#------------------------------------------------------------------------------
#$Date: 2016-02-16 22:30:59 +0200 (Tue, 16 Feb 2016) $
#$Revision: 176467 $
#$URL: svn://www.crystallography.net/cod/cif/4/11/56/4115642.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4115642
loop_
_publ_author_name
'Quan-Ming Wang'
'Thomas C. W. Mak'
_publ_section_title
;
 Argentophilicity and Solvent-Induced Structural Diversity in Double Salts
 of Silver Acetylide with Silver Perfluoroalkyl Carboxylates
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              7594
_journal_page_last               7600
_journal_paper_doi               10.1021/ja0043441
_journal_volume                  123
_journal_year                    2001
_chemical_formula_sum            'C32 H19 Ag12 F50 O29.5'
_chemical_formula_weight         3119.91
_chemical_name_systematic
;
 ?
;
_space_group_IT_number           2
_symmetry_cell_setting           triclinic
_symmetry_space_group_name_Hall  '-P 1'
_symmetry_space_group_name_H-M   'P -1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                111.716(2)
_cell_angle_beta                 94.238(2)
_cell_angle_gamma                104.719(2)
_cell_formula_units_Z            2
_cell_length_a                   15.6000(12)
_cell_length_b                   16.9494(13)
_cell_length_c                   17.1426(13)
_cell_measurement_temperature    293(2)
_cell_volume                     4001.1(5)
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      293(2)
_diffrn_measured_fraction_theta_full 0.976
_diffrn_measured_fraction_theta_max 0.976
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0374
_diffrn_reflns_av_sigmaI/netI    0.2202
_diffrn_reflns_limit_h_max       20
_diffrn_reflns_limit_h_min       -20
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_l_max       22
_diffrn_reflns_limit_l_min       -22
_diffrn_reflns_number            27111
_diffrn_reflns_theta_full        28.05
_diffrn_reflns_theta_max         28.05
_diffrn_reflns_theta_min         1.61
_exptl_absorpt_coefficient_mu    3.051
_exptl_absorpt_correction_T_max  1.000
_exptl_absorpt_correction_T_min  0.756
_exptl_absorpt_correction_type   SADABS
_exptl_crystal_colour            colorless
_exptl_crystal_density_diffrn    2.590
_exptl_crystal_description       'rhombic plate'
_exptl_crystal_F_000             2922
_exptl_crystal_size_max          0.28
_exptl_crystal_size_mid          0.21
_exptl_crystal_size_min          0.11
_refine_diff_density_max         1.532
_refine_diff_density_min         -0.792
_refine_diff_density_rms         0.135
_refine_ls_extinction_coef       0.01396(18)
_refine_ls_extinction_expression Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^
_refine_ls_extinction_method     SHELXL
_refine_ls_goodness_of_fit_ref   0.750
_refine_ls_hydrogen_treatment    mixed
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1121
_refine_ls_number_reflns         18971
_refine_ls_number_restraints     184
_refine_ls_restrained_S_all      0.758
_refine_ls_R_factor_all          0.1348
_refine_ls_R_factor_gt           0.0456
_refine_ls_shift/su_max          0.013
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0405P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1062
_refine_ls_wR_factor_ref         0.1189
_reflns_number_gt                6715
_reflns_number_total             18971
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ja0043441_4.cif
_cod_data_source_block           compound4
_cod_original_formula_sum        'C32 H19 Ag12 F50 O29.50'
_cod_database_code               4115642
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
Ag1 Ag 0.51386(5) 0.45235(5) 0.56235(4) 0.0442(2) Uani 1 1 d .
Ag2 Ag 0.49453(6) 0.25369(5) 0.42046(5) 0.0575(3) Uani 1 1 d .
Ag3 Ag 0.38950(5) 0.23531(5) 0.26214(5) 0.0545(2) Uani 1 1 d .
Ag4 Ag 0.32267(5) 0.38624(6) 0.34532(5) 0.0510(2) Uani 1 1 d .
Ag5 Ag 0.66160(5) 0.42243(5) 0.47281(5) 0.0461(2) Uani 1 1 d .
Ag6 Ag 0.57846(5) 0.30068(6) 0.28770(5) 0.0546(2) Uani 1 1 d .
Ag7 Ag 0.46723(6) 0.41869(6) 0.25507(5) 0.0583(3) Uani 1 1 d .
Ag8 Ag 0.51616(6) 0.07773(6) 0.48170(6) 0.0613(3) Uani 1 1 d .
Ag9 Ag 0.90828(5) 0.46676(6) 0.51323(6) 0.0591(3) Uani 1 1 d .
Ag10 Ag 0.49093(7) 0.06765(6) 0.07970(5) 0.0684(3) Uani 1 1 d .
Ag11 Ag 0.49272(7) 0.47759(7) 0.07219(6) 0.0766(3) Uani 1 1 d .
Ag12 Ag 0.1393(2) 0.3009(3) 0.1564(2) 0.1299(15) Uani 0.70 1 d P
Ag13 Ag 0.1430(7) 0.2562(5) 0.1260(5) 0.147(4) Uani 0.30 1 d P
C1 C 0.5191(6) 0.3865(6) 0.4181(5) 0.036(2) Uani 1 1 d .
C2 C 0.4668(7) 0.3841(7) 0.3647(6) 0.046(3) Uani 1 1 d .
O11 O 0.3781(6) -0.0563(6) -0.1243(5) 0.080(3) Uani 1 1 d .
O12 O 0.3600(5) 0.0459(5) 0.0000(5) 0.079(2) Uani 1 1 d .
C11 C 0.3392(7) -0.0039(9) -0.0784(9) 0.071(4) Uani 1 1 d D
C12 C 0.2476(7) -0.0127(11) -0.1223(7) 0.125(7) Uani 1 1 d D
F11 F 0.1897(6) 0.0042(13) -0.0715(8) 0.235(8) Uani 1 1 d D
F12 F 0.2162(8) -0.0766(8) -0.1994(9) 0.266(9) Uani 1 1 d D
C13 C 0.2543(7) 0.0647(10) -0.1488(7) 0.173(10) Uani 1 1 d D
F13 F 0.2817(12) 0.1400(7) -0.0805(9) 0.291(11) Uani 1 1 d D
F14 F 0.1781(7) 0.0589(9) -0.1920(7) 0.196(6) Uani 1 1 d D
F15 F 0.3167(7) 0.0666(11) -0.1957(10) 0.256(10) Uani 1 1 d D
O21 O 0.6404(5) 0.5432(6) 0.0989(5) 0.083(3) Uani 1 1 d .
O22 O 0.6511(6) 0.5788(6) -0.0115(5) 0.085(3) Uani 1 1 d .
C21 C 0.6852(9) 0.5777(9) 0.0557(8) 0.088(4) Uani 1 1 d D
C22 C 0.7708(13) 0.6501(12) 0.1103(9) 0.304(14) Uani 1 1 d DU
F21 F 0.8097(10) 0.7116(14) 0.0833(15) 0.297(10) Uani 1 1 d DU
F22 F 0.7955(10) 0.7025(15) 0.1927(9) 0.314(12) Uani 1 1 d DU
C23 C 0.8444(14) 0.6045(11) 0.0967(8) 0.372(16) Uani 1 1 d DU
F23 F 0.9166(8) 0.6740(14) 0.1386(11) 0.457(17) Uani 1 1 d DU
F24 F 0.8256(8) 0.5677(14) 0.0125(8) 0.319(11) Uani 1 1 d DU
F25 F 0.8144(8) 0.5513(12) 0.1349(14) 0.321(11) Uani 1 1 d DU
O31 O 0.1919(5) 0.2585(5) 0.2586(5) 0.070(2) Uani 1 1 d .
O32 O 0.2496(5) 0.1764(6) 0.3066(5) 0.076(2) Uani 1 1 d .
C31 C 0.1886(7) 0.1884(8) 0.2697(7) 0.056(3) Uani 1 1 d D
C32 C 0.0991(6) 0.1156(8) 0.2423(10) 0.121(6) Uani 1 1 d D
F31 F 0.0276(6) 0.1434(7) 0.2351(8) 0.162(4) Uani 1 1 d D
F32 F 0.0861(7) 0.0664(7) 0.2882(8) 0.177(5) Uani 1 1 d D
C33 C 0.0911(7) 0.0468(8) 0.1516(10) 0.30(2) Uani 1 1 d D
F33 F 0.0148(8) -0.0182(7) 0.1332(9) 0.283(9) Uani 1 1 d D
F34 F 0.1623(8) 0.0181(8) 0.1489(9) 0.222(6) Uani 1 1 d D
F35 F 0.0918(11) 0.0878(11) 0.0992(8) 0.292(11) Uani 1 1 d D
O41 O 0.5433(5) 0.4628(5) 0.7759(4) 0.057(2) Uani 1 1 d .
O42 O 0.5619(4) 0.3802(4) 0.6481(4) 0.0475(17) Uani 1 1 d .
C41 C 0.5499(6) 0.3939(6) 0.7207(7) 0.043(3) Uani 1 1 d D
C42 C 0.5473(6) 0.3192(5) 0.7495(5) 0.066(4) Uani 1 1 d D
F41 F 0.5798(5) 0.3457(5) 0.8310(5) 0.109(3) Uani 1 1 d D
F42 F 0.5845(6) 0.2611(6) 0.7016(6) 0.138(4) Uani 1 1 d D
C43 C 0.4498(7) 0.2671(5) 0.7414(6) 0.097(5) Uani 1 1 d D
F43 F 0.4367(6) 0.1907(5) 0.7481(6) 0.151(4) Uani 1 1 d D
F44 F 0.3999(7) 0.2481(7) 0.6684(7) 0.214(7) Uani 1 1 d D
F45 F 0.4084(6) 0.3118(6) 0.7977(8) 0.185(6) Uani 1 1 d D
O51 O 0.7579(5) 0.5384(6) 0.7044(5) 0.070(2) Uani 1 1 d .
O52 O 0.7670(4) 0.4338(5) 0.5842(5) 0.0551(19) Uani 1 1 d .
C51 C 0.7828(7) 0.4695(8) 0.6634(8) 0.060(3) Uani 1 1 d D
C52 C 0.8248(6) 0.4099(8) 0.6927(14) 0.200 Uiso 1 1 d D
F51 F 0.9099(5) 0.4254(8) 0.6780(6) 0.149(4) Uani 1 1 d D
F52 F 0.7728(7) 0.3280(6) 0.6815(7) 0.152(4) Uani 1 1 d D
C53 C 0.8458(7) 0.4472(8) 0.7906(14) 0.37(2) Uani 1 1 d DU
F53 F 0.7616(6) 0.4381(8) 0.8050(6) 0.175(5) Uani 1 1 d DU
F54 F 0.8999(7) 0.5282(6) 0.8041(8) 0.209(6) Uani 1 1 d DU
F55 F 0.8810(7) 0.3873(8) 0.8028(8) 0.213(6) Uani 1 1 d DU
O61 O 0.9451(5) 0.3465(5) 0.4978(5) 0.066(2) Uani 1 1 d .
O62 O 1.0834(5) 0.3954(5) 0.4692(5) 0.063(2) Uani 1 1 d .
C61 C 1.0213(8) 0.3391(7) 0.4837(7) 0.055(3) Uani 1 1 d D
C62 C 1.0413(6) 0.2556(6) 0.4840(8) 0.109(6) Uani 1 1 d D
F61 F 0.9702(6) 0.1830(5) 0.4506(7) 0.146(4) Uani 1 1 d D
F62 F 1.1114(5) 0.2432(5) 0.4461(6) 0.131(3) Uani 1 1 d D
C63 C 1.0729(7) 0.2682(7) 0.5760(8) 0.139(7) Uani 1 1 d D
F63 F 1.0959(7) 0.1986(8) 0.5774(9) 0.228(7) Uani 1 1 d D
F64 F 1.1437(8) 0.3406(8) 0.6144(7) 0.228(7) Uani 1 1 d D
F65 F 1.0092(8) 0.2798(9) 0.6218(7) 0.197(6) Uani 1 1 d D
O71 O 0.5013(5) 0.3549(5) 0.1234(4) 0.064(2) Uani 1 1 d .
O72 O 0.5285(5) 0.2376(5) 0.1370(4) 0.062(2) Uani 1 1 d .
C71 C 0.5243(7) 0.2869(7) 0.0977(5) 0.047(3) Uani 1 1 d D
C72 C 0.5486(6) 0.2600(5) 0.0099(5) 0.064(3) Uani 1 1 d D
F71 F 0.5156(6) 0.1731(5) -0.0349(4) 0.124(3) Uani 1 1 d D
F72 F 0.5223(6) 0.3031(6) -0.0328(4) 0.126(3) Uani 1 1 d D
C73 C 0.6511(7) 0.2843(6) 0.0165(5) 0.106(5) Uani 1 1 d D
F73 F 0.6784(5) 0.2769(6) -0.0560(5) 0.130(3) Uani 1 1 d D
F74 F 0.6826(7) 0.2315(8) 0.0427(7) 0.192(6) Uani 1 1 d D
F75 F 0.6926(5) 0.3649(6) 0.0745(6) 0.148(4) Uani 1 1 d D
O81 O 0.7116(5) 0.3923(5) 0.2725(5) 0.072(2) Uani 1 1 d .
O82 O 0.7827(4) 0.4032(5) 0.3956(4) 0.056(2) Uani 1 1 d .
C81 C 0.7786(6) 0.4006(7) 0.3232(7) 0.053(3) Uani 1 1 d D
C82 C 0.8642(5) 0.4067(7) 0.2864(5) 0.086(5) Uani 1 1 d D
F81 F 0.8646(4) 0.4360(6) 0.2243(5) 0.108(3) Uani 1 1 d D
F82 F 0.9359(4) 0.4600(6) 0.3471(4) 0.112(3) Uani 1 1 d D
C83 C 0.8804(6) 0.3159(7) 0.2475(6) 0.105(5) Uani 1 1 d D
F83 F 0.9577(6) 0.3203(8) 0.2204(7) 0.196(5) Uani 1 1 d D
F84 F 0.8165(7) 0.2594(6) 0.1812(5) 0.159(4) Uani 1 1 d D
F85 F 0.8815(6) 0.2796(6) 0.3037(6) 0.141(4) Uani 1 1 d D
O91 O 0.4579(5) 0.1054(4) 0.3501(5) 0.062(2) Uani 1 1 d .
O92 O 0.4279(5) 0.1042(5) 0.2201(4) 0.061(2) Uani 1 1 d .
C91 C 0.4366(8) 0.0701(6) 0.2705(8) 0.060(3) Uani 1 1 d D
C92 C 0.4182(9) -0.0298(6) 0.2284(7) 0.107(6) Uani 1 1 d D
F91 F 0.3850(13) -0.0676(6) 0.1460(6) 0.290(11) Uani 1 1 d D
F92 F 0.4806(7) -0.0541(7) 0.2605(13) 0.287(10) Uani 1 1 d D
C93 C 0.3360(9) -0.0818(6) 0.2509(6) 0.171(12) Uani 1 1 d D
F93 F 0.2660(7) -0.0539(8) 0.2439(11) 0.265(10) Uani 1 1 d D
F94 F 0.3094(8) -0.1693(5) 0.2101(5) 0.174(5) Uani 1 1 d D
F95 F 0.3526(10) -0.0703(7) 0.3316(6) 0.234(8) Uani 1 1 d D
O101 O 0.3773(5) 0.0675(5) 0.5082(5) 0.064(2) Uani 1 1 d .
O102 O 0.3487(5) -0.0572(5) 0.5315(5) 0.069(2) Uani 1 1 d .
C101 C 0.3258(7) 0.0055(7) 0.5245(7) 0.065(3) Uani 1 1 d D
C102 C 0.2383(8) 0.0176(7) 0.5524(9) 0.190(14) Uani 1 1 d D
F101 F 0.2028(5) -0.0288(7) 0.5960(7) 0.152(4) Uani 1 1 d D
F102 F 0.2355(7) 0.0995(6) 0.5952(9) 0.184(5) Uani 1 1 d D
C103 C 0.1663(9) -0.0224(7) 0.4717(9) 0.184(12) Uani 1 1 d D
F103 F 0.1917(6) 0.0273(8) 0.4292(7) 0.184(5) Uani 1 1 d D
F104 F 0.0914(6) -0.0149(9) 0.5004(12) 0.337(13) Uani 1 1 d D
F105 F 0.1683(6) -0.1045(6) 0.4309(8) 0.191(6) Uani 1 1 d D
O1W O 0.2910(6) 0.3561(6) 0.1331(5) 0.095(3) Uani 1 1 d .
O2W O 0.3645(4) 0.3788(4) 0.5780(4) 0.0493(18) Uani 1 1 d .
O3W O 0.3470(4) 0.2074(4) 0.4688(4) 0.0569(19) Uani 1 1 d .
O4W O 0.3110(5) 0.1839(6) 0.1199(5) 0.083(3) Uani 1 1 d .
O5W O 0.6454(5) 0.1939(5) 0.2921(5) 0.081(2) Uani 1 1 d .
O6W O 0.5989(4) 0.2408(4) 0.5211(4) 0.0539(19) Uani 1 1 d .
O7W O 0.7503(5) 0.2188(5) 0.4488(5) 0.064(2) Uani 1 1 d .
O8W O 0.6506(5) 0.5276(5) 0.2623(5) 0.076(2) Uani 1 1 d .
O9W O 0.7377(4) 0.5848(4) 0.5271(4) 0.0424(16) Uani 1 1 d .
O10W O 0.0048(14) 0.2529(11) 0.0306(13) 0.128(9) Uani 0.50 1 d P
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
F F 0.0171 0.0103 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ag Ag -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
C1 Ag1 O42 114.8(3) . .
C1 Ag1 O2W 106.0(3) . .
O42 Ag1 O2W 82.9(2) . .
C1 Ag1 C2 121.3(3) . 2_666
O42 Ag1 C2 117.5(3) . 2_666
O2W Ag1 C2 105.0(3) . 2_666
C1 Ag1 Ag5 47.7(2) . .
O42 Ag1 Ag5 87.40(15) . .
O2W Ag1 Ag5 143.46(17) . .
C2 Ag1 Ag5 110.7(2) 2_666 .
C1 Ag1 Ag7 165.2(2) . 2_666
O42 Ag1 Ag7 75.37(16) . 2_666
O2W Ag1 Ag7 85.51(16) . 2_666
C2 Ag1 Ag7 44.9(2) 2_666 2_666
Ag5 Ag1 Ag7 125.81(3) . 2_666
C1 Ag1 Ag4 110.7(2) . 2_666
O42 Ag1 Ag4 89.79(15) . 2_666
O2W Ag1 Ag4 142.27(17) . 2_666
C2 Ag1 Ag4 47.1(2) 2_666 2_666
Ag5 Ag1 Ag4 72.42(3) . 2_666
Ag7 Ag1 Ag4 56.90(3) 2_666 2_666
C1 Ag1 Ag1 58.9(2) . 2_666
O42 Ag1 Ag1 169.13(15) . 2_666
O2W Ag1 Ag1 107.02(14) . 2_666
C2 Ag1 Ag1 64.9(2) 2_666 2_666
Ag5 Ag1 Ag1 81.96(3) . 2_666
Ag7 Ag1 Ag1 109.19(4) 2_666 2_666
Ag4 Ag1 Ag1 84.89(3) 2_666 2_666
C1 Ag1 Ag2 42.4(2) . .
O42 Ag1 Ag2 77.11(16) . .
O2W Ag1 Ag2 83.07(17) . .
C2 Ag1 Ag2 163.7(2) 2_666 .
Ag5 Ag1 Ag2 60.42(3) . .
Ag7 Ag1 Ag2 151.27(3) 2_666 .
Ag4 Ag1 Ag2 131.26(3) 2_666 .
Ag1 Ag1 Ag2 99.36(3) 2_666 .
C1 Ag2 O91 149.6(3) . .
C1 Ag2 O6W 116.3(3) . .
O91 Ag2 O6W 87.1(2) . .
C1 Ag2 O3W 111.2(3) . .
O91 Ag2 O3W 80.3(2) . .
O6W Ag2 O3W 101.3(2) . .
C1 Ag2 Ag3 71.2(2) . .
O91 Ag2 Ag3 81.44(19) . .
O6W Ag2 Ag3 163.57(17) . .
O3W Ag2 Ag3 88.41(15) . .
C1 Ag2 Ag6 57.2(2) . .
O91 Ag2 Ag6 96.87(18) . .
O6W Ag2 Ag6 113.37(16) . .
O3W Ag2 Ag6 145.07(15) . .
Ag3 Ag2 Ag6 56.93(3) . .
C1 Ag2 Ag5 44.4(2) . .
O91 Ag2 Ag5 139.2(2) . .
O6W Ag2 Ag5 74.98(15) . .
O3W Ag2 Ag5 138.44(16) . .
Ag3 Ag2 Ag5 106.45(3) . .
Ag6 Ag2 Ag5 59.72(3) . .
C1 Ag2 Ag1 45.3(2) . .
O91 Ag2 Ag1 162.87(18) . .
O6W Ag2 Ag1 87.86(17) . .
O3W Ag2 Ag1 84.61(16) . .
Ag3 Ag2 Ag1 106.39(3) . .
Ag6 Ag2 Ag1 100.16(3) . .
Ag5 Ag2 Ag1 54.15(2) . .
O92 Ag3 O4W 87.9(3) . .
O92 Ag3 C2 132.3(3) . .
O4W Ag3 C2 130.3(3) . .
O92 Ag3 O32 95.1(3) . .
O4W Ag3 O32 90.9(3) . .
C2 Ag3 O32 109.3(3) . .
O92 Ag3 Ag6 78.70(19) . .
O4W Ag3 Ag6 116.08(18) . .
C2 Ag3 Ag6 60.3(2) . .
O32 Ag3 Ag6 151.8(2) . .
O92 Ag3 Ag4 166.24(18) . .
O4W Ag3 Ag4 99.6(2) . .
C2 Ag3 Ag4 49.1(2) . .
O32 Ag3 Ag4 73.4(2) . .
Ag6 Ag3 Ag4 107.81(3) . .
O92 Ag3 Ag2 77.30(17) . .
O4W Ag3 Ag2 165.2(2) . .
C2 Ag3 Ag2 63.0(2) . .
O32 Ag3 Ag2 89.7(2) . .
Ag6 Ag3 Ag2 62.07(3) . .
Ag4 Ag3 Ag2 94.82(3) . .
O92 Ag3 Ag7 135.28(18) . .
O4W Ag3 Ag7 87.6(2) . .
C2 Ag3 Ag7 44.4(2) . .
O32 Ag3 Ag7 129.4(2) . .
Ag6 Ag3 Ag7 63.82(3) . .
Ag4 Ag3 Ag7 57.20(3) . .
Ag2 Ag3 Ag7 103.41(3) . .
C2 Ag4 O51 137.9(3) . 2_666
C2 Ag4 O9W 112.6(3) . 2_666
O51 Ag4 O9W 93.4(2) 2_666 2_666
C2 Ag4 O31 125.9(3) . .
O51 Ag4 O31 82.0(3) 2_666 .
O9W Ag4 O31 94.0(2) 2_666 .
C2 Ag4 Ag7 48.0(2) . .
O51 Ag4 Ag7 93.99(18) 2_666 .
O9W Ag4 Ag7 151.55(14) 2_666 .
O31 Ag4 Ag7 114.19(18) . .
C2 Ag4 Ag3 53.4(3) . .
O51 Ag4 Ag3 134.0(2) 2_666 .
O9W Ag4 Ag3 125.49(15) 2_666 .
O31 Ag4 Ag3 72.7(2) . .
Ag7 Ag4 Ag3 64.28(3) . .
C2 Ag4 Ag1 54.4(3) . 2_666
O51 Ag4 Ag1 94.8(2) 2_666 2_666
O9W Ag4 Ag1 90.51(14) 2_666 2_666
O31 Ag4 Ag1 174.62(18) . 2_666
Ag7 Ag4 Ag1 61.51(3) . 2_666
Ag3 Ag4 Ag1 106.94(3) . 2_666
C1 Ag5 O52 146.6(3) . .
C1 Ag5 O82 126.8(3) . .
O52 Ag5 O82 82.1(2) . .
C1 Ag5 O9W 112.3(3) . .
O52 Ag5 O9W 82.5(2) . .
O82 Ag5 O9W 86.8(2) . .
C1 Ag5 Ag1 52.0(2) . .
O52 Ag5 Ag1 100.04(18) . .
O82 Ag5 Ag1 176.98(17) . .
O9W Ag5 Ag1 91.32(14) . .
C1 Ag5 Ag6 56.0(2) . .
O52 Ag5 Ag6 139.60(19) . .
O82 Ag5 Ag6 72.22(16) . .
O9W Ag5 Ag6 125.24(13) . .
Ag1 Ag5 Ag6 107.11(3) . .
C1 Ag5 Ag2 44.8(2) . .
O52 Ag5 Ag2 111.37(17) . .
O82 Ag5 Ag2 115.92(17) . .
O9W Ag5 Ag2 154.18(14) . .
Ag1 Ag5 Ag2 65.44(3) . .
Ag6 Ag5 Ag2 57.54(2) . .
O5W Ag6 O81 93.4(3) . .
O5W Ag6 O72 96.7(3) . .
O81 Ag6 O72 89.7(3) . .
O5W Ag6 C1 119.7(3) . .
O81 Ag6 C1 111.0(3) . .
O72 Ag6 C1 135.5(3) . .
O5W Ag6 C2 139.8(3) . .
O81 Ag6 C2 115.6(3) . .
O72 Ag6 C2 109.9(3) . .
C1 Ag6 C2 25.7(2) . .
O5W Ag6 Ag3 111.34(19) . .
O81 Ag6 Ag3 151.79(19) . .
O72 Ag6 Ag3 74.61(18) . .
C1 Ag6 Ag3 69.0(2) . .
C2 Ag6 Ag3 52.1(2) . .
O5W Ag6 Ag2 79.7(2) . .
O81 Ag6 Ag2 140.40(19) . .
O72 Ag6 Ag2 129.68(18) . .
C1 Ag6 Ag2 46.3(2) . .
C2 Ag6 Ag2 60.1(2) . .
Ag3 Ag6 Ag2 61.00(3) . .
O5W Ag6 Ag5 92.26(19) . .
O81 Ag6 Ag5 78.8(2) . .
O72 Ag6 Ag5 165.86(17) . .
C1 Ag6 Ag5 45.0(2) . .
C2 Ag6 Ag5 68.7(2) . .
Ag3 Ag6 Ag5 112.20(3) . .
Ag2 Ag6 Ag5 62.74(3) . .
O5W Ag6 Ag7 170.56(19) . .
O81 Ag6 Ag7 91.2(2) . .
O72 Ag6 Ag7 75.09(18) . .
C1 Ag6 Ag7 65.9(2) . .
C2 Ag6 Ag7 43.1(2) . .
Ag3 Ag6 Ag7 62.40(3) . .
Ag2 Ag6 Ag7 101.78(3) . .
Ag5 Ag6 Ag7 96.71(3) . .
C2 Ag7 O71 132.6(3) . .
C2 Ag7 O41 137.7(3) . 2_666
O71 Ag7 O41 89.1(3) . 2_666
C2 Ag7 Ag4 50.9(3) . .
O71 Ag7 Ag4 138.44(19) . .
O41 Ag7 Ag4 105.37(18) 2_666 .
C2 Ag7 Ag1 54.9(3) . 2_666
O71 Ag7 Ag1 159.97(19) . 2_666
O41 Ag7 Ag1 83.62(18) 2_666 2_666
Ag4 Ag7 Ag1 61.59(3) . 2_666
C2 Ag7 Ag3 50.8(3) . .
O71 Ag7 Ag3 91.84(19) . .
O41 Ag7 Ag3 153.73(18) 2_666 .
Ag4 Ag7 Ag3 58.52(3) . .
Ag1 Ag7 Ag3 102.92(3) 2_666 .
C2 Ag7 Ag6 56.5(3) . .
O71 Ag7 Ag6 78.77(19) . .
O41 Ag7 Ag6 151.26(18) 2_666 .
Ag4 Ag7 Ag6 100.87(3) . .
Ag1 Ag7 Ag6 98.97(3) 2_666 .
Ag3 Ag7 Ag6 53.78(3) . .
O101 Ag8 O102 163.6(2) . 2_656
O101 Ag8 O6W 108.1(2) . .
O102 Ag8 O6W 85.2(2) 2_656 .
O101 Ag8 Ag8 81.30(17) . 2_656
O102 Ag8 Ag8 82.50(18) 2_656 2_656
O6W Ag8 Ag8 150.35(15) . 2_656
O61 Ag9 O62 162.1(2) . 2_766
O61 Ag9 O82 99.1(3) . .
O62 Ag9 O82 92.7(3) 2_766 .
O61 Ag9 Ag9 84.39(17) . 2_766
O62 Ag9 Ag9 78.08(18) 2_766 2_766
O82 Ag9 Ag9 120.09(16) . 2_766
O11 Ag10 O12 163.1(3) 2_655 .
O11 Ag10 O72 100.2(3) 2_655 .
O12 Ag10 O72 92.5(3) . .
O11 Ag10 O92 99.7(3) 2_655 .
O12 Ag10 O92 93.7(3) . .
O72 Ag10 O92 78.0(2) . .
O11 Ag10 Ag10 81.3(2) 2_655 2_655
O12 Ag10 Ag10 81.9(2) . 2_655
O72 Ag10 Ag10 133.16(15) . 2_655
O92 Ag10 Ag10 148.44(17) . 2_655
O22 Ag11 O21 162.9(3) 2_665 .
O22 Ag11 O71 97.2(3) 2_665 .
O21 Ag11 O71 95.9(3) . .
O22 Ag11 O41 92.8(3) 2_665 2_666
O21 Ag11 O41 100.9(3) . 2_666
O71 Ag11 O41 77.2(2) . 2_666
O22 Ag11 Ag11 82.2(2) 2_665 2_665
O21 Ag11 Ag11 80.6(2) . 2_665
O71 Ag11 Ag11 141.99(17) . 2_665
O41 Ag11 Ag11 140.73(16) 2_666 2_665
Ag13 Ag12 O31 82.6(10) . .
Ag13 Ag12 O1W 82.7(10) . .
O31 Ag12 O1W 91.9(3) . .
Ag12 Ag13 O31 78.4(9) . .
Ag12 Ag13 O1W 79.3(10) . .
O31 Ag13 O1W 90.7(4) . .
Ag12 Ag13 O10W 84.5(11) . .
O31 Ag13 O10W 143.1(6) . .
O1W Ag13 O10W 118.1(5) . .
C2 C1 Ag5 146.7(8) . .
C2 C1 Ag2 110.3(8) . .
Ag5 C1 Ag2 90.7(4) . .
C2 C1 Ag1 122.5(8) . .
Ag5 C1 Ag1 80.3(3) . .
Ag2 C1 Ag1 92.3(3) . .
C2 C1 Ag6 81.1(6) . .
Ag5 C1 Ag6 79.0(3) . .
Ag2 C1 Ag6 76.6(3) . .
Ag1 C1 Ag6 156.3(4) . .
C1 C2 Ag7 138.0(8) . .
C1 C2 Ag4 138.2(8) . .
Ag7 C2 Ag4 81.1(4) . .
C1 C2 Ag3 113.1(8) . .
Ag7 C2 Ag3 84.9(3) . .
Ag4 C2 Ag3 77.6(3) . .
C1 C2 Ag1 92.5(7) . 2_666
Ag7 C2 Ag1 80.2(3) . 2_666
Ag4 C2 Ag1 78.5(3) . 2_666
Ag3 C2 Ag1 153.4(5) . 2_666
C1 C2 Ag6 73.2(7) . .
Ag7 C2 Ag6 80.4(3) . .
Ag4 C2 Ag6 141.7(5) . .
Ag3 C2 Ag6 67.5(2) . .
Ag1 C2 Ag6 130.3(4) 2_666 .
C11 O11 Ag10 124.4(7) . 2_655
C11 O12 Ag10 122.1(8) . .
O12 C11 O11 129.9(10) . .
O12 C11 C12 115.4(12) . .
O11 C11 C12 114.1(11) . .
F11 C12 F12 117.6(15) . .
F11 C12 C11 114.8(10) . .
F12 C12 C11 117.0(10) . .
F11 C12 C13 96.7(11) . .
F12 C12 C13 96.5(11) . .
C11 C12 C13 109.7(10) . .
F15 C13 F13 106.8(13) . .
F15 C13 F14 109.2(10) . .
F13 C13 F14 109.8(11) . .
F15 C13 C12 108.1(10) . .
F13 C13 C12 109.4(10) . .
F14 C13 C12 113.3(10) . .
C21 O21 Ag11 127.5(8) . .
C21 O22 Ag11 126.4(8) . 2_665
O22 C21 O21 123.3(12) . .
O22 C21 C22 119.9(13) . .
O21 C21 C22 111.6(11) . .
F21 C22 F22 95.8(15) . .
F21 C22 C21 118.8(14) . .
F22 C22 C21 133.9(16) . .
F21 C22 C23 95.1(16) . .
F22 C22 C23 101.1(17) . .
C21 C22 C23 104.7(14) . .
F25 C23 F24 115.8(11) . .
F25 C23 F23 117.2(11) . .
F24 C23 F23 121.3(12) . .
F25 C23 C22 96.3(15) . .
F24 C23 C22 97.3(15) . .
F23 C23 C22 100.2(15) . .
C31 O31 Ag12 139.4(7) . .
C31 O31 Ag13 122.4(7) . .
Ag12 O31 Ag13 19.0(2) . .
C31 O31 Ag4 114.4(7) . .
Ag12 O31 Ag4 103.2(3) . .
Ag13 O31 Ag4 114.0(4) . .
C31 O32 Ag3 108.1(7) . .
O32 C31 O31 125.4(10) . .
O32 C31 C32 115.8(11) . .
O31 C31 C32 118.5(10) . .
F31 C32 F32 109.4(11) . .
F31 C32 C31 114.2(10) . .
F32 C32 C31 115.6(10) . .
F31 C32 C33 102.6(10) . .
F32 C32 C33 103.3(10) . .
C31 C32 C33 110.5(9) . .
F34 C33 F35 108.5(12) . .
F34 C33 F33 112.2(11) . .
F35 C33 F33 111.7(11) . .
F34 C33 C32 108.5(10) . .
F35 C33 C32 107.7(11) . .
F33 C33 C32 108.0(10) . .
C41 O41 Ag7 121.7(5) . 2_666
C41 O41 Ag11 140.9(6) . 2_666
Ag7 O41 Ag11 96.4(3) 2_666 2_666
C41 O42 Ag1 125.1(6) . .
O42 C41 O41 128.4(7) . .
O42 C41 C42 116.5(9) . .
O41 C41 C42 115.0(8) . .
F41 C42 F42 110.9(8) . .
F41 C42 C41 114.5(7) . .
F42 C42 C41 112.5(7) . .
F41 C42 C43 102.6(7) . .
F42 C42 C43 106.0(8) . .
C41 C42 C43 109.5(6) . .
F44 C43 F43 104.8(8) . .
F44 C43 F45 103.1(9) . .
F43 C43 F45 105.6(8) . .
F44 C43 C42 112.8(7) . .
F43 C43 C42 116.1(7) . .
F45 C43 C42 113.1(7) . .
C51 O51 Ag4 130.6(7) . 2_666
C51 O52 Ag5 137.0(7) . .
O52 C51 O51 121.4(9) . .
O52 C51 C52 105.6(13) . .
O51 C51 C52 132.7(12) . .
F51 C52 F52 122.5(12) . .
F51 C52 C53 98.9(11) . .
F52 C52 C53 95.7(11) . .
F51 C52 C51 106.7(9) . .
F52 C52 C51 119.4(10) . .
C53 C52 C51 110.2(11) . .
F53 C53 F55 113.6(8) . .
F53 C53 F54 119.3(10) . .
F55 C53 F54 119.9(10) . .
F53 C53 C52 98.6(11) . .
F55 C53 C52 101.0(11) . .
F54 C53 C52 97.4(12) . .
C61 O61 Ag9 122.4(6) . .
C61 O62 Ag9 128.3(6) . 2_766
O61 C61 O62 125.9(9) . .
O61 C61 C62 116.7(9) . .
O62 C61 C62 117.4(9) . .
F61 C62 F62 111.4(9) . .
F61 C62 C61 113.5(9) . .
F62 C62 C61 110.6(8) . .
F61 C62 C63 106.7(9) . .
F62 C62 C63 103.9(9) . .
C61 C62 C63 110.2(8) . .
F65 C63 F63 108.7(9) . .
F65 C63 F64 106.7(10) . .
F63 C63 F64 108.6(10) . .
F65 C63 C62 111.1(8) . .
F63 C63 C62 111.2(9) . .
F64 C63 C62 110.4(8) . .
C71 O71 Ag7 125.4(6) . .
C71 O71 Ag11 136.9(6) . .
Ag7 O71 Ag11 97.3(3) . .
C71 O72 Ag6 120.6(6) . .
C71 O72 Ag10 130.0(6) . .
Ag6 O72 Ag10 109.5(3) . .
O71 C71 O72 126.4(8) . .
O71 C71 C72 116.0(9) . .
O72 C71 C72 117.6(9) . .
F72 C72 F71 110.2(9) . .
F72 C72 C71 112.2(7) . .
F71 C72 C71 111.4(7) . .
F72 C72 C73 105.0(8) . .
F71 C72 C73 107.0(8) . .
C71 C72 C73 110.7(7) . .
F75 C73 F73 108.7(8) . .
F75 C73 F74 104.7(9) . .
F73 C73 F74 106.2(8) . .
F75 C73 C72 112.1(7) . .
F73 C73 C72 114.4(7) . .
F74 C73 C72 110.1(7) . .
C81 O81 Ag6 111.5(6) . .
C81 O82 Ag5 121.7(6) . .
C81 O82 Ag9 130.7(6) . .
Ag5 O82 Ag9 100.0(2) . .
O82 C81 O81 128.8(8) . .
O82 C81 C82 117.9(9) . .
O81 C81 C82 113.3(9) . .
F82 C82 F81 107.9(8) . .
F82 C82 C81 110.8(8) . .
F81 C82 C81 114.1(8) . .
F82 C82 C83 106.3(8) . .
F81 C82 C83 105.6(8) . .
C81 C82 C83 111.7(7) . .
F83 C83 F84 106.7(9) . .
F83 C83 F85 106.8(9) . .
F84 C83 F85 107.3(9) . .
F83 C83 C82 112.9(8) . .
F84 C83 C82 111.5(8) . .
F85 C83 C82 111.3(8) . .
C91 O91 Ag2 120.5(6) . .
C91 O92 Ag3 120.4(6) . .
C91 O92 Ag10 124.3(7) . .
Ag3 O92 Ag10 113.2(3) . .
O92 C91 O91 129.6(9) . .
O92 C91 C92 113.7(10) . .
O91 C91 C92 116.7(10) . .
F92 C92 F91 120.6(15) . .
F92 C92 C91 110.9(9) . .
F91 C92 C91 116.0(9) . .
F92 C92 C93 99.3(10) . .
F91 C92 C93 93.7(10) . .
C91 C92 C93 113.3(9) . .
F93 C93 F94 107.8(10) . .
F93 C93 F95 105.2(11) . .
F94 C93 F95 102.7(8) . .
F93 C93 C92 112.3(9) . .
F94 C93 C92 117.4(9) . .
F95 C93 C92 110.4(9) . .
C101 O101 Ag8 126.6(6) . .
C101 O102 Ag8 125.4(6) . 2_656
O102 C101 O101 124.1(9) . .
O102 C101 C102 116.9(9) . .
O101 C101 C102 118.0(9) . .
F102 C102 F101 105.5(11) . .
F102 C102 C101 118.4(10) . .
F101 C102 C101 116.2(9) . .
F102 C102 C103 106.3(10) . .
F101 C102 C103 101.6(10) . .
C101 C102 C103 107.1(10) . .
F103 C103 F105 112.1(10) . .
F103 C103 F104 112.9(10) . .
F105 C103 F104 115.5(11) . .
F103 C103 C102 105.3(10) . .
F105 C103 C102 105.6(10) . .
F104 C103 C102 104.1(11) . .
Ag12 O1W Ag13 18.0(2) . .
Ag2 O6W Ag8 93.4(2) . .
Ag4 O9W Ag5 92.48(18) 2_666 .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Ag1 C1 2.325(9) .
Ag1 O42 2.418(6) .
Ag1 O2W 2.433(5) .
Ag1 C2 2.509(10) 2_666
Ag1 Ag5 2.9095(10) .
Ag1 Ag7 3.0223(11) 2_666
Ag1 Ag4 3.0244(11) 2_666
Ag1 Ag1 3.1843(14) 2_666
Ag1 Ag2 3.2649(12) .
Ag2 C1 2.201(9) .
Ag2 O91 2.241(7) .
Ag2 O6W 2.392(6) .
Ag2 O3W 2.538(6) .
Ag2 Ag3 2.9335(11) .
Ag2 Ag6 2.9632(11) .
Ag2 Ag5 3.1217(11) .
Ag3 O92 2.318(7) .
Ag3 O4W 2.377(7) .
Ag3 C2 2.401(10) .
Ag3 O32 2.459(7) .
Ag3 Ag6 2.8105(11) .
Ag3 Ag4 2.9225(12) .
Ag3 Ag7 3.0874(12) .
Ag4 C2 2.261(10) .
Ag4 O51 2.324(7) 2_666
Ag4 O9W 2.378(6) 2_666
Ag4 O31 2.447(7) .
Ag4 Ag7 2.8805(11) .
Ag4 Ag1 3.0244(11) 2_666
Ag5 C1 2.185(9) .
Ag5 O52 2.343(6) .
Ag5 O82 2.407(6) .
Ag5 O9W 2.476(6) .
Ag5 Ag6 3.0326(11) .
Ag6 O5W 2.328(8) .
Ag6 O81 2.352(7) .
Ag6 O72 2.380(6) .
Ag6 C1 2.560(9) .
Ag6 C2 2.642(10) .
Ag6 Ag7 3.1262(12) .
Ag7 C2 2.167(9) .
Ag7 O71 2.282(7) .
Ag7 O41 2.300(7) 2_666
Ag7 Ag1 3.0223(11) 2_666
Ag8 O101 2.223(7) .
Ag8 O102 2.236(7) 2_656
Ag8 O6W 2.537(6) .
Ag8 Ag8 2.8612(15) 2_656
Ag9 O61 2.185(8) .
Ag9 O62 2.211(7) 2_766
Ag9 O82 2.408(7) .
Ag9 Ag9 2.9319(15) 2_766
Ag10 O11 2.207(8) 2_655
Ag10 O12 2.238(8) .
Ag10 O72 2.563(7) .
Ag10 O92 2.589(7) .
Ag10 Ag10 2.9347(18) 2_655
Ag11 O22 2.205(9) 2_665
Ag11 O21 2.218(8) .
Ag11 O71 2.566(7) .
Ag11 O41 2.583(7) 2_666
Ag11 Ag11 2.8534(15) 2_665
Ag12 Ag13 0.764(9) .
Ag12 O31 2.298(8) .
Ag12 O1W 2.433(9) .
Ag13 O31 2.327(12) .
Ag13 O1W 2.456(13) .
Ag13 O10W 2.58(3) .
C1 C2 1.161(11) .
C2 Ag1 2.509(10) 2_666
O11 C11 1.267(14) .
O11 Ag10 2.207(8) 2_655
O12 C11 1.257(14) .
C11 C12 1.511(5) .
C12 F11 1.312(5) .
C12 F12 1.316(5) .
C12 C13 1.521(5) .
C13 F15 1.310(5) .
C13 F13 1.314(5) .
C13 F14 1.314(5) .
O21 C21 1.252(13) .
O22 C21 1.241(13) .
O22 Ag11 2.205(9) 2_665
C21 C22 1.517(5) .
C22 F21 1.320(5) .
C22 F22 1.323(5) .
C22 C23 1.526(5) .
C23 F25 1.315(5) .
C23 F24 1.318(5) .
C23 F23 1.324(5) .
O31 C31 1.259(12) .
O32 C31 1.206(12) .
C31 C32 1.514(5) .
C32 F31 1.332(5) .
C32 F32 1.334(5) .
C32 C33 1.532(5) .
C33 F34 1.320(5) .
C33 F35 1.322(5) .
C33 F33 1.324(5) .
O41 C41 1.236(11) .
O41 Ag7 2.300(7) 2_666
O41 Ag11 2.583(7) 2_666
O42 C41 1.217(11) .
C41 C42 1.514(5) .
C42 F41 1.313(5) .
C42 F42 1.320(5) .
C42 C43 1.518(5) .
C43 F44 1.307(5) .
C43 F43 1.308(5) .
C43 F45 1.312(5) .
O51 C51 1.293(13) .
O51 Ag4 2.324(7) 2_666
O52 C51 1.240(13) .
C51 C52 1.539(5) .
C52 F51 1.347(5) .
C52 F52 1.353(5) .
C52 C53 1.534(5) .
C53 F53 1.336(5) .
C53 F55 1.340(5) .
C53 F54 1.341(5) .
O61 C61 1.259(11) .
O62 C61 1.285(11) .
O62 Ag9 2.211(7) 2_766
C61 C62 1.526(5) .
C62 F61 1.327(5) .
C62 F62 1.335(5) .
C62 C63 1.535(5) .
C63 F65 1.321(5) .
C63 F63 1.326(5) .
C63 F64 1.328(5) .
O71 C71 1.229(11) .
O72 C71 1.261(11) .
C71 C72 1.511(5) .
C72 F72 1.319(5) .
C72 F71 1.321(5) .
C72 C73 1.530(5) .
C73 F75 1.313(5) .
C73 F73 1.316(5) .
C73 F74 1.317(5) .
O81 C81 1.252(11) .
O82 C81 1.222(11) .
C81 C82 1.515(5) .
C82 F82 1.329(5) .
C82 F81 1.331(5) .
C82 C83 1.531(5) .
C83 F83 1.318(5) .
C83 F84 1.321(5) .
C83 F85 1.322(5) .
O91 C91 1.248(12) .
O92 C91 1.221(12) .
C91 C92 1.512(5) .
C92 F92 1.310(5) .
C92 F91 1.313(5) .
C92 C93 1.524(5) .
C93 F93 1.310(5) .
C93 F94 1.318(5) .
C93 F95 1.318(5) .
O101 C101 1.283(11) .
O102 C101 1.247(11) .
O102 Ag8 2.236(7) 2_656
C101 C102 1.516(5) .
C102 F102 1.322(5) .
C102 F101 1.325(5) .
C102 C103 1.526(5) .
C103 F103 1.313(5) .
C103 F105 1.316(5) .
C103 F104 1.317(5) .
O9W Ag4 2.378(6) 2_666
