#------------------------------------------------------------------------------
#$Date: 2016-03-22 10:32:06 +0200 (Tue, 22 Mar 2016) $
#$Revision: 178874 $
#$URL: svn://www.crystallography.net/cod/cif/4/11/03/4110392.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4110392
loop_
_publ_author_name
'H. Martin Dietrich'
'Hilde Grove'
'Karl W. Törnroos'
'Reiner Anwander'
_publ_contact_author_address
;
Department of Chemistry
University of Bergen
Allégaten 41
N-5007 Bergen
Norway
;
_publ_contact_author_name        'Reiner Anwander'
_publ_section_title
;
 Multiple C-H Bond Activation in Group 3 Chemistry: Synthesis and
 Structural Characterization of an Yttrium-Aluminum-Methine Cluster
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              1458
_journal_page_last               1459
_journal_paper_doi               10.1021/ja057618z
_journal_volume                  128
_journal_year                    2006
_chemical_formula_moiety         'C28 H52 Al2 Y2'
_chemical_formula_sum            'C28 H52 Al2 Y2'
_chemical_formula_weight         620.48
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                110.4430(10)
_cell_angle_beta                 91.2250(10)
_cell_angle_gamma                109.7880(10)
_cell_formula_units_Z            4
_cell_length_a                   10.9530(4)
_cell_length_b                   15.6798(6)
_cell_length_c                   21.1344(8)
_cell_measurement_reflns_used    16085
_cell_measurement_temperature    153(2)
_cell_measurement_theta_max      29.57
_cell_measurement_theta_min      2.37
_cell_volume                     3159.8(2)
_computing_cell_refinement
;
Bruker (2001). SAINT, version 6.02a, Bruker AXS Inc., Madison, 
Wisconsin, USA.
;
_computing_data_collection
;
Bruker (1999). SMART, version 5.059, Bruker AXS Inc., Madison, 
Wisconsin, USA.
;
_computing_data_reduction
;
Bruker (2001). SAINT, version 6.02a, Bruker AXS Inc., Madison, 
Wisconsin, USA.
;
_computing_molecular_graphics
;
Bruker AXS (2003). SHELXTL. Version 6.14. Bruker AXS Inc., Madison, 
Wisconsin, USA.
;
_computing_publication_material
;
Bruker AXS (2003). SHELXTL. Version 6.14. Bruker AXS Inc., Madison, 
Wisconsin, USA.
;
_computing_structure_refinement
;
Sheldrick, G. M. (1997). SHELXS97 and SHELXL97. University of 
Göttingen, Germany.
;
_computing_structure_solution
;     
Sheldrick, G. M. (1997). SHELXS97 and SHELXL97. University of 
Göttingen, Germany. 
;
_diffrn_ambient_temperature      153(2)
_diffrn_detector_area_resol_mean '48 \um'
_diffrn_measured_fraction_theta_full 0.996
_diffrn_measured_fraction_theta_max 0.996
_diffrn_measurement_device_type  'Bruker-AXS SMART 2K CCD'
_diffrn_measurement_method       'omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'normal-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0230
_diffrn_reflns_av_sigmaI/netI    0.0271
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_k_min       -21
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            51357
_diffrn_reflns_theta_full        29.59
_diffrn_reflns_theta_max         29.59
_diffrn_reflns_theta_min         1.46
_diffrn_standards_decay_%        0
_diffrn_standards_interval_count 1
_diffrn_standards_interval_time  '28 h'
_diffrn_standards_number         696
_exptl_absorpt_coefficient_mu    3.723
_exptl_absorpt_correction_T_max  0.52837
_exptl_absorpt_correction_T_min  0.27850
_exptl_absorpt_correction_type   numerical
_exptl_absorpt_process_details
; 
Bruker AXS (2003). SHELXTL. Version 6.14. 
Bruker AXS Inc., Madison, Wisconsin, USA. 
;
_exptl_crystal_colour            colourless
_exptl_crystal_density_diffrn    1.304
_exptl_crystal_description       prism
_exptl_crystal_F_000             1296
_exptl_crystal_size_max          0.44
_exptl_crystal_size_mid          0.23
_exptl_crystal_size_min          0.21
_refine_diff_density_max         1.025
_refine_diff_density_min         -0.631
_refine_diff_density_rms         0.085
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.119
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     633
_refine_ls_number_reflns         17672
_refine_ls_number_restraints     8
_refine_ls_restrained_S_all      1.121
_refine_ls_R_factor_all          0.0443
_refine_ls_R_factor_gt           0.0344
_refine_ls_shift/su_max          0.002
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0278P)²+5.9284P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.0907
_refine_ls_wR_factor_ref         0.0939
_reflns_number_gt                14922
_reflns_number_total             17672
_reflns_threshold_expression     I>2σ(I)
_cod_data_source_file            ja057618zsi20051108_120907.cif
_cod_data_source_block           3
_cod_database_code               4110392
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Y1 Y 0.25922(3) 0.362881(18) 0.359308(13) 0.02133(6) Uani 1 1 d .
Y2 Y 0.43597(3) 0.271587(18) 0.504287(13) 0.02102(6) Uani 1 1 d .
Y3 Y 0.20000(2) 0.727338(18) 0.002261(13) 0.02048(6) Uani 1 1 d .
Y4 Y -0.09891(2) 0.647229(17) 0.131686(13) 0.01991(6) Uani 1 1 d .
Al1 Al 0.16669(8) 0.27765(6) 0.46786(4) 0.02458(17) Uani 1 1 d .
Al2 Al 0.44267(9) 0.24994(6) 0.35447(4) 0.02322(16) Uani 1 1 d .
Al3 Al 0.20241(8) 0.74122(6) 0.15133(4) 0.02136(16) Uani 1 1 d .
Al4 Al -0.06546(8) 0.74415(6) 0.02550(4) 0.02233(16) Uani 1 1 d .
C1 C 0.2896(3) 0.24525(19) 0.40424(13) 0.0218(5) Uani 1 1 d D
H1 H 0.243(3) 0.1764(14) 0.3772(15) 0.026 Uiso 1 1 d D
C2 C 0.1359(3) 0.4007(2) 0.46744(17) 0.0341(7) Uani 1 1 d .
H2A H 0.0592 0.4056 0.4893 0.041 Uiso 1 1 calc R
H2B H 0.1204 0.3955 0.4202 0.041 Uiso 1 1 calc R
H2C H 0.2135 0.4592 0.4927 0.041 Uiso 1 1 calc R
C3 C 0.4944(3) 0.3655(2) 0.32225(16) 0.0301(6) Uani 1 1 d .
H3A H 0.5366 0.4270 0.3617 0.036 Uiso 1 1 calc R
H3B H 0.4156 0.3664 0.3002 0.036 Uiso 1 1 calc R
H3C H 0.5557 0.3578 0.2895 0.036 Uiso 1 1 calc R
C4 C 0.6135(3) 0.2989(2) 0.42154(16) 0.0316(6) Uani 1 1 d .
H4A H 0.6830 0.2861 0.3958 0.038 Uiso 1 1 calc R
H4B H 0.5984 0.2644 0.4531 0.038 Uiso 1 1 calc R
H4C H 0.6402 0.3694 0.4476 0.038 Uiso 1 1 calc R
C5 C 0.2614(3) 0.3397(2) 0.56755(14) 0.0284(6) Uani 1 1 d .
H5A H 0.3300 0.4034 0.5754 0.034 Uiso 1 1 calc R
H5B H 0.3013 0.2966 0.5759 0.034 Uiso 1 1 calc R
H5C H 0.1979 0.3488 0.5988 0.034 Uiso 1 1 calc R
C6 C -0.0035(3) 0.1721(3) 0.45641(19) 0.0408(8) Uani 1 1 d .
H6A H -0.0622 0.1996 0.4835 0.061 Uiso 1 1 calc R
H6B H 0.0103 0.1235 0.4720 0.061 Uiso 1 1 calc R
H6C H -0.0431 0.1405 0.4080 0.061 Uiso 1 1 calc R
C7 C 0.4292(4) 0.1294(2) 0.27763(17) 0.0386(7) Uani 1 1 d .
H7A H 0.4535 0.0862 0.2952 0.058 Uiso 1 1 calc R
H7B H 0.4888 0.1463 0.2462 0.058 Uiso 1 1 calc R
H7C H 0.3387 0.0958 0.2532 0.058 Uiso 1 1 calc R
C8 C 0.3963(3) 0.54754(19) 0.41742(14) 0.0226(5) Uani 1 1 d D
H8A H 0.438(3) 0.557(3) 0.3822(14) 0.034 Uiso 1 1 d D
H8B H 0.333(3) 0.571(2) 0.4323(17) 0.034 Uiso 1 1 d D
H8C H 0.447(3) 0.541(3) 0.4512(15) 0.034 Uiso 1 1 d D
C9 C 0.1849(3) 0.3771(2) 0.24640(16) 0.0343(7) Uani 1 1 d .
C10 C 0.1794(3) 0.2799(2) 0.22623(15) 0.0337(7) Uani 1 1 d .
C11 C 0.0789(3) 0.2287(2) 0.25399(17) 0.0368(7) Uani 1 1 d .
C12 C 0.0190(3) 0.2935(3) 0.29036(18) 0.0412(8) Uani 1 1 d .
C13 C 0.0847(4) 0.3852(3) 0.28548(17) 0.0381(7) Uani 1 1 d .
C14 C 0.2773(4) 0.4562(3) 0.2263(2) 0.0634(14) Uani 1 1 d .
H14A H 0.2286 0.4677 0.1927 0.095 Uiso 1 1 calc R
H14B H 0.3473 0.4355 0.2063 0.095 Uiso 1 1 calc R
H14C H 0.3159 0.5168 0.2669 0.095 Uiso 1 1 calc R
C15 C 0.2575(5) 0.2353(4) 0.17628(19) 0.0711(15) Uani 1 1 d .
H15A H 0.2029 0.1975 0.1311 0.107 Uiso 1 1 calc R
H15B H 0.2856 0.1919 0.1919 0.107 Uiso 1 1 calc R
H15C H 0.3350 0.2874 0.1733 0.107 Uiso 1 1 calc R
C16 C 0.0356(5) 0.1207(3) 0.2405(3) 0.0765(18) Uani 1 1 d .
H16A H -0.0415 0.0841 0.2045 0.115 Uiso 1 1 calc R
H16B H 0.0131 0.1100 0.2824 0.115 Uiso 1 1 calc R
H16C H 0.1072 0.0980 0.2258 0.115 Uiso 1 1 calc R
C17 C -0.1055(4) 0.2664(5) 0.3211(3) 0.0839(19) Uani 1 1 d .
H17A H -0.1819 0.2331 0.2847 0.126 Uiso 1 1 calc R
H17B H -0.1125 0.3260 0.3541 0.126 Uiso 1 1 calc R
H17C H -0.1026 0.2227 0.3443 0.126 Uiso 1 1 calc R
C18 C 0.0489(6) 0.4746(4) 0.3131(3) 0.0758(16) Uani 1 1 d .
H18A H 0.0092 0.4838 0.2752 0.114 Uiso 1 1 calc R
H18B H 0.1282 0.5323 0.3374 0.114 Uiso 1 1 calc R
H18C H -0.0141 0.4658 0.3447 0.114 Uiso 1 1 calc R
C19 C 0.4921(3) 0.1151(2) 0.48654(16) 0.0319(6) Uani 1 1 d .
C20 C 0.5558(3) 0.1836(2) 0.55305(16) 0.0332(7) Uani 1 1 d .
C21 C 0.4600(3) 0.1964(2) 0.59464(15) 0.0323(6) Uani 1 1 d .
C22 C 0.3345(3) 0.1348(2) 0.55383(16) 0.0309(6) Uani 1 1 d .
C23 C 0.3544(3) 0.0856(2) 0.48707(15) 0.0306(6) Uani 1 1 d .
C24 C 0.5562(4) 0.0695(3) 0.42865(19) 0.0447(9) Uani 1 1 d .
H24A H 0.5561 0.0074 0.4296 0.067 Uiso 1 1 calc R
H24B H 0.6469 0.1140 0.4337 0.067 Uiso 1 1 calc R
H24C H 0.5073 0.0573 0.3850 0.067 Uiso 1 1 calc R
C25 C 0.7022(4) 0.2304(3) 0.5768(2) 0.0530(10) Uani 1 1 d .
H25A H 0.7319 0.1868 0.5914 0.079 Uiso 1 1 calc R
H25B H 0.7230 0.2930 0.6153 0.079 Uiso 1 1 calc R
H25C H 0.7469 0.2417 0.5391 0.079 Uiso 1 1 calc R
C26 C 0.4836(5) 0.2567(3) 0.67011(17) 0.0481(9) Uani 1 1 d .
H26A H 0.4803 0.2150 0.6959 0.072 Uiso 1 1 calc R
H26B H 0.4155 0.2848 0.6809 0.072 Uiso 1 1 calc R
H26C H 0.5701 0.3096 0.6826 0.072 Uiso 1 1 calc R
C27 C 0.2049(4) 0.1144(3) 0.5799(2) 0.0481(9) Uani 1 1 d .
H27A H 0.1841 0.0559 0.5910 0.072 Uiso 1 1 calc R
H27B H 0.1356 0.1036 0.5447 0.072 Uiso 1 1 calc R
H27C H 0.2107 0.1706 0.6211 0.072 Uiso 1 1 calc R
C28 C 0.2483(4) 0.0078(2) 0.42956(19) 0.0471(9) Uani 1 1 d .
H28A H 0.2207 -0.0539 0.4368 0.071 Uiso 1 1 calc R
H28B H 0.2822 -0.0011 0.3861 0.071 Uiso 1 1 calc R
H28C H 0.1730 0.0279 0.4283 0.071 Uiso 1 1 calc R
C29 C 0.0736(3) 0.76123(19) 0.09561(13) 0.0203(5) Uani 1 1 d D
H29 H 0.092(3) 0.8299(14) 0.1235(14) 0.024 Uiso 1 1 d D
C30 C 0.3251(3) 0.6860(2) 0.09174(16) 0.0301(6) Uani 1 1 d .
H30A H 0.3998 0.6914 0.1212 0.036 Uiso 1 1 calc R
H30B H 0.3571 0.7233 0.0628 0.036 Uiso 1 1 calc R
H30C H 0.2767 0.6170 0.0629 0.036 Uiso 1 1 calc R
C31 C -0.0294(3) 0.6758(2) -0.07138(15) 0.0289(6) Uani 1 1 d .
H31A H -0.0528 0.6059 -0.0811 0.035 Uiso 1 1 calc R
H31B H 0.0640 0.7053 -0.0737 0.035 Uiso 1 1 calc R
H31C H -0.0824 0.6840 -0.1052 0.035 Uiso 1 1 calc R
C32 C -0.2373(3) 0.6306(2) 0.01919(16) 0.0306(6) Uani 1 1 d .
H32A H -0.3074 0.6281 -0.0118 0.037 Uiso 1 1 calc R
H32B H -0.2626 0.6414 0.0647 0.037 Uiso 1 1 calc R
H32C H -0.2233 0.5685 0.0017 0.037 Uiso 1 1 calc R
C33 C 0.1127(3) 0.6212(2) 0.17648(15) 0.0275(6) Uani 1 1 d .
H33A H 0.0980 0.5611 0.1366 0.033 Uiso 1 1 calc R
H33B H 0.0282 0.6218 0.1906 0.033 Uiso 1 1 calc R
H33C H 0.1692 0.6237 0.2142 0.033 Uiso 1 1 calc R
C34 C 0.3091(3) 0.8527(2) 0.23398(16) 0.0345(7) Uani 1 1 d .
H34A H 0.2560 0.8607 0.2708 0.052 Uiso 1 1 calc R
H34B H 0.3393 0.9125 0.2241 0.052 Uiso 1 1 calc R
H34C H 0.3853 0.8406 0.2482 0.052 Uiso 1 1 calc R
C35 C -0.1017(3) 0.8627(2) 0.03419(17) 0.0328(6) Uani 1 1 d .
H35A H -0.0311 0.9055 0.0190 0.049 Uiso 1 1 calc R
H35B H -0.1063 0.8976 0.0821 0.049 Uiso 1 1 calc R
H35C H -0.1856 0.8437 0.0058 0.049 Uiso 1 1 calc R
C36 C -0.1697(3) 0.45975(19) 0.07279(14) 0.0220(5) Uani 1 1 d D
H36B H -0.145(3) 0.445(3) 0.1086(14) 0.033 Uiso 1 1 d D
H36A H -0.2563(19) 0.440(3) 0.0589(17) 0.033 Uiso 1 1 d D
H36C H -0.118(3) 0.459(3) 0.0382(14) 0.033 Uiso 1 1 d D
C37 C 0.4234(3) 0.8093(2) -0.03251(19) 0.0359(7) Uani 1 1 d .
C38 C 0.4177(3) 0.8798(2) 0.03039(17) 0.0313(6) Uani 1 1 d .
C39 C 0.3171(3) 0.9130(2) 0.01884(16) 0.0283(6) Uani 1 1 d .
C40 C 0.2604(3) 0.8640(2) -0.05095(15) 0.0283(6) Uani 1 1 d .
C41 C 0.3255(3) 0.7995(2) -0.08296(16) 0.0321(6) Uani 1 1 d .
C42 C 0.5190(4) 0.7577(3) -0.0453(3) 0.0569(11) Uani 1 1 d .
H42A H 0.6004 0.7991 -0.0546 0.085 Uiso 1 1 calc R
H42B H 0.4806 0.6956 -0.0847 0.085 Uiso 1 1 calc R
H42C H 0.5384 0.7448 -0.0048 0.085 Uiso 1 1 calc R
C43 C 0.5126(4) 0.9239(3) 0.0960(2) 0.0520(10) Uani 1 1 d .
H43A H 0.5642 0.9927 0.1049 0.078 Uiso 1 1 calc R
H43B H 0.5717 0.8879 0.0922 0.078 Uiso 1 1 calc R
H43C H 0.4636 0.9197 0.1338 0.078 Uiso 1 1 calc R
C44 C 0.2891(4) 0.9958(2) 0.07104(19) 0.0429(8) Uani 1 1 d .
H44A H 0.3616 1.0578 0.0793 0.064 Uiso 1 1 calc R
H44B H 0.2804 0.9848 0.1139 0.064 Uiso 1 1 calc R
H44C H 0.2072 0.9984 0.0538 0.064 Uiso 1 1 calc R
C45 C 0.1612(4) 0.8854(3) -0.0873(2) 0.0409(8) Uani 1 1 d .
H45A H 0.2055 0.9450 -0.0960 0.061 Uiso 1 1 calc R
H45B H 0.0939 0.8947 -0.0587 0.061 Uiso 1 1 calc R
H45C H 0.1197 0.8303 -0.1309 0.061 Uiso 1 1 calc R
C46 C 0.3028(5) 0.7397(3) -0.15831(19) 0.0524(10) Uani 1 1 d .
H46A H 0.3398 0.7831 -0.1827 0.079 Uiso 1 1 calc R
H46B H 0.2082 0.7052 -0.1747 0.079 Uiso 1 1 calc R
H46C H 0.3455 0.6919 -0.1666 0.079 Uiso 1 1 calc R
C47 C -0.2237(3) 0.6278(2) 0.23370(14) 0.0255(5) Uani 1 1 d .
C48 C -0.3057(3) 0.6474(2) 0.19201(15) 0.0267(6) Uani 1 1 d .
C49 C -0.2416(3) 0.7459(2) 0.19734(15) 0.0271(6) Uani 1 1 d .
C50 C -0.1206(3) 0.7866(2) 0.24144(14) 0.0255(5) Uani 1 1 d .
C51 C -0.1088(3) 0.7139(2) 0.26428(14) 0.0249(5) Uani 1 1 d .
C52 C -0.2587(4) 0.5343(2) 0.24608(17) 0.0361(7) Uani 1 1 d .
H52A H -0.3165 0.5350 0.2809 0.054 Uiso 1 1 calc R
H52B H -0.1784 0.5284 0.2621 0.054 Uiso 1 1 calc R
H52C H -0.3040 0.4785 0.2034 0.054 Uiso 1 1 calc R
C53 C -0.4411(3) 0.5790(3) 0.15406(18) 0.0389(7) Uani 1 1 d .
H53A H -0.5061 0.5882 0.1843 0.058 Uiso 1 1 calc R
H53B H -0.4460 0.5112 0.1393 0.058 Uiso 1 1 calc R
H53C H -0.4593 0.5931 0.1140 0.058 Uiso 1 1 calc R
C54 C -0.3010(3) 0.8015(3) 0.16887(19) 0.0385(7) Uani 1 1 d .
H54A H -0.3551 0.8278 0.2006 0.058 Uiso 1 1 calc R
H54B H -0.3557 0.7572 0.1245 0.058 Uiso 1 1 calc R
H54C H -0.2306 0.8555 0.1631 0.058 Uiso 1 1 calc R
C55 C -0.0273(3) 0.8915(2) 0.26573(17) 0.0360(7) Uani 1 1 d .
H55A H -0.0606 0.9325 0.3020 0.054 Uiso 1 1 calc R
H55B H -0.0200 0.9135 0.2275 0.054 Uiso 1 1 calc R
H55C H 0.0593 0.8967 0.2836 0.054 Uiso 1 1 calc R
C56 C -0.0017(3) 0.7315(3) 0.31836(16) 0.0341(7) Uani 1 1 d .
H56A H -0.0168 0.7691 0.3634 0.051 Uiso 1 1 calc R
H56B H 0.0835 0.7684 0.3094 0.051 Uiso 1 1 calc R
H56C H -0.0020 0.6686 0.3176 0.051 Uiso 1 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Al Al 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Y Y -2.7962 3.5667 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C1 Y1 C8 121.12(9) . .
C1 Y1 C9 142.05(10) . .
C8 Y1 C9 93.46(9) . .
C1 Y1 C13 141.62(10) . .
C8 Y1 C13 94.64(10) . .
C9 Y1 C13 31.00(11) . .
C1 Y1 C10 110.87(9) . .
C8 Y1 C10 121.04(10) . .
C9 Y1 C10 31.21(10) . .
C13 Y1 C10 51.01(10) . .
C1 Y1 C11 94.98(9) . .
C8 Y1 C11 143.86(9) . .
C9 Y1 C11 51.56(9) . .
C13 Y1 C11 51.32(10) . .
C10 Y1 C11 30.74(11) . .
C1 Y1 C12 110.54(10) . .
C8 Y1 C12 122.84(11) . .
C9 Y1 C12 51.35(10) . .
C13 Y1 C12 31.10(11) . .
C10 Y1 C12 50.72(11) . .
C11 Y1 C12 30.81(12) . .
C1 Y1 Al1 40.26(6) . .
C8 Y1 Al1 109.94(7) . .
C9 Y1 Al1 144.83(7) . .
C13 Y1 Al1 118.15(9) . .
C10 Y1 Al1 127.88(8) . .
C11 Y1 Al1 98.58(7) . .
C12 Y1 Al1 93.50(8) . .
C1 Y1 Al2 40.27(6) . .
C8 Y1 Al2 108.32(7) . .
C9 Y1 Al2 118.16(8) . .
C13 Y1 Al2 144.30(8) . .
C10 Y1 Al2 93.35(7) . .
C11 Y1 Al2 97.95(8) . .
C12 Y1 Al2 127.20(9) . .
Al1 Y1 Al2 79.82(2) . .
C1 Y2 C20 142.00(10) . .
C1 Y2 C21 142.46(10) . .
C20 Y2 C21 31.10(10) . .
C1 Y2 C23 94.98(9) . .
C20 Y2 C23 51.79(10) . .
C21 Y2 C23 51.97(9) . .
C1 Y2 C19 110.67(9) . .
C20 Y2 C19 31.36(10) . .
C21 Y2 C19 51.83(9) . .
C23 Y2 C19 31.36(10) . .
C1 Y2 C22 110.98(10) . .
C20 Y2 C22 51.58(11) . .
C21 Y2 C22 31.51(10) . .
C23 Y2 C22 31.17(9) . .
C19 Y2 C22 51.63(10) . .
C1 Y2 C8 120.54(9) . 2_666
C20 Y2 C8 94.13(10) . 2_666
C21 Y2 C8 94.19(9) . 2_666
C23 Y2 C8 144.47(9) . 2_666
C19 Y2 C8 121.83(10) . 2_666
C22 Y2 C8 122.39(9) . 2_666
C1 Y2 Al2 40.40(6) . .
C20 Y2 Al2 118.48(8) . .
C21 Y2 Al2 145.50(7) . .
C23 Y2 Al2 99.14(7) . .
C19 Y2 Al2 93.68(7) . .
C22 Y2 Al2 128.82(7) . .
C8 Y2 Al2 107.44(6) 2_666 .
C1 Y2 Al1 40.17(7) . .
C20 Y2 Al1 144.33(8) . .
C21 Y2 Al1 118.16(8) . .
C23 Y2 Al1 97.49(7) . .
C19 Y2 Al1 127.19(8) . .
C22 Y2 Al1 92.83(8) . .
C8 Y2 Al1 109.89(6) 2_666 .
Al2 Y2 Al1 79.85(2) . .
C29 Y3 C37 139.84(10) . .
C29 Y3 C38 108.31(10) . .
C37 Y3 C38 31.55(11) . .
C29 Y3 C41 143.09(9) . .
C37 Y3 C41 31.64(11) . .
C38 Y3 C41 51.97(10) . .
C29 Y3 C39 94.60(9) . .
C37 Y3 C39 51.93(10) . .
C38 Y3 C39 31.30(10) . .
C41 Y3 C39 51.58(9) . .
C29 Y3 C40 112.07(9) . .
C37 Y3 C40 51.98(10) . .
C38 Y3 C40 51.66(9) . .
C41 Y3 C40 31.25(9) . .
C39 Y3 C40 30.95(9) . .
C29 Y3 C36 119.59(9) . 2_565
C37 Y3 C36 96.58(10) . 2_565
C38 Y3 C36 125.37(10) . 2_565
C41 Y3 C36 94.93(9) . 2_565
C39 Y3 C36 145.78(9) . 2_565
C40 Y3 C36 121.75(9) . 2_565
C29 Y3 Al4 40.59(6) . .
C37 Y3 Al4 142.81(7) . .
C38 Y3 Al4 122.93(7) . .
C41 Y3 Al4 118.00(8) . .
C39 Y3 Al4 94.00(7) . .
C40 Y3 Al4 91.42(7) . .
C36 Y3 Al4 110.59(6) 2_565 .
C29 Y3 Al3 40.21(6) . .
C37 Y3 Al3 117.35(8) . .
C38 Y3 Al3 94.11(7) . .
C41 Y3 Al3 146.00(8) . .
C39 Y3 Al3 101.81(7) . .
C40 Y3 Al3 131.73(7) . .
C36 Y3 Al3 105.49(6) 2_565 .
Al4 Y3 Al3 80.12(2) . .
C29 Y4 C36 122.23(9) . .
C29 Y4 C48 137.45(9) . .
C36 Y4 C48 96.96(9) . .
C29 Y4 C47 144.66(9) . .
C36 Y4 C47 90.75(9) . .
C48 Y4 C47 31.38(9) . .
C29 Y4 C49 106.27(9) . .
C36 Y4 C49 127.31(9) . .
C48 Y4 C49 31.41(9) . .
C47 Y4 C49 51.72(9) . .
C29 Y4 C51 114.11(9) . .
C36 Y4 C51 115.46(9) . .
C48 Y4 C51 51.78(9) . .
C47 Y4 C51 31.32(9) . .
C49 Y4 C51 51.45(9) . .
C29 Y4 C50 94.63(9) . .
C36 Y4 C50 142.43(9) . .
C48 Y4 C50 51.66(9) . .
C47 Y4 C50 51.69(9) . .
C49 Y4 C50 30.90(9) . .
C51 Y4 C50 31.20(8) . .
C29 Y4 Al3 40.26(6) . .
C36 Y4 Al3 108.94(7) . .
C48 Y4 Al3 144.19(7) . .
C47 Y4 Al3 121.70(7) . .
C49 Y4 Al3 121.71(7) . .
C51 Y4 Al3 93.94(6) . .
C50 Y4 Al3 94.18(6) . .
C29 Y4 Al4 39.96(6) . .
C36 Y4 Al4 111.11(6) . .
C48 Y4 Al4 114.20(7) . .
C47 Y4 Al4 143.57(6) . .
C49 Y4 Al4 92.34(6) . .
C51 Y4 Al4 132.45(6) . .
C50 Y4 Al4 101.75(6) . .
Al3 Y4 Al4 79.52(2) . .
C6 Al1 C1 116.98(14) . .
C6 Al1 C5 111.19(14) . .
C1 Al1 C5 109.95(12) . .
C6 Al1 C2 109.76(15) . .
C1 Al1 C2 110.86(12) . .
C5 Al1 C2 96.15(13) . .
C6 Al1 Y1 124.64(11) . .
C1 Al1 Y1 53.14(8) . .
C5 Al1 Y1 123.42(9) . .
C2 Al1 Y1 58.88(9) . .
C6 Al1 Y2 124.71(12) . .
C1 Al1 Y2 52.81(8) . .
C5 Al1 Y2 58.53(9) . .
C2 Al1 Y2 124.83(10) . .
Y1 Al1 Y2 93.12(2) . .
C7 Al2 C1 117.28(14) . .
C7 Al2 C3 109.44(14) . .
C1 Al2 C3 111.09(12) . .
C7 Al2 C4 109.42(15) . .
C1 Al2 C4 110.77(12) . .
C3 Al2 C4 96.93(13) . .
C7 Al2 Y2 125.47(11) . .
C1 Al2 Y2 52.87(8) . .
C3 Al2 Y2 124.29(9) . .
C4 Al2 Y2 58.85(9) . .
C7 Al2 Y1 124.21(12) . .
C1 Al2 Y1 52.86(8) . .
C3 Al2 Y1 59.54(9) . .
C4 Al2 Y1 125.67(9) . .
Y2 Al2 Y1 92.95(2) . .
C34 Al3 C29 117.97(13) . .
C34 Al3 C30 108.98(14) . .
C29 Al3 C30 110.92(12) . .
C34 Al3 C33 109.23(13) . .
C29 Al3 C33 110.88(11) . .
C30 Al3 C33 96.78(13) . .
C34 Al3 Y4 123.47(11) . .
C29 Al3 Y4 53.12(8) . .
C30 Al3 Y4 126.69(9) . .
C33 Al3 Y4 59.37(8) . .
C34 Al3 Y3 127.35(11) . .
C29 Al3 Y3 52.45(8) . .
C30 Al3 Y3 59.14(8) . .
C33 Al3 Y3 122.60(9) . .
Y4 Al3 Y3 92.52(2) . .
C35 Al4 C29 116.15(13) . .
C35 Al4 C31 112.05(13) . .
C29 Al4 C31 109.99(12) . .
C35 Al4 C32 110.52(14) . .
C29 Al4 C32 110.73(12) . .
C31 Al4 C32 95.51(13) . .
C35 Al4 Y3 123.03(10) . .
C29 Al4 Y3 53.29(8) . .
C31 Al4 Y3 58.56(8) . .
C32 Al4 Y3 125.78(9) . .
C35 Al4 Y4 125.92(10) . .
C29 Al4 Y4 52.91(8) . .
C31 Al4 Y4 121.36(9) . .
C32 Al4 Y4 58.67(8) . .
Y3 Al4 Y4 93.06(2) . .
Al1 C1 Al2 164.71(15) . .
Al1 C1 Y2 87.03(10) . .
Al2 C1 Y2 86.73(10) . .
Al1 C1 Y1 86.60(10) . .
Al2 C1 Y1 86.87(10) . .
Y2 C1 Y1 130.49(11) . .
Y1 C8 Y2 167.82(13) . 2_666
C13 C9 C10 107.4(3) . .
C13 C9 C14 126.4(4) . .
C10 C9 C14 126.1(4) . .
C13 C9 Y1 75.23(18) . .
C10 C9 Y1 75.27(17) . .
C14 C9 Y1 117.9(2) . .
C11 C10 C9 108.9(3) . .
C11 C10 C15 125.2(4) . .
C9 C10 C15 125.5(4) . .
C11 C10 Y1 75.18(18) . .
C9 C10 Y1 73.52(17) . .
C15 C10 Y1 123.1(2) . .
C10 C11 C12 107.4(3) . .
C10 C11 C16 125.2(4) . .
C12 C11 C16 127.1(4) . .
C10 C11 Y1 74.07(17) . .
C12 C11 Y1 74.65(18) . .
C16 C11 Y1 121.7(2) . .
C11 C12 C13 108.1(3) . .
C11 C12 C17 125.9(4) . .
C13 C12 C17 125.5(4) . .
C11 C12 Y1 74.54(18) . .
C13 C12 Y1 73.69(18) . .
C17 C12 Y1 124.0(2) . .
C9 C13 C12 108.1(3) . .
C9 C13 C18 125.3(4) . .
C12 C13 C18 126.6(4) . .
C9 C13 Y1 73.77(18) . .
C12 C13 Y1 75.20(18) . .
C18 C13 Y1 120.1(2) . .
C20 C19 C23 107.5(3) . .
C20 C19 C24 126.8(3) . .
C23 C19 C24 125.1(3) . .
C20 C19 Y2 73.71(17) . .
C23 C19 Y2 74.22(16) . .
C24 C19 Y2 124.7(2) . .
C21 C20 C19 108.9(3) . .
C21 C20 C25 125.3(3) . .
C19 C20 C25 125.8(3) . .
C21 C20 Y2 74.63(17) . .
C19 C20 Y2 74.93(17) . .
C25 C20 Y2 119.8(2) . .
C20 C21 C22 107.6(3) . .
C20 C21 C26 126.9(3) . .
C22 C21 C26 125.4(3) . .
C20 C21 Y2 74.27(17) . .
C22 C21 Y2 74.74(16) . .
C26 C21 Y2 120.8(2) . .
C23 C22 C21 108.1(3) . .
C23 C22 C27 125.7(3) . .
C21 C22 C27 125.6(3) . .
C23 C22 Y2 74.24(16) . .
C21 C22 Y2 73.74(16) . .
C27 C22 Y2 124.8(2) . .
C22 C23 C19 107.9(3) . .
C22 C23 C28 125.4(3) . .
C19 C23 C28 126.4(3) . .
C22 C23 Y2 74.59(16) . .
C19 C23 Y2 74.42(16) . .
C28 C23 Y2 122.0(2) . .
Al4 C29 Al3 164.86(15) . .
Al4 C29 Y3 86.11(10) . .
Al3 C29 Y3 87.34(10) . .
Al4 C29 Y4 87.14(10) . .
Al3 C29 Y4 86.62(9) . .
Y3 C29 Y4 129.91(11) . .
Y4 C36 Y3 168.01(13) . 2_565
C38 C37 C41 107.6(3) . .
C38 C37 C42 126.7(4) . .
C41 C37 C42 125.6(3) . .
C38 C37 Y3 74.63(17) . .
C41 C37 Y3 74.94(18) . .
C42 C37 Y3 118.7(2) . .
C39 C38 C37 108.1(3) . .
C39 C38 C43 124.3(3) . .
C37 C38 C43 127.0(3) . .
C39 C38 Y3 75.38(16) . .
C37 C38 Y3 73.82(17) . .
C43 C38 Y3 123.5(2) . .
C40 C39 C38 108.4(3) . .
C40 C39 C44 126.6(3) . .
C38 C39 C44 124.6(3) . .
C40 C39 Y3 75.03(16) . .
C38 C39 Y3 73.31(16) . .
C44 C39 Y3 123.5(2) . .
C39 C40 C41 107.8(3) . .
C39 C40 C45 126.3(3) . .
C41 C40 C45 125.5(3) . .
C39 C40 Y3 74.02(16) . .
C41 C40 Y3 73.20(16) . .
C45 C40 Y3 124.5(2) . .
C40 C41 C37 108.1(3) . .
C40 C41 C46 125.0(3) . .
C37 C41 C46 126.7(3) . .
C40 C41 Y3 75.55(16) . .
C37 C41 Y3 73.42(17) . .
C46 C41 Y3 121.7(2) . .
C48 C47 C51 108.0(2) . .
C48 C47 C52 125.0(3) . .
C51 C47 C52 126.9(3) . .
C48 C47 Y4 74.05(16) . .
C51 C47 Y4 74.99(16) . .
C52 C47 Y4 120.0(2) . .
C47 C48 C49 107.8(3) . .
C47 C48 C53 125.8(3) . .
C49 C48 C53 126.2(3) . .
C47 C48 Y4 74.57(16) . .
C49 C48 Y4 75.14(16) . .
C53 C48 Y4 120.3(2) . .
C50 C49 C48 108.3(2) . .
C50 C49 C54 125.5(3) . .
C48 C49 C54 125.7(3) . .
C50 C49 Y4 74.94(16) . .
C48 C49 Y4 73.45(16) . .
C54 C49 Y4 124.0(2) . .
C49 C50 C51 108.1(2) . .
C49 C50 C55 125.7(3) . .
C51 C50 C55 125.9(3) . .
C49 C50 Y4 74.15(16) . .
C51 C50 Y4 74.07(16) . .
C55 C50 Y4 122.5(2) . .
C47 C51 C50 107.9(2) . .
C47 C51 C56 126.9(3) . .
C50 C51 C56 124.7(3) . .
C47 C51 Y4 73.69(16) . .
C50 C51 Y4 74.72(16) . .
C56 C51 Y4 123.6(2) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Y1 C1 2.458(3) .
Y1 C2 2.670(3) .
Y1 C3 2.700(3) .
Y1 C8 2.577(3) .
Y1 C9 2.611(3) .
Y1 C13 2.630(3) .
Y1 C10 2.634(3) .
Y1 C11 2.648(3) .
Y1 C12 2.649(3) .
Y1 Al1 3.0661(9) .
Y1 Al2 3.0782(9) .
Y2 C1 2.452(3) .
Y2 C4 2.670(3) .
Y2 C5 2.661(3) .
Y2 C20 2.616(3) .
Y2 C21 2.621(3) .
Y2 C23 2.630(3) .
Y2 C19 2.632(3) .
Y2 C22 2.634(3) .
Y2 C8 2.687(3) 2_666
Y2 Al2 3.0696(9) .
Y2 Al1 3.0733(9) .
Y3 C29 2.444(3) .
Y3 C30 2.687(3) .
Y3 C31 2.640(3) .
Y3 C37 2.605(3) .
Y3 C38 2.616(3) .
Y3 C41 2.625(3) .
Y3 C39 2.642(3) .
Y3 C40 2.655(3) .
Y3 C36 2.702(3) 2_565
Y3 Al4 3.0421(9) .
Y3 Al3 3.0800(9) .
Y4 C29 2.464(3) .
Y4 C32 2.677(3) .
Y4 C33 2.692(3) .
Y4 C36 2.579(3) .
Y4 C48 2.622(3) .
Y4 C47 2.629(3) .
Y4 C49 2.644(3) .
Y4 C51 2.646(3) .
Y4 C50 2.654(3) .
Y4 Al3 3.0753(9) .
Y4 Al4 3.0855(8) .
Al1 C6 1.971(3) .
Al1 C1 1.985(3) .
Al1 C5 2.062(3) .
Al1 C2 2.071(3) .
Al2 C7 1.972(3) .
Al2 C1 1.993(3) .
Al2 C3 2.061(3) .
Al2 C4 2.062(3) .
Al3 C34 1.967(3) .
Al3 C29 1.991(3) .
Al3 C30 2.059(3) .
Al3 C33 2.063(3) .
Al4 C35 1.977(3) .
Al4 C29 1.984(3) .
Al4 C31 2.070(3) .
Al4 C32 2.071(3) .
C8 Y2 2.687(3) 2_666
C9 C13 1.401(5) .
C9 C10 1.411(5) .
C9 C14 1.509(5) .
C10 C11 1.400(5) .
C10 C15 1.505(5) .
C11 C12 1.407(5) .
C11 C16 1.512(5) .
C12 C13 1.415(5) .
C12 C17 1.517(5) .
C13 C18 1.507(5) .
C19 C20 1.419(4) .
C19 C23 1.422(5) .
C19 C24 1.505(4) .
C20 C21 1.404(5) .
C20 C25 1.508(5) .
C21 C22 1.427(5) .
C21 C26 1.506(4) .
C22 C23 1.414(4) .
C22 C27 1.507(5) .
C23 C28 1.503(5) .
C36 Y3 2.702(3) 2_565
C37 C38 1.420(5) .
C37 C41 1.426(5) .
C37 C42 1.503(5) .
C38 C39 1.419(4) .
C38 C43 1.505(5) .
C39 C40 1.413(4) .
C39 C44 1.510(4) .
C40 C41 1.422(4) .
C40 C45 1.508(4) .
C41 C46 1.503(5) .
C47 C48 1.420(4) .
C47 C51 1.424(4) .
C47 C52 1.502(4) .
C48 C49 1.426(4) .
C48 C53 1.505(4) .
C49 C50 1.412(4) .
C49 C54 1.509(4) .
C50 C51 1.425(4) .
C50 C55 1.503(4) .
C51 C56 1.503(4) .
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_4
C1 Y1 Al1 C6 -99.85(18) . .
C8 Y1 Al1 C6 145.17(16) . .
C9 Y1 Al1 C6 16.4(2) . .
C13 Y1 Al1 C6 38.22(17) . .
C10 Y1 Al1 C6 -22.58(18) . .
C11 Y1 Al1 C6 -12.28(17) . .
C12 Y1 Al1 C6 18.30(17) . .
Al2 Y1 Al1 C6 -108.89(15) . .
C8 Y1 Al1 C1 -114.98(12) . .
C9 Y1 Al1 C1 116.26(17) . .
C13 Y1 Al1 C1 138.07(13) . .
C10 Y1 Al1 C1 77.27(13) . .
C11 Y1 Al1 C1 87.57(13) . .
C12 Y1 Al1 C1 118.15(13) . .
Al2 Y1 Al1 C1 -9.04(10) . .
C1 Y1 Al1 C5 90.92(15) . .
C8 Y1 Al1 C5 -24.05(13) . .
C9 Y1 Al1 C5 -152.82(17) . .
C13 Y1 Al1 C5 -131.01(14) . .
C10 Y1 Al1 C5 168.19(14) . .
C11 Y1 Al1 C5 178.50(14) . .
C12 Y1 Al1 C5 -150.93(14) . .
Al2 Y1 Al1 C5 81.89(11) . .
C1 Y1 Al1 C2 166.54(15) . .
C8 Y1 Al1 C2 51.57(13) . .
C9 Y1 Al1 C2 -77.20(18) . .
C13 Y1 Al1 C2 -55.39(14) . .
C10 Y1 Al1 C2 -116.19(15) . .
C11 Y1 Al1 C2 -105.88(14) . .
C12 Y1 Al1 C2 -75.31(15) . .
Al2 Y1 Al1 C2 157.51(12) . .
C1 Y1 Al1 Y2 37.10(9) . .
C8 Y1 Al1 Y2 -77.87(7) . .
C9 Y1 Al1 Y2 153.36(14) . .
C13 Y1 Al1 Y2 175.17(8) . .
C10 Y1 Al1 Y2 114.37(9) . .
C11 Y1 Al1 Y2 124.68(8) . .
C12 Y1 Al1 Y2 155.25(9) . .
Al2 Y1 Al1 Y2 28.07(2) . .
C1 Y2 Al1 C6 99.62(17) . .
C20 Y2 Al1 C6 -16.77(19) . .
C21 Y2 Al1 C6 -39.87(16) . .
C23 Y2 Al1 C6 10.76(15) . .
C19 Y2 Al1 C6 21.85(17) . .
C22 Y2 Al1 C6 -20.20(15) . .
C8 Y2 Al1 C6 -146.23(15) 2_666 .
Al2 Y2 Al1 C6 108.76(14) . .
C20 Y2 Al1 C1 -116.39(16) . .
C21 Y2 Al1 C1 -139.48(12) . .
C23 Y2 Al1 C1 -88.86(12) . .
C19 Y2 Al1 C1 -77.76(13) . .
C22 Y2 Al1 C1 -119.82(12) . .
C8 Y2 Al1 C1 114.15(12) 2_666 .
Al2 Y2 Al1 C1 9.14(10) . .
C1 Y2 Al1 C5 -165.12(14) . .
C20 Y2 Al1 C5 78.49(16) . .
C21 Y2 Al1 C5 55.40(13) . .
C23 Y2 Al1 C5 106.02(12) . .
C19 Y2 Al1 C5 117.11(13) . .
C22 Y2 Al1 C5 75.06(12) . .
C8 Y2 Al1 C5 -50.97(12) 2_666 .
Al2 Y2 Al1 C5 -155.98(10) . .
C1 Y2 Al1 C2 -90.95(15) . .
C20 Y2 Al1 C2 152.66(16) . .
C21 Y2 Al1 C2 129.57(14) . .
C23 Y2 Al1 C2 -179.81(13) . .
C19 Y2 Al1 C2 -168.72(14) . .
C22 Y2 Al1 C2 149.23(13) . .
C8 Y2 Al1 C2 23.20(13) 2_666 .
Al2 Y2 Al1 C2 -81.81(11) . .
C1 Y2 Al1 Y1 -37.29(9) . .
C20 Y2 Al1 Y1 -153.68(12) . .
C21 Y2 Al1 Y1 -176.78(8) . .
C23 Y2 Al1 Y1 -126.15(7) . .
C19 Y2 Al1 Y1 -115.06(9) . .
C22 Y2 Al1 Y1 -157.11(7) . .
C8 Y2 Al1 Y1 76.86(7) 2_666 .
Al2 Y2 Al1 Y1 -28.15(2) . .
C1 Y2 Al2 C7 -99.59(18) . .
C20 Y2 Al2 C7 38.64(17) . .
C21 Y2 Al2 C7 17.2(2) . .
C23 Y2 Al2 C7 -12.64(16) . .
C19 Y2 Al2 C7 18.45(17) . .
C22 Y2 Al2 C7 -23.26(18) . .
C8 Y2 Al2 C7 143.49(16) 2_666 .
Al1 Y2 Al2 C7 -108.69(15) . .
C20 Y2 Al2 C1 138.23(13) . .
C21 Y2 Al2 C1 116.77(17) . .
C23 Y2 Al2 C1 86.95(12) . .
C19 Y2 Al2 C1 118.04(12) . .
C22 Y2 Al2 C1 76.33(13) . .
C8 Y2 Al2 C1 -116.92(11) 2_666 .
Al1 Y2 Al2 C1 -9.10(10) . .
C1 Y2 Al2 C3 91.72(15) . .
C20 Y2 Al2 C3 -130.04(14) . .
C21 Y2 Al2 C3 -151.50(17) . .
C23 Y2 Al2 C3 178.67(13) . .
C19 Y2 Al2 C3 -150.23(14) . .
C22 Y2 Al2 C3 168.06(14) . .
C8 Y2 Al2 C3 -25.19(13) 2_666 .
Al1 Y2 Al2 C3 82.62(11) . .
C1 Y2 Al2 C4 167.75(14) . .
C20 Y2 Al2 C4 -54.02(14) . .
C21 Y2 Al2 C4 -75.48(17) . .
C23 Y2 Al2 C4 -105.31(13) . .
C19 Y2 Al2 C4 -74.21(13) . .
C22 Y2 Al2 C4 -115.92(14) . .
C8 Y2 Al2 C4 50.83(12) 2_666 .
Al1 Y2 Al2 C4 158.65(11) . .
C1 Y2 Al2 Y1 37.13(9) . .
C20 Y2 Al2 Y1 175.36(8) . .
C21 Y2 Al2 Y1 153.90(14) . .
C23 Y2 Al2 Y1 124.07(8) . .
C19 Y2 Al2 Y1 155.17(8) . .
C22 Y2 Al2 Y1 113.46(9) . .
C8 Y2 Al2 Y1 -79.79(7) 2_666 .
Al1 Y2 Al2 Y1 28.03(2) . .
C1 Y1 Al2 C7 100.40(16) . .
C8 Y1 Al2 C7 -142.78(15) . .
C9 Y1 Al2 C7 -38.34(16) . .
C13 Y1 Al2 C7 -15.4(2) . .
C10 Y1 Al2 C7 -18.48(15) . .
C11 Y1 Al2 C7 12.08(15) . .
C12 Y1 Al2 C7 22.77(17) . .
Al1 Y1 Al2 C7 109.43(13) . .
C8 Y1 Al2 C1 116.83(12) . .
C9 Y1 Al2 C1 -138.74(12) . .
C13 Y1 Al2 C1 -115.82(17) . .
C10 Y1 Al2 C1 -118.88(12) . .
C11 Y1 Al2 C1 -88.32(12) . .
C12 Y1 Al2 C1 -77.62(14) . .
Al1 Y1 Al2 C1 9.03(10) . .
C1 Y1 Al2 C3 -165.76(15) . .
C8 Y1 Al2 C3 -48.93(13) . .
C9 Y1 Al2 C3 55.51(13) . .
C13 Y1 Al2 C3 78.42(18) . .
C10 Y1 Al2 C3 75.37(13) . .
C11 Y1 Al2 C3 105.92(13) . .
C12 Y1 Al2 C3 116.62(14) . .
Al1 Y1 Al2 C3 -156.72(11) . .
C1 Y1 Al2 C4 -90.23(15) . .
C8 Y1 Al2 C4 26.60(13) . .
C9 Y1 Al2 C4 131.03(14) . .
C13 Y1 Al2 C4 153.95(18) . .
C10 Y1 Al2 C4 150.90(14) . .
C11 Y1 Al2 C4 -178.55(14) . .
C12 Y1 Al2 C4 -167.85(14) . .
Al1 Y1 Al2 C4 -81.19(11) . .
C1 Y1 Al2 Y2 -37.13(9) . .
C8 Y1 Al2 Y2 79.69(7) . .
C9 Y1 Al2 Y2 -175.87(8) . .
C13 Y1 Al2 Y2 -152.96(14) . .
C10 Y1 Al2 Y2 -156.01(8) . .
C11 Y1 Al2 Y2 -125.45(8) . .
C12 Y1 Al2 Y2 -114.76(10) . .
Al1 Y1 Al2 Y2 -28.10(2) . .
C29 Y4 Al3 C34 101.94(15) . .
C36 Y4 Al3 C34 -140.22(14) . .
C48 Y4 Al3 C34 -6.22(17) . .
C47 Y4 Al3 C34 -37.03(14) . .
C49 Y4 Al3 C34 24.65(14) . .
C51 Y4 Al3 C34 -21.58(14) . .
C50 Y4 Al3 C34 9.71(14) . .
Al4 Y4 Al3 C34 110.90(12) . .
C36 Y4 Al3 C29 117.85(12) . .
C48 Y4 Al3 C29 -108.16(15) . .
C47 Y4 Al3 C29 -138.96(12) . .
C49 Y4 Al3 C29 -77.28(12) . .
C51 Y4 Al3 C29 -123.51(11) . .
C50 Y4 Al3 C29 -92.23(11) . .
Al4 Y4 Al3 C29 8.96(10) . .
C29 Y4 Al3 C30 -89.87(15) . .
C36 Y4 Al3 C30 27.98(13) . .
C48 Y4 Al3 C30 161.97(15) . .
C47 Y4 Al3 C30 131.17(13) . .
C49 Y4 Al3 C30 -167.15(13) . .
C51 Y4 Al3 C30 146.62(12) . .
C50 Y4 Al3 C30 177.90(12) . .
Al4 Y4 Al3 C30 -80.90(11) . .
C29 Y4 Al3 C33 -164.20(14) . .
C36 Y4 Al3 C33 -46.35(12) . .
C48 Y4 Al3 C33 87.64(15) . .
C47 Y4 Al3 C33 56.84(12) . .
C49 Y4 Al3 C33 118.52(12) . .
C51 Y4 Al3 C33 72.29(12) . .
C50 Y4 Al3 C33 103.57(12) . .
Al4 Y4 Al3 C33 -155.23(10) . .
C29 Y4 Al3 Y3 -37.28(9) . .
C36 Y4 Al3 Y3 80.57(7) . .
C48 Y4 Al3 Y3 -145.44(11) . .
C47 Y4 Al3 Y3 -176.24(7) . .
C49 Y4 Al3 Y3 -114.56(7) . .
C51 Y4 Al3 Y3 -160.79(6) . .
C50 Y4 Al3 Y3 -129.51(6) . .
Al4 Y4 Al3 Y3 -28.31(2) . .
C29 Y3 Al3 C34 -99.06(16) . .
C37 Y3 Al3 C34 37.08(16) . .
C38 Y3 Al3 C34 14.70(15) . .
C41 Y3 Al3 C34 18.40(19) . .
C39 Y3 Al3 C34 -15.97(15) . .
C40 Y3 Al3 C34 -25.02(17) . .
C36 Y3 Al3 C34 143.17(15) 2_565 .
Al4 Y3 Al3 C34 -108.03(14) . .
C37 Y3 Al3 C29 136.14(12) . .
C38 Y3 Al3 C29 113.76(12) . .
C41 Y3 Al3 C29 117.46(16) . .
C39 Y3 Al3 C29 83.09(12) . .
C40 Y3 Al3 C29 74.04(13) . .
C36 Y3 Al3 C29 -117.77(11) 2_565 .
Al4 Y3 Al3 C29 -8.97(9) . .
C29 Y3 Al3 C30 169.77(14) . .
C37 Y3 Al3 C30 -54.09(13) . .
C38 Y3 Al3 C30 -76.47(13) . .
C41 Y3 Al3 C30 -72.77(16) . .
C39 Y3 Al3 C30 -107.14(13) . .
C40 Y3 Al3 C30 -116.19(14) . .
C36 Y3 Al3 C30 52.00(12) 2_565 .
Al4 Y3 Al3 C30 160.79(11) . .
C29 Y3 Al3 C33 92.41(14) . .
C37 Y3 Al3 C33 -131.45(13) . .
C38 Y3 Al3 C33 -153.83(12) . .
C41 Y3 Al3 C33 -150.13(16) . .
C39 Y3 Al3 C33 175.50(12) . .
C40 Y3 Al3 C33 166.45(13) . .
C36 Y3 Al3 C33 -25.36(12) 2_565 .
Al4 Y3 Al3 C33 83.44(10) . .
C29 Y3 Al3 Y4 37.67(9) . .
C37 Y3 Al3 Y4 173.81(8) . .
C38 Y3 Al3 Y4 151.43(7) . .
C41 Y3 Al3 Y4 155.13(13) . .
C39 Y3 Al3 Y4 120.76(7) . .
C40 Y3 Al3 Y4 111.71(9) . .
C36 Y3 Al3 Y4 -80.10(7) 2_565 .
Al4 Y3 Al3 Y4 28.69(2) . .
C29 Y3 Al4 C35 99.85(15) . .
C37 Y3 Al4 C35 -14.05(19) . .
C38 Y3 Al4 C35 20.25(15) . .
C41 Y3 Al4 C35 -40.61(15) . .
C39 Y3 Al4 C35 7.45(14) . .
C40 Y3 Al4 C35 -23.43(14) . .
C36 Y3 Al4 C35 -148.30(13) 2_565 .
Al3 Y3 Al4 C35 108.75(12) . .
C37 Y3 Al4 C29 -113.90(17) . .
C38 Y3 Al4 C29 -79.60(12) . .
C41 Y3 Al4 C29 -140.46(12) . .
C39 Y3 Al4 C29 -92.40(11) . .
C40 Y3 Al4 C29 -123.28(11) . .
C36 Y3 Al4 C29 111.85(11) 2_565 .
Al3 Y3 Al4 C29 8.90(9) . .
C29 Y3 Al4 C31 -162.83(14) . .
C37 Y3 Al4 C31 83.27(17) . .
C38 Y3 Al4 C31 117.57(13) . .
C41 Y3 Al4 C31 56.71(13) . .
C39 Y3 Al4 C31 104.77(12) . .
C40 Y3 Al4 C31 73.89(12) . .
C36 Y3 Al4 C31 -50.98(12) 2_565 .
Al3 Y3 Al4 C31 -153.93(10) . .
C29 Y3 Al4 C32 -90.40(14) . .
C37 Y3 Al4 C32 155.70(17) . .
C38 Y3 Al4 C32 -169.99(14) . .
C41 Y3 Al4 C32 129.14(14) . .
C39 Y3 Al4 C32 177.20(13) . .
C40 Y3 Al4 C32 146.32(13) . .
C36 Y3 Al4 C32 21.45(13) 2_565 .
Al3 Y3 Al4 C32 -81.50(11) . .
C29 Y3 Al4 Y4 -37.51(9) . .
C37 Y3 Al4 Y4 -151.41(14) . .
C38 Y3 Al4 Y4 -117.10(8) . .
C41 Y3 Al4 Y4 -177.97(8) . .
C39 Y3 Al4 Y4 -129.91(7) . .
C40 Y3 Al4 Y4 -160.79(7) . .
C36 Y3 Al4 Y4 74.34(7) 2_565 .
Al3 Y3 Al4 Y4 -28.61(2) . .
C29 Y4 Al4 C35 -97.73(16) . .
C36 Y4 Al4 C35 146.84(14) . .
C48 Y4 Al4 C35 38.43(15) . .
C47 Y4 Al4 C35 23.72(17) . .
C49 Y4 Al4 C35 15.08(14) . .
C51 Y4 Al4 C35 -21.02(16) . .
C50 Y4 Al4 C35 -14.62(14) . .
Al3 Y4 Al4 C35 -106.75(13) . .
C36 Y4 Al4 C29 -115.43(12) . .
C48 Y4 Al4 C29 136.16(12) . .
C47 Y4 Al4 C29 121.45(14) . .
C49 Y4 Al4 C29 112.81(12) . .
C51 Y4 Al4 C29 76.71(13) . .
C50 Y4 Al4 C29 83.11(12) . .
Al3 Y4 Al4 C29 -9.02(10) . .
C29 Y4 Al4 C31 92.35(14) . .
C36 Y4 Al4 C31 -23.08(13) . .
C48 Y4 Al4 C31 -131.49(12) . .
C47 Y4 Al4 C31 -146.20(15) . .
C49 Y4 Al4 C31 -154.84(12) . .
C51 Y4 Al4 C31 169.06(13) . .
C50 Y4 Al4 C31 175.46(12) . .
Al3 Y4 Al4 C31 83.33(11) . .
C29 Y4 Al4 C32 168.50(15) . .
C36 Y4 Al4 C32 53.07(13) . .
C48 Y4 Al4 C32 -55.34(13) . .
C47 Y4 Al4 C32 -70.05(15) . .
C49 Y4 Al4 C32 -78.69(13) . .
C51 Y4 Al4 C32 -114.80(14) . .
C50 Y4 Al4 C32 -108.39(13) . .
Al3 Y4 Al4 C32 159.48(11) . .
C29 Y4 Al4 Y3 37.73(9) . .
C36 Y4 Al4 Y3 -77.69(7) . .
C48 Y4 Al4 Y3 173.89(7) . .
C47 Y4 Al4 Y3 159.19(11) . .
C49 Y4 Al4 Y3 150.54(7) . .
C51 Y4 Al4 Y3 114.44(9) . .
C50 Y4 Al4 Y3 120.84(7) . .
Al3 Y4 Al4 Y3 28.71(2) . .
C6 Al1 C1 Al2 179.4(6) . .
C5 Al1 C1 Al2 -52.5(6) . .
C2 Al1 C1 Al2 52.6(6) . .
Y1 Al1 C1 Al2 64.9(6) . .
Y2 Al1 C1 Al2 -66.0(6) . .
C6 Al1 C1 Y2 -114.57(14) . .
C5 Al1 C1 Y2 13.47(13) . .
C2 Al1 C1 Y2 118.56(12) . .
Y1 Al1 C1 Y2 130.87(10) . .
C6 Al1 C1 Y1 114.55(14) . .
C5 Al1 C1 Y1 -117.40(11) . .
C2 Al1 C1 Y1 -12.31(14) . .
Y2 Al1 C1 Y1 -130.87(10) . .
C7 Al2 C1 Al1 -178.6(6) . .
C3 Al2 C1 Al1 -51.7(6) . .
C4 Al2 C1 Al1 54.8(6) . .
Y2 Al2 C1 Al1 66.0(6) . .
Y1 Al2 C1 Al1 -64.8(6) . .
C7 Al2 C1 Y2 115.37(13) . .
C3 Al2 C1 Y2 -117.74(12) . .
C4 Al2 C1 Y2 -11.20(13) . .
Y1 Al2 C1 Y2 -130.88(10) . .
C7 Al2 C1 Y1 -113.76(13) . .
C3 Al2 C1 Y1 13.14(13) . .
C4 Al2 C1 Y1 119.67(11) . .
Y2 Al2 C1 Y1 130.88(10) . .
C20 Y2 C1 Al1 121.97(15) . .
C21 Y2 C1 Al1 70.07(17) . .
C23 Y2 C1 Al1 95.71(10) . .
C19 Y2 C1 Al1 123.68(10) . .
C22 Y2 C1 Al1 68.14(11) . .
C8 Y2 C1 Al1 -85.03(11) 2_666 .
Al2 Y2 C1 Al1 -166.03(15) . .
C20 Y2 C1 Al2 -72.00(17) . .
C21 Y2 C1 Al2 -123.90(14) . .
C23 Y2 C1 Al2 -98.25(10) . .
C19 Y2 C1 Al2 -70.28(12) . .
C22 Y2 C1 Al2 -125.83(10) . .
C8 Y2 C1 Al2 81.00(11) 2_666 .
Al1 Y2 C1 Al2 166.03(15) . .
C20 Y2 C1 Y1 -155.06(14) . .
C21 Y2 C1 Y1 153.04(14) . .
C23 Y2 C1 Y1 178.68(15) . .
C19 Y2 C1 Y1 -153.35(14) . .
C22 Y2 C1 Y1 151.11(14) . .
C8 Y2 C1 Y1 -2.06(19) 2_666 .
Al2 Y2 C1 Y1 -83.06(15) . .
Al1 Y2 C1 Y1 82.97(15) . .
C8 Y1 C1 Al1 84.47(11) . .
C9 Y1 C1 Al1 -122.87(15) . .
C13 Y1 C1 Al1 -71.63(18) . .
C10 Y1 C1 Al1 -124.52(11) . .
C11 Y1 C1 Al1 -97.41(11) . .
C12 Y1 C1 Al1 -70.03(12) . .
Al2 Y1 C1 Al1 166.16(15) . .
C8 Y1 C1 Al2 -81.69(11) . .
C9 Y1 C1 Al2 70.97(18) . .
C13 Y1 C1 Al2 122.21(15) . .
C10 Y1 C1 Al2 69.31(12) . .
C11 Y1 C1 Al2 96.43(11) . .
C12 Y1 C1 Al2 123.81(11) . .
Al1 Y1 C1 Al2 -166.16(15) . .
C8 Y1 C1 Y2 1.31(19) . .
C9 Y1 C1 Y2 153.97(14) . .
C13 Y1 C1 Y2 -154.79(15) . .
C10 Y1 C1 Y2 152.31(14) . .
C11 Y1 C1 Y2 179.43(16) . .
C12 Y1 C1 Y2 -153.19(15) . .
Al1 Y1 C1 Y2 -83.16(15) . .
Al2 Y1 C1 Y2 83.00(15) . .
C1 Y1 C8 Y2 2.6(6) . 2_666
C9 Y1 C8 Y2 -161.0(6) . 2_666
C13 Y1 C8 Y2 167.9(6) . 2_666
C10 Y1 C8 Y2 -145.5(5) . 2_666
C11 Y1 C8 Y2 -174.3(5) . 2_666
C12 Y1 C8 Y2 153.9(5) . 2_666
Al1 Y1 C8 Y2 45.7(6) . 2_666
Al2 Y1 C8 Y2 -39.8(6) . 2_666
C1 Y1 C9 C13 109.9(2) . .
C8 Y1 C9 C13 -93.3(2) . .
C10 Y1 C9 C13 112.9(3) . .
C11 Y1 C9 C13 76.8(2) . .
C12 Y1 C9 C13 37.1(2) . .
Al1 Y1 C9 C13 39.5(3) . .
Al2 Y1 C9 C13 153.82(17) . .
C1 Y1 C9 C10 -3.0(3) . .
C8 Y1 C9 C10 153.8(2) . .
C13 Y1 C9 C10 -112.9(3) . .
C11 Y1 C9 C10 -36.1(2) . .
C12 Y1 C9 C10 -75.8(2) . .
Al1 Y1 C9 C10 -73.4(3) . .
Al2 Y1 C9 C10 40.9(2) . .
C1 Y1 C9 C14 -126.4(3) . .
C8 Y1 C9 C14 30.4(3) . .
C13 Y1 C9 C14 123.7(4) . .
C10 Y1 C9 C14 -123.4(4) . .
C11 Y1 C9 C14 -159.6(4) . .
C12 Y1 C9 C14 160.7(4) . .
Al1 Y1 C9 C14 163.1(3) . .
Al2 Y1 C9 C14 -82.5(3) . .
C13 C9 C10 C11 -1.5(3) . .
C14 C9 C10 C11 -178.5(3) . .
Y1 C9 C10 C11 67.5(2) . .
C13 C9 C10 C15 171.8(3) . .
C14 C9 C10 C15 -5.2(5) . .
Y1 C9 C10 C15 -119.2(3) . .
C13 C9 C10 Y1 -69.0(2) . .
C14 C9 C10 Y1 114.0(3) . .
C1 Y1 C10 C11 62.7(2) . .
C8 Y1 C10 C11 -146.30(19) . .
C9 Y1 C10 C11 -115.4(3) . .
C13 Y1 C10 C11 -77.8(2) . .
C12 Y1 C10 C11 -37.3(2) . .
Al1 Y1 C10 C11 20.2(2) . .
Al2 Y1 C10 C11 99.95(19) . .
C1 Y1 C10 C9 178.04(19) . .
C8 Y1 C10 C9 -30.9(2) . .
C13 Y1 C10 C9 37.6(2) . .
C11 Y1 C10 C9 115.4(3) . .
C12 Y1 C10 C9 78.1(2) . .
Al1 Y1 C10 C9 135.61(18) . .
Al2 Y1 C10 C9 -144.68(19) . .
C1 Y1 C10 C15 -60.0(4) . .
C8 Y1 C10 C15 91.0(4) . .
C9 Y1 C10 C15 122.0(4) . .
C13 Y1 C10 C15 159.6(4) . .
C11 Y1 C10 C15 -122.7(4) . .
C12 Y1 C10 C15 -160.0(4) . .
Al1 Y1 C10 C15 -102.4(4) . .
Al2 Y1 C10 C15 -22.7(4) . .
C9 C10 C11 C12 1.4(3) . .
C15 C10 C11 C12 -171.9(3) . .
Y1 C10 C11 C12 67.8(2) . .
C9 C10 C11 C16 175.8(3) . .
C15 C10 C11 C16 2.4(5) . .
Y1 C10 C11 C16 -117.9(3) . .
C9 C10 C11 Y1 -66.4(2) . .
C15 C10 C11 Y1 120.3(3) . .
C1 Y1 C11 C10 -123.57(19) . .
C8 Y1 C11 C10 53.7(3) . .
C9 Y1 C11 C10 36.70(19) . .
C13 Y1 C11 C10 76.7(2) . .
C12 Y1 C11 C10 113.6(3) . .
Al1 Y1 C11 C10 -163.97(18) . .
Al2 Y1 C11 C10 -83.13(19) . .
C1 Y1 C11 C12 122.8(2) . .
C8 Y1 C11 C12 -59.9(3) . .
C9 Y1 C11 C12 -76.9(2) . .
C13 Y1 C11 C12 -37.0(2) . .
C10 Y1 C11 C12 -113.6(3) . .
Al1 Y1 C11 C12 82.39(19) . .
Al2 Y1 C11 C12 163.22(19) . .
C1 Y1 C11 C16 -1.6(4) . .
C8 Y1 C11 C16 175.6(3) . .
C9 Y1 C11 C16 158.6(4) . .
C13 Y1 C11 C16 -161.4(4) . .
C10 Y1 C11 C16 121.9(5) . .
C12 Y1 C11 C16 -124.4(5) . .
Al1 Y1 C11 C16 -42.0(4) . .
Al2 Y1 C11 C16 38.8(4) . .
C10 C11 C12 C13 -0.8(4) . .
C16 C11 C12 C13 -175.0(3) . .
Y1 C11 C12 C13 66.6(2) . .
C10 C11 C12 C17 171.5(3) . .
C16 C11 C12 C17 -2.7(6) . .
Y1 C11 C12 C17 -121.1(4) . .
C10 C11 C12 Y1 -67.4(2) . .
C16 C11 C12 Y1 118.4(3) . .
C1 Y1 C12 C11 -63.4(2) . .
C8 Y1 C12 C11 142.59(19) . .
C9 Y1 C12 C11 77.7(2) . .
C13 Y1 C12 C11 114.6(3) . .
C10 Y1 C12 C11 37.23(18) . .
Al1 Y1 C12 C11 -100.91(19) . .
Al2 Y1 C12 C11 -21.0(2) . .
C1 Y1 C12 C13 -178.1(2) . .
C8 Y1 C12 C13 27.9(3) . .
C9 Y1 C12 C13 -37.0(2) . .
C10 Y1 C12 C13 -77.4(2) . .
C11 Y1 C12 C13 -114.6(3) . .
Al1 Y1 C12 C13 144.4(2) . .
Al2 Y1 C12 C13 -135.68(19) . .
C1 Y1 C12 C17 59.8(4) . .
C8 Y1 C12 C17 -94.2(4) . .
C9 Y1 C12 C17 -159.1(5) . .
C13 Y1 C12 C17 -122.1(5) . .
C10 Y1 C12 C17 160.4(5) . .
C11 Y1 C12 C17 123.2(5) . .
Al1 Y1 C12 C17 22.3(4) . .
Al2 Y1 C12 C17 102.2(4) . .
C10 C9 C13 C12 1.0(4) . .
C14 C9 C13 C12 178.0(3) . .
Y1 C9 C13 C12 -68.0(2) . .
C10 C9 C13 C18 -175.3(3) . .
C14 C9 C13 C18 1.7(5) . .
Y1 C9 C13 C18 115.7(3) . .
C10 C9 C13 Y1 69.0(2) . .
C14 C9 C13 Y1 -114.0(3) . .
C11 C12 C13 C9 -0.1(4) . .
C17 C12 C13 C9 -172.5(3) . .
Y1 C12 C13 C9 67.0(2) . .
C11 C12 C13 C18 176.1(3) . .
C17 C12 C13 C18 3.8(6) . .
Y1 C12 C13 C18 -116.7(4) . .
C11 C12 C13 Y1 -67.2(2) . .
C17 C12 C13 Y1 120.5(4) . .
C1 Y1 C13 C9 -111.4(2) . .
C8 Y1 C13 C9 89.0(2) . .
C10 Y1 C13 C9 -37.88(19) . .
C11 Y1 C13 C9 -77.7(2) . .
C12 Y1 C13 C9 -114.3(3) . .
Al1 Y1 C13 C9 -155.45(17) . .
Al2 Y1 C13 C9 -41.8(3) . .
C1 Y1 C13 C12 2.9(3) . .
C8 Y1 C13 C12 -156.7(2) . .
C9 Y1 C13 C12 114.3(3) . .
C10 Y1 C13 C12 76.4(2) . .
C11 Y1 C13 C12 36.6(2) . .
Al1 Y1 C13 C12 -41.2(2) . .
Al2 Y1 C13 C12 72.5(3) . .
C1 Y1 C13 C18 126.9(4) . .
C8 Y1 C13 C18 -32.8(4) . .
C9 Y1 C13 C18 -121.7(5) . .
C10 Y1 C13 C18 -159.6(4) . .
C11 Y1 C13 C18 160.6(4) . .
C12 Y1 C13 C18 124.0(5) . .
Al1 Y1 C13 C18 82.8(4) . .
Al2 Y1 C13 C18 -163.5(3) . .
C1 Y2 C19 C20 -177.97(19) . .
C21 Y2 C19 C20 -36.58(19) . .
C23 Y2 C19 C20 -114.1(3) . .
C22 Y2 C19 C20 -77.0(2) . .
C8 Y2 C19 C20 31.2(2) 2_666 .
Al2 Y2 C19 C20 144.34(19) . .
Al1 Y2 C19 C20 -135.62(18) . .
C1 Y2 C19 C23 -63.86(19) . .
C20 Y2 C19 C23 114.1(3) . .
C21 Y2 C19 C23 77.53(19) . .
C22 Y2 C19 C23 37.06(17) . .
C8 Y2 C19 C23 145.28(17) 2_666 .
Al2 Y2 C19 C23 -101.55(17) . .
Al1 Y2 C19 C23 -21.5(2) . .
C1 Y2 C19 C24 58.2(3) . .
C20 Y2 C19 C24 -123.8(4) . .
C21 Y2 C19 C24 -160.4(4) . .
C23 Y2 C19 C24 122.1(4) . .
C22 Y2 C19 C24 159.2(3) . .
C8 Y2 C19 C24 -92.6(3) 2_666 .
Al2 Y2 C19 C24 20.6(3) . .
Al1 Y2 C19 C24 100.6(3) . .
C23 C19 C20 C21 0.5(3) . .
C24 C19 C20 C21 -171.0(3) . .
Y2 C19 C20 C21 67.5(2) . .
C23 C19 C20 C25 176.8(3) . .
C24 C19 C20 C25 5.3(5) . .
Y2 C19 C20 C25 -116.2(3) . .
C23 C19 C20 Y2 -67.1(2) . .
C24 C19 C20 Y2 121.5(3) . .
C1 Y2 C20 C21 -111.8(2) . .
C23 Y2 C20 C21 -77.7(2) . .
C19 Y2 C20 C21 -114.9(3) . .
C22 Y2 C20 C21 -37.65(18) . .
C8 Y2 C20 C21 91.26(19) 2_666 .
Al2 Y2 C20 C21 -156.34(16) . .
Al1 Y2 C20 C21 -42.0(2) . .
C1 Y2 C20 C19 3.1(3) . .
C21 Y2 C20 C19 114.9(3) . .
C23 Y2 C20 C19 37.20(18) . .
C22 Y2 C20 C19 77.2(2) . .
C8 Y2 C20 C19 -153.84(19) 2_666 .
Al2 Y2 C20 C19 -41.4(2) . .
Al1 Y2 C20 C19 72.9(2) . .
C1 Y2 C20 C25 126.0(3) . .
C21 Y2 C20 C25 -122.2(4) . .
C23 Y2 C20 C25 160.1(3) . .
C19 Y2 C20 C25 122.9(4) . .
C22 Y2 C20 C25 -159.8(3) . .
C8 Y2 C20 C25 -30.9(3) 2_666 .
Al2 Y2 C20 C25 81.5(3) . .
Al1 Y2 C20 C25 -164.2(2) . .
C19 C20 C21 C22 0.2(3) . .
C25 C20 C21 C22 -176.1(3) . .
Y2 C20 C21 C22 67.9(2) . .
C19 C20 C21 C26 175.2(3) . .
C25 C20 C21 C26 -1.1(5) . .
Y2 C20 C21 C26 -117.0(3) . .
C19 C20 C21 Y2 -67.7(2) . .
C25 C20 C21 Y2 115.9(3) . .
C1 Y2 C21 C20 110.3(2) . .
C23 Y2 C21 C20 77.1(2) . .
C19 Y2 C21 C20 36.90(19) . .
C22 Y2 C21 C20 113.7(3) . .
C8 Y2 C21 C20 -91.06(19) 2_666 .
Al2 Y2 C21 C20 38.5(3) . .
Al1 Y2 C21 C20 153.72(17) . .
C1 Y2 C21 C22 -3.4(3) . .
C20 Y2 C21 C22 -113.7(3) . .
C23 Y2 C21 C22 -36.63(17) . .
C19 Y2 C21 C22 -76.81(19) . .
C8 Y2 C21 C22 155.23(18) 2_666 .
Al2 Y2 C21 C22 -75.2(2) . .
Al1 Y2 C21 C22 40.01(19) . .
C1 Y2 C21 C26 -125.8(3) . .
C20 Y2 C21 C26 123.9(4) . .
C23 Y2 C21 C26 -159.0(3) . .
C19 Y2 C21 C26 160.8(4) . .
C22 Y2 C21 C26 -122.4(4) . .
C8 Y2 C21 C26 32.8(3) 2_666 .
Al2 Y2 C21 C26 162.4(2) . .
Al1 Y2 C21 C26 -82.4(3) . .
C20 C21 C22 C23 -0.7(3) . .
C26 C21 C22 C23 -175.9(3) . .
Y2 C21 C22 C23 66.8(2) . .
C20 C21 C22 C27 170.9(3) . .
C26 C21 C22 C27 -4.2(5) . .
Y2 C21 C22 C27 -121.5(3) . .
C20 C21 C22 Y2 -67.6(2) . .
C26 C21 C22 Y2 117.2(3) . .
C1 Y2 C22 C23 63.0(2) . .
C20 Y2 C22 C23 -77.6(2) . .
C21 Y2 C22 C23 -114.8(3) . .
C19 Y2 C22 C23 -37.30(18) . .
C8 Y2 C22 C23 -144.43(18) 2_666 .
Al2 Y2 C22 C23 20.6(2) . .
Al1 Y2 C22 C23 99.81(18) . .
C1 Y2 C22 C21 177.75(17) . .
C20 Y2 C22 C21 37.13(18) . .
C23 Y2 C22 C21 114.8(3) . .
C19 Y2 C22 C21 77.5(2) . .
C8 Y2 C22 C21 -29.7(2) 2_666 .
Al2 Y2 C22 C21 135.34(16) . .
Al1 Y2 C22 C21 -145.42(17) . .
C1 Y2 C22 C27 -59.8(3) . .
C20 Y2 C22 C27 159.5(3) . .
C21 Y2 C22 C27 122.4(4) . .
C23 Y2 C22 C27 -122.8(4) . .
C19 Y2 C22 C27 -160.1(3) . .
C8 Y2 C22 C27 92.8(3) 2_666 .
Al2 Y2 C22 C27 -102.3(3) . .
Al1 Y2 C22 C27 -23.0(3) . .
C21 C22 C23 C19 1.0(3) . .
C27 C22 C23 C19 -170.6(3) . .
Y2 C22 C23 C19 67.5(2) . .
C21 C22 C23 C28 174.9(3) . .
C27 C22 C23 C28 3.2(5) . .
Y2 C22 C23 C28 -118.6(3) . .
C21 C22 C23 Y2 -66.5(2) . .
C27 C22 C23 Y2 121.8(3) . .
C20 C19 C23 C22 -0.9(3) . .
C24 C19 C23 C22 170.7(3) . .
Y2 C19 C23 C22 -67.7(2) . .
C20 C19 C23 C28 -174.7(3) . .
C24 C19 C23 C28 -3.1(5) . .
Y2 C19 C23 C28 118.6(3) . .
C20 C19 C23 Y2 66.7(2) . .
C24 C19 C23 Y2 -121.7(3) . .
C1 Y2 C23 C22 -123.39(19) . .
C20 Y2 C23 C22 76.9(2) . .
C21 Y2 C23 C22 37.05(19) . .
C19 Y2 C23 C22 114.1(3) . .
C8 Y2 C23 C22 57.7(3) 2_666 .
Al2 Y2 C23 C22 -163.91(18) . .
Al1 Y2 C23 C22 -83.05(19) . .
C1 Y2 C23 C19 122.53(18) . .
C20 Y2 C23 C19 -37.19(17) . .
C21 Y2 C23 C19 -77.0(2) . .
C22 Y2 C23 C19 -114.1(3) . .
C8 Y2 C23 C19 -56.4(2) 2_666 .
Al2 Y2 C23 C19 82.01(17) . .
Al1 Y2 C23 C19 162.87(16) . .
C1 Y2 C23 C28 -1.0(3) . .
C20 Y2 C23 C28 -160.7(3) . .
C21 Y2 C23 C28 159.5(3) . .
C19 Y2 C23 C28 -123.5(4) . .
C22 Y2 C23 C28 122.4(4) . .
C8 Y2 C23 C28 -179.9(2) 2_666 .
Al2 Y2 C23 C28 -41.5(3) . .
Al1 Y2 C23 C28 39.4(3) . .
C35 Al4 C29 Al3 -177.6(6) . .
C31 Al4 C29 Al3 -49.0(6) . .
C32 Al4 C29 Al3 55.3(6) . .
Y3 Al4 C29 Al3 -64.6(6) . .
Y4 Al4 C29 Al3 65.8(6) . .
C35 Al4 C29 Y3 -113.04(13) . .
C31 Al4 C29 Y3 15.55(13) . .
C32 Al4 C29 Y3 119.84(11) . .
Y4 Al4 C29 Y3 130.34(10) . .
C35 Al4 C29 Y4 116.63(13) . .
C31 Al4 C29 Y4 -114.79(11) . .
C32 Al4 C29 Y4 -10.49(13) . .
Y3 Al4 C29 Y4 -130.34(10) . .
C34 Al3 C29 Al4 -178.3(6) . .
C30 Al3 C29 Al4 55.0(6) . .
C33 Al3 C29 Al4 -51.3(6) . .
Y4 Al3 C29 Al4 -65.8(6) . .
Y3 Al3 C29 Al4 64.4(6) . .
C34 Al3 C29 Y3 117.27(13) . .
C30 Al3 C29 Y3 -9.40(13) . .
C33 Al3 C29 Y3 -115.73(11) . .
Y4 Al3 C29 Y3 -130.25(10) . .
C34 Al3 C29 Y4 -112.48(13) . .
C30 Al3 C29 Y4 120.85(11) . .
C33 Al3 C29 Y4 14.52(13) . .
Y3 Al3 C29 Y4 130.25(10) . .
C37 Y3 C29 Al4 121.03(14) . .
C38 Y3 C29 Al4 119.59(10) . .
C41 Y3 C29 Al4 69.37(18) . .
C39 Y3 C29 Al4 90.79(10) . .
C40 Y3 C29 Al4 64.40(11) . .
C36 Y3 C29 Al4 -87.65(10) 2_565 .
Al3 Y3 C29 Al4 -166.34(14) . .
C37 Y3 C29 Al3 -72.63(16) . .
C38 Y3 C29 Al3 -74.07(11) . .
C41 Y3 C29 Al3 -124.29(15) . .
C39 Y3 C29 Al3 -102.87(10) . .
C40 Y3 C29 Al3 -129.26(9) . .
C36 Y3 C29 Al3 78.69(11) 2_565 .
Al4 Y3 C29 Al3 166.34(14) . .
C37 Y3 C29 Y4 -155.98(13) . .
C38 Y3 C29 Y4 -157.42(13) . .
C41 Y3 C29 Y4 152.36(14) . .
C39 Y3 C29 Y4 173.78(14) . .
C40 Y3 C29 Y4 147.39(13) . .
C36 Y3 C29 Y4 -4.66(17) 2_565 .
Al4 Y3 C29 Y4 82.99(14) . .
Al3 Y3 C29 Y4 -83.35(14) . .
C36 Y4 C29 Al4 84.86(11) . .
C48 Y4 C29 Al4 -69.11(15) . .
C47 Y4 C29 Al4 -118.85(14) . .
C49 Y4 C29 Al4 -73.62(11) . .
C51 Y4 C29 Al4 -128.12(9) . .
C50 Y4 C29 Al4 -102.80(10) . .
Al3 Y4 C29 Al4 166.20(15) . .
C36 Y4 C29 Al3 -81.34(11) . .
C48 Y4 C29 Al3 124.69(12) . .
C47 Y4 C29 Al3 74.95(17) . .
C49 Y4 C29 Al3 120.18(10) . .
C51 Y4 C29 Al3 65.68(11) . .
C50 Y4 C29 Al3 91.00(10) . .
Al4 Y4 C29 Al3 -166.20(15) . .
C36 Y4 C29 Y3 2.34(18) . .
C48 Y4 C29 Y3 -151.63(12) . .
C47 Y4 C29 Y3 158.63(12) . .
C49 Y4 C29 Y3 -156.14(13) . .
C51 Y4 C29 Y3 149.36(12) . .
C50 Y4 C29 Y3 174.69(14) . .
Al3 Y4 C29 Y3 83.68(14) . .
Al4 Y4 C29 Y3 -82.51(14) . .
C29 Y4 C36 Y3 9.0(6) . 2_565
C48 Y4 C36 Y3 171.6(6) . 2_565
C47 Y4 C36 Y3 -157.6(6) . 2_565
C49 Y4 C36 Y3 162.7(5) . 2_565
C51 Y4 C36 Y3 -137.6(5) . 2_565
C50 Y4 C36 Y3 -158.5(5) . 2_565
Al3 Y4 C36 Y3 -33.5(6) . 2_565
Al4 Y4 C36 Y3 52.2(6) . 2_565
C29 Y3 C37 C38 -2.6(3) . .
C41 Y3 C37 C38 113.5(3) . .
C39 Y3 C37 C38 37.01(17) . .
C40 Y3 C37 C38 76.62(19) . .
C36 Y3 C37 C38 -157.77(18) 2_565 .
Al4 Y3 C37 C38 64.7(2) . .
Al3 Y3 C37 C38 -46.5(2) . .
C29 Y3 C37 C41 -116.1(2) . .
C38 Y3 C37 C41 -113.5(3) . .
C39 Y3 C37 C41 -76.49(19) . .
C40 Y3 C37 C41 -36.89(17) . .
C36 Y3 C37 C41 88.73(19) 2_565 .
Al4 Y3 C37 C41 -48.8(3) . .
Al3 Y3 C37 C41 -160.04(16) . .
C29 Y3 C37 C42 121.2(3) . .
C38 Y3 C37 C42 123.8(4) . .
C41 Y3 C37 C42 -122.7(4) . .
C39 Y3 C37 C42 160.8(4) . .
C40 Y3 C37 C42 -159.6(4) . .
C36 Y3 C37 C42 -33.9(3) 2_565 .
Al4 Y3 C37 C42 -171.5(3) . .
Al3 Y3 C37 C42 77.3(3) . .
C41 C37 C38 C39 0.1(3) . .
C42 C37 C38 C39 177.2(3) . .
Y3 C37 C38 C39 -68.2(2) . .
C41 C37 C38 C43 -171.7(3) . .
C42 C37 C38 C43 5.4(5) . .
Y3 C37 C38 C43 120.0(3) . .
C41 C37 C38 Y3 68.3(2) . .
C42 C37 C38 Y3 -114.6(3) . .
C29 Y3 C38 C39 -67.57(19) . .
C37 Y3 C38 C39 114.2(3) . .
C41 Y3 C38 C39 76.56(19) . .
C40 Y3 C38 C39 36.49(17) . .
C36 Y3 C38 C39 141.65(17) 2_565 .
Al4 Y3 C38 C39 -25.2(2) . .
Al3 Y3 C38 C39 -106.06(17) . .
C29 Y3 C38 C37 178.23(18) . .
C41 Y3 C38 C37 -37.64(18) . .
C39 Y3 C38 C37 -114.2(3) . .
C40 Y3 C38 C37 -77.7(2) . .
C36 Y3 C38 C37 27.5(2) 2_565 .
Al4 Y3 C38 C37 -139.38(17) . .
Al3 Y3 C38 C37 139.74(18) . .
C29 Y3 C38 C43 54.2(3) . .
C37 Y3 C38 C43 -124.0(4) . .
C41 Y3 C38 C43 -161.7(4) . .
C39 Y3 C38 C43 121.8(4) . .
C40 Y3 C38 C43 158.2(4) . .
C36 Y3 C38 C43 -96.6(3) 2_565 .
Al4 Y3 C38 C43 96.6(3) . .
Al3 Y3 C38 C43 15.7(3) . .
C37 C38 C39 C40 -0.3(3) . .
C43 C38 C39 C40 171.8(3) . .
Y3 C38 C39 C40 -67.4(2) . .
C37 C38 C39 C44 -173.3(3) . .
C43 C38 C39 C44 -1.2(5) . .
Y3 C38 C39 C44 119.6(3) . .
C37 C38 C39 Y3 67.2(2) . .
C43 C38 C39 Y3 -120.8(3) . .
C29 Y3 C39 C40 -126.79(18) . .
C37 Y3 C39 C40 77.6(2) . .
C38 Y3 C39 C40 114.9(3) . .
C41 Y3 C39 C40 36.95(18) . .
C36 Y3 C39 C40 50.8(3) 2_565 .
Al4 Y3 C39 C40 -86.08(17) . .
Al3 Y3 C39 C40 -166.81(16) . .
C29 Y3 C39 C38 118.31(19) . .
C37 Y3 C39 C38 -37.32(19) . .
C41 Y3 C39 C38 -77.9(2) . .
C40 Y3 C39 C38 -114.9(3) . .
C36 Y3 C39 C38 -64.1(2) 2_565 .
Al4 Y3 C39 C38 159.02(17) . .
Al3 Y3 C39 C38 78.30(18) . .
C29 Y3 C39 C44 -2.6(3) . .
C37 Y3 C39 C44 -158.2(3) . .
C38 Y3 C39 C44 -120.9(4) . .
C41 Y3 C39 C44 161.2(3) . .
C40 Y3 C39 C44 124.2(4) . .
C36 Y3 C39 C44 175.0(2) 2_565 .
Al4 Y3 C39 C44 38.1(3) . .
Al3 Y3 C39 C44 -42.6(3) . .
C38 C39 C40 C41 0.4(3) . .
C44 C39 C40 C41 173.2(3) . .
Y3 C39 C40 C41 -65.9(2) . .
C38 C39 C40 C45 -172.3(3) . .
C44 C39 C40 C45 0.5(5) . .
Y3 C39 C40 C45 121.4(3) . .
C38 C39 C40 Y3 66.3(2) . .
C44 C39 C40 Y3 -120.9(3) . .
C29 Y3 C40 C39 59.47(19) . .
C37 Y3 C40 C39 -77.4(2) . .
C38 Y3 C40 C39 -36.93(18) . .
C41 Y3 C40 C39 -114.8(3) . .
C36 Y3 C40 C39 -149.17(17) 2_565 .
Al4 Y3 C40 C39 95.42(17) . .
Al3 Y3 C40 C39 17.4(2) . .
C29 Y3 C40 C41 174.24(18) . .
C37 Y3 C40 C41 37.37(19) . .
C38 Y3 C40 C41 77.8(2) . .
C39 Y3 C40 C41 114.8(3) . .
C36 Y3 C40 C41 -34.4(2) 2_565 .
Al4 Y3 C40 C41 -149.81(18) . .
Al3 Y3 C40 C41 132.19(17) . .
C29 Y3 C40 C45 -63.9(3) . .
C37 Y3 C40 C45 159.2(3) . .
C38 Y3 C40 C45 -160.3(3) . .
C41 Y3 C40 C45 121.9(4) . .
C39 Y3 C40 C45 -123.4(4) . .
C36 Y3 C40 C45 87.5(3) 2_565 .
Al4 Y3 C40 C45 -27.9(3) . .
Al3 Y3 C40 C45 -105.9(3) . .
C39 C40 C41 C37 -0.3(3) . .
C45 C40 C41 C37 172.4(3) . .
Y3 C40 C41 C37 -66.8(2) . .
C39 C40 C41 C46 -174.7(3) . .
C45 C40 C41 C46 -1.9(5) . .
Y3 C40 C41 C46 118.9(3) . .
C39 C40 C41 Y3 66.5(2) . .
C45 C40 C41 Y3 -120.8(3) . .
C38 C37 C41 C40 0.1(3) . .
C42 C37 C41 C40 -177.0(3) . .
Y3 C37 C41 C40 68.2(2) . .
C38 C37 C41 C46 174.4(3) . .
C42 C37 C41 C46 -2.8(5) . .
Y3 C37 C41 C46 -117.6(3) . .
C38 C37 C41 Y3 -68.1(2) . .
C42 C37 C41 Y3 114.8(3) . .
C29 Y3 C41 C40 -8.9(3) . .
C37 Y3 C41 C40 -114.3(3) . .
C38 Y3 C41 C40 -76.8(2) . .
C39 Y3 C41 C40 -36.59(17) . .
C36 Y3 C41 C40 151.17(18) 2_565 .
Al4 Y3 C41 C40 34.7(2) . .
Al3 Y3 C41 C40 -81.4(2) . .
C29 Y3 C41 C37 105.4(2) . .
C38 Y3 C41 C37 37.53(19) . .
C39 Y3 C41 C37 77.7(2) . .
C40 Y3 C41 C37 114.3(3) . .
C36 Y3 C41 C37 -94.54(19) 2_565 .
Al4 Y3 C41 C37 148.99(17) . .
Al3 Y3 C41 C37 32.8(3) . .
C29 Y3 C41 C46 -131.3(3) . .
C37 Y3 C41 C46 123.3(4) . .
C38 Y3 C41 C46 160.8(3) . .
C39 Y3 C41 C46 -159.0(3) . .
C40 Y3 C41 C46 -122.4(4) . .
C36 Y3 C41 C46 28.7(3) 2_565 .
Al4 Y3 C41 C46 -87.7(3) . .
Al3 Y3 C41 C46 156.1(2) . .
C29 Y4 C47 C48 97.7(2) . .
C36 Y4 C47 C48 -102.20(17) . .
C49 Y4 C47 C48 37.43(16) . .
C51 Y4 C47 C48 114.1(2) . .
C50 Y4 C47 C48 77.12(18) . .
Al3 Y4 C47 C48 144.87(15) . .
Al4 Y4 C47 C48 26.4(2) . .
C29 Y4 C47 C51 -16.4(2) . .
C36 Y4 C47 C51 143.68(17) . .
C48 Y4 C47 C51 -114.1(2) . .
C49 Y4 C47 C51 -76.68(18) . .
C50 Y4 C47 C51 -36.99(16) . .
Al3 Y4 C47 C51 30.75(18) . .
Al4 Y4 C47 C51 -87.71(18) . .
C29 Y4 C47 C52 -140.7(2) . .
C36 Y4 C47 C52 19.4(2) . .
C48 Y4 C47 C52 121.6(3) . .
C49 Y4 C47 C52 159.0(3) . .
C51 Y4 C47 C52 -124.3(3) . .
C50 Y4 C47 C52 -161.3(3) . .
Al3 Y4 C47 C52 -93.6(2) . .
Al4 Y4 C47 C52 147.98(19) . .
C51 C47 C48 C49 -0.5(3) . .
C52 C47 C48 C49 175.9(3) . .
Y4 C47 C48 C49 -68.4(2) . .
C51 C47 C48 C53 -175.5(3) . .
C52 C47 C48 C53 0.8(5) . .
Y4 C47 C48 C53 116.5(3) . .
C51 C47 C48 Y4 67.9(2) . .
C52 C47 C48 Y4 -115.7(3) . .
C29 Y4 C48 C47 -122.04(17) . .
C36 Y4 C48 C47 79.93(17) . .
C49 Y4 C48 C47 -113.7(2) . .
C51 Y4 C48 C47 -37.15(16) . .
C50 Y4 C48 C47 -77.22(18) . .
Al3 Y4 C48 C47 -56.8(2) . .
Al4 Y4 C48 C47 -163.17(14) . .
C29 Y4 C48 C49 -8.3(2) . .
C36 Y4 C48 C49 -166.37(17) . .
C47 Y4 C48 C49 113.7(2) . .
C51 Y4 C48 C49 76.56(18) . .
C50 Y4 C48 C49 36.49(16) . .
Al3 Y4 C48 C49 56.9(2) . .
Al4 Y4 C48 C49 -49.46(18) . .
C29 Y4 C48 C53 115.2(2) . .
C36 Y4 C48 C53 -42.9(2) . .
C47 Y4 C48 C53 -122.8(3) . .
C49 Y4 C48 C53 123.5(3) . .
C51 Y4 C48 C53 -159.9(3) . .
C50 Y4 C48 C53 160.0(3) . .
Al3 Y4 C48 C53 -179.59(18) . .
Al4 Y4 C48 C53 74.0(2) . .
C47 C48 C49 C50 0.6(3) . .
C53 C48 C49 C50 175.6(3) . .
Y4 C48 C49 C50 -67.5(2) . .
C47 C48 C49 C54 -171.6(3) . .
C53 C48 C49 C54 3.4(5) . .
Y4 C48 C49 C54 120.4(3) . .
C47 C48 C49 Y4 68.0(2) . .
C53 C48 C49 Y4 -117.0(3) . .
C29 Y4 C49 C50 -71.11(17) . .
C36 Y4 C49 C50 131.86(16) . .
C48 Y4 C49 C50 114.7(2) . .
C47 Y4 C49 C50 77.35(18) . .
C51 Y4 C49 C50 37.04(16) . .
Al3 Y4 C49 C50 -30.06(18) . .
Al4 Y4 C49 C50 -109.18(16) . .
C29 Y4 C49 C48 174.14(16) . .
C36 Y4 C49 C48 17.1(2) . .
C47 Y4 C49 C48 -37.40(16) . .
C51 Y4 C49 C48 -77.71(18) . .
C50 Y4 C49 C48 -114.7(2) . .
Al3 Y4 C49 C48 -144.81(15) . .
Al4 Y4 C49 C48 136.07(16) . .
C29 Y4 C49 C54 51.8(3) . .
C36 Y4 C49 C54 -105.2(3) . .
C48 Y4 C49 C54 -122.3(3) . .
C47 Y4 C49 C54 -159.7(3) . .
C51 Y4 C49 C54 160.0(3) . .
C50 Y4 C49 C54 122.9(3) . .
Al3 Y4 C49 C54 92.9(3) . .
Al4 Y4 C49 C54 13.7(3) . .
C48 C49 C50 C51 -0.4(3) . .
C54 C49 C50 C51 171.8(3) . .
Y4 C49 C50 C51 -66.9(2) . .
C48 C49 C50 C55 -174.6(3) . .
C54 C49 C50 C55 -2.3(5) . .
Y4 C49 C50 C55 119.0(3) . .
C48 C49 C50 Y4 66.5(2) . .
C54 C49 C50 Y4 -121.3(3) . .
C29 Y4 C50 C49 114.33(17) . .
C36 Y4 C50 C49 -76.3(2) . .
C48 Y4 C50 C49 -37.11(16) . .
C47 Y4 C50 C49 -77.44(18) . .
C51 Y4 C50 C49 -114.6(2) . .
Al3 Y4 C50 C49 154.70(16) . .
Al4 Y4 C50 C49 74.56(16) . .
C29 Y4 C50 C51 -131.09(17) . .
C36 Y4 C50 C51 38.3(2) . .
C48 Y4 C50 C51 77.47(18) . .
C47 Y4 C50 C51 37.14(16) . .
C49 Y4 C50 C51 114.6(2) . .
Al3 Y4 C50 C51 -90.71(16) . .
Al4 Y4 C50 C51 -170.86(15) . .
C29 Y4 C50 C55 -8.3(3) . .
C36 Y4 C50 C55 161.1(2) . .
C48 Y4 C50 C55 -159.7(3) . .
C47 Y4 C50 C55 160.0(3) . .
C49 Y4 C50 C55 -122.6(3) . .
C51 Y4 C50 C55 122.8(3) . .
Al3 Y4 C50 C55 32.1(2) . .
Al4 Y4 C50 C55 -48.0(2) . .
C48 C47 C51 C50 0.2(3) . .
C52 C47 C51 C50 -176.0(3) . .
Y4 C47 C51 C50 67.5(2) . .
C48 C47 C51 C56 172.6(3) . .
C52 C47 C51 C56 -3.7(5) . .
Y4 C47 C51 C56 -120.1(3) . .
C48 C47 C51 Y4 -67.3(2) . .
C52 C47 C51 Y4 116.5(3) . .
C49 C50 C51 C47 0.1(3) . .
C55 C50 C51 C47 174.3(3) . .
Y4 C50 C51 C47 -66.80(19) . .
C49 C50 C51 C56 -172.4(3) . .
C55 C50 C51 C56 1.7(5) . .
Y4 C50 C51 C56 120.6(3) . .
C49 C50 C51 Y4 66.9(2) . .
C55 C50 C51 Y4 -118.9(3) . .
C29 Y4 C51 C47 169.68(15) . .
C36 Y4 C51 C47 -40.99(18) . .
C48 Y4 C51 C47 37.23(16) . .
C49 Y4 C51 C47 77.62(18) . .
C50 Y4 C51 C47 114.3(2) . .
Al3 Y4 C51 C47 -154.15(15) . .
Al4 Y4 C51 C47 126.46(15) . .
C29 Y4 C51 C50 55.38(18) . .
C36 Y4 C51 C50 -155.28(16) . .
C48 Y4 C51 C50 -77.07(18) . .
C47 Y4 C51 C50 -114.3(2) . .
C49 Y4 C51 C50 -36.67(16) . .
Al3 Y4 C51 C50 91.56(16) . .
Al4 Y4 C51 C50 12.2(2) . .
C29 Y4 C51 C56 -66.4(3) . .
C36 Y4 C51 C56 82.9(2) . .
C48 Y4 C51 C56 161.1(3) . .
C47 Y4 C51 C56 123.9(3) . .
C49 Y4 C51 C56 -158.5(3) . .
C50 Y4 C51 C56 -121.8(3) . .
Al3 Y4 C51 C56 -30.3(2) . .
Al4 Y4 C51 C56 -109.7(2) . .
