B C14B 99(2) . .
C15B C14B C13B 104.4(19) . .
C16B C15B C14B 111(2) . .
C15B C16B C17B 112(2) . .
C18B C17B C16B 116(2) . .
C17B C18B P4 119.1(14) . .
C2' C1' Pt3 166.7(14) . .
C2C C1C P5 113.4(14) . .
C3C C2C C1C 111(2) . .
C4C C3C C2C 117(2) . .
C3C C4C C5C 115(2) . .
C6C C5C C4C 120(2) . .
C7C C6C C5C 116(2) . .
C6C C7C C8C 115(2) . .
C9C C8C C7C 115(2) . .
C10C C9C C8C 144(3) . .
C9C C10C C11C 132(3) . .
C12C C11C C10C 132(3) . .
C11C C12C C13C 127(3) . .
C14C C13C C12C 125(2) . .
C13C C14C C15C 126(2) . .
C16C C15C C14C 129(2) . .
C15C C16C C17C 127(2) . .
C18C C17C C16C 116(2) . .
C17C C18C P6 113.9(14) . 2_166
C12 Pt2 C101 178.6(6) . .
C12 Pt2 P4 87.4(5) . .
C101 Pt2 P4 93.1(4) . .
C12 Pt2 P3 87.5(5) . .
C101 Pt2 P3 92.0(4) . .
P4 Pt2 P3 174.84(14) . .
C12 Pt2 Pt1 3.3(4) . .
C101 Pt2 Pt1 177.5(4) . .
P4 Pt2 Pt1 84.40(10) . .
P3 Pt2 Pt1 90.44(9) . .
C61 P2 C71 102.1(7) . .
C61 P2 C1B 107.9(8) . .
C71 P2 C1B 101.5(7) . .
C61 P2 Pt1 116.7(5) . .
C71 P2 Pt1 116.2(6) . .
C1B P2 Pt1 111.0(5) . .
C1 C2 C3 174.7(18) . .
C1' C2' C3' 170.8(18) . .
C1' Pt3 C181 175.9(6) . .
C1' Pt3 P5 87.6(4) . .
C181 Pt3 P5 93.6(4) . .
C1' Pt3 P6 87.1(4) . .
C181 Pt3 P6 91.6(4) . .
P5 Pt3 P6 174.72(15) . .
C1' Pt3 Pt3 20.6(4) . 2_166
C181 Pt3 Pt3 155.4(4) . 2_166
P5 Pt3 Pt3 97.93(11) . 2_166
P6 Pt3 Pt3 77.34(10) . 2_166
C81 P3 C18A 102.3(7) . .
C81 P3 C91 100.7(7) . .
C18A P3 C91 106.0(8) . .
C81 P3 Pt2 115.6(6) . .
C18A P3 Pt2 110.2(5) . .
C91 P3 Pt2 120.1(5) . .
C4 C3 C2 178(2) . .
C4' C3' C2' 174.5(18) . .
C111 P4 C121 101.7(7) . .
C111 P4 C18B 107.7(7) . .
C121 P4 C18B 101.8(7) . .
C111 P4 Pt2 117.7(5) . .
C121 P4 Pt2 115.8(6) . .
C18B P4 Pt2 110.7(5) . .
C3 C4 C5 177(2) . .
C3' C4' C5' 176(2) . .
C191 P5 C1C 107.3(8) . .
C191 P5 C201 102.1(7) . .
C1C P5 C201 104.2(9) . .
C191 P5 Pt3 118.3(5) . .
C1C P5 Pt3 110.8(6) . .
C201 P5 Pt3 113.0(7) . .
C6 C5 C4 174(2) . .
C6' C5' C4' 178(2) . .
C171 P6 C161 102.0(7) . .
C171 P6 C18C 106.7(7) . 2_166
C161 P6 C18C 104.9(7) . 2_166
C171 P6 Pt3 117.5(5) . .
C161 P6 Pt3 113.5(5) . .
C18C P6 Pt3 111.2(5) 2_166 .
C5 C6 C7 174(2) . .
C5' C6' C6' 178(2) . 2_166
C8 C7 C6 178(2) . .
C7 C8 C9 177(3) . .
C10 C9 C8 180(3) . .
C9 C10 C11 178(2) . .
C12 C11 C10 176.9(18) . .
C11 C12 Pt2 177.8(15) . .
C32 C31 C36 119.0(15) . .
C32 C31 P1 121.9(13) . .
C36 C31 P1 118.9(12) . .
C31 C32 C33 118.8(17) . .
C34 C33 C32 121.3(17) . .
C35 C34 C33 120.3(16) . .
C34 C35 C36 119.2(18) . .
C35 C36 C31 121.2(17) . .
C42 C41 C46 120.9(15) . .
C42 C41 P1 118.0(12) . .
C46 C41 P1 121.1(13) . .
C41 C42 C43 123.1(17) . .
C44 C43 C42 117.7(18) . .
C43 C44 C45 120.7(17) . .
C44 C45 C46 123.0(18) . .
C41 C46 C45 114.4(17) . .
C56 C51 C52 114.0(13) . .
C56 C51 Pt1 122.6(10) . .
C52 C51 Pt1 123.4(10) . .
F52 C52 C51 119.0(12) . .
F52 C52 C53 115.7(13) . .
C51 C52 C53 125.1(13) . .
F53 C53 C54 119.8(14) . .
F53 C53 C52 121.2(15) . .
C54 C53 C52 118.9(14) . .
F54 C54 C55 120.9(17) . .
F54 C54 C53 120.6(16) . .
C55 C54 C53 118.1(15) . .
F55 C55 C54 118.4(16) . .
F55 C55 C56 121.3(16) . .
C54 C55 C56 120.3(16) . .
F56 C56 C51 121.9(12) . .
F56 C56 C55 114.7(14) . .
C51 C56 C55 123.3(15) . .
C66 C61 C62 119.2(15) . .
C66 C61 P2 119.6(13) . .
C62 C61 P2 120.9(13) . .
C61 C62 C63 117.3(16) . .
C64 C63 C62 121.5(17) . .
C65 C64 C63 118.1(16) . .
C64 C65 C66 122.2(17) . .
C65 C66 C61 121.4(16) . .
C72 C71 C76 120.4(15) . .
C72 C71 P2 119.4(13) . .
C76 C71 P2 120.0(13) . .
C73 C72 C71 117.7(16) . .
C72 C73 C74A 121.2(17) . .
C75 C74A C73 119.7(17) . .
C76 C75 C74A 121.1(19) . .
C75 C76 C71 119.7(18) . .
C86 C81 C82 120.0(15) . .
C86 C81 P3 120.5(12) . .
C82 C81 P3 119.4(13) . .
C83 C82 C81 117.4(17) . .
C84 C83 C82 120.0(18) . .
C83 C84 C85 122.9(17) . .
C86 C85 C84 117.2(17) . .
C85 C86 C81 122.5(17) . .
C92 C91 C96 121.7(14) . .
C92 C91 P3 122.1(12) . .
C96 C91 P3 116.1(12) . .
C91 C92 C93 117.0(17) . .
C94 C93 C92 121.5(19) . .
C95 C94 C93 118.5(18) . .
C96 C95 C94 123.5(18) . .
C95 C96 C91 117.7(16) . .
C106 C101 C102 114.3(13) . .
C106 C101 Pt2 122.4(10) . .
C102 C101 Pt2 123.3(11) . .
F102 C102 C101 120.7(13) . .
F102 C102 C103 116.9(13) . .
C101 C102 C103 122.4(14) . .
F103 C103 C104 122.2(15) . .
F103 C103 C102 117.8(15) . .
C104 C103 C102 119.9(14) . .
F104 C104 C105 120.6(15) . .
F104 C104 C103 119.6(15) . .
C105 C104 C103 119.7(13) . .
F105 C105 C104 120.7(13) . .
F105 C105 C106 120.6(14) . .
C104 C105 C106 118.7(14) . .
F106 C106 C101 119.7(12) . .
F106 C106 C105 115.3(13) . .
C101 C106 C105 124.9(14) . .
C112 C111 C116 120.3(14) . .
C112 C111 P4 121.7(12) . .
C116 C111 P4 118.0(11) . .
C111 C112 C113 117.3(15) . .
C114 C113 C112 124.0(18) . .
C113 C114 C115 116.6(18) . .
C116 C115 C114 122.7(17) . .
C115 C116 C111 119.1(16) . .
C126 C121 C122 118.3(14) . .
C126 C121 P4 122.8(13) . .
C122 C121 P4 118.9(12) . .
C121 C122 C123 119.8(16) . .
C124 C123 C122 118.7(17) . .
C125 C124 C123 120.2(16) . .
C126 C125 C124 120.7(17) . .
C125 C126 C121 121.9(16) . .
C162 C161 C166 117.3(15) . .
C162 C161 P6 123.3(13) . .
C166 C161 P6 119.5(12) . .
C161 C162 C163 121.7(16) . .
C164 C163 C162 120.1(16) . .
C163 C164 C165 120.6(17) . .
C164 C165 C166 120.2(17) . .
C165 C166 C161 120.1(16) . .
C176 C171 C172 120.4(14) . .
C176 C171 P6 119.2(12) . .
C172 C171 P6 120.4(12) . .
C173 C172 C171 117.6(17) . .
C174 C173 C172 121.8(18) . .
C173 C174 C175 119.6(18) . .
C176 C175 C174 121.2(16) . .
C175 C176 C171 119.3(15) . .
C182 C181 C186 110.9(12) . .
C182 C181 Pt3 123.1(11) . .
C186 C181 Pt3 125.7(10) . .
F182 C182 C181 120.7(12) . .
F182 C182 C183 114.5(13) . .
C181 C182 C183 124.9(13) . .
F183 C183 C184 120.5(15) . .
F183 C183 C182 120.9(14) . .
C184 C183 C182 118.5(14) . .
F184 C184 C183 119.9(16) . .
F184 C184 C185 121.3(16) . .
C183 C184 C185 118.8(14) . .
C186 C185 F185 123.8(15) . .
C186 C185 C184 118.7(15) . .
F185 C185 C184 117.5(15) . .
C185 C186 F186 115.4(14) . .
C185 C186 C181 128.2(14) . .
F186 C186 C181 116.4(12) . .
C192 C191 C196 119.4(16) . .
C192 C191 P5 123.8(13) . .
C196 C191 P5 116.8(12) . .
C191 C192 C193 116.6(17) . .
C194 C193 C192 122.6(17) . .
C193 C194 C195 118.8(18) . .
C196 C195 C194 122.6(17) . .
C195 C196 C191 119.7(15) . .
C202 C201 C206 125.3(18) . .
C202 C201 P5 118.1(15) . .
C206 C201 P5 116.5(17) . .
C201 C202 C203 119(2) . .
C202 C203 C204 116(2) . .
C205 C204 C203 122(2) . .
C206 C205 C204 123(2) . .
C205 C206 C201 115(2) . .
Cl31 C300 Cl32 95(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Pt1 C1 1.962(13) .
Pt1 C51 2.047(13) .
Pt1 P1 2.300(4) .
Pt1 P2 2.309(4) .
Pt1 Pt2 17.9897(8) .
P1 C31 1.806(16) .
P1 C41 1.839(15) .
P1 C1A 1.857(16) .
C1 C2 1.207(19) .
C1A C2A 1.52(2) .
C2A C3A 1.54(2) .
C3A C4A 1.46(2) .
C4A C5A 1.47(2) .
C5A C6A 1.56(2) .
C6A C7A 1.41(2) .
C7A C8A 1.61(2) .
C8A C9A 1.44(2) .
C9A C10A 1.52(2) .
C10A C11A 1.44(3) .
C11A C12A 1.62(3) .
C12A C13A 1.33(2) .
C13A C14A 1.66(3) .
C14A C15A 1.39(2) .
C15A C16A 1.53(2) .
C16A C17A 1.51(3) .
C17A C18A 1.51(2) .
C18A P3 1.818(15) .
C1B C2B 1.52(3) .
C1B P2 1.840(15) .
C2B C3B 1.51(3) .
C3B C4B 1.51(3) .
C4B C5B 1.55(3) .
C5B C6B 1.51(3) .
C6B C7B 1.52(3) .
C7B C8B 1.42(2) .
C8B C9B 1.35(2) .
C9B C10B 1.53(3) .
C10B C11B 1.29(3) .
C11B C12B 1.71(3) .
C12B C13B 1.42(3) .
C13B C14B 1.78(3) .
C14B C15B 1.55(3) .
C15B C16B 1.50(3) .
C16B C17B 1.52(3) .
C17B C18B 1.47(2) .
C18B P4 1.816(15) .
C1' C2' 1.23(2) .
C1' Pt3 1.960(16) .
C1C C2C 1.57(3) .
C1C P5 1.839(18) .
C2C C3C 1.49(3) .
C3C C4C 1.43(3) .
C4C C5C 1.57(3) .
C5C C6C 1.57(3) .
C6C C7C 1.36(3) .
C7C C8C 1.57(3) .
C8C C9C 1.46(3) .
C9C C10C 1.33(2) .
C10C C11C 1.37(2) .
C11C C12C 1.28(3) .
C12C C13C 1.43(3) .
C13C C14C 1.40(3) .
C14C C15C 1.42(3) .
C15C C16C 1.35(3) .
C16C C17C 1.51(3) .
C17C C18C 1.50(2) .
C18C P6 1.828(16) 2_166
Pt2 C12 1.998(15) .
Pt2 C101 2.052(13) .
Pt2 P4 2.301(4) .
Pt2 P3 2.307(4) .
P2 C61 1.791(17) .
P2 C71 1.818(15) .
C2 C3 1.38(2) .
C2' C3' 1.36(2) .
Pt3 C181 2.007(13) .
Pt3 P5 2.303(4) .
Pt3 P6 2.321(4) .
Pt3 Pt3 17.6087(13) 2_166
P3 C81 1.799(16) .
P3 C91 1.845(15) .
C3 C4 1.23(2) .
C3' C4' 1.19(2) .
P4 C111 1.805(14) .
P4 C121 1.821(15) .
C4 C5 1.37(2) .
C4' C5' 1.38(3) .
P5 C191 1.809(18) .
P5 C201 1.869(18) .
C5 C6 1.16(2) .
C5' C6' 1.24(2) .
P6 C171 1.810(15) .
P6 C161 1.811(17) .
P6 C18C 1.828(16) 2_166
C6 C7 1.36(2) .
C6' C6' 1.34(4) 2_166
C7 C8 1.22(2) .
C8 C9 1.34(2) .
C9 C10 1.21(2) .
C10 C11 1.41(2) .
C11 C12 1.176(19) .
C31 C32 1.41(2) .
C31 C36 1.42(2) .
C32 C33 1.41(2) .
C33 C34 1.39(2) .
C34 C35 1.39(3) .
C35 C36 1.40(2) .
C41 C42 1.35(2) .
C41 C46 1.43(2) .
C42 C43 1.42(2) .
C43 C44 1.35(2) .
C44 C45 1.39(3) .
C45 C46 1.44(3) .
C51 C56 1.357(19) .
C51 C52 1.380(18) .
F52 C52 1.350(15) .
C52 C53 1.395(19) .
F53 C53 1.330(17) .
C53 C54 1.37(2) .
F54 C54 1.320(16) .
C54 C55 1.37(2) .
F55 C55 1.368(18) .
C55 C56 1.41(2) .
F56 C56 1.343(16) .
C61 C66 1.39(2) .
C61 C62 1.41(2) .
C62 C63 1.46(2) .
C63 C64 1.39(3) .
C64 C65 1.37(2) .
C65 C66 1.38(2) .
C71 C72 1.42(2) .
C71 C76 1.43(2) .
C72 C73 1.41(2) .
C73 C74A 1.39(2) .
C74A C75 1.41(3) .
C75 C76 1.36(2) .
C81 C86 1.41(2) .
C81 C82 1.44(2) .
C82 C83 1.43(2) .
C83 C84 1.39(3) .
C84 C85 1.41(3) .
C85 C86 1.38(2) .
C91 C92 1.40(2) .
C91 C96 1.42(2) .
C92 C93 1.41(2) .
C93 C94 1.39(3) .
C94 C95 1.37(3) .
C95 C96 1.36(2) .
C101 C106 1.368(18) .
C101 C102 1.377(18) .
F102 C102 1.326(16) .
C102 C103 1.43(2) .
F103 C103 1.347(16) .
C103 C104 1.36(2) .
F104 C104 1.344(15) .
C104 C105 1.35(2) .
F105 C105 1.336(16) .
C105 C106 1.410(19) .
F106 C106 1.358(15) .
C111 C112 1.40(2) .
C111 C116 1.418(19) .
C112 C113 1.42(2) .
C113 C114 1.35(3) .
C114 C115 1.43(3) .
C115 C116 1.36(2) .
C121 C126 1.39(2) .
C121 C122 1.41(2) .
C122 C123 1.41(2) .
C123 C124 1.40(3) .
C124 C125 1.37(2) .
C125 C126 1.35(2) .
C161 C162 1.36(2) .
C161 C166 1.44(2) .
C162 C163 1.41(2) .
C163 C164 1.36(2) .
C164 C165 1.37(2) .
C165 C166 1.39(2) .
C171 C176 1.39(2) .
C171 C172 1.44(2) .
C172 C173 1.41(2) .
C173 C174 1.36(2) .
C174 C175 1.41(2) .
C175 C176 1.39(2) .
C181 C182 1.375(18) .
C181 C186 1.41(2) .
F182 C182 1.320(15) .
C182 C183 1.425(19) .
F183 C183 1.336(16) .
C183 C184 1.38(2) .
F184 C184 1.338(16) .
C184 C185 1.39(2) .
F185 C185 1.340(16) .
C185 C186 1.33(2) .
F186 C186 1.368(16) .
C191 C192 1.41(2) .
C191 C196 1.42(2) .
C192 C193 1.44(3) .
C193 C194 1.33(3) .
C194 C195 1.38(2) .
C195 C196 1.34(2) .
C201 C202 1.39(3) .
C201 C206 1.42(3) .
C202 C203 1.40(3) .
C203 C204 1.44(4) .
C204 C205 1.39(3) .
C205 C206 1.34(3) .
C300 Cl31 1.65(3) .
C300 Cl32 2.08(9) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C1 Pt1 P1 C31 -63.1(6) . .
C51 Pt1 P1 C31 117.2(6) . .
P2 Pt1 P1 C31 -55(2) . .
Pt2 Pt1 P1 C31 -66.7(5) . .
C1 Pt1 P1 C41 177.7(7) . .
C51 Pt1 P1 C41 -2.1(7) . .
P2 Pt1 P1 C41 -174.0(18) . .
Pt2 Pt1 P1 C41 174.0(6) . .
C1 Pt1 P1 C1A 53.6(7) . .
C51 Pt1 P1 C1A -126.1(7) . .
P2 Pt1 P1 C1A 62(2) . .
Pt2 Pt1 P1 C1A 49.9(5) . .
C51 Pt1 C1 C2 -41(100) . .
P1 Pt1 C1 C2 -53(93) . .
P2 Pt1 C1 C2 128(93) . .
Pt2 Pt1 C1 C2 83(93) . .
C31 P1 C1A C2A 167.8(13) . .
C41 P1 C1A C2A -84.3(13) . .
Pt1 P1 C1A C2A 43.9(14) . .
P1 C1A C2A C3A -179.8(13) . .
C1A C2A C3A C4A 67(2) . .
C2A C3A C4A C5A 64(3) . .
C3A C4A C5A C6A 170.4(18) . .
C4A C5A C6A C7A -170.6(18) . .
C5A C6A C7A C8A 174.2(17) . .
C6A C7A C8A C9A -63(3) . .
C7A C8A C9A C10A -168.5(18) . .
C8A C9A C10A C11A -63(3) . .
C9A C10A C11A C12A -176.5(17) . .
C10A C11A C12A C13A -68(3) . .
C11A C12A C13A C14A -179.9(16) . .
C12A C13A C14A C15A -171(2) . .
C13A C14A C15A C16A 164.0(17) . .
C14A C15A C16A C17A 70(3) . .
C15A C16A C17A C18A 65(2) . .
C16A C17A C18A P3 -178.9(13) . .
P2 C1B C2B C3B 179.0(16) . .
C1B C2B C3B C4B 62(3) . .
C2B C3B C4B C5B 63(3) . .
C3B C4B C5B C6B 175(2) . .
C4B C5B C6B C7B 178(2) . .
C5B C6B C7B C8B -175(2) . .
C6B C7B C8B C9B -170(3) . .
C7B C8B C9B C10B -175(3) . .
C8B C9B C10B C11B -79(5) . .
C9B C10B C11B C12B -163(2) . .
C10B C11B C12B C13B -76(3) . .
C11B C12B C13B C14B -178.3(17) . .
C12B C13B C14B C15B -165(2) . .
C13B C14B C15B C16B -174(2) . .
C14B C15B C16B C17B -164(2) . .
C15B C16B C17B C18B 68(3) . .
C16B C17B C18B P4 -176.5(16) . .
P5 C1C C2C C3C -174.1(18) . .
C1C C2C C3C C4C 60(3) . .
C2C C3C C4C C5C 56(3) . .
C3C C4C C5C C6C 164(2) . .
C4C C5C C6C C7C 80(3) . .
C5C C6C C7C C8C 171(2) . .
C6C C7C C8C C9C 175(3) . .
C7C C8C C9C C10C -41(5) . .
C8C C9C C10C C11C -175(3) . .
C9C C10C C11C C12C -168(3) . .
C10C C11C C12C C13C 175(3) . .
C11C C12C C13C C14C 40(5) . .
C12C C13C C14C C15C -168(3) . .
C13C C14C C15C C16C -171(3) . .
C14C C15C C16C C17C -177(3) . .
C15C C16C C17C C18C -30(4) . .
C16C C17C C18C P6 -178.0(18) . 2_166
C1 Pt1 Pt2 C12 127(9) . .
C51 Pt1 Pt2 C12 -68(9) . .
P1 Pt1 Pt2 C12 171(8) . .
P2 Pt1 Pt2 C12 -8(8) . .
C1 Pt1 Pt2 C101 -30(10) . .
C51 Pt1 Pt2 C101 136(10) . .
P1 Pt1 Pt2 C101 15(9) . .
P2 Pt1 Pt2 C101 -164(9) . .
C1 Pt1 Pt2 P4 -28(4) . .
C51 Pt1 Pt2 P4 137(5) . .
P1 Pt1 Pt2 P4 16.40(14) . .
P2 Pt1 Pt2 P4 -162.70(14) . .
C1 Pt1 Pt2 P3 152(4) . .
C51 Pt1 Pt2 P3 -43(5) . .
P1 Pt1 Pt2 P3 -163.71(13) . .
P2 Pt1 Pt2 P3 17.18(14) . .
C2B C1B P2 C61 -83.8(16) . .
C2B C1B P2 C71 169.3(15) . .
C2B C1B P2 Pt1 45.2(16) . .
C1 Pt1 P2 C61 179.7(7) . .
C51 Pt1 P2 C61 -0.6(7) . .
P1 Pt1 P2 C61 171.3(18) . .
Pt2 Pt1 P2 C61 -176.6(6) . .
C1 Pt1 P2 C71 -59.8(7) . .
C51 Pt1 P2 C71 120.0(6) . .
P1 Pt1 P2 C71 -68(2) . .
Pt2 Pt1 P2 C71 -56.1(5) . .
C1 Pt1 P2 C1B 55.5(7) . .
C51 Pt1 P2 C1B -124.8(7) . .
P1 Pt1 P2 C1B 47(2) . .
Pt2 Pt1 P2 C1B 59.2(6) . .
Pt1 C1 C2 C3 -84(96) . .
Pt3 C1' C2' C3' 23(16) . .
C2' C1' Pt3 C181 1(12) . .
C2' C1' Pt3 P5 109(6) . .
C2' C1' Pt3 P6 -72(6) . .
C2' C1' Pt3 Pt3 -11(5) . 2_166
C17A C18A P3 C81 170.8(13) . .
C17A C18A P3 C91 -84.1(14) . .
C17A C18A P3 Pt2 47.3(14) . .
C12 Pt2 P3 C81 -65.3(6) . .
C101 Pt2 P3 C81 113.4(6) . .
P4 Pt2 P3 C81 -65.4(17) . .
Pt1 Pt2 P3 C81 -66.7(5) . .
C12 Pt2 P3 C18A 50.1(7) . .
C101 Pt2 P3 C18A -131.3(6) . .
P4 Pt2 P3 C18A 50.0(17) . .
Pt1 Pt2 P3 C18A 48.7(5) . .
C12 Pt2 P3 C91 173.6(8) . .
C101 Pt2 P3 C91 -7.7(7) . .
P4 Pt2 P3 C91 173.6(16) . .
Pt1 Pt2 P3 C91 172.2(6) . .
C1 C2 C3 C4 135(52) . .
C1' C2' C3' C4' -4(28) . .
C17B C18B P4 C111 -88.2(16) . .
C17B C18B P4 C121 165.4(16) . .
C17B C18B P4 Pt2 41.8(17) . .
C12 Pt2 P4 C111 178.9(7) . .
C101 Pt2 P4 C111 0.2(7) . .
P3 Pt2 P4 C111 179(100) . .
Pt1 Pt2 P4 C111 -179.7(6) . .
C12 Pt2 P4 C121 -60.7(7) . .
C101 Pt2 P4 C121 120.6(6) . .
P3 Pt2 P4 C121 -60.6(17) . .
Pt1 Pt2 P4 C121 -59.3(5) . .
C12 Pt2 P4 C18B 54.5(7) . .
C101 Pt2 P4 C18B -124.2(7) . .
P3 Pt2 P4 C18B 54.5(17) . .
Pt1 Pt2 P4 C18B 55.9(6) . .
C2 C3 C4 C5 -165(41) . .
C2' C3' C4' C5' 6(43) . .
C2C C1C P5 C191 -77.6(17) . .
C2C C1C P5 C201 174.6(16) . .
C2C C1C P5 Pt3 52.8(17) . .
C1' Pt3 P5 C191 -178.7(7) . .
C181 Pt3 P5 C191 -2.6(7) . .
P6 Pt3 P5 C191 173.0(16) . .
Pt3 Pt3 P5 C191 -160.8(6) 2_166 .
C1' Pt3 P5 C1C 56.9(8) . .
C181 Pt3 P5 C1C -126.9(8) . .
P6 Pt3 P5 C1C 48.6(19) . .
Pt3 Pt3 P5 C1C 74.8(7) 2_166 .
C1' Pt3 P5 C201 -59.6(7) . .
C181 Pt3 P5 C201 116.6(7) . .
P6 Pt3 P5 C201 -67.9(18) . .
Pt3 Pt3 P5 C201 -41.6(6) 2_166 .
C3 C4 C5 C6 0(46) . .
C3' C4' C5' C6' -3(78) . .
C1' Pt3 P6 C171 167.8(7) . .
C181 Pt3 P6 C171 -8.3(7) . .
P5 Pt3 P6 C171 176.1(17) . .
Pt3 Pt3 P6 C171 149.5(6) 2_166 .
C1' Pt3 P6 C161 -73.4(7) . .
C181 Pt3 P6 C161 110.5(7) . .
P5 Pt3 P6 C161 -65.1(18) . .
Pt3 Pt3 P6 C161 -91.7(6) 2_166 .
C1' Pt3 P6 C18C 44.6(7) . 2_166
C181 Pt3 P6 C18C -131.5(7) . 2_166
P5 Pt3 P6 C18C 52.9(19) . 2_166
Pt3 Pt3 P6 C18C 26.2(6) 2_166 2_166
C4 C5 C6 C7 -157(17) . .
C4' C5' C6' C6' -92(100) . 2_166
C5 C6 C7 C8 -42(85) . .
C6 C7 C8 C9 -162(56) . .
C7 C8 C9 C10 -148(100) . .
C8 C9 C10 C11 -24(100) . .
C9 C10 C11 C12 -49(77) . .
C10 C11 C12 Pt2 54(64) . .
C101 Pt2 C12 C11 103(43) . .
P4 Pt2 C12 C11 -7(38) . .
P3 Pt2 C12 C11 173(100) . .
Pt1 Pt2 C12 C11 -32(33) . .
C41 P1 C31 C32 134.6(12) . .
C1A P1 C31 C32 -113.8(12) . .
Pt1 P1 C31 C32 8.6(13) . .
C41 P1 C31 C36 -49.8(13) . .
C1A P1 C31 C36 61.8(13) . .
Pt1 P1 C31 C36 -175.9(10) . .
C36 C31 C32 C33 3(2) . .
P1 C31 C32 C33 178.1(11) . .
C31 C32 C33 C34 -2(2) . .
C32 C33 C34 C35 -2(3) . .
C33 C34 C35 C36 4(3) . .
C34 C35 C36 C31 -3(3) . .
C32 C31 C36 C35 0(2) . .
P1 C31 C36 C35 -175.9(14) . .
C31 P1 C41 C42 -57.4(13) . .
C1A P1 C41 C42 -165.0(12) . .
Pt1 P1 C41 C42 68.4(12) . .
C31 P1 C41 C46 124.1(13) . .
C1A P1 C41 C46 16.6(14) . .
Pt1 P1 C41 C46 -110.1(12) . .
C46 C41 C42 C43 5(2) . .
P1 C41 C42 C43 -173.3(12) . .
C41 C42 C43 C44 -3(2) . .
C42 C43 C44 C45 1(3) . .
C43 C44 C45 C46 1(3) . .
C42 C41 C46 C45 -4(2) . .
P1 C41 C46 C45 174.7(13) . .
C44 C45 C46 C41 1(3) . .
C1 Pt1 C51 C56 58(25) . .
P1 Pt1 C51 C56 69.8(12) . .
P2 Pt1 C51 C56 -110.8(12) . .
Pt2 Pt1 C51 C56 -51(5) . .
C1 Pt1 C51 C52 -119(25) . .
P1 Pt1 C51 C52 -107.4(12) . .
P2 Pt1 C51 C52 72.0(12) . .
Pt2 Pt1 C51 C52 132(4) . .
C56 C51 C52 F52 -178.4(13) . .
Pt1 C51 C52 F52 -1.0(19) . .
C56 C51 C52 C53 -3(2) . .
Pt1 C51 C52 C53 174.3(13) . .
F52 C52 C53 F53 -3(2) . .
C51 C52 C53 F53 -178.6(15) . .
F52 C52 C53 C54 179.0(15) . .
C51 C52 C53 C54 4(3) . .
F53 C53 C54 F54 5(3) . .
C52 C53 C54 F54 -176.7(15) . .
F53 C53 C54 C55 177.3(16) . .
C52 C53 C54 C55 -5(3) . .
F54 C54 C55 F55 -3(3) . .
C53 C54 C55 F55 -174.5(16) . .
F54 C54 C55 C56 177.9(15) . .
C53 C54 C55 C56 6(3) . .
C52 C51 C56 F56 179.9(13) . .
Pt1 C51 C56 F56 2(2) . .
C52 C51 C56 C55 4(2) . .
Pt1 C51 C56 C55 -173.2(12) . .
F55 C55 C56 F56 -1(2) . .
C54 C55 C56 F56 178.0(15) . .
F55 C55 C56 C51 174.5(14) . .
C54 C55 C56 C51 -6(3) . .
C71 P2 C61 C66 -60.2(15) . .
C1B P2 C61 C66 -166.6(14) . .
Pt1 P2 C61 C66 67.6(15) . .
C71 P2 C61 C62 126.4(14) . .
C1B P2 C61 C62 20.0(16) . .
Pt1 P2 C61 C62 -105.8(13) . .
C66 C61 C62 C63 3(3) . .
P2 C61 C62 C63 176.6(13) . .
C61 C62 C63 C64 0(3) . .
C62 C63 C64 C65 -5(3) . .
C63 C64 C65 C66 6(3) . .
C64 C65 C66 C61 -3(3) . .
C62 C61 C66 C65 -2(3) . .
P2 C61 C66 C65 -175.5(15) . .
C61 P2 C71 C72 138.2(12) . .
C1B P2 C71 C72 -110.4(13) . .
Pt1 P2 C71 C72 10.1(13) . .
C61 P2 C71 C76 -46.5(15) . .
C1B P2 C71 C76 64.9(14) . .
Pt1 P2 C71 C76 -174.6(12) . .
C76 C71 C72 C73 -3(2) . .
P2 C71 C72 C73 172.0(12) . .
C71 C72 C73 C74A 3(2) . .
C72 C73 C74A C75 -1(3) . .
C73 C74A C75 C76 0(3) . .
C74A C75 C76 C71 -1(3) . .
C72 C71 C76 C75 2(3) . .
P2 C71 C76 C75 -173.0(15) . .
C18A P3 C81 C86 67.7(13) . .
C91 P3 C81 C86 -41.4(14) . .
Pt2 P3 C81 C86 -172.5(11) . .
C18A P3 C81 C82 -108.5(12) . .
C91 P3 C81 C82 142.3(11) . .
Pt2 P3 C81 C82 11.2(12) . .
C86 C81 C82 C83 0(2) . .
P3 C81 C82 C83 176.2(12) . .
C81 C82 C83 C84 2(2) . .
C82 C83 C84 C85 -3(3) . .
C83 C84 C85 C86 2(3) . .
C84 C85 C86 C81 0(3) . .
C82 C81 C86 C85 -1(2) . .
P3 C81 C86 C85 -177.3(13) . .
C81 P3 C91 C92 122.8(13) . .
C18A P3 C91 C92 16.5(14) . .
Pt2 P3 C91 C92 -109.1(12) . .
C81 P3 C91 C96 -59.9(13) . .
C18A P3 C91 C96 -166.2(11) . .
Pt2 P3 C91 C96 68.3(12) . .
C96 C91 C92 C93 0(2) . .
P3 C91 C92 C93 177.0(13) . .
C91 C92 C93 C94 4(3) . .
C92 C93 C94 C95 -5(3) . .
C93 C94 C95 C96 3(3) . .
C94 C95 C96 C91 1(3) . .
C92 C91 C96 C95 -2(2) . .
P3 C91 C96 C95 -179.3(12) . .
C12 Pt2 C101 C106 -47(26) . .
P4 Pt2 C101 C106 63.5(12) . .
P3 Pt2 C101 C106 -116.4(11) . .
Pt1 Pt2 C101 C106 65(9) . .
C12 Pt2 C101 C102 134(25) . .
P4 Pt2 C101 C102 -115.8(11) . .
P3 Pt2 C101 C102 64.4(12) . .
Pt1 Pt2 C101 C102 -114(9) . .
C106 C101 C102 F102 -177.7(12) . .
Pt2 C101 C102 F102 1.7(19) . .
C106 C101 C102 C103 3(2) . .
Pt2 C101 C102 C103 -177.6(11) . .
F102 C102 C103 F103 -4(2) . .
C101 C102 C103 F103 175.7(13) . .
F102 C102 C103 C104 179.4(13) . .
C101 C102 C103 C104 -1(2) . .
F103 C103 C104 F104 5(2) . .
C102 C103 C104 F104 -178.6(13) . .
F103 C103 C104 C105 -177.6(14) . .
C102 C103 C104 C105 -1(2) . .
F104 C104 C105 F105 0(2) . .
C103 C104 C105 F105 -177.8(14) . .
F104 C104 C105 C106 178.7(13) . .
C103 C104 C105 C106 1(2) . .
C102 C101 C106 F106 -179.3(12) . .
Pt2 C101 C106 F106 1.3(18) . .
C102 C101 C106 C105 -3(2) . .
Pt2 C101 C106 C105 177.6(11) . .
F105 C105 C106 F106 -4(2) . .
C104 C105 C106 F106 177.6(13) . .
F105 C105 C106 C101 179.8(13) . .
C104 C105 C106 C101 1(2) . .
C121 P4 C111 C112 126.0(13) . .
C18B P4 C111 C112 19.5(15) . .
Pt2 P4 C111 C112 -106.4(13) . .
C121 P4 C111 C116 -55.7(13) . .
C18B P4 C111 C116 -162.2(12) . .
Pt2 P4 C111 C116 71.9(13) . .
C116 C111 C112 C113 0(2) . .
P4 C111 C112 C113 178.8(14) . .
C111 C112 C113 C114 0(3) . .
C112 C113 C114 C115 0(3) . .
C113 C114 C115 C116 1(3) . .
C114 C115 C116 C111 -1(3) . .
C112 C111 C116 C115 0(2) . .
P4 C111 C116 C115 -178.3(13) . .
C111 P4 C121 C126 132.8(13) . .
C18B P4 C121 C126 -116.1(13) . .
Pt2 P4 C121 C126 4.0(14) . .
C111 P4 C121 C122 -46.9(13) . .
C18B P4 C121 C122 64.2(13) . .
Pt2 P4 C121 C122 -175.7(10) . .
C126 C121 C122 C123 4(2) . .
P4 C121 C122 C123 -176.1(13) . .
C121 C122 C123 C124 -1(3) . .
C122 C123 C124 C125 -4(3) . .
C123 C124 C125 C126 6(3) . .
C124 C125 C126 C121 -4(3) . .
C122 C121 C126 C125 -2(2) . .
P4 C121 C126 C125 178.5(14) . .
C171 P6 C161 C162 141.7(14) . .
C18C P6 C161 C162 -107.2(15) 2_166 .
Pt3 P6 C161 C162 14.4(16) . .
C171 P6 C161 C166 -39.4(14) . .
C18C P6 C161 C166 71.7(14) 2_166 .
Pt3 P6 C161 C166 -166.7(11) . .
C166 C161 C162 C163 0(2) . .
P6 C161 C162 C163 178.8(13) . .
C161 C162 C163 C164 -1(3) . .
C162 C163 C164 C165 2(3) . .
C163 C164 C165 C166 -3(3) . .
C164 C165 C166 C161 2(3) . .
C162 C161 C166 C165 0(2) . .
P6 C161 C166 C165 -179.4(13) . .
C161 P6 C171 C176 -60.0(13) . .
C18C P6 C171 C176 -169.7(12) 2_166 .
Pt3 P6 C171 C176 64.7(13) . .
C161 P6 C171 C172 122.1(13) . .
C18C P6 C171 C172 12.4(14) 2_166 .
Pt3 P6 C171 C172 -113.2(12) . .
C176 C171 C172 C173 -4(2) . .
P6 C171 C172 C173 174.1(13) . .
C171 C172 C173 C174 1(3) . .
C172 C173 C174 C175 1(3) . .
C173 C174 C175 C176 1(3) . .
C174 C175 C176 C171 -4(2) . .
C172 C171 C176 C175 6(2) . .
P6 C171 C176 C175 -172.2(12) . .
C1' Pt3 C181 C182 -6(8) . .
P5 Pt3 C181 C182 -114.5(11) . .
P6 Pt3 C181 C182 65.9(11) . .
Pt3 Pt3 C181 C182 3.5(17) 2_166 .
C1' Pt3 C181 C186 -180(100) . .
P5 Pt3 C181 C186 72.2(12) . .
P6 Pt3 C181 C186 -107.4(12) . .
Pt3 Pt3 C181 C186 -169.8(8) 2_166 .
C186 C181 C182 F182 -177.0(12) . .
Pt3 C181 C182 F182 8.8(18) . .
C186 C181 C182 C183 1.2(19) . .
Pt3 C181 C182 C183 -173.0(11) . .
F182 C182 C183 F183 -4.8(19) . .
C181 C182 C183 F183 176.9(13) . .
F182 C182 C183 C184 178.7(13) . .
C181 C182 C183 C184 0(2) . .
F183 C183 C184 F184 0(2) . .
C182 C183 C184 F184 176.7(13) . .
F183 C183 C184 C185 -178.6(14) . .
C182 C183 C184 C185 -2(2) . .
F184 C184 C185 C186 -176.7(15) . .
C183 C184 C185 C186 2(2) . .
F184 C184 C185 F185 4(2) . .
C183 C184 C185 F185 -177.6(14) . .
F185 C185 C186 F186 -2(2) . .
C184 C185 C186 F186 178.9(14) . .
F185 C185 C186 C181 179.3(14) . .
C184 C185 C186 C181 0(3) . .
C182 C181 C186 C185 -1(2) . .
Pt3 C181 C186 C185 172.7(13) . .
C182 C181 C186 F186 179.6(11) . .
Pt3 C181 C186 F186 -6.4(18) . .
C1C P5 C191 C192 7.8(17) . .
C201 P5 C191 C192 117.0(15) . .
Pt3 P5 C191 C192 -118.3(13) . .
C1C P5 C191 C196 -171.3(12) . .
C201 P5 C191 C196 -62.1(13) . .
Pt3 P5 C191 C196 62.6(13) . .
C196 C191 C192 C193 -2(3) . .
P5 C191 C192 C193 179.1(14) . .
C191 C192 C193 C194 4(3) . .
C192 C193 C194 C195 -6(3) . .
C193 C194 C195 C196 5(3) . .
C194 C195 C196 C191 -3(2) . .
C192 C191 C196 C195 1(2) . .
P5 C191 C196 C195 -179.7(12) . .
C191 P5 C201 C202 115.4(14) . .
C1C P5 C201 C202 -133.0(14) . .
Pt3 P5 C201 C202 -12.7(15) . .
C191 P5 C201 C206 -61.9(15) . .
C1C P5 C201 C206 49.7(15) . .
Pt3 P5 C201 C206 170.0(12) . .
C206 C201 C202 C203 0(3) . .
P5 C201 C202 C203 -177.2(14) . .
C201 C202 C203 C204 0(3) . .
C202 C203 C204 C205 1(3) . .
C203 C204 C205 C206 -1(4) . .
C204 C205 C206 C201 1(3) . .
C202 C201 C206 C205 0(3) . .
P5 C201 C206 C205 176.8(16) . .
