#------------------------------------------------------------------------------
#$Date: 2016-03-22 12:15:05 +0200 (Tue, 22 Mar 2016) $
#$Revision: 178943 $
#$URL: svn://www.crystallography.net/cod/cif/4/11/72/4117286.cif $
#------------------------------------------------------------------------------
#
# This file is available in the Crystallography Open Database (COD),
# http://www.crystallography.net/
#
# All data on this site have been placed in the public domain by the
# contributors.
#
data_4117286
loop_
_publ_author_name
'Yan-Zhen Zheng'
'Marco Evangelisti'
'Floriana Tuna'
'Richard E. P. Winpenny'
_publ_section_title
;
 Co-Ln Mixed-Metal Phosphonate Grids and Cages as Molecular Magnetic
 Refrigerants
;
_journal_name_full               'Journal of the American Chemical Society'
_journal_page_first              1057
_journal_page_last               1065
_journal_paper_doi               10.1021/ja208367k
_journal_volume                  134
_journal_year                    2012
_chemical_formula_sum            'C112 H220 Co8 Dy8 N4 O72 P8'
_chemical_formula_weight         4794.12
_chemical_name_systematic
; 
 ? 
;
_space_group_IT_number           15
_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_Hall  '-C 2yc'
_symmetry_space_group_name_H-M   'C 1 2/c 1'
_atom_sites_solution_hydrogens   geom
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_audit_creation_method           SHELXL-97
_cell_angle_alpha                90.00
_cell_angle_beta                 101.5460(10)
_cell_angle_gamma                90.00
_cell_formula_units_Z            4
_cell_length_a                   35.6135(18)
_cell_length_b                   20.6435(10)
_cell_length_c                   24.9843(12)
_cell_measurement_temperature    100(2)
_cell_volume                     17996.4(15)
_computing_cell_refinement       'Bruker SMART'
_computing_data_collection       'Bruker SMART'
_computing_data_reduction        'Bruker SAINT'
_computing_molecular_graphics    'Bruker SHELXTL'
_computing_publication_material  'Bruker SHELXTL'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1990)'
_diffrn_ambient_temperature      100(2)
_diffrn_measured_fraction_theta_full 0.999
_diffrn_measured_fraction_theta_max 0.999
_diffrn_measurement_device_type  'CCD area detector'
_diffrn_measurement_method       'phi and omega scans'
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_source         'fine-focus sealed tube'
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_reflns_av_R_equivalents  0.0649
_diffrn_reflns_av_sigmaI/netI    0.0836
_diffrn_reflns_limit_h_max       42
_diffrn_reflns_limit_h_min       -42
_diffrn_reflns_limit_k_max       24
_diffrn_reflns_limit_k_min       -14
_diffrn_reflns_limit_l_max       29
_diffrn_reflns_limit_l_min       -29
_diffrn_reflns_number            44426
_diffrn_reflns_theta_full        25.00
_diffrn_reflns_theta_max         25.00
_diffrn_reflns_theta_min         1.48
_exptl_absorpt_coefficient_mu    4.143
_exptl_absorpt_correction_T_max  0.6362
_exptl_absorpt_correction_T_min  0.1471
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   SADABS
_exptl_crystal_colour            purple
_exptl_crystal_density_diffrn    1.769
_exptl_crystal_description       needle
_exptl_crystal_F_000             9440
_exptl_crystal_size_max          0.75
_exptl_crystal_size_mid          0.16
_exptl_crystal_size_min          0.12
_refine_diff_density_max         3.824
_refine_diff_density_min         -4.421
_refine_diff_density_rms         0.210
_refine_ls_extinction_method     none
_refine_ls_goodness_of_fit_ref   1.089
_refine_ls_hydrogen_treatment    constr
_refine_ls_matrix_type           full
_refine_ls_number_parameters     1353
_refine_ls_number_reflns         15859
_refine_ls_number_restraints     2254
_refine_ls_restrained_S_all      1.113
_refine_ls_R_factor_all          0.1642
_refine_ls_R_factor_gt           0.0962
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000
_refine_ls_structure_factor_coef Fsqd
_refine_ls_weighting_details
'calc w=1/[σ²(Fo²)+(0.0340P)²+1075.8903P] where P=(Fo²+2Fc²)/3'
_refine_ls_weighting_scheme      calc
_refine_ls_wR_factor_gt          0.1910
_refine_ls_wR_factor_ref         0.2301
_reflns_number_gt                8960
_reflns_number_total             15859
_reflns_threshold_expression     >2sigma(I)
_cod_data_source_file            ja208367k_si_019.cif
_cod_data_source_block           codym
_cod_database_code               4117286
loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, y, -z+1/2'
'x+1/2, y+1/2, z'
'-x+1/2, y+1/2, -z+1/2'
'-x, -y, -z'
'x, -y, z-1/2'
'-x+1/2, -y+1/2, -z'
'x+1/2, -y+1/2, z-1/2'
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Dy1 Dy 0.55893(2) 1.66823(4) 0.83708(4) 0.0559(3) Uani 1 1 d U . .
Dy2 Dy 0.63316(3) 1.54161(7) 0.88909(4) 0.0922(5) Uani 1 1 d U A .
Dy3 Dy 0.65122(4) 1.29684(6) 0.82128(5) 0.0910(4) Uani 1 1 d DU . .
Dy4 Dy 0.58779(6) 1.16589(9) 0.78172(9) 0.0508(4) Uani 0.5279(18) 1 d PDU A 1
O34 O 0.5922(5) 1.2770(9) 0.7604(11) 0.062(2) Uani 0.5279(18) 1 d PDU A 1
H34D H 0.5890 1.2906 0.7213 0.075 Uiso 0.5279(18) 1 calc PR A 1
C81 C 0.6495(6) 1.1519(10) 0.8728(8) 0.094(3) Uani 0.5279(18) 1 d PDU A 1
C90 C 0.6829(6) 1.1277(11) 0.9155(9) 0.101(4) Uani 0.5279(18) 1 d PDU A 1
O22 O 0.6399(8) 1.2077(11) 0.8513(11) 0.086(2) Uani 0.5279(18) 1 d PDU A 1
O38 O 0.6244(6) 1.1073(13) 0.8528(9) 0.091(3) Uani 0.5279(18) 1 d PDU A 1
C88 C 0.6685(9) 1.0782(16) 0.9517(11) 0.113(7) Uani 0.5279(18) 1 d PDU A 1
H88A H 0.6489 1.0981 0.9688 0.170 Uiso 0.5279(18) 1 calc PR A 1
H88B H 0.6900 1.0635 0.9801 0.170 Uiso 0.5279(18) 1 calc PR A 1
H88C H 0.6575 1.0411 0.9295 0.170 Uiso 0.5279(18) 1 calc PR A 1
C85 C 0.7118(7) 1.0960(15) 0.8871(14) 0.108(6) Uani 0.5279(18) 1 d PDU A 1
H85A H 0.7218 1.1282 0.8647 0.161 Uiso 0.5279(18) 1 calc PR A 1
H85B H 0.6995 1.0607 0.8638 0.161 Uiso 0.5279(18) 1 calc PR A 1
H85C H 0.7330 1.0786 0.9145 0.161 Uiso 0.5279(18) 1 calc PR A 1
C91 C 0.7016(8) 1.1834(14) 0.9500(13) 0.113(7) Uani 0.5279(18) 1 d PDU A 1
H91A H 0.6826 1.2049 0.9674 0.169 Uiso 0.5279(18) 1 calc PRD A 1
H91B H 0.7117 1.2145 0.9268 0.169 Uiso 0.5279(18) 1 calc PR A 1
H91C H 0.7226 1.1670 0.9782 0.169 Uiso 0.5279(18) 1 calc PR A 1
O24 O 0.5455(8) 0.9753(12) 0.7489(14) 0.098(4) Uani 0.5279(18) 1 d PDU A 1
P4 P 0.5207(3) 1.1689(5) 0.8420(5) 0.063(2) Uani 0.5279(18) 1 d PDU A 1
O23 O 0.5512(7) 1.2209(13) 0.8357(11) 0.064(3) Uani 0.5279(18) 1 d PU A 1
O21 O 0.5345(7) 1.1048(10) 0.8145(9) 0.068(3) Uani 0.5279(18) 1 d PDU A 1
O36 O 0.4794(9) 1.1853(13) 0.8113(11) 0.058(4) Uani 0.5279(18) 1 d PU A 1
C55 C 0.5200(5) 1.1529(10) 0.9143(15) 0.068(4) Uani 0.5279(18) 1 d PDU A 1
C80 C 0.5077(9) 1.2150(15) 0.9384(11) 0.071(7) Uani 0.5279(18) 1 d PDU A 1
H80D H 0.5063 1.2077 0.9766 0.107 Uiso 0.5279(18) 1 calc PR A 1
H80E H 0.4825 1.2282 0.9177 0.107 Uiso 0.5279(18) 1 calc PR A 1
H80F H 0.5265 1.2492 0.9362 0.107 Uiso 0.5279(18) 1 calc PR A 1
C57 C 0.5602(9) 1.1332(16) 0.9421(11) 0.078(7) Uani 0.5279(18) 1 d PDU A 1
H57D H 0.5607 1.1231 0.9805 0.117 Uiso 0.5279(18) 1 calc PR A 1
H57E H 0.5780 1.1689 0.9398 0.117 Uiso 0.5279(18) 1 calc PR A 1
H57F H 0.5680 1.0949 0.9239 0.117 Uiso 0.5279(18) 1 calc PR A 1
C56 C 0.4915(9) 1.0987(14) 0.9158(14) 0.073(6) Uani 0.5279(18) 1 d PDU A 1
H56D H 0.4902 1.0891 0.9538 0.109 Uiso 0.5279(18) 1 calc PR A 1
H56E H 0.4997 1.0599 0.8987 0.109 Uiso 0.5279(18) 1 calc PR A 1
H56F H 0.4661 1.1121 0.8959 0.109 Uiso 0.5279(18) 1 calc PR A 1
O20 O 0.5873(9) 1.0594(11) 0.7533(13) 0.094(4) Uani 0.5279(18) 1 d PDU A 1
Dy4' Dy 0.56742(7) 1.16296(11) 0.75589(10) 0.0508(4) Uani 0.4721(18) 1 d PU . 2
O34' O 0.5885(9) 1.2738(13) 0.7720(13) 0.059(3) Uani 0.4721(18) 1 d PU A 2
H34E H 0.5857 1.2953 0.7355 0.070 Uiso 0.4721(18) 1 calc PR A 2
C81' C 0.6526(9) 1.1737(14) 0.8635(15) 0.093(3) Uani 0.4721(18) 1 d PDU A 2
O22' O 0.6200(8) 1.1748(16) 0.8299(12) 0.083(2) Uani 0.4721(18) 1 d PDU A 2
O38' O 0.6805(8) 1.2131(15) 0.8821(13) 0.097(3) Uani 0.4721(18) 1 d PDU A 2
C90' C 0.6681(7) 1.1082(14) 0.8830(10) 0.100(3) Uani 0.4721(18) 1 d PDU A 2
C91' C 0.6365(11) 1.0613(16) 0.8876(19) 0.109(7) Uani 0.4721(18) 1 d PDU A 2
H91D H 0.6476 1.0194 0.9008 0.163 Uiso 0.4721(18) 1 calc PR A 2
H91E H 0.6197 1.0557 0.8517 0.163 Uiso 0.4721(18) 1 calc PR A 2
H91F H 0.6215 1.0784 0.9135 0.163 Uiso 0.4721(18) 1 calc PR A 2
C85' C 0.6910(12) 1.079(2) 0.8446(16) 0.112(7) Uani 0.4721(18) 1 d PDU A 2
H85D H 0.6966 1.0331 0.8546 0.169 Uiso 0.4721(18) 1 calc PR A 2
H85E H 0.7151 1.1023 0.8472 0.169 Uiso 0.4721(18) 1 calc PR A 2
H85F H 0.6763 1.0809 0.8071 0.169 Uiso 0.4721(18) 1 calc PR A 2
C88' C 0.6942(11) 1.112(2) 0.9386(13) 0.113(6) Uani 0.4721(18) 1 d PDU A 2
H88D H 0.7021 1.0684 0.9514 0.169 Uiso 0.4721(18) 1 calc PR A 2
H88E H 0.6805 1.1326 0.9645 0.169 Uiso 0.4721(18) 1 calc PR A 2
H88F H 0.7169 1.1379 0.9361 0.169 Uiso 0.4721(18) 1 calc PR A 2
P4' P 0.5007(4) 1.1676(6) 0.8168(5) 0.058(2) Uani 0.4721(18) 1 d PDU . 2
O23' O 0.5326(8) 1.2188(13) 0.8162(12) 0.061(3) Uani 0.4721(18) 1 d PU A 2
O36' O 0.4591(9) 1.1867(11) 0.7848(12) 0.052(4) Uani 0.4721(18) 1 d PU . 2
O21' O 0.5161(8) 1.1102(13) 0.7904(12) 0.064(3) Uani 0.4721(18) 1 d PU A 2
C55' C 0.4984(6) 1.1496(10) 0.8871(16) 0.067(4) Uani 0.4721(18) 1 d PDU A 2
C56' C 0.4687(9) 1.0945(16) 0.8882(14) 0.067(6) Uani 0.4721(18) 1 d PDU A 2
H56A H 0.4672 1.0850 0.9261 0.101 Uiso 0.4721(18) 1 calc PR A 2
H56B H 0.4767 1.0555 0.8711 0.101 Uiso 0.4721(18) 1 calc PR A 2
H56C H 0.4435 1.1084 0.8680 0.101 Uiso 0.4721(18) 1 calc PR A 2
C57' C 0.5387(10) 1.1276(17) 0.9183(12) 0.075(6) Uani 0.4721(18) 1 d PDU A 2
H57A H 0.5375 1.1174 0.9562 0.113 Uiso 0.4721(18) 1 calc PR A 2
H57B H 0.5572 1.1625 0.9176 0.113 Uiso 0.4721(18) 1 calc PR A 2
H57C H 0.5467 1.0890 0.9006 0.113 Uiso 0.4721(18) 1 calc PR A 2
C80' C 0.4858(10) 1.2117(17) 0.9144(12) 0.071(7) Uani 0.4721(18) 1 d PDU A 2
H80A H 0.4840 1.2019 0.9522 0.107 Uiso 0.4721(18) 1 calc PR A 2
H80B H 0.4608 1.2261 0.8940 0.107 Uiso 0.4721(18) 1 calc PR A 2
H80C H 0.5048 1.2460 0.9142 0.107 Uiso 0.4721(18) 1 calc PR A 2
O24' O 0.5342(7) 0.9927(17) 0.7167(15) 0.096(4) Uani 0.4721(18) 1 d PDU A 2
O20' O 0.5707(11) 1.0674(10) 0.7250(16) 0.095(4) Uani 0.4721(18) 1 d PDU A 2
Co1 Co 0.56173(6) 1.51688(11) 0.77443(9) 0.0454(5) Uani 1 1 d U . .
Co2 Co 0.5000 1.78728(18) 0.7500 0.0816(13) Uani 1 2 d SU . .
Co3 Co 0.55208(8) 1.31535(12) 0.81068(11) 0.0642(7) Uani 1 1 d DU . .
Co4 Co 0.70889(9) 1.4213(2) 0.90852(14) 0.1175(14) Uani 1 1 d U . .
Co5 Co 0.5000 1.0455(2) 0.7500 0.1178(16) Uani 1 2 d SDU . .
P1 P 0.54272(13) 1.6656(2) 0.7122(2) 0.0511(10) Uani 1 1 d U A .
P2 P 0.65603(15) 1.4675(3) 0.7946(2) 0.0693(13) Uani 1 1 d U . .
P3 P 0.6269(6) 1.3808(10) 0.9155(8) 0.0873(15) Uani 0.50 1 d PU A 1
P3' P 0.6213(6) 1.3618(10) 0.9094(9) 0.0873(15) Uani 0.50 1 d PU A 2
O2 O 0.5604(3) 1.6131(5) 0.7536(5) 0.0493(19) Uani 1 1 d U A .
O3 O 0.5677(3) 1.5566(6) 0.8517(5) 0.0595(18) Uani 1 1 d U A .
H3D H 0.5502 1.5371 0.8741 0.071 Uiso 1 1 calc R . .
O4 O 0.5429(3) 1.7256(6) 0.7490(5) 0.061(2) Uani 1 1 d U A .
O5 O 0.6210(3) 1.5100(7) 0.7950(5) 0.066(2) Uani 1 1 d U A .
O6 O 0.5037(3) 1.6489(5) 0.6802(5) 0.048(2) Uani 1 1 d U . .
O7 O 0.6140(4) 1.4421(8) 0.9055(5) 0.085(2) Uani 1 1 d U . .
O9 O 0.6467(3) 1.3957(7) 0.7862(5) 0.066(2) Uani 1 1 d U A .
O10 O 0.5645(4) 1.6592(8) 0.9284(6) 0.084(3) Uani 1 1 d DU A .
O46 O 0.6019(4) 1.3266(7) 0.8681(5) 0.077(2) Uani 1 1 d U A .
O45 O 0.6813(4) 1.4821(8) 0.8511(5) 0.083(2) Uani 1 1 d U A .
C21 C 0.5734(6) 1.6788(11) 0.6634(9) 0.075(4) Uani 1 1 d U . .
O13 O 0.5513(5) 1.7723(8) 0.8597(7) 0.099(3) Uani 1 1 d U A .
C24 C 0.6817(6) 1.4946(12) 0.7423(9) 0.079(4) Uani 1 1 d U A .
O14 O 0.6705(10) 1.3678(19) 0.9115(15) 0.090(3) Uani 0.5279(18) 1 d PU A 1
O14' O 0.6610(11) 1.347(2) 0.9045(17) 0.091(2) Uani 0.4721(18) 1 d PU A 2
O16 O 0.7155(5) 1.3068(10) 0.8383(8) 0.114(3) Uani 1 1 d DU A .
C27 C 0.5286(6) 1.6345(13) 1.0148(9) 0.093(6) Uani 1 1 d U A .
H27A H 0.5217 1.6313 1.0507 0.140 Uiso 1 1 calc R . .
H27B H 0.5133 1.6038 0.9896 0.140 Uiso 1 1 calc R . .
H27C H 0.5237 1.6786 1.0007 0.140 Uiso 1 1 calc R . .
O11 O 0.6110(4) 1.5867(9) 0.9592(6) 0.099(3) Uani 1 1 d DU . .
C29 C 0.5456(9) 1.8737(13) 0.9034(13) 0.111(4) Uani 1 1 d U A .
O17 O 0.7530(4) 1.3783(10) 0.8903(8) 0.118(4) Uani 1 1 d DU A .
C34 C 0.6561(6) 1.4845(12) 0.6871(8) 0.086(5) Uani 1 1 d U . .
H34A H 0.6696 1.4979 0.6584 0.129 Uiso 1 1 calc R A .
H34B H 0.6327 1.5104 0.6845 0.129 Uiso 1 1 calc R . .
H34C H 0.6493 1.4386 0.6824 0.129 Uiso 1 1 calc R . .
O19 O 0.6670(5) 1.2444(8) 0.7484(7) 0.092(3) Uani 1 1 d U A .
O18 O 0.6166(9) 1.1687(15) 0.7077(12) 0.081(4) Uani 0.5279(18) 1 d PU A 1
O18' O 0.6354(9) 1.1666(17) 0.7332(14) 0.081(4) Uani 0.4721(18) 1 d PU A 2
C38 C 0.5575(6) 1.7337(10) 0.6257(9) 0.082(5) Uani 1 1 d U A .
H38A H 0.5740 1.7410 0.5994 0.123 Uiso 1 1 calc R . .
H38B H 0.5564 1.7731 0.6472 0.123 Uiso 1 1 calc R . .
H38C H 0.5316 1.7225 0.6062 0.123 Uiso 1 1 calc R . .
O15 O 0.7348(5) 1.4711(12) 0.9736(7) 0.136(4) Uani 1 1 d DU A .
C47 C 0.5745(6) 1.6158(10) 0.6323(8) 0.076(5) Uani 1 1 d U A .
H47A H 0.5910 1.6212 0.6055 0.114 Uiso 1 1 calc R . .
H47B H 0.5485 1.6045 0.6133 0.114 Uiso 1 1 calc R . .
H47C H 0.5847 1.5812 0.6579 0.114 Uiso 1 1 calc R . .
C46 C 0.5729(10) 1.9227(13) 0.8860(13) 0.138(7) Uani 1 1 d U . .
H46A H 0.5812 1.9537 0.9157 0.207 Uiso 1 1 calc R . .
H46B H 0.5598 1.9457 0.8533 0.207 Uiso 1 1 calc R . .
H46C H 0.5953 1.9000 0.8780 0.207 Uiso 1 1 calc R . .
O12 O 0.5080(13) 1.843(3) 0.808(2) 0.090(5) Uani 0.5279(18) 1 d PU A 1
O12' O 0.5190(15) 1.843(3) 0.818(3) 0.090(5) Uani 0.4721(18) 1 d PU A 2
C53 C 0.5811(15) 1.621(3) 0.9699(15) 0.089(3) Uani 0.5279(18) 1 d PDU A 1
C53' C 0.5839(19) 1.622(4) 0.959(2) 0.090(3) Uani 0.4721(18) 1 d PDU A 2
C54 C 0.6256(8) 1.2748(15) 0.9865(10) 0.153(8) Uani 1 1 d U A .
H54A H 0.6196 1.2600 1.0211 0.229 Uiso 1 1 calc R . .
H54B H 0.6528 1.2679 0.9869 0.229 Uiso 1 1 calc RD . .
H54C H 0.6102 1.2503 0.9563 0.229 Uiso 1 1 calc R . .
C58 C 0.6431(7) 1.3842(18) 1.0232(9) 0.142(8) Uani 1 1 d U A .
H58A H 0.6410 1.3688 1.0596 0.213 Uiso 1 1 calc R . .
H58B H 0.6354 1.4298 1.0193 0.213 Uiso 1 1 calc R . .
H58C H 0.6697 1.3799 1.0187 0.213 Uiso 1 1 calc R . .
C59 C 0.7476(6) 1.3299(12) 0.8599(10) 0.123(3) Uani 1 1 d DU . .
C60 C 0.6166(8) 1.3435(19) 0.9792(10) 0.138(7) Uani 1 1 d U . .
C61 C 0.5104(9) 1.9096(14) 0.9096(13) 0.140(7) Uani 1 1 d U . .
H61A H 0.5167 1.9401 0.9401 0.210 Uiso 1 1 calc R . .
H61B H 0.4911 1.8788 0.9169 0.210 Uiso 1 1 calc R . .
H61C H 0.5002 1.9334 0.8759 0.210 Uiso 1 1 calc R . .
C62 C 0.5743(8) 1.3554(18) 0.9812(10) 0.145(8) Uani 1 1 d U A .
H62A H 0.5685 1.3354 1.0141 0.218 Uiso 1 1 calc R . .
H62B H 0.5580 1.3362 0.9488 0.218 Uiso 1 1 calc R . .
H62C H 0.5695 1.4021 0.9818 0.218 Uiso 1 1 calc R . .
C63 C 0.6526(7) 1.2015(12) 0.7139(11) 0.088(3) Uani 1 1 d U . .
C71 C 0.5332(9) 1.8262(13) 0.8533(12) 0.095(4) Uani 1 1 d U . .
C74 C 0.5636(9) 1.8389(13) 0.9540(11) 0.122(7) Uani 1 1 d U . .
H74A H 0.5707 1.8701 0.9838 0.183 Uiso 1 1 calc R A .
H74B H 0.5866 1.8162 0.9480 0.183 Uiso 1 1 calc R . .
H74C H 0.5454 1.8075 0.9635 0.183 Uiso 1 1 calc R . .
C82 C 0.7027(7) 1.1418(12) 0.6825(11) 0.108(6) Uani 1 1 d U . .
H82A H 0.7216 1.1593 0.7131 0.162 Uiso 1 1 calc R A .
H82B H 0.7154 1.1317 0.6521 0.162 Uiso 1 1 calc R . .
H82C H 0.6914 1.1022 0.6941 0.162 Uiso 1 1 calc R . .
C87 C 0.6422(7) 1.1648(13) 0.6170(11) 0.106(6) Uani 1 1 d U . .
H87A H 0.6214 1.1962 0.6061 0.158 Uiso 1 1 calc R A .
H87B H 0.6317 1.1243 0.6284 0.158 Uiso 1 1 calc R . .
H87C H 0.6545 1.1562 0.5861 0.158 Uiso 1 1 calc R . .
C48 C 0.6386(6) 0.9728(12) 0.7522(12) 0.150(7) Uani 1 1 d DU . .
H48A H 0.6579 0.9440 0.7419 0.225 Uiso 1 1 calc R . .
H48B H 0.6369 0.9647 0.7903 0.225 Uiso 1 1 calc R . .
H48C H 0.6459 1.0180 0.7481 0.225 Uiso 1 1 calc R . .
C92 C 0.7181(6) 1.4536(12) 0.7468(9) 0.088(6) Uani 1 1 d U . .
H92A H 0.7320 1.4670 0.7185 0.133 Uiso 1 1 calc R A .
H92B H 0.7111 1.4078 0.7419 0.133 Uiso 1 1 calc R . .
H92C H 0.7345 1.4599 0.7829 0.133 Uiso 1 1 calc R . .
C93 C 0.5823(7) 1.5581(14) 1.0514(10) 0.112(6) Uani 1 1 d U A .
H93A H 0.5731 1.5586 1.0858 0.167 Uiso 1 1 calc R . .
H93B H 0.6103 1.5553 1.0591 0.167 Uiso 1 1 calc R . .
H93C H 0.5716 1.5204 1.0297 0.167 Uiso 1 1 calc R . .
C95 C 0.6878(7) 1.2550(11) 0.6489(10) 0.093(6) Uani 1 1 d U . .
H95A H 0.7070 1.2707 0.6799 0.140 Uiso 1 1 calc R A .
H95B H 0.6673 1.2872 0.6395 0.140 Uiso 1 1 calc R . .
H95C H 0.7000 1.2481 0.6174 0.140 Uiso 1 1 calc R . .
C97 C 0.6712(7) 1.1919(12) 0.6639(11) 0.093(4) Uani 1 1 d U A .
C100 C 0.5699(6) 1.6191(14) 1.0199(9) 0.092(3) Uani 1 1 d U . .
C103 C 0.6135(6) 1.6960(13) 0.6950(10) 0.101(6) Uani 1 1 d U A .
H10A H 0.6306 1.7032 0.6693 0.152 Uiso 1 1 calc R . .
H10B H 0.6234 1.6603 0.7197 0.152 Uiso 1 1 calc R . .
H10C H 0.6122 1.7355 0.7164 0.152 Uiso 1 1 calc R . .
C50 C 0.5712(6) 1.0061(9) 0.7320(9) 0.100(3) Uani 1 1 d DU . .
C146 C 0.6916(7) 1.5652(12) 0.7510(11) 0.104(6) Uani 1 1 d U . .
H14A H 0.7055 1.5798 0.7231 0.157 Uiso 1 1 calc R A .
H14B H 0.7078 1.5711 0.7873 0.157 Uiso 1 1 calc R . .
H14C H 0.6681 1.5905 0.7484 0.157 Uiso 1 1 calc R . .
C150 C 0.5931(7) 1.6772(15) 1.0525(10) 0.119(7) Uani 1 1 d U A .
H15A H 0.5871 1.6800 1.0890 0.178 Uiso 1 1 calc R . .
H15B H 0.5860 1.7178 1.0328 0.178 Uiso 1 1 calc R . .
H15C H 0.6207 1.6696 1.0558 0.178 Uiso 1 1 calc R . .
O25 O 0.6205(6) 1.6684(16) 0.8505(14) 0.089(2) Uani 0.5279(18) 1 d PDU A 1
O26 O 0.6810(7) 1.6409(17) 0.8754(12) 0.109(3) Uani 0.5279(18) 1 d PDU A 1
C75 C 0.6560(7) 1.6864(13) 0.8602(15) 0.102(3) Uani 0.5279(18) 1 d PDU A 1
C4 C 0.6677(6) 1.7561(14) 0.8682(10) 0.107(4) Uani 0.5279(18) 1 d PDU A 1
C36 C 0.6441(11) 1.7947(19) 0.8213(15) 0.119(7) Uani 0.5279(18) 1 d PDU A 1
H36A H 0.6493 1.7788 0.7866 0.179 Uiso 0.5279(18) 1 calc PR A 1
H36B H 0.6511 1.8406 0.8257 0.179 Uiso 0.5279(18) 1 calc PR A 1
H36C H 0.6168 1.7896 0.8215 0.179 Uiso 0.5279(18) 1 calc PR A 1
C37 C 0.7102(9) 1.761(2) 0.8678(15) 0.110(6) Uani 0.5279(18) 1 d PDU A 1
H37A H 0.7152 1.7419 0.8339 0.165 Uiso 0.5279(18) 1 calc PR A 1
H37B H 0.7248 1.7371 0.8991 0.165 Uiso 0.5279(18) 1 calc PR A 1
H37C H 0.7180 1.8064 0.8701 0.165 Uiso 0.5279(18) 1 calc PR A 1
C77 C 0.6593(10) 1.778(2) 0.9228(15) 0.109(6) Uani 0.5279(18) 1 d PDU A 1
H77A H 0.6741 1.7515 0.9522 0.163 Uiso 0.5279(18) 1 calc PR A 1
H77B H 0.6319 1.7730 0.9224 0.163 Uiso 0.5279(18) 1 calc PR A 1
H77C H 0.6666 1.8236 0.9290 0.163 Uiso 0.5279(18) 1 calc PR A 1
O25' O 0.6281(8) 1.6452(18) 0.8531(16) 0.087(2) Uani 0.4721(18) 1 d PDU A 2
O26' O 0.6834(9) 1.6153(19) 0.9033(14) 0.109(3) Uani 0.4721(18) 1 d PDU A 2
C75' C 0.6603(9) 1.6621(19) 0.8835(15) 0.103(3) Uani 0.4721(18) 1 d PDU A 2
C4' C 0.6827(8) 1.7240(18) 0.8901(11) 0.108(4) Uani 0.4721(18) 1 d PDU A 2
C77' C 0.6789(12) 1.745(2) 0.9427(17) 0.111(7) Uani 0.4721(18) 1 d PDU A 2
H77D H 0.6909 1.7879 0.9502 0.166 Uiso 0.4721(18) 1 calc PR A 2
H77E H 0.6914 1.7142 0.9703 0.166 Uiso 0.4721(18) 1 calc PR A 2
H77F H 0.6516 1.7483 0.9441 0.166 Uiso 0.4721(18) 1 calc PR A 2
C37' C 0.7199(10) 1.703(3) 0.8860(18) 0.121(7) Uani 0.4721(18) 1 d PDU A 2
H37D H 0.7378 1.7397 0.8930 0.181 Uiso 0.4721(18) 1 calc PR A 2
H37E H 0.7194 1.6863 0.8491 0.181 Uiso 0.4721(18) 1 calc PR A 2
H37F H 0.7284 1.6689 0.9129 0.181 Uiso 0.4721(18) 1 calc PR A 2
C36' C 0.6633(13) 1.762(2) 0.8459(17) 0.114(6) Uani 0.4721(18) 1 d PDU A 2
H36D H 0.6729 1.8066 0.8500 0.171 Uiso 0.4721(18) 1 calc PR A 2
H36E H 0.6358 1.7617 0.8457 0.171 Uiso 0.4721(18) 1 calc PR A 2
H36F H 0.6678 1.7439 0.8115 0.171 Uiso 0.4721(18) 1 calc PR A 2
C127 C 0.7826(6) 1.2953(11) 0.8459(9) 0.131(3) Uani 0.5279(18) 1 d PDU A 1
C39 C 0.8179(8) 1.331(2) 0.872(2) 0.134(6) Uani 0.5279(18) 1 d PDU A 1
H39A H 0.8294 1.3518 0.8441 0.201 Uiso 0.5279(18) 1 calc PR A 1
H39B H 0.8363 1.3011 0.8936 0.201 Uiso 0.5279(18) 1 calc PR A 1
H39C H 0.8111 1.3647 0.8966 0.201 Uiso 0.5279(18) 1 calc PR A 1
C2 C 0.7782(14) 1.296(2) 0.7849(12) 0.141(6) Uani 0.5279(18) 1 d PDU A 1
H2A H 0.7525 1.2806 0.7679 0.212 Uiso 0.5279(18) 1 calc PR A 1
H2B H 0.7974 1.2673 0.7742 0.212 Uiso 0.5279(18) 1 calc PR A 1
H2C H 0.7817 1.3401 0.7725 0.212 Uiso 0.5279(18) 1 calc PR A 1
C3 C 0.7830(7) 1.2276(11) 0.8668(11) 0.138(5) Uani 0.5279(18) 1 d PDU A 1
H3A H 0.8044 1.2039 0.8567 0.207 Uiso 0.5279(18) 1 calc PR A 1
H3B H 0.7589 1.2061 0.8508 0.207 Uiso 0.5279(18) 1 calc PR A 1
H3C H 0.7861 1.2283 0.9067 0.207 Uiso 0.5279(18) 1 calc PR A 1
C227 C 0.7826(6) 1.2953(11) 0.8459(9) 0.131(3) Uani 0.4721(18) 1 d PDU A 2
C2' C 0.7862(17) 1.296(2) 0.797(2) 0.141(6) Uani 0.4721(18) 1 d PDU A 2
H2D H 0.7623 1.2811 0.7738 0.211 Uiso 0.4721(18) 1 calc PR A 2
H2E H 0.8072 1.2668 0.7929 0.211 Uiso 0.4721(18) 1 calc PR A 2
H2F H 0.7920 1.3399 0.7869 0.211 Uiso 0.4721(18) 1 calc PR A 2
C39' C 0.8194(14) 1.317(3) 0.882(2) 0.134(7) Uani 0.4721(18) 1 d PDU A 2
H39D H 0.8409 1.2927 0.8729 0.200 Uiso 0.4721(18) 1 calc PR A 2
H39E H 0.8182 1.3103 0.9202 0.200 Uiso 0.4721(18) 1 calc PR A 2
H39F H 0.8232 1.3636 0.8756 0.200 Uiso 0.4721(18) 1 calc PR A 2
C3' C 0.7830(7) 1.2276(11) 0.8668(11) 0.138(5) Uani 0.4721(18) 1 d PDU A 2
HD H 0.8038 1.2033 0.8554 0.207 Uiso 0.4721(18) 1 calc PR A 2
HE H 0.7584 1.2067 0.8520 0.207 Uiso 0.4721(18) 1 calc PR A 2
HF H 0.7872 1.2282 0.9068 0.207 Uiso 0.4721(18) 1 calc PR A 2
C44 C 0.6028(8) 0.9713(12) 0.6584(10) 0.151(7) Uani 1 1 d DU . .
H44A H 0.6219 0.9422 0.6480 0.227 Uiso 1 1 calc R A .
H44B H 0.6101 1.0163 0.6536 0.227 Uiso 1 1 calc R . .
H44C H 0.5777 0.9627 0.6352 0.227 Uiso 1 1 calc R . .
C45 C 0.6009(7) 0.9601(9) 0.7164(8) 0.119(4) Uani 1 1 d DU A .
C43 C 0.5891(8) 0.8919(9) 0.7237(11) 0.137(7) Uani 1 1 d DU . .
H43A H 0.6078 0.8623 0.7131 0.205 Uiso 1 1 calc R A .
H43B H 0.5638 0.8841 0.7008 0.205 Uiso 1 1 calc R . .
H43C H 0.5879 0.8847 0.7621 0.205 Uiso 1 1 calc R . .
N1 N 0.5619(9) 1.4096(15) 0.7232(13) 0.060(4) Uani 0.50 1 d PU . 1
O31 O 0.5675(9) 1.3591(15) 0.6948(13) 0.072(5) Uani 0.50 1 d PU . 1
O32 O 0.5585(7) 1.4041(12) 0.7731(11) 0.061(3) Uani 0.50 1 d PU A 1
O33 O 0.5626(8) 1.4656(13) 0.7039(10) 0.056(4) Uani 0.50 1 d PU A 1
N2 N 0.4823(11) 1.3372(16) 0.8103(16) 0.076(4) Uani 0.50 1 d PU . 1
O28 O 0.5103(11) 1.3430(14) 0.8517(16) 0.072(4) Uani 0.50 1 d PU A 1
O29 O 0.4895(8) 1.3221(11) 0.7634(11) 0.069(4) Uani 0.50 1 d PU . 1
O30 O 0.4491(10) 1.3458(17) 0.8188(15) 0.086(6) Uani 0.50 1 d PU . 1
N1' N 0.5274(10) 1.4227(16) 0.8434(14) 0.069(4) Uani 0.50 1 d PU . 2
O31' O 0.5164(10) 1.4651(15) 0.8691(14) 0.082(5) Uani 0.50 1 d PU . 2
O32' O 0.5481(7) 1.4280(12) 0.8055(11) 0.063(3) Uani 0.50 1 d PU A 2
O33' O 0.5203(10) 1.3666(15) 0.8580(15) 0.069(4) Uani 0.50 1 d PU A 2
N2' N 0.5106(10) 1.4959(15) 0.6841(13) 0.062(4) Uani 0.50 1 d PU . 2
O28' O 0.4959(7) 1.5115(10) 0.7262(9) 0.054(5) Uani 0.50 1 d PU . 2
O29' O 0.5474(8) 1.4941(12) 0.6923(10) 0.058(4) Uani 0.50 1 d PU A 2
O30' O 0.4915(9) 1.4951(14) 0.6333(13) 0.076(6) Uani 0.50 1 d PU . 2
O8 O 0.6818(11) 1.512(3) 0.9671(17) 0.127(4) Uani 0.5279(18) 1 d PDU A 1
C42 C 0.7159(10) 1.515(2) 0.988(2) 0.132(4) Uani 0.5279(18) 1 d PDU A 1
C32 C 0.7298(6) 1.5522(17) 1.0395(19) 0.137(4) Uani 0.5279(18) 1 d PDU A 1
C51 C 0.7249(10) 1.5113(19) 1.0873(17) 0.149(7) Uani 0.5279(18) 1 d PDU A 1
H51A H 0.7401 1.4716 1.0881 0.223 Uiso 0.5279(18) 1 calc PR A 1
H51B H 0.6978 1.5000 1.0838 0.223 Uiso 0.5279(18) 1 calc PR A 1
H51C H 0.7335 1.5356 1.1212 0.223 Uiso 0.5279(18) 1 calc PR A 1
C40 C 0.7053(11) 1.6127(14) 1.0377(16) 0.146(7) Uani 0.5279(18) 1 d PDU A 1
H40A H 0.6788 1.6003 1.0381 0.219 Uiso 0.5279(18) 1 calc PR A 1
H40B H 0.7061 1.6372 1.0043 0.219 Uiso 0.5279(18) 1 calc PR A 1
H40C H 0.7153 1.6398 1.0697 0.219 Uiso 0.5279(18) 1 calc PR A 1
C41 C 0.7712(5) 1.5701(15) 1.0426(10) 0.143(5) Uani 0.5279(18) 1 d PDU A 1
H41A H 0.7854 1.5320 1.0342 0.215 Uiso 0.5279(18) 1 calc PR A 1
H41B H 0.7823 1.5853 1.0796 0.215 Uiso 0.5279(18) 1 calc PR A 1
H41C H 0.7729 1.6046 1.0162 0.215 Uiso 0.5279(18) 1 calc PR A 1
O8' O 0.6812(12) 1.536(3) 0.9560(19) 0.125(4) Uani 0.4721(18) 1 d PDU A 2
C51' C 0.7125(13) 1.562(3) 1.0759(17) 0.140(6) Uani 0.4721(18) 1 d PDU A 2
H51D H 0.7199 1.5192 1.0910 0.210 Uiso 0.4721(18) 1 calc PR A 2
H51E H 0.6844 1.5650 1.0661 0.210 Uiso 0.4721(18) 1 calc PR A 2
H51F H 0.7222 1.5953 1.1034 0.210 Uiso 0.4721(18) 1 calc PR A 2
C32' C 0.7290(7) 1.573(2) 1.0261(18) 0.137(4) Uani 0.4721(18) 1 d PDU A 2
C40' C 0.7184(14) 1.641(2) 1.007(2) 0.145(8) Uani 0.4721(18) 1 d PDU A 2
H40D H 0.7310 1.6521 0.9773 0.217 Uiso 0.4721(18) 1 calc PR A 2
H40E H 0.7266 1.6710 1.0378 0.217 Uiso 0.4721(18) 1 calc PR A 2
H40F H 0.6905 1.6439 0.9950 0.217 Uiso 0.4721(18) 1 calc PR A 2
C42' C 0.7135(11) 1.523(4) 0.981(2) 0.132(4) Uani 0.4721(18) 1 d PDU A 2
C41' C 0.7712(5) 1.5701(15) 1.0426(10) 0.143(5) Uani 0.4721(18) 1 d PDU A 2
H41D H 0.7828 1.5821 1.0116 0.215 Uiso 0.4721(18) 1 calc PR A 2
H41E H 0.7789 1.5259 1.0543 0.215 Uiso 0.4721(18) 1 calc PR A 2
H41F H 0.7799 1.6001 1.0729 0.215 Uiso 0.4721(18) 1 calc PR A 2
loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Co Co 0.3494 0.9721 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Dy Dy -0.1892 4.4098 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
O25 Dy1 O6 169.5(8) . 2_656
O25 Dy1 O13 97.5(9) . .
O6 Dy1 O13 93.0(5) 2_656 .
O25 Dy1 O10 87.8(10) . .
O6 Dy1 O10 93.7(5) 2_656 .
O13 Dy1 O10 79.4(6) . .
O25 Dy1 O3 83.0(10) . .
O6 Dy1 O3 87.2(4) 2_656 .
O13 Dy1 O3 156.6(5) . .
O10 Dy1 O3 77.3(5) . .
O25 Dy1 O2 86.4(8) . .
O6 Dy1 O2 86.6(4) 2_656 .
O13 Dy1 O2 134.4(5) . .
O10 Dy1 O2 146.2(5) . .
O3 Dy1 O2 69.0(4) . .
O25 Dy1 O25' 11.3(15) . .
O6 Dy1 O25' 158.4(9) 2_656 .
O13 Dy1 O25' 108.1(9) . .
O10 Dy1 O25' 86.3(10) . .
O3 Dy1 O25' 71.7(10) . .
O2 Dy1 O25' 81.6(8) . .
O25 Dy1 O4 100.7(11) . .
O6 Dy1 O4 82.4(4) 2_656 .
O13 Dy1 O4 75.4(5) . .
O10 Dy1 O4 154.2(5) . .
O3 Dy1 O4 127.7(4) . .
O2 Dy1 O4 59.3(4) . .
O25' Dy1 O4 106.5(11) . .
O25 Dy1 P1 97.9(9) . .
O6 Dy1 P1 79.7(3) 2_656 .
O13 Dy1 P1 105.4(5) . .
O10 Dy1 P1 171.9(4) . .
O3 Dy1 P1 97.7(3) . .
O2 Dy1 P1 29.8(3) . .
O25' Dy1 P1 98.1(9) . .
O4 Dy1 P1 30.0(3) . .
O25 Dy1 Dy2 47.4(10) . .
O6 Dy1 Dy2 123.5(3) 2_656 .
O13 Dy1 Dy2 133.5(4) . .
O10 Dy1 Dy2 71.3(4) . .
O3 Dy1 Dy2 36.9(3) . .
O2 Dy1 Dy2 80.4(3) . .
O25' Dy1 Dy2 36.7(10) . .
O4 Dy1 Dy2 131.6(3) . .
P1 Dy1 Dy2 108.45(9) . .
O8' Dy2 O7 91.8(17) . .
O8' Dy2 O11 76.5(14) . .
O7 Dy2 O11 94.0(6) . .
O8' Dy2 O25' 110.0(18) . .
O7 Dy2 O25' 157.1(8) . .
O11 Dy2 O25' 84.7(9) . .
O8' Dy2 O26' 56.3(18) . .
O7 Dy2 O26' 146.2(9) . .
O11 Dy2 O26' 89.5(9) . .
O25' Dy2 O26' 56.8(10) . .
O8' Dy2 O3 153.0(14) . .
O7 Dy2 O3 83.0(5) . .
O11 Dy2 O3 77.4(4) . .
O25' Dy2 O3 74.3(7) . .
O26' Dy2 O3 130.4(9) . .
O8' Dy2 O5 135.2(14) . .
O7 Dy2 O5 85.9(5) . .
O11 Dy2 O5 148.3(4) . .
O25' Dy2 O5 83.5(9) . .
O26' Dy2 O5 108.1(9) . .
O3 Dy2 O5 71.1(4) . .
O8' Dy2 O8 13(3) . .
O7 Dy2 O8 79.3(14) . .
O11 Dy2 O8 77.6(12) . .
O25' Dy2 O8 122.4(15) . .
O26' Dy2 O8 68.6(16) . .
O3 Dy2 O8 148.1(11) . .
O5 Dy2 O8 133.1(12) . .
O8' Dy2 O45 76.3(14) . .
O7 Dy2 O45 82.7(5) . .
O11 Dy2 O45 152.5(5) . .
O25' Dy2 O45 108.6(8) . .
O26' Dy2 O45 79.0(9) . .
O3 Dy2 O45 128.8(4) . .
O5 Dy2 O45 59.0(4) . .
O8 Dy2 O45 75.0(11) . .
O8' Dy2 C75' 81.4(18) . .
O7 Dy2 C75' 172.4(8) . .
O11 Dy2 C75' 81.0(10) . .
O25' Dy2 C75' 28.8(6) . .
O26' Dy2 C75' 29.0(5) . .
O3 Dy2 C75' 101.3(7) . .
O5 Dy2 C75' 101.4(9) . .
O8 Dy2 C75' 93.9(15) . .
O45 Dy2 C75' 99.0(9) . .
O8' Dy2 O26 73.6(17) . .
O7 Dy2 O26 159.5(6) . .
O11 Dy2 O26 96.4(8) . .
O25' Dy2 O26 42.2(9) . .
O26' Dy2 O26 17.4(10) . .
O3 Dy2 O26 116.4(6) . .
O5 Dy2 O26 94.3(7) . .
O8 Dy2 O26 85.8(14) . .
O45 Dy2 O26 79.9(7) . .
C75' Dy2 O26 19.4(10) . .
O8' Dy2 O25 111.6(18) . .
O7 Dy2 O25 153.2(6) . .
O11 Dy2 O25 79.9(8) . .
O25' Dy2 O25 5.8(11) . .
O26' Dy2 O25 60.4(10) . .
O3 Dy2 O25 70.2(6) . .
O5 Dy2 O25 86.1(7) . .
O8 Dy2 O25 123.8(15) . .
O45 Dy2 O25 114.4(7) . .
C75' Dy2 O25 31.6(9) . .
O26 Dy2 O25 46.8(5) . .
O22 Dy3 O9 164.8(8) . .
O22 Dy3 O16 106.1(9) . .
O9 Dy3 O16 88.9(6) . .
O22 Dy3 O19 87.9(9) . .
O9 Dy3 O19 97.6(5) . .
O16 Dy3 O19 78.0(6) . .
O22 Dy3 O14' 94.5(14) . .
O9 Dy3 O14' 85.9(12) . .
O16 Dy3 O14' 79.8(11) . .
O19 Dy3 O14' 157.4(11) . .
O22 Dy3 O34' 77.1(11) . .
O9 Dy3 O34' 89.6(8) . .
O16 Dy3 O34' 158.7(7) . .
O19 Dy3 O34' 81.2(7) . .
O14' Dy3 O34' 121.3(11) . .
O22 Dy3 O34 82.3(11) . .
O9 Dy3 O34 85.4(7) . .
O16 Dy3 O34 150.9(5) . .
O19 Dy3 O34 74.6(5) . .
O14' Dy3 O34 128.0(10) . .
O34' Dy3 O34 8.4(9) . .
O22 Dy3 O46 80.5(8) . .
O9 Dy3 O46 87.4(4) . .
O16 Dy3 O46 134.9(6) . .
O19 Dy3 O46 147.0(6) . .
O14' Dy3 O46 55.1(10) . .
O34' Dy3 O46 66.2(7) . .
O34 Dy3 O46 73.3(4) . .
O22 Dy3 O38' 38.4(10) . .
O9 Dy3 O38' 154.6(8) . .
O16 Dy3 O38' 69.5(9) . .
O19 Dy3 O38' 91.1(9) . .
O14' Dy3 O38' 77.4(13) . .
O34' Dy3 O38' 115.4(10) . .
O34 Dy3 O38' 120.0(10) . .
O46 Dy3 O38' 98.3(8) . .
O22 Dy3 O14 102.7(12) . .
O9 Dy3 O14 79.3(10) . .
O16 Dy3 O14 73.1(9) . .
O19 Dy3 O14 150.9(9) . .
O14' Dy3 O14 9.5(18) . .
O34' Dy3 O14 127.3(9) . .
O34 Dy3 O14 133.2(8) . .
O46 Dy3 O14 62.1(9) . .
O38' Dy3 O14 81.6(11) . .
O22 Dy3 C81' 12.2(10) . .
O9 Dy3 C81' 176.9(7) . .
O16 Dy3 C81' 94.1(8) . .
O19 Dy3 C81' 83.1(9) . .
O14' Dy3 C81' 94.7(14) . .
O34' Dy3 C81' 87.5(9) . .
O34 Dy3 C81' 91.9(9) . .
O46 Dy3 C81' 90.5(9) . .
O38' Dy3 C81' 28.1(4) . .
O14 Dy3 C81' 101.6(12) . .
O22 Dy3 O22' 18.3(9) . .
O9 Dy3 O22' 150.2(6) . .
O16 Dy3 O22' 118.4(7) . .
O19 Dy3 O22' 78.4(7) . .
O14' Dy3 O22' 109.2(13) . .
O34' Dy3 O22' 60.6(9) . .
O34 Dy3 O22' 64.9(8) . .
O46 Dy3 O22' 81.3(7) . .
O38' Dy3 O22' 55.1(6) . .
O14 Dy3 O22' 118.2(11) . .
C81' Dy3 O22' 27.0(3) . .
O18 Dy4 O20 75.7(11) . .
O18 Dy4 O38 111.0(10) . .
O20 Dy4 O38 73.0(11) . .
O18 Dy4 O23 147.4(10) . .
O20 Dy4 O23 131.8(10) . .
O38 Dy4 O23 95.9(9) . .
O18 Dy4 O34 74.5(8) . .
O20 Dy4 O34 148.2(9) . .
O38 Dy4 O34 128.7(9) . .
O23 Dy4 O34 74.3(6) . .
O18 Dy4 O22 99.6(11) . .
O20 Dy4 O22 121.0(10) . .
O38 Dy4 O22 53.6(7) . .
O23 Dy4 O22 81.4(9) . .
O34 Dy4 O22 75.0(8) . .
O18 Dy4 O21 139.1(10) . .
O20 Dy4 O21 70.6(9) . .
O38 Dy4 O21 80.6(8) . .
O23 Dy4 O21 61.3(8) . .
O34 Dy4 O21 129.8(5) . .
O22 Dy4 O21 117.2(8) . .
O18 Dy4 C81 104.5(9) . .
O20 Dy4 C81 96.1(9) . .
O38 Dy4 C81 27.1(4) . .
O23 Dy4 C81 91.0(7) . .
O34 Dy4 C81 101.7(8) . .
O22 Dy4 C81 26.8(4) . .
O21 Dy4 C81 101.5(7) . .
O18 Dy4 P4 156.2(9) . .
O20 Dy4 P4 102.3(8) . .
O38 Dy4 P4 90.5(7) . .
O23 Dy4 P4 29.8(7) . .
O34 Dy4 P4 100.6(2) . .
O22 Dy4 P4 101.6(7) . .
O21 Dy4 P4 31.7(5) . .
C81 Dy4 P4 99.3(4) . .
O18 Dy4 Co3 112.9(8) . .
O20 Dy4 Co3 158.6(8) . .
O38 Dy4 Co3 118.5(6) . .
O23 Dy4 Co3 35.0(6) . .
O34 Dy4 Co3 39.52(12) . .
O22 Dy4 Co3 78.2(5) . .
O21 Dy4 Co3 92.6(5) . .
C81 Dy4 Co3 100.4(4) . .
P4 Dy4 Co3 61.7(2) . .
O18 Dy4 Dy3 80.9(9) . .
O20 Dy4 Dy3 141.2(8) . .
O38 Dy4 Dy3 87.4(7) . .
O23 Dy4 Dy3 82.3(7) . .
O34 Dy4 Dy3 41.8(6) . .
O22 Dy4 Dy3 34.5(5) . .
O21 Dy4 Dy3 139.9(5) . .
C81 Dy4 Dy3 60.4(5) . .
P4 Dy4 Dy3 111.3(3) . .
Co3 Dy4 Dy3 60.12(6) . .
Co3 O34 Dy4 97.9(7) . .
Co3 O34 Dy3 99.4(7) . .
Dy4 O34 Dy3 96.5(12) . .
Co3 O34 H34D 119.4 . .
Dy4 O34 H34D 119.4 . .
Dy3 O34 H34D 119.4 . .
O22 C81 O38 111(2) . .
O22 C81 C90 134(2) . .
O38 C81 C90 114.5(8) . .
O22 C81 Dy4 58.5(17) . .
O38 C81 Dy4 53.7(11) . .
C90 C81 Dy4 165.6(9) . .
C91 C90 C85 109.4(9) . .
C91 C90 C81 110.2(10) . .
C85 C90 C81 109.0(9) . .
C91 C90 C88 109.6(9) . .
C85 C90 C88 109.3(10) . .
C81 C90 C88 109.4(8) . .
C81 O22 Dy3 154(2) . .
C81 O22 Dy4 94.7(19) . .
Dy3 O22 Dy4 103.5(10) . .
C81 O38 Dy4 99.3(14) . .
C90 C88 H88A 109.5 . .
C90 C88 H88B 109.5 . .
H88A C88 H88B 109.5 . .
C90 C88 H88C 109.5 . .
H88A C88 H88C 109.5 . .
H88B C88 H88C 109.5 . .
C90 C85 H85A 109.5 . .
C90 C85 H85B 109.5 . .
H85A C85 H85B 109.5 . .
C90 C85 H85C 109.5 . .
H85A C85 H85C 109.5 . .
H85B C85 H85C 109.5 . .
C90 C91 H91A 109.5 . .
C90 C91 H91B 109.5 . .
H91A C91 H91B 109.5 . .
C90 C91 H91C 109.5 . .
H91A C91 H91C 109.5 . .
H91B C91 H91C 109.5 . .
C50 O24 Co5 105.2(18) . .
O23 P4 O36 114.3(14) . .
O23 P4 O21 104.2(13) . .
O36 P4 O21 107.8(16) . .
O23 P4 C55 111.6(14) . .
O36 P4 C55 109.0(11) . .
O21 P4 C55 109.6(11) . .
O23 P4 Dy4 48.5(9) . .
O36 P4 Dy4 121.0(11) . .
O21 P4 Dy4 56.0(8) . .
C55 P4 Dy4 130.0(7) . .
P4 O23 Co3 137.7(15) . .
P4 O23 Dy4 101.7(14) . .
Co3 O23 Dy4 103.9(10) . .
P4 O21 Co5 126.7(14) . .
P4 O21 Dy4 92.3(10) . .
Co5 O21 Dy4 112.6(9) . .
C56 C55 C57 111.5(15) . .
C56 C55 C80 111.5(15) . .
C57 C55 C80 111.5(15) . .
C56 C55 P4 107.3(16) . .
C57 C55 P4 107.4(16) . .
C80 C55 P4 107.3(16) . .
C55 C80 H80D 109.5 . .
C55 C80 H80E 109.5 . .
H80D C80 H80E 109.5 . .
C55 C80 H80F 109.5 . .
H80D C80 H80F 109.5 . .
H80E C80 H80F 109.5 . .
C55 C57 H57D 109.5 . .
C55 C57 H57E 109.5 . .
H57D C57 H57E 109.5 . .
C55 C57 H57F 109.5 . .
H57D C57 H57F 109.5 . .
H57E C57 H57F 109.5 . .
C55 C56 H56D 109.5 . .
C55 C56 H56E 109.5 . .
H56D C56 H56E 109.5 . .
C55 C56 H56F 109.5 . .
H56D C56 H56F 109.5 . .
H56E C56 H56F 109.5 . .
C50 O20 Dy4 155(2) . .
O36' Dy4' O20' 98.4(15) 2_656 .
O36' Dy4' O22' 152.4(12) 2_656 .
O20' Dy4' O22' 106.7(14) . .
O36' Dy4' O34' 85.9(13) 2_656 .
O20' Dy4' O34' 154.1(11) . .
O22' Dy4' O34' 66.5(12) . .
O36' Dy4' O21' 88.1(11) 2_656 .
O20' Dy4' O21' 79.2(11) . .
O22' Dy4' O21' 107.6(11) . .
O34' Dy4' O21' 126.6(8) . .
O36' Dy4' O23' 85.8(12) 2_656 .
O20' Dy4' O23' 137.5(11) . .
O22' Dy4' O23' 83.5(10) . .
O34' Dy4' O23' 68.1(9) . .
O21' Dy4' O23' 58.6(10) . .
O36' Dy4' O18' 111.8(12) 2_656 .
O20' Dy4' O18' 80.1(13) . .
O22' Dy4' O18' 62.7(11) . .
O34' Dy4' O18' 74.7(10) . .
O21' Dy4' O18' 153.1(9) . .
O23' Dy4' O18' 137.4(11) . .
O36' Dy4' P4' 23.0(9) 2_656 2_656
O20' Dy4' P4' 84.1(12) . 2_656
O22' Dy4' P4' 167.5(7) . 2_656
O34' Dy4' P4' 106.4(9) . 2_656
O21' Dy4' P4' 67.6(7) . 2_656
O23' Dy4' P4' 84.3(8) . 2_656
O18' Dy4' P4' 126.8(8) . 2_656
O36' Dy4' P4' 82.3(10) 2_656 .
O20' Dy4' P4' 108.2(9) . .
O22' Dy4' P4' 100.3(7) . .
O34' Dy4' P4' 97.7(6) . .
O21' Dy4' P4' 29.1(7) . .
O23' Dy4' P4' 30.1(8) . .
O18' Dy4' P4' 162.9(9) . .
P4' Dy4' P4' 69.8(4) 2_656 .
O36' Dy4' Co5 81.0(9) 2_656 .
O20' Dy4' Co5 54.0(10) . .
O22' Dy4' Co5 123.3(8) . .
O34' Dy4' Co5 151.3(6) . .
O21' Dy4' Co5 28.3(7) . .
O23' Dy4' Co5 85.5(7) . .
O18' Dy4' Co5 133.9(8) . .
P4' Dy4' Co5 57.9(3) 2_656 .
P4' Dy4' Co5 55.5(3) . .
Co3 O34' Dy3 107.6(13) . .
Co3 O34' Dy4' 106.3(11) . .
Dy3 O34' Dy4' 120.3(14) . .
Co3 O34' H34E 107.3 . .
Dy3 O34' H34E 107.3 . .
Dy4' O34' H34E 107.3 . .
O22' C81' O38' 138(3) . .
O22' C81' C90' 117(2) . .
O38' C81' C90' 104(2) . .
O22' C81' Dy3 78(2) . .
O38' C81' Dy3 60.7(18) . .
C90' C81' Dy3 158.9(18) . .
C81' O22' Dy4' 167(3) . .
C81' O22' Dy3 75(2) . .
Dy4' O22' Dy3 107.4(10) . .
C81' O38' Dy3 91(2) . .
C81' C90' C85' 111.7(11) . .
C81' C90' C91' 111.7(12) . .
C85' C90' C91' 107.2(12) . .
C81' C90' C88' 111.6(11) . .
C85' C90' C88' 107.2(12) . .
C91' C90' C88' 107.2(11) . .
C90' C91' H91D 109.5 . .
C90' C91' H91E 109.5 . .
H91D C91' H91E 109.5 . .
C90' C91' H91F 109.5 . .
H91D C91' H91F 109.5 . .
H91E C91' H91F 109.5 . .
C90' C85' H85D 109.5 . .
C90' C85' H85E 109.5 . .
H85D C85' H85E 109.5 . .
C90' C85' H85F 109.5 . .
H85D C85' H85F 109.5 . .
H85E C85' H85F 109.5 . .
C90' C88' H88D 109.5 . .
C90' C88' H88E 109.5 . .
H88D C88' H88E 109.5 . .
C90' C88' H88F 109.5 . .
H88D C88' H88F 109.5 . .
H88E C88' H88F 109.5 . .
O21' P4' O23' 101.6(16) . .
O21' P4' O36' 111.0(18) . .
O23' P4' O36' 116.0(15) . .
O21' P4' C55' 110.6(12) . .
O23' P4' C55' 108.9(15) . .
O36' P4' C55' 108.7(12) . .
O21' P4' Dy4' 91.9(14) . 2_656
O23' P4' Dy4' 125.0(12) . 2_656
O36' P4' Dy4' 19.2(10) . 2_656
C55' P4' Dy4' 115.5(8) . 2_656
O21' P4' Dy4' 51.3(11) . .
O23' P4' Dy4' 51.4(10) . .
O36' P4' Dy4' 119.7(10) . .
C55' P4' Dy4' 131.6(8) . .
Dy4' P4' Dy4' 110.1(4) 2_656 .
P4' O23' Co3 152.6(15) . .
P4' O23' Dy4' 98.5(15) . .
Co3 O23' Dy4' 101.0(10) . .
Dy4' O36' P4' 137.8(17) 2_656 .
P4' O21' Co5 140(2) . .
P4' O21' Dy4' 99.6(14) . .
Co5 O21' Dy4' 109.2(12) . .
C57' C55' C56' 109.8(17) . .
C57' C55' C80' 109.7(17) . .
C56' C55' C80' 109.7(17) . .
C57' C55' P4' 109.2(17) . .
C56' C55' P4' 109.2(17) . .
C80' C55' P4' 109.2(17) . .
C55' C56' H56A 109.5 . .
C55' C56' H56B 109.5 . .
H56A C56' H56B 109.5 . .
C55' C56' H56C 109.5 . .
H56A C56' H56C 109.5 . .
H56B C56' H56C 109.5 . .
C55' C57' H57A 109.5 . .
C55' C57' H57B 109.5 . .
H57A C57' H57B 109.5 . .
C55' C57' H57C 109.5 . .
H57A C57' H57C 109.5 . .
H57B C57' H57C 109.5 . .
C55' C80' H80A 109.5 . .
C55' C80' H80B 109.5 . .
H80A C80' H80B 109.5 . .
C55' C80' H80C 109.5 . .
H80A C80' H80C 109.5 . .
H80B C80' H80C 109.5 . .
C50 O24' Co5 116(2) . .
C50 O20' Dy4' 150(3) . .
O28' Co1 O2 94.5(6) 2_656 .
O28' Co1 O33 98.8(10) 2_656 .
O2 Co1 O33 106.5(8) . .
O28' Co1 O29' 86.1(10) 2_656 .
O2 Co1 O29' 88.8(8) . .
O33 Co1 O29' 22.7(8) . .
O28' Co1 O3 86.8(7) 2_656 .
O2 Co1 O3 81.2(5) . .
O33 Co1 O3 170.0(8) . .
O29' Co1 O3 167.3(9) . .
O28' Co1 O5 164.7(7) 2_656 .
O2 Co1 O5 95.7(5) . .
O33 Co1 O5 89.2(8) . .
O29' Co1 O5 105.5(9) . .
O3 Co1 O5 83.5(5) . .
O28' Co1 O32' 69.4(9) 2_656 .
O2 Co1 O32' 161.9(7) . .
O33 Co1 O32' 84.9(10) . .
O29' Co1 O32' 98.0(10) . .
O3 Co1 O32' 89.4(8) . .
O5 Co1 O32' 98.6(8) . .
O28' Co1 O32 84.2(9) 2_656 .
O2 Co1 O32 164.8(7) . .
O33 Co1 O32 58.9(10) . .
O29' Co1 O32 75.9(10) . .
O3 Co1 O32 113.9(7) . .
O5 Co1 O32 88.8(7) . .
O32' Co1 O32 27.5(8) . .
O28' Co1 Dy2 125.6(6) 2_656 .
O2 Co1 Dy2 92.5(3) . .
O33 Co1 Dy2 130.3(8) . .
O29' Co1 Dy2 148.0(8) . .
O3 Co1 Dy2 41.3(3) . .
O5 Co1 Dy2 42.6(3) . .
O32' Co1 Dy2 90.5(8) . .
O32 Co1 Dy2 100.6(7) . .
O12 Co2 O12 102(3) 2_656 .
O12 Co2 O4 113.0(18) 2_656 .
O12 Co2 O4 114.6(14) . .
O12 Co2 O4 114.6(15) 2_656 2_656
O12 Co2 O4 113.0(18) . 2_656
O4 Co2 O4 100.5(7) . 2_656
O12 Co2 O12' 105.7(12) 2_656 .
O12 Co2 O12' 11(3) . .
O4 Co2 O12' 104.1(15) . .
O4 Co2 O12' 118.6(19) 2_656 .
O12 Co2 O12' 11(3) 2_656 2_656
O12 Co2 O12' 105.7(12) . 2_656
O4 Co2 O12' 118.6(19) . 2_656
O4 Co2 O12' 104.1(15) 2_656 2_656
O12' Co2 O12' 111(4) . 2_656
O34' Co3 O23 77.7(10) . .
O34' Co3 O28 170.2(11) . .
O23 Co3 O28 93.2(11) . .
O34' Co3 O46 80.3(11) . .
O23 Co3 O46 87.6(9) . .
O28 Co3 O46 103.3(13) . .
O34' Co3 O33' 171.7(14) . .
O23 Co3 O33' 105.5(11) . .
O28 Co3 O33' 16.8(13) . .
O46 Co3 O33' 92.1(11) . .
O34' Co3 O32 91.1(11) . .
O23 Co3 O32 168.4(10) . .
O28 Co3 O32 97.8(11) . .
O46 Co3 O32 93.3(9) . .
O33' Co3 O32 86.0(11) . .
O34' Co3 O23' 83.0(10) . .
O23 Co3 O23' 20.4(10) . .
O28 Co3 O23' 87.1(11) . .
O46 Co3 O23' 107.9(9) . .
O33' Co3 O23' 102.6(11) . .
O32 Co3 O23' 156.6(11) . .
O34' Co3 O29 90.8(12) . 2_656
O23 Co3 O29 106.1(10) . 2_656
O28 Co3 O29 88.2(14) . 2_656
O46 Co3 O29 161.8(7) . 2_656
O33' Co3 O29 95.6(12) . 2_656
O32 Co3 O29 70.9(10) . 2_656
O23' Co3 O29 86.5(10) . 2_656
O34' Co3 O34 6.2(16) . .
O23 Co3 O34 83.4(9) . .
O28 Co3 O34 173.0(11) . .
O46 Co3 O34 82.7(7) . .
O33' Co3 O34 169.6(9) . .
O32 Co3 O34 85.3(10) . .
O23' Co3 O34 87.6(8) . .
O29 Co3 O34 86.9(10) 2_656 .
O34' Co3 O29 116.1(12) . .
O23 Co3 O29 98.1(10) . .
O28 Co3 O29 61.0(13) . .
O46 Co3 O29 163.4(7) . .
O33' Co3 O29 71.4(12) . .
O32 Co3 O29 84.2(9) . .
O23' Co3 O29 78.2(9) . .
O29 Co3 O29 28.4(11) 2_656 .
O34 Co3 O29 113.3(9) . .
O34' Co3 O32' 116.6(10) . .
O23 Co3 O32' 163.9(10) . .
O28 Co3 O32' 73.0(10) . .
O46 Co3 O32' 87.7(8) . .
O33' Co3 O32' 59.4(11) . .
O32 Co3 O32' 27.5(8) . .
O23' Co3 O32' 157.3(9) . .
O29 Co3 O32' 82.1(9) 2_656 .
O34 Co3 O32' 111.2(8) . .
O29 Co3 O32' 82.5(9) . .
O34' Co3 Dy4 37.1(8) . .
O23 Co3 Dy4 41.1(6) . .
O28 Co3 Dy4 133.3(8) . .
O46 Co3 Dy4 86.9(4) . .
O33' Co3 Dy4 146.5(9) . .
O32 Co3 Dy4 127.4(7) . .
O23' Co3 Dy4 46.9(6) . .
O29 Co3 Dy4 95.5(6) 2_656 .
O34 Co3 Dy4 42.5(6) . .
O29 Co3 Dy4 107.7(6) . .
O32' Co3 Dy4 153.7(6) . .
O14 Co4 O17 113.2(14) . .
O14 Co4 O15 121.5(13) . .
O17 Co4 O15 99.5(8) . .
O14 Co4 O45 98.5(13) . .
O17 Co4 O45 115.0(7) . .
O15 Co4 O45 110.0(8) . .
O14 Co4 O14' 6(2) . .
O17 Co4 O14' 108.4(12) . .
O15 Co4 O14' 127.2(12) . .
O45 Co4 O14' 97.7(12) . .
O21' Co5 O21' 76.7(17) . 2_656
O21' Co5 O24' 110.6(14) . 2_656
O21' Co5 O24' 121.9(12) 2_656 2_656
O21' Co5 O24' 121.9(12) . .
O21' Co5 O24' 110.6(14) 2_656 .
O24' Co5 O24' 112(2) 2_656 .
O21' Co5 O24 132.6(11) . 2_656
O21' Co5 O24 111.5(13) 2_656 2_656
O24' Co5 O24 24.4(12) 2_656 2_656
O24' Co5 O24 99.5(12) . 2_656
O21' Co5 O24 111.5(13) . .
O21' Co5 O24 132.6(11) 2_656 .
O24' Co5 O24 99.5(12) 2_656 .
O24' Co5 O24 24.4(12) . .
O24 Co5 O24 96.6(13) 2_656 .
O21' Co5 O21 18.9(9) . .
O21' Co5 O21 94.0(11) 2_656 .
O24' Co5 O21 107.8(12) 2_656 .
O24' Co5 O21 108.7(10) . .
O24 Co5 O21 132.1(10) 2_656 .
O24 Co5 O21 94.1(11) . .
O21' Co5 O21 94.0(11) . 2_656
O21' Co5 O21 18.9(9) 2_656 2_656
O24' Co5 O21 108.7(10) 2_656 2_656
O24' Co5 O21 107.8(12) . 2_656
O24 Co5 O21 94.1(11) 2_656 2_656
O24 Co5 O21 132.1(10) . 2_656
O21 Co5 O21 112.1(12) . 2_656
O21' Co5 Dy4' 42.5(9) . .
O21' Co5 Dy4' 67.4(9) 2_656 .
O24' Co5 Dy4' 151.8(11) 2_656 .
O24' Co5 Dy4' 85.4(9) . .
O24 Co5 Dy4' 175.0(6) 2_656 .
O24 Co5 Dy4' 87.4(7) . .
O21 Co5 Dy4' 44.1(6) . .
O21 Co5 Dy4' 85.4(6) 2_656 .
O21' Co5 Dy4' 67.4(9) . 2_656
O21' Co5 Dy4' 42.5(9) 2_656 2_656
O24' Co5 Dy4' 85.4(9) 2_656 2_656
O24' Co5 Dy4' 151.8(11) . 2_656
O24 Co5 Dy4' 87.4(7) 2_656 2_656
O24 Co5 Dy4' 175.0(7) . 2_656
O21 Co5 Dy4' 85.4(6) . 2_656
O21 Co5 Dy4' 44.1(6) 2_656 2_656
Dy4' Co5 Dy4' 88.82(13) . 2_656
O6 P1 O2 114.0(6) . .
O6 P1 O4 113.3(7) . .
O2 P1 O4 102.3(7) . .
O6 P1 C21 107.2(9) . .
O2 P1 C21 109.6(8) . .
O4 P1 C21 110.5(9) . .
O6 P1 Dy1 121.0(4) . .
O2 P1 Dy1 50.2(4) . .
O4 P1 Dy1 53.1(5) . .
C21 P1 Dy1 131.8(8) . .
O9 P2 O5 113.8(8) . .
O9 P2 O45 112.8(9) . .
O5 P2 O45 102.0(7) . .
O9 P2 C24 109.1(9) . .
O5 P2 C24 110.7(9) . .
O45 P2 C24 108.1(10) . .
O9 P2 Dy2 120.6(5) . .
O5 P2 Dy2 50.5(5) . .
O45 P2 Dy2 52.6(5) . .
C24 P2 Dy2 130.3(8) . .
O7 P3 O14 116(2) . .
O7 P3 O46 111.5(15) . .
O14 P3 O46 102.9(16) . .
O7 P3 C60 115.1(17) . .
O14 P3 C60 110(2) . .
O46 P3 C60 98.8(17) . .
O7 P3 Dy3 120.5(13) . .
O14 P3 Dy3 56.7(13) . .
O46 P3 Dy3 47.5(6) . .
C60 P3 Dy3 122.4(15) . .
O46 P3' O14' 100(2) . .
O46 P3' O7 116.2(17) . .
O14' P3' O7 110(2) . .
O46 P3' C60 120(2) . .
O14' P3' C60 108(2) . .
O7 P3' C60 102.5(16) . .
O46 P3' Dy3 52.1(9) . .
O14' P3' Dy3 49.3(16) . .
O7 P3' Dy3 118.7(12) . .
C60 P3' Dy3 137.3(15) . .
P1 O2 Co1 146.7(7) . .
P1 O2 Dy1 100.0(5) . .
Co1 O2 Dy1 104.1(5) . .
Co1 O3 Dy1 105.0(5) . .
Co1 O3 Dy2 103.2(4) . .
Dy1 O3 Dy2 106.3(5) . .
Co1 O3 H3D 113.8 . .
Dy1 O3 H3D 113.8 . .
Dy2 O3 H3D 113.8 . .
P1 O4 Co2 127.5(8) . .
P1 O4 Dy1 96.9(6) . .
Co2 O4 Dy1 109.7(5) . .
P2 O5 Co1 146.1(9) . .
P2 O5 Dy2 100.1(6) . .
Co1 O5 Dy2 101.4(4) . .
P1 O6 Dy1 148.3(7) . 2_656
P3 O7 P3' 12.0(15) . .
P3 O7 Dy2 142.3(13) . .
P3' O7 Dy2 150.7(11) . .
P2 O9 Dy3 147.7(8) . .
C53' O10 C53 12(2) . .
C53' O10 Dy1 129(2) . .
C53 O10 Dy1 139.9(17) . .
P3' O46 P3 7.7(17) . .
P3' O46 Co3 147.2(12) . .
P3 O46 Co3 143.2(10) . .
P3' O46 Dy3 101.6(12) . .
P3 O46 Dy3 99.9(9) . .
Co3 O46 Dy3 104.2(5) . .
P2 O45 Co4 130.0(10) . .
P2 O45 Dy2 97.4(6) . .
Co4 O45 Dy2 108.5(6) . .
C38 C21 C47 111.6(19) . .
C38 C21 C103 110.1(19) . .
C47 C21 C103 110.3(18) . .
C38 C21 P1 109.2(13) . .
C47 C21 P1 107.3(14) . .
C103 C21 P1 108.3(15) . .
C71 O13 Dy1 151.8(19) . .
C146 C24 C34 110(2) . .
C146 C24 C92 111(2) . .
C34 C24 C92 109.7(17) . .
C146 C24 P2 109.3(15) . .
C34 C24 P2 108.3(16) . .
C92 C24 P2 108.4(16) . .
P3 O14 Co4 132(2) . .
P3 O14 Dy3 93.2(16) . .
Co4 O14 Dy3 112.2(18) . .
P3' O14' Co4 125(3) . .
P3' O14' Dy3 101(2) . .
Co4 O14' Dy3 108.7(18) . .
C59 O16 Dy3 156.8(16) . .
C100 C27 H27A 109.5 . .
C100 C27 H27B 109.5 . .
H27A C27 H27B 109.5 . .
C100 C27 H27C 109.5 . .
H27A C27 H27C 109.5 . .
H27B C27 H27C 109.5 . .
C53' O11 C53 12(3) . .
C53' O11 Dy2 131(3) . .
C53 O11 Dy2 141(2) . .
C74 C29 C61 112(3) . .
C74 C29 C46 112(3) . .
C61 C29 C46 107(2) . .
C74 C29 C71 112(2) . .
C61 C29 C71 107(3) . .
C46 C29 C71 106(2) . .
C59 O17 Co4 118.6(16) . .
C24 C34 H34A 109.5 . .
C24 C34 H34B 109.5 . .
H34A C34 H34B 109.5 . .
C24 C34 H34C 109.5 . .
H34A C34 H34C 109.5 . .
H34B C34 H34C 109.5 . .
C63 O19 Dy3 138.0(14) . .
C63 O18 Dy4 118(2) . .
C63 O18' Dy4' 137(3) . .
C21 C38 H38A 109.5 . .
C21 C38 H38B 109.5 . .
H38A C38 H38B 109.5 . .
C21 C38 H38C 109.5 . .
H38A C38 H38C 109.5 . .
H38B C38 H38C 109.5 . .
C42 O15 C42' 10(4) . .
C42 O15 Co4 116(3) . .
C42' O15 Co4 110(3) . .
C21 C47 H47A 109.5 . .
C21 C47 H47B 109.5 . .
H47A C47 H47B 109.5 . .
C21 C47 H47C 109.5 . .
H47A C47 H47C 109.5 . .
H47B C47 H47C 109.5 . .
C29 C46 H46A 109.5 . .
C29 C46 H46B 109.5 . .
H46A C46 H46B 109.5 . .
C29 C46 H46C 109.5 . .
H46A C46 H46C 109.5 . .
H46B C46 H46C 109.5 . .
C71 O12 Co2 118(3) . .
C71 O12' Co2 124(5) . .
O10 C53 O11 113.3(18) . .
O10 C53 C100 123.3(16) . .
O11 C53 C100 123.3(19) . .
O10 C53' O11 137(4) . .
O10 C53' C100 112(2) . .
O11 C53' C100 111(2) . .
C60 C54 H54A 109.5 . .
C60 C54 H54B 109.5 . .
H54A C54 H54B 109.5 . .
C60 C54 H54C 109.5 . .
H54A C54 H54C 109.5 . .
H54B C54 H54C 109.5 . .
C60 C58 H58A 109.5 . .
C60 C58 H58B 109.5 . .
H58A C58 H58B 109.5 . .
C60 C58 H58C 109.5 . .
H58A C58 H58C 109.5 . .
H58B C58 H58C 109.5 . .
O17 C59 O16 125(2) . .
O17 C59 C127 118.7(18) . .
O16 C59 C127 115.8(18) . .
C54 C60 C62 110(3) . .
C54 C60 C58 111(2) . .
C62 C60 C58 111(3) . .
C54 C60 P3' 105(2) . .
C62 C60 P3' 106.0(17) . .
C58 C60 P3' 114(2) . .
C54 C60 P3 116(2) . .
C62 C60 P3 108.8(18) . .
C58 C60 P3 101(2) . .
P3' C60 P3 14.0(11) . .
C29 C61 H61A 109.5 . .
C29 C61 H61B 109.5 . .
H61A C61 H61B 109.5 . .
C29 C61 H61C 109.5 . .
H61A C61 H61C 109.5 . .
H61B C61 H61C 109.5 . .
C60 C62 H62A 109.5 . .
C60 C62 H62B 109.5 . .
H62A C62 H62B 109.5 . .
C60 C62 H62C 109.5 . .
H62A C62 H62C 109.5 . .
H62B C62 H62C 109.5 . .
O18' C63 O19 110(3) . .
O18' C63 O18 35(2) . .
O19 C63 O18 129(2) . .
O18' C63 C97 129(3) . .
O19 C63 C97 117(2) . .
O18 C63 C97 112(2) . .
O12' C71 O13 125(5) . .
O12' C71 O12 12(6) . .
O13 C71 O12 125(3) . .
O12' C71 C29 120(5) . .
O13 C71 C29 113(3) . .
O12 C71 C29 122(3) . .
C29 C74 H74A 109.5 . .
C29 C74 H74B 109.5 . .
H74A C74 H74B 109.5 . .
C29 C74 H74C 109.5 . .
H74A C74 H74C 109.5 . .
H74B C74 H74C 109.5 . .
C97 C82 H82A 109.5 . .
C97 C82 H82B 109.5 . .
H82A C82 H82B 109.5 . .
C97 C82 H82C 109.5 . .
H82A C82 H82C 109.5 . .
H82B C82 H82C 109.5 . .
C97 C87 H87A 109.5 . .
C97 C87 H87B 109.5 . .
H87A C87 H87B 109.5 . .
C97 C87 H87C 109.5 . .
H87A C87 H87C 109.5 . .
H87B C87 H87C 109.5 . .
C45 C48 H48A 109.5 . .
C45 C48 H48B 109.5 . .
H48A C48 H48B 109.5 . .
C45 C48 H48C 109.5 . .
H48A C48 H48C 109.5 . .
H48B C48 H48C 109.5 . .
C24 C92 H92A 109.5 . .
C24 C92 H92B 109.5 . .
H92A C92 H92B 109.5 . .
C24 C92 H92C 109.5 . .
H92A C92 H92C 109.5 . .
H92B C92 H92C 109.5 . .
C100 C93 H93A 109.5 . .
C100 C93 H93B 109.5 . .
H93A C93 H93B 109.5 . .
C100 C93 H93C 109.5 . .
H93A C93 H93C 109.5 . .
H93B C93 H93C 109.5 . .
C97 C95 H95A 109.5 . .
C97 C95 H95B 109.5 . .
H95A C95 H95B 109.5 . .
C97 C95 H95C 109.5 . .
H95A C95 H95C 109.5 . .
H95B C95 H95C 109.5 . .
C87 C97 C95 112(2) . .
C87 C97 C82 109(2) . .
C95 C97 C82 111(2) . .
C87 C97 C63 110(2) . .
C95 C97 C63 110(2) . .
C82 C97 C63 104.5(19) . .
C53 C100 C27 112(2) . .
C53 C100 C93 113(2) . .
C27 C100 C93 114(2) . .
C53 C100 C150 103(4) . .
C27 C100 C150 107(2) . .
C93 C100 C150 107(2) . .
C53 C100 C53' 1(7) . .
C27 C100 C53' 112(2) . .
C93 C100 C53' 113(2) . .
C150 C100 C53' 102(4) . .
C21 C103 H10A 109.5 . .
C21 C103 H10B 109.5 . .
H10A C103 H10B 109.5 . .
C21 C103 H10C 109.5 . .
H10A C103 H10C 109.5 . .
H10B C103 H10C 109.5 . .
O24 C50 O20' 124(3) . .
O24 C50 O20 125(3) . .
O20' C50 O20 38(2) . .
O24 C50 O24' 41(2) . .
O20' C50 O24' 100(3) . .
O20 C50 O24' 129(3) . .
O24 C50 C45 111.1(17) . .
O20' C50 C45 125(2) . .
O20 C50 C45 111(2) . .
O24' C50 C45 120(2) . .
C24 C146 H14A 109.5 . .
C24 C146 H14B 109.5 . .
H14A C146 H14B 109.5 . .
C24 C146 H14C 109.5 . .
H14A C146 H14C 109.5 . .
H14B C146 H14C 109.5 . .
C100 C150 H15A 109.5 . .
C100 C150 H15B 109.5 . .
H15A C150 H15B 109.5 . .
C100 C150 H15C 109.5 . .
H15A C150 H15C 109.5 . .
H15B C150 H15C 109.5 . .
C75 O25 Dy1 163(2) . .
C75 O25 Dy2 96.9(15) . .
Dy1 O25 Dy2 98.1(12) . .
C75 O26 Dy2 99.9(15) . .
O25 C75 O26 115.7(13) . .
O25 C75 C4 122(2) . .
O26 C75 C4 120(2) . .
C75 C4 C37 108.1(16) . .
C75 C4 C77 107.8(16) . .
C37 C4 C77 111.2(16) . .
C75 C4 C36 107.7(16) . .
C37 C4 C36 110.9(16) . .
C77 C4 C36 110.9(16) . .
C4 C36 H36A 109.5 . .
C4 C36 H36B 109.5 . .
H36A C36 H36B 109.5 . .
C4 C36 H36C 109.5 . .
H36A C36 H36C 109.5 . .
H36B C36 H36C 109.5 . .
C4 C37 H37A 109.5 . .
C4 C37 H37B 109.5 . .
H37A C37 H37B 109.5 . .
C4 C37 H37C 109.5 . .
H37A C37 H37C 109.5 . .
H37B C37 H37C 109.5 . .
C4 C77 H77A 109.5 . .
C4 C77 H77B 109.5 . .
H77A C77 H77B 109.5 . .
C4 C77 H77C 109.5 . .
H77A C77 H77C 109.5 . .
H77B C77 H77C 109.5 . .
C75' O25' Dy2 92(3) . .
C75' O25' Dy1 142(2) . .
Dy2 O25' Dy1 103.9(14) . .
C75' O26' Dy2 91(2) . .
O25' C75' O26' 116(4) . .
O25' C75' C4' 133(3) . .
O26' C75' C4' 108(3) . .
O25' C75' Dy2 59(2) . .
O26' C75' Dy2 60(2) . .
C4' C75' Dy2 167.1(17) . .
C36' C4' C37' 115.4(16) . .
C36' C4' C77' 115.4(16) . .
C37' C4' C77' 115.3(16) . .
C36' C4' C75' 103(2) . .
C37' C4' C75' 103(2) . .
C77' C4' C75' 103(2) . .
C4' C77' H77D 109.5 . .
C4' C77' H77E 109.5 . .
H77D C77' H77E 109.5 . .
C4' C77' H77F 109.5 . .
H77D C77' H77F 109.5 . .
H77E C77' H77F 109.5 . .
C4' C37' H37D 109.5 . .
C4' C37' H37E 109.5 . .
H37D C37' H37E 109.5 . .
C4' C37' H37F 109.5 . .
H37D C37' H37F 109.5 . .
H37E C37' H37F 109.5 . .
C4' C36' H36D 109.5 . .
C4' C36' H36E 109.5 . .
H36D C36' H36E 109.5 . .
C4' C36' H36F 109.5 . .
H36D C36' H36F 109.5 . .
H36E C36' H36F 109.5 . .
C3 C127 C39 111.2(18) . .
C3 C127 C2 110.8(18) . .
C39 C127 C2 110.6(18) . .
C3 C127 C59 108.1(17) . .
C39 C127 C59 108(2) . .
C2 C127 C59 107.6(18) . .
C127 C39 H39A 109.5 . .
C127 C39 H39B 109.5 . .
H39A C39 H39B 109.5 . .
C127 C39 H39C 109.5 . .
H39A C39 H39C 109.5 . .
H39B C39 H39C 109.5 . .
C127 C2 H2A 109.5 . .
C127 C2 H2B 109.5 . .
H2A C2 H2B 109.5 . .
C127 C2 H2C 109.5 . .
H2A C2 H2C 109.5 . .
H2B C2 H2C 109.5 . .
C127 C3 H3A 109.5 . .
C127 C3 H3B 109.5 . .
H3A C3 H3B 109.5 . .
C127 C3 H3C 109.5 . .
H3A C3 H3C 109.5 . .
H3B C3 H3C 109.5 . .
H2D C2' H2E 109.5 . .
H2D C2' H2F 109.5 . .
H2E C2' H2F 109.5 . .
H39D C39' H39E 109.5 . .
H39D C39' H39F 109.5 . .
H39E C39' H39F 109.5 . .
C45 C44 H44A 109.5 . .
C45 C44 H44B 109.5 . .
H44A C44 H44B 109.5 . .
C45 C44 H44C 109.5 . .
H44A C44 H44C 109.5 . .
H44B C44 H44C 109.5 . .
C48 C45 C44 110.5(15) . .
C48 C45 C43 109.6(15) . .
C44 C45 C43 109.7(14) . .
C48 C45 C50 109.0(14) . .
C44 C45 C50 108.8(15) . .
C43 C45 C50 109.2(14) . .
C45 C43 H43A 109.5 . .
C45 C43 H43B 109.5 . .
H43A C43 H43B 109.5 . .
C45 C43 H43C 109.5 . .
H43A C43 H43C 109.5 . .
H43B C43 H43C 109.5 . .
O33 N1 O32 118(3) . .
O33 N1 O31 121(3) . .
O32 N1 O31 121(3) . .
O33 N1 O30 120(3) . 2_656
O32 N1 O30 119(3) . 2_656
O31 N1 O30 21.8(19) . 2_656
O30 O31 N1 113(6) 2_656 .
O30 O31 N2 28(4) 2_656 2_656
N1 O31 N2 89(3) . 2_656
N1 O32 Co3 124(2) . .
N1 O32 Co1 84.9(18) . .
Co3 O32 Co1 151.4(13) . .
N1 O33 Co1 98(2) . .
O30 N2 O29 124(4) . .
O30 N2 O28 117(4) . .
O29 N2 O28 119(3) . .
O30 N2 O31 15(2) . 2_656
O29 N2 O31 112(3) . 2_656
O28 N2 O31 129(3) . 2_656
N2 O28 Co3 96(2) . .
O29 O29 N2 147(5) 2_656 .
O29 O29 Co3 85(3) 2_656 2_656
N2 O29 Co3 125(2) . 2_656
O29 O29 Co3 67(3) 2_656 .
N2 O29 Co3 84(2) . .
Co3 O29 Co3 150.7(11) 2_656 .
O31 O30 N2 137(6) 2_656 .
O31 O30 N1 45(4) 2_656 2_656
N2 O30 N1 97(3) . 2_656
O31' N1' O33' 114(3) . .
O31' N1' O32' 128(4) . .
O33' N1' O32' 117(3) . .
O31' N1' O30' 13(2) . 2_656
O33' N1' O30' 124(3) . 2_656
O32' N1' O30' 118(3) . 2_656
O30' O31' N1' 143(6) 2_656 .
O30' O31' N2' 53(5) 2_656 2_656
N1' O31' N2' 93(3) . 2_656
N1' O32' Co1 123(2) . .
N1' O32' Co3 85.1(19) . .
Co1 O32' Co3 151.8(12) . .
N1' O33' Co3 98(2) . .
O29' N2' O28' 116(3) . .
O29' N2' O30' 118(3) . .
O28' N2' O30' 124(3) . .
O29' N2' O31' 123(3) . 2_656
O28' N2' O31' 119(3) . 2_656
O30' N2' O31' 24.2(17) . 2_656
O28' O28' N2' 139(4) 2_656 .
O28' O28' Co1 93(3) 2_656 2_656
N2' O28' Co1 125(2) . 2_656
N2' O29' Co1 101(2) . .
O31' O30' N2' 103(6) 2_656 .
O31' O30' N1' 24(4) 2_656 2_656
N2' O30' N1' 81(2) . 2_656
C42 O8 Dy2 146(4) . .
O15 C42 O8 113(5) . .
O15 C42 C32 122(3) . .
O8 C42 C32 122(3) . .
C42 C32 C51 108(3) . .
C42 C32 C41 109(2) . .
C51 C32 C41 111(2) . .
C42 C32 C40 108(2) . .
C51 C32 C40 109(2) . .
C41 C32 C40 110(2) . .
C32 C51 H51A 109.5 . .
C32 C51 H51B 109.5 . .
H51A C51 H51B 109.5 . .
C32 C51 H51C 109.5 . .
H51A C51 H51C 109.5 . .
H51B C51 H51C 109.5 . .
C32 C40 H40A 109.5 . .
C32 C40 H40B 109.5 . .
H40A C40 H40B 109.5 . .
C32 C40 H40C 109.5 . .
H40A C40 H40C 109.5 . .
H40B C40 H40C 109.5 . .
C32 C41 H41A 109.5 . .
C32 C41 H41B 109.5 . .
H41A C41 H41B 109.5 . .
C32 C41 H41C 109.5 . .
H41A C41 H41C 109.5 . .
H41B C41 H41C 109.5 . .
C42' O8' Dy2 159(5) . .
C32' C51' H51D 109.5 . .
C32' C51' H51E 109.5 . .
H51D C51' H51E 109.5 . .
C32' C51' H51F 109.5 . .
H51D C51' H51F 109.5 . .
H51E C51' H51F 109.5 . .
C51' C32' C40' 106(3) . .
C51' C32' C42' 111(3) . .
C40' C32' C42' 112(3) . .
C32' C40' H40D 109.5 . .
C32' C40' H40E 109.5 . .
H40D C40' H40E 109.5 . .
C32' C40' H40F 109.5 . .
H40D C40' H40F 109.5 . .
H40E C40' H40F 109.5 . .
O8' C42' O15 127(6) . .
O8' C42' C32' 113(5) . .
O15 C42' C32' 120(3) . .
loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
Dy1 O25 2.15(2) .
Dy1 O6 2.220(11) 2_656
Dy1 O13 2.253(16) .
Dy1 O10 2.258(14) .
Dy1 O3 2.345(13) .
Dy1 O2 2.386(11) .
Dy1 O25' 2.46(3) .
Dy1 O4 2.462(13) .
Dy1 P1 3.057(5) .
Dy1 Dy2 3.7596(15) .
Dy2 O8' 2.14(4) .
Dy2 O7 2.229(18) .
Dy2 O11 2.260(12) .
Dy2 O25' 2.31(4) .
Dy2 O26' 2.32(4) .
Dy2 O3 2.352(11) .
Dy2 O5 2.395(12) .
Dy2 O8 2.41(3) .
Dy2 O45 2.449(12) .
Dy2 C75' 2.68(4) .
Dy2 O26 2.73(4) .
Dy2 O25 2.79(4) .
Dy3 O22 2.06(2) .
Dy3 O9 2.214(14) .
Dy3 O16 2.252(17) .
Dy3 O19 2.282(15) .
Dy3 O14' 2.28(4) .
Dy3 O34' 2.37(4) .
Dy3 O34 2.37(2) .
Dy3 O46 2.379(11) .
Dy3 O38' 2.40(3) .
Dy3 O14 2.66(3) .
Dy3 C81' 2.75(3) .
Dy3 O22' 2.78(4) .
Dy4 O18 2.29(3) .
Dy4 O20 2.31(2) .
Dy4 O38 2.32(2) .
Dy4 O23 2.35(2) .
Dy4 O34 2.37(2) .
Dy4 O22 2.43(3) .
Dy4 O21 2.55(2) .
Dy4 C81 2.84(2) .
Dy4 P4 3.068(9) .
Dy4 Co3 3.468(3) .
O34 Co3 2.228(4) .
O34 H34D 1.0000 .
C81 O22 1.287(10) .
C81 O38 1.311(10) .
C81 C90 1.515(9) .
C90 C91 1.511(13) .
C90 C85 1.513(9) .
C90 C88 1.517(13) .
C88 H88A 0.9800 .
C88 H88B 0.9800 .
C88 H88C 0.9800 .
C85 H85A 0.9800 .
C85 H85B 0.9800 .
C85 H85C 0.9800 .
C91 H91A 0.9800 .
C91 H91B 0.9800 .
C91 H91C 0.9800 .
O24 C50 1.256(19) .
O24 Co5 2.18(2) .
P4 O23 1.56(3) .
P4 O36 1.55(3) .
P4 O21 1.61(2) .
P4 C55 1.84(4) .
O23 Co3 2.05(3) .
O21 Co5 2.19(2) .
C55 C56 1.52(2) .
C55 C57 1.52(2) .
C55 C80 1.52(2) .
C80 H80D 0.9800 .
C80 H80E 0.9800 .
C80 H80F 0.9800 .
C57 H57D 0.9800 .
C57 H57E 0.9800 .
C57 H57F 0.9800 .
C56 H56D 0.9800 .
C56 H56E 0.9800 .
C56 H56F 0.9800 .
O20 C50 1.305(19) .
Dy4' O36' 1.33(3) 2_656
Dy4' O20' 2.13(2) .
Dy4' O22' 2.37(3) .
Dy4' O34' 2.42(3) .
Dy4' O21' 2.43(3) .
Dy4' O23' 2.43(3) .
Dy4' O18' 2.59(3) .
Dy4' P4' 2.726(16) 2_656
Dy4' P4' 3.069(12) .
Dy4' Co5 3.396(4) .
O34' Co3 1.96(2) .
O34' H34E 1.0000 .
C81' O22' 1.292(10) .
C81' O38' 1.295(11) .
C81' C90' 1.504(10) .
C90' C85' 1.508(10) .
C90' C91' 1.508(13) .
C90' C88' 1.511(14) .
C91' H91D 0.9800 .
C91' H91E 0.9800 .
C91' H91F 0.9800 .
C85' H85D 0.9800 .
C85' H85E 0.9800 .
C85' H85F 0.9800 .
C88' H88D 0.9800 .
C88' H88E 0.9800 .
C88' H88F 0.9800 .
P4' O21' 1.51(3) .
P4' O23' 1.55(3) .
P4' O36' 1.59(3) .
P4' C55' 1.81(4) .
P4' Dy4' 2.726(16) 2_656
O23' Co3 2.12(3) .
O36' Dy4' 1.33(3) 2_656
O21' Co5 1.70(3) .
C55' C57' 1.56(3) .
C55' C56' 1.56(3) .
C55' C80' 1.56(3) .
C56' H56A 0.9800 .
C56' H56B 0.9800 .
C56' H56C 0.9800 .
C57' H57A 0.9800 .
C57' H57B 0.9800 .
C57' H57C 0.9800 .
C80' H80A 0.9800 .
C80' H80B 0.9800 .
C80' H80C 0.9800 .
O24' C50 1.32(2) .
O24' Co5 1.94(3) .
O20' C50 1.277(19) .
Co1 O28' 2.05(3) 2_656
Co1 O2 2.052(12) .
Co1 O33 2.06(2) .
Co1 O29' 2.07(3) .
Co1 O3 2.068(11) .
Co1 O5 2.077(12) .
Co1 O32' 2.09(2) .
Co1 O32 2.33(2) .
Co2 O12 1.84(5) 2_656
Co2 O12 1.84(5) .
Co2 O4 1.993(12) .
Co2 O4 1.993(12) 2_656
Co2 O12' 2.05(6) .
Co2 O12' 2.05(6) 2_656
Co3 O28 2.05(3) .
Co3 O46 2.059(15) .
Co3 O33' 2.08(3) .
Co3 O32 2.09(2) .
Co3 O29 2.13(3) 2_656
Co3 O29 2.31(3) .
Co3 O32' 2.33(2) .
Co4 O14 1.77(4) .
Co4 O17 1.937(15) .
Co4 O15 1.989(19) .
Co4 O45 2.010(15) .
Co4 O14' 2.28(4) .
Co5 O21' 1.70(3) 2_656
Co5 O24' 1.94(3) 2_656
Co5 O24 2.18(2) 2_656
Co5 O21 2.19(2) 2_656
Co5 Dy4' 3.396(4) 2_656
P1 O6 1.500(12) .
P1 O2 1.542(12) .
P1 O4 1.541(13) .
P1 C21 1.814(17) .
P2 O9 1.523(15) .
P2 O5 1.526(12) .
P2 O45 1.543(14) .
P2 C24 1.83(2) .
P3 O7 1.35(2) .
P3 O14 1.60(4) .
P3 O46 1.74(3) .
P3 C60 1.87(3) .
P3' O46 1.34(2) .
P3' O14' 1.47(4) .
P3' O7 1.68(3) .
P3' C60 1.82(3) .
O3 H3D 1.0000 .
O6 Dy1 2.220(11) 2_656
O10 C53' 1.20(2) .
O10 C53 1.345(10) .
C21 C38 1.51(3) .
C21 C47 1.52(3) .
C21 C103 1.53(3) .
O13 C71 1.28(3) .
C24 C146 1.50(3) .
C24 C34 1.51(3) .
C24 C92 1.53(3) .
O16 C59 1.259(18) .
C27 C100 1.48(3) .
C27 H27A 0.9800 .
C27 H27B 0.9800 .
C27 H27C 0.9800 .
O11 C53' 1.21(2) .
O11 C53 1.347(10) .
C29 C74 1.48(4) .
C29 C61 1.49(4) .
C29 C46 1.53(3) .
C29 C71 1.58(4) .
O17 C59 1.246(18) .
C34 H34A 0.9800 .
C34 H34B 0.9800 .
C34 H34C 0.9800 .
O19 C63 1.27(3) .
O18 C63 1.43(4) .
O18' C63 1.12(4) .
C38 H38A 0.9800 .
C38 H38B 0.9800 .
C38 H38C 0.9800 .
O15 C42 1.22(3) .
O15 C42' 1.35(7) .
C47 H47A 0.9800 .
C47 H47B 0.9800 .
C47 H47C 0.9800 .
C46 H46A 0.9800 .
C46 H46B 0.9800 .
C46 H46C 0.9800 .
O12 C71 1.34(5) .
O12' C71 0.99(6) .
C53 C100 1.39(3) .
C53' C100 1.69(5) .
C54 C60 1.46(4) .
C54 H54A 0.9800 .
C54 H54B 0.9800 .
C54 H54C 0.9800 .
C58 C60 1.55(4) .
C58 H58A 0.9800 .
C58 H58B 0.9800 .
C58 H58C 0.9800 .
C59 C127 1.53(3) .
C60 C62 1.54(3) .
C61 H61A 0.9800 .
C61 H61B 0.9800 .
C61 H61C 0.9800 .
C62 H62A 0.9800 .
C62 H62B 0.9800 .
C62 H62C 0.9800 .
C63 C97 1.54(3) .
C74 H74A 0.9800 .
C74 H74B 0.9800 .
C74 H74C 0.9800 .
C82 C97 1.53(3) .
C82 H82A 0.9800 .
C82 H82B 0.9800 .
C82 H82C 0.9800 .
C87 C97 1.51(3) .
C87 H87A 0.9800 .
C87 H87B 0.9800 .
C87 H87C 0.9800 .
C48 C45 1.48(2) .
C48 H48A 0.9800 .
C48 H48B 0.9800 .
C48 H48C 0.9800 .
C92 H92A 0.9800 .
C92 H92B 0.9800 .
C92 H92C 0.9800 .
C93 C100 1.50(3) .
C93 H93A 0.9800 .
C93 H93B 0.9800 .
C93 H93C 0.9800 .
C95 C97 1.51(3) .
C95 H95A 0.9800 .
C95 H95B 0.9800 .
C95 H95C 0.9800 .
C100 C150 1.59(3) .
C103 H10A 0.9800 .
C103 H10B 0.9800 .
C103 H10C 0.9800 .
C50 C45 1.53(3) .
C146 H14A 0.9800 .
C146 H14B 0.9800 .
C146 H14C 0.9800 .
C150 H15A 0.9800 .
C150 H15B 0.9800 .
C150 H15C 0.9800 .
O25 C75 1.294(9) .
O26 C75 1.298(9) .
C75 C4 1.499(11) .
C4 C37 1.52(3) .
C4 C77 1.52(3) .
C4 C36 1.52(3) .
C36 H36A 0.9800 .
C36 H36B 0.9800 .
C36 H36C 0.9800 .
C37 H37A 0.9800 .
C37 H37B 0.9800 .
C37 H37C 0.9800 .
C77 H77A 0.9800 .
C77 H77B 0.9800 .
C77 H77C 0.9800 .
O25' C75' 1.292(11) .
O26' C75' 1.301(11) .
C75' C4' 1.498(11) .
C4' C36' 1.42(3) .
C4' C37' 1.42(3) .
C4' C77' 1.42(3) .
C77' H77D 0.9800 .
C77' H77E 0.9800 .
C77' H77F 0.9800 .
C37' H37D 0.9800 .
C37' H37E 0.9800 .
C37' H37F 0.9800 .
C36' H36D 0.9800 .
C36' H36E 0.9800 .
C36' H36F 0.9800 .
C127 C3 1.49(2) .
C127 C39 1.498(10) .
C127 C2 1.50(2) .
C39 H39A 0.9800 .
C39 H39B 0.9800 .
C39 H39C 0.9800 .
C2 H2A 0.9800 .
C2 H2B 0.9800 .
C2 H2C 0.9800 .
C3 H3A 0.9800 .
C3 H3B 0.9800 .
C3 H3C 0.9800 .
C2' H2D 0.9800 .
C2' H2E 0.9800 .
C2' H2F 0.9800 .
C39' H39D 0.9800 .
C39' H39E 0.9800 .
C39' H39F 0.9800 .
C44 C45 1.48(2) .
C44 H44A 0.9800 .
C44 H44B 0.9800 .
C44 H44C 0.9800 .
C45 C43 1.49(2) .
C43 H43A 0.9800 .
C43 H43B 0.9800 .
C43 H43C 0.9800 .
N1 O33 1.25(4) .
N1 O32 1.28(4) .
N1 O31 1.30(4) .
N1 O30 1.68(4) 2_656
O31 O30 0.68(4) 2_656
O31 N2 1.81(5) 2_656
N2 O30 1.25(4) .
N2 O29 1.29(4) .
N2 O28 1.29(5) .
N2 O31 1.81(5) 2_656
O29 O29 1.10(4) 2_656
O29 Co3 2.13(3) 2_656
O30 O31 0.68(4) 2_656
O30 N1 1.68(4) 2_656
N1' O31' 1.20(4) .
N1' O33' 1.26(4) .
N1' O32' 1.31(4) .
N1' O30' 1.78(4) 2_656
O31' O30' 0.68(3) 2_656
O31' N2' 1.61(4) 2_656
N2' O29' 1.28(4) .
N2' O28' 1.31(4) .
N2' O30' 1.32(4) .
N2' O31' 1.61(4) 2_656
O28' O28' 1.17(4) 2_656
O28' Co1 2.05(2) 2_656
O30' O31' 0.68(3) 2_656
O30' N1' 1.78(4) 2_656
O8 C42 1.22(3) .
C42 C32 1.49(8) .
C32 C51 1.502(10) .
C32 C41 1.51(2) .
C32 C40 1.52(2) .
C51 H51A 0.9800 .
C51 H51B 0.9800 .
C51 H51C 0.9800 .
C40 H40A 0.9800 .
C40 H40B 0.9800 .
C40 H40C 0.9800 .
C41 H41A 0.9800 .
C41 H41B 0.9800 .
C41 H41C 0.9800 .
O8' C42' 1.22(3) .
C51' C32' 1.497(10) .
C51' H51D 0.9800 .
C51' H51E 0.9800 .
C51' H51F 0.9800 .
C32' C40' 1.50(2) .
C32' C42' 1.55(9) .
C40' H40D 0.9800 .
C40' H40E 0.9800 .
C40' H40F 0.9800 .
