#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/11/56/4115641.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4115641
loop_
_publ_author_name
'Quan-Ming Wang'
'Thomas C. W. Mak'
_publ_section_title
;
 Argentophilicity and Solvent-Induced Structural Diversity in Double Salts
 of Silver Acetylide with Silver Perfluoroalkyl Carboxylates
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              7594
_journal_page_last               7600
_journal_paper_doi               10.1021/ja0043441
_journal_volume                  123
_journal_year                    2001
_chemical_formula_sum            'C75 H40 Ag31 F69 N7 O48.5'
_chemical_formula_weight         6470.11
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           14
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-P 2ybc'
_symmetry_space_group_name_H-M   'P 1 21/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 106.021(3)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   17.205(2)
_cell_length_b                   32.735(4)
_cell_length_c                   27.257(4)
_cell_measurement_temperature    293(2)
_cell_volume                     14755(3)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.915
_diffrn_measured_fraction_theta_max 0.915
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0471
_diffrn_reflns_av_sigmaI/netI    0.1205
_diffrn_reflns_limit_h_max       22
_diffrn_reflns_limit_h_min       -22
_diffrn_reflns_limit_k_max       39
_diffrn_reflns_limit_k_min       -33
_diffrn_reflns_limit_l_max       9
_diffrn_reflns_limit_l_min       -35
_diffrn_reflns_number            47304
_diffrn_reflns_theta_full        27.99
_diffrn_reflns_theta_max         27.99
_diffrn_reflns_theta_min         1.23
_exptl_absorpt_coefficient_mu    4.167
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.601
_exptl_absorpt_correction_type   SADABS
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.913
_exptl_crystal_description       block
_exptl_crystal_F_000             12020
_exptl_crystal_size_max          0.56
_exptl_crystal_size_mid          0.36
_exptl_crystal_size_min          0.32
_refine_diff_density_max         1.550
_refine_diff_density_min         -1.216
_refine_diff_density_rms         0.169
_refine_ls_extinction_coef       0.000021(7)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.908
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     2082
_refine_ls_number_reflns         32571
_refine_ls_number_restraints     155
_refine_ls_restrained_S_all      0.908
_refine_ls_R_factor_all          0.1502
_refine_ls_R_factor_gt           0.0595
_refine_ls_shift/su_max          0.004
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0596P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1306
_refine_ls_wR_factor_ref         0.1559
_reflns_number_gt                13755
_reflns_number_total             32571
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ja0043441_3.cif
_cod_data_source_block           compound3
_cod_original_formula_sum        'C75 H40 Ag31 F69 N7 O48.50'
_cod_database_code               4115641
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y-1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.71194(5) 0.12626(3) 0.28904(4) 0.0611(3) Uani 1 1 d .
Ag2 Ag 0.63736(8) 0.20139(3) 0.20634(5) 0.0804(4) Uani 1 1 d .
Ag3 Ag 0.60025(6) 0.05551(3) 0.25768(4) 0.0577(3) Uani 1 1 d .
Ag4 Ag 0.55436(6) 0.18833(3) 0.28549(4) 0.0556(3) Uani 1 1 d .
Ag5 Ag 0.50288(9) 0.10840(3) 0.30450(5) 0.0901(4) Uani 1 1 d .
Ag6 Ag 0.52931(5) 0.13265(3) 0.13400(4) 0.0501(2) Uani 1 1 d .
Ag7 Ag 0.44500(5) 0.08156(3) 0.19626(4) 0.0476(2) Uani 1 1 d .
Ag8 Ag 0.41103(6) 0.17422(3) 0.18231(4) 0.0538(3) Uani 1 1 d .
Ag9 Ag 0.34571(6) 0.19697(3) 0.25985(4) 0.0543(3) Uani 1 1 d .
Ag10 Ag 0.25490(6) 0.13295(3) 0.13806(4) 0.0563(3) Uani 1 1 d .
Ag11 Ag 0.35950(6) 0.05287(3) 0.27901(4) 0.0619(3) Uani 1 1 d .
Ag12 Ag 0.22076(6) 0.06211(3) 0.19152(4) 0.0583(3) Uani 1 1 d .
Ag13 Ag 0.20025(6) 0.14207(3) 0.24496(4) 0.0563(3) Uani 1 1 d .
Ag14 Ag 0.18390(6) 0.06018(3) 0.30164(4) 0.0567(3) Uani 1 1 d .
Ag15 Ag 0.14305(6) 0.12954(3) 0.35574(4) 0.0581(3) Uani 1 1 d .
Ag16 Ag 0.04490(6) 0.05210(3) 0.21507(4) 0.0574(3) Uani 1 1 d .
Ag17 Ag 0.04274(6) 0.19334(3) 0.22342(4) 0.0615(3) Uani 1 1 d .
Ag18 Ag -0.01429(7) 0.17057(3) 0.30505(4) 0.0592(3) Uani 1 1 d .
Ag19 Ag -0.03943(6) 0.07877(3) 0.30192(4) 0.0533(3) Uani 1 1 d .
Ag20 Ag -0.11998(5) 0.12290(3) 0.36212(4) 0.0545(3) Uani 1 1 d .
Ag21 Ag -0.07253(6) 0.11845(3) 0.19652(4) 0.0580(3) Uani 1 1 d .
Ag22 Ag -0.20460(5) 0.06072(3) 0.23643(4) 0.0524(3) Uani 1 1 d .
Ag23 Ag -0.18219(7) 0.19836(3) 0.20535(5) 0.0774(4) Uani 1 1 d .
Ag24 Ag -0.27446(7) 0.12806(3) 0.16732(5) 0.0777(4) Uani 1 1 d .
Ag25 Ag 0.69664(8) -0.03538(4) 0.24409(7) 0.1135(6) Uani 1 1 d .
Ag26 Ag 0.50469(7) 0.24723(4) 0.10151(5) 0.0788(4) Uani 1 1 d .
Ag27 Ag 0.47643(10) 0.27500(4) 0.33924(5) 0.0978(5) Uani 1 1 d .
Ag28 Ag 0.31566(10) -0.02415(4) 0.35978(6) 0.1069(5) Uani 1 1 d .
Ag29 Ag 0.05142(10) -0.02164(5) 0.12456(6) 0.1207(6) Uani 1 1 d .
Ag30 Ag -0.05441(11) 0.27591(4) 0.14721(6) 0.1161(6) Uani 1 1 d .
Ag31 Ag -0.11796(10) 0.24176(4) 0.37362(7) 0.1139(6) Uani 1 1 d .
C1 C 0.5818(7) 0.1470(4) 0.2223(5) 0.047(3) Uani 1 1 d .
C2 C 0.5621(6) 0.1172(4) 0.2372(5) 0.051(3) Uani 1 1 d .
C3 C 0.3402(6) 0.1373(4) 0.2242(5) 0.046(3) Uani 1 1 d .
C4 C 0.3175(7) 0.1047(4) 0.2318(5) 0.049(3) Uani 1 1 d .
C5 C 0.0548(8) 0.1348(3) 0.2598(5) 0.053(3) Uani 1 1 d .
C6 C 0.0937(7) 0.1039(3) 0.2669(4) 0.040(3) Uani 1 1 d .
C7 C -0.1822(6) 0.1401(4) 0.2393(4) 0.044(3) Uani 1 1 d .
C8 C -0.1490(7) 0.1202(3) 0.2769(4) 0.046(3) Uani 1 1 d .
O11 O -0.0069(5) 0.1854(3) 0.3864(3) 0.061(2) Uani 1 1 d .
O12 O 0.1116(5) 0.1569(3) 0.4233(3) 0.059(2) Uani 1 1 d .
O21 O -0.1535(5) -0.0050(2) 0.2525(4) 0.076(3) Uani 1 1 d .
O22 O -0.0228(5) 0.0107(3) 0.2834(4) 0.064(3) Uani 1 1 d .
O31 O 0.0451(5) 0.0658(3) 0.3821(3) 0.061(2) Uani 1 1 d .
O32 O -0.0287(5) 0.0939(3) 0.4296(3) 0.058(2) Uani 1 1 d .
O41 O 0.4663(5) 0.2405(2) 0.1888(3) 0.052(2) Uani 1 1 d .
O42 O 0.4075(5) 0.2589(2) 0.2489(4) 0.061(2) Uani 1 1 d .
O51 O 0.4008(5) 0.1891(2) 0.0990(3) 0.056(2) Uani 1 1 d .
O52 O 0.2830(5) 0.1585(3) 0.0672(3) 0.066(3) Uani 1 1 d .
O61 O -0.0736(5) 0.2389(3) 0.2927(4) 0.070(3) Uani 1 1 d .
O62 O -0.0082(6) 0.2571(2) 0.2374(4) 0.068(3) Uani 1 1 d .
O71 O 0.4249(5) 0.0081(2) 0.2067(3) 0.059(2) Uani 1 1 d .
O72 O 0.5564(5) -0.0098(2) 0.2385(4) 0.074(3) Uani 1 1 d .
O81 O -0.2116(6) 0.2608(3) 0.1779(4) 0.078(3) Uani 1 1 d .
O82 O -0.3472(6) 0.2541(3) 0.1610(4) 0.076(3) Uani 1 1 d .
O91 O 0.7121(5) 0.0211(3) 0.3033(3) 0.067(3) Uani 1 1 d .
O92 O 0.7587(5) 0.0719(3) 0.3568(4) 0.071(3) Uani 1 1 d .
O101 O 0.1327(6) -0.0076(3) 0.2133(4) 0.079(3) Uani 1 1 d .
O102 O 0.2435(6) -0.0048(2) 0.2761(4) 0.066(2) Uani 1 1 d .
O111 O -0.3168(5) 0.0279(2) 0.1865(3) 0.053(2) Uani 1 1 d .
O112 O -0.3585(5) 0.0772(3) 0.1262(3) 0.058(2) Uani 1 1 d .
O121 O -0.0407(5) 0.0129(3) 0.1580(3) 0.072(3) Uani 1 1 d .
O122 O -0.1407(5) 0.0573(3) 0.1545(4) 0.074(3) Uani 1 1 d .
O131 O 0.3626(5) 0.0706(3) 0.1172(3) 0.060(2) Uani 1 1 d .
O132 O 0.4393(5) 0.0982(3) 0.0715(3) 0.062(2) Uani 1 1 d .
O141 O -0.0882(7) 0.1434(3) 0.1170(4) 0.090(4) Uani 1 1 d .
O142 O -0.0913(6) 0.2073(3) 0.1449(4) 0.065(3) Uani 1 1 d .
O151 O 0.4823(5) 0.2011(3) 0.3435(3) 0.064(2) Uani 1 1 d .
O152 O 0.4767(6) 0.1379(3) 0.3714(3) 0.072(3) Uani 1 1 d .
O161 O 0.2973(6) 0.2342(3) 0.3119(4) 0.072(3) Uani 1 1 d .
O162 O 0.2041(6) 0.1885(3) 0.3144(4) 0.079(3) Uani 1 1 d .
O171 O 0.1947(6) 0.1942(3) 0.1777(4) 0.079(3) Uani 1 1 d .
O172 O 0.0863(6) 0.2320(3) 0.1691(4) 0.086(3) Uani 1 1 d .
O181 O 0.8131(6) 0.1801(3) 0.3845(4) 0.089(3) Uani 1 1 d .
O182 O 0.6837(6) 0.1624(3) 0.3582(4) 0.068(3) Uani 1 1 d .
O191 O 0.5422(6) 0.0432(3) 0.3441(4) 0.076(3) Uani 1 1 d .
O192 O 0.4282(5) 0.0059(3) 0.3270(4) 0.074(3) Uani 1 1 d .
O201 O 0.7022(6) 0.1648(3) 0.0941(4) 0.085(3) Uani 1 1 d .
O202 O 0.5762(6) 0.1843(3) 0.0889(4) 0.079(3) Uani 1 1 d .
O211 O 0.1355(6) 0.1074(3) 0.0867(4) 0.093(4) Uani 1 1 d .
O212 O 0.1023(5) 0.0570(3) 0.1290(4) 0.075(3) Uani 1 1 d .
O221 O 0.5931(6) 0.2555(3) 0.3009(4) 0.074(3) Uani 1 1 d .
O222 O 0.7144(8) 0.2465(3) 0.2890(7) 0.150(7) Uani 1 1 d .
O231 O 0.2981(5) 0.0523(3) 0.3646(3) 0.064(2) Uani 1 1 d .
O232 O 0.2619(5) 0.1029(3) 0.4093(3) 0.075(3) Uani 1 1 d .
C11 C 0.0511(8) 0.1759(4) 0.4234(5) 0.052(3) Uani 1 1 d D
C12 C 0.0466(10) 0.1909(5) 0.4757(6) 0.082(5) Uani 1 1 d D
C21 C -0.0808(8) -0.0127(3) 0.2692(5) 0.060(4) Uani 1 1 d D
C22 C -0.0600(11) -0.0577(5) 0.2697(11) 0.117(8) Uani 1 1 d D
C31 C 0.0272(7) 0.0738(4) 0.4223(5) 0.050(3) Uani 1 1 d D
C32 C 0.0802(10) 0.0536(5) 0.4698(6) 0.075(4) Uani 1 1 d D
C41 C 0.4441(7) 0.2652(3) 0.2163(5) 0.051(3) Uani 1 1 d D
C42 C 0.4622(10) 0.3104(4) 0.2089(6) 0.069(4) Uani 1 1 d D
C51 C 0.3387(9) 0.1774(4) 0.0643(5) 0.053(3) Uani 1 1 d D
C52 C 0.3339(10) 0.1962(5) 0.0118(5) 0.075(5) Uani 1 1 d D
C61 C -0.0465(7) 0.2635(3) 0.2681(5) 0.047(3) Uani 1 1 d D
C62 C -0.0657(11) 0.3093(4) 0.2757(7) 0.079(5) Uani 1 1 d D
C71 C 0.4853(8) -0.0167(3) 0.2185(5) 0.048(3) Uani 1 1 d D
C72 C 0.4633(10) -0.0612(4) 0.2060(10) 0.114(8) Uani 1 1 d D
C81 C -0.2800(10) 0.2730(4) 0.1622(6) 0.064(4) Uani 1 1 d D
C82 C -0.2948(10) 0.3147(4) 0.1386(8) 0.088(6) Uani 1 1 d D
C91 C 0.7541(7) 0.0354(4) 0.3433(5) 0.054(3) Uani 1 1 d D
C92 C 0.8079(9) 0.0060(5) 0.3819(6) 0.076(5) Uani 1 1 d D
C101 C 0.1882(8) -0.0232(3) 0.2434(5) 0.053(3) Uani 1 1 d D
C102 C 0.1961(12) -0.0683(4) 0.2415(9) 0.096(6) Uani 1 1 d D
C111 C -0.3575(7) 0.0413(4) 0.1445(5) 0.052(3) Uani 1 1 d D
C112 C -0.4132(7) 0.0100(4) 0.1101(5) 0.059(4) Uani 1 1 d D
C121 C -0.1122(9) 0.0264(5) 0.1425(5) 0.069(4) Uani 1 1 d D
C122 C -0.1684(10) -0.0017(6) 0.1037(9) 0.112(8) Uani 1 1 d D
C131 C 0.3820(7) 0.0783(4) 0.0775(5) 0.048(3) Uani 1 1 d D
C132 C 0.3315(11) 0.0560(5) 0.0297(6) 0.086(5) Uani 1 1 d D
C141 C -0.0901(8) 0.1812(5) 0.1121(6) 0.071(4) Uani 1 1 d D
C142 C -0.0912(15) 0.1973(7) 0.0601(7) 0.104(6) Uani 1 1 d D
C151 C 0.4737(7) 0.1763(4) 0.3743(4) 0.053(3) Uani 1 1 d D
C152 C 0.4539(10) 0.1906(5) 0.4212(5) 0.070(4) Uani 1 1 d D
C161 C 0.2411(7) 0.2211(4) 0.3290(4) 0.052(3) Uani 1 1 d D
C162 C 0.2122(10) 0.2464(5) 0.3662(7) 0.090(6) Uani 1 1 d D
C171 C 0.1492(9) 0.2213(4) 0.1596(5) 0.057(3) Uani 1 1 d D
C172 C 0.1738(11) 0.2480(6) 0.1201(7) 0.095(5) Uani 1 1 d D
C181 C 0.7395(9) 0.1801(4) 0.3869(6) 0.066(4) Uani 1 1 d D
C182 C 0.7248(9) 0.2060(5) 0.4279(6) 0.075(5) Uani 1 1 d D
C191 C 0.5021(8) 0.0122(4) 0.3469(5) 0.059(4) Uani 1 1 d D
C192 C 0.5510(14) -0.0210(6) 0.3778(10) 0.121(8) Uani 1 1 d D
C201 C 0.6408(9) 0.1844(4) 0.0753(5) 0.063(4) Uani 1 1 d D
C202 C 0.6451(12) 0.2121(7) 0.0314(7) 0.104(7) Uani 1 1 d D
C211 C 0.0939(7) 0.0792(5) 0.0921(5) 0.054(3) Uani 1 1 d D
C212 C 0.0235(12) 0.0705(7) 0.0465(7) 0.106(7) Uani 1 1 d D
C221 C 0.6665(11) 0.2643(4) 0.3027(7) 0.090(5) Uani 1 1 d D
C222 C 0.6854(14) 0.3076(6) 0.3241(10) 0.124(8) Uani 1 1 d D
C231 C 0.3043(7) 0.0741(4) 0.4029(5) 0.055(3) Uani 1 1 d D
C232 C 0.3724(11) 0.0643(6) 0.4499(6) 0.093(6) Uani 1 1 d D
F11 F -0.0260(7) 0.1978(4) 0.4787(4) 0.155(5) Uani 1 1 d D
F12 F 0.0859(7) 0.2256(3) 0.4867(4) 0.143(5) Uani 1 1 d D
F13 F 0.0790(6) 0.1660(3) 0.5120(3) 0.113(3) Uani 1 1 d D
F21 F -0.0985(9) -0.0779(4) 0.2982(7) 0.212(9) Uani 1 1 d D
F22 F -0.0870(11) -0.0751(4) 0.2277(6) 0.221(10) Uani 1 1 d D
F23 F 0.0101(6) -0.0659(3) 0.2881(7) 0.221(9) Uani 1 1 d D
F31 F 0.0865(9) 0.0706(5) 0.5110(4) 0.205(8) Uani 1 1 d D
F32 F 0.0582(9) 0.0197(4) 0.4765(6) 0.246(11) Uani 1 1 d D
F33 F 0.1508(7) 0.0489(5) 0.4692(4) 0.210(9) Uani 1 1 d D
F41 F 0.5233(6) 0.3164(2) 0.1902(4) 0.119(4) Uani 1 1 d D
F42 F 0.4759(6) 0.3318(2) 0.2512(4) 0.111(3) Uani 1 1 d D
F43 F 0.3986(6) 0.3282(3) 0.1763(4) 0.126(4) Uani 1 1 d D
F51 F 0.2870(6) 0.2270(3) 0.0009(3) 0.123(4) Uani 1 1 d D
F52 F 0.4039(6) 0.2062(3) 0.0047(3) 0.110(3) Uani 1 1 d D
F53 F 0.3045(6) 0.1677(3) -0.0245(3) 0.116(3) Uani 1 1 d D
F61 F -0.0036(7) 0.3249(3) 0.3095(4) 0.149(5) Uani 1 1 d D
F62 F -0.1272(6) 0.3146(3) 0.2906(5) 0.149(5) Uani 1 1 d D
F63 F -0.0735(7) 0.3303(2) 0.2337(4) 0.123(4) Uani 1 1 d D
F71 F 0.3948(8) -0.0659(3) 0.1711(6) 0.213(9) Uani 1 1 d D
F72 F 0.4501(12) -0.0790(4) 0.2453(6) 0.226(10) Uani 1 1 d D
F73 F 0.5142(7) -0.0814(3) 0.1931(6) 0.182(7) Uani 1 1 d D
F81 F -0.2399(7) 0.3247(4) 0.1172(6) 0.219(9) Uani 1 1 d D
F82 F -0.2920(10) 0.3421(3) 0.1720(6) 0.209(8) Uani 1 1 d D
F83 F -0.3618(6) 0.3196(3) 0.1048(5) 0.158(6) Uani 1 1 d D
F91 F 0.8114(7) 0.0135(4) 0.4282(4) 0.164(6) Uani 1 1 d D
F92 F 0.7877(6) -0.0316(3) 0.3728(4) 0.130(4) Uani 1 1 d D
F93 F 0.8835(5) 0.0089(3) 0.3794(4) 0.125(4) Uani 1 1 d D
F101 F 0.1946(12) -0.0850(3) 0.2821(5) 0.219(9) Uani 1 1 d D
F102 F 0.1423(10) -0.0872(4) 0.2107(6) 0.211(9) Uani 1 1 d D
F103 F 0.2568(10) -0.0794(4) 0.2339(9) 0.341(17) Uani 1 1 d D
F111 F -0.3873(5) -0.0264(2) 0.1190(4) 0.110(4) Uani 1 1 d D
F112 F -0.4251(5) 0.0181(3) 0.0613(3) 0.107(3) Uani 1 1 d D
F113 F -0.4852(4) 0.0122(2) 0.1178(3) 0.080(2) Uani 1 1 d D
F121 F -0.1927(9) -0.0316(4) 0.1276(5) 0.188(7) Uani 1 1 d D
F122 F -0.2337(7) 0.0153(4) 0.0788(5) 0.186(7) Uani 1 1 d D
F123 F -0.1372(6) -0.0181(4) 0.0728(5) 0.193(8) Uani 1 1 d D
F131 F 0.3503(9) 0.0212(4) 0.0273(5) 0.232(10) Uani 1 1 d D
F132 F 0.3233(9) 0.0727(4) -0.0113(4) 0.198(8) Uani 1 1 d D
F133 F 0.2542(7) 0.0524(5) 0.0307(4) 0.196(8) Uani 1 1 d D
F141 F -0.0184(8) 0.1933(5) 0.0547(4) 0.188(7) Uani 1 1 d D
F142 F -0.1084(10) 0.2336(4) 0.0508(4) 0.197(8) Uani 1 1 d D
F143 F -0.1334(9) 0.1767(4) 0.0223(4) 0.171(6) Uani 1 1 d D
F151 F 0.4996(6) 0.1778(4) 0.4629(3) 0.145(5) Uani 1 1 d D
F152 F 0.4479(7) 0.2306(3) 0.4251(4) 0.133(4) Uani 1 1 d D
F153 F 0.3780(6) 0.1782(3) 0.4217(4) 0.135(4) Uani 1 1 d D
F161 F 0.1350(6) 0.2520(4) 0.3514(5) 0.164(6) Uani 1 1 d D
F162 F 0.2222(7) 0.2256(3) 0.4109(4) 0.127(4) Uani 1 1 d D
F163 F 0.2498(6) 0.2789(3) 0.3791(4) 0.124(4) Uani 1 1 d D
F171 F 0.2506(7) 0.2556(4) 0.1356(5) 0.181(6) Uani 1 1 d D
F172 F 0.1658(7) 0.2274(3) 0.0769(4) 0.139(4) Uani 1 1 d D
F173 F 0.1363(7) 0.2812(3) 0.1083(4) 0.151(5) Uani 1 1 d D
F181 F 0.6524(7) 0.2106(5) 0.4264(5) 0.217(9) Uani 1 1 d D
F182 F 0.7566(10) 0.1906(5) 0.4723(4) 0.216(9) Uani 1 1 d D
F183 F 0.7566(9) 0.2408(4) 0.4333(5) 0.176(7) Uani 1 1 d D
F191 F 0.5191(9) -0.0365(7) 0.4082(8) 0.267(14) Uani 1 1 d D
F192 F 0.6187(8) -0.0148(5) 0.4032(8) 0.258(12) Uani 1 1 d D
F193 F 0.5596(17) -0.0499(5) 0.3526(6) 0.326(17) Uani 1 1 d D
F201 F 0.5829(8) 0.2358(5) 0.0173(5) 0.236(10) Uani 1 1 d D
F202 F 0.6536(10) 0.1927(4) -0.0064(4) 0.197(8) Uani 1 1 d D
F203 F 0.7081(9) 0.2366(4) 0.0450(5) 0.193(7) Uani 1 1 d D
F211 F -0.0340(7) 0.0529(6) 0.0546(5) 0.233(10) Uani 1 1 d D
F212 F -0.0038(8) 0.1000(4) 0.0181(5) 0.177(6) Uani 1 1 d D
F213 F 0.0478(8) 0.0456(5) 0.0159(6) 0.242(11) Uani 1 1 d D
F221 F 0.6885(9) 0.3330(4) 0.2874(6) 0.194(7) Uani 1 1 d D
F222 F 0.7609(6) 0.3100(4) 0.3543(5) 0.166(6) Uani 1 1 d D
F223 F 0.6402(7) 0.3242(4) 0.3482(6) 0.193(8) Uani 1 1 d D
F231 F 0.3494(8) 0.0354(5) 0.4756(5) 0.215(8) Uani 1 1 d D
F232 F 0.4344(7) 0.0480(5) 0.4382(4) 0.193(7) Uani 1 1 d D
F233 F 0.4016(7) 0.0911(4) 0.4816(4) 0.152(5) Uani 1 1 d D
O1W O 0.2648(5) 0.0061(3) 0.1463(4) 0.085(3) Uani 1 1 d .
O2W O 0.1385(5) 0.0032(3) 0.3512(4) 0.074(3) Uani 1 1 d .
O3W O -0.2076(14) 0.2026(6) 0.275(2) 0.30(3) Uani 0.50 1 d P
N1 N 0.7090(9) -0.0984(4) 0.2378(8) 0.138(7) Uani 1 1 d D
N2 N 0.4212(8) 0.2963(4) 0.0637(5) 0.090(4) Uani 1 1 d D
N3 N 0.4657(9) 0.3257(4) 0.3843(6) 0.094(5) Uani 1 1 d D
N4 N 0.3324(8) -0.0655(4) 0.4229(6) 0.101(5) Uani 1 1 d D
N5 N 0.1141(11) -0.0581(8) 0.0879(7) 0.193(11) Uani 1 1 d D
N6 N -0.0515(10) 0.3317(4) 0.1084(7) 0.125(6) Uani 1 1 d D
N7 N -0.0394(12) 0.2911(6) 0.4162(9) 0.147(8) Uani 1 1 d D
C011 C 0.7268(10) -0.1322(5) 0.2386(8) 0.113(7) Uani 1 1 d D
C012 C 0.7541(12) -0.1760(4) 0.2425(10) 0.153(10) Uani 1 1 d D
C013 C 0.8394(11) -0.1793(6) 0.2566(11) 0.166(11) Uani 1 1 d D
C021 C 0.3640(10) 0.3152(5) 0.0482(6) 0.087(5) Uani 1 1 d D
C022 C 0.2908(10) 0.3404(5) 0.0288(6) 0.101(6) Uani 1 1 d D
C023 C 0.2863(14) 0.3704(6) 0.0671(8) 0.137(8) Uani 1 1 d D
C031 C 0.4635(11) 0.3522(5) 0.4109(7) 0.111(7) Uani 1 1 d D
C032 C 0.4639(15) 0.3871(6) 0.4473(10) 0.186(14) Uani 1 1 d D
C033 C 0.5406(14) 0.4068(7) 0.4639(9) 0.161(10) Uani 1 1 d D
C041 C 0.3502(11) -0.0809(6) 0.4611(7) 0.111(7) Uani 1 1 d D
C042 C 0.3701(14) -0.1029(8) 0.5115(8) 0.187(13) Uani 1 1 d D
C043 C 0.3301(18) -0.0875(9) 0.5466(10) 0.194(13) Uani 1 1 d D
C051 C 0.1563(13) -0.0788(9) 0.0733(10) 0.196(14) Uani 1 1 d D
C052 C 0.2151(19) -0.1082(10) 0.0593(11) 0.212(15) Uani 1 1 d D
C053 C 0.2353(17) -0.0882(10) 0.0181(15) 0.241(19) Uani 1 1 d D
C061 C -0.0552(15) 0.3606(6) 0.0852(9) 0.150(10) Uani 1 1 d D
C062 C -0.061(2) 0.3950(7) 0.0479(13) 0.26(2) Uani 1 1 d D
C063 C -0.1172(16) 0.4233(8) 0.0530(13) 0.212(15) Uani 1 1 d D
C071 C 0.0157(14) 0.3110(8) 0.4350(10) 0.143(10) Uani 1 1 d D
C072 C 0.0918(11) 0.3339(7) 0.4605(9) 0.133(8) Uani 1 1 d D
C073 C 0.1001(14) 0.3663(8) 0.4262(9) 0.183(13) Uani 1 1 d D
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O182 Ag1 C8 123.5(4) . 1_655
O182 Ag1 O92 82.2(3) . .
C8 Ag1 O92 85.3(3) 1_655 .
O182 Ag1 C1 95.8(3) . .
C8 Ag1 C1 127.3(4) 1_655 .
O92 Ag1 C1 138.2(3) . .
O182 Ag1 C7 130.6(4) . 1_655
C8 Ag1 C7 27.5(3) 1_655 1_655
O92 Ag1 C7 112.1(3) . 1_655
C1 Ag1 C7 100.7(4) . 1_655
O182 Ag1 C2 95.7(3) . .
C8 Ag1 C2 139.4(4) 1_655 .
O92 Ag1 C2 112.7(4) . .
C1 Ag1 C2 25.6(3) . .
C7 Ag1 C2 118.1(4) 1_655 .
O182 Ag1 Ag3 110.9(2) . .
C8 Ag1 Ag3 117.6(3) 1_655 .
O92 Ag1 Ag3 73.3(2) . .
C1 Ag1 Ag3 68.5(3) . .
C7 Ag1 Ag3 118.5(3) 1_655 .
C2 Ag1 Ag3 44.7(3) . .
O182 Ag1 Ag20 82.2(2) . 1_655
C8 Ag1 Ag20 46.5(3) 1_655 1_655
O92 Ag1 Ag20 56.0(2) . 1_655
C1 Ag1 Ag20 165.5(3) . 1_655
C7 Ag1 Ag20 70.7(2) 1_655 1_655
C2 Ag1 Ag20 168.6(3) . 1_655
Ag3 Ag1 Ag20 125.71(5) . 1_655
O182 Ag1 Ag22 156.6(2) . 1_655
C8 Ag1 Ag22 46.7(3) 1_655 1_655
O92 Ag1 Ag22 76.1(2) . 1_655
C1 Ag1 Ag22 106.1(3) . 1_655
C7 Ag1 Ag22 53.5(3) 1_655 1_655
C2 Ag1 Ag22 100.6(3) . 1_655
Ag3 Ag1 Ag22 71.21(4) . 1_655
Ag20 Ag1 Ag22 78.55(3) 1_655 1_655
O182 Ag1 Ag2 92.5(2) . .
C8 Ag1 Ag2 99.8(3) 1_655 .
O92 Ag1 Ag2 174.1(2) . .
C1 Ag1 Ag2 39.4(3) . .
C7 Ag1 Ag2 73.3(3) 1_655 .
C2 Ag1 Ag2 65.0(3) . .
Ag3 Ag1 Ag2 106.34(4) . .
Ag20 Ag1 Ag2 126.12(4) 1_655 .
Ag22 Ag1 Ag2 109.48(4) 1_655 .
O182 Ag1 Ag4 52.1(2) . .
C8 Ag1 Ag4 146.3(3) 1_655 .
O92 Ag1 Ag4 122.4(2) . .
C1 Ag1 Ag4 43.9(3) . .
C7 Ag1 Ag4 123.7(3) 1_655 .
C2 Ag1 Ag4 51.8(3) . .
Ag3 Ag1 Ag4 90.60(4) . .
Ag20 Ag1 Ag4 131.00(4) 1_655 .
Ag22 Ag1 Ag4 149.90(4) 1_655 .
Ag2 Ag1 Ag4 51.74(3) . .
C1 Ag2 O82 155.8(4) . 1_655
C1 Ag2 Ag4 52.2(3) . .
O82 Ag2 Ag4 133.9(3) 1_655 .
C1 Ag2 Ag23 118.8(3) . 1_655
O82 Ag2 Ag23 75.1(2) 1_655 1_655
Ag4 Ag2 Ag23 133.77(6) . 1_655
C1 Ag2 Ag24 73.6(3) . 1_655
O82 Ag2 Ag24 105.3(3) 1_655 1_655
Ag4 Ag2 Ag24 120.77(5) . 1_655
Ag23 Ag2 Ag24 53.38(4) 1_655 1_655
C1 Ag2 Ag6 47.4(3) . .
O82 Ag2 Ag6 110.2(3) 1_655 .
Ag4 Ag2 Ag6 91.87(4) . .
Ag23 Ag2 Ag6 112.38(4) 1_655 .
Ag24 Ag2 Ag6 61.02(3) 1_655 .
C1 Ag2 Ag1 49.9(3) . .
O82 Ag2 Ag1 151.7(3) 1_655 .
Ag4 Ag2 Ag1 64.56(4) . .
Ag23 Ag2 Ag1 77.55(4) 1_655 .
Ag24 Ag2 Ag1 62.61(4) 1_655 .
Ag6 Ag2 Ag1 87.02(4) . .
C2 Ag3 O91 139.3(4) . .
C2 Ag3 O72 139.8(4) . .
O91 Ag3 O72 80.6(3) . .
C2 Ag3 Ag7 53.1(3) . .
O91 Ag3 Ag7 167.7(2) . .
O72 Ag3 Ag7 87.1(2) . .
C2 Ag3 Ag5 52.3(3) . .
O91 Ag3 Ag5 123.5(2) . .
O72 Ag3 Ag5 117.4(2) . .
Ag7 Ag3 Ag5 61.71(4) . .
C2 Ag3 Ag1 58.1(3) . .
O91 Ag3 Ag1 81.2(2) . .
O72 Ag3 Ag1 160.2(2) . .
Ag7 Ag3 Ag1 111.09(4) . .
Ag5 Ag3 Ag1 79.46(4) . .
O221 Ag4 O151 83.4(3) . .
O221 Ag4 C1 125.5(4) . .
O151 Ag4 C1 150.2(4) . .
O221 Ag4 C2 149.7(4) . .
O151 Ag4 C2 126.9(4) . .
C1 Ag4 C2 25.0(3) . .
O221 Ag4 Ag5 158.5(3) . .
O151 Ag4 Ag5 77.8(2) . .
C1 Ag4 Ag5 74.9(3) . .
C2 Ag4 Ag5 50.0(3) . .
O221 Ag4 Ag2 79.6(3) . .
O151 Ag4 Ag2 160.8(2) . .
C1 Ag4 Ag2 45.8(3) . .
C2 Ag4 Ag2 70.5(3) . .
Ag5 Ag4 Ag2 120.41(5) . .
O221 Ag4 Ag8 114.2(2) . .
O151 Ag4 Ag8 101.4(2) . .
C1 Ag4 Ag8 62.3(3) . .
C2 Ag4 Ag8 65.1(2) . .
Ag5 Ag4 Ag8 79.98(4) . .
Ag2 Ag4 Ag8 77.83(4) . .
O221 Ag4 Ag1 112.4(2) . .
O151 Ag4 Ag1 132.2(2) . .
C1 Ag4 Ag1 49.3(3) . .
C2 Ag4 Ag1 49.1(2) . .
Ag5 Ag4 Ag1 74.30(4) . .
Ag2 Ag4 Ag1 63.70(4) . .
Ag8 Ag4 Ag1 110.78(4) . .
O152 Ag5 C2 145.0(4) . .
O152 Ag5 O191 96.6(3) . .
C2 Ag5 O191 109.3(4) . .
O152 Ag5 Ag4 83.9(2) . .
C2 Ag5 Ag4 61.5(3) . .
O191 Ag5 Ag4 146.4(2) . .
O152 Ag5 Ag3 152.2(3) . .
C2 Ag5 Ag3 46.4(3) . .
O191 Ag5 Ag3 63.1(2) . .
Ag4 Ag5 Ag3 102.64(5) . .
O152 Ag5 Ag7 148.9(3) . .
C2 Ag5 Ag7 50.2(3) . .
O191 Ag5 Ag7 99.1(2) . .
Ag4 Ag5 Ag7 97.26(5) . .
Ag3 Ag5 Ag7 57.95(3) . .
O152 Ag5 Ag11 96.6(3) . .
C2 Ag5 Ag11 113.6(3) . .
O191 Ag5 Ag11 71.1(2) . .
Ag4 Ag5 Ag11 142.46(6) . .
Ag3 Ag5 Ag11 94.23(4) . .
Ag7 Ag5 Ag11 63.95(4) . .
O132 Ag6 O202 103.2(3) . .
O132 Ag6 C1 148.4(4) . .
O202 Ag6 C1 107.3(4) . .
O132 Ag6 Ag7 79.1(2) . .
O202 Ag6 Ag7 167.1(2) . .
C1 Ag6 Ag7 69.3(3) . .
O132 Ag6 Ag8 98.5(2) . .
O202 Ag6 Ag8 105.7(2) . .
C1 Ag6 Ag8 65.4(3) . .
Ag7 Ag6 Ag8 61.40(3) . .
O132 Ag6 Ag2 165.6(2) . .
O202 Ag6 Ag2 66.1(3) . .
C1 Ag6 Ag2 41.2(3) . .
Ag7 Ag6 Ag2 109.14(4) . .
Ag8 Ag6 Ag2 76.35(4) . .
O132 Ag6 Ag24 129.1(2) . 1_655
O202 Ag6 Ag24 72.6(2) . 1_655
C1 Ag6 Ag24 69.5(3) . 1_655
Ag7 Ag6 Ag24 116.11(4) . 1_655
Ag8 Ag6 Ag24 132.00(4) . 1_655
Ag2 Ag6 Ag24 58.78(3) . 1_655
O131 Ag7 C2 140.3(4) . .
O131 Ag7 O71 83.3(3) . .
C2 Ag7 O71 124.5(4) . .
O131 Ag7 Ag3 138.6(2) . .
C2 Ag7 Ag3 47.6(3) . .
O71 Ag7 Ag3 77.25(19) . .
O131 Ag7 Ag5 160.7(2) . .
C2 Ag7 Ag5 50.8(3) . .
O71 Ag7 Ag5 101.1(2) . .
Ag3 Ag7 Ag5 60.33(4) . .
O131 Ag7 Ag6 79.9(2) . .
C2 Ag7 Ag6 60.4(3) . .
O71 Ag7 Ag6 135.3(2) . .
Ag3 Ag7 Ag6 88.76(4) . .
Ag5 Ag7 Ag6 108.20(4) . .
O131 Ag7 Ag8 89.5(2) . .
C2 Ag7 Ag8 71.1(3) . .
O71 Ag7 Ag8 161.11(19) . .
Ag3 Ag7 Ag8 118.57(4) . .
Ag5 Ag7 Ag8 80.35(4) . .
Ag6 Ag7 Ag8 59.48(3) . .
O131 Ag7 Ag11 109.9(2) . .
C2 Ag7 Ag11 108.6(3) . .
O71 Ag7 Ag11 61.2(2) . .
Ag3 Ag7 Ag11 92.12(4) . .
Ag5 Ag7 Ag11 58.23(4) . .
Ag6 Ag7 Ag11 162.96(4) . .
Ag8 Ag7 Ag11 105.67(4) . .
C3 Ag8 O51 136.0(4) . .
C3 Ag8 O41 136.4(4) . .
O51 Ag8 O41 78.3(3) . .
C3 Ag8 Ag9 50.2(3) . .
O51 Ag8 Ag9 140.3(2) . .
O41 Ag8 Ag9 86.3(2) . .
C3 Ag8 Ag10 53.1(3) . .
O51 Ag8 Ag10 83.1(2) . .
O41 Ag8 Ag10 139.1(2) . .
Ag9 Ag8 Ag10 85.37(4) . .
C3 Ag8 Ag6 120.3(3) . .
O51 Ag8 Ag6 62.6(2) . .
O41 Ag8 Ag6 98.1(2) . .
Ag9 Ag8 Ag6 156.68(5) . .
Ag10 Ag8 Ag6 105.13(4) . .
C3 Ag8 Ag7 61.3(3) . .
O51 Ag8 Ag7 107.0(2) . .
O41 Ag8 Ag7 146.6(2) . .
Ag9 Ag8 Ag7 105.90(4) . .
Ag10 Ag8 Ag7 73.80(3) . .
Ag6 Ag8 Ag7 59.12(3) . .
C3 Ag8 Ag4 91.5(3) . .
O51 Ag8 Ag4 132.0(2) . .
O41 Ag8 Ag4 66.8(2) . .
Ag9 Ag8 Ag4 70.59(4) . .
Ag10 Ag8 Ag4 144.46(4) . .
Ag6 Ag8 Ag4 89.98(4) . .
Ag7 Ag8 Ag4 87.72(3) . .
C3 Ag9 O161 144.0(4) . .
C3 Ag9 O42 133.3(4) . .
O161 Ag9 O42 82.5(3) . .
C3 Ag9 Ag8 52.4(3) . .
O161 Ag9 Ag8 162.0(2) . .
O42 Ag9 Ag8 80.8(2) . .
C3 Ag9 Ag13 58.1(3) . .
O161 Ag9 Ag13 88.2(2) . .
O42 Ag9 Ag13 152.4(2) . .
Ag8 Ag9 Ag13 103.57(4) . .
O52 Ag10 O211 88.9(4) . .
O52 Ag10 C3 126.2(4) . .
O211 Ag10 C3 144.9(4) . .
O52 Ag10 C4 145.2(4) . .
O211 Ag10 C4 121.1(4) . .
C3 Ag10 C4 26.4(3) . .
O52 Ag10 Ag12 147.7(3) . .
O211 Ag10 Ag12 75.1(3) . .
C3 Ag10 Ag12 73.1(3) . .
C4 Ag10 Ag12 46.9(3) . .
O52 Ag10 Ag8 78.2(2) . .
O211 Ag10 Ag8 167.0(3) . .
C3 Ag10 Ag8 48.1(3) . .
C4 Ag10 Ag8 71.6(3) . .
Ag12 Ag10 Ag8 116.80(4) . .
O52 Ag10 Ag13 153.1(3) . .
O211 Ag10 Ag13 98.4(3) . .
C3 Ag10 Ag13 51.8(3) . .
C4 Ag10 Ag13 47.3(3) . .
Ag12 Ag10 Ag13 58.75(3) . .
Ag8 Ag10 Ag13 92.66(4) . .
C4 Ag11 O192 167.1(4) . .
C4 Ag11 Ag12 49.6(4) . .
O192 Ag11 Ag12 140.2(3) . .
C4 Ag11 Ag5 77.1(3) . .
O192 Ag11 Ag5 90.8(3) . .
Ag12 Ag11 Ag5 124.73(5) . .
C4 Ag11 Ag7 58.6(3) . .
O192 Ag11 Ag7 111.2(3) . .
Ag12 Ag11 Ag7 79.67(4) . .
Ag5 Ag11 Ag7 57.82(3) . .
C4 Ag11 Ag14 83.0(3) . .
O192 Ag11 Ag14 108.7(3) . .
Ag12 Ag11 Ag14 63.24(3) . .
Ag5 Ag11 Ag14 131.40(5) . .
Ag7 Ag11 Ag14 138.89(4) . .
C4 Ag12 O212 144.4(4) . .
C4 Ag12 O1W 115.3(4) . .
O212 Ag12 O1W 84.6(3) . .
C4 Ag12 Ag10 61.0(3) . .
O212 Ag12 Ag10 86.9(3) . .
O1W Ag12 Ag10 102.3(3) . .
C4 Ag12 Ag11 47.1(3) . .
O212 Ag12 Ag11 167.8(3) . .
O1W Ag12 Ag11 92.2(2) . .
Ag10 Ag12 Ag11 105.33(4) . .
C4 Ag12 Ag13 52.9(3) . .
O212 Ag12 Ag13 102.8(3) . .
O1W Ag12 Ag13 166.8(2) . .
Ag10 Ag12 Ag13 67.63(4) . .
Ag11 Ag12 Ag13 82.77(4) . .
C4 Ag12 Ag14 82.3(3) . .
O212 Ag12 Ag14 109.2(3) . .
O1W Ag12 Ag14 128.4(3) . .
Ag10 Ag12 Ag14 127.15(4) . .
Ag11 Ag12 Ag14 63.94(3) . .
Ag13 Ag12 Ag14 59.85(3) . .
C4 Ag12 Ag16 125.0(3) . .
O212 Ag12 Ag16 56.9(3) . .
O1W Ag12 Ag16 117.1(2) . .
Ag10 Ag12 Ag16 120.46(4) . .
Ag11 Ag12 Ag16 115.16(4) . .
Ag13 Ag12 Ag16 76.03(3) . .
Ag14 Ag12 Ag16 52.30(3) . .
O162 Ag13 C6 89.4(3) . .
O162 Ag13 C4 125.4(4) . .
C6 Ag13 C4 118.9(4) . .
O162 Ag13 O171 97.6(3) . .
C6 Ag13 O171 131.1(3) . .
C4 Ag13 O171 95.7(3) . .
O162 Ag13 C3 112.2(3) . .
C6 Ag13 C3 145.4(4) . .
C4 Ag13 C3 26.5(3) . .
O171 Ag13 C3 74.5(3) . .
O162 Ag13 C5 76.1(3) . .
C6 Ag13 C5 26.9(3) . .
C4 Ag13 C5 145.1(4) . .
O171 Ag13 C5 109.1(3) . .
C3 Ag13 C5 170.8(4) . .
O162 Ag13 Ag9 71.2(2) . .
C6 Ag13 Ag9 158.3(3) . .
C4 Ag13 Ag9 68.6(3) . .
O171 Ag13 Ag9 63.4(2) . .
C3 Ag13 Ag9 44.6(3) . .
C5 Ag13 Ag9 144.6(3) . .
O162 Ag13 Ag12 158.3(3) . .
C6 Ag13 Ag12 82.6(3) . .
C4 Ag13 Ag12 45.6(3) . .
O171 Ag13 Ag12 102.8(2) . .
C3 Ag13 Ag12 67.3(3) . .
C5 Ag13 Ag12 103.5(3) . .
Ag9 Ag13 Ag12 111.90(4) . .
O162 Ag13 Ag17 69.0(3) . .
C6 Ag13 Ag17 69.2(3) . .
C4 Ag13 Ag17 161.2(3) . .
O171 Ag13 Ag17 68.6(2) . .
C3 Ag13 Ag17 142.8(3) . .
C5 Ag13 Ag17 42.8(3) . .
Ag9 Ag13 Ag17 110.61(4) . .
Ag12 Ag13 Ag17 125.56(4) . .
O162 Ag13 Ag14 97.9(2) . .
C6 Ag13 Ag14 42.6(3) . .
C4 Ag13 Ag14 80.6(3) . .
O171 Ag13 Ag14 163.0(3) . .
C3 Ag13 Ag14 105.5(3) . .
C5 Ag13 Ag14 68.5(3) . .
Ag9 Ag13 Ag14 128.69(4) . .
Ag12 Ag13 Ag14 62.80(3) . .
Ag17 Ag13 Ag14 111.23(4) . .
O162 Ag13 Ag10 142.5(2) . .
C6 Ag13 Ag10 126.0(3) . .
C4 Ag13 Ag10 52.1(3) . .
O171 Ag13 Ag10 51.4(2) . .
C3 Ag13 Ag10 46.0(3) . .
C5 Ag13 Ag10 129.4(3) . .
Ag9 Ag13 Ag10 75.27(3) . .
Ag12 Ag13 Ag10 53.62(3) . .
Ag17 Ag13 Ag10 109.11(4) . .
Ag14 Ag13 Ag10 116.16(4) . .
C6 Ag14 O231 142.7(4) . .
C6 Ag14 O102 137.7(4) . .
O231 Ag14 O102 77.2(3) . .
C6 Ag14 O2W 115.7(3) . .
O231 Ag14 O2W 80.9(3) . .
O102 Ag14 O2W 74.9(3) . .
C6 Ag14 Ag16 50.0(3) . .
O231 Ag14 Ag16 167.2(2) . .
O102 Ag14 Ag16 90.3(2) . .
O2W Ag14 Ag16 93.5(2) . .
C6 Ag14 Ag15 56.7(3) . .
O231 Ag14 Ag15 89.1(2) . .
O102 Ag14 Ag15 165.6(2) . .
O2W Ag14 Ag15 98.6(2) . .
Ag16 Ag14 Ag15 103.09(4) . .
C6 Ag14 Ag13 50.4(3) . .
O231 Ag14 Ag13 107.2(2) . .
O102 Ag14 Ag13 118.8(2) . .
O2W Ag14 Ag13 165.01(19) . .
Ag16 Ag14 Ag13 80.90(4) . .
Ag15 Ag14 Ag13 69.47(4) . .
C6 Ag14 Ag12 83.1(3) . .
O231 Ag14 Ag12 111.0(2) . .
O102 Ag14 Ag12 64.2(2) . .
O2W Ag14 Ag12 132.4(2) . .
Ag16 Ag14 Ag12 64.62(3) . .
Ag15 Ag14 Ag12 126.44(4) . .
Ag13 Ag14 Ag12 57.35(3) . .
C6 Ag14 Ag11 124.5(3) . .
O231 Ag14 Ag11 58.2(2) . .
O102 Ag14 Ag11 54.6(2) . .
O2W Ag14 Ag11 118.90(19) . .
Ag16 Ag14 Ag11 116.34(4) . .
Ag15 Ag14 Ag11 121.48(4) . .
Ag13 Ag14 Ag11 75.88(3) . .
Ag12 Ag14 Ag11 52.83(3) . .
O12 Ag15 O232 90.2(3) . .
O12 Ag15 C6 147.3(3) . .
O232 Ag15 C6 119.3(4) . .
O12 Ag15 O162 106.1(3) . .
O232 Ag15 O162 99.2(3) . .
C6 Ag15 O162 84.2(3) . .
O12 Ag15 C5 125.7(4) . .
O232 Ag15 C5 144.1(4) . .
C6 Ag15 C5 26.9(3) . .
O162 Ag15 C5 73.3(3) . .
O12 Ag15 Ag14 151.4(2) . .
O232 Ag15 Ag14 74.4(3) . .
C6 Ag15 Ag14 45.9(3) . .
O162 Ag15 Ag14 100.2(2) . .
C5 Ag15 Ag14 72.6(3) . .
O12 Ag15 Ag18 78.9(2) . .
O232 Ag15 Ag18 169.2(3) . .
C6 Ag15 Ag18 71.3(3) . .
O162 Ag15 Ag18 83.6(2) . .
C5 Ag15 Ag18 46.7(3) . .
Ag14 Ag15 Ag18 115.58(4) . .
C6 Ag16 O121 161.0(4) . .
C6 Ag16 O101 119.3(4) . .
O121 Ag16 O101 79.7(3) . .
C6 Ag16 Ag14 47.4(3) . .
O121 Ag16 Ag14 150.0(3) . .
O101 Ag16 Ag14 73.4(2) . .
C6 Ag16 Ag21 70.3(3) . .
O121 Ag16 Ag21 90.9(2) . .
O101 Ag16 Ag21 168.9(2) . .
Ag14 Ag16 Ag21 117.02(4) . .
C6 Ag16 Ag19 59.5(3) . .
O121 Ag16 Ag19 108.9(2) . .
O101 Ag16 Ag19 129.0(2) . .
Ag14 Ag16 Ag19 79.22(4) . .
Ag21 Ag16 Ag19 59.60(3) . .
C6 Ag16 Ag12 80.9(3) . .
O121 Ag16 Ag12 112.9(2) . .
O101 Ag16 Ag12 58.3(2) . .
Ag14 Ag16 Ag12 63.08(3) . .
Ag21 Ag16 Ag12 121.65(4) . .
Ag19 Ag16 Ag12 138.11(4) . .
C5 Ag17 O172 143.9(4) . .
C5 Ag17 O62 135.8(4) . .
O172 Ag17 O62 79.1(3) . .
C5 Ag17 Ag18 52.9(4) . .
O172 Ag17 Ag18 160.9(3) . .
O62 Ag17 Ag18 82.9(2) . .
C5 Ag17 Ag13 57.4(3) . .
O172 Ag17 Ag13 89.8(2) . .
O62 Ag17 Ag13 143.1(2) . .
Ag18 Ag17 Ag13 100.78(4) . .
C5 Ag17 Ag21 51.5(3) . .
O172 Ag17 Ag21 126.9(3) . .
O62 Ag17 Ag21 120.0(2) . .
Ag18 Ag17 Ag21 68.49(4) . .
Ag13 Ag17 Ag21 94.88(4) . .
O11 Ag18 C5 139.2(4) . .
O11 Ag18 O61 81.1(3) . .
C5 Ag18 O61 131.4(4) . .
O11 Ag18 Ag17 143.3(2) . .
C5 Ag18 Ag17 49.1(3) . .
O61 Ag18 Ag17 82.5(2) . .
O11 Ag18 Ag15 81.0(2) . .
C5 Ag18 Ag15 58.4(3) . .
O61 Ag18 Ag15 139.8(2) . .
Ag17 Ag18 Ag15 90.91(4) . .
O11 Ag18 Ag19 102.2(2) . .
C5 Ag18 Ag19 64.2(3) . .
O61 Ag18 Ag19 148.5(2) . .
Ag17 Ag18 Ag19 108.86(4) . .
Ag15 Ag18 Ag19 70.88(3) . .
O11 Ag18 Ag20 59.7(2) . .
C5 Ag18 Ag20 118.7(3) . .
O61 Ag18 Ag20 104.4(2) . .
Ag17 Ag18 Ag20 156.91(5) . .
Ag15 Ag18 Ag20 97.04(4) . .
Ag19 Ag18 Ag20 54.55(3) . .
O11 Ag18 Ag21 156.1(2) . .
C5 Ag18 Ag21 47.4(3) . .
O61 Ag18 Ag21 109.6(2) . .
Ag17 Ag18 Ag21 60.62(4) . .
Ag15 Ag18 Ag21 101.10(4) . .
Ag19 Ag18 Ag21 57.35(3) . .
Ag20 Ag18 Ag21 96.49(4) . .
C8 Ag19 O31 130.5(4) . .
C8 Ag19 O22 130.6(4) . .
O31 Ag19 O22 86.9(3) . .
C8 Ag19 Ag20 50.8(3) . .
O31 Ag19 Ag20 80.0(2) . .
O22 Ag19 Ag20 136.7(2) . .
C8 Ag19 Ag22 50.3(3) . .
O31 Ag19 Ag22 141.5(2) . .
O22 Ag19 Ag22 80.4(2) . .
Ag20 Ag19 Ag22 84.79(4) . .
C8 Ag19 Ag18 61.1(3) . .
O31 Ag19 Ag18 96.2(2) . .
O22 Ag19 Ag18 158.8(2) . .
Ag20 Ag19 Ag18 64.25(3) . .
Ag22 Ag19 Ag18 108.63(4) . .
C8 Ag19 Ag21 62.6(3) . .
O31 Ag19 Ag21 150.8(2) . .
O22 Ag19 Ag21 101.9(2) . .
Ag20 Ag19 Ag21 109.56(4) . .
Ag22 Ag19 Ag21 67.71(3) . .
Ag18 Ag19 Ag21 66.05(3) . .
C8 Ag19 Ag16 116.5(3) . .
O31 Ag19 Ag16 110.6(2) . .
O22 Ag19 Ag16 58.2(2) . .
Ag20 Ag19 Ag16 163.76(5) . .
Ag22 Ag19 Ag16 93.14(4) . .
Ag18 Ag19 Ag16 101.51(4) . .
Ag21 Ag19 Ag16 55.23(3) . .
C8 Ag20 O32 136.9(4) . .
C8 Ag20 O181 108.3(4) . 1_455
O32 Ag20 O181 113.5(4) . 1_455
C8 Ag20 Ag19 51.8(3) . .
O32 Ag20 Ag19 85.2(2) . .
O181 Ag20 Ag19 155.3(3) 1_455 .
C8 Ag20 Ag1 54.5(3) . 1_455
O32 Ag20 Ag1 150.4(2) . 1_455
O181 Ag20 Ag1 72.3(3) 1_455 1_455
Ag19 Ag20 Ag1 99.75(4) . 1_455
C8 Ag20 Ag18 59.7(3) . .
O32 Ag20 Ag18 104.2(2) . .
O181 Ag20 Ag18 97.2(3) 1_455 .
Ag19 Ag20 Ag18 61.20(3) . .
Ag1 Ag20 Ag18 103.66(4) 1_455 .
O141 Ag21 O122 86.1(4) . .
O141 Ag21 C5 116.4(4) . .
O122 Ag21 C5 137.1(4) . .
O141 Ag21 C7 115.2(4) . .
O122 Ag21 C7 97.0(3) . .
C5 Ag21 C7 104.2(4) . .
O141 Ag21 Ag16 109.2(3) . .
O122 Ag21 Ag16 72.0(2) . .
C5 Ag21 Ag16 66.3(3) . .
C7 Ag21 Ag16 133.3(3) . .
O141 Ag21 Ag19 174.4(3) . .
O122 Ag21 Ag19 91.9(2) . .
C5 Ag21 Ag19 62.1(3) . .
C7 Ag21 Ag19 70.2(3) . .
Ag16 Ag21 Ag19 65.18(3) . .
O141 Ag21 Ag17 80.8(3) . .
O122 Ag21 Ag17 161.7(2) . .
C5 Ag21 Ag17 43.3(3) . .
C7 Ag21 Ag17 100.1(3) . .
Ag16 Ag21 Ag17 100.37(4) . .
Ag19 Ag21 Ag17 99.90(4) . .
O141 Ag21 Ag23 82.1(3) . .
O122 Ag21 Ag23 118.6(2) . .
C5 Ag21 Ag23 101.2(3) . .
C7 Ag21 Ag23 40.3(3) . .
Ag16 Ag21 Ag23 165.73(5) . .
Ag19 Ag21 Ag23 103.41(4) . .
Ag17 Ag21 Ag23 72.29(4) . .
O141 Ag21 Ag18 126.5(3) . .
O122 Ag21 Ag18 145.9(2) . .
C5 Ag21 Ag18 42.9(3) . .
C7 Ag21 Ag18 62.2(2) . .
Ag16 Ag21 Ag18 101.77(4) . .
Ag19 Ag21 Ag18 56.60(3) . .
Ag17 Ag21 Ag18 50.89(3) . .
Ag23 Ag21 Ag18 64.03(3) . .
O141 Ag21 Ag24 84.1(3) . .
O122 Ag21 Ag24 68.5(2) . .
C5 Ag21 Ag24 144.4(3) . .
C7 Ag21 Ag24 40.8(2) . .
Ag16 Ag21 Ag24 137.17(4) . .
Ag19 Ag21 Ag24 100.05(4) . .
Ag17 Ag21 Ag24 122.18(4) . .
Ag23 Ag21 Ag24 50.42(3) . .
Ag18 Ag21 Ag24 101.60(4) . .
O141 Ag21 Ag22 126.9(3) . .
O122 Ag21 Ag22 53.9(2) . .
C5 Ag21 Ag22 116.7(3) . .
C7 Ag21 Ag22 50.4(3) . .
Ag16 Ag21 Ag22 91.32(4) . .
Ag19 Ag21 Ag22 54.85(3) . .
Ag17 Ag21 Ag22 144.22(4) . .
Ag23 Ag21 Ag22 88.32(4) . .
Ag18 Ag21 Ag22 93.75(4) . .
Ag24 Ag21 Ag22 51.78(3) . .
O111 Ag22 C8 147.7(3) . .
O111 Ag22 O21 83.7(3) . .
C8 Ag22 O21 127.3(4) . .
O111 Ag22 C7 124.9(3) . .
C8 Ag22 C7 27.5(3) . .
O21 Ag22 C7 150.2(3) . .
O111 Ag22 Ag24 80.9(2) . .
C8 Ag22 Ag24 73.5(3) . .
O21 Ag22 Ag24 152.2(3) . .
C7 Ag22 Ag24 46.1(2) . .
O111 Ag22 Ag19 163.22(19) . .
C8 Ag22 Ag19 49.0(3) . .
O21 Ag22 Ag19 79.7(2) . .
C7 Ag22 Ag19 71.1(2) . .
Ag24 Ag22 Ag19 113.03(4) . .
O111 Ag22 Ag1 100.1(2) . 1_455
C8 Ag22 Ag1 52.2(3) . 1_455
O21 Ag22 Ag1 138.2(3) . 1_455
C7 Ag22 Ag1 52.5(3) . 1_455
Ag24 Ag22 Ag1 67.78(4) . 1_455
Ag19 Ag22 Ag1 94.13(4) . 1_455
O111 Ag22 Ag21 127.1(2) . .
C8 Ag22 Ag21 56.8(3) . .
O21 Ag22 Ag21 109.1(2) . .
C7 Ag22 Ag21 49.2(3) . .
Ag24 Ag22 Ag21 64.09(4) . .
Ag19 Ag22 Ag21 57.44(3) . .
Ag1 Ag22 Ag21 101.48(4) 1_455 .
O3W Ag23 C7 68.5(7) . .
O3W Ag23 O81 99.4(7) . .
C7 Ag23 O81 164.2(4) . .
O3W Ag23 O142 153.8(7) . .
C7 Ag23 O142 117.0(4) . .
O81 Ag23 O142 78.5(3) . .
O3W Ag23 Ag24 98.8(6) . .
C7 Ag23 Ag24 50.2(3) . .
O81 Ag23 Ag24 125.6(3) . .
O142 Ag23 Ag24 103.6(2) . .
O3W Ag23 Ag2 61.7(8) . 1_455
C7 Ag23 Ag2 84.5(3) . 1_455
O81 Ag23 Ag2 80.6(3) . 1_455
O142 Ag23 Ag2 141.5(2) . 1_455
Ag24 Ag23 Ag2 64.44(4) . 1_455
O3W Ag23 Ag21 113.2(7) . .
C7 Ag23 Ag21 51.9(3) . .
O81 Ag23 Ag21 143.6(3) . .
O142 Ag23 Ag21 65.18(19) . .
Ag24 Ag23 Ag21 66.35(4) . .
Ag2 Ag23 Ag21 128.50(4) 1_455 .
C7 Ag24 O201 126.9(4) . 1_455
C7 Ag24 O112 140.7(4) . .
O201 Ag24 O112 91.2(3) 1_455 .
C7 Ag24 Ag23 48.0(3) . .
O201 Ag24 Ag23 80.6(3) 1_455 .
O112 Ag24 Ag23 171.3(2) . .
C7 Ag24 Ag22 59.6(3) . .
O201 Ag24 Ag22 154.8(3) 1_455 .
O112 Ag24 Ag22 81.9(2) . .
Ag23 Ag24 Ag22 106.70(4) . .
C7 Ag24 Ag2 81.9(3) . 1_455
O201 Ag24 Ag2 84.8(3) 1_455 1_455
O112 Ag24 Ag2 114.7(2) . 1_455
Ag23 Ag24 Ag2 62.18(4) . 1_455
Ag22 Ag24 Ag2 120.13(5) . 1_455
C7 Ag24 Ag6 133.0(3) . 1_455
O201 Ag24 Ag6 79.1(2) 1_455 1_455
O112 Ag24 Ag6 55.1(2) . 1_455
Ag23 Ag24 Ag6 120.01(5) . 1_455
Ag22 Ag24 Ag6 115.11(5) . 1_455
Ag2 Ag24 Ag6 60.20(4) 1_455 1_455
C7 Ag24 Ag21 50.1(3) . .
O201 Ag24 Ag21 100.3(3) 1_455 .
O112 Ag24 Ag21 121.4(2) . .
Ag23 Ag24 Ag21 63.23(4) . .
Ag22 Ag24 Ag21 64.13(3) . .
Ag2 Ag24 Ag21 123.37(4) 1_455 .
Ag6 Ag24 Ag21 176.39(5) 1_455 .
N1 Ag25 O91 144.6(6) . .
N1 Ag25 O72 116.2(4) . .
O91 Ag25 O72 73.4(3) . .
N1 Ag25 O111 137.8(6) . 1_655
O91 Ag25 O111 76.5(3) . 1_655
O72 Ag25 O111 76.8(3) . 1_655
N2 Ag26 O202 145.6(4) . .
N2 Ag26 O51 99.5(4) . .
O202 Ag26 O51 75.6(3) . .
N3 Ag27 O151 140.3(4) . .
N3 Ag27 O42 130.8(5) . .
O151 Ag27 O42 80.7(3) . .
N3 Ag27 O221 129.3(4) . .
O151 Ag27 O221 75.3(3) . .
O42 Ag27 O221 76.0(3) . .
N4 Ag28 O102 149.6(5) . .
N4 Ag28 O231 125.0(5) . .
O102 Ag28 O231 75.3(3) . .
N4 Ag28 O192 125.4(4) . .
O102 Ag28 O192 78.8(3) . .
O231 Ag28 O192 75.4(3) . .
N5 Ag29 O121 169.3(6) . .
N5 Ag29 O101 110.7(5) . .
O121 Ag29 O101 77.9(3) . .
N6 Ag30 O142 149.5(6) . .
N6 Ag30 O62 132.3(6) . .
O142 Ag30 O62 78.2(3) . .
N7 Ag31 O181 142.9(6) . 1_455
N7 Ag31 O61 101.4(6) . .
O181 Ag31 O61 110.8(3) 1_455 .
C2 C1 Ag2 169.5(12) . .
C2 C1 Ag4 95.3(10) . .
Ag2 C1 Ag4 81.9(4) . .
C2 C1 Ag6 97.1(10) . .
Ag2 C1 Ag6 91.4(4) . .
Ag4 C1 Ag6 139.8(5) . .
C2 C1 Ag1 79.0(8) . .
Ag2 C1 Ag1 90.7(4) . .
Ag4 C1 Ag1 86.8(4) . .
Ag6 C1 Ag1 133.1(5) . .
C1 C2 Ag3 142.6(10) . .
C1 C2 Ag7 124.1(11) . .
Ag3 C2 Ag7 79.4(4) . .
C1 C2 Ag5 128.1(10) . .
Ag3 C2 Ag5 81.3(5) . .
Ag7 C2 Ag5 79.0(4) . .
C1 C2 Ag1 75.4(8) . .
Ag3 C2 Ag1 77.2(3) . .
Ag7 C2 Ag1 156.5(6) . .
Ag5 C2 Ag1 99.7(5) . .
C1 C2 Ag4 59.7(8) . .
Ag3 C2 Ag4 137.5(6) . .
Ag7 C2 Ag4 120.9(4) . .
Ag5 C2 Ag4 68.5(3) . .
Ag1 C2 Ag4 79.1(3) . .
C4 C3 Ag9 135.6(11) . .
C4 C3 Ag8 146.5(11) . .
Ag9 C3 Ag8 77.3(4) . .
C4 C3 Ag10 88.5(8) . .
Ag9 C3 Ag10 115.5(5) . .
Ag8 C3 Ag10 78.8(4) . .
C4 C3 Ag13 69.3(8) . .
Ag9 C3 Ag13 77.3(4) . .
Ag8 C3 Ag13 137.6(5) . .
Ag10 C3 Ag13 82.3(3) . .
C3 C4 Ag11 139.1(10) . .
C3 C4 Ag12 136.5(10) . .
Ag11 C4 Ag12 83.2(4) . .
C3 C4 Ag13 84.2(8) . .
Ag11 C4 Ag13 117.5(5) . .
Ag12 C4 Ag13 81.5(4) . .
C3 C4 Ag10 65.1(8) . .
Ag11 C4 Ag10 147.2(6) . .
Ag12 C4 Ag10 72.1(3) . .
Ag13 C4 Ag10 80.6(3) . .
C6 C5 Ag17 143.9(11) . .
C6 C5 Ag18 134.7(11) . .
Ag17 C5 Ag18 78.0(4) . .
C6 C5 Ag21 106.2(9) . .
Ag17 C5 Ag21 85.2(4) . .
Ag18 C5 Ag21 89.7(4) . .
C6 C5 Ag15 69.1(8) . .
Ag17 C5 Ag15 118.2(5) . .
Ag18 C5 Ag15 74.9(4) . .
Ag21 C5 Ag15 147.4(5) . .
C6 C5 Ag13 66.0(8) . .
Ag17 C5 Ag13 79.9(4) . .
Ag18 C5 Ag13 134.2(5) . .
Ag21 C5 Ag13 127.6(5) . .
Ag15 C5 Ag13 81.3(4) . .
C5 C6 Ag14 160.7(10) . .
C5 C6 Ag16 116.5(9) . .
Ag14 C6 Ag16 82.6(4) . .
C5 C6 Ag13 87.2(8) . .
Ag14 C6 Ag13 87.0(4) . .
Ag16 C6 Ag13 114.5(5) . .
C5 C6 Ag15 84.1(8) . .
Ag14 C6 Ag15 77.4(3) . .
Ag16 C6 Ag15 148.0(5) . .
Ag13 C6 Ag15 89.3(3) . .
C8 C7 Ag23 142.5(10) . .
C8 C7 Ag24 135.6(10) . .
Ag23 C7 Ag24 81.8(4) . .
C8 C7 Ag21 90.0(8) . .
Ag23 C7 Ag21 87.8(4) . .
Ag24 C7 Ag21 89.1(4) . .
C8 C7 Ag1 72.6(8) . 1_455
Ag23 C7 Ag1 118.1(5) . 1_455
Ag24 C7 Ag1 89.8(4) . 1_455
Ag21 C7 Ag1 153.7(5) . 1_455
C8 C7 Ag22 61.7(8) . .
Ag23 C7 Ag22 153.5(5) . .
Ag24 C7 Ag22 74.4(3) . .
Ag21 C7 Ag22 80.4(3) . .
Ag1 C7 Ag22 74.0(3) 1_455 .
C7 C8 Ag20 140.5(10) . .
C7 C8 Ag19 137.1(10) . .
Ag20 C8 Ag19 77.4(4) . .
C7 C8 Ag22 90.8(9) . .
Ag20 C8 Ag22 118.1(5) . .
Ag19 C8 Ag22 80.8(4) . .
C7 C8 Ag1 79.9(8) . 1_455
Ag20 C8 Ag1 78.9(4) . 1_455
Ag19 C8 Ag1 138.5(5) . 1_455
Ag22 C8 Ag1 81.1(3) . 1_455
C11 O11 Ag18 124.1(8) . .
C11 O12 Ag15 127.3(8) . .
C21 O21 Ag22 123.6(8) . .
C21 O22 Ag19 121.9(7) . .
C31 O31 Ag19 123.4(7) . .
C31 O32 Ag20 119.3(8) . .
C41 O41 Ag8 117.6(7) . .
C41 O42 Ag9 124.9(8) . .
C41 O42 Ag27 118.6(8) . .
Ag9 O42 Ag27 99.6(3) . .
C51 O51 Ag8 119.6(8) . .
C51 O51 Ag26 132.0(8) . .
Ag8 O51 Ag26 105.4(3) . .
C51 O52 Ag10 128.9(9) . .
C61 O61 Ag18 118.1(8) . .
C61 O61 Ag31 135.2(8) . .
Ag18 O61 Ag31 97.4(3) . .
C61 O62 Ag17 124.3(8) . .
C61 O62 Ag30 124.1(8) . .
Ag17 O62 Ag30 95.3(3) . .
C71 O71 Ag7 121.1(7) . .
C71 O72 Ag3 120.3(7) . .
C71 O72 Ag25 142.6(8) . .
Ag3 O72 Ag25 92.7(3) . .
C81 O81 Ag23 122.9(9) . .
C81 O82 Ag2 127.3(8) . 1_455
C91 O91 Ag3 119.9(8) . .
C91 O91 Ag25 144.7(8) . .
Ag3 O91 Ag25 95.4(3) . .
C91 O92 Ag1 118.6(8) . .
C101 O101 Ag16 134.7(9) . .
C101 O101 Ag29 136.2(9) . .
Ag16 O101 Ag29 89.0(3) . .
C101 O102 Ag28 130.2(8) . .
C101 O102 Ag14 108.2(8) . .
Ag28 O102 Ag14 96.0(3) . .
C111 O111 Ag22 123.2(7) . .
C111 O111 Ag25 141.1(7) . 1_455
Ag22 O111 Ag25 95.5(3) . 1_455
C111 O112 Ag24 122.8(7) . .
C121 O121 Ag16 115.2(8) . .
C121 O121 Ag29 138.1(9) . .
Ag16 O121 Ag29 99.3(3) . .
C121 O122 Ag21 129.6(8) . .
C131 O131 Ag7 123.3(8) . .
C131 O132 Ag6 124.9(8) . .
C141 O141 Ag21 117.0(10) . .
C141 O142 Ag30 128.6(9) . .
C141 O142 Ag23 121.1(9) . .
Ag30 O142 Ag23 107.4(4) . .
C151 O151 Ag4 123.3(8) . .
C151 O151 Ag27 133.9(8) . .
Ag4 O151 Ag27 99.9(3) . .
C151 O152 Ag5 120.6(8) . .
C161 O161 Ag9 121.0(8) . .
C161 O162 Ag13 133.5(8) . .
C161 O162 Ag15 136.7(8) . .
Ag13 O162 Ag15 86.9(3) . .
C171 O171 Ag13 134.5(9) . .
C171 O172 Ag17 117.0(8) . .
C181 O181 Ag20 124.7(9) . 1_655
C181 O181 Ag31 122.3(9) . 1_655
Ag20 O181 Ag31 109.9(4) 1_655 1_655
C181 O182 Ag1 116.8(9) . .
C191 O191 Ag5 131.4(8) . .
C191 O192 Ag11 117.8(8) . .
C191 O192 Ag28 133.7(8) . .
Ag11 O192 Ag28 98.5(3) . .
C201 O201 Ag24 124.9(9) . 1_655
C201 O202 Ag6 127.4(9) . .
C201 O202 Ag26 123.5(9) . .
Ag6 O202 Ag26 105.7(4) . .
C211 O211 Ag10 131.7(9) . .
C211 O212 Ag12 116.9(8) . .
C221 O221 Ag4 117.1(9) . .
C221 O221 Ag27 142.6(10) . .
Ag4 O221 Ag27 95.3(4) . .
C231 O231 Ag14 115.5(8) . .
C231 O231 Ag28 128.9(8) . .
Ag14 O231 Ag28 99.6(3) . .
C231 O232 Ag15 130.5(9) . .
O12 C11 O11 128.6(12) . .
O12 C11 C12 115.5(13) . .
O11 C11 C12 115.9(12) . .
F13 C12 F11 106.5(15) . .
F13 C12 F12 106.5(13) . .
F11 C12 F12 106.1(13) . .
F13 C12 C11 113.1(13) . .
F11 C12 C11 114.5(13) . .
F12 C12 C11 109.5(14) . .
O22 C21 O21 129.7(11) . .
O22 C21 C22 115.6(12) . .
O21 C21 C22 114.6(13) . .
F23 C22 F22 111.0(17) . .
F23 C22 F21 104(2) . .
F22 C22 F21 101.0(14) . .
F23 C22 C21 115.3(15) . .
F22 C22 C21 114(2) . .
F21 C22 C21 109.6(16) . .
O32 C31 O31 130.7(11) . .
O32 C31 C32 114.1(13) . .
O31 C31 C32 115.1(13) . .
F32 C32 F33 103.9(15) . .
F32 C32 F31 103.3(15) . .
F33 C32 F31 103.3(13) . .
F32 C32 C31 113.2(14) . .
F33 C32 C31 114.0(15) . .
F31 C32 C31 117.6(15) . .
O41 C41 O42 129.1(11) . .
O41 C41 C42 116.3(12) . .
O42 C41 C42 114.6(12) . .
F41 C42 F42 107.1(12) . .
F41 C42 F43 106.0(11) . .
F42 C42 F43 105.4(11) . .
F41 C42 C41 114.4(12) . .
F42 C42 C41 113.0(12) . .
F43 C42 C41 110.3(12) . .
O52 C51 O51 130.2(12) . .
O52 C51 C52 116.4(12) . .
O51 C51 C52 112.9(12) . .
F51 C52 F52 108.5(12) . .
F51 C52 F53 106.9(12) . .
F52 C52 F53 103.7(12) . .
F51 C52 C51 113.6(13) . .
F52 C52 C51 114.8(13) . .
F53 C52 C51 108.5(12) . .
O62 C61 O61 128.9(11) . .
O62 C61 C62 115.4(12) . .
O61 C61 C62 115.7(13) . .
F62 C62 F61 108.6(14) . .
F62 C62 F63 108.8(13) . .
F61 C62 F63 106.2(13) . .
F62 C62 C61 113.9(14) . .
F61 C62 C61 107.9(12) . .
F63 C62 C61 111.2(13) . .
O72 C71 O71 129.6(10) . .
O72 C71 C72 115.9(11) . .
O71 C71 C72 114.5(11) . .
F73 C72 F72 107.3(15) . .
F73 C72 F71 107.5(19) . .
F72 C72 F71 102.9(16) . .
F73 C72 C71 115.4(16) . .
F72 C72 C71 109.6(19) . .
F71 C72 C71 113.2(14) . .
O81 C81 O82 128.7(12) . .
O81 C81 C82 119.2(14) . .
O82 C81 C82 112.1(13) . .
F82 C82 F83 106.2(15) . .
F82 C82 F81 105.0(13) . .
F83 C82 F81 105.8(16) . .
F82 C82 C81 111.6(17) . .
F83 C82 C81 115.9(14) . .
F81 C82 C81 111.6(15) . .
O91 C91 O92 127.1(11) . .
O91 C91 C92 117.9(13) . .
O92 C91 C92 115.0(13) . .
F91 C92 F92 108.2(13) . .
F91 C92 F93 105.1(13) . .
F92 C92 F93 106.1(13) . .
F91 C92 C91 114.5(14) . .
F92 C92 C91 112.9(14) . .
F93 C92 C91 109.5(12) . .
O101 C101 O102 125.8(11) . .
O101 C101 C102 117.9(14) . .
O102 C101 C102 116.3(14) . .
F103 C102 F102 105.1(18) . .
F103 C102 F101 105.0(16) . .
F102 C102 F101 101.1(16) . .
F103 C102 C101 113.9(18) . .
F102 C102 C101 117.7(17) . .
F101 C102 C101 112.5(18) . .
O111 C111 O112 128.8(10) . .
O111 C111 C112 115.2(12) . .
O112 C111 C112 116.0(12) . .
F111 C112 F113 108.6(11) . .
F111 C112 F112 109.2(12) . .
F113 C112 F112 105.0(10) . .
F111 C112 C111 112.5(11) . .
F113 C112 C111 108.9(11) . .
F112 C112 C111 112.3(12) . .
O122 C121 O121 129.2(12) . .
O122 C121 C122 117.8(15) . .
O121 C121 C122 113.0(14) . .
F123 C122 F122 108.1(18) . .
F123 C122 F121 105.9(16) . .
F122 C122 F121 103.8(15) . .
F123 C122 C121 114.9(16) . .
F122 C122 C121 113.7(16) . .
F121 C122 C121 109.5(19) . .
O132 C131 O131 129.9(11) . .
O132 C131 C132 115.1(13) . .
O131 C131 C132 114.7(12) . .
F131 C132 F132 109.9(16) . .
F131 C132 F133 101.5(14) . .
F132 C132 F133 101.2(14) . .
F131 C132 C131 113.9(15) . .
F132 C132 C131 117.5(15) . .
F133 C132 C131 110.9(15) . .
O142 C141 O141 127.9(14) . .
O142 C141 C142 116.0(15) . .
O141 C141 C142 116.2(16) . .
F142 C142 F143 107.0(18) . .
F142 C142 F141 104.8(17) . .
F143 C142 F141 102.0(15) . .
F142 C142 C141 118.1(17) . .
F143 C142 C141 115.4(18) . .
F141 C142 C141 107.9(17) . .
O151 C151 O152 127.6(12) . .
O151 C151 C152 119.2(13) . .
O152 C151 C152 113.1(13) . .
F151 C152 F152 107.6(13) . .
F151 C152 F153 104.6(12) . .
F152 C152 F153 101.5(12) . .
F151 C152 C151 115.8(13) . .
F152 C152 C151 115.0(13) . .
F153 C152 C151 111.1(13) . .
O162 C161 O161 123.4(11) . .
O162 C161 C162 116.9(12) . .
O161 C161 C162 119.6(12) . .
F163 C162 F161 112.1(16) . .
F163 C162 F162 104.2(14) . .
F161 C162 F162 102.4(12) . .
F163 C162 C161 114.9(12) . .
F161 C162 C161 111.9(14) . .
F162 C162 C161 110.2(15) . .
O171 C171 O172 129.7(12) . .
O171 C171 C172 115.9(14) . .
O172 C171 C172 114.4(13) . .
F173 C172 F171 108.7(16) . .
F173 C172 F172 106.9(14) . .
F171 C172 F172 103.5(14) . .
F173 C172 C171 116.8(15) . .
F171 C172 C171 109.5(15) . .
F172 C172 C171 110.6(15) . .
O182 C181 O181 126.0(13) . .
O182 C181 C182 119.5(14) . .
O181 C181 C182 114.4(13) . .
F181 C182 F183 107.1(15) . .
F181 C182 F182 103.9(14) . .
F183 C182 F182 100.8(13) . .
F181 C182 C181 114.9(14) . .
F183 C182 C181 116.7(14) . .
F182 C182 C181 111.7(15) . .
O191 C191 O192 128.5(12) . .
O191 C191 C192 113.3(14) . .
O192 C191 C192 118.1(15) . .
F192 C192 F193 102(2) . .
F192 C192 F191 103(2) . .
F193 C192 F191 102.2(17) . .
F192 C192 C191 121(2) . .
F193 C192 C191 113(2) . .
F191 C192 C191 113(2) . .
O201 C201 O202 127.1(13) . .
O201 C201 C202 114.9(14) . .
O202 C201 C202 118.0(13) . .
F202 C202 F201 109.5(16) . .
F202 C202 F203 105.4(15) . .
F201 C202 F203 105.6(18) . .
F202 C202 C201 112.7(19) . .
F201 C202 C201 112.2(15) . .
F203 C202 C201 110.9(16) . .
O211 C211 O212 128.5(12) . .
O211 C211 C212 114.6(15) . .
O212 C211 C212 117.0(14) . .
F211 C212 F212 107.1(17) . .
F211 C212 F213 103.8(16) . .
F212 C212 F213 102.6(16) . .
F211 C212 C211 116.8(17) . .
F212 C212 C211 116.4(16) . .
F213 C212 C211 108.5(18) . .
O222 C221 O221 131.1(15) . .
O222 C221 C222 119.7(16) . .
O221 C221 C222 109.1(16) . .
F223 C222 F221 106.5(19) . .
F223 C222 F222 106.7(18) . .
F221 C222 F222 101.3(14) . .
F223 C222 C221 119.8(17) . .
F221 C222 C221 110.1(19) . .
F222 C222 C221 110.9(19) . .
O232 C231 O231 129.7(12) . .
O232 C231 C232 113.2(14) . .
O231 C231 C232 117.0(14) . .
F233 C232 F231 105.3(14) . .
F233 C232 F232 104.9(16) . .
F231 C232 F232 102.9(14) . .
F233 C232 C231 120.8(15) . .
F231 C232 C231 109.3(16) . .
F232 C232 C231 112.0(14) . .
C011 N1 Ag25 170.3(16) . .
C021 N2 Ag26 161.9(14) . .
C031 N3 Ag27 176.0(18) . .
C041 N4 Ag28 166.1(17) . .
C051 N5 Ag29 171(2) . .
C061 N6 Ag30 175(2) . .
C071 N7 Ag31 163(3) . .
N1 C011 C012 177(2) . .
C013 C012 C011 112.0(15) . .
N2 C021 C022 179(2) . .
C023 C022 C021 109.4(15) . .
N3 C031 C032 178(2) . .
C033 C032 C031 112.8(17) . .
N4 C041 C042 177(2) . .
C043 C042 C041 115(2) . .
N5 C051 C052 174(4) . .
C053 C052 C051 103(3) . .
N6 C061 C062 172(3) . .
C063 C062 C061 111(2) . .
N7 C071 C072 175(3) . .
C073 C072 C071 107.2(19) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 O182 2.387(9) .
Ag1 C8 2.513(11) 1_655
Ag1 O92 2.530(9) .
Ag1 C1 2.556(12) .
Ag1 C7 2.592(11) 1_655
Ag1 C2 2.593(11) .
Ag1 Ag3 2.9800(14) .
Ag1 Ag20 3.0271(13) 1_655
Ag1 Ag22 3.1395(14) 1_655
Ag1 Ag2 3.3435(16) .
Ag1 Ag4 3.3680(14) .
Ag2 C1 2.122(12) .
Ag2 O82 2.182(9) 1_655
Ag2 Ag4 2.9286(15) .
Ag2 Ag23 3.1136(17) 1_655
Ag2 Ag24 3.1759(17) 1_655
Ag2 Ag6 3.2225(16) .
Ag3 C2 2.149(13) .
Ag3 O91 2.280(8) .
Ag3 O72 2.280(8) .
Ag3 Ag7 2.8628(13) .
Ag3 Ag5 2.9347(16) .
Ag4 O221 2.301(9) .
Ag4 O151 2.301(8) .
Ag4 C1 2.339(12) .
Ag4 C2 2.697(12) .
Ag4 Ag5 2.8555(15) .
Ag4 Ag8 3.2210(15) .
Ag5 O152 2.217(9) .
Ag5 C2 2.350(13) .
Ag5 O191 2.404(10) .
Ag5 Ag7 2.9742(16) .
Ag5 Ag11 2.9875(16) .
Ag6 O132 2.262(8) .
Ag6 O202 2.360(9) .
Ag6 C1 2.373(13) .
Ag6 Ag7 3.0231(13) .
Ag6 Ag8 3.0343(14) .
Ag6 Ag24 3.2486(15) 1_655
Ag7 O131 2.258(8) .
Ag7 C2 2.328(12) .
Ag7 O71 2.457(8) .
Ag7 Ag8 3.0926(13) .
Ag7 Ag11 3.1568(14) .
Ag8 C3 2.239(12) .
Ag8 O51 2.282(8) .
Ag8 O41 2.355(7) .
Ag8 Ag9 2.7558(13) .
Ag8 Ag10 2.9508(14) .
Ag9 C3 2.171(12) .
Ag9 O161 2.202(9) .
Ag9 O42 2.347(8) .
Ag9 Ag13 3.0160(13) .
Ag10 O52 2.275(9) .
Ag10 O211 2.300(10) .
Ag10 C3 2.405(12) .
Ag10 C4 2.650(11) .
Ag10 Ag12 2.8841(14) .
Ag10 Ag13 3.3128(15) .
Ag11 C4 2.131(11) .
Ag11 O192 2.149(8) .
Ag11 Ag12 2.8868(14) .
Ag11 Ag14 3.2546(15) .
Ag12 C4 2.214(13) .
Ag12 O212 2.274(9) .
Ag12 O1W 2.443(9) .
Ag12 Ag13 3.0626(14) .
Ag12 Ag14 3.2350(15) .
Ag12 Ag16 3.2780(15) .
Ag13 O162 2.414(9) .
Ag13 C6 2.427(10) .
Ag13 C4 2.469(12) .
Ag13 O171 2.487(9) .
Ag13 C3 2.626(11) .
Ag13 C5 2.654(13) .
Ag13 Ag17 3.1028(14) .
Ag13 Ag14 3.1451(14) .
Ag14 C6 2.131(11) .
Ag14 O231 2.239(8) .
Ag14 O102 2.539(9) .
Ag14 O2W 2.549(9) .
Ag14 Ag16 2.8708(13) .
Ag14 Ag15 2.8976(14) .
Ag15 O12 2.245(9) .
Ag15 O232 2.329(9) .
Ag15 C6 2.481(11) .
Ag15 O162 2.598(9) .
Ag15 C5 2.642(13) .
Ag15 Ag18 2.9962(15) .
Ag16 C6 2.218(10) .
Ag16 O121 2.231(8) .
Ag16 O101 2.477(9) .
Ag16 Ag21 2.9140(14) .
Ag16 Ag19 3.2197(15) .
Ag17 C5 2.141(12) .
Ag17 O172 2.230(9) .
Ag17 O62 2.336(8) .
Ag17 Ag18 2.7701(15) .
Ag17 Ag21 3.1108(14) .
Ag18 O11 2.240(8) .
Ag18 C5 2.260(13) .
Ag18 O61 2.443(9) .
Ag18 Ag19 3.0340(14) .
Ag18 Ag20 3.1182(14) .
Ag18 Ag21 3.3212(15) .
Ag19 C8 2.269(11) .
Ag19 O31 2.305(8) .
Ag19 O22 2.320(8) .
Ag19 Ag20 2.8204(14) .
Ag19 Ag22 2.9683(13) .
Ag19 Ag21 3.0597(15) .
Ag20 C8 2.239(12) .
Ag20 O32 2.271(8) .
Ag20 O181 2.365(9) 1_455
Ag20 Ag1 3.0271(13) 1_455
Ag21 O141 2.263(10) .
Ag21 O122 2.438(9) .
Ag21 C5 2.445(12) .
Ag21 C7 2.577(12) .
Ag21 Ag23 3.2728(16) .
Ag21 Ag24 3.3578(15) .
Ag21 Ag22 3.3588(14) .
Ag22 O111 2.298(8) .
Ag22 C8 2.312(12) .
Ag22 O21 2.319(8) .
Ag22 C7 2.626(12) .
Ag22 Ag24 2.9328(14) .
Ag22 Ag1 3.1395(14) 1_455
Ag23 O3W 2.07(5) .
Ag23 C7 2.120(11) .
Ag23 O81 2.187(8) .
Ag23 O142 2.582(9) .
Ag23 Ag24 2.8254(15) .
Ag23 Ag2 3.1136(17) 1_455
Ag24 C7 2.193(11) .
Ag24 O201 2.268(10) 1_455
Ag24 O112 2.285(8) .
Ag24 Ag2 3.1759(16) 1_455
Ag24 Ag6 3.2486(15) 1_455
Ag25 N1 2.086(13) .
Ag25 O91 2.418(9) .
Ag25 O72 2.517(8) .
Ag25 O111 2.571(8) 1_655
Ag26 N2 2.211(13) .
Ag26 O202 2.470(10) .
Ag26 O51 2.599(8) .
Ag27 N3 2.101(11) .
Ag27 O151 2.423(9) .
Ag27 O42 2.478(9) .
Ag27 O221 2.586(10) .
Ag28 N4 2.146(13) .
Ag28 O102 2.362(9) .
Ag28 O231 2.528(9) .
Ag28 O192 2.543(9) .
Ag29 N5 2.045(16) .
Ag29 O121 2.327(9) .
Ag29 O101 2.479(9) .
Ag30 N6 2.118(13) .
Ag30 O142 2.331(9) .
Ag30 O62 2.445(10) .
Ag31 N7 2.22(2) .
Ag31 O181 2.402(11) 1_455
Ag31 O61 2.526(10) .
C1 C2 1.143(14) .
C3 C4 1.177(14) .
C5 C6 1.201(14) .
C7 C8 1.214(14) .
C7 Ag1 2.592(11) 1_455
C8 Ag1 2.513(11) 1_455
O11 C11 1.246(14) .
O12 C11 1.212(14) .
O21 C21 1.234(14) .
O22 C21 1.233(14) .
O31 C31 1.245(14) .
O32 C31 1.227(14) .
O41 C41 1.235(14) .
O42 C41 1.238(14) .
O51 C51 1.274(14) .
O52 C51 1.163(14) .
O61 C61 1.219(14) .
O62 C61 1.217(14) .
O71 C71 1.290(13) .
O72 C71 1.215(13) .
O81 C81 1.204(15) .
O82 C81 1.303(15) .
O82 Ag2 2.182(9) 1_455
O91 C91 1.224(14) .
O92 C91 1.248(14) .
O101 C101 1.191(14) .
O102 C101 1.263(14) .
O111 C111 1.244(14) .
O111 Ag25 2.571(8) 1_455
O112 C111 1.276(14) .
O121 C121 1.264(17) .
O122 C121 1.210(16) .
O131 C131 1.242(14) .
O132 C131 1.228(13) .
O141 C141 1.242(16) .
O142 C141 1.240(17) .
O151 C151 1.206(14) .
O152 C151 1.260(14) .
O161 C161 1.258(14) .
O162 C161 1.250(13) .
O171 C171 1.195(15) .
O172 C171 1.230(15) .
O181 C181 1.284(15) .
O181 Ag20 2.365(9) 1_655
O181 Ag31 2.402(11) 1_655
O182 C181 1.205(15) .
O191 C191 1.239(15) .
O192 C191 1.255(15) .
O201 C201 1.221(15) .
O201 Ag24 2.268(10) 1_655
O202 C201 1.266(15) .
O211 C211 1.202(15) .
O212 C211 1.217(15) .
O221 C221 1.283(17) .
O222 C221 1.154(18) .
O231 C231 1.245(15) .
O232 C231 1.233(15) .
C11 C12 1.530(14) .
C12 F13 1.283(17) .
C12 F11 1.294(17) .
C12 F12 1.315(18) .
C21 C22 1.515(14) .
C22 F23 1.201(19) .
C22 F22 1.25(3) .
C22 F21 1.33(3) .
C31 C32 1.514(14) .
C32 F32 1.203(18) .
C32 F33 1.229(18) .
C32 F31 1.230(18) .
C41 C42 1.538(13) .
C42 F41 1.303(16) .
C42 F42 1.314(15) .
C42 F43 1.336(17) .
C51 C52 1.539(14) .
C52 F51 1.274(18) .
C52 F52 1.313(16) .
C52 F53 1.351(16) .
C61 C62 1.563(13) .
C62 F62 1.245(17) .
C62 F61 1.307(18) .
C62 F63 1.310(17) .
C71 C72 1.520(14) .
C72 F73 1.22(2) .
C72 F72 1.29(3) .
C72 F71 1.304(19) .
C81 C82 1.501(14) .
C82 F82 1.27(2) .
C82 F83 1.272(17) .
C82 F81 1.28(2) .
C91 C92 1.533(14) .
C92 F91 1.271(18) .
C92 F92 1.283(18) .
C92 F93 1.325(16) .
C101 C102 1.484(14) .
C102 F103 1.18(2) .
C102 F102 1.23(2) .
C102 F101 1.24(2) .
C111 C112 1.533(13) .
C112 F111 1.270(14) .
C112 F113 1.315(14) .
C112 F112 1.316(15) .
C121 C122 1.528(14) .
C122 F123 1.24(2) .
C122 F122 1.27(2) .
C122 F121 1.31(3) .
C131 C132 1.536(14) .
C132 F131 1.193(19) .
C132 F132 1.217(18) .
C132 F133 1.34(2) .
C141 C142 1.509(15) .
C142 F142 1.23(2) .
C142 F143 1.28(2) .
C142 F141 1.31(2) .
C151 C152 1.487(14) .
C152 F151 1.263(16) .
C152 F152 1.318(16) .
C152 F153 1.370(17) .
C161 C162 1.497(14) .
C162 F163 1.244(15) .
C162 F161 1.291(18) .
C162 F162 1.36(2) .
C171 C172 1.535(15) .
C172 F173 1.260(19) .
C172 F171 1.295(19) .
C172 F172 1.33(2) .
C181 C182 1.480(14) .
C182 F181 1.244(16) .
C182 F183 1.255(17) .
C182 F182 1.29(2) .
C191 C192 1.487(14) .
C192 F192 1.20(2) .
C192 F193 1.20(3) .
C192 F191 1.22(3) .
C201 C202 1.519(15) .
C202 F202 1.25(2) .
C202 F201 1.29(2) .
C202 F203 1.32(2) .
C211 C212 1.505(14) .
C212 F211 1.22(2) .
C212 F212 1.25(2) .
C212 F213 1.31(2) .
C221 C222 1.533(16) .
C222 F223 1.27(2) .
C222 F221 1.31(3) .
C222 F222 1.34(2) .
C231 C232 1.512(14) .
C232 F233 1.238(19) .
C232 F231 1.30(2) .
C232 F232 1.307(19) .
N1 C011 1.147(13) .
N2 C021 1.139(13) .
N3 C031 1.140(13) .
N4 C041 1.120(13) .
N5 C051 1.141(14) .
N6 C061 1.130(13) .
N7 C071 1.149(15) .
C011 C012 1.502(15) .
C012 C013 1.415(17) .
C021 C022 1.477(15) .
C022 C023 1.450(16) .
C031 C032 1.511(15) .
C032 C033 1.426(17) .
C041 C042 1.504(16) .
C042 C043 1.416(18) .
C051 C052 1.521(17) .
C052 C053 1.423(18) .
C061 C062 1.502(16) .
C062 C063 1.370(18) .
C071 C072 1.502(16) .
C072 C073 1.447(18) .
