#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/11/54/4115431.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4115431
loop_
_publ_author_name
'Yong-Shou Lin'
'Hanae Misawa'
'Jun Yamada'
'Kazuko Matsumoto'
_publ_section_title
;
 Synthesis of Ketonylplatinum(III) Dinuclear Complexes: Observation of the
 Competitive Radical vs Electrophilic Displacement in Pt(III)-Promoted C-H
 Bond Activation of Ketones
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              569
_journal_page_last               575
_journal_paper_doi               10.1021/ja9943041
_journal_volume                  123
_journal_year                    2001
_chemical_formula_sum            'C26 H47 N9 O13 Pt2'
_chemical_formula_weight         1083.89
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_Int_Tables_number      14
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_cell_angle_alpha                90
_cell_angle_beta                 90.86(2)
_cell_angle_gamma                90
_cell_formula_units_Z            4
_cell_length_a                   10.133(2)
_cell_length_b                   9.684(2)
_cell_length_c                   38.10(1)
_cell_measurement_reflns_used    21
_cell_measurement_temperature    298.2
_cell_measurement_theta_max      12.3
_cell_measurement_theta_min      10.1
_cell_volume                     3738.3(15)
_computing_cell_refinement       'MSC/AFC Diffractometer Control'
_computing_data_collection       'MSC/AFC Diffractometer Control'
_computing_data_reduction        'teXsan Ver. 1.10'
_computing_publication_material  'teXsan Ver. 1.10'
_computing_structure_refinement  'teXsan Ver. 1.10'
_computing_structure_solution    'DIRDIF94 (PATTY)'
_diffrn_measurement_device_type  'Rigaku AFC7R'
_diffrn_measurement_method       ω
_diffrn_radiation_type           'Mo K\a'
_diffrn_radiation_wavelength     0.7107
_diffrn_reflns_av_R_equivalents  0.067
_diffrn_reflns_number            7564
_diffrn_standards_decay_%        14.44
_diffrn_standards_interval_count 150
_diffrn_standards_number         3
_exptl_absorpt_coefficient_mu    7.517
_exptl_absorpt_correction_T_max  0.222
_exptl_absorpt_correction_T_min  0.118
_exptl_absorpt_correction_type   refdelf
_exptl_absorpt_process_details   '(Walker & Stuart, 1983)'
_exptl_crystal_colour            yellow
_exptl_crystal_density_diffrn    1.926
_exptl_crystal_description       prismatic
_exptl_crystal_size_max          0.300
_exptl_crystal_size_mid          0.200
_exptl_crystal_size_min          0.200
_refine_diff_density_max         1.39
_refine_diff_density_min         -1.75
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.554
_refine_ls_number_parameters     451
_refine_ls_number_reflns         3390
_refine_ls_R_factor_gt           0.0683
_refine_ls_shift/su_max          0.0360
_refine_ls_structure_factor_coef F
_refine_ls_weighting_details     'w = 1/[σ²(Fo) + 0.00040|Fo|²]'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_ref         0.0723
_reflns_number_gt                3390
_reflns_number_total             0
_reflns_threshold_expression     F²>2.0σ(F²)
_cod_data_source_file            ja9943041_1.cif
_cod_data_source_block           C26H47N9O13Pt2
_cod_original_cell_volume        3738(1)
_cod_original_formula_sum        'C26 H47 N9 O13 Pt2 '
_cod_database_code               4115431
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,1/2+y,1/2-z
-x,-y,-z
x,1/2-y,1/2+z
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_calc_flag
Pt(1) Pt 0.38914(10) 0.2944(1) 0.07551(3) 0.0433(3) Uani 1.00 d
Pt(2) Pt 0.18042(10) 0.1515(1) 0.05161(3) 0.0422(3) Uani 1.00 d
O(1) O 0.662(2) 0.264(3) 0.1301(5) 0.103(9) Uani 1.00 d
O(2) O 0.257(2) 0.436(2) 0.0900(5) 0.064(6) Uani 1.00 d
O(3) O 0.366(2) 0.189(2) 0.1202(4) 0.063(6) Uani 1.00 d
O(4) O 0.895(3) 0.083(4) 0.0882(7) 0.18(1) Uani 1.00 d
O(5) O 0.980(2) -0.001(2) 0.0426(5) 0.066(6) Uani 1.00 d
O(6) O 0.778(2) -0.035(2) 0.0520(6) 0.097(8) Uani 1.00 d
O(7) O 0.858(2) 0.254(3) 0.0128(7) 0.13(1) Uani 1.00 d
O(8) O 0.673(2) 0.341(2) 0.0085(6) 0.099(9) Uani 1.00 d
O(9) O 0.833(2) 0.452(2) -0.0070(7) 0.11(1) Uani 1.00 d
O(10) O 0.461(2) 0.140(2) 0.9807(5) 0.058(6) Uani 1.00 d
O(11) O 0.406(2) 0.320(2) 0.9550(6) 0.091(9) Uani 1.00 d
O(12) O 0.523(2) 0.167(2) 0.9294(5) 0.092(8) Uani 1.00 d
O(13) O 0.104(4) -0.150(4) 0.773(1) 0.21(2) Uani 1.00 d
N(1) N 0.080(2) 0.312(2) 0.0725(6) 0.065(8) Uani 1.00 d
N(2) N 0.195(2) 0.062(2) 0.0981(5) 0.050(6) Uani 1.00 d
N(3) N 0.419(2) 0.415(2) 0.0325(5) 0.058(7) Uani 1.00 d
N(4) N 0.536(2) 0.158(2) 0.0624(5) 0.058(7) Uani 1.00 d
N(5) N 0.148(2) 0.236(2) 0.0031(5) 0.048(6) Uani 1.00 d
N(6) N 0.263(2) -0.018(2) 0.0266(6) 0.054(7) Uani 1.00 d
N(7) N 0.883(3) 0.013(2) 0.0614(7) 0.068(9) Uani 1.00 d
N(8) N 0.789(3) 0.349(3) 0.0066(7) 0.073(9) Uani 1.00 d
N(9) N 0.459(2) 0.210(3) 0.9555(7) 0.065(9) Uani 1.00 d
C(1) C 0.541(3) 0.426(3) 0.0968(7) 0.08(1) Uani 1.00 d
C(2) C 0.582(4) 0.364(3) 0.1309(10) 0.10(1) Uani 1.00 d
C(3) C 0.542(4) 0.404(4) 0.1672(9) 0.09(1) Uani 1.00 d
C(4) C 0.614(5) 0.341(4) 0.1952(9) 0.13(2) Uani 1.00 d
C(5) C 0.567(5) 0.383(5) 0.228(1) 0.13(2) Uani 1.00 d
C(6) C 0.469(6) 0.487(6) 0.233(1) 0.17(3) Uani 1.00 d
C(7) C 0.395(5) 0.546(5) 0.205(1) 0.14(2) Uani 1.00 d
C(8) C 0.446(4) 0.509(4) 0.1695(10) 0.10(1) Uani 1.00 d
C(9) C 0.125(2) 0.416(3) 0.0878(6) 0.038(7) Uani 1.00 d
C(10) C 0.042(3) 0.533(3) 0.1013(7) 0.063(10) Uani 1.00 d
C(11) C 0.091(4) 0.678(3) 0.0884(9) 0.09(1) Uani 1.00 d
C(12) C 0.059(4) 0.531(3) 0.1409(8) 0.11(1) Uani 1.00 d
C(13) C -0.098(3) 0.521(4) 0.086(1) 0.12(1) Uani 1.00 d
C(14) C 0.279(3) 0.101(3) 0.1244(7) 0.056(9) Uani 1.00 d
C(15) C 0.273(3) 0.031(4) 0.1610(8) 0.09(1) Uani 1.00 d
C(16) C 0.413(3) -0.024(6) 0.168(1) 0.18(2) Uani 1.00 d
C(17) C 0.261(4) 0.142(4) 0.1869(7) 0.11(1) Uani 1.00 d
C(18) C 0.169(4) -0.076(4) 0.1630(8) 0.12(2) Uani 1.00 d
C(19) C 0.033(8) 0.027(8) 0.736(1) 0.30(4) Uani 1.00 d
C(20) C 0.115(6) -0.023(5) 0.770(2) 0.17(3) Uani 1.00 d
C(21) C 0.168(4) 0.060(5) 0.798(2) 0.17(3) Uani 1.00 d
C(22) C 0.210(6) 0.02(1) 0.833(2) 0.26(4) Uani 1.00 d
C(23) C 0.271(6) 0.129(8) 0.851(2) 0.20(4) Uani 1.00 d
C(24) C 0.276(7) 0.247(7) 0.842(2) 0.25(4) Uani 1.00 d
C(25) C 0.265(5) 0.303(6) 0.809(1) 0.17(3) Uani 1.00 d
C(26) C 0.191(5) 0.192(7) 0.788(1) 0.14(2) Uani 1.00 d
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.003 0.002
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.1)
;
H H 0.000 0.000
;International Tables for Crystallography
(1992, Vol. C, Table 6.1.1.2)
;
O O 0.011 0.006
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.1)
;
N N 0.006 0.003
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.1)
;
Pt Pt -1.703 8.390
;International Tables for Crystallography
(1992, Vol. C, Tables 4.2.6.8 and 6.1.1.1)
;
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_2
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
Pt(2) Pt(1) O(2) 85.4(4) 1_555 1_555 yes
Pt(2) Pt(1) O(3) 85.7(5) 1_555 1_555 yes
Pt(2) Pt(1) N(3) 98.5(5) 1_555 1_555 yes
Pt(2) Pt(1) N(4) 98.8(5) 1_555 1_555 yes
Pt(2) Pt(1) C(1) 173.6(9) 1_555 1_555 yes
O(2) Pt(1) O(3) 91.6(7) 1_555 1_555 yes
O(2) Pt(1) N(3) 86.3(8) 1_555 1_555 yes
O(2) Pt(1) N(4) 175.7(7) 1_555 1_555 yes
O(2) Pt(1) C(1) 88(1) 1_555 1_555 yes
O(3) Pt(1) N(3) 175.1(8) 1_555 1_555 yes
O(3) Pt(1) N(4) 88.4(8) 1_555 1_555 yes
O(3) Pt(1) C(1) 94.2(9) 1_555 1_555 yes
N(3) Pt(1) N(4) 93.4(8) 1_555 1_555 yes
N(3) Pt(1) C(1) 81.3(9) 1_555 1_555 yes
N(4) Pt(1) C(1) 87(1) 1_555 1_555 yes
Pt(1) Pt(2) N(1) 82.3(6) 1_555 1_555 yes
Pt(1) Pt(2) N(2) 82.6(5) 1_555 1_555 yes
Pt(1) Pt(2) N(5) 102.5(5) 1_555 1_555 yes
Pt(1) Pt(2) N(6) 104.1(5) 1_555 1_555 yes
N(1) Pt(2) N(2) 90.9(8) 1_555 1_555 yes
N(1) Pt(2) N(5) 88.3(8) 1_555 1_555 yes
N(1) Pt(2) N(6) 173.2(8) 1_555 1_555 yes
N(2) Pt(2) N(5) 174.7(7) 1_555 1_555 yes
N(2) Pt(2) N(6) 92.3(8) 1_555 1_555 yes
N(5) Pt(2) N(6) 87.9(8) 1_555 1_555 yes
Pt(1) O(2) C(9) 123(1) 1_555 1_555 yes
Pt(1) O(3) C(14) 123(1) 1_555 1_555 yes
Pt(2) N(1) C(9) 128(1) 1_555 1_555 yes
Pt(2) N(2) C(14) 125(1) 1_555 1_555 yes
O(4) N(7) O(5) 118(2) 1_555 1_555 yes
O(4) N(7) O(6) 121(2) 1_555 1_555 yes
O(5) N(7) O(6) 119(2) 1_555 1_555 yes
O(7) N(8) O(8) 122(3) 1_555 1_555 yes
O(7) N(8) O(9) 120(3) 1_555 1_555 yes
O(8) N(8) O(9) 117(2) 1_555 1_555 yes
O(10) N(9) O(11) 122(2) 1_555 1_555 yes
O(10) N(9) O(12) 116(2) 1_555 1_555 yes
O(11) N(9) O(12) 121(2) 1_555 1_555 yes
Pt(1) C(1) C(2) 106(2) 1_555 1_555 yes
O(1) C(2) C(1) 117(3) 1_555 1_555 yes
O(1) C(2) C(3) 113(3) 1_555 1_555 yes
C(1) C(2) C(3) 129(3) 1_555 1_555 yes
C(2) C(3) C(4) 116(3) 1_555 1_555 yes
C(2) C(3) C(8) 115(3) 1_555 1_555 yes
C(4) C(3) C(8) 127(3) 1_555 1_555 yes
C(3) C(4) C(5) 111(4) 1_555 1_555 yes
C(4) C(5) C(6) 124(4) 1_555 1_555 yes
C(5) C(6) C(7) 123(4) 1_555 1_555 yes
C(6) C(7) C(8) 113(4) 1_555 1_555 yes
C(3) C(8) C(7) 118(3) 1_555 1_555 yes
O(2) C(9) N(1) 120(2) 1_555 1_555 yes
O(2) C(9) C(10) 114(2) 1_555 1_555 yes
N(1) C(9) C(10) 124(2) 1_555 1_555 yes
C(9) C(10) C(11) 112(2) 1_555 1_555 yes
C(9) C(10) C(12) 105(2) 1_555 1_555 yes
C(9) C(10) C(13) 109(2) 1_555 1_555 yes
C(11) C(10) C(12) 107(2) 1_555 1_555 yes
C(11) C(10) C(13) 104(2) 1_555 1_555 yes
C(12) C(10) C(13) 117(2) 1_555 1_555 yes
O(3) C(14) N(2) 122(2) 1_555 1_555 yes
O(3) C(14) C(15) 116(2) 1_555 1_555 yes
N(2) C(14) C(15) 120(2) 1_555 1_555 yes
C(14) C(15) C(16) 105(2) 1_555 1_555 yes
C(14) C(15) C(17) 106(2) 1_555 1_555 yes
C(14) C(15) C(18) 112(2) 1_555 1_555 yes
C(16) C(15) C(17) 102(3) 1_555 1_555 yes
C(16) C(15) C(18) 113(3) 1_555 1_555 yes
C(17) C(15) C(18) 114(3) 1_555 1_555 yes
O(13) C(20) C(19) 110(5) 1_555 1_555 yes
O(13) C(20) C(21) 119(6) 1_555 1_555 yes
C(19) C(20) C(21) 128(5) 1_555 1_555 yes
C(20) C(21) C(22) 128(7) 1_555 1_555 yes
C(20) C(21) C(26) 111(7) 1_555 1_555 yes
C(22) C(21) C(26) 118(5) 1_555 1_555 yes
C(21) C(22) C(23) 110(6) 1_555 1_555 yes
C(22) C(23) C(24) 127(9) 1_555 1_555 yes
C(23) C(24) C(25) 129(9) 1_555 1_555 yes
C(24) C(25) C(26) 103(5) 1_555 1_555 yes
C(21) C(26) C(25) 126(5) 1_555 1_555 yes
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_publ_flag
Pt(1) Pt(2) 2.676(1) yes
Pt(1) O(2) 2.00(2) yes
Pt(1) O(3) 2.00(2) yes
Pt(1) N(3) 2.04(2) yes
Pt(1) N(4) 2.06(2) yes
Pt(1) C(1) 2.15(2) yes
Pt(2) N(1) 2.03(2) yes
Pt(2) N(2) 1.98(2) yes
Pt(2) N(5) 2.04(2) yes
Pt(2) N(6) 2.08(2) yes
O(1) C(2) 1.27(3) yes
O(2) C(9) 1.35(2) yes
O(3) C(14) 1.24(3) yes
O(4) N(7) 1.23(3) yes
O(5) N(7) 1.23(3) yes
O(6) N(7) 1.22(3) yes
O(7) N(8) 1.18(3) yes
O(8) N(8) 1.17(3) yes
O(9) N(8) 1.22(3) yes
O(10) N(9) 1.18(3) yes
O(11) N(9) 1.20(3) yes
O(12) N(9) 1.26(3) yes
O(13) C(20) 1.24(4) yes
N(1) C(9) 1.24(3) yes
N(2) C(14) 1.35(3) yes
C(1) C(2) 1.48(4) yes
C(2) C(3) 1.49(4) yes
C(3) C(4) 1.41(5) yes
C(3) C(8) 1.41(5) yes
C(4) C(5) 1.40(6) yes
C(5) C(6) 1.43(6) yes
C(6) C(7) 1.40(6) yes
C(7) C(8) 1.51(5) yes
C(9) C(10) 1.51(3) yes
C(10) C(11) 1.57(4) yes
C(10) C(12) 1.51(4) yes
C(10) C(13) 1.53(4) yes
C(14) C(15) 1.55(4) yes
C(15) C(16) 1.54(4) yes
C(15) C(17) 1.47(4) yes
C(15) C(18) 1.48(4) yes
C(19) C(20) 1.59(8) yes
C(20) C(21) 1.45(7) yes
C(21) C(22) 1.43(8) yes
C(21) C(26) 1.36(6) yes
C(22) C(23) 1.4(1) yes
C(23) C(24) 1.19(8) yes
C(24) C(25) 1.38(8) yes
C(25) C(26) 1.53(7) yes
loop_
_geom_contact_atom_site_label_1
_geom_contact_atom_site_label_2
_geom_contact_distance
_geom_contact_site_symmetry_2
Pt(1) Pt(2) 2.676(1) .
Pt(2) O(5) 2.53(2) 1_455
Pt(2) O(4) 3.30(2) 1_455
Pt(2) N(7) 3.32(3) 1_455
O(1) C(22) 3.33(7) 3_656
O(1) O(4) 3.36(4) .
O(2) O(9) 3.45(3) 3_665
O(4) N(1) 2.97(4) 1_655
O(4) N(2) 3.07(3) 1_655
O(4) O(7) 3.33(4) .
O(4) C(22) 3.36(5) 3_656
O(4) C(23) 3.54(9) 3_656
O(5) N(6) 2.94(2) 1_655
O(5) O(7) 2.98(3) .
O(5) N(2) 3.08(2) 1_655
O(5) N(5) 3.14(2) 3_655
O(5) N(5) 3.24(3) 1_655
O(5) O(5) 3.28(4) 3_755
O(5) N(1) 3.39(3) 1_655
O(5) N(6) 3.59(3) 3_655
O(6) O(10) 2.89(3) 3_656
O(6) N(9) 2.95(3) 3_656
O(6) N(5) 2.97(3) 3_655
O(6) N(6) 3.06(3) 3_655
O(6) N(4) 3.11(3) .
O(6) O(7) 3.28(3) .
O(6) O(11) 3.34(3) 3_656
O(6) O(12) 3.38(3) 3_656
O(7) N(5) 2.97(3) 1_655
O(7) N(7) 2.99(3) .
O(7) N(6) 2.99(3) 3_655
O(7) N(1) 3.22(3) 1_655
O(8) N(3) 2.85(3) .
O(8) N(3) 2.98(3) 3_665
O(8) N(4) 3.06(3) .
O(8) O(10) 3.08(3) 1_554
O(8) N(9) 3.20(3) 1_554
O(8) O(11) 3.37(3) 1_554
O(8) N(6) 3.47(3) 3_655
O(9) N(3) 3.00(3) 3_665
O(9) N(5) 3.03(3) 3_665
O(9) C(9) 3.37(3) 3_665
O(9) C(11) 3.44(4) 3_665
O(9) N(1) 3.50(3) 3_665
O(9) O(9) 3.54(5) 3_765
O(10) N(6) 3.06(2) 3_656
O(10) N(6) 3.08(3) 1_556
O(10) O(10) 3.17(4) 3_657
O(10) N(4) 3.19(3) 1_556
O(10) N(4) 3.31(3) 3_656
O(10) N(3) 3.35(3) 1_556
O(10) N(5) 3.43(3) 1_556
O(11) N(3) 3.10(3) 1_556
O(11) N(3) 3.15(3) 3_666
O(11) C(1) 3.20(3) 3_666
O(11) N(5) 3.32(3) 1_556
O(12) N(6) 3.08(3) 3_656
O(12) N(4) 3.21(3) 3_656
O(13) C(19) 3.43(9) 2_546
O(13) C(4) 3.60(6) 3_656
N(1) N(7) 3.54(4) 1_455
N(2) N(7) 3.47(3) 1_455
N(3) N(3) 3.42(4) 3_665
N(3) N(8) 3.43(3) 3_665
N(3) N(9) 3.58(3) 1_554
N(5) N(7) 3.46(3) 3_655
N(6) N(9) 3.44(3) 3_656
N(6) N(8) 3.48(3) 3_655
C(3) C(25) 3.55(7) 3_666
C(8) C(25) 3.52(7) 3_666
C(16) C(23) 3.45(8) 3_656
loop_
_geom_torsion_atom_site_label_1
_geom_torsion_atom_site_label_2
_geom_torsion_atom_site_label_3
_geom_torsion_atom_site_label_4
_geom_torsion
_geom_torsion_site_symmetry_1
_geom_torsion_site_symmetry_2
_geom_torsion_site_symmetry_3
_geom_torsion_site_symmetry_4
_geom_torsion_publ_flag
Pt(1) Pt(2) N(1) C(9) 0(2) 1_555 1_555 1_555 1_555 yes
Pt(1) Pt(2) N(2) C(14) 6(1) 1_555 1_555 1_555 1_555 yes
Pt(1) O(2) C(9) N(1) -8(3) 1_555 1_555 1_555 1_555 yes
Pt(1) O(2) C(9) C(10) 177(1) 1_555 1_555 1_555 1_555 yes
Pt(1) O(3) C(14) N(2) 3(3) 1_555 1_555 1_555 1_555 yes
Pt(1) O(3) C(14) C(15) -178(2) 1_555 1_555 1_555 1_555 yes
Pt(1) C(1) C(2) O(1) 80(3) 1_555 1_555 1_555 1_555 yes
Pt(1) C(1) C(2) C(3) -99(3) 1_555 1_555 1_555 1_555 yes
Pt(2) Pt(1) O(2) C(9) 6(1) 1_555 1_555 1_555 1_555 yes
Pt(2) Pt(1) O(3) C(14) 0(1) 1_555 1_555 1_555 1_555 yes
Pt(2) Pt(1) C(1) C(2) 100(6) 1_555 1_555 1_555 1_555 yes
Pt(2) N(1) C(9) O(2) 4(3) 1_555 1_555 1_555 1_555 yes
Pt(2) N(1) C(9) C(10) 177(1) 1_555 1_555 1_555 1_555 yes
Pt(2) N(2) C(14) O(3) -8(3) 1_555 1_555 1_555 1_555 yes
Pt(2) N(2) C(14) C(15) 174(2) 1_555 1_555 1_555 1_555 yes
O(1) C(2) C(3) C(4) 9(5) 1_555 1_555 1_555 1_555 yes
O(1) C(2) C(3) C(8) -176(3) 1_555 1_555 1_555 1_555 yes
O(2) Pt(1) Pt(2) N(1) -3.0(8) 1_555 1_555 1_555 1_555 yes
O(2) Pt(1) Pt(2) N(2) -94.9(8) 1_555 1_555 1_555 1_555 yes
O(2) Pt(1) Pt(2) N(5) 83.6(8) 1_555 1_555 1_555 1_555 yes
O(2) Pt(1) Pt(2) N(6) 174.5(8) 1_555 1_555 1_555 1_555 yes
O(2) Pt(1) O(3) C(14) 85(2) 1_555 1_555 1_555 1_555 yes
O(2) Pt(1) C(1) C(2) 103(2) 1_555 1_555 1_555 1_555 yes
O(2) C(9) C(10) C(11) 45(3) 1_555 1_555 1_555 1_555 yes
O(2) C(9) C(10) C(12) -72(2) 1_555 1_555 1_555 1_555 yes
O(2) C(9) C(10) C(13) 160(2) 1_555 1_555 1_555 1_555 yes
O(3) Pt(1) Pt(2) N(1) 89.0(8) 1_555 1_555 1_555 1_555 yes
O(3) Pt(1) Pt(2) N(2) -3.0(8) 1_555 1_555 1_555 1_555 yes
O(3) Pt(1) Pt(2) N(5) 175.5(7) 1_555 1_555 1_555 1_555 yes
O(3) Pt(1) Pt(2) N(6) -93.5(8) 1_555 1_555 1_555 1_555 yes
O(3) Pt(1) O(2) C(9) -78(1) 1_555 1_555 1_555 1_555 yes
O(3) Pt(1) C(1) C(2) 11(2) 1_555 1_555 1_555 1_555 yes
O(3) C(14) C(15) C(16) -53(4) 1_555 1_555 1_555 1_555 yes
O(3) C(14) C(15) C(17) 55(3) 1_555 1_555 1_555 1_555 yes
O(3) C(14) C(15) C(18) -177(2) 1_555 1_555 1_555 1_555 yes
O(13) C(20) C(21) C(22) -1(8) 1_555 1_555 1_555 1_555 yes
O(13) C(20) C(21) C(26) 170(5) 1_555 1_555 1_555 1_555 yes
N(1) Pt(2) Pt(1) N(3) -88.5(9) 1_555 1_555 1_555 1_555 yes
N(1) Pt(2) Pt(1) N(4) 176.7(9) 1_555 1_555 1_555 1_555 yes
N(1) Pt(2) Pt(1) C(1) 0(6) 1_555 1_555 1_555 1_555 yes
N(1) Pt(2) N(2) C(14) -75(2) 1_555 1_555 1_555 1_555 yes
N(1) C(9) C(10) C(11) -128(2) 1_555 1_555 1_555 1_555 yes
N(1) C(9) C(10) C(12) 114(2) 1_555 1_555 1_555 1_555 yes
N(1) C(9) C(10) C(13) -12(3) 1_555 1_555 1_555 1_555 yes
N(2) Pt(2) Pt(1) N(3) 179.6(8) 1_555 1_555 1_555 1_555 yes
N(2) Pt(2) Pt(1) N(4) 84.8(8) 1_555 1_555 1_555 1_555 yes
N(2) Pt(2) Pt(1) C(1) -91(6) 1_555 1_555 1_555 1_555 yes
N(2) Pt(2) N(1) C(9) 82(2) 1_555 1_555 1_555 1_555 yes
N(2) C(14) C(15) C(16) 124(3) 1_555 1_555 1_555 1_555 yes
N(2) C(14) C(15) C(17) -126(3) 1_555 1_555 1_555 1_555 yes
N(2) C(14) C(15) C(18) 0(4) 1_555 1_555 1_555 1_555 yes
N(3) Pt(1) Pt(2) N(5) -1.9(8) 1_555 1_555 1_555 1_555 yes
N(3) Pt(1) Pt(2) N(6) 89.0(8) 1_555 1_555 1_555 1_555 yes
N(3) Pt(1) O(2) C(9) 105(1) 1_555 1_555 1_555 1_555 yes
N(3) Pt(1) O(3) C(14) 149(8) 1_555 1_555 1_555 1_555 yes
N(3) Pt(1) C(1) C(2) -170(2) 1_555 1_555 1_555 1_555 yes
N(4) Pt(1) Pt(2) N(5) -96.7(8) 1_555 1_555 1_555 1_555 yes
N(4) Pt(1) Pt(2) N(6) -5.8(8) 1_555 1_555 1_555 1_555 yes
N(4) Pt(1) O(2) C(9) -168(10) 1_555 1_555 1_555 1_555 yes
N(4) Pt(1) O(3) C(14) -98(2) 1_555 1_555 1_555 1_555 yes
N(4) Pt(1) C(1) C(2) -76(2) 1_555 1_555 1_555 1_555 yes
N(5) Pt(2) Pt(1) C(1) 86(6) 1_555 1_555 1_555 1_555 yes
N(5) Pt(2) N(1) C(9) -102(2) 1_555 1_555 1_555 1_555 yes
N(5) Pt(2) N(2) C(14) -157(7) 1_555 1_555 1_555 1_555 yes
N(6) Pt(2) Pt(1) C(1) 177(6) 1_555 1_555 1_555 1_555 yes
N(6) Pt(2) N(1) C(9) -159(5) 1_555 1_555 1_555 1_555 yes
N(6) Pt(2) N(2) C(14) 110(2) 1_555 1_555 1_555 1_555 yes
C(1) Pt(1) O(2) C(9) -172(1) 1_555 1_555 1_555 1_555 yes
C(1) Pt(1) O(3) C(14) 174(2) 1_555 1_555 1_555 1_555 yes
C(1) C(2) C(3) C(4) -169(3) 1_555 1_555 1_555 1_555 yes
C(1) C(2) C(3) C(8) 4(5) 1_555 1_555 1_555 1_555 yes
C(2) C(3) C(4) C(5) -178(3) 1_555 1_555 1_555 1_555 yes
C(2) C(3) C(8) C(7) 175(3) 1_555 1_555 1_555 1_555 yes
C(3) C(4) C(5) C(6) -6(6) 1_555 1_555 1_555 1_555 yes
C(3) C(8) C(7) C(6) 11(5) 1_555 1_555 1_555 1_555 yes
C(4) C(3) C(8) C(7) -11(6) 1_555 1_555 1_555 1_555 yes
C(4) C(5) C(6) C(7) 9(8) 1_555 1_555 1_555 1_555 yes
C(5) C(4) C(3) C(8) 7(6) 1_555 1_555 1_555 1_555 yes
C(5) C(6) C(7) C(8) -11(7) 1_555 1_555 1_555 1_555 yes
C(19) C(20) C(21) C(22) 161(5) 1_555 1_555 1_555 1_555 yes
C(19) C(20) C(21) C(26) -26(7) 1_555 1_555 1_555 1_555 yes
C(20) C(21) C(22) C(23) 172(5) 1_555 1_555 1_555 1_555 yes
C(20) C(21) C(26) C(25) -170(4) 1_555 1_555 1_555 1_555 yes
C(21) C(22) C(23) C(24) 8(11) 1_555 1_555 1_555 1_555 yes
C(21) C(26) C(25) C(24) -11(7) 1_555 1_555 1_555 1_555 yes
C(22) C(21) C(26) C(25) 2(7) 1_555 1_555 1_555 1_555 yes
C(22) C(23) C(24) C(25) -22(14) 1_555 1_555 1_555 1_555 yes
C(23) C(22) C(21) C(26) 0(7) 1_555 1_555 1_555 1_555 yes
C(23) C(24) C(25) C(26) 21(10) 1_555 1_555 1_555 1_555 yes
