#------------------------------------------------------------------------------
#$Date: 2016-03-22 11:46:30 +0200 (Tue, 22 Mar 2016) $
#$Revision: 178915 $
#$URL: svn://www.crystallography.net/cod/cif/4/11/44/4114482.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4114482
loop_
_publ_author_name
'Eric G. Tulsky'
'Nathan R. M. Crawford'
'Stéphane A. Baudron'
'Patrick Batail'
'Jeffrey R. Long'
_publ_section_title
;
 Cluster-to-Metal Magnetic Coupling: Synthesis and Characterization of
 25-Electron [Re6-nOsnSe8(CN)6](5-n)- (n = 1, 2) Clusters and
 {Re6-nOsnSe8[CNCu(Me6tren)]6}9+ (n = 0, 1, 2) Assemblies
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              15543
_journal_page_last               15553
_journal_paper_doi               10.1021/ja037444q
_journal_volume                  125
_journal_year                    2003
_chemical_formula_sum            'C78 H60 N6 Os P3 Re5 Se8'
_chemical_formula_weight         2927.11
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL
_cell_angle_alpha                91.5910(10)
_cell_angle_beta                 91.1040(10)
_cell_angle_gamma                104.4740(10)
_cell_formula_units_Z            2
_cell_length_a                   13.1760(3)
_cell_length_b                   13.4661(3)
_cell_length_c                   23.1766(5)
_cell_measurement_temperature    159(2)
_cell_volume                     3978.70(15)
_computing_cell_refinement       'Siemens XSCANS'
_computing_data_collection       'Siemens XSCANS'
_computing_data_reduction        'Siemens SHELXTL'
_computing_molecular_graphics    'Siemens SHELXTL'
_computing_publication_material  'Siemens SHELXTL'
_computing_structure_refinement  'SHELXL-93 (Sheldrick, 1993)'
_computing_structure_solution    'SHELXS-86 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measurement_device       'Siemens P4'
_diffrn_measurement_method       'ω scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0302
_diffrn_reflns_av_sigmaI/netI    0.0724
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_k_max       14
_diffrn_reflns_limit_k_min       -15
_diffrn_reflns_limit_l_max       28
_diffrn_reflns_limit_l_min       -19
_diffrn_reflns_number            20354
_diffrn_reflns_theta_max         25.68
_diffrn_reflns_theta_min         1.76
_exptl_absorpt_coefficient_mu    12.932
_exptl_absorpt_correction_type   none
_exptl_crystal_colour            red-orange
_exptl_crystal_density_diffrn    2.443
_exptl_crystal_description       block
_exptl_crystal_F_000             2676
_exptl_crystal_size_max          0.23
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_min          0.09
_refine_diff_density_max         2.551
_refine_diff_density_min         -2.141
_refine_diff_density_rms         0.214
_refine_ls_extinction_coef       0.000046(10)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_all   0.903
_refine_ls_goodness_of_fit_obs   1.075
_refine_ls_matrix_type           full
_refine_ls_number_parameters     907
_refine_ls_number_reflns         12819
_refine_ls_number_restraints     0
_refine_ls_restrained_S_all      0.903
_refine_ls_restrained_S_obs      1.075
_refine_ls_R_factor_all          0.0732
_refine_ls_R_factor_obs          0.0408
_refine_ls_shift/esd_max         0.013
_refine_ls_shift/esd_mean        0.001
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0469P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_all         0.0946
_refine_ls_wR_factor_obs         0.0878
_reflns_number_observed          8129
_reflns_number_total             12819
_reflns_observed_criterion       >2sigma(I)
_cod_data_source_file            ja037444qsi20031002_112603_1.cif
_cod_data_source_block           1
_cod_depositor_comments
;
The following automatic conversions were performed:

'_refine_ls_weighting_scheme' value 'calc
w=1/[\s^2^(Fo^2^)+(0.0469P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' was
changed to 'calc'. New tag '_refine_ls_weighting_details' was
created. The value of the new tag was set to
'w=1/[\s^2^(Fo^2^)+(0.0469P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3'.

Automatic conversion script
Id: cif_fix_values 3143 2015-03-26 13:38:13Z robertas 
;
_cod_original_cell_volume        3978.7(2)
_cod_database_code               4114482
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_thermal_displace_type
_atom_site_occupancy
_atom_site_calc_flag
_atom_site_refinement_flags
Re1 Re 0.90411(4) 0.40287(3) 0.03972(2) 0.03109(13) Uani 0.83 d P
Re2 Re 1.02161(4) 0.58783(3) 0.06496(2) 0.03051(13) Uani 0.83 d P
Re3 Re 1.10746(4) 0.44386(3) 0.02553(2) 0.03054(13) Uani 0.83 d P
Re4 Re 0.44041(4) 0.91830(4) 0.43601(2) 0.03406(13) Uani 0.83 d P
Re5 Re 0.51351(4) 1.11640(4) 0.45712(2) 0.03589(14) Uani 0.83 d P
Re6 Re 0.63219(4) 0.99056(4) 0.47819(2) 0.03579(14) Uani 0.83 d P
Os1 Os 0.90411(4) 0.40287(3) 0.03972(2) 0.03109(13) Uani 0.17 d P
Os2 Os 1.02161(4) 0.58783(3) 0.06496(2) 0.03051(13) Uani 0.17 d P
Os3 Os 1.10746(4) 0.44386(3) 0.02553(2) 0.03054(13) Uani 0.17 d P
Os4 Os 0.44041(4) 0.91830(4) 0.43601(2) 0.03406(13) Uani 0.17 d P
Os5 Os 0.51351(4) 1.11640(4) 0.45712(2) 0.03589(14) Uani 0.17 d P
Os6 Os 0.63219(4) 0.99056(4) 0.47819(2) 0.03579(14) Uani 0.17 d P
Se1 Se 0.99107(10) 0.26932(9) 0.00005(5) 0.0351(3) Uani 1 d .
Se2 Se 0.78467(10) 0.37657(9) -0.04846(5) 0.0371(3) Uani 1 d .
Se3 Se 1.03180(10) 0.43794(9) 0.12432(4) 0.0367(3) Uani 1 d .
Se4 Se 0.82630(10) 0.54520(9) 0.07570(5) 0.0365(3) Uani 1 d .
Se5 Se 0.55584(11) 0.80133(10) 0.46010(5) 0.0478(3) Uani 1 d .
Se6 Se 0.33072(9) 1.04182(10) 0.41794(5) 0.0378(3) Uani 1 d .
Se7 Se 0.30349(10) 0.81983(10) 0.50110(5) 0.0460(4) Uani 1 d .
Se8 Se 0.58176(10) 1.02468(11) 0.37657(5) 0.0450(3) Uani 1 d .
C1 C 0.7942(10) 0.2937(9) 0.0841(4) 0.042(3) Uani 1 d .
N1 N 0.7379(9) 0.2341(8) 0.1105(5) 0.064(4) Uani 1 d .
C2 C 1.0460(9) 0.6862(9) 0.1386(5) 0.039(3) Uani 1 d .
N2 N 1.0602(9) 0.7366(8) 0.1804(4) 0.053(3) Uani 1 d .
C3 C 1.2280(11) 0.3799(9) 0.0539(5) 0.041(3) Uani 1 d .
N3 N 1.2948(9) 0.3438(8) 0.0668(4) 0.047(3) Uani 1 d .
C4 C 0.3737(10) 0.8257(11) 0.3632(5) 0.053(4) Uani 1 d .
N4 N 0.3331(9) 0.7738(9) 0.3254(5) 0.066(4) Uani 1 d .
C5 C 0.5239(12) 1.2524(10) 0.4148(5) 0.065(5) Uani 1 d .
N5 N 0.5454(19) 1.3138(20) 0.3862(10) 0.056(4) Uiso 0.50 d P
N5A N 0.5093(19) 1.3381(19) 0.4003(10) 0.056(4) Uiso 0.50 d P
C6 C 0.7782(9) 0.9771(11) 0.4533(5) 0.053(4) Uani 1 d .
N6 N 0.8574(10) 0.9678(11) 0.4364(5) 0.076(4) Uani 1 d .
P1 P 1.2311(2) 0.2409(2) 0.25024(12) 0.0339(7) Uani 1 d .
C7 C 1.1336(8) 0.1601(8) 0.2038(4) 0.029(3) Uani 1 d .
C8 C 1.0522(9) 0.1934(9) 0.1787(5) 0.040(3) Uani 1 d .
H8 H 1.0478(9) 0.2607(9) 0.1852(5) 0.061 Uiso 1 calc R
C9 C 0.9788(10) 0.1275(10) 0.1447(5) 0.045(3) Uani 1 d .
H9 H 0.9246(10) 0.1509(10) 0.1281(5) 0.068 Uiso 1 calc R
C10 C 0.9818(10) 0.0292(9) 0.1340(5) 0.042(3) Uani 1 d .
H10 H 0.9315(10) -0.0141(9) 0.1100(5) 0.063 Uiso 1 calc R
C11 C 1.0605(10) -0.0052(9) 0.1594(5) 0.041(3) Uani 1 d .
H11 H 1.0632(10) -0.0730(9) 0.1530(5) 0.062 Uiso 1 calc R
C12 C 1.1356(9) 0.0587(9) 0.1942(4) 0.036(3) Uani 1 d .
H12 H 1.1882(9) 0.0339(9) 0.2115(4) 0.053 Uiso 1 calc R
C13 C 1.2354(9) 0.3742(9) 0.2414(4) 0.035(3) Uani 1 d .
C14 C 1.2995(9) 0.4324(10) 0.2020(5) 0.040(3) Uani 1 d .
H14 H 1.3432(9) 0.4029(10) 0.1799(5) 0.060 Uiso 1 calc R
C15 C 1.2997(11) 0.5320(10) 0.1952(5) 0.054(4) Uani 1 d .
H15 H 1.3432(11) 0.5699(10) 0.1682(5) 0.081 Uiso 1 calc R
C16 C 1.2367(11) 0.5782(10) 0.2275(5) 0.054(4) Uani 1 d .
H16 H 1.2387(11) 0.6472(10) 0.2234(5) 0.080 Uiso 1 calc R
C17 C 1.1720(12) 0.5211(11) 0.2654(6) 0.061(4) Uani 1 d .
H17 H 1.1288(12) 0.5521(11) 0.2870(6) 0.092 Uiso 1 calc R
C18 C 1.1671(10) 0.4189(10) 0.2734(5) 0.048(3) Uani 1 d .
H18 H 1.1206(10) 0.3809(10) 0.2990(5) 0.072 Uiso 1 calc R
C19 C 1.3551(9) 0.2166(9) 0.2322(4) 0.035(3) Uani 1 d .
C20 C 1.3800(10) 0.2110(9) 0.1737(5) 0.045(3) Uani 1 d .
H20 H 1.3327(10) 0.2181(9) 0.1447(5) 0.067 Uiso 1 calc R
C21 C 1.4746(11) 0.1951(11) 0.1603(6) 0.058(4) Uani 1 d .
H21 H 1.4913(11) 0.1896(11) 0.1217(6) 0.087 Uiso 1 calc R
C22 C 1.5457(11) 0.1872(11) 0.2024(6) 0.066(4) Uani 1 d .
H22 H 1.6098(11) 0.1756(11) 0.1922(6) 0.099 Uiso 1 calc R
C23 C 1.5238(11) 0.1961(12) 0.2587(6) 0.067(5) Uani 1 d .
H23 H 1.5741(11) 0.1937(12) 0.2870(6) 0.100 Uiso 1 calc R
C24 C 1.4274(10) 0.2087(10) 0.2745(5) 0.052(4) Uani 1 d .
H24 H 1.4112(10) 0.2119(10) 0.3133(5) 0.077 Uiso 1 calc R
C25 C 1.1987(9) 0.2139(9) 0.3237(4) 0.034(3) Uani 1 d .
C26 C 1.2571(10) 0.2760(10) 0.3675(5) 0.047(3) Uani 1 d .
H26 H 1.3137(10) 0.3303(10) 0.3594(5) 0.071 Uiso 1 calc R
C27 C 1.2268(12) 0.2532(10) 0.4257(5) 0.055(4) Uani 1 d .
H27 H 1.2642(12) 0.2932(10) 0.4562(5) 0.082 Uiso 1 calc R
C28 C 1.1437(12) 0.1734(11) 0.4368(5) 0.058(4) Uani 1 d .
H28 H 1.1264(12) 0.1585(11) 0.4749(5) 0.088 Uiso 1 calc R
C29 C 1.0867(11) 0.1160(11) 0.3939(5) 0.059(4) Uani 1 d .
H29 H 1.0285(11) 0.0637(11) 0.4023(5) 0.089 Uiso 1 calc R
C30 C 1.1137(10) 0.1339(10) 0.3375(5) 0.048(3) Uani 1 d .
H30 H 1.0747(10) 0.0922(10) 0.3081(5) 0.072 Uiso 1 calc R
P2 P 0.6416(3) 0.8277(2) 0.13687(12) 0.0365(8) Uani 1 d .
C31 C 0.7107(8) 0.8873(9) 0.0762(4) 0.033(3) Uani 1 d .
C32 C 0.7280(9) 0.9938(9) 0.0718(4) 0.037(3) Uani 1 d .
H32 H 0.7012(9) 1.0311(9) 0.0994(4) 0.056 Uiso 1 calc R
C33 C 0.7839(9) 1.0438(9) 0.0274(5) 0.038(3) Uani 1 d .
H33 H 0.7940(9) 1.1143(9) 0.0244(5) 0.056 Uiso 1 calc R
C34 C 0.8248(9) 0.9888(10) -0.0128(4) 0.042(3) Uani 1 d .
H34 H 0.8633(9) 1.0232(10) -0.0427(4) 0.063 Uiso 1 calc R
C35 C 0.8105(10) 0.8835(10) -0.0100(5) 0.044(3) Uani 1 d .
H35 H 0.8398(10) 0.8477(10) -0.0372(5) 0.066 Uiso 1 calc R
C36 C 0.7513(9) 0.8327(9) 0.0342(5) 0.037(3) Uani 1 d .
H36 H 0.7387(9) 0.7618(9) 0.0359(5) 0.055 Uiso 1 calc R
C37 C 0.7277(9) 0.8632(9) 0.1984(4) 0.035(3) Uani 1 d .
C38 C 0.8157(9) 0.8243(9) 0.2011(4) 0.041(3) Uani 1 d .
H38 H 0.8275(9) 0.7810(9) 0.1714(4) 0.061 Uiso 1 calc R
C39 C 0.8875(10) 0.8500(10) 0.2484(5) 0.050(4) Uani 1 d .
H39 H 0.9446(10) 0.8212(10) 0.2509(5) 0.074 Uiso 1 calc R
C40 C 0.8724(10) 0.9179(11) 0.2909(5) 0.053(4) Uani 1 d .
H40 H 0.9192(10) 0.9349(11) 0.3223(5) 0.080 Uiso 1 calc R
C41 C 0.7875(11) 0.9610(10) 0.2868(5) 0.053(4) Uani 1 d .
H41 H 0.7790(11) 1.0083(10) 0.3151(5) 0.079 Uiso 1 calc R
C42 C 0.7140(10) 0.9347(9) 0.2406(5) 0.045(3) Uani 1 d .
H42 H 0.6573(10) 0.9642(9) 0.2382(5) 0.068 Uiso 1 calc R
C43 C 0.6050(9) 0.6908(9) 0.1277(5) 0.039(3) Uani 1 d .
C44 C 0.6289(10) 0.6245(10) 0.1667(5) 0.047(3) Uani 1 d .
H44 H 0.6705(10) 0.6500(10) 0.1993(5) 0.071 Uiso 1 calc R
C45 C 0.5915(10) 0.5214(11) 0.1575(6) 0.054(4) Uani 1 d .
H45 H 0.6095(10) 0.4773(11) 0.1838(6) 0.081 Uiso 1 calc R
C46 C 0.5289(12) 0.4809(12) 0.1112(7) 0.071(5) Uani 1 d .
H46 H 0.5059(12) 0.4102(12) 0.1052(7) 0.106 Uiso 1 calc R
C47 C 0.4999(13) 0.5467(12) 0.0730(6) 0.077(5) Uani 1 d .
H47 H 0.4537(13) 0.5205(12) 0.0422(6) 0.115 Uiso 1 calc R
C48 C 0.5389(11) 0.6490(10) 0.0806(5) 0.060(4) Uani 1 d .
H48 H 0.5215(11) 0.6927(10) 0.0539(5) 0.090 Uiso 1 calc R
C49 C 0.5222(10) 0.8677(10) 0.1425(5) 0.044(3) Uani 1 d .
C50 C 0.4626(10) 0.8484(9) 0.1918(5) 0.047(3) Uani 1 d .
H50 H 0.4895(10) 0.8234(9) 0.2241(5) 0.071 Uiso 1 calc R
C51 C 0.3632(11) 0.8660(11) 0.1930(6) 0.063(4) Uani 1 d .
H51 H 0.3249(11) 0.8546(11) 0.2266(6) 0.095 Uiso 1 calc R
C52 C 0.3213(13) 0.8998(12) 0.1454(7) 0.078(5) Uani 1 d .
H52 H 0.2537(13) 0.9089(12) 0.1457(7) 0.117 Uiso 1 calc R
C53 C 0.3813(12) 0.9205(12) 0.0960(6) 0.071(5) Uani 1 d .
H53 H 0.3545(12) 0.9454(12) 0.0635(6) 0.106 Uiso 1 calc R
C54 C 0.4799(11) 0.9040(11) 0.0958(5) 0.059(4) Uani 1 d .
H54 H 0.5192(11) 0.9180(11) 0.0627(5) 0.089 Uiso 1 calc R
P3 P 0.2001(3) 0.4557(3) 0.61766(13) 0.0426(9) Uani 1 d .
C55 C 0.0814(10) 0.3544(9) 0.6170(5) 0.046(3) Uani 1 d .
C56 C 0.0163(9) 0.3387(9) 0.6637(5) 0.041(3) Uani 1 d .
H56 H 0.0314(9) 0.3840(9) 0.6956(5) 0.062 Uiso 1 calc R
C57 C -0.0697(10) 0.2580(10) 0.6638(6) 0.052(4) Uani 1 d .
H57 H -0.1123(10) 0.2478(10) 0.6957(6) 0.078 Uiso 1 calc R
C58 C -0.0933(10) 0.1928(11) 0.6176(6) 0.057(4) Uani 1 d .
H58 H -0.1533(10) 0.1389(11) 0.6174(6) 0.085 Uiso 1 calc R
C59 C -0.0295(11) 0.2050(11) 0.5707(6) 0.070(5) Uani 1 d .
H59 H -0.0451(11) 0.1576(11) 0.5399(6) 0.105 Uiso 1 calc R
C60 C 0.0566(11) 0.2863(10) 0.5689(5) 0.059(4) Uani 1 d .
H60 H 0.0979(11) 0.2963(10) 0.5365(5) 0.088 Uiso 1 calc R
C61 C 0.2301(10) 0.4918(9) 0.5447(5) 0.042(3) Uani 1 d .
C62 C 0.3321(10) 0.5012(10) 0.5244(5) 0.052(4) Uani 1 d .
H62 H 0.3845(10) 0.4867(10) 0.5477(5) 0.079 Uiso 1 calc R
C63 C 0.3513(12) 0.5334(11) 0.4677(5) 0.067(5) Uani 1 d .
H63 H 0.4180(12) 0.5413(11) 0.4531(5) 0.100 Uiso 1 calc R
C64 C 0.2735(14) 0.5533(11) 0.4336(6) 0.068(5) Uani 1 d .
H64 H 0.2884(14) 0.5736(11) 0.3960(6) 0.101 Uiso 1 calc R
C65 C 0.1749(13) 0.5442(12) 0.4529(6) 0.077(5) Uani 1 d .
H65 H 0.1239(13) 0.5610(12) 0.4295(6) 0.115 Uiso 1 calc R
C66 C 0.1515(11) 0.5097(12) 0.5082(5) 0.068(5) Uani 1 d .
H66 H 0.0832(11) 0.4985(12) 0.5209(5) 0.101 Uiso 1 calc R
C67 C 0.1838(10) 0.5671(10) 0.6588(5) 0.050(4) Uani 1 d .
C68 C 0.1843(11) 0.5618(11) 0.7195(6) 0.064(4) Uani 1 d .
H68 H 0.1932(11) 0.5032(11) 0.7371(6) 0.096 Uiso 1 calc R
C69 C 0.1713(12) 0.6461(14) 0.7531(7) 0.083(6) Uani 1 d .
C70 C 0.1682(23) 0.7203(24) 0.7371(12) 0.045(5) Uiso 0.50 d P
C70A C 0.1484(22) 0.7411(21) 0.7143(12) 0.045(5) Uiso 0.50 d P
C71 C 0.1591(14) 0.7409(13) 0.6639(9) 0.098(6) Uani 1 d .
C72 C 0.1741(11) 0.6555(11) 0.6316(7) 0.071(5) Uani 1 d .
H72 H 0.1776(11) 0.6582(11) 0.5916(7) 0.106 Uiso 1 calc R
C73 C 0.3042(9) 0.4118(10) 0.6503(5) 0.042(3) Uani 1 d .
C74 C 0.3026(10) 0.3096(10) 0.6490(5) 0.048(3) Uani 1 d .
H74 H 0.2439(10) 0.2617(10) 0.6339(5) 0.072 Uiso 1 calc R
C75 C 0.3889(13) 0.2768(12) 0.6703(5) 0.063(4) Uani 1 d .
H75 H 0.3873(13) 0.2073(12) 0.6697(5) 0.094 Uiso 1 calc R
C76 C 0.4741(12) 0.3471(15) 0.6918(6) 0.070(5) Uani 1 d .
H76 H 0.5323(12) 0.3257(15) 0.7046(6) 0.106 Uiso 1 calc R
C77 C 0.4761(11) 0.4491(14) 0.6950(6) 0.068(5) Uani 1 d .
H77 H 0.5337(11) 0.4966(14) 0.7116(6) 0.102 Uiso 1 calc R
C78 C 0.3899(11) 0.4811(11) 0.6730(5) 0.060(4) Uani 1 d .
H78 H 0.3914(11) 0.5505(11) 0.6740(5) 0.090 Uiso 1 calc R
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Se Se -0.0929 2.2259 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Re Re -1.0185 7.2310 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Os Os -1.2165 7.6030 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C1 Re1 Se3 92.6(3) . .
C1 Re1 Se2 91.2(3) . .
Se3 Re1 Se2 176.25(4) . .
C1 Re1 Se4 91.5(3) . .
Se3 Re1 Se4 89.76(4) . .
Se2 Re1 Se4 90.04(4) . .
C1 Re1 Se1 92.4(3) . .
Se3 Re1 Se1 90.06(4) . .
Se2 Re1 Se1 89.88(4) . .
Se4 Re1 Se1 176.09(4) . .
C1 Re1 Os3 134.2(3) . 2_765
Se3 Re1 Os3 118.35(3) . 2_765
Se2 Re1 Os3 58.55(3) . 2_765
Se4 Re1 Os3 58.47(3) . 2_765
Se1 Re1 Os3 118.36(3) . 2_765
C1 Re1 Re3 134.2(3) . 2_765
Se3 Re1 Re3 118.35(3) . 2_765
Se2 Re1 Re3 58.55(3) . 2_765
Se4 Re1 Re3 58.47(3) . 2_765
Se1 Re1 Re3 118.36(3) . 2_765
Os3 Re1 Re3 0.00(3) 2_765 2_765
C1 Re1 Re3 135.7(3) . .
Se3 Re1 Re3 58.41(3) . .
Se2 Re1 Re3 118.58(3) . .
Se4 Re1 Re3 118.43(3) . .
Se1 Re1 Re3 58.35(3) . .
Os3 Re1 Re3 90.11(2) 2_765 .
Re3 Re1 Re3 90.11(2) 2_765 .
C1 Re1 Os3 135.7(3) . .
Se3 Re1 Os3 58.41(3) . .
Se2 Re1 Os3 118.58(3) . .
Se4 Re1 Os3 118.43(3) . .
Se1 Re1 Os3 58.35(3) . .
Os3 Re1 Os3 90.11(2) 2_765 .
Re3 Re1 Os3 90.11(2) 2_765 .
Re3 Re1 Os3 0.00(3) . .
C1 Re1 Os2 135.0(3) . .
Se3 Re1 Os2 58.23(3) . .
Se2 Re1 Os2 118.67(3) . .
Se4 Re1 Os2 58.38(3) . .
Se1 Re1 Os2 118.40(3) . .
Os3 Re1 Os2 60.13(2) 2_765 .
Re3 Re1 Os2 60.13(2) 2_765 .
Re3 Re1 Os2 60.06(2) . .
Os3 Re1 Os2 60.06(2) . .
C1 Re1 Re2 135.0(3) . .
Se3 Re1 Re2 58.23(3) . .
Se2 Re1 Re2 118.67(3) . .
Se4 Re1 Re2 58.38(3) . .
Se1 Re1 Re2 118.40(3) . .
Os3 Re1 Re2 60.13(2) 2_765 .
Re3 Re1 Re2 60.13(2) 2_765 .
Re3 Re1 Re2 60.06(2) . .
Os3 Re1 Re2 60.06(2) . .
Os2 Re1 Re2 0.00(3) . .
C1 Re1 Re2 134.8(3) . 2_765
Se3 Re1 Re2 118.49(3) . 2_765
Se2 Re1 Re2 58.49(3) . 2_765
Se4 Re1 Re2 118.51(3) . 2_765
Se1 Re1 Re2 58.32(3) . 2_765
Os3 Re1 Re2 60.06(2) 2_765 2_765
Re3 Re1 Re2 60.06(2) 2_765 2_765
Re3 Re1 Re2 60.10(2) . 2_765
Os3 Re1 Re2 60.10(2) . 2_765
Os2 Re1 Re2 90.19(2) . 2_765
Re2 Re1 Re2 90.19(2) . 2_765
C2 Re2 Se3 91.4(3) . .
C2 Re2 Se4 91.8(3) . .
Se3 Re2 Se4 90.18(4) . .
C2 Re2 Se1 92.2(3) . 2_765
Se3 Re2 Se1 176.40(4) . 2_765
Se4 Re2 Se1 89.52(4) . 2_765
C2 Re2 Se2 91.8(3) . 2_765
Se3 Re2 Se2 89.87(4) . 2_765
Se4 Re2 Se2 176.36(4) . 2_765
Se1 Re2 Se2 90.20(4) 2_765 2_765
C2 Re2 Re1 134.8(3) . .
Se3 Re2 Re1 58.64(3) . .
Se4 Re2 Re1 58.67(3) . .
Se1 Re2 Re1 118.32(3) 2_765 .
Se2 Re2 Re1 118.46(3) 2_765 .
C2 Re2 Os1 134.8(3) . .
Se3 Re2 Os1 58.64(3) . .
Se4 Re2 Os1 58.67(3) . .
Se1 Re2 Os1 118.32(3) 2_765 .
Se2 Re2 Os1 118.46(3) 2_765 .
Re1 Re2 Os1 0.00(3) . .
C2 Re2 Os1 135.4(3) . 2_765
Se3 Re2 Os1 118.40(3) . 2_765
Se4 Re2 Os1 118.38(3) . 2_765
Se1 Re2 Os1 58.77(3) 2_765 2_765
Se2 Re2 Os1 58.55(3) 2_765 2_765
Re1 Re2 Os1 89.81(2) . 2_765
Os1 Re2 Os1 89.81(2) . 2_765
C2 Re2 Re1 135.4(3) . 2_765
Se3 Re2 Re1 118.40(3) . 2_765
Se4 Re2 Re1 118.38(3) . 2_765
Se1 Re2 Re1 58.77(3) 2_765 2_765
Se2 Re2 Re1 58.55(3) 2_765 2_765
Re1 Re2 Re1 89.81(2) . 2_765
Os1 Re2 Re1 89.81(2) . 2_765
Os1 Re2 Re1 0.00(3) 2_765 2_765
C2 Re2 Re3 134.8(3) . .
Se3 Re2 Re3 58.50(3) . .
Se4 Re2 Re3 118.61(3) . .
Se1 Re2 Re3 118.67(3) 2_765 .
Se2 Re2 Re3 58.52(3) 2_765 .
Re1 Re2 Re3 59.96(2) . .
Os1 Re2 Re3 59.96(2) . .
Os1 Re2 Re3 59.92(2) 2_765 .
Re1 Re2 Re3 59.92(2) 2_765 .
C2 Re2 Os3 134.8(3) . .
Se3 Re2 Os3 58.50(3) . .
Se4 Re2 Os3 118.61(3) . .
Se1 Re2 Os3 118.67(3) 2_765 .
Se2 Re2 Os3 58.52(3) 2_765 .
Re1 Re2 Os3 59.96(2) . .
Os1 Re2 Os3 59.96(2) . .
Os1 Re2 Os3 59.92(2) 2_765 .
Re1 Re2 Os3 59.92(2) 2_765 .
Re3 Re2 Os3 0.00(3) . .
C2 Re2 Re3 135.3(3) . 2_765
Se3 Re2 Re3 118.53(3) . 2_765
Se4 Re2 Re3 58.48(3) . 2_765
Se1 Re2 Re3 58.42(3) 2_765 2_765
Se2 Re2 Re3 118.46(3) 2_765 2_765
Re1 Re2 Re3 59.91(2) . 2_765
Os1 Re2 Re3 59.91(2) . 2_765
Os1 Re2 Re3 59.91(2) 2_765 2_765
Re1 Re2 Re3 59.91(2) 2_765 2_765
Re3 Re2 Re3 89.92(2) . 2_765
Os3 Re2 Re3 89.92(2) . 2_765
C3 Re3 Se3 92.1(3) . .
C3 Re3 Se1 91.4(4) . .
Se3 Re3 Se1 90.43(4) . .
C3 Re3 Se4 91.7(3) . 2_765
Se3 Re3 Se4 176.24(5) . 2_765
Se1 Re3 Se4 89.46(4) . 2_765
C3 Re3 Se2 92.1(4) . 2_765
Se3 Re3 Se2 89.70(4) . 2_765
Se1 Re3 Se2 176.44(4) . 2_765
Se4 Re3 Se2 90.18(4) 2_765 2_765
C3 Re3 Os1 135.2(3) . 2_765
Se3 Re3 Os1 118.27(3) . 2_765
Se1 Re3 Os1 118.37(3) . 2_765
Se4 Re3 Os1 58.66(3) 2_765 2_765
Se2 Re3 Os1 58.58(3) 2_765 2_765
C3 Re3 Re1 135.2(3) . 2_765
Se3 Re3 Re1 118.27(3) . 2_765
Se1 Re3 Re1 118.37(3) . 2_765
Se4 Re3 Re1 58.66(3) 2_765 2_765
Se2 Re3 Re1 58.58(3) 2_765 2_765
Os1 Re3 Re1 0.00(3) 2_765 2_765
C3 Re3 Os1 134.9(3) . .
Se3 Re3 Os1 58.57(3) . .
Se1 Re3 Os1 58.80(3) . .
Se4 Re3 Os1 118.36(3) 2_765 .
Se2 Re3 Os1 118.45(4) 2_765 .
Os1 Re3 Os1 89.89(2) 2_765 .
Re1 Re3 Os1 89.89(2) 2_765 .
C3 Re3 Re1 134.9(3) . .
Se3 Re3 Re1 58.57(3) . .
Se1 Re3 Re1 58.80(3) . .
Se4 Re3 Re1 118.36(3) 2_765 .
Se2 Re3 Re1 118.45(4) 2_765 .
Os1 Re3 Re1 89.89(2) 2_765 .
Re1 Re3 Re1 89.89(2) 2_765 .
Os1 Re3 Re1 0.00(3) . .
C3 Re3 Os2 135.3(3) . .
Se3 Re3 Os2 58.25(3) . .
Se1 Re3 Os2 118.76(4) . .
Se4 Re3 Os2 118.67(3) 2_765 .
Se2 Re3 Os2 58.49(3) 2_765 .
Os1 Re3 Os2 60.03(2) 2_765 .
Re1 Re3 Os2 60.03(2) 2_765 .
Os1 Re3 Os2 59.98(2) . .
Re1 Re3 Os2 59.98(2) . .
C3 Re3 Re2 135.3(3) . .
Se3 Re3 Re2 58.25(3) . .
Se1 Re3 Re2 118.76(4) . .
Se4 Re3 Re2 118.67(3) 2_765 .
Se2 Re3 Re2 58.49(3) 2_765 .
Os1 Re3 Re2 60.03(2) 2_765 .
Re1 Re3 Re2 60.03(2) 2_765 .
Os1 Re3 Re2 59.98(2) . .
Re1 Re3 Re2 59.98(2) . .
Os2 Re3 Re2 0.00(3) . .
C3 Re3 Os2 134.6(3) . 2_765
Se3 Re3 Os2 118.54(4) . 2_765
Se1 Re3 Os2 58.42(3) . 2_765
Se4 Re3 Os2 58.38(3) 2_765 2_765
Se2 Re3 Os2 118.54(3) 2_765 2_765
Os1 Re3 Os2 59.96(2) 2_765 2_765
Re1 Re3 Os2 59.96(2) 2_765 2_765
Os1 Re3 Os2 59.99(2) . 2_765
Re1 Re3 Os2 59.99(2) . 2_765
Os2 Re3 Os2 90.08(2) . 2_765
Re2 Re3 Os2 90.08(2) . 2_765
C4 Re4 Se6 91.9(4) . .
C4 Re4 Se8 91.6(3) . .
Se6 Re4 Se8 89.38(4) . .
C4 Re4 Se7 92.2(3) . .
Se6 Re4 Se7 90.15(4) . .
Se8 Re4 Se7 176.20(5) . .
C4 Re4 Se5 92.0(4) . .
Se6 Re4 Se5 176.15(4) . .
Se8 Re4 Se5 90.60(5) . .
Se7 Re4 Se5 89.62(5) . .
C4 Re4 Os5 135.1(4) . 2_676
Se6 Re4 Os5 118.83(3) . 2_676
Se8 Re4 Os5 118.52(3) . 2_676
Se7 Re4 Os5 58.60(3) . 2_676
Se5 Re4 Os5 57.96(3) . 2_676
C4 Re4 Re5 135.1(4) . 2_676
Se6 Re4 Re5 118.83(3) . 2_676
Se8 Re4 Re5 118.52(3) . 2_676
Se7 Re4 Re5 58.60(3) . 2_676
Se5 Re4 Re5 57.96(3) . 2_676
Os5 Re4 Re5 0.00(3) 2_676 2_676
C4 Re4 Os6 135.4(4) . 2_676
Se6 Re4 Os6 58.79(3) . 2_676
Se8 Re4 Os6 118.26(4) . 2_676
Se7 Re4 Os6 58.44(4) . 2_676
Se5 Re4 Os6 118.00(3) . 2_676
Os5 Re4 Os6 60.05(2) 2_676 2_676
Re5 Re4 Os6 60.05(2) 2_676 2_676
C4 Re4 Re6 135.4(4) . 2_676
Se6 Re4 Re6 58.79(3) . 2_676
Se8 Re4 Re6 118.26(4) . 2_676
Se7 Re4 Re6 58.44(4) . 2_676
Se5 Re4 Re6 118.00(3) . 2_676
Os5 Re4 Re6 60.05(2) 2_676 2_676
Re5 Re4 Re6 60.05(2) 2_676 2_676
Os6 Re4 Re6 0.00(3) 2_676 2_676
C4 Re4 Os5 135.1(4) . .
Se6 Re4 Os5 58.50(3) . .
Se8 Re4 Os5 58.50(3) . .
Se7 Re4 Os5 118.20(4) . .
Se5 Re4 Os5 118.40(4) . .
Os5 Re4 Os5 89.76(2) 2_676 .
Re5 Re4 Os5 89.76(2) 2_676 .
Os6 Re4 Os5 59.77(2) 2_676 .
Re6 Re4 Os5 59.77(2) 2_676 .
C4 Re4 Re5 135.1(4) . .
Se6 Re4 Re5 58.50(3) . .
Se8 Re4 Re5 58.50(3) . .
Se7 Re4 Re5 118.20(4) . .
Se5 Re4 Re5 118.40(4) . .
Os5 Re4 Re5 89.76(2) 2_676 .
Re5 Re4 Re5 89.76(2) 2_676 .
Os6 Re4 Re5 59.77(2) 2_676 .
Re6 Re4 Re5 59.77(2) 2_676 .
Os5 Re4 Re5 0.00(3) . .
C4 Re4 Os6 134.7(4) . .
Se6 Re4 Os6 118.43(4) . .
Se8 Re4 Os6 58.70(3) . .
Se7 Re4 Os6 118.42(3) . .
Se5 Re4 Os6 58.50(3) . .
Os5 Re4 Os6 59.84(2) 2_676 .
Re5 Re4 Os6 59.84(2) 2_676 .
Os6 Re4 Os6 89.89(2) 2_676 .
Re6 Re4 Os6 89.89(2) 2_676 .
Os5 Re4 Os6 59.94(2) . .
Re5 Re4 Os6 59.94(2) . .
C5 Re5 Se5 86.5(4) . 2_676
C5 Re5 Se6 91.8(4) . .
Se5 Re5 Se6 90.57(4) 2_676 .
C5 Re5 Se8 96.5(4) . .
Se5 Re5 Se8 176.92(5) 2_676 .
Se6 Re5 Se8 89.11(4) . .
C5 Re5 Se7 91.8(4) . 2_676
Se5 Re5 Se7 90.12(5) 2_676 2_676
Se6 Re5 Se7 176.36(5) . 2_676
Se8 Re5 Se7 90.01(5) . 2_676
C5 Re5 Os6 131.4(5) . 2_676
Se5 Re5 Os6 58.92(4) 2_676 2_676
Se6 Re5 Os6 58.81(3) . 2_676
Se8 Re5 Os6 118.45(4) . 2_676
Se7 Re5 Os6 118.74(3) 2_676 2_676
C5 Re5 Re6 131.4(5) . 2_676
Se5 Re5 Re6 58.92(4) 2_676 2_676
Se6 Re5 Re6 58.81(3) . 2_676
Se8 Re5 Re6 118.45(4) . 2_676
Se7 Re5 Re6 118.74(3) 2_676 2_676
Os6 Re5 Re6 0.00(3) 2_676 2_676
C5 Re5 Os4 131.3(4) . 2_676
Se5 Re5 Os4 58.86(3) 2_676 2_676
Se6 Re5 Os4 119.02(3) . 2_676
Se8 Re5 Os4 118.77(4) . 2_676
Se7 Re5 Os4 58.53(3) 2_676 2_676
Os6 Re5 Os4 60.23(2) 2_676 2_676
Re6 Re5 Os4 60.23(2) 2_676 2_676
C5 Re5 Re4 131.3(4) . 2_676
Se5 Re5 Re4 58.86(3) 2_676 2_676
Se6 Re5 Re4 119.02(3) . 2_676
Se8 Re5 Re4 118.77(4) . 2_676
Se7 Re5 Re4 58.53(3) 2_676 2_676
Os6 Re5 Re4 60.23(2) 2_676 2_676
Re6 Re5 Re4 60.23(2) 2_676 2_676
Os4 Re5 Re4 0.00(3) 2_676 2_676
C5 Re5 Re6 138.2(5) . .
Se5 Re5 Re6 118.94(3) 2_676 .
Se6 Re5 Re6 118.22(4) . .
Se8 Re5 Re6 58.70(3) . .
Se7 Re5 Re6 58.43(4) 2_676 .
Os6 Re5 Re6 90.14(2) 2_676 .
Re6 Re5 Re6 90.14(2) 2_676 .
Os4 Re5 Re6 60.08(2) 2_676 .
Re4 Re5 Re6 60.08(2) 2_676 .
C5 Re5 Os6 138.2(5) . .
Se5 Re5 Os6 118.94(3) 2_676 .
Se6 Re5 Os6 118.22(4) . .
Se8 Re5 Os6 58.70(3) . .
Se7 Re5 Os6 58.43(4) 2_676 .
Os6 Re5 Os6 90.14(2) 2_676 .
Re6 Re5 Os6 90.14(2) 2_676 .
Os4 Re5 Os6 60.08(2) 2_676 .
Re4 Re5 Os6 60.08(2) 2_676 .
Re6 Re5 Os6 0.00(3) . .
C5 Re5 Os4 138.2(4) . .
Se5 Re5 Os4 119.00(4) 2_676 .
Se6 Re5 Os4 58.18(3) . .
Se8 Re5 Os4 58.37(3) . .
Se7 Re5 Os4 118.46(4) 2_676 .
Os6 Re5 Os4 60.09(2) 2_676 .
Re6 Re5 Os4 60.09(2) 2_676 .
Os4 Re5 Os4 90.24(2) 2_676 .
Re4 Re5 Os4 90.24(2) 2_676 .
Re6 Re5 Os4 60.04(2) . .
Os6 Re5 Os4 60.04(2) . .
C6 Re6 Se7 92.9(4) . 2_676
C6 Re6 Se5 91.0(4) . .
Se7 Re6 Se5 176.08(5) 2_676 .
C6 Re6 Se6 92.4(3) . 2_676
Se7 Re6 Se6 89.74(4) 2_676 2_676
Se5 Re6 Se6 89.75(4) . 2_676
C6 Re6 Se8 91.9(3) . .
Se7 Re6 Se8 89.90(4) 2_676 .
Se5 Re6 Se8 90.32(4) . .
Se6 Re6 Se8 175.65(5) 2_676 .
C6 Re6 Os5 134.3(4) . 2_676
Se7 Re6 Os5 118.62(4) 2_676 2_676
Se5 Re6 Os5 57.98(3) . 2_676
Se6 Re6 Os5 58.41(3) 2_676 2_676
Se8 Re6 Os5 118.18(3) . 2_676
C6 Re6 Re5 134.3(4) . 2_676
Se7 Re6 Re5 118.62(4) 2_676 2_676
Se5 Re6 Re5 57.98(3) . 2_676
Se6 Re6 Re5 58.41(3) 2_676 2_676
Se8 Re6 Re5 118.18(3) . 2_676
Os5 Re6 Re5 0.00(3) 2_676 2_676
C6 Re6 Re5 135.8(4) . .
Se7 Re6 Re5 58.54(3) 2_676 .
Se5 Re6 Re5 118.46(4) . .
Se6 Re6 Re5 117.93(4) 2_676 .
Se8 Re6 Re5 58.39(3) . .
Os5 Re6 Re5 89.86(2) 2_676 .
Re5 Re6 Re5 89.86(2) 2_676 .
C6 Re6 Os5 135.8(4) . .
Se7 Re6 Os5 58.54(3) 2_676 .
Se5 Re6 Os5 118.46(4) . .
Se6 Re6 Os5 117.93(4) 2_676 .
Se8 Re6 Os5 58.39(3) . .
Os5 Re6 Os5 89.86(2) 2_676 .
Re5 Re6 Os5 89.86(2) 2_676 .
Re5 Re6 Os5 0.00(3) . .
C6 Re6 Re4 135.9(4) . 2_676
Se7 Re6 Re4 58.48(3) 2_676 2_676
Se5 Re6 Re4 118.12(4) . 2_676
Se6 Re6 Re4 58.08(3) 2_676 2_676
Se8 Re6 Re4 118.24(4) . 2_676
Os5 Re6 Re4 60.15(2) 2_676 2_676
Re5 Re6 Re4 60.15(2) 2_676 2_676
Re5 Re6 Re4 59.86(2) . 2_676
Os5 Re6 Re4 59.86(2) . 2_676
C6 Re6 Os4 135.9(4) . 2_676
Se7 Re6 Os4 58.48(3) 2_676 2_676
Se5 Re6 Os4 118.12(4) . 2_676
Se6 Re6 Os4 58.08(3) 2_676 2_676
Se8 Re6 Os4 118.24(4) . 2_676
Os5 Re6 Os4 60.15(2) 2_676 2_676
Re5 Re6 Os4 60.15(2) 2_676 2_676
Re5 Re6 Os4 59.86(2) . 2_676
Os5 Re6 Os4 59.86(2) . 2_676
Re4 Re6 Os4 0.00(3) 2_676 2_676
C6 Re6 Os4 134.0(4) . .
Se7 Re6 Os4 118.56(4) 2_676 .
Se5 Re6 Os4 58.47(3) . .
Se6 Re6 Os4 118.32(3) 2_676 .
Se8 Re6 Os4 58.27(3) . .
Os5 Re6 Os4 59.93(2) 2_676 .
Re5 Re6 Os4 59.93(2) 2_676 .
Re5 Re6 Os4 60.02(2) . .
Os5 Re6 Os4 60.02(2) . .
Re4 Re6 Os4 90.11(2) 2_676 .
Os4 Re6 Os4 90.11(2) 2_676 .
C1 Os1 Se3 92.6(3) . .
C1 Os1 Se2 91.2(3) . .
Se3 Os1 Se2 176.25(4) . .
C1 Os1 Se4 91.5(3) . .
Se3 Os1 Se4 89.76(4) . .
Se2 Os1 Se4 90.04(4) . .
C1 Os1 Se1 92.4(3) . .
Se3 Os1 Se1 90.06(4) . .
Se2 Os1 Se1 89.88(4) . .
Se4 Os1 Se1 176.09(4) . .
C1 Os1 Os3 134.2(3) . 2_765
Se3 Os1 Os3 118.35(3) . 2_765
Se2 Os1 Os3 58.55(3) . 2_765
Se4 Os1 Os3 58.47(3) . 2_765
Se1 Os1 Os3 118.36(3) . 2_765
C1 Os1 Re3 134.2(3) . 2_765
Se3 Os1 Re3 118.35(3) . 2_765
Se2 Os1 Re3 58.55(3) . 2_765
Se4 Os1 Re3 58.47(3) . 2_765
Se1 Os1 Re3 118.36(3) . 2_765
Os3 Os1 Re3 0.00(3) 2_765 2_765
C1 Os1 Re3 135.7(3) . .
Se3 Os1 Re3 58.41(3) . .
Se2 Os1 Re3 118.58(3) . .
Se4 Os1 Re3 118.43(3) . .
Se1 Os1 Re3 58.35(3) . .
Os3 Os1 Re3 90.11(2) 2_765 .
Re3 Os1 Re3 90.11(2) 2_765 .
C1 Os1 Os3 135.7(3) . .
Se3 Os1 Os3 58.41(3) . .
Se2 Os1 Os3 118.58(3) . .
Se4 Os1 Os3 118.43(3) . .
Se1 Os1 Os3 58.35(3) . .
Os3 Os1 Os3 90.11(2) 2_765 .
Re3 Os1 Os3 90.11(2) 2_765 .
Re3 Os1 Os3 0.00(3) . .
C1 Os1 Os2 135.0(3) . .
Se3 Os1 Os2 58.23(3) . .
Se2 Os1 Os2 118.67(3) . .
Se4 Os1 Os2 58.38(3) . .
Se1 Os1 Os2 118.40(3) . .
Os3 Os1 Os2 60.13(2) 2_765 .
Re3 Os1 Os2 60.13(2) 2_765 .
Re3 Os1 Os2 60.06(2) . .
Os3 Os1 Os2 60.06(2) . .
C1 Os1 Re2 135.0(3) . .
Se3 Os1 Re2 58.23(3) . .
Se2 Os1 Re2 118.67(3) . .
Se4 Os1 Re2 58.38(3) . .
Se1 Os1 Re2 118.40(3) . .
Os3 Os1 Re2 60.13(2) 2_765 .
Re3 Os1 Re2 60.13(2) 2_765 .
Re3 Os1 Re2 60.06(2) . .
Os3 Os1 Re2 60.06(2) . .
Os2 Os1 Re2 0.00(3) . .
C1 Os1 Re2 134.8(3) . 2_765
Se3 Os1 Re2 118.49(3) . 2_765
Se2 Os1 Re2 58.49(3) . 2_765
Se4 Os1 Re2 118.51(3) . 2_765
Se1 Os1 Re2 58.32(3) . 2_765
Os3 Os1 Re2 60.06(2) 2_765 2_765
Re3 Os1 Re2 60.06(2) 2_765 2_765
Re3 Os1 Re2 60.10(2) . 2_765
Os3 Os1 Re2 60.10(2) . 2_765
Os2 Os1 Re2 90.19(2) . 2_765
Re2 Os1 Re2 90.19(2) . 2_765
C2 Os2 Se3 91.4(3) . .
C2 Os2 Se4 91.8(3) . .
Se3 Os2 Se4 90.18(4) . .
C2 Os2 Se1 92.2(3) . 2_765
Se3 Os2 Se1 176.40(4) . 2_765
Se4 Os2 Se1 89.52(4) . 2_765
C2 Os2 Se2 91.8(3) . 2_765
Se3 Os2 Se2 89.87(4) . 2_765
Se4 Os2 Se2 176.36(4) . 2_765
Se1 Os2 Se2 90.20(4) 2_765 2_765
C2 Os2 Re1 134.8(3) . .
Se3 Os2 Re1 58.64(3) . .
Se4 Os2 Re1 58.67(3) . .
Se1 Os2 Re1 118.32(3) 2_765 .
Se2 Os2 Re1 118.46(3) 2_765 .
C2 Os2 Os1 134.8(3) . .
Se3 Os2 Os1 58.64(3) . .
Se4 Os2 Os1 58.67(3) . .
Se1 Os2 Os1 118.32(3) 2_765 .
Se2 Os2 Os1 118.46(3) 2_765 .
Re1 Os2 Os1 0.00(3) . .
C2 Os2 Os1 135.4(3) . 2_765
Se3 Os2 Os1 118.40(3) . 2_765
Se4 Os2 Os1 118.38(3) . 2_765
Se1 Os2 Os1 58.77(3) 2_765 2_765
Se2 Os2 Os1 58.55(3) 2_765 2_765
Re1 Os2 Os1 89.81(2) . 2_765
Os1 Os2 Os1 89.81(2) . 2_765
C2 Os2 Re1 135.4(3) . 2_765
Se3 Os2 Re1 118.40(3) . 2_765
Se4 Os2 Re1 118.38(3) . 2_765
Se1 Os2 Re1 58.77(3) 2_765 2_765
Se2 Os2 Re1 58.55(3) 2_765 2_765
Re1 Os2 Re1 89.81(2) . 2_765
Os1 Os2 Re1 89.81(2) . 2_765
Os1 Os2 Re1 0.00(3) 2_765 2_765
C2 Os2 Re3 134.8(3) . .
Se3 Os2 Re3 58.50(3) . .
Se4 Os2 Re3 118.61(3) . .
Se1 Os2 Re3 118.67(3) 2_765 .
Se2 Os2 Re3 58.52(3) 2_765 .
Re1 Os2 Re3 59.96(2) . .
Os1 Os2 Re3 59.96(2) . .
Os1 Os2 Re3 59.92(2) 2_765 .
Re1 Os2 Re3 59.92(2) 2_765 .
C2 Os2 Os3 134.8(3) . .
Se3 Os2 Os3 58.50(3) . .
Se4 Os2 Os3 118.61(3) . .
Se1 Os2 Os3 118.67(3) 2_765 .
Se2 Os2 Os3 58.52(3) 2_765 .
Re1 Os2 Os3 59.96(2) . .
Os1 Os2 Os3 59.96(2) . .
Os1 Os2 Os3 59.92(2) 2_765 .
Re1 Os2 Os3 59.92(2) 2_765 .
Re3 Os2 Os3 0.00(3) . .
C2 Os2 Re3 135.3(3) . 2_765
Se3 Os2 Re3 118.53(3) . 2_765
Se4 Os2 Re3 58.48(3) . 2_765
Se1 Os2 Re3 58.42(3) 2_765 2_765
Se2 Os2 Re3 118.46(3) 2_765 2_765
Re1 Os2 Re3 59.91(2) . 2_765
Os1 Os2 Re3 59.91(2) . 2_765
Os1 Os2 Re3 59.91(2) 2_765 2_765
Re1 Os2 Re3 59.91(2) 2_765 2_765
Re3 Os2 Re3 89.92(2) . 2_765
Os3 Os2 Re3 89.92(2) . 2_765
C3 Os3 Se3 92.1(3) . .
C3 Os3 Se1 91.4(4) . .
Se3 Os3 Se1 90.43(4) . .
C3 Os3 Se4 91.7(3) . 2_765
Se3 Os3 Se4 176.24(5) . 2_765
Se1 Os3 Se4 89.46(4) . 2_765
C3 Os3 Se2 92.1(4) . 2_765
Se3 Os3 Se2 89.70(4) . 2_765
Se1 Os3 Se2 176.44(4) . 2_765
Se4 Os3 Se2 90.18(4) 2_765 2_765
C3 Os3 Os1 135.2(3) . 2_765
Se3 Os3 Os1 118.27(3) . 2_765
Se1 Os3 Os1 118.37(3) . 2_765
Se4 Os3 Os1 58.66(3) 2_765 2_765
Se2 Os3 Os1 58.58(3) 2_765 2_765
C3 Os3 Re1 135.2(3) . 2_765
Se3 Os3 Re1 118.27(3) . 2_765
Se1 Os3 Re1 118.37(3) . 2_765
Se4 Os3 Re1 58.66(3) 2_765 2_765
Se2 Os3 Re1 58.58(3) 2_765 2_765
Os1 Os3 Re1 0.00(3) 2_765 2_765
C3 Os3 Os1 134.9(3) . .
Se3 Os3 Os1 58.57(3) . .
Se1 Os3 Os1 58.80(3) . .
Se4 Os3 Os1 118.36(3) 2_765 .
Se2 Os3 Os1 118.45(4) 2_765 .
Os1 Os3 Os1 89.89(2) 2_765 .
Re1 Os3 Os1 89.89(2) 2_765 .
C3 Os3 Re1 134.9(3) . .
Se3 Os3 Re1 58.57(3) . .
Se1 Os3 Re1 58.80(3) . .
Se4 Os3 Re1 118.36(3) 2_765 .
Se2 Os3 Re1 118.45(4) 2_765 .
Os1 Os3 Re1 89.89(2) 2_765 .
Re1 Os3 Re1 89.89(2) 2_765 .
Os1 Os3 Re1 0.00(3) . .
C3 Os3 Os2 135.3(3) . .
Se3 Os3 Os2 58.25(3) . .
Se1 Os3 Os2 118.76(4) . .
Se4 Os3 Os2 118.67(3) 2_765 .
Se2 Os3 Os2 58.49(3) 2_765 .
Os1 Os3 Os2 60.03(2) 2_765 .
Re1 Os3 Os2 60.03(2) 2_765 .
Os1 Os3 Os2 59.98(2) . .
Re1 Os3 Os2 59.98(2) . .
C3 Os3 Re2 135.3(3) . .
Se3 Os3 Re2 58.25(3) . .
Se1 Os3 Re2 118.76(4) . .
Se4 Os3 Re2 118.67(3) 2_765 .
Se2 Os3 Re2 58.49(3) 2_765 .
Os1 Os3 Re2 60.03(2) 2_765 .
Re1 Os3 Re2 60.03(2) 2_765 .
Os1 Os3 Re2 59.98(2) . .
Re1 Os3 Re2 59.98(2) . .
Os2 Os3 Re2 0.00(3) . .
C3 Os3 Os2 134.6(3) . 2_765
Se3 Os3 Os2 118.54(4) . 2_765
Se1 Os3 Os2 58.42(3) . 2_765
Se4 Os3 Os2 58.38(3) 2_765 2_765
Se2 Os3 Os2 118.54(3) 2_765 2_765
Os1 Os3 Os2 59.96(2) 2_765 2_765
Re1 Os3 Os2 59.96(2) 2_765 2_765
Os1 Os3 Os2 59.99(2) . 2_765
Re1 Os3 Os2 59.99(2) . 2_765
Os2 Os3 Os2 90.08(2) . 2_765
Re2 Os3 Os2 90.08(2) . 2_765
C4 Os4 Se6 91.9(4) . .
C4 Os4 Se8 91.6(3) . .
Se6 Os4 Se8 89.38(4) . .
C4 Os4 Se7 92.2(3) . .
Se6 Os4 Se7 90.15(4) . .
Se8 Os4 Se7 176.20(5) . .
C4 Os4 Se5 92.0(4) . .
Se6 Os4 Se5 176.15(4) . .
Se8 Os4 Se5 90.60(5) . .
Se7 Os4 Se5 89.62(5) . .
C4 Os4 Os5 135.1(4) . 2_676
Se6 Os4 Os5 118.83(3) . 2_676
Se8 Os4 Os5 118.52(3) . 2_676
Se7 Os4 Os5 58.60(3) . 2_676
Se5 Os4 Os5 57.96(3) . 2_676
C4 Os4 Re5 135.1(4) . 2_676
Se6 Os4 Re5 118.83(3) . 2_676
Se8 Os4 Re5 118.52(3) . 2_676
Se7 Os4 Re5 58.60(3) . 2_676
Se5 Os4 Re5 57.96(3) . 2_676
Os5 Os4 Re5 0.00(3) 2_676 2_676
C4 Os4 Os6 135.4(4) . 2_676
Se6 Os4 Os6 58.79(3) . 2_676
Se8 Os4 Os6 118.26(4) . 2_676
Se7 Os4 Os6 58.44(4) . 2_676
Se5 Os4 Os6 118.00(3) . 2_676
Os5 Os4 Os6 60.05(2) 2_676 2_676
Re5 Os4 Os6 60.05(2) 2_676 2_676
C4 Os4 Re6 135.4(4) . 2_676
Se6 Os4 Re6 58.79(3) . 2_676
Se8 Os4 Re6 118.26(4) . 2_676
Se7 Os4 Re6 58.44(4) . 2_676
Se5 Os4 Re6 118.00(3) . 2_676
Os5 Os4 Re6 60.05(2) 2_676 2_676
Re5 Os4 Re6 60.05(2) 2_676 2_676
Os6 Os4 Re6 0.00(3) 2_676 2_676
C4 Os4 Os5 135.1(4) . .
Se6 Os4 Os5 58.50(3) . .
Se8 Os4 Os5 58.50(3) . .
Se7 Os4 Os5 118.20(4) . .
Se5 Os4 Os5 118.40(4) . .
Os5 Os4 Os5 89.76(2) 2_676 .
Re5 Os4 Os5 89.76(2) 2_676 .
Os6 Os4 Os5 59.77(2) 2_676 .
Re6 Os4 Os5 59.77(2) 2_676 .
C4 Os4 Re5 135.1(4) . .
Se6 Os4 Re5 58.50(3) . .
Se8 Os4 Re5 58.50(3) . .
Se7 Os4 Re5 118.20(4) . .
Se5 Os4 Re5 118.40(4) . .
Os5 Os4 Re5 89.76(2) 2_676 .
Re5 Os4 Re5 89.76(2) 2_676 .
Os6 Os4 Re5 59.77(2) 2_676 .
Re6 Os4 Re5 59.77(2) 2_676 .
Os5 Os4 Re5 0.00(3) . .
C4 Os4 Os6 134.7(4) . .
Se6 Os4 Os6 118.43(4) . .
Se8 Os4 Os6 58.70(3) . .
Se7 Os4 Os6 118.42(3) . .
Se5 Os4 Os6 58.50(3) . .
Os5 Os4 Os6 59.84(2) 2_676 .
Re5 Os4 Os6 59.84(2) 2_676 .
Os6 Os4 Os6 89.89(2) 2_676 .
Re6 Os4 Os6 89.89(2) 2_676 .
Os5 Os4 Os6 59.94(2) . .
Re5 Os4 Os6 59.94(2) . .
C5 Os5 Se5 86.5(4) . 2_676
C5 Os5 Se6 91.8(4) . .
Se5 Os5 Se6 90.57(4) 2_676 .
C5 Os5 Se8 96.5(4) . .
Se5 Os5 Se8 176.92(5) 2_676 .
Se6 Os5 Se8 89.11(4) . .
C5 Os5 Se7 91.8(4) . 2_676
Se5 Os5 Se7 90.12(5) 2_676 2_676
Se6 Os5 Se7 176.36(5) . 2_676
Se8 Os5 Se7 90.01(5) . 2_676
C5 Os5 Os6 131.4(5) . 2_676
Se5 Os5 Os6 58.92(4) 2_676 2_676
Se6 Os5 Os6 58.81(3) . 2_676
Se8 Os5 Os6 118.45(4) . 2_676
Se7 Os5 Os6 118.74(3) 2_676 2_676
C5 Os5 Re6 131.4(5) . 2_676
Se5 Os5 Re6 58.92(4) 2_676 2_676
Se6 Os5 Re6 58.81(3) . 2_676
Se8 Os5 Re6 118.45(4) . 2_676
Se7 Os5 Re6 118.74(3) 2_676 2_676
Os6 Os5 Re6 0.00(3) 2_676 2_676
C5 Os5 Os4 131.3(4) . 2_676
Se5 Os5 Os4 58.86(3) 2_676 2_676
Se6 Os5 Os4 119.02(3) . 2_676
Se8 Os5 Os4 118.77(4) . 2_676
Se7 Os5 Os4 58.53(3) 2_676 2_676
Os6 Os5 Os4 60.23(2) 2_676 2_676
Re6 Os5 Os4 60.23(2) 2_676 2_676
C5 Os5 Re4 131.3(4) . 2_676
Se5 Os5 Re4 58.86(3) 2_676 2_676
Se6 Os5 Re4 119.02(3) . 2_676
Se8 Os5 Re4 118.77(4) . 2_676
Se7 Os5 Re4 58.53(3) 2_676 2_676
Os6 Os5 Re4 60.23(2) 2_676 2_676
Re6 Os5 Re4 60.23(2) 2_676 2_676
Os4 Os5 Re4 0.00(3) 2_676 2_676
C5 Os5 Re6 138.2(5) . .
Se5 Os5 Re6 118.94(3) 2_676 .
Se6 Os5 Re6 118.22(4) . .
Se8 Os5 Re6 58.70(3) . .
Se7 Os5 Re6 58.43(4) 2_676 .
Os6 Os5 Re6 90.14(2) 2_676 .
Re6 Os5 Re6 90.14(2) 2_676 .
Os4 Os5 Re6 60.08(2) 2_676 .
Re4 Os5 Re6 60.08(2) 2_676 .
C5 Os5 Os6 138.2(5) . .
Se5 Os5 Os6 118.94(3) 2_676 .
Se6 Os5 Os6 118.22(4) . .
Se8 Os5 Os6 58.70(3) . .
Se7 Os5 Os6 58.43(4) 2_676 .
Os6 Os5 Os6 90.14(2) 2_676 .
Re6 Os5 Os6 90.14(2) 2_676 .
Os4 Os5 Os6 60.08(2) 2_676 .
Re4 Os5 Os6 60.08(2) 2_676 .
Re6 Os5 Os6 0.00(3) . .
C5 Os5 Os4 138.2(4) . .
Se5 Os5 Os4 119.00(4) 2_676 .
Se6 Os5 Os4 58.18(3) . .
Se8 Os5 Os4 58.37(3) . .
Se7 Os5 Os4 118.46(4) 2_676 .
Os6 Os5 Os4 60.09(2) 2_676 .
Re6 Os5 Os4 60.09(2) 2_676 .
Os4 Os5 Os4 90.24(2) 2_676 .
Re4 Os5 Os4 90.24(2) 2_676 .
Re6 Os5 Os4 60.04(2) . .
Os6 Os5 Os4 60.04(2) . .
C6 Os6 Se7 92.9(4) . 2_676
C6 Os6 Se5 91.0(4) . .
Se7 Os6 Se5 176.08(5) 2_676 .
C6 Os6 Se6 92.4(3) . 2_676
Se7 Os6 Se6 89.74(4) 2_676 2_676
Se5 Os6 Se6 89.75(4) . 2_676
C6 Os6 Se8 91.9(3) . .
Se7 Os6 Se8 89.90(4) 2_676 .
Se5 Os6 Se8 90.32(4) . .
Se6 Os6 Se8 175.65(5) 2_676 .
C6 Os6 Os5 134.3(4) . 2_676
Se7 Os6 Os5 118.62(4) 2_676 2_676
Se5 Os6 Os5 57.98(3) . 2_676
Se6 Os6 Os5 58.41(3) 2_676 2_676
Se8 Os6 Os5 118.18(3) . 2_676
C6 Os6 Re5 134.3(4) . 2_676
Se7 Os6 Re5 118.62(4) 2_676 2_676
Se5 Os6 Re5 57.98(3) . 2_676
Se6 Os6 Re5 58.41(3) 2_676 2_676
Se8 Os6 Re5 118.18(3) . 2_676
Os5 Os6 Re5 0.00(3) 2_676 2_676
C6 Os6 Re5 135.8(4) . .
Se7 Os6 Re5 58.54(3) 2_676 .
Se5 Os6 Re5 118.46(4) . .
Se6 Os6 Re5 117.93(4) 2_676 .
Se8 Os6 Re5 58.39(3) . .
Os5 Os6 Re5 89.86(2) 2_676 .
Re5 Os6 Re5 89.86(2) 2_676 .
C6 Os6 Os5 135.8(4) . .
Se7 Os6 Os5 58.54(3) 2_676 .
Se5 Os6 Os5 118.46(4) . .
Se6 Os6 Os5 117.93(4) 2_676 .
Se8 Os6 Os5 58.39(3) . .
Os5 Os6 Os5 89.86(2) 2_676 .
Re5 Os6 Os5 89.86(2) 2_676 .
Re5 Os6 Os5 0.00(3) . .
C6 Os6 Re4 135.9(4) . 2_676
Se7 Os6 Re4 58.48(3) 2_676 2_676
Se5 Os6 Re4 118.12(4) . 2_676
Se6 Os6 Re4 58.08(3) 2_676 2_676
Se8 Os6 Re4 118.24(4) . 2_676
Os5 Os6 Re4 60.15(2) 2_676 2_676
Re5 Os6 Re4 60.15(2) 2_676 2_676
Re5 Os6 Re4 59.86(2) . 2_676
Os5 Os6 Re4 59.86(2) . 2_676
C6 Os6 Os4 135.9(4) . 2_676
Se7 Os6 Os4 58.48(3) 2_676 2_676
Se5 Os6 Os4 118.12(4) . 2_676
Se6 Os6 Os4 58.08(3) 2_676 2_676
Se8 Os6 Os4 118.24(4) . 2_676
Os5 Os6 Os4 60.15(2) 2_676 2_676
Re5 Os6 Os4 60.15(2) 2_676 2_676
Re5 Os6 Os4 59.86(2) . 2_676
Os5 Os6 Os4 59.86(2) . 2_676
Re4 Os6 Os4 0.00(3) 2_676 2_676
C6 Os6 Os4 134.0(4) . .
Se7 Os6 Os4 118.56(4) 2_676 .
Se5 Os6 Os4 58.47(3) . .
Se6 Os6 Os4 118.32(3) 2_676 .
Se8 Os6 Os4 58.27(3) . .
Os5 Os6 Os4 59.93(2) 2_676 .
Re5 Os6 Os4 59.93(2) 2_676 .
Re5 Os6 Os4 60.02(2) . .
Os5 Os6 Os4 60.02(2) . .
Re4 Os6 Os4 90.11(2) 2_676 .
Os4 Os6 Os4 90.11(2) 2_676 .
Os2 Se1 Re2 0.00(3) 2_765 2_765
Os2 Se1 Re3 63.16(3) 2_765 .
Re2 Se1 Re3 63.16(3) 2_765 .
Os2 Se1 Os3 63.16(3) 2_765 .
Re2 Se1 Os3 63.16(3) 2_765 .
Re3 Se1 Os3 0.00(3) . .
Os2 Se1 Re1 62.91(3) 2_765 .
Re2 Se1 Re1 62.91(3) 2_765 .
Re3 Se1 Re1 62.85(3) . .
Os3 Se1 Re1 62.85(3) . .
Os2 Se1 Os1 62.91(3) 2_765 .
Re2 Se1 Os1 62.91(3) 2_765 .
Re3 Se1 Os1 62.85(3) . .
Os3 Se1 Os1 62.85(3) . .
Re1 Se1 Os1 0.00(3) . .
Os2 Se2 Re2 0.00(3) 2_765 2_765
Os2 Se2 Os3 62.99(3) 2_765 2_765
Re2 Se2 Os3 62.99(3) 2_765 2_765
Os2 Se2 Re3 62.99(3) 2_765 2_765
Re2 Se2 Re3 62.99(3) 2_765 2_765
Os3 Se2 Re3 0.00(3) 2_765 2_765
Os2 Se2 Os1 62.96(3) 2_765 .
Re2 Se2 Os1 62.96(3) 2_765 .
Os3 Se2 Os1 62.87(3) 2_765 .
Re3 Se2 Os1 62.87(3) 2_765 .
Os2 Se2 Re1 62.96(3) 2_765 .
Re2 Se2 Re1 62.96(3) 2_765 .
Os3 Se2 Re1 62.87(3) 2_765 .
Re3 Se2 Re1 62.87(3) 2_765 .
Os1 Se2 Re1 0.00(3) . .
Os2 Se3 Re2 0.00(3) . .
Os2 Se3 Os3 63.25(3) . .
Re2 Se3 Os3 63.25(3) . .
Os2 Se3 Re3 63.25(3) . .
Re2 Se3 Re3 63.25(3) . .
Os3 Se3 Re3 0.00(3) . .
Os2 Se3 Os1 63.13(3) . .
Re2 Se3 Os1 63.13(3) . .
Os3 Se3 Os1 63.02(3) . .
Re3 Se3 Os1 63.02(3) . .
Os2 Se3 Re1 63.13(3) . .
Re2 Se3 Re1 63.13(3) . .
Os3 Se3 Re1 63.02(3) . .
Re3 Se3 Re1 63.02(3) . .
Os1 Se3 Re1 0.00(3) . .
Os2 Se4 Re2 0.00(3) . .
Os2 Se4 Os3 63.14(3) . 2_765
Re2 Se4 Os3 63.14(3) . 2_765
Os2 Se4 Re3 63.14(3) . 2_765
Re2 Se4 Re3 63.14(3) . 2_765
Os3 Se4 Re3 0.00(3) 2_765 2_765
Os2 Se4 Os1 62.95(3) . .
Re2 Se4 Os1 62.95(3) . .
Os3 Se4 Os1 62.87(3) 2_765 .
Re3 Se4 Os1 62.87(3) 2_765 .
Os2 Se4 Re1 62.95(3) . .
Re2 Se4 Re1 62.95(3) . .
Os3 Se4 Re1 62.87(3) 2_765 .
Re3 Se4 Re1 62.87(3) 2_765 .
Os1 Se4 Re1 0.00(3) . .
Os5 Se5 Re5 0.00(3) 2_676 2_676
Os5 Se5 Re4 63.18(4) 2_676 .
Re5 Se5 Re4 63.18(4) 2_676 .
Os5 Se5 Os4 63.18(4) 2_676 .
Re5 Se5 Os4 63.18(4) 2_676 .
Re4 Se5 Os4 0.00(3) . .
Os5 Se5 Os6 63.10(4) 2_676 .
Re5 Se5 Os6 63.10(4) 2_676 .
Re4 Se5 Os6 63.04(4) . .
Os4 Se5 Os6 63.04(4) . .
Os5 Se5 Re6 63.10(4) 2_676 .
Re5 Se5 Re6 63.10(4) 2_676 .
Re4 Se5 Re6 63.04(4) . .
Os4 Se5 Re6 63.04(4) . .
Os6 Se5 Re6 0.00(3) . .
Os4 Se6 Re4 0.00(3) . .
Os4 Se6 Os5 63.32(3) . .
Re4 Se6 Os5 63.32(3) . .
Os4 Se6 Re5 63.32(3) . .
Re4 Se6 Re5 63.32(3) . .
Os5 Se6 Re5 0.00(3) . .
Os4 Se6 Os6 63.13(3) . 2_676
Re4 Se6 Os6 63.13(3) . 2_676
Os5 Se6 Os6 62.78(3) . 2_676
Re5 Se6 Os6 62.78(3) . 2_676
Os4 Se6 Re6 63.13(3) . 2_676
Re4 Se6 Re6 63.13(3) . 2_676
Os5 Se6 Re6 62.78(3) . 2_676
Re5 Se6 Re6 62.78(3) . 2_676
Os6 Se6 Re6 0.00(3) 2_676 2_676
Os6 Se7 Re6 0.00(3) 2_676 2_676
Os6 Se7 Re4 63.08(3) 2_676 .
Re6 Se7 Re4 63.08(3) 2_676 .
Os6 Se7 Os4 63.08(3) 2_676 .
Re6 Se7 Os4 63.08(3) 2_676 .
Re4 Se7 Os4 0.00(3) . .
Os6 Se7 Re5 63.03(3) 2_676 2_676
Re6 Se7 Re5 63.03(3) 2_676 2_676
Re4 Se7 Re5 62.88(3) . 2_676
Os4 Se7 Re5 62.88(3) . 2_676
Os6 Se7 Os5 63.03(3) 2_676 2_676
Re6 Se7 Os5 63.03(3) 2_676 2_676
Re4 Se7 Os5 62.88(3) . 2_676
Os4 Se7 Os5 62.88(3) . 2_676
Re5 Se7 Os5 0.00(3) 2_676 2_676
Os4 Se8 Re4 0.00(3) . .
Os4 Se8 Os5 63.14(3) . .
Re4 Se8 Os5 63.14(3) . .
Os4 Se8 Re5 63.14(3) . .
Re4 Se8 Re5 63.14(3) . .
Os5 Se8 Re5 0.00(3) . .
Os4 Se8 Os6 63.03(3) . .
Re4 Se8 Os6 63.03(3) . .
Os5 Se8 Os6 62.91(3) . .
Re5 Se8 Os6 62.91(3) . .
Os4 Se8 Re6 63.03(3) . .
Re4 Se8 Re6 63.03(3) . .
Os5 Se8 Re6 62.91(3) . .
Re5 Se8 Re6 62.91(3) . .
Os6 Se8 Re6 0.00(3) . .
N1 C1 Re1 176.5(12) . .
N1 C1 Os1 176.5(12) . .
Re1 C1 Os1 0.00(4) . .
N2 C2 Re2 177.0(10) . .
N2 C2 Os2 177.0(10) . .
Re2 C2 Os2 0.00(4) . .
N3 C3 Re3 176.8(10) . .
N3 C3 Os3 176.8(10) . .
Re3 C3 Os3 0.00(4) . .
N4 C4 Re4 176.5(12) . .
N4 C4 Os4 176.5(12) . .
Re4 C4 Os4 0.00(4) . .
N5 C5 N5A 34.5(16) . .
N5 C5 Os5 163.3(21) . .
N5A C5 Os5 162.2(17) . .
N5 C5 Re5 163.3(21) . .
N5A C5 Re5 162.2(17) . .
Os5 C5 Re5 0.00(4) . .
N5A N5 C5 88.9(35) . .
N5 N5A C5 56.6(30) . .
N6 C6 Re6 176.3(12) . .
N6 C6 Os6 176.3(12) . .
Re6 C6 Os6 0.00(4) . .
C7 P1 C25 109.2(5) . .
C7 P1 C13 111.4(5) . .
C25 P1 C13 106.6(5) . .
C7 P1 C19 107.3(5) . .
C25 P1 C19 112.3(5) . .
C13 P1 C19 110.1(5) . .
C12 C7 C8 118.1(10) . .
C12 C7 P1 119.3(9) . .
C8 C7 P1 122.5(9) . .
C9 C8 C7 119.8(12) . .
C10 C9 C8 122.3(12) . .
C9 C10 C11 118.5(12) . .
C10 C11 C12 120.9(12) . .
C11 C12 C7 120.4(11) . .
C14 C13 C18 119.1(11) . .
C14 C13 P1 121.8(10) . .
C18 C13 P1 119.1(9) . .
C15 C14 C13 120.7(12) . .
C14 C15 C16 121.2(12) . .
C17 C16 C15 118.5(13) . .
C16 C17 C18 122.9(14) . .
C17 C18 C13 117.6(12) . .
C24 C19 C20 119.9(11) . .
C24 C19 P1 121.2(8) . .
C20 C19 P1 118.8(9) . .
C21 C20 C19 118.6(12) . .
C20 C21 C22 121.2(13) . .
C23 C22 C21 120.6(13) . .
C22 C23 C24 120.3(13) . .
C23 C24 C19 119.3(11) . .
C26 C25 C30 119.7(10) . .
C26 C25 P1 119.1(9) . .
C30 C25 P1 121.2(8) . .
C25 C26 C27 117.3(12) . .
C28 C27 C26 120.6(12) . .
C29 C28 C27 121.2(11) . .
C28 C29 C30 120.2(13) . .
C29 C30 C25 121.0(12) . .
C37 P2 C31 107.0(5) . .
C37 P2 C43 109.3(5) . .
C31 P2 C43 111.7(5) . .
C37 P2 C49 113.8(5) . .
C31 P2 C49 108.5(5) . .
C43 P2 C49 106.6(6) . .
C36 C31 C32 118.7(10) . .
C36 C31 P2 122.7(9) . .
C32 C31 P2 118.6(8) . .
C33 C32 C31 120.9(11) . .
C32 C33 C34 119.4(11) . .
C33 C34 C35 121.9(11) . .
C34 C35 C36 118.6(11) . .
C35 C36 C31 120.5(11) . .
C38 C37 C42 119.8(11) . .
C38 C37 P2 117.6(9) . .
C42 C37 P2 122.3(10) . .
C37 C38 C39 120.6(11) . .
C40 C39 C38 119.5(13) . .
C39 C40 C41 119.9(12) . .
C40 C41 C42 121.3(12) . .
C37 C42 C41 118.7(12) . .
C44 C43 C48 118.0(12) . .
C44 C43 P2 124.4(10) . .
C48 C43 P2 117.3(10) . .
C45 C44 C43 119.8(13) . .
C46 C45 C44 122.1(14) . .
C45 C46 C47 118.8(15) . .
C48 C47 C46 119.7(15) . .
C47 C48 C43 121.5(13) . .
C54 C49 C50 118.0(12) . .
C54 C49 P2 120.7(10) . .
C50 C49 P2 120.6(9) . .
C51 C50 C49 120.6(12) . .
C52 C51 C50 120.4(13) . .
C51 C52 C53 119.3(14) . .
C54 C53 C52 119.5(13) . .
C49 C54 C53 122.1(13) . .
C73 P3 C61 110.7(6) . .
C73 P3 C55 109.3(6) . .
C61 P3 C55 108.9(6) . .
C73 P3 C67 108.8(6) . .
C61 P3 C67 108.8(6) . .
C55 P3 C67 110.5(6) . .
C56 C55 C60 118.9(12) . .
C56 C55 P3 121.8(9) . .
C60 C55 P3 119.2(10) . .
C57 C56 C55 120.9(12) . .
C58 C57 C56 120.1(13) . .
C57 C58 C59 120.6(13) . .
C60 C59 C58 120.7(13) . .
C59 C60 C55 118.7(12) . .
C66 C61 C62 120.4(11) . .
C66 C61 P3 119.5(10) . .
C62 C61 P3 120.1(10) . .
C63 C62 C61 117.2(13) . .
C64 C63 C62 121.1(14) . .
C65 C64 C63 121.9(13) . .
C64 C65 C66 119.0(14) . .
C65 C66 C61 120.3(14) . .
C72 C67 C68 121.3(13) . .
C72 C67 P3 121.3(10) . .
C68 C67 P3 117.4(11) . .
C69 C68 C67 119.3(15) . .
C70 C69 C68 125.9(22) . .
C70 C69 C70A 15.1(20) . .
C68 C69 C70A 113.8(15) . .
C70A C70 C69 140.4(54) . .
C70A C70 C71 28.4(34) . .
C69 C70 C71 121.8(25) . .
C70 C70A C71 135.6(52) . .
C70 C70A C69 24.5(35) . .
C71 C70A C69 120.5(24) . .
C70A C71 C72 123.3(23) . .
C70A C71 C70 16.0(19) . .
C72 C71 C70 109.9(17) . .
C67 C72 C71 120.9(16) . .
C78 C73 C74 119.2(13) . .
C78 C73 P3 119.6(11) . .
C74 C73 P3 121.0(10) . .
C73 C74 C75 120.5(13) . .
C76 C75 C74 119.3(15) . .
C75 C76 C77 121.1(16) . .
C76 C77 C78 119.0(15) . .
C73 C78 C77 120.8(15) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Re1 C1 2.096(11) .
Re1 Se3 2.5144(13) .
Re1 Se2 2.5172(12) .
Re1 Se4 2.5192(13) .
Re1 Se1 2.5242(13) .
Re1 Os3 2.6251(6) 2_765
Re1 Re3 2.6251(6) 2_765
Re1 Re3 2.6260(7) .
Re1 Os3 2.6260(7) .
Re1 Os2 2.6267(6) .
Re1 Re2 2.6267(6) .
Re1 Re2 2.6280(6) 2_765
Re2 C2 2.101(13) .
Re2 Se3 2.5035(12) .
Re2 Se4 2.5116(13) .
Re2 Se1 2.5121(12) 2_765
Re2 Se2 2.5155(13) 2_765
Re2 Os1 2.6267(6) .
Re2 Os1 2.6280(6) 2_765
Re2 Re1 2.6280(6) 2_765
Re2 Re3 2.6289(7) .
Re2 Os3 2.6289(7) .
Re2 Re3 2.6310(6) 2_765
Re3 C3 2.091(13) .
Re3 Se3 2.5101(11) .
Re3 Se1 2.5122(13) .
Re3 Se4 2.5142(11) 2_765
Re3 Se2 2.5163(13) 2_765
Re3 Os1 2.6252(6) 2_765
Re3 Re1 2.6252(6) 2_765
Re3 Os1 2.6260(7) .
Re3 Os2 2.6289(7) .
Re3 Os2 2.6310(6) 2_765
Re4 C4 2.110(13) .
Re4 Se6 2.4997(14) .
Re4 Se8 2.5086(12) .
Re4 Se7 2.5118(12) .
Re4 Se5 2.5138(15) .
Re4 Os5 2.6210(6) 2_676
Re4 Re5 2.6210(6) 2_676
Re4 Os6 2.6270(7) 2_676
Re4 Re6 2.6270(7) 2_676
Re4 Os5 2.6284(7) .
Re4 Re5 2.6284(7) .
Re4 Os6 2.6288(7) .
Re5 C5 2.077(13) .
Re5 Se5 2.4897(14) 2_676
Re5 Se6 2.5081(13) .
Re5 Se8 2.5122(14) .
Re5 Se7 2.5136(13) 2_676
Re5 Os6 2.6186(6) 2_676
Re5 Re6 2.6186(6) 2_676
Re5 Os4 2.6210(6) 2_676
Re5 Re4 2.6210(6) 2_676
Re5 Re6 2.6261(7) .
Re5 Os6 2.6261(7) .
Re5 Os4 2.6284(7) .
Re6 C6 2.068(12) .
Re6 Se7 2.5105(14) 2_676
Re6 Se5 2.5147(15) .
Re6 Se6 2.5188(11) 2_676
Re6 Se8 2.5203(12) .
Re6 Os5 2.6185(6) 2_676
Re6 Re5 2.6185(6) 2_676
Re6 Os5 2.6261(7) .
Re6 Re4 2.6270(7) 2_676
Re6 Os4 2.6270(7) 2_676
Re6 Os4 2.6288(7) .
Os1 C1 2.096(11) .
Os1 Se3 2.5144(13) .
Os1 Se2 2.5172(12) .
Os1 Se4 2.5192(13) .
Os1 Se1 2.5242(13) .
Os1 Os3 2.6251(6) 2_765
Os1 Re3 2.6251(6) 2_765
Os1 Os3 2.6260(7) .
Os1 Os2 2.6267(6) .
Os1 Re2 2.6280(6) 2_765
Os2 C2 2.101(13) .
Os2 Se3 2.5035(12) .
Os2 Se4 2.5116(13) .
Os2 Se1 2.5121(12) 2_765
Os2 Se2 2.5155(13) 2_765
Os2 Os1 2.6280(6) 2_765
Os2 Re1 2.6280(6) 2_765
Os2 Os3 2.6289(7) .
Os2 Re3 2.6310(6) 2_765
Os3 C3 2.091(13) .
Os3 Se3 2.5101(11) .
Os3 Se1 2.5122(13) .
Os3 Se4 2.5142(11) 2_765
Os3 Se2 2.5163(13) 2_765
Os3 Os1 2.6252(6) 2_765
Os3 Re1 2.6252(6) 2_765
Os3 Os2 2.6310(6) 2_765
Os4 C4 2.110(13) .
Os4 Se6 2.4997(14) .
Os4 Se8 2.5086(12) .
Os4 Se7 2.5118(12) .
Os4 Se5 2.5138(15) .
Os4 Os5 2.6210(6) 2_676
Os4 Re5 2.6210(6) 2_676
Os4 Os6 2.6270(7) 2_676
Os4 Re6 2.6270(7) 2_676
Os4 Os5 2.6284(7) .
Os4 Os6 2.6288(7) .
Os5 C5 2.077(13) .
Os5 Se5 2.4897(14) 2_676
Os5 Se6 2.5081(13) .
Os5 Se8 2.5122(14) .
Os5 Se7 2.5136(13) 2_676
Os5 Os6 2.6186(6) 2_676
Os5 Re6 2.6186(6) 2_676
Os5 Os4 2.6210(6) 2_676
Os5 Re4 2.6210(6) 2_676
Os5 Os6 2.6261(7) .
Os6 C6 2.068(12) .
Os6 Se7 2.5105(14) 2_676
Os6 Se5 2.5147(15) .
Os6 Se6 2.5188(11) 2_676
Os6 Se8 2.5203(12) .
Os6 Os5 2.6185(6) 2_676
Os6 Re5 2.6185(6) 2_676
Os6 Re4 2.6270(7) 2_676
Os6 Os4 2.6270(7) 2_676
Se1 Os2 2.5120(12) 2_765
Se1 Re2 2.5120(12) 2_765
Se2 Os2 2.5155(13) 2_765
Se2 Re2 2.5155(13) 2_765
Se2 Os3 2.5163(13) 2_765
Se2 Re3 2.5163(13) 2_765
Se4 Os3 2.5142(11) 2_765
Se4 Re3 2.5142(11) 2_765
Se5 Os5 2.4897(14) 2_676
Se5 Re5 2.4897(14) 2_676
Se6 Os6 2.5189(11) 2_676
Se6 Re6 2.5189(11) 2_676
Se7 Os6 2.5105(14) 2_676
Se7 Re6 2.5105(14) 2_676
Se7 Re5 2.5135(13) 2_676
Se7 Os5 2.5135(13) 2_676
C1 N1 1.148(13) .
C2 N2 1.152(14) .
C3 N3 1.145(14) .
C4 N4 1.142(14) .
C5 N5 1.06(3) .
C5 N5A 1.27(3) .
N5 N5A 0.72(3) .
C6 N6 1.157(15) .
P1 C7 1.782(11) .
P1 C25 1.789(10) .
P1 C13 1.799(12) .
P1 C19 1.799(12) .
C7 C12 1.384(15) .
C7 C8 1.386(15) .
C8 C9 1.360(15) .
C9 C10 1.35(2) .
C10 C11 1.37(2) .
C11 C12 1.369(15) .
C13 C14 1.378(15) .
C13 C18 1.41(2) .
C14 C15 1.36(2) .
C15 C16 1.38(2) .
C16 C17 1.35(2) .
C17 C18 1.38(2) .
C19 C24 1.379(15) .
C19 C20 1.406(14) .
C20 C21 1.36(2) .
C21 C22 1.36(2) .
C22 C23 1.35(2) .
C23 C24 1.38(2) .
C25 C26 1.386(15) .
C25 C30 1.40(2) .
C26 C27 1.43(2) .
C27 C28 1.36(2) .
C28 C29 1.34(2) .
C29 C30 1.37(2) .
P2 C37 1.783(11) .
P2 C31 1.787(11) .
P2 C43 1.791(12) .
P2 C49 1.791(13) .
C31 C36 1.397(15) .
C31 C32 1.401(14) .
C32 C33 1.370(15) .
C33 C34 1.37(2) .
C34 C35 1.39(2) .
C35 C36 1.390(15) .
C37 C38 1.39(2) .
C37 C42 1.40(2) .
C38 C39 1.41(2) .
C39 C40 1.38(2) .
C40 C41 1.39(2) .
C41 C42 1.41(2) .
C43 C44 1.37(2) .
C43 C48 1.40(2) .
C44 C45 1.36(2) .
C45 C46 1.36(2) .
C46 C47 1.38(2) .
C47 C48 1.35(2) .
C49 C54 1.37(2) .
C49 C50 1.39(2) .
C50 C51 1.39(2) .
C51 C52 1.36(2) .
C52 C53 1.40(2) .
C53 C54 1.37(2) .
P3 C73 1.787(13) .
P3 C61 1.797(11) .
P3 C55 1.800(13) .
P3 C67 1.815(13) .
C55 C56 1.38(2) .
C55 C60 1.40(2) .
C56 C57 1.36(2) .
C57 C58 1.35(2) .
C58 C59 1.37(2) .
C59 C60 1.37(2) .
C61 C66 1.40(2) .
C61 C62 1.41(2) .
C62 C63 1.40(2) .
C63 C64 1.37(2) .
C64 C65 1.36(2) .
C65 C66 1.39(2) .
C67 C72 1.40(2) .
C67 C68 1.41(2) .
C68 C69 1.41(2) .
C69 C70 1.08(3) .
C69 C70A 1.67(3) .
C70 C70A 0.68(3) .
C70 C71 1.73(3) .
C70A C71 1.18(3) .
C71 C72 1.41(2) .
C73 C78 1.36(2) .
C73 C74 1.37(2) .
C74 C75 1.41(2) .
C75 C76 1.35(2) .
C76 C77 1.37(2) .
C77 C78 1.40(2) .
